ERT - COMPOSITIONAL ANALYSES OF SAMPLES · 2020. 11. 30. · OF SAMPLES COLLECTED BY ERT. 000332 FIELD DATA SHEET Environmental Response Team, Environmental Protection Agency Woodbrldge

000331

EPA Region 5 Records Ctr

231015

ATTACHMENT C

COMPOSITIONAL ANALYSESOF SAMPLES COLLECTED BY ERT

000332

FIELD DATA SHEETEnvironmental Response Team, Environmental Protection Agency

Woodbrldge Avt., Edison, N J. 08837(201) 321-6680

Lab Number (Consec.ft's) Oat* Collected Tim* (24 hr)

NO 561 Mo1DayI

Yr ,.1''-

c/

SOIL LAND VEGETATION GROUNDWATER

DeviceAugerCoraSplit Spoon

Spade

DepthFtorIn.

Soil TypeRockGravelSandClaySiltMuckLoamPeat

Color

Upland-DryLowland-DryFloodplalnWetlandGully

Slope >15"

Old Field ResidentialWooded IndustrialFarmland Commercial

HerbaceousShrubsTrees

DBH

Water Table Depth

Sample Depth Ft

Color .Odor. .Oil:Device:.

SURFACE WATER SAMPLE PREPARATION

Color.Odor .

Temp.PH

STREAM Width

Depth

Velocity

OW DIRECTION.

Ft.

FtorIn.

Ft/Sec

Pools. .% Riffles.

DeviceKemmererPetersenSurberManualNetSeineTrowlBucket

SurfaceClean

OHGarbage

TrashBubbles

OeadFtshSewage

Ind. WasteFloat Solids

Bottom %OozeSandGravelClayRubbleRockShellOrganic

Glass JarPlastic JarMetalAcetate CorePaper CapTeflon CapFoil Cap

StorageWet IceAmbientDry Ice

Low eiHlgh ContinuationDetergent WaanWater Rlnee jAcetone RinseHexane RinseOther Solvent RinseSpecify:

TRANSECT INFORMATION

Letter Station*

-£-

Compass Direction Distance Between Stations

is Ft

Remarks and Site Description

000333

INTERNATIONALTECHNOLOGYCORPORATION

Enviresponse, IncGSA Raritan Depot, Woodbridge Ave,Building 209, Bay FEdison, N. J. 08837Attn. of: Ms. Janet CullinaneN. J. Lab Certification ID# 12064

Job # 5702Date:Auth:Lot #: 0485Invoice #:Sample Date: 5/21/86

Sample #55914A-05614,Liquid

(ppm)

E. P. ToxicityLeachate(mg/L)

EPAMaximumLeachateConcentration(mg/L)

Cyanide

C^Flash Point (°F)

OQ03&4S ANALYSIS DATA SHEET SAMPLE tt: B05614

IT/CERR36989EB2

LABORATORY:LABORATORY ID:MATRIX:

DATA RELEASE AUTHORIZED BY:

CASE #/SAS #: IT-PAS-12OC REPORT #: P/QI-33CONTRACT *: IT-PAS-59999^-°5 ~c>7

ATE RECEIVED:

VOLATILE COMPOUNDS

ALL SOLID RESULTS REPORTED ON A DRY WEIGHT BASIS

PP # CAS *

45V46V88V16V44V13H15H29V13V30V23V,0VT4H11V6V19H48V32V33VT87V51V14V4V33VC19V47V16H17H85V15V86V7V38V'18H20H

74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5108-05-475-27-478-87-5

10061-02-679-01-6124-48-179-00-571-43-2

10061-01-5110-75-875-25-2519-78-6108-10-1127-18-479-34-5108-88-3108-90-7100-41-4100-42-595-47-6

LEVEL:DATE EXT/PREP:DATE ANALYZED:SPL—>EXTRACT:PH:•/. MOISTURE (NOT DEC. ):V. MOISTURE (DEC. >:STANDARD ID:SENSITIVITY ID:UNITS:

MED06/12/8606/12/864. 005G+10MLMEOH

MSVEB124BFBEB097UG/KG

# - USED FOR DRY WEIGHT CALCULATION

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDEACETONECARBON DISULFIDE1*1-DICHLOROETHENEli1-DICHLOROETHANETRANS-1, 2-DICHLOROETHENECHLOROFORM1.2-DICHLOROETHANE2-BUTANONE1*1.1-TRICHLOROETHANECARBON TETRACHLORIDEVINYL ACETATEBROMODICHLOROMETHANE1*2-DICHLOROPROPANETRANS-I,3-DICHLOROPROPENETRICHLOROETHENECHLORODIBROMOMETHANE1.1.2-TRICHLOROETHANEBENZENECIS-1,3-DICHLOROPROPENE2-CHLOROETHYLVINYL ETHERBROMOFORM2-HEXANONE4-METHYL-2-PENTANONETETRACHLOROETHENE1> 1,2, 2-TETRACHLOROETHANETOLUENECHLOROBENZENEETHYLBENZENESTYRENETOTAL XYLENES

CONC• ====

2000QOCO a20000CCD U

20000. 000 \J800COOO

3200043008000.0000

8000 £tfo ^8000.00?^BOOOQOO V

eooo.ocoiy

20000£00 \)8000500^

BQQQOOO '

BOOOQOO V

20000COD (JBOOOOCO V

20000000^

8000000 0BOOOCGO U

200000C7080000 OOJ

7300CCOO

240000^

000335

ORGANICS ANALYSIS DATA SHEET

IT/CERR36989CJ10



SAMPLE ft: B05614

IT/PAS-12CASE #/SAS ft:QC REPORT ft:CONTRACT ft:DATE RECEIVED: 05/22/86A

~A ,

SEMIVOLATILE COMPOUNDS (PAGE 1)


LEVEL:DATE EXT/PREP:DATE ANALYZED:SPL-->EXTRACT:PH:% MOISTURE (NOT DEC. )% MOISTURE (DEC. ):STANDARD ID:SENSITIVITY ID:UNITS:

MEDIUM GPC05/28/86 SEP. FUNNEL06/10/86 CONT. EXT.1. OOG: 10ML — SOUL: 1ML

,M/A-0. 00

NSW—BDCEJ122DFTEJ111UG/KG-

* - USED FOR DRY WEIGHT CALCULATION

PP CAS *

65A18B24A26B27B6H25B2H42B

*3H&3B12B56B54B57A34A1H

43B31ASB55B7H52B22A9H53B21A4H20B10H71B77B

108-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-7

39638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-33-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3208-96-8

PHENOLBIS (2-CHLOROETHYL) ETHER2-CHLOROPHENOLli3-DXCHLOROBENZENEii 4-DICHLOROBENZENEBENZYL ALCOHOL1,2-DICHLOROBENZENE2-KETHYLPHENOLBIS (2-CHLOROISOPROPYL> ETHER4-METHYLPHENOLN-NITROSO-DI-N-PROPLYAMINEHEXACHLOROETHANENITROBENZENEISOPHORONES-NITROPHENOL2,4-DIMETHYLPHENQLBENZOIC ACIDBIS (2-CHLOROETHOXY) METHANE2,4-DICHLOROPHENDL1,2,4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2-METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2,4,6-TRICHLOROPHENOL2,4,5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINEDIMETHYLPHTHALATEACENAPHTHALENE

Y.y'mY

N'

CONC==z =

200000 O.U200000C.U200ooo:.u

200000C.U200000C.U200000CU200000D.U200000C.U200000CU200000C.U2000000. U2000005.U200000£.U2000005.U200000̂ U1000000GU200000CU200000 CU200000CU200000; u

200000 au2000003 U2000000.U200000I).U200000 aulOOOOOOfiU200000f.U1000000!?U200000t'U200000.'.U

OOO336

ORGANICS ANALYSIS DATA SHEET

LABORATORY: IT/CERRLABORATORY ID. 36989CJ10MATRIX: SOIL

SAMPLE »: B05614

IT/PAS-12CASE #/SAS #:QC REPORT *:CONTRACT #: IT/PAS-DATE RECEIVED: 05/22/86




LEVEL:DATE EXT/PREP.DATE ANALYZED:SPL—>EXTRACT:PH:% MOISTURE (NOT DEC. >% MOISTURE (DEC.):STANDARD ID:SENSITIVITY ID:UNITS:

MEDIUM GPC Y05/28/86 SEP. FUNNEL Y.06/10/86 CONT. EXT. Y1.OOG:10ML--50UL:1ML

-NSW- jvi/BDCEJ122DFTEJ111UG/KG-


PP # CAS #

3-NITROANILINEACENAPHTHENE2,4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2/4-DINITROTOLUENE2,6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYLPHENYL ETHERFLUORENE4-NITROANILINE4,6-DINITRO-O-CRESOLN-NITROSODIPHENYLAMINE4-OROMOPHENOXYBENZENEHEXACHLOROBENZENEPENTACHLOROPHENQLPHENANTHRENEANTHRACENEDI-N-BUTYLPHTHALATEFLUORANTHENEPYRENESUTYLBENZYLPHTHALATE3,3'-DICHLOROBENZIDINEEENZO (A) ANTHRACENEBIS (2-ETHYLHEXYL) PHTHALATECHRYSENEDI-N-OCTYLPHTHALATEBENZO (B & K) FLUORANTHENEBENZO (A) PYRENEINDENO-1,2,3 (C,D) PYRENEDIBENZO PERYLENE

11HIB

59A58A8H35B36B70B40B^OB12H60A62B4IB9B64ASIB78B68B39B84B67B28B72B66B76B69B74B73B83B82B79B

99-O9-283-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-2

7005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-250-32-8193-39-553-70-3191-24-2

CONC====

10000000.U200000C.U1 0000000 U1 000000 £.U2000000.U200000 C,U200000CU200000£i.U200000GU2000005.U1000000CUlOOOOOOGU2000009.U

2000005.U1 000000 C-.U200000i.U20000Q0.U20oooo:.u2Doooo:.u200000 CU200000CVU4000005.U2ooooo:.u200000C.U2oooooau200000PU200000CU

200000CU200000L.U

000337

Laboratory:Lab Sample ID:Sample Matrix: Ut-anData Release Authorize

IT/CerritoB

Sample «:

Case »/SASQC Report <Contract f:JDate Rec'd:

Organics^nalvsis Data Sheet Column *Pestieide/PCB's

Sample Level:Date Extracted: _Date 10 Analyzed:Spl->Extract: ^For Dilution:

PH:ft Moisturex Moisture

10 Sample File10 Std File ID

ID:

(for MB'e)

Mbeta-BHCdelta-BHCqamma-BHC (Lindane)HeptachlorAldrinHeptachlor EpoxideEndosulfan I \l/Dleldrin &-OCU.4.4'-DDEEndrinEndoaulfan II4.4 '-DDDEndosulfan Sulfate4. 4' -DDT /

Methoxvchlor \ Q C - O HEndrin Ketone OC-**cJ*&lS-&\~\' v*Arochlor-1260 O-OOOU

1°

ALL SOLID RESULTS AREREPORTED ON DRY WEIGHT BASIS

Additional SampleSpecific Qualifiers:A •*>

1° - Primary Analysis2° - Secondary AnalysisQ - OC* *o«?̂̂d,' L--I T ̂ rO- OO 0 u

Va

/" VtVi

Aj/fl B! orô ' *̂ ^ Si

Ĵ C .000 ul.5" ul

Circle Units: (uo/Kc?, ua/LCone. SampleV»)0k ,0̂ 0

Q (*•$

• - Asterisked Values are outside QC Limits.* - Recoveries due to Dilution.

:onc. Spikedf^>C'C>

NA - NolNR - No1

S - , Recoveries due to Katrix Effects. NS - NoIT/Cerritos Form I

x RecoveryS 3-

: Analyzedt ReportedI Spiked

Rev 4/86



IT/CERR369B9EB2ORGANIC

COf?POUNI

, 000338

CASE #/SAS #: IT-PAS-12QC REPORT #: ?QS-*?CONTRACT ft: IT-PAS-599994-OI-CDATE RECEIVED: 05/&2/86

VOLATILE COMPOUNDS

(ALL SOLID RESULTS REPORTED ON A DRY WEIGHT BASIS)

LEVEL:DATE EXT/PREP:DATE ANALYZED:SPL—>EXTRACT:PH:7. MOISTURE (NOT DEC. )7. MOISTURE (DEC. ):STANDARD ID:SENSITIVITY ID:UNITS:

MED06/12/8606/12/864. 005G-HOMLMEOH--

EB124BFBEB097UG/KG

LAB ID

36989EB2


COMPOUND SAMPLE SPIKED

78100.009

78100COO

TOLUENE-D84-BROMOFLUOROBENZENE1. 2-DICHLOROETHANE-D4

7590000079000C00B9600O00

'/. RECOVERY

97101115

* - ASTERISKED VALUES ARE OUTSIDE QC LIMITStt - _ RECOVERIES DUE TO DILUTION

RECOVERIES DUE TO MATRIX EFFECTS

NS - NOT SPIKED

$ -

CAS *»

TENTATIVELY IDENTIFIED COMPOUNDS

COMPOUND NAME SCAN # CONC(J)

/ MOO; OOP

000339

IT/CERR36989CJ10

LABORATORY.LABORATORY ID:MATRIX:

DATA RELEASE AUTHORIZED BY

CASE */SAS ft: IT/PAS-12QC REPORT *: PdS-53 9-6CONTRACT #: IT/PAS-S9999J>o%DATE RECEIVED: 05/22/86

SEMIVOLATILE COMPOUNDS(ALL SOLID RESULTS REPORTED ON A DRY WEIGHT BASIS)

LEVEL:DATE EXT/PREP:DATE ANALYZED:SPL—>EXTRACT:PH:X MOISTURE (NOT DEC. ):% MOISTURE (DEC. >:STANDARD ID:SENSITIVITY ID:UNITS:

MEDIUM GPC05/28/86 SEP. FUNNEL06/10/86 CONT. EXT.1.OOG:10ML—SOUL: 1MLM ©0. OQ !«»*-

-NSW- N/ABDCEJ122DFTEJ111UG/KG

YYY

N


SURROGATE SPIKE RECOVERIES

LAB ID

36989CJ10

COMPOUNDNITROBENZENE-D52-FLUOROBIPHENYLP-TERPHENYL-D14PHENOL-D52-FLUOROPHENOL2, 4,6-TRIBROMOPHENOL

SAMPLE2000000. U2000000. U2000000. U2000000. U2000000. U2000000. U

SPIKED50900.50100.53000.103000.102000.102000.

RECOVERY0 * ^0 */o *^000

» .*-*>

»#*

ASTERISKED VALUES ARE OUTSIDE QC LIMITSRECOVERIES DUE TO DILUTIONRECOVERIES DUE TO MATRIX EFFECTS

NS - NOT SPIKED

CAS #


COMPOUND NAME SCAN CONC(J)

123456789

1011121314151617181920

O 0 O

S? I / 2 0 -50OOO

M-l 1 1

/ Mpt.hyignp CMoridfl"'Acetone Fc"c^i',r r-1-.--3--' Reported in Method £-Iar±

000340

Laboratory: IT/Carrltoa

Organice Analvaia Data SheetData Reporting Qualifiers

General Data Qualifiers:

Value - Concentration Found (Value >. DL>DL - Detection Limit ~U - Analyzed for but not detected (Reported Value la Detection Limit)J * Estimated Value: Target Compound - 0 < Value < DL; or

Tent. ID'« - A 1:1 response ia assumed for Ouantitation.B - Compound found in Blank. Sample reaulta are not Blank Corrected.II/A - Not AnalyzedMR - Not ReportedMS - Not Spiked

Pesticide Qualifiers;

C - Confirmed by GC/MS; GC Ouantitation Reported•• - Detected and Confirmed by GC below GC/HS DL; ' •-

GC Ouantitation ReportedN - Not Confirmed by GC/KS; Attempted and unsuccessful••N - GC/HS Confirmation attempted and unsuccessful becauae concentration

is < GC/HS DL; GC Ouantitation reportedUN - GC/KS Confirmation attempted and unsuccessful although suspect

compound concentration is >GC/MS DL; GC/HS DL ReportedUNI - GC/HS Confirmation attempted and unaucceaaful due to interferencea

although suspect compound concentration is >GC/HS DL;Ad mated GC/HS DL Reported •

LID - Lost In Dilution; Sample was diluted so much that Dibutyl chlorendatewas Lost In Dilution.

CEP - Co-Eluting Peak; An apparent shift in Dibutyl chlorendate RT wascaused by a Co-Eluting Peak, not a true unacceptable RT Shift.

Surrogate and Spike Qualifiers;

• - Asterisked Values are outside QC Limitsi - High/Low Recoveries due to Dilution.9 - High/Low Recoveries due to Matrix Effects.

Soil Sample Result Qualifiers;

x Moisture « - fc Moisture value used for Dry Weight CalculationsNOTE: « Moisture(type) used in caluclation should Batch

Sample weight(typo).

NSW - No Standing WaterxM(n) - * Moisture (Not Decanted)xM(d) - x Moisture (Decanted)g(n) - Sample weight taken from sample which was Not Decantedg(d) - Sample weight taken from sample which was Decanted

IT/Cerritoa Form I Rev 4/86

rf(f/0(j•> iYX) ft-Gu3 /Y)n /vrxj•") fW>.(VY)u

iy,i>££>,tXtt>t.i

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if: JT/P/)S-/3, Laboratory: IT/CerritosMftKurh Quality Control Report

Or«i

7

FIELD DATA SHEET

Environmental Response Team, Environmental Protection AgencyWoodbridge Ave., Edison, N J. 08837

(201) 321^660

000343

Location:

Collectors:

Lab Number (Consec.0'8) ' . Date Collected

VEGETATION GROUNDWATERUpland-DryLowland-DryFloodplainWetlandGully ••-_ ,.

Old Field ̂ ResidentialWooded ^Industrial

AugeiCore .Split SpoonCylinder Cup

Water Table Depth

Farmland _ Commercial

Sample DepthHerbaceousShrubsTreesSlope >15*

SAMPLE PREPARATION

Container asssa -ar Cleaning Procedure* ~~-ggKemmerer

-~ 5.-

PetersenLow—^Hiflh CoĵGlass Jar

^Plastic Jart̂ Metal. Acetate Core

™ Paper Cap. JTeflonCap

. Acetone Rinse— Hexane Rinse--Other

Velocity

DIRECTIONFloat. Solids

v Ambient ~-Dry Ice

TRANSECT INFORMATION

Letter Station *

1- - - - - . .. Compass Direction - -:~-

:_-. - - - - - -:--- • - r."

'~. Distance Between Stations -.u ^ r^-^f'-'v

, -T

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to is ~ .;.-:|̂ j*

/v f •**-• r* -•*^ f^ ^^f-'^ r ~..L^SSj.-.'/,'̂ ;.'-^^-/ ^i'Jte>n.lL-J^tt'-'' ""':i?jf2.>

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• /- •-,-.:'••£.ko'\/£ buna

OOO344

EE3 INTERNATIONALTECHNOLOGYCORPORATION

Enviresponse, IncGSA Raritan Depot, Woodbridge Ave.Building 209, Bay FEdison, N. J. 08837Attn. of: Ms. Janet CullinaneN. J. Lab Certification ID# 12064


Sample #55915A-05615, Liquid

EPAMaximum

E. P. Toxicity LeachateLeachate Concentration

(mg/L) (mg/L)

CyanideSulfida, 24Flash PointCorrosivity (mmpy]

O00345ANALYSIS DATA 3H6.ET

LABORATORY: IT/CERRLABORATORY ID: 369B9EB12MATRIX: ORGANlC,UEXTRACT:PH:'/. MOISTURE (NOT DEC.'/. MOISTURE

3000000061QOOOO44000 OOO

10000A3O y10000 OOO U

1 0000(7̂6500000̂

1 OOOCOC?C>3QOOOOOO

10000^7001000000010000OCO

U30000000 VIOOOOOOO O30000.̂ ^ u

30000000 u10000 DOOU10000000 t>30000C/OO10000OOOI/

.10000000̂270000000

000346


IT/CERR36989CJ13SOIL-


CASE #/SAS #:QC REPORT #:CONTRACT #: IT/PAS-39999V-DATE RECEIVED: 05/22/86

IT/PAS-12~ 3 ?



LEVEL:DATE EXT/PREP:DATE ANALYZED:SPL-->EXTRACT:PH:X MOISTURE (NOT DEC. )% MOISTURE (DEC.):STANDARD ID:SENSITIVITY ID:UNITS:

MEDIUM GPC Y N<05/28/86 SEP. FUNNEL Y~~ N"06/10/86 CONT. EXT. Y~ N~100.G:10ML—SOUL:1ML

-ô oo

BDCEJ122DFTEJ111UG/KG

» - USED FOR DRY WEIGHT CALCULATION

PP # CAS «

65A18B24A26 B27B6H25B2H42B3H63B12B56B54B57A34A1H43B31A8B55B7H52B22A9H53B21A4HSOB10H71B77B

108-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-7

39638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-33-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3208-96-8

PHENOLBIS (2-CHLOROETHYL) ETHER2-CHLOROPHENOLli3-DICHLORODENZENEli4-DICHLOROBENZENEBENZYL ALCOHOLli2-DICHLOROBENZENE2-METHYLPHENOLBIS (2-CHLOROISOPROPYL) ETHER4-METHYLPHENOLN-NITROSQ-DI-N-PROPLYAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2.4-DIMETHYLPHENOLBENZOIC ACIDBIS (2-CHLOROETHOXY) METHANE2.4-DICHLOROPHENOLI.2.4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2-METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2,4,6-TRICHLOROPHENOL2,4,5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINEDIKETHYLPHTHALATEACENAPHTHALENE

CONCS = = B

2000000.U2000000.U2000000.U2000000.U200000C.U

. 2000000.U2000000U200000i>U2000006.U200000D.U2000000.U200000C.U200000DU200000DU2000000.U200000f)Ulooooooo^u2000000.U2000000U200000C U200000CU2000000U200000CU2000000U2000000.U200000fU200000CU10000000U200000CUlOOOOOOOU2000000U200000DU

.f-.'i,',.;. O00347

LABORATORY:LABORATORY ID:MATRI X:

IT/CERR36989CJ13

CASE ft/SAS ft:QC REPORT ft:CONTRACT ft:DATE RECEIVED:

IT/PAS-12/M5-33

^DATA RELEASE AUTHORIZED BY:

SEMIVOLATILE COMPOUNDS (PACE 2>


LEVEL:DATE EXT/PREP:DATE ANALYZED:SPL—^EXTRACT:PH:% MOISTURE (NOT DEC. )'/i MOISTURE (DEC. >:STANDARD ID:SENSITIVITY ID:UNITS:

MEDIUM GPC Y.05/28/86 SEP. FUNNEL Y06/10/86 CONT. EXT. Y100.G: 10ML-=50UL: 1ML

-WitJi/\T/ ANSW M/ABDCEJ122DFTEJ111UG/KG


PP CAS

11HIB59A58A8H35B36B70B40BSOB12H

62B41B9B64A81B78B68B39B84B67B28B72B'. 6B76B69B74B73B83B82 B79B

99-09-283-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-2

7005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-250-32-8193-39-553-70-3191-24-2

3-NITROANILINEACENAPHTHENE2,4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2,4-DINITROTOLUENE2,6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYLPHENYL ETHERFLUORENE4-NITROANILINE4,6-DINITRO-O-CRESQLN-NITROSODIPHENYLAMINE4-BROMOPHENOXYBENZENEHEXACHLOROBENZENEPENTACHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYLPHTHALATEFLUORANTHENEPYRENEBUTYLBENZYLPHTHALATE3,3'-DICHLOROBENZIDINEBENZO (A) ANTHRACENEBIS (2-ETHYLHEXYL) PHTHALATECHRYSENEDI-N-OC TYLPHTHALATEBENZO (B & K) FLUORANTHENEBENZO (A) PYRENEINDENO-1,2,3 (C,D> PYRENEDIBENZO (A ,H ) ANTHRACENEBENZO ( G < H , I ) PERYLENE

CONCssss

looooooDu2000001/.U1000000D.U1000000D.U200000D.U2000000U200000D.U200000D.U200000 D.U2000000.UlOOOOOOilU10000000.U2000000, U200000f,U200000D.UlooooooAu200000C.U

200000l'.U2000001'. U200000 £U200000PU400000 TU200000CU200000 ru200000i'.U200000AU200000 ru200000AU200000 r.U200000: u200000 l",U

Laboratory:Lab Sample ID:Sample Matrix;Data Releaae Authorized

IT/Cerritoa Case */SAS »:QC Report #:Contract f:

Rec'd:

- 336̂S-C~.

Organiea Analysis Data Sheet Column ft (for KB'*>Peaticide/PCB'a

Sample Level:Date Extracted: ̂Date 10 Analyzed:Spl->Extract: jFor Dilution:

pH:k Moisture* Moisture

10 Sample File ID:10 Std File ID:

20 Sample File ID:20 Std File ID:

f-iQ3T-_/Wt of sample ext'd (g)Vol of total ext (ul>

Va

Vt

ml or

JC'O.OOP ul0j • - Asterisked Values are outside OC Limits. NA - Notf - Recoveries due to Dilution. NR - No13 - Recoveries due to Matrix Effects. NS - No1

. VCerritos Form I

litsVuCTKo^ ua/Lst êô ery/^TJL

; Analyzed: ReportedL Spiked

Rev 4/86

- - - ••:,:,,,,-;, ̂ ;.VS:;S L..T, ;̂ =.T .V.:-L?. : -S6- 000343

LABORATORY: IT/CERR CASE #/SAS #: IT-PAS-12LABORATORY ID: 369B9EB12 . QC REPORT t:MATRIX: ORGANICuCMJ^ .fl CONTRACT #: IT-PAS-599994

J\L /* DATE RECEIVED: 05/,JZ/86DATA RELEASE AUTHORIZED BY: ̂^̂ AAĴ -Z .

I/ /̂VOLATILE COMPOUNDS

(ALL SOLID RESULTS REPORTED ON A DRY WEIGHT BASIS)

LEVEL: MEDDATE EXT/PREP: 06/13/86DATE ANALYZED: 06/SPL—>EXTRACT: 4. 0PH: AlA _7. MOISTURE (NOT DEC. ): juM"X MOISTURE (DEC. >: ,. |U/ASTANDARD ID: MSVEB130SENSITIVITY ID: BFBEB101

1 UNITS: UG/KG


LAB ID COMPOUND SAMPLE SPIKED 7. RECOVERY

TOLUENE-D8 11B0000C0 125000pCO 94369B9EB12 4-BROMOFLUOROBENZENE 1200000O? 125000#0 96

1,2-DICHLOROETHANE-D4 1330006̂ ^ 125000


IT/CERR36989CJ13


r :j3*-..!j 000350

CASE */SAS #. IT/PAS-12QC REPORT *:CONTRACT #:DATE RECEIVED: 05/22/86

SEMIVOLATILE COMPOUNDS(ALL SOLID RESULTS REPORTED ON A DRY WEIGHT BASIS)

LEVEL:DATE EXT/PREP:DATE ANALYZED:SPL—>EXTRACT:PH:X MOISTURE (NOT DEC. )% MOISTURE (DEC. ):STANDARD ID:SENSITIVITY ID:UNITS:

MEDIUM GPC05/28/86 SEP. FUNNEL06/10/86 CONT. EXT.100. G: 10ML---SOUL: 1ML

.0AQ. 00 •-NSW-BDCEJ122DFTEJ111UG/KG

YYY

NN"N


SURROGATE SPIKE RECOVERIES

LAB ID

36989CJ13

COMPOUNDNITROBENZENE-D52-FLUOROBIPHENYLP-TERPHENYL-D14PHENOL-D52-FLUOROPHENOL2, 4,6-TRIBROMOPHENOL

SAMPLE2000000. U2000000. U2000000. U2000000. U2000000. U2000000. U

SPIKED50900.50100.53000.103000.102000.102000.

*/. RECOVERY0 *1?0 * &0 * *0 *^0 * i£0 *^

» - ASTERISKED VALUES ARE OUTSIDE QC LIMITS* - ZTVJ RECOVERIES DUE TO DILUTION* - RECOVERIES DUE TO MATRIX EFFECTS

NS - NOT SPIKED

CAS *


COMPOUND NAME SCAN # CONC(J)

1 lcw

000351

Laboratory: IT/Cerritoa

OrganiCB Analysis Data SheetData Reporting Qualifiers

General Data Qualifiers:

J

Value - Concentration Found (Value >. DL)DL - Detection LimitQ - Analyzed for but not detected (Reported Value ia Detection Limit)J - Estimated Value: Target Compound - 0 < Value < OL; or

Tent. ID'a - A 1:1 reaponae ia aaaumed for Quantitation.B - Compound found in Blank. Sample reaulta are not Blank Corrected.N/A - Not AnalyzedMR - Not ReportedIS - Not Spiked

Pesticide Qualifiers;

C - Confirmed by GC/HS; GC Ouantitation Reported• • - Detected end Confirmed by GC below GC/HS DL; * ~ ~ .

CC Quantitation ReportedN - Not Confirmed by GC/NS; Attempted and unauccesaful••N - GC/HS Confirmation attempted and unaucceaaful becauae concentration

ia < GC/HS DL; GC Ouantitation reportedUN . - GC/HS Confirmation attempted and unsuccessful although auapect

compound concentration ia >GC/HS DL; GC/MS DL ReportedONI - GC/HS Confirmation attempted and unaucceaaful due to interferencea

although auapect compound concentration ia >GC/HS DL;Adjusted GC/HS DL Reported

LID - Loat In Dilution; Sample was diluted so much that Dibutyl chlorendatewaa Loat In Dilution.

CEP - Co-Eluting Peak; An apparent shift in Dibutyl chlorendate RT waacauaed by a Co-Eluting Peak, not a true unacceptable RT Shift.

Surrogate end Spike Qualifiers:

• - Aateriaked Valuea are outside QC Limitsf - High/Low Recoveriea due to Dilution.3 - High/Low Recoveriea due to Hatrlx Effects.

Soil Sample Result Qualifiers:

ft Hoisture • - * Hoiature valua used for Dry Weight CalculationsNOTE: x Moisture(type) used in caluclation should match

Sample weight(type).

NSW - No Standing WaterXHCn) - ft Moisture (Not Decanted)ftM(d) - ft Moiature (Decanted)g(n) - Sample weight taken from sample which was Not Decantedg(d) - Sample weight taken from sample which was Decanted

IT/Cerritos Form I R«v 4/86

Case I/SAS 1: rr P/K5 - nO

OO

352

Level :Matrix:QC Report

FractionPest.SMO

Sample I

—•v /V\£/til/ >M,V .

/to*J.So*4- Or^»*tic LlVnuJIr-^ PAS- 33

CompoundLindane (ganuna-BHC)HeptachlorAldrinDieldrinEndrin4 ? 4 ' - D D TDibutyl chlorendate **

i!

ug/KgSpiked/00.5

/ 00$3.$5o5-5c

000353

FIELD DATA SHEETEnvkoiNiMntal RccponM TOMB, EnvtromiMotal Protection Agency

ftAv*..Ed(201) 121-

4* ttamtar

OOO354




Sample #55910A-05610,Solid

EPAMaximum

E. P. Toxicit-y LeachateLeachate Concentration

(mg/L) (mg/L)

J

Cyanide 3.2Sulfide

OOD3S5

FIELD DATA SHEETEmrironnwntal Racoon** T**m, Cnvtronmratal Protection Agency

Woodbrtdoe Av*n Edison, N J. OSS37(201)221- •••**

Upland-DryLotwtandOryFloodptainWetlandOuHy

SKS:.. m*'I*---latft"«:

*!-..-.Sd£'

*™s*': .:.j

^^w'V'glC.^.,

i..;. -i: .-•'--

' = • • *oria

Ft^-K

*-' -•- r*" -̂.^ • •,%

Tiowl

EHEBES r̂il̂ Sw

Tntt

OeedFWi

Ind.FtoetSoHdi

^CJ»«nJnj(P»pcedun»____txLam i»Hlph Conoentratic

Other Soivent RimeSpecify:

Compus OifecMon OltUuc* Bctaeen Stations

it->^^"j 4

Ft

000356


Enviresponse, IncGSA Raritan Depot, Woodbridge AveBuilding 209, Bay FEdison, N. J. 08837Attn. of: Ms. Janet CullinaneN. J. Lab Certification ID# 12064

Job # 5702Date:Auth:Lot «: 0485Invoice #:Sample Date: 5/21/86

Sample #55912A-05612,Solid

(ppm)

E. P. ToxicityLeachate(mg/L)


Cyanide

pvM^JSwf,;̂ ..S f * " • • • • ; . •

tor "~" 000357

FIELD DATA SHEETEnvironmental Responae Team, Environmental Protection Agency

Woodbridae Ave., Edteon, N J. 04*37(201) 121-6660

UptancKkyLowtan«-OryFloodptain .

000358




Sample #55911A-05611, Solid

(ppm')

EPAMaximum

E. P. Toxicity LeachateLeachate Concentration

(mg/L) (rog/L)

Cyanide

000359



Job t 5702Date:Auth:Lot #: 0485Invoice £:Sample Date: 5/21/86

Sample #55913A-05613,Semi-Solids

(ppm)

P. ToxicityLeachate(mg/L)


CyanideSulfideIgnitabilityCorrosivity (mmpy)

ArsenicBariumCadmiumChromium

LeadMercurySeleniumSilver

EndrinLindaneMethoxychlorToxaphene

2 , 4-D2,4,5-TP

Documents

ERT - COMPOSITIONAL ANALYSES OF SAMPLES · 2020. 11. 30. · OF SAMPLES COLLECTED BY ERT. 000332 FIELD DATA SHEET Environmental Response Team, Environmental Protection Agency Woodbrldge