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    Low-cycle fatigue properties of steel 42CrMo4

    R. Kunc , I. Prebil

    Faculty of Mechanical Engineering, Askerceva c. 6, SI-1000 Ljubljana, Slovenia

    Received 22 November 2001; received in revised form 25 June 2002

    Abstract

    In structures subjected to heavy cyclic loading, fatigue damage of material during cyclic plasticity is one of the most frequentfailure mechanisms. For determining the low-cycle fatigue lifetime, it is essential to know the elasto-plastical response of the material

    to a cyclic load, since the accumulated plastic strain has a direct influence on the lifetime of the material. The elasto-plastic response

    of the material under a cyclic load is described here by using the constituti ve macroscopic model of small deformations. This model

    considers isotropic and kinematic hardening or softening in connection with material damage. The procedure of determining the

    material parameters by the described model is illustrated for normalised and tempered states of a low-alloy steel 42CrMo4 (ISO 683/

    1).

    # 2002 Elsevier Science B.V. All rights reserved.

    Keywords: Low cycle fatigue; Cyclic plasticity; Material parameters; Damage mechanics; Kinematic hardening; Isotropic hardening

    1. Introduction

    The fatigue life of highly loaded engineering compo-

    nents is influenced by repeated plastic deformation,

    which causes the accumulation of plastic strain in

    material. Shortening of fatigue life of such components

    can be estimated by means of non-linear response of

    material to a cyclic load. A plethora of numerical

    models for describing material response have been

    developed e.g. [1

    /9]. The microscopic fatigue processeswithin the material (dislocations, sliding systems of the

    principal sliding planes etc.) are described by means of

    models of Bauschinger effect, cyclic hardening or soft-

    ening, ratchetting and mean stress relaxation. There are

    also several theories that have been developed for the

    purpose of determining the failure moment of a material

    under plastic load. The theory of continuum damage

    mechanics attempts to compose several micromechani-

    cal damage mechanisms into a single mechanisms e.g.

    [1,3,7,9]. The damage parameter of a material and,

    respectively, the continuum damage theory is in this case

    included into the constitutive equation and thereby

    influences the elasto-plastical response of the material.

    An alternative to the damage mechanics of continuum is

    a series of damage criteria that have no influence on the

    constitutive equation e.g. [10].

    To simulate the non-linear cyclic response of thematerial, we have decided to use the material model,

    which unites non-linear kinematic hardening, isotropic

    hardening or softening and simplified damage me-

    chanics of continuum, where we have used the same

    damage evolution for negative and positive stresses[1,4].

    The decision to use such a model was based upon the

    results of own experimental research of a low-alloy steel

    42CrMo4 (ISO 683/1), which show the influence of

    material damage on cyclic strain/stress response of the

    material, as well as the results of experiments and

    numerical simulation of material response [4] and the

    quickest possible*/and thus cheap*/procedure of de-

    Corresponding author. Tel.:/386-1-4771-128; fax: /386-1-2518-

    567

    E-mail addresses: [email protected] (R. Kunc ),

    [email protected] (I. Prebil).

    Materials Science and Engineering A345 (2003) 278/285

    www.elsevier.com/locate/msea

    0921-5093/02/$ - see front matter# 2002 Elsevier Science B.V. All rights reserved.

    PII: S 0 9 2 1 - 5 0 9 3 ( 0 2 ) 0 0 4 6 4 - 1

    mailto:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]
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    termining the material properties. The article demon-

    strates the procedure of determining all the material

    parameters of the steel 42CrMo4 (ISO 683/1) in normal-

    ised state with hardness of 195 HV and tempered state

    with hardness of 462 HV, by using the described

    material model.

    2. Modelling of cyclic plastification and damage

    2.1. The mechanical principle

    The existence of microscopic cracks and defects the

    size of crystal grains is in macroscopic mechanics

    referred to as material damage. The nucleation process,

    growth and merging ofvoids that represent initiation of

    macrocrack and induce progressive weakening of mate-

    rial toughness and stiffness is referred to as damage

    evolution. The state of damage in the material, D , istheoretically determined by the common influence of

    size and configuration of microcracks and microvoids.

    The actual macroscopic stress within the damaged

    material s is determined by assuming that the nominal

    cross-section A is reduced by the size of the damaged

    area AD [1,3,7,10,11].

    D(M; n; x)dADx

    dA[ s

    F

    AAD

    F=A

    1AD=A

    s

    1D: (1)

    The material damage concept is built into the

    constitutive model of small deformation oij, which are

    split into their elastic and their plastic part:

    oijoeijo

    pij; (2)

    where the relationship between elastic stresssij strainoij,

    damage D and elasticity modulus tensor Lijkl is deter-

    mined by:

    sij (1D)Lijkloekl: (3)

    The elasticity modulus tensor is determined by

    Youngs modulus Eand Poissons ratio n .

    Lijkl E

    1 n

    1

    2(dikdjldildjk)

    n

    1 2ndijdkl

    : (4)

    The rate of plastic strain is derived from the normality

    rule:

    opij l

    @f

    @sij; (5)

    where l is the plastic multiplier, derived from the

    consistency condition f0: The stress potential f [1]is a function of stress tensor sij, the components of

    kinematics (Xij) and isotropic (R ) hardening and the

    material damage D . For an isothermal state dT/dt/0,

    the rheological model and the evolution equation of the

    stress potential is determined by[1,4]:

    f seq(Rk)0; (6)

    seq ffiffiffiffiffiffiffiffiffiffiffiffiffi3

    2 sijsijs

    ; sij

    sij

    1

    3 dijsk;

    sij sij

    1DXij:

    (7)

    Taking the derivative ofEq. (5)yields:

    f@f

    @sijsij

    @f

    @XijXij

    @f

    @RR

    @f

    @DD; (8)

    where:

    @f

    @sij

    3

    2

    sij

    (1D)seq;

    @f

    @R1; (9)

    @f

    @XDij

    3

    2

    sij

    seq;

    @f

    @D

    3

    2

    sijsij

    (1D)seq:

    2.1.1. The isotropical model of hardening/softening

    If the yield surface is enlarged or reduced during a

    cycle loading process, the material is subject to cyclic

    hardening or softening. The evolution of a yield surface

    is described by scalars R and k. R represents the

    variable that describes isotropic hardening or softening

    stress of the material, while k represents the size of the

    elastic area. The initial values for the size of the yield

    surface are determining by using the criterionk/syand

    R/0, wheresyrepresents the yield stress. The evolution

    equation for isotropic hardening or softeningR has the

    form:[1]

    Rb(RR)l; (10)

    where b represents the material parameter, which

    determines the level of isotropic hardening or softening,

    while the parameter R determines the boundary of

    isotropic cyclic hardening or softening.

    2.1.2. The kinematic hardening model

    Kinematic hardening is essential for the description of

    cyclic effect as ratchetting and mean stress relaxation as

    well as the Bauschinger effect. It is described by the back

    stress tensor Xij that determines the centre of the yield

    surface in stress space and is taken to be the sum of three

    non-dependent contribution:

    XijX3n1

    X(n)ij : (11)

    To determine the values of each of the three-tensor

    components Xij(n ), the evolution equations proposed by

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    Armstrong, Frederick and Chaboche [12,14/18] have

    been used. The boundary value of hardening is deter-

    mined by the kinematic hardening coefficient X(n ),

    whilst the value of plastic extension at which the

    respective components Xij(n ) reach their boundary value

    is determined by the kinematic hardening level g(n ). The

    influence of the rate of reduction of the mean stressvalue is controlled by the Ohno/Wang material para-

    meter mn .

    X(n)ij

    2

    3g(n)X(n)

    (1D)opl;cij

    X(n)eq

    X(n)

    mnX

    (n)ij g

    (n)l; (12)

    where the effectivevalue of the stress space centre tensor

    is:

    X(n)eq

    ffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi2

    3X

    (n)ij X

    (n)ij

    s : (13)

    2.1.3. The continuum damage mechanics

    The continuum damage mechanics deals with the

    material damage during cyclic loading. A damaged

    material contains microcracks and defects that reduce

    the load carrying capacity of material. The problem

    arises when trying to determine the initiation and

    growth of the material damage during loading process.

    The material damage can only be determined with

    sufficient accuracy by using the failure method, where

    the size of the microcrack area is measured on arepresentative volume element. Even this method fails,

    though, when the distribution of cracks and defects is

    non-homogenous.

    Experiments on low-cycle lifetime of sub-eutectiod

    steels have verified the statements[1,3/6]that measure-

    ment of the increase in material damage can be done by

    using the indirect experimental method of observing the

    change of the modulus of elasticity:

    E(1D)E: (14)

    The increase of the damage is described by an

    evolution equation[1,12,13], which considers a propor-

    tional influence of the effective plastic deformation onthe change of damage, of the form:

    Ds2eq(2=3(1 n) 3(1 2n)(skk=3seq)

    2)

    2SE(1D)2 pa(p);

    a(p) 1; for p]pD

    0; for pBpD:

    (15)

    The initial damage threshold pD is determined by the

    accumulated plastic deformation p :

    pl

    1D; pDmax(p(D0)): (16)

    3. The experimental work

    The test pieces were manufactured of a rolled plate

    made of low-alloy tempering steel 42CrMo4 (ISO 683/1;

    W.Nr. 1.7225). Chemical composition of the steel is

    presented inTable 1.The principal axis of the test pieces

    was perpendicular to the axis of rolling. The test pieceswere shaped as to ensure minimal stress concentration in

    the areas of change in diameter [19]. The steel was

    normalised at 840 8C and cooled down in a stove. The

    tempered pieces were heated up to a temperature of

    830 8C and quenched in oil and then tempered at

    400 8C for 1 h.

    The first series of tests were monotonic tensile/

    compressive tests to failure, the second series of tests

    were 20 cyclic uniaxial tests with control of extension

    amplitude for determining the cyclic parameters of the

    material. The extension was measured directly on the

    test piece by means of a dynamical measuring device[19]. In practice, it is sufficient to conduct eight cyclic

    tests for a good simulation of material response.

    To avoid the local cross-section contraction within the

    probe length of the test piece, the tensile/compressive

    test was conducted at constant extension amplitude. The

    mechanical properties were measured at 20 8C. Heating

    of test pieces was prevented by the low loading

    frequency of 2 Hz.

    4. Determining the material parameters

    4.1. The monotonic parameters

    The described damaged model contains 17 material

    parameters (Table 2). The basic material parameters like

    the modulus of elasticity E, the Poisson ratio n and the

    yield stress sy were determined by a series of standard

    monotonic uniaxial tensile/compressive tests[19].

    4.2. The parameters of isotropic and kinematic hardening

    The parameters that describe kinematic hardening

    were determined from thes /ocyclic curve at a constantamplitude of extension Do. Different extension ampli-

    tudes after stabilisation give hysteresis loops (Ns) of

    respective amplitudes of plastic extension Dop and

    amplitudes of stress Ds (Fig. 1). The levels g1, g2 and

    g3 and the boundary values X1 , X

    2 and X3 of

    kinematic hardening are derived from the course of

    the experimentally determined stable hysteresis loop by

    means of theEq. (16)[1].

    The levels of kinematic hardening g(n ) determine the

    values of plastic extension at which the respective

    components of the kinematic hardening tensor Xij(n )

    reach their boundary value X(n ) (Fig. 1).

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    Ds

    2 (R

    k)X1

    tanh

    g1

    Dop

    2

    X2

    tanh

    g3

    Dop

    2

    X3

    tanh

    g3

    Dop

    2

    : (17)

    Simultaneously, the boundary value of isotropic soft-

    ening R and the size of the elastic area k are

    determined from the experimental stable hysteresis

    loop and the mutual influence of the kinematic hard-

    ening. The experiment shows the trend of reduction of

    the maximal and minimal stress dependant on the

    number of cycles which means that the material issubject to softening (Figs. 4 and 6). The values of the

    Ohno/Wang factorsm1,m2and m3are determined from

    the course of experimental curves of amplitudes and

    from the mean value of the stress, dependant on the

    number of cycles (Fig. 4). They depend on the rate of

    reduction of the mean value of stress until stabilisation

    of the hysteresis loops. To determine these factors, a

    non-symetrical uniaxial cyclic test with a constant non-

    zero extension amplitude is used.

    The isotropic hardening or softening level is deter-

    mined by the parameter b . It depends on the ratio of

    experimental course of stress amplitudes smaxN

    at aconstant strain amplitude, from the first cycle smaxl to

    stabilisation of hysteresis loop smaxS (Fig. 2). It is

    described byEq. (17) [1]:

    bln[1 (sNmax s

    lmax)=(s

    Smax s

    lmax)]

    2DopN: (18)

    4.3. The damage parameters

    The experiments have shown, that in low-cycle

    loading of a sub-eutectiod steel 42CrMo4 in the begin-ning of growth of the accumulated plastic deformation

    p , the modulus of elasticity can decrease as much as 5%.

    The cause of this decrease is in connection of micro-

    plastifications with reversible travel of dislocations and

    in forming of Luders bands, and not in the growth of

    material damage [1,21]. This phenomenon is soon

    saturated, therefore, the further change of the modulus

    of elasticity is considered as the criterion of damage

    growth.

    In numerical observation of damage growth, we need

    to know the initial damage threshold pD, the resistive

    energy of the damageSand the damage critical valueDc

    [1]. The value of the pD parameter equals 0 for the

    chosen steel. This is proven by the experimentally

    determined curve of damage growth (Fig. 3), which

    continuously rises from thevery beginning of the plastic

    deformation in the material. The average value of the

    damage resistive energy S for the subeutectoid steel

    42CrMo4 at different heat treatments is determined

    experimentally (Fig. 3), by using the Eqs. (18) and (13)

    [1]:

    S s

    2E(1D)2 dD=

    dp; p2X

    N

    i1

    Dop

    i: (19)

    Theoretically, the critical damage value Dc reaches 1

    in the moment of material breakdown (Nf). In the

    majority of cases, though, the material breaks down

    instantly, which causes a fall in the value of Dc.

    Determining the actual value of the Dc parameter is

    based on the experiments and the Eq. (19). The

    progressive damage growth immediately before the

    failure limit represents the initiation of a macro crack

    and is the critical limit of Dc (Fig. 3). The average

    critical values for the 42CrMo4 steel are around 0.16 in

    normalised state and around 0.06 in tempered state.

    Dcmax(D(p)): (20)

    5. Model verification

    The numerical damage model has been incorporated

    into a computer programme based on the finite element

    method [20]. In programme development, a common

    symbolic approach was used [20], which enables the

    creation of an effective, quadratically convergent im-

    plicit numerical scheme, even in cases with largenumbers of evolution equations and interconnected

    non-linear systems.

    From the comparison of numerical and experimental

    results, avery good accordance of maximal and minimal

    stress in relation to the number of load cycles is obvious

    (Figs. 4 and 6), as well as matching in the size and the

    shape of the hysteresis loops (Figs. 5 and 7). The

    verification of the isotropic softening and kinematic

    hardening runs from the start of loading to stabilisation

    of the hysteresis loops (Figs. 4 and 6). The isotropic

    softening is compared with the course of change in

    maximal and minimal stress amplitudes, while the

    Table 1

    Chemical composition of 42CrMo4 steel (values in %)

    C Si Mn P S Cr Ni Mo Cu Al Sn

    42 CrMo4 0.43 0.26 0.65 0.015 0.021 1.07 0.19 0.16 0.16 0.021 0.006

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    Table 2

    Material parameters of the damage model for the 42CrMo4 steel

    42CrMo4 (HV) E (Mpa) sy (MPa) n b R g1 g2 g3 X

    1 (Mpa) X2 (Mpa) X

    3 (Mpa)

    195 2.05105 180 0.3 4 80 3700 860 30 100 100 400

    462 2.11105 650 0.3 5 380 15 000 2000 190 200 250 900

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    kinematic hardening is compared with the course of the

    mean stress value (Fig. 6). After stabilisation of the

    hysteresis loops or, respectively, after the decrease in

    influence of kinematic and isotropical hardening, the

    main influences on the stress/strain state is by the

    material damage growth. The growth of damage causes

    a slight decrease of the stress amplitude all the way to

    the terminal failure.

    The good match between the calculated strain/stress

    response and the measured values is also obvious in the

    course of the plastic elongation as it depends of the

    number of oscillations (Figs. 8 and 9). The matching is

    good in the surge at the beginning, as well as in the

    further course of the plastic elongation, which is the

    base for verifying the suitability of the model in

    Fig. 1. Determination of the components of hardening parameters

    X(n ) and g(n ) and the limit of isotropic hardening R from the

    experimentally determined stable hysteresis loop for the normalised

    steel 42CrMo4 with hardness of 195 HV. A symmetrical load case with

    constant extension ofDo/1.2%.

    Fig. 2. Determination of isotropic hardening level parameterb for the

    normalised steel 42CrMo4 with hardness of 195 HV. Various

    symmetrical load cases at a constant extension.

    Fig. 3. Determination of material damage parameters (pD,Dcand dD /

    dp ) for the normalised steel 42CrMo4 with hardness of 195 HV. A

    symmetrical load case with a constant extension ofDo/1.2%.

    Fig. 4. Comparison of the course of amplitudes in relation to the

    number of cycles between the measured values and the numerical

    calculations for the normalised steel 42CrMo4 with hardness of 195

    HV. A symetrical load case at a constant extension ofDo/1.2%.

    Fig. 5. A comparison of hystreresis loops in relation to the number of

    cycles between measurement and numerical calculation for the

    tempered steel 42CrMo4 normalised steel 42CrMo4 with hardness of

    195 HV. A symmetrical load case at a constant extension ofDo/1.2%.

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    following the damage growth and the accumulated

    plastic strain.

    Fig. 5 shows the phenomenon of natural yield stress

    for the normalised 42CrMo4 steel with a sharp yield

    stress boundary and a steep fall down to the so called

    lower yield stress. This phenomenon is not that obvious

    for the tempered state of the same steel (Fig. 7). The first

    decrease in the modulus of elasticity for the values of up

    to 5% actually occurs in the area of crossing the Lu ders

    elongation. This initial decrease in the modulus of

    elasticity, though, is not taken into account in determin-

    ing the material damage growth. The chosen model is

    not able to accurately describe the natural yield stress

    phenomenon and thus the numerical non-linear re-

    sponse in the first load cycles deviates from the real

    material behaviour (Figs. 5 and 7).

    6. Conclusions

    Comparing the results obtained from the measure-

    ments and from the chosen numerical model shows that

    the simulation of the material response to a low-cycle

    loading to destruction is very reliable. The numerical

    model incorporates non-linear kinematic hardening,

    isotropical hardening or softening and the continuum

    damage mechanics.

    Simulations of low-cycle material response to destruc-

    tion have shown that all the required parameters of

    normalised (195 HV) and tempered (462 HV) low alloy

    steel 42CrMo4 can be accurately determined from a

    number of experiments as low as ten.

    Fig. 6. Comparison of the course of amplitudes in relation to the

    number of cycles between the measured values and the numerical

    calculations for the tempered steel 42CrMo4 with hardness of 462 HV.

    A non-symetrical load case at a constant extension ofDo/1.4% and a

    mean value ofomean/0.5%.

    Fig. 7. A comparison of hystreresis loops in relation to the number of

    cycles between measurement and numerical calculation the tempered

    steel 42CrMo4 with hardness of 462 HV. A non-symmetrical load case

    at a constant extension ofDo/1.4% and a meanvalue ofomean/0.5%.

    Fig. 8. A comparison of plastic strain in relation to the number of

    cycles between measurement and numerical calculation for the

    normalised steel 42CrMo4 with hardness of 195 HV.

    Fig. 9. A comparison of plastic strain in relation to the number of

    cycles between measurement and numerical calculation for the

    tempered steel 42CrMo4 with hardness of 462 HV.

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    The experiments conducted to determine the low-

    cycle lifetime of sub-eutectoid steels have shown that the

    damage increment can also be determined with sufficient

    accuracy by indirectly observing the change in the

    modulus of elasticity.

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