Test Report. No. SHAHG1118138102 Date: 01 Dec · PDF filetest report.no. shahg1118138102 date: 01 dec 2011.page 1 of 12. ningbo you plastic industrial company limited. hengshan villiage,hongtang

Test Report. No. SHAHG1118138102 Date: 01 Dec 2011 . Page 1 of 12.

NINGBO YOU PLASTIC INDUSTRIAL COMPANY LIMITED .

HENGSHAN VILLIAGE,HONGTANG STREET,JIANBEI DISTRICT,NINGBO CITY,ZHEJIANG

PROVINCE,CHINA

.

.

The following sample(s) was/were submitted and identified on behalf of the clients as : TRITAN BOTTLE .

SGS Job No. : SHHG1111034452CW - SH .

Manufacturer : . NINGBO YOU PLASTIC INDUSTRIAL COMPANY LIMITED .

Country of Origin : . CHINA.

Style No. :. 900ML.

Client Ref. Information : . 350ML;600ML;700ML;800ML;Y-01001;Y-01004;Y-01002;Y-01005;Y-01003 .

Date of Sample Received : . 10 Nov 2011.

Testing Period : . 10 Nov 2011 - 01 Dec 2011 .

Test Requested : . Selected test(s) as requested by client. .

Test Method : . Please refer to next page(s). .

Test Results : . Please refer to next page(s). .

Signed for and on behalf of

SGS-CSTC Ltd. .

Wang Lini, Renee.

Approved Signatory . . .

0000567815


Test Results : .

Test Part Description : .

Specimen No.. SGS Sample ID. Description.

1. SHA11-181381.001 Bottle.

2. SHA11-181381.002 Light grey plastic lid .

3. SHA11-181381.003 Translucent plastic straw .

4. SHA11-181381.004 Pink transparent plastic body .

5. SHA11-181381.007 Translucent silicone rubber ring .

Overall migration.

Test Requested : . In accordance with German Food, Articles of Daily Use and Feed Code of September 1, 2005

(LFGB), Section 30 and 31, Commission Regulation (EU) No 10/2011 of 14 January 2011 and

BfR recommendation.

To determine Overall migration. .

Test Method : . For samples 002~003:

With reference to 82/711/EEC with its amendments and 2002/72/EC with its amendments for

selection of condition and EN1186-1:2002 for selection of test method;

EN1186-3:2002 aqueous food simulants by total immersion method;

For sample 004:

With reference to 82/711/EEC with its amendments and 2002/72/EC with its amendments for

selection of condition and EN1186-1:2002 for selection of test method;

EN1186-9:2002 aqueous food simulants by article filling method. .

Simulant Used. Time. Temperature. Max. Permissible

Limit.

Result of 002

Overall Migration

Deionized Water .. <20mg/kg..60mg/kg.70℃..24.0hr..

3% Acetic Acid (W/V)

Aqueous Solution ..

<20mg/kg..60mg/kg.70℃..24.0hr..


Limit.

Result of 003

Overall Migration

Deionized Water .. <3.0mg/dm²..10mg/dm²..70℃..24.0hr..


Aqueous Solution ..

<3.0mg/dm²..10mg/dm²..70℃..24.0hr..


Limit.

Result of 004

Overall Migration

0000567815


Deionized Water .. <20mg/kg..60mg/kg.70℃..24.0hr..


Aqueous Solution ..

<20mg/kg..60mg/kg.70℃..24.0hr..

Notes :.

(1) mg/dm²=milligram per square decimeter

(2) mg/kg = milligram per kilogram

(3) ℃=degree Celsius

(4) <= less than

(5) Analytical tolerance of aqueous simulants is 1 mg/dm² or 6mg/kg

(6) Test condition & simulant were specified by client. .

Extractable component.


(LFGB), Section 30 and 31, BfR recommendation.

To determine Extractable component .

Test Method : . With reference to 61st Communication on testing of plastics in Bundesgesundheitsbl

46 (2003) 362. .


Limit.

Result of 007

Extactives

Distilled water .. <0.1% (w/w)..0.5% (w/w).reflux

temperature..

5.0hr..

3% Acetic Acid .. 0.1% (w/w)..0.5% (w/w).reflux

temperature..

5.0hr..

Peroxide value.



To determine Peroxide value .

Test Method : . With reference to European pharmacopoeia, 2005 Appendix X F. Peroxide Value method A .

Test Item(s). Limit. 003. 004. 007.

Peroxide Value . Absent. Absent. Absent. Absent.

0000567815


Sensorial examination odour and taste test.



Sensorial examination odour and taste test .

Test Method : . Sensory test with reference to DIN 10955:1983 (2004).

Odour test condition: 23℃ 24 hours;

Taste test condition: 70℃ 24 hours;

Test media: Distilled water;

No.of panelist: 5 .

Test Item(s). Limit. 001.

Sensorial examination odour (Point scale) . 2.5. 0.

Sensorial examination taste (Point scale) . 2.5. 0.

Notes :.

Scale evaluation:

0: No perceptible odour

1: Odour just perceptible (still difficult to define)

2: Moderate odour

3: Moderately strong odour

4: Strong odour .

Specific Migration of Heavy Metal.



BfR recommendation.

To determine Specific Migration of Heavy Metal. .

Test Method : . With reference to 82/711/EEC with its amendments and 2002/72/EC with its amendments for

selection of condition and EN13130-1:2004 for selection of test method; analysis was performed by

ICP-OES..

Sample 002.

Simulant Used : . 3% Acetic Acid (W/V) Aqueous Solution ..

Test Condition : . 70.℃ 24.0.hr.

0000567815


MDLTest Item(s). Max. Permissible

Limit.

Unit. Test Result.

ND.0.25mg/kg.1Barium.

ND.0.05mg/kg.0.05Cobalt.

ND.0.25mg/kg.5Copper.

ND.0.25mg/kg.48Iron.

ND.0.5mg/kg.0.6Lithium.

ND.0.25mg/kg.0.6Manganese.

ND.0.5mg/kg.25Zinc.

Sample 003.




Limit.

Unit. Test Result.







ND.0.5mg/kg.25Zinc.

Sample 004.




Limit.

Unit. Test Result.







ND.0.5mg/kg.25Zinc.

Notes :

0000567815



(2) MDL = Method Detection Limit

(3) ND = Not Detected (< MDL)

(4) Test condition & simulant were specified by client. .

Chromium, Vanadium and Zirconium content.



BfR recommendation.

To determine Catalyst residue, Chromium, Vanadium and Zirconium content. .

Test Method : . Acid digestion, analysis was performed by ICP-OES. .

MDLTest Item(s). Limit. Unit. 002. 003.

Total Chromium. 10 mg/kg. 5 ND ND

Total Vanadium. 20 mg/kg. 20 ND ND

Total Zirconium. 100 mg/kg. 20 ND ND

Lead(Pb) and Cadmium(Cd).



To determine Lead(Pb) and Cadmium (Cd) content. .

Test Method : . Total Lead and Cadmium: Acidic digestion, analysis was performed by ICP-OES. .

MDLTest Item(s). Limit. Unit. 002. 003. 004.

Total Lead. Absent. mg/kg. 2 ND ND ND

Total Cadmium. Absent. mg/kg. 2 ND ND ND

MDLTest Item(s). Limit. Unit. 007.

Total Lead. Absent. mg/kg. 2 ND

Total Cadmium. Absent. mg/kg. 2 ND

Notes :.

0000567815




(3) ND = Not Detected ( < MDL) .

Volatile organic matter.



To determine Volatile organic matter (VOM) content .

Test Method : . With reference to 60. Mitteilung über die Untersuchung von Kunststoffen, Bundesgesundheitsbl 45

(2002) 462 and LFGB § 64 BVL B 80.30.1(EG).

Test condition : 70℃, 24 hours .


Volatile organic matter (VOM) . 0.5 % (w/w). 0.1 ND

Organotin content (Monobutyltin, Dibutyltin, Tributyltin, Tetrabutyltin, Triphenyltin, Mono-octyltin, Di-octyltin).



To determine Organotin content (Monobutyltin, Dibutyltin, Tributyltin, Tetrabutyltin, Triphenyltin,

Mono-octyltin, Di-octyltin). .

Test Method : . Solvent extraction followed by analysis using GC-MS. .


Monobutyl tin (MBT) . Absent. mg/kg. 0.02 ND

Dibutyl tin (DBT) . Absent. mg/kg. 0.02 ND

Tributyl tin (TBT) . Absent. mg/kg. 0.02 ND

Monooctyl tin (MOT) . Absent. mg/kg. 0.02 ND

Tetrabutyl tin (TTBT) . Absent. mg/kg. 0.02 ND

Dioctyl tin (DOT) . Absent. mg/kg. 0.02 ND

Triphenyl tin (TPT) . Absent. mg/kg. 0.02 ND

Notes :.

0000567815




(3) ND = Not Detected ( < MDL) .

Total Zinc, Lead content.



BfR recommendation.

For material: PET - Total Zinc, Lead content .

Test Method : . Acid digestion, followed by analysis using ICP-OES. .


Total Zinc. 1 %. 0.01 ND

Total Lead. 40 mg/kg. 5 ND

0000567815


Sample photo: .

SHAHG1118138102

SHA11-181381.001 .

SHAHG1118138102

SHA11-181381.002 .

0000567815


SHAHG1118138102

SHA11-181381.003 .

SHAHG1118138102

SHA11-181381.004 .

0000567815


SHAHG1118138102

SHA11-181381.005 .

SHAHG1118138102

.

0000567815


SHAHG1118138102

SHA11-181381.007 .

SGS authenticate the photo on original report only .

*** End of Report *** .

0000567815

Documents

Test Report. No. SHAHG1118138102 Date: 01 Dec · PDF filetest report.no. shahg1118138102 date: 01 dec 2011.page 1 of 12. ningbo you plastic industrial company limited. hengshan villiage,hongtang