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resultados del segundo experimento reactores UNAM CELE QUIMICA
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Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1.751 543.447 17.629 100 100 0.49Total 543.447 17.629 100 100 0.49
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)0.564 189.133 13.919 75.4 84.4 0.232.018 61.646 2.577 24.6 15.6 0.36Total 250.779 16.496 100 100 0.59
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)0.253 242.589 32.499 94.7 96.1 0.130.596 8.309 1.057 3.2 3.1 0.122.093 5.177 0.262 2 0.8 0.32Total 256.075 33.818 100 100 0.57
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)0.262 14.241 3.204 2.2 14.5 0.050.582 3.804 0.429 0.6 1.9 0.141.098 7.603 0.628 1.2 2.8 0.191.711 615.479 17.778 96 80.7 0.57Total 641.127 22.039 100 99.9 0.95
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)0.24 4.584 0.503 1.5 4 0.12
0.578 4.196 0.419 1.4 3.3 0.151.084 9.118 0.541 2.9 4.3 0.241.924 291.947 11.132 94.2 88.4 0.4Total 309.845 12.595 100 100 0.91
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)0.267 0.907 0.312 0.2 2 0.041.707 538.505 15.681 99.8 98 0.56Total 539.412 15.993 100 100 0.6
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1.707 549.488 15.596 100 100 0.58Total 549.488 15.596 100 100 0.58
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1.858 532.57 16.395 100 100 0.52Total 532.57 16.395 100 100 0.52
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1.796 509.615 15.173 100 100 0.54Total 509.615 15.173 100 100 0.54
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)0.267 1.713 0.226 0.5 1.7 0.1
1.849 372.076 13.216 99.5 98.3 0.44Total 373.789 13.442 100 100 0.54
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1.813 492.315 15.666 100 100 0.51Total 492.315 15.666 100 100 0.51
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1.831 498.046 15.999 100 100 0.5Total 498.046 15.999 100 100 0.5
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1.796 483.163 15.007 100 100 0.52Total 483.163 15.007 100 100 0.52
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1.809 593.193 17.209 100 100 0.56Total 593.193 17.209 100 100 0.56
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)0.28 0.822 0.241 0.2 1.5 0.05
1.778 538.207 16.147 99.8 98.5 0.54Total 539.029 16.388 100 100 0.59
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)0.28 1.95 0.291 0.8 2.9 0.1
1.996 253.124 9.843 99.2 97.1 0.4Total 255.074 10.134 100 100 0.5
Compuesto Tiempo de retención Tiempo de reacción Area %Ác. Acético 0.264142857142857 3 0
6 010 94.715 2.220 1.525 0.230 035 040 050 0.260 0.8
Compuesto Tiempo de retención Tiempo de reacción Area %Etilenglicol 0.58 3 0
6 75.410 3.215 0.620 1.425 030 035 040 050 060 0
Compuesto Tiempo de retención Tiempo de reacción Area %Monoacetato 1.091 3 0
6 010 015 1.220 2.925 030 035 040 050 060 0
Compuesto Tiempo de retención Tiempo de reacción Area %DAEG 1.82392857142857 3 100
6 24.610 215 9620 94.225 99.830 100
35 10040 10050 99.560 100
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EtilenglicolÁcido aceticoMonoacetato de etilenglicolDiacetato de etilenglicol
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asa
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.28 53.967 11.291 5.2 22 0.062 0.609 5.633 0.786 0.5 1.5 0.113 1.116 66.24 5.767 6.4 11.2 0.184 1.804 909.552 33.542 87.8 65.3 0.4
Total 1035.392 51.386 100 100
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.284 139.534 28.294 11 35.6 0.082 0.618 21.669 2.823 1.7 3.6 0.123 1.124 207.454 16.323 16.4 20.5 0.24 1.849 895.16 32.059 70.8 40.3 0.41
Total 1263.817 79.499 99.9 100
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.289 157.992 35.56 14.3 41.3 0.072 0.618 31.81 4.617 2.9 5.4 0.13 1.12 273.222 21.225 24.7 24.6 0.194 1.92 643.189 24.717 58.1 28.7 0.39
Total 1106.213 86.119 100 100
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.289 177.733 35.464 16.9 43.8 0.062 0.618 40.288 4.925 3.8 6.1 0.113 1.129 315.477 21.294 30 26.3 0.224 1.982 516.563 19.284 49.2 23.8 0.4
Total 1050.061 80.967 99.9 100
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.289 210.914 35.343 18.5 42.1 0.062 0.622 51.931 5.583 4.6 6.7 0.163 1.142 350.242 23.156 30.8 27.6 0.234 2 523.982 19.82 46.1 23.6 0.4
Total 1137.069 83.902 100 100
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.284 214.626 42.493 16.9 41.2 0.082 0.622 65.709 9.05 5.2 8.8 0.113 1.111 406.284 29.181 32.1 28.3 0.214 1.951 580.662 22.36 45.8 21.7 0.39
Total 1267.281 103.084 100 100
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.258 236.272 39.826 19.4 41.9 0.072 0.591 64.822 7.759 5.3 8.2 0.133 1.098 391.962 26.747 32.2 28.2 0.234 1.951 525.963 20.68 43.1 21.8 0.39
Total 1219.019 95.012 100 100.1
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.267 264.533 39.574 18.7 38.7 0.12 0.596 79.133 9.322 5.6 9.1 0.123 1.084 452.262 30.362 32 29.7 0.234 1.929 617.427 23.072 43.7 22.5 0.4
Total 1413.355 102.330 100 100
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.262 217.865 37.861 21.2 44.5 0.072 0.6 70.316 8.15 6.8 9.6 0.143 1.116 349.78 23.798 34 28 0.224 2.004 390.471 15.324 38 18 0.38
Total 1028.432 85.133 100 100.1
Reten. Time(min) Area (mvs) Height (mv) Area % Height % W05(min)1 0.253 233.873 33.989 64.3 84.9 0.112 1.164 38.108 2.289 10.5 5.7 0.243 2.12 91.974 3.759 25.3 9.4 0.37
Total 363.955 40.037 100.1 100
Compuesto Tiempo de retención Tiempo de reacción Area %Ác. Acético 0.2755 5 5.2
10 1115 14.320 16.925 18.530 16.940 19.450 18.760 21.2
Compuesto Tiempo de retención Tiempo de reacción Area %Etilenglicol 0.610 5 0.5
10 1.715 2.920 3.825 4.630 5.240 5.350 5.660 6.8
Compuesto Tiempo de retención Tiempo de reacción Area %Monoacetato 1.120 5 6.4
10 16.415 24.720 3025 30.830 32.140 32.250 3260 34
Compuesto Tiempo de retención Tiempo de reacción Area %DAEG 1.951 5 87.8
10 70.815 58.120 49.225 46.130 45.840 43.150 43.7
60 38
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Monoacetato de etilenglicolDAEGEtilenglicolác acético
Tiempo(min)
%m
