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POLLEN ENVIRONMENTAL, LLC. CHAIN OF CUSTODY /WORKORDER FORM 3536 International Street
Fairbanks, AK 99701
(907) 479-8368 Phone (907) 452-6853 Fax
CLIENT INFORMATION
Company: Barrow Utilities & Electric Coop.
Address: P.O. Box 449
City, State Zip: Barrow, AK 99723
Phone: 907-852-8427
Fax: 907-852-5164
Email: [email protected]
Project Name: PFC Monitoring
Sampled By: --15w\ n r-.-:..~a, ll=
Contact Person: Jim Murphy
Perservatlve Added
WWTP APDES #:
PWS ID #: 320078
Send Results to ADEC:
v Yes □ No (/}
0 Purchase Order/Charge Code: 20190015 LL
c..
c?0\9-53 ~ <( 0 LL c..
Samole Identification Samole Point ID: Samole Date Samole Time Matrix Lab ID# Sub Lab ID#
Raw Water Tao SPIN0001 1t1,rh9 I ~ \ 17 .) w ~vf4l0ii, 2 X
MG Tank SPTP0001 /Jtrll Ci i4 '. S"'<l w (~rf6t'JJ 2 X
Possible Hazard Identification: Sample Co:!{11'
□ Non-Hazardous □ Flammable D Skin Irritant □ Unknown Pollen Env Temperature on arrival: •c Sub Lab Temperature on arrival: _ _ •c
Special Instructions/QC Requirements & Comments:
Requested Analysis
CDC Seal:
CDC Seal:
~(nquished by: Comt y: [ Daj e; f ;nq I ( '1, :1 -~ffltloA tnr\fVNii(ii Company: Pollen Env.
"l'i,..,,\ ,,, ~ - ,(11 GC. Relio;;»;J:f ~ 7 Compan%//UJ cm/ Date & Timei i &,
,-r~✓ J/00 Ret:elved by : ~ Company:
RJ/quis~ by: Company: Date & Time: Received by : Company:
Accuracy, Precision, and Professional Service
COC# BUECI PFC
Page 1 of 1
\ Normal Turnaround
D RUSH - day(s)
Samole Comments
□ Intact □ Broken □ Absent
□ Intact □ Broken □ Absent
Df1e\~f\eq tO)l0 Daile & Time:
Date & Time:
Barrow Utilities and Electric Coop. Report Date: 1/29/2019Attn: Jim Murphy Receipt Date: 1/16/2019PO Box 449 Sampled By: Tom Drake IIBarrow, AK 99723Phone: (907) 852-5164Fax: (907) 852-6751E-mail: [email protected]
Project Name: PFOA and PFOS MonitoringSampled By: Tom Drake IIPWS ID: 320078
Sample ID: Pollen Env ID: Eurofins ID: Date: Time:
Raw Water Tap PEF46821 1/15/2019 3:00 PMMG Tank PEF46822 1/15/2019 2:58 PM
Jerry PollenPollen Environmental, LLC - Fairbanks
CERTIFICATE OF ANALYSIS
41774754177476
Pollen Environmental, LLC
LABORATORY REPORT
This report may not be reproduced, except in full, without written approval from EEA.
If you have any questions concerning this report, please do not hesitate to call us at (800) 332-4345 or (574) 233-4777.
Page 1 of 11
=::: e u rofi n s I Eaton Analytical
Revision date: 01/02/2018
STATE CERTIFICATION LIST
State Certification State Certification Alabama 40700 Missouri 880 Alaska IN00035 Montana CERT0026 Arizona AZ0432 Nebraska NE-OS-05-04
Arkansas IN00035 Nevada IN00035 California 2920 New Hampshire* 2124 Colorado IN035 New Jersey* IN598
Colorado Radiochemistry IN035 New Mexico IN00035 Connecticut PH-0132 New York* 11398 Delaware IN035 North Carolina 18700 Florida* E87775 North Dakota R-035 Georgia 929 Ohio 87775 Hawaii IN035 Oklahoma D9508 Idaho IN00035 Oregon (Primary AB)* 4074-001
Illinois* 200001 Pennsylvania* 68-00466 Illinois Microbiology 17767 Puerto Rico IN00035
Illinois Radiochemistry IN00035 Rhode Island LAO00343 Indiana Chemistry C-71-01 South Carolina 95005
Indiana Microbiology M-76-07 South Dakota IN00035 Iowa 098 Tennessee TN02973
Kansas* E-10233 Texas* T104704187-15-8Kentucky 90056 Texas/TCEQ TX207
Louisiana* LA180008 Utah* IN00035 Maine IN00035 Vermont VT-8775
Maryland 209 Virginia* 460275 Massachusetts M-IN035 Washington C837
Michigan 9926 West Virginia 9927 C Minnesota* 018-999-338 Wisconsin 999766900 Mississippi IN035 Wyoming IN035
EPA IN00035 *NELAP/TNI Recognized Accreditation Bodies
Page 2 of 11
·=- eurofins I t Analytical -:.• Ea on
Laboratory Report
Client:
Attn:
Report:
Priority:
Status:
PWS ID:
Pollen Environmental LLC
Jerry Pollen
3536 International Avenue
441145
AK2320078
Standard Written
Final
IN00035Alaska Lab ID #
Fairbanks, AK 99701
110 South Hill StreetSouth Bend, IN 46617Tel: (574) 233-4777Fax: (574) 233-82071 800 332 4345
*NR = The chlorine demand was not performed for this analytical sample, at the request of the client.
EEA ID #
Client ID Method CollectedDate / Time
CollectedBy:
ReceivedDate / Time
4177475 PEF46821 Raw Water Tap 537 01/15/19 15:00 Client 01/18/19 08:30
4177476 PEF46822 MG Tank 537 01/15/19 14:58 Client 01/18/19 08:30
Sample Information
Report Summary
Detailed quantitative results are presented on the following pages. The results presented relate only to the samples provided for analysis.
We appreciate the opportunity to provide you with this analysis. If you have any questions concerning this report, please do not hesitate to call Traci Chlebowski at (574) 233-4777.
Note: This report may not be reproduced, except in full, without written approval from EEA.
Client Name:
Report #:
Pollen Environmental LLC
441145
Authorized Signature Title Date
01/29/2019
Page 1 of 3
Page 3 of 11
=:~ eurofins I Eaton Analytical
Client Name: Report #: 441145Pollen Environmental LLC
Sampling Point: PWS ID:PEF46821 Raw Water Tap AK2320078
EEA Methods
AnalyteID #
Analyte Method RegLimit
MRL† Result Units Preparation Date
AnalyzedDate
EEAID #
417747501/24/19 01:3701/23/19 07:30ng/L812.0---537Perfluorooctanesulfonic acid (PFOS)1763-23-1
417747501/24/19 01:3701/23/19 07:30ng/L7.22.0---537Perfluorooctanoic acid (PFOA)335-67-1
Sampling Point: PWS ID:PEF46822 MG Tank AK2320078
EEA Methods
AnalyteID #
Analyte Method RegLimit
MRL† Result Units Preparation Date
AnalyzedDate
EEAID #
417747601/24/19 01:5401/23/19 07:30ng/L< 2.02.0---537Perfluorooctanesulfonic acid (PFOS)1763-23-1
417747601/24/19 01:5401/23/19 07:30ng/L< 2.02.0---537Perfluorooctanoic acid (PFOA)335-67-1
Reg Limit Type:
Symbol:
MCL SMCL AL
* ^ !
† EEA has demonstrated it can achieve these report limits in reagent water, but can not document them in all sample matrices.
Page 2 of 3Page 4 of 11
B I I
B I I
Client Name: Report #: 441145Pollen Environmental LLC
Lab Definitions
Continuing Calibration Check Standard (CCC) / Continuing Calibration Verification (CCV) / Initial Calibration Verification Standard (ICV) / Initial Performance Check (IPC) - is a standard containing one or more of the target analytes that is prepared from the same standards used to calibrate the instrument. This standard is used to verify the calibration curve at the beginning of each analytical sequence, and may also be analyzed throughout and at the end of the sequence. The concentration of continuing standards may be varied, when prescribed by the reference method, so that the range of the calibration curve is verified on a regular basis. CCL, CCM, and CCH are the CCC standards at low, mid, and high concentration levels, respectively.
Internal Standards (IS) - are pure compounds with properties similar to the analytes of interest, which are added to field samples or extracts, calibration standards, and quality control standards at a known concentration. They are used to measure the relative responses of the analytes of interest and surrogates in the sample, calibration standard or quality control standard.
Laboratory Duplicate (LD) - is a field sample aliquot taken from the same sample container in the laboratory and analyzed separately using identical procedures. Analysis of laboratory duplicates provides a measure of the precision of the laboratory procedures.
Laboratory Fortified Blank (LFB) / Laboratory Control Sample (LCS) - is an aliquot of reagent water to which known concentrations of the analytes of interest are added. The LFB is analyzed exactly the same as the field samples. LFBs are used to determine whether the method is in control. FBL, FBM, and FBH are the LFB samples at low, mid, and high concentration levels, respectively.
Laboratory Method Blank (LMB) / Laboratory Reagent Blank (LRB) - is a sample of reagent water included in the sample batch analyzed in the same way as the associated field samples. The LMB is used to determine if method analytes or other background contamination have been introduced during the preparation or analytical procedure. The LMB is analyzed exactly the same as the field samples.
Laboratory Trip Blank (LTB) / Field Reagent Blank (FRB) - is a sample of laboratory reagent water placed in a sample container in the laboratory and treated as a field sample, including storage, preservation, and all analytical procedures. The FRB/LTB container follows the collection bottles to and from the collection site, but the FRB/LTB is not opened at any time during the trip. The FRB/LTB is primarily a travel blank used to verify that the samples were not contaminated during shipment.
Matrix Spike Duplicate Sample (MSD) / Laboratory Fortified Sample Matrix Duplicate (LFSMD) - is a sample aliquot taken from the same field sample source as the Matrix Spike Sample to which known quantities of the analytes of interest are added in the laboratory. The MSD is analyzed exactly the same as the field samples. Analysis of the MSD provides a measure of the precision of the laboratory procedures in a specific matrix. SDL, SDM, and SDH / LFSMDL, LFSMDM, and LFSMDH are the MSD or LFSMD at low, mid, and high concentration levels, respectively.
Matrix Spike Sample (MS) / Laboratory Fortified Sample Matrix (LFSM) - is a sample aliquot taken from field sample source to which known quantities of the analytes of interest are added in the laboratory. The MS is analyzed exactly the same as the field samples. The purpose is to demonstrate recovery of the analytes from a sample matrix to determine if the specific matrix contributes bias to the analytical results. MSL, MSM, and MSH / LFSML, LFSMM, and LFSMH are the MS or LFSM at low, mid, and high concentration levels, respectively.
Quality Control Standard (QCS) / Second Source Calibration Verification (SSCV) - is a solution containing known concentrations of the analytes of interest prepared from a source different from the source of the calibration standards. The solution is obtained from a second manufacturer or lot if the lot can be demonstrated by the manufacturer as prepared independently from other lots. The QCS sample is analyzed using the same procedures as field samples. The QCS is used as a check on the calibration standards used in the method on a routine basis.
Reporting Limit Check (RLC) / Initial Calibration Check Standard (ICCS) - is a procedural standard that is analyzed each day to evaluate instrument performance at or below the minimum reporting limit (MRL).
Surrogate Standard (SS) / Surrogate Analyte (SUR) - is a pure compound with properties similar to the analytes of interest, which is highly unlikely to be found in any field sample, that is added to the field samples, calibration standards, blanks and quality control standards before sample preparation. The SS is used to evaluate the efficiency of the sample preparation process.
Page 3 of 3Page 5 of 11
Page 6 of 11
E NVIRONMENTAL, LLC. 3536 International Street
Fairbanks, AK 99701
(907) 479-8368 Phone (907) 452-6853 Fax
CLIENT INFORMATION
Company: Barrow Utilities & Electric Coop.
Address: P.O. Box 449
City, State Zip: Barrow, AIC 99723
Phone: 907-852-8427
Fax: 907-852-5164
Contact Person : Jim Murphy
WWTP APDES # :
PWS ID #: 320078
Send Results to ADEC:
v Yes D No
4~\\~s CHAIN OF USTO Y /WORKORDE FORM
3-e; I 012. c:oc ur:c1 p c
Requested Analysis
Page 1 of 1
Perservative Added
\ Normal Turnaround
U) 0
Email: [email protected] Purchase Order/Charge Code: 20190015 LL. D RUSH --day(s) c..
Project Name: PFC Monitoring J0\9·-53 cxS <(
Sampled By: -- . 0 l-8w\ 1Jr-.:..~ll- rJ: LL.
c.. Sample Identification Samnle Point I D: Samnle Date Samnle Tim• Matrix Lab ID# Sub Lab I D# Samnle Comments
Raw Water Tao SPIN0001 i /L')IL9 I >'·o .1 w -PvfAij?ii\ 411,41c; 2 xl ) C '-A .... i\ MG Tank SPTP0001 J/1rl1.C1 i'-1 '. i'l w i W\\ntfL1 L-frn 1.J.11 .. 2 xl ) (!_ '-It )ss1 1ttt
Possible Hazard Identification: Sample Co% W
□ Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temperature on arrival: _ °C COC Seal : □ Intact D Broken D Absent
Sub Lab Temperature on arrival : I 0c coc Seal : ( i ntact D Broken D Absent
Special Instructions/QC Requirements & Comments:
Relinquished by: l'i"''i)r-,A:,/J_ u:,_
Com1«1ny: \S,1,, Gt I
Dati & T!LJe: I J(' .le, ,c1 ~ -~M~ ~foA ti)(j/VMVi1
Company: Pollen Env. Df1e\t l~°b\ - l01IO Rell"fp}'Jt)1~ 7 Companf(}/; rn11 Date & Tlmei i (B_ //()0
Re~ ve ~' Q.,( ~ Compan~G/.J- oar-,. Pl,~ Ot80 0 Ul /-- /7- .,,. >5 ,., I
RJ/quls"(f by: Company: Date & Time: Recelv~ u Company: Date & Time:
Accuracy, Precision, and Professional Service
Eurofins Eaton AnalyticalRun Log
Run ID: 254373 Method: 537
Sample SiteSample IdType Instrument ID Calibration FileAnalysis DateMatrix
CCL 4180605 FL 012319M537a-FL-PFC-Ext.mdb01/23/2019 19:40OS
LRB 4180592 FL 012319M537a-FL-PFC-Ext.mdb01/23/2019 20:14RW
FBL 4180595 FL 012319M537a-FL-PFC-Ext.mdb01/23/2019 20:48RW
CCM 4180606 FL 012319M537a-FL-PFC-Ext.mdb01/24/2019 00:29OS
FS 4177475 PEF46821 Raw Water Tap FL 012319M537a-FL-PFC-Ext.mdb01/24/2019 01:37DW
FS 4177476 PEF46822 MG Tank FL 012319M537a-FL-PFC-Ext.mdb01/24/2019 01:54DW
CCH 4180609 FL 012319M537a-FL-PFC-Ext.mdb01/24/2019 03:52OS
0.00
Page 1 of 3 EEA Run ID 254373 / EEA Report # 441145
Page 7 of 11
=::: e u rof i n s I Eaton Analytical
QC
Su
mm
ary
Re
po
rt
EE
AID
#R
PD
Un
its
Ta
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L1
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/L1
.04
18
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05
---
---
---
50
- 1
50
10
01
02
33
90
0
1/1
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01
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30
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3/2
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9 1
9:4
0F
als
e
IS-P
FO
A-1
3C
2537
N/A
CC
L1
83
02
80
.00
ng
/L1
.04
18
06
05
---
---
---
50
- 1
50
10
01
83
02
80
0
1/1
4/2
01
9 1
0:3
30
1/2
3/2
01
9 1
9:4
0F
als
e
IS-P
FO
S-1
3C
4537
N/A
CC
L4
01
40
6.0
0ng
/L1
.04
18
06
05
---
---
---
50
- 1
50
10
04
01
40
6
01
/14
/20
19
10
:33
01
/23
/20
19
19
:40
Fals
e
IS-G
enX
-13C
3537
N/A
CC
L1
82
40
1.0
0ng
/L1
.04
18
06
05
---
---
---
50
- 1
50
10
01
82
40
1
01
/14
/20
19
10
:33
01
/23
/20
19
19
:40
Fals
e
SS
-NE
tFO
SA
A-d
5537
N/A
CC
L2
01
.51
20
ng
/L1
.04
18
06
05
---
---
---
70
- 1
30
10
12
00
0
1/1
4/2
01
9 1
0:3
30
1/2
3/2
01
9 1
9:4
0F
als
e
SS
-PF
DA
-13C
2537
N/A
CC
L9
9.7
98
1ng
/L1
.04
18
06
05
---
---
---
70
- 1
30
10
01
00
0
1/1
4/2
01
9 1
0:3
30
1/2
3/2
01
9 1
9:4
0F
als
e
SS
-PF
HxA
-13C
2537
N/A
CC
L4
9.4
67
2ng
/L1
.04
18
06
05
---
---
---
70
- 1
30
99
50
.0
01
/14
/20
19
10
:33
01
/23
/20
19
19
:40
Fals
e
Perf
luoro
oct
anesu
lfonic
aci
d (
PF
OS
)537
2.0
CC
L2
.00
75
ng
/L1
.04
18
06
05
---
---
---
50
- 1
50
10
02
.0
01
/14
/20
19
10
:33
01
/23
/20
19
19
:40
Fals
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
CC
L1
.91
52
ng
/L1
.04
18
06
05
---
---
---
50
- 1
50
96
2.0
0
1/1
4/2
01
9 1
0:3
30
1/2
3/2
01
9 1
9:4
0T
rue
IS-N
MeF
OS
AA
-d3
537
N/A
LR
B1
01
38
10
.00
ng
/L0
.91
41
80
59
2--
---
---
-5
0 -
15
09
91
02
33
90
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:1
4T
rue
IS-P
FO
A-1
3C
2537
N/A
LR
B1
79
87
50
.00
ng
/L0
.91
41
80
59
2--
---
---
-5
0 -
15
09
81
83
02
80
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:1
4T
rue
IS-P
FO
S-1
3C
4537
N/A
LR
B3
87
83
5.0
0ng
/L0
.91
41
80
59
2--
---
---
-5
0 -
15
09
74
01
40
6
01
/23
/20
19
07
:30
01
/23
/20
19
20
:14
Tru
e
IS-G
enX
-13C
3537
N/A
LR
B1
80
64
9.0
0ng
/L0
.91
41
80
59
2--
---
---
-5
0 -
15
09
91
82
40
1
01
/23
/20
19
07
:30
01
/23
/20
19
20
:14
Tru
e
SS
-NE
tFO
SA
A-d
5537
N/A
LR
B1
63
.86
50
ng
/L0
.91
41
80
59
2--
---
---
-7
0 -
13
09
02
00
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:1
4T
rue
SS
-PF
DA
-13C
2537
N/A
LR
B8
7.4
81
3ng
/L0
.91
41
80
59
2--
---
---
-7
0 -
13
09
61
00
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:1
4T
rue
SS
-PF
HxA
-13C
2537
N/A
LR
B4
4.9
65
7ng
/L0
.91
41
80
59
2--
---
---
-7
0 -
13
09
95
0.0
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:1
4T
rue
Perf
luoro
oct
anesu
lfonic
aci
d (
PF
OS
)537
2.0
LR
B2
.0ng
/L0
.91
41
80
59
2--
---
---
---
---
-
<0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:1
4T
rue
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
LR
B2
.0ng
/L0
.91
41
80
59
2--
---
---
---
---
-
<0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:1
4F
als
e
IS-N
MeF
OS
AA
-d3
537
N/A
FB
L9
60
25
7.0
0ng
/L1
.04
18
05
95
---
---
---
50
- 1
50
94
10
23
39
0
01
/23
/20
19
07
:30
01
/23
/20
19
20
:48
Fals
e
IS-P
FO
A-1
3C
2537
N/A
FB
L1
73
04
50
.00
ng
/L1
.04
18
05
95
---
---
---
50
- 1
50
95
18
30
28
0
01
/23
/20
19
07
:30
01
/23
/20
19
20
:48
Fals
e
IS-P
FO
S-1
3C
4537
N/A
FB
L3
74
73
9.0
0ng
/L1
.04
18
05
95
---
---
---
50
- 1
50
93
40
14
06
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:4
8F
als
e
IS-G
enX
-13C
3537
N/A
FB
L1
71
31
5.0
0ng
/L1
.04
18
05
95
---
---
---
50
- 1
50
94
18
24
01
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:4
8F
als
e
SS
-NE
tFO
SA
A-d
5537
N/A
FB
L1
94
.88
60
ng
/L1
.04
18
05
95
---
---
---
70
- 1
30
97
20
0
01
/23
/20
19
07
:30
01
/23
/20
19
20
:48
Fals
e
SS
-PF
DA
-13C
2537
N/A
FB
L1
01
.36
00
ng
/L1
.04
18
05
95
---
---
---
70
- 1
30
10
11
00
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:4
8F
als
e
SS
-PF
HxA
-13C
2537
N/A
FB
L5
1.3
78
4ng
/L1
.04
18
05
95
---
---
---
70
- 1
30
10
35
0.0
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:4
8F
als
e
Perf
luoro
oct
anesu
lfonic
aci
d (
PF
OS
)537
2.0
FB
L1
.77
88
ng
/L1
.04
18
05
95
---
---
---
50
- 1
50
89
2.0
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:4
8F
als
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
FB
L1
.80
97
ng
/L1
.04
18
05
95
---
---
---
50
- 1
50
90
2.0
0
1/2
3/2
01
9 0
7:3
00
1/2
3/2
01
9 2
0:4
8T
rue
IS-N
MeF
OS
AA
-d3
537
N/A
CC
M9
30
52
0.0
0ng
/L1
.04
18
06
06
---
---
---
50
- 1
50
10
09
30
52
0
01
/14
/20
19
10
:33
01
/24
/20
19
00
:29
Tru
e
IS-P
FO
A-1
3C
2537
N/A
CC
M1
63
45
80
.00
ng
/L1
.04
18
06
06
---
---
---
50
- 1
50
10
01
63
45
80
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
0:2
9T
rue
IS-P
FO
S-1
3C
4537
N/A
CC
M3
53
04
0.0
0ng
/L1
.04
18
06
06
---
---
---
50
- 1
50
10
03
53
04
0
01
/14
/20
19
10
:33
01
/24
/20
19
00
:29
Tru
e
IS-G
enX
-13C
3537
N/A
CC
M1
62
28
9.0
0ng
/L1
.04
18
06
06
---
---
---
50
- 1
50
10
01
62
28
9
01
/14
/20
19
10
:33
01
/24
/20
19
00
:29
Tru
e
SS
-NE
tFO
SA
A-d
5537
N/A
CC
M2
06
.51
90
ng
/L1
.04
18
06
06
---
---
---
70
- 1
30
10
32
00
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
0:2
9T
rue
SS
-PF
DA
-13C
2537
N/A
CC
M1
02
.10
00
ng
/L1
.04
18
06
06
---
---
---
70
- 1
30
10
21
00
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
0:2
9T
rue
SS
-PF
HxA
-13C
2537
N/A
CC
M4
9.9
26
4ng
/L1
.04
18
06
06
---
---
---
70
- 1
30
10
05
0.0
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
0:2
9T
rue
Perf
luoro
oct
anesu
lfonic
aci
d (
PF
OS
)537
2.0
CC
M1
04
.59
60
ng
/L1
.04
18
06
06
---
---
---
70
- 1
30
10
51
00
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
0:2
9T
rue
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
CC
M1
03
.84
70
ng
/L1
.04
18
06
06
---
---
---
70
- 1
30
10
41
00
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
0:2
9F
als
e
IS-N
MeF
OS
AA
-d3
537
N/A
FS
92
24
53
.00
ng
/L0
.88
41
77
47
5P
EF
46
82
1 R
aw
Wa
ter
Ta
p--
---
-5
0 -
15
09
99
30
52
0
01
/23
/20
19
07
:30
01
/24
/20
19
01
:37
Fals
e
IS-P
FO
A-1
3C
2537
N/A
FS
16
84
47
0.0
0ng
/L0
.88
41
77
47
5P
EF
46
82
1 R
aw
Wa
ter
Ta
p--
---
-5
0 -
15
01
03
16
34
58
0
01
/23
/20
19
07
:30
01
/24
/20
19
01
:37
Fals
e
IS-P
FO
S-1
3C
4537
N/A
FS
36
27
24
.00
ng
/L0
.88
41
77
47
5P
EF
46
82
1 R
aw
Wa
ter
Ta
p--
---
-5
0 -
15
01
03
35
30
40
0
1/2
3/2
01
9 0
7:3
00
1/2
4/2
01
9 0
1:3
7F
als
e
IS-G
enX
-13C
3537
N/A
FS
18
22
93
.00
ng
/L0
.88
41
77
47
5P
EF
46
82
1 R
aw
Wa
ter
Ta
p--
---
-5
0 -
15
011
21
62
28
9
01
/23
/20
19
07
:30
01
/24
/20
19
01
:37
Page 2
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3E
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Run I
D 2
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A R
eport
# 4
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45
Page 8 of 11
~ ~
D D DJ D
□□□□--□□--□--□ DODD □--□--□□--□--□
Sa
mp
leTyp
eE
EA
ID #
An
aly
zed
Ex
tra
cte
dR
PD
Un
its
Ta
rge
tA
mo
un
tC
lie
nt
IDM
RL
Me
tho
dA
na
lyte
Dil
Fa
cto
rR
PD
Lim
itR
ec
ove
ryL
imit
s%
R
ec
ove
ryR
es
ult
Fla
g
QC
Su
mm
ary
Rep
ort
(co
nt.
)
Fals
e
SS
-NE
tFO
SA
A-d
5537
N/A
FS
16
7.8
33
0ng
/L0
.88
41
77
47
5P
EF
46
82
1 R
aw
Wa
ter
Ta
p--
---
-7
0 -
13
09
52
00
0
1/2
3/2
01
9 0
7:3
00
1/2
4/2
01
9 0
1:3
7F
als
e
SS
-PF
DA
-13C
2537
N/A
FS
88
.74
34
ng
/L0
.88
41
77
47
5P
EF
46
82
1 R
aw
Wa
ter
Ta
p--
---
-7
0 -
13
01
01
10
0
01
/23
/20
19
07
:30
01
/24
/20
19
01
:37
Fals
e
SS
-PF
HxA
-13
C2
537
N/A
FS
46
.02
98
ng
/L0
.88
41
77
47
5P
EF
46
82
1 R
aw
Wa
ter
Ta
p--
---
-7
0 -
13
01
05
50
.0
01
/23
/20
19
07
:30
01
/24
/20
19
01
:37
Fals
e
Perf
luoro
oct
anesu
lfonic
aci
d (
PF
OS
)537
2.0
FS
81
ng
/L0
.88
41
77
47
5P
EF
46
82
1 R
aw
Wa
ter
Ta
p--
---
---
---
-
0
1/2
3/2
01
9 0
7:3
00
1/2
4/2
01
9 0
1:3
7F
als
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
FS
7.2
ng
/L0
.88
41
77
47
5P
EF
46
82
1 R
aw
Wa
ter
Ta
p--
---
---
---
-
0
1/2
3/2
01
9 0
7:3
00
1/2
4/2
01
9 0
1:3
7T
rue
IS-N
MeF
OS
AA
-d3
537
N/A
FS
88
17
08
.00
ng
/L0
.94
17
74
76
PE
F4
68
22
MG
Ta
nk
---
---
50
- 1
50
95
93
05
20
0
1/2
3/2
01
9 0
7:3
00
1/2
4/2
01
9 0
1:5
4T
rue
IS-P
FO
A-1
3C
2537
N/A
FS
15
37
40
0.0
0ng
/L0
.94
17
74
76
PE
F4
68
22
MG
Ta
nk
---
---
50
- 1
50
94
16
34
58
0
01
/23
/20
19
07
:30
01
/24
/20
19
01
:54
Tru
e
IS-P
FO
S-1
3C
4537
N/A
FS
33
44
85
.00
ng
/L0
.94
17
74
76
PE
F4
68
22
MG
Ta
nk
---
---
50
- 1
50
95
35
30
40
0
1/2
3/2
01
9 0
7:3
00
1/2
4/2
01
9 0
1:5
4T
rue
IS-G
enX
-13C
3537
N/A
FS
15
58
04
.00
ng
/L0
.94
17
74
76
PE
F4
68
22
MG
Ta
nk
---
---
50
- 1
50
96
16
22
89
0
1/2
3/2
01
9 0
7:3
00
1/2
4/2
01
9 0
1:5
4T
rue
SS
-NE
tFO
SA
A-d
5537
N/A
FS
17
0.9
09
0ng
/L0
.94
17
74
76
PE
F4
68
22
MG
Ta
nk
---
---
70
- 1
30
95
20
0
01
/23
/20
19
07
:30
01
/24
/20
19
01
:54
Tru
e
SS
-PF
DA
-13C
2537
N/A
FS
91
.71
57
ng
/L0
.94
17
74
76
PE
F4
68
22
MG
Ta
nk
---
---
70
- 1
30
10
21
00
0
1/2
3/2
01
9 0
7:3
00
1/2
4/2
01
9 0
1:5
4T
rue
SS
-PF
HxA
-13
C2
537
N/A
FS
45
.99
39
ng
/L0
.94
17
74
76
PE
F4
68
22
MG
Ta
nk
---
---
70
- 1
30
10
25
0.0
0
1/2
3/2
01
9 0
7:3
00
1/2
4/2
01
9 0
1:5
4T
rue
Perf
luoro
oct
anesu
lfonic
aci
d (
PF
OS
)537
2.0
FS
2.0
ng
/L0
.94
17
74
76
PE
F4
68
22
MG
Ta
nk
---
---
---
---
<
01
/23
/20
19
07
:30
01
/24
/20
19
01
:54
Tru
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
FS
2.0
ng
/L0
.94
17
74
76
PE
F4
68
22
MG
Ta
nk
---
---
---
---
<
01
/23
/20
19
07
:30
01
/24
/20
19
01
:54
Fals
e
IS-N
MeF
OS
AA
-d3
537
N/A
CC
H9
55
84
4.0
0ng
/L1
.04
18
06
09
---
---
---
50
- 1
50
10
09
55
84
4
01
/14
/20
19
10
:33
01
/24
/20
19
03
:52
Fals
e
IS-P
FO
A-1
3C
2537
N/A
CC
H1
64
64
90
.00
ng
/L1
.04
18
06
09
---
---
---
50
- 1
50
10
01
64
64
90
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
3:5
2F
als
e
IS-P
FO
S-1
3C
4537
N/A
CC
H3
55
39
4.0
0ng
/L1
.04
18
06
09
---
---
---
50
- 1
50
10
03
55
39
4
01
/14
/20
19
10
:33
01
/24
/20
19
03
:52
Fals
e
IS-G
enX
-13C
3537
N/A
CC
H1
61
09
1.0
0ng
/L1
.04
18
06
09
---
---
---
50
- 1
50
10
01
61
09
1
01
/14
/20
19
10
:33
01
/24
/20
19
03
:52
Fals
e
SS
-NE
tFO
SA
A-d
5537
N/A
CC
H1
97
.63
70
ng
/L1
.04
18
06
09
---
---
---
70
- 1
30
99
20
0
01
/14
/20
19
10
:33
01
/24
/20
19
03
:52
Fals
e
SS
-PF
DA
-13C
2537
N/A
CC
H1
01
.23
50
ng
/L1
.04
18
06
09
---
---
---
70
- 1
30
10
11
00
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
3:5
2F
als
e
SS
-PF
HxA
-13
C2
537
N/A
CC
H4
9.2
30
9ng
/L1
.04
18
06
09
---
---
---
70
- 1
30
98
50
.0
01
/14
/20
19
10
:33
01
/24
/20
19
03
:52
Fals
e
Perf
luoro
oct
anesu
lfonic
aci
d (
PF
OS
)537
2.0
CC
H1
99
.19
30
ng
/L1
.04
18
06
09
---
---
---
70
- 1
30
10
02
00
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
3:5
2F
als
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
CC
H2
00
.87
30
ng
/L1
.04
18
06
09
---
---
---
70
- 1
30
10
02
00
0
1/1
4/2
01
9 1
0:3
30
1/2
4/2
01
9 0
3:5
2
Page 3
of
3E
EA
Run I
D 2
54373 /
EE
A R
eport
# 4
411
45
Page 9 of 11
l R DD D
JODI
JD□
-□□--□□- -□--□ DODD DD
Sa
mp
le T
yp
e K
ey
Typ
e (
Ab
br.
)S
am
ple
Typ
eTyp
e (
Ab
br.
)S
am
ple
Typ
e
CC
HC
ontin
uin
g C
alib
ratio
n H
igh
CC
LC
ontin
uin
g C
alib
ratio
n L
ow
CC
MC
ontin
uin
g C
alib
ratio
n M
id
FS
Fie
ld S
am
ple
FB
LF
ort
ifie
d B
lank L
ow
LR
BLabora
tory
Reagent
Bla
nk
1.0
0
Page 10 of 11
END OF REPORT
Page 11 of 11
