ERIE DIVISION 1962 WAGER ROAD MARK MATROZZA , … · date timtech accrede . on fbex7402 continued solids, total date sampled: 8/30/2007 a2540g time sampled: 11:15 am 9/7/2007 10:56

286107

Microbac Laboratories, Inc.ERIE DIVISION

1962 WAGER ROADERIE, PA 16509

(814)825-8533 FAX (814)825-9254

MARK MATROZZA , MANAGING DIRECTOR

http://ww\v.microbac.com E-Mail: [email protected]

Page 1 of 8U

STATE CERT ID.25-067, 10121C-PA-05

CHEMISTRY • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTSWATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS

PRELIMINARY CERTIFICATE OF ANALYSIS

DEMAXIMIS, INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANE

KNOXVILLE,TN 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Cust#

9/5/20070709-01502

004229

Permit No.Cust P.O. PROJECT 3075F

SUBJECT: SOLID SAMPLES FOR ANALYSIS

TEST METHOD RESULT UNITS

001 FBEXB14

Date Sampled: 9/4/2007PCBs ON SOLID

AROCHLOR-1016, DRY WT.







DECACHLOROBIPHENYL

TETRACHLORO-M-XYLENE

SOLIDS, TOTAL

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G

<57.2

<57.2

<57.2

<57.2

150

<57.2

<57.2

57.4

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

%

%

%

ANALYSIS

DATE TIME

Time Sampled:

DRY WT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/5/2007

TECH ACCRED.

12:57 pm

11:12

11:12

11:12

11:12

11:12

11:12

11:12

11:12

OST

OST

OST

OST

OST

OST

OST

OST

002 FBEXB15

PCBs ON SOLID





AROCHLOR-1248, DRYWT.



DECACHLOROBIPHENYL


SOLIDS, TOTAL

003 FBEXB16

PCBs ON SOLID


Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G

Date Sampled:E8082

E8082

9/4/2007

9/4/2007

Time Sampled: 1:01 pm

<5.73 MG/KG

<5.73 MG/KG

<5.73 MG/KG

<5.73 MG/KG

9.39 MG/KG

<5.73 MG/KG

<5.73 MG/KG

87.2 %

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/11/2007

9/5/2007

Time Sampled:

<563 MG/KG DRYWT 9/10/2007

11:12

11:14

11:14

11:14

11:14

11:14

11:14

11:14

OST

OST

OST

OST

OST

OST

OST

OST

1:05 pm

11:14 OST

The data and information on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition

that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory.

USDA EPA NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research

NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditations for

various drinking water, wastewater and solid & chemical materials,air & emissions analytes Acr



(814)825-8533 FAX (814)825-9254


http://\v\v\v.microbac.com E-Mail: [email protected]

Page 7 of 7


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTSWATER • AIR • WASTES • FOOD PHARMACEUTICALS • NUTRACEUTICALS


DEMAXIMIS, INC.MS. VALERIA A. RULE, P.E.

450 MONTBROOK LANE

KNOXVILLEJN 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Cust #

8/31/20070709-01402

004229


SUBJECT: SOLID SAMPLES RECEIVED 8/31/07


ANALYSIS

DATE TIME TECH ACCRED.

Alt samples received in proper condition and results conform to ISO 17025 standards unless otlienwse noted

JJ£ This symbol at the end of the test line means the test analysis met the requirements of NELAC (PA ID 25-00067)

*J» This symbol at the end of the test line means the test analysis met the requirements of A1HA (ID 100386)

^ This symbol at the end of the test line means the test analysis met the requirements of NY ELAP (NY ID 10121)

ABBREVIATIONS:

TNTC = Too Numerous To CountUG/L = Micrograms per Liter (PPB)UG/KG = Micrograms per Kilogram (PPB)MG/L = Milligrams per Liter (PPM)1000 UG = 1 MGPostive = Bacteria or target analyte detected

MG/KG = Milligram per Kilogram (PPM)CFU = Colony Forming UnitND = Not detected at or below the reporting limitTIC = Tentatively Identified Compound"<" = less than (also see "ND")

= Bacteria or target analyte not detectedNegative

For any feedback concerning our services, please contact Mark Matrozza, Managing Director at [email protected] or Trevor Boyce,President at [email protected]



USDA-EPA-N1OSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research

NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid & chemical materials,air & emissions analytes

ACI



(814)825-8533 FAX (814)825-9254


http://www.microbac.com E-Mail: [email protected]

Page 6 of 7




DEMAXIMIS, INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK. LANE

KNOXVILLE.TN 37919


8/31/20070709-01402

004229



TEST METHOD RESULT UNITSANALYSIS


ON FBEX7402

continuedSOLIDS, TOTAL

Date Sampled: 8/30/2007

A2540G

Time Sampled: 11:15 am

9/7/2007 10:56 OST

012 FBEX7501

Date Sampled: 8/30/2007PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G

<:0.060

<0.060

<0.060

<0.060

O.OSO

<0.060

<0.060

84.0

Time Sampled:

MG/KG DRYWT

MG/KG DRYWT

MG/KG DRYWT

MG/KG DRYWT

MG/KG DRYWT

MG/KG DRYWT

MG/KG DRYWT

%

%

%

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

1 :45 pm

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

The data and information On this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition

that it is not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratory

USDA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research


various drinking water, wastewater and solid & chemical materials,air & emissions anaiyt.es AO



(814)825-8533 FAX (814)825-9254



Page 5 of 7




DEMAXIMIS , INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANE

KNOXVILLE,TN 37919


8/31/20070709-01402

004229





009 FBEX74SWNcontinued


DECACHLOROBIPHENYL


SOLIDS, TOTAL

E8082

E8082

E8082

A2540G

<0.060 MG/KG DRYWT 9/7/2007 10:56 OST

83.2 % 9/7/2007 10:56 OST

010 FBEX7401

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G

8/30/2007 Time Sampled: 11:12 am

<33.7

<33.7

<33.7

<33.7

56.1

<33.7

<33.7

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

74.2 9/7/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

Oil FBEX7402

PCBs ON SOLID








DECACHLOROBIPHENYL


Date Sampled: 8/30/2007E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082


that it [S not to be reproduced wholly or in part for advertising or other purposes without approval from the laboratorv.


NELAP accredited by PA, NV. visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid & chemical matehals,air & emissions analytes


<0.061 MG/KG

<0.061 MG/KG

<0.061 MG/KG

<0.061 MG/KG

0.044 MG/KG

<0.061 MG/KG

<0.061 MG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

MEMBER

ACI


1962 WAGER ROAD

ERIE. PA 16509

(814)825-8533 FAX (814)825-9254


http://\vw\v.microbac.com E-Mail: [email protected]

Page 4 of 7


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTSWATER • AIR • WASTES FOOD • PHARMACEUTICALS • NUTRACEUTICALS



450 MONTBROOK LANE

KNOXV1LLE,TN 37919


8/31/20070709-0)402

004229


SUBJECT: SOLID SAMPLES RECEIVED 8/31 /07



007 FBEX7302

continuedAROCHLOR-1242, DRY WT.




DECACHLOROBIPHENYL

TETRACHLOROM-XYLENE

SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<0.056 MG/KG DRY WT 9/7/2007

0.043 MG/KG DRY WT 9/7/2007

<0.056 MG/KG DRY WT 9/7/2007

<0.056 MG/KG DRY WT 9/7/2007

89.2 % 9/7/2007

10:56 OST

10:56 OST

10:56 OST

10:56 OST

10:56 OST

008 FBEX7303

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<0.057 MG/KG

<0.057 MG/KG

<0.057 MG/KG

<0.057 MG/KG

0.023 MG/KG

<0.057 MG/KG

<0.057 MG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

88.3 % 9/7/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

009 FBEX74SWN

PCBs ON SOLID







E8082

E8082

E8082

E8082

E8082

E8082

E8082

<0.060 MG/KG DRYWT 9/7/2007 10:56

<0.060 MG/KG DRYWT 9/7/2007 10:56

<0.060 MG/KG DRYWT 9/7/2007 10:56

<0.060 MG/KG DRYWT 9/7/2007 10:56

0.112 MG/KG DRYWT 9/7/2007 10:56

<0.060 MG/KG DRYWT 9/7/2007 10:56

Trie data and information on this, and other accompanying documents, represent only the sample(s) analyzed and is rendered upon condition

tnat it is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory.


NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditations torvarious drinking water, wastewater and solid & chemical materials,air a emissions analytes

OST

OST

OST

OST

OST

OST

ACI


1962 WAGER ROADE R I E , PA 16509

(814)825-8533 FAX (814)825-9254

MARK. MATROZZA . MANAGING DIRECTOR

http://\vw\v.microbac.com F.-Mail: [email protected]

Page 3 of 7




DEMAXIMIS , INC.MS. VALERIA A. RULE, P.E.450 MONTBROOK LANE

KNOXVILLE.TN 37919


8/31/20070709-01402

004229



TESTANALYSIS

METHOD RESULT UNITS DATE TIME TECH ACCRED.

5 FBEX73SWW






DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<0.560 MG/KG DRY WT 9/7/2007 10:56 OST

<0.560 MG/KG DRY WT 9/7/2007 10:56 OST

1.18 MG/KG DRYWT 9/7/2007 10:56 OST

<0.560 MG/KG DRYWT 9/7/2007 10:56 OST

<0.560 MG/KG DRYWT 9/7/2007 10:56 OST

89.1 % 9/7/2007 10:56 OST

006 FBEX7301

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<234 MG/KG

<234 MG/KG

<234 MG/KG

<234 MG/KG

599 MG/KG

<234 MG/KG

<234 MG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

85.6 % 9/7/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

007 FBEX7302

PCBs ON SOLID




Date Sampled:E8082

E8082

E8082

E8082


<0.056 MG/KG DRY WT 9/7/2007 10:56 OST

<0.056 MG/KG DRYWT 9/7/2007 10:56 OST

<0.056 MG/KG DRYWT 9/7/2007 10:56 OST



USDA-EPA-NIOSH Testing Food Sanitation Consulting Cnemical and Microbiological Analyses and Research

NELAP accredited by PA, NY. visit our website to view our current NELAC accreditations for

various drinking water, wastewater and solid & chemical matenals,air & emissions analytesACI



(814)825-8533 FAX (814)825-9254


http://ww\v.microbac.com E-Mail: [email protected]

Page 2 of 7


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTSWATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUT1CALS



450 MONTBROOK LANE

KNOXVILLE/TN 37919


8/31/20070709-01402

004229


SUBJECT: SOLID SAMPLES RECEIVED 8/31 /07

TESTANALYSIS


3 FBEX7701







DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082E8082E8082E8082E8082E8082E8082E8082A2540G


<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

0.510 MG/KG DRYWT 9/7/2007 10:56 OST

<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

<0.661 MG/KG DRYWT 9/7/2007 10:56 OST

75.7 % 8/31/2007 10:56 OST

004 FBEX7702

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

005 FBEX73SWW

PCBs ON SOLID



Date Sampled:E8082E8082E8082E8082E8082E8082E8082E8082E8082E8082A2540G

Date Sampled:E8082E8082E8082

8/30/2007

8/30/2007


< 6,680 MG/KG

< 6,680 MG/KG

<6,680 MG/KG

<6,680 MG/KG

26,300 MG/KG

<6,680 MG/KG

<6,680 MG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

74.9 % 9/7/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST


<0.560 MG/KG DRYWT 9/7/2007 10:56 OST

<0.560 MG/KG DRYWT 9/7/2007 10:56 OST


that it is not to pe reproduced wholly or in part fpr advertising or other purposes without approval from the laporatory.

U5DA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research

NELAP accredited hy PA, NY. Visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid & chemical matenals,air & emissions analytes ACI



(814)825-8533 FAX (814)825-9254


http://\v\vw.microbac.com E-Mail: [email protected]

Page 1 of 7





KNOXVILLE.TN 37919


8/31/20070709-01402

004229




ANALYSISDATE TIME TECH ACCRED.

001 FBEXB13

PCBs ON SOLID

AROCHLOR-1016,

AROCHLOR-1221,

AROCHLOR-1232,

AROCHLOR-12<12,

AROCHLOR-1248,

AROCHLOR-1254,

AROCHLOR-1260,

DRY WT.

DRY WT.

DRY WT.

DRY WT.

DRY WT.

DRY WT.

DRY WT.

DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G

<2.27

<2.27

<2.27

<2.27

3.31

<2.27

<2.27

88.3

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

MG/KG

%

%

%

Time

DRY WT

DRY WT

DRY WT

DRY WT

DRYWT

DRYWT

DRYWT

Sampled:

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

8/31/2007

2:25 pm

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

002 FBEX77SWS

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL



<0.289 MG/KG

<0.28y MG/KG

<0.289 MG/KG

<0.289 MG/KG

0.002 MG/KG

<0.289 MG/KG

<0.289 MG/KG

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

9/7/2007

86.5 % 8/31/2007

10:56

10:56

10:56

10:56

10:56

10:56

10:56

10:56

OST

OST

OST

OST

OST

OST

OST

OST

003 FBEX7701

PCBs ON SOLID


Date Sampled:E8082

E8082


<0.661 MG/KG DRYWT 9/7/2007 10:56 OST



U5DA-EPA-NIO5H Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research

NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid S chemical materials,air & emissions analytes

ACI

Microbac Laboratories, Inc.ERIE DIVISION1962 WAGER ROAD

ERIE, PA 16509

(814)825-8533 FAX (814)825-9254



Page 8 of 8





K.NOXVILLE.TN 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Gust #

9/5/20070709-01502

004229




ANALYSIS


All samples received in proper condition and results conform to ISO 17025 standards unless otherwise noted

Accred.

JJg This symbol at the end of the test line means the test analysis met the requirements of NELAC (PA ID 25-00067)

»5» This symbol at the end of the test l ine means the test analysis met the requirements of AIHA (ID 100386)

+ This symbol at the end of the test line means the test analysis met the requirements of NY ELAP (NY ID 10121)

ABBREVIATIONS:

TNTC = Too Numerous To CountUG/L = Micrograms per Liter (PPB)UG/KG = Micrograms per Kilogram (PPB)MG/L = Milligrams per Liter (PPM)1000 UG =1MGPostive = Bacteria or target analyte detected

MG/KG = Milligram per Kilogram (PPM)CPU = Colony Forming UnitND = Not detected at or below the reporting limitTIC = Tentatively Identified Compound"<" = less than (also see "ND")Necative - Bacteria or target analyte not detected

For any feedback concerning our services, please contact Mark Matrozza, Managing Director at [email protected] or Trevor Boyce,President at presidenttgjmicrobac.com




NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid & chemical materials,ak & emissions analytes ACI



(814)825-8533 FAX (814)825-9254

MARK MATROZZA . MANAGING DIRECTOR


Page 7 of 8

STATE CERT ID.25-067. 10121C-PA-05




450 MONTBROOK LANE

KNOXVILLE.TN 37919


9/5/20070709-01502

004229





013 FBEXMSD2


DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

A2540G


UG/KG DRYWT

014 FBEXB23

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

%

%

%

THE TECH INITIALS "OST" (OUTSIDE TESTING) INDICATE THAT THE PCBANALYSES WERE SUB-CONTRACTED TO MICROBAC, PITTSBURGH DIVISION.

The1 data and information on this, and otner accompanying documents, represent only the sample(s) analyzed and is rendered upon c

that it is not to be reproduced wholly or In part for advertising or other purposes without approval from the laboratory.



various drinking water, wastewater and solid & chemical materials,air & emissions analytesAO



(814)825-8533 FAX (814)825-9254


http://\v\v\v.microbac.com E-Mail: [email protected]

Page 6 of 8


CHEMISTRY • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTSWATER • AIR • WASTES • FOOD PHARMACEUTICALS • NUTRACEUT1CALS


DEMAXIM1S, INC.MS. VALERIA A. RULE. P.E.450 MONTBROOK LANE

KNOXVILLE,™ 37919

Date ReportedDate ReceivedOrder NumberInvoice No.Custtf

9/5/20070709-01502

004229



TESTANALYSIS


1 FBEXB22



DECACHLOROBIPHENYL


SOUDS, TOTAL


E8082E8082E8082E8082A2540G


UG/KG DRYWT

UG/KG DRYWT

012 FBEXEMS2

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL


9/4/2007 Time Sampled: 1:55 pm

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

DRYWT

DRYWT

DRYWT

DRYWT.

DRYWT.

DRYWT.

DRYWT.

013 FBEXMSD2

PCBs ON SOLID







Date Sampled:E8082E8082E8082E8082E8082E8082E8082


UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT.

UG/KG DRYWT.

UG/KG DRYWT.

UG/KG DRYWT.


that it Is not to be reproduced wholly or in part tor advertistng or other purposes without approval from the laboratory.



various drinking water, wastewater and solid & chemical materials,air & emissions analytes ACI



(814)825-8533 FAX (814)825-9254



Page 5 of 8




D E M A X I M I S , INC.MS. VALERIA A. RULE, P.E.

450 MONTBROOK LANE

KNOXVILLE.TN 37919


9/5/20070709-01502

004229



TESTANALYSIS


9 FBEXDUP2




DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082E8082E8082E8082E8082A2540G

Time Sampled:

384 MG/KG DRYWT 9/11/2007<551 MG/KG DRYWT 9/11/2007<551 MG/KG DRYWT 9/11/2007

90.8 % 9/5/2007

11:14

11:14

11:14

11:14

OST

OST

OST

OST

010 FBEXB21

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E8082E8082E8082E8082E8082E8082E8082E8082E8082E8082

A2540G


UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

UG/KG

DRYWT

DRYWT

DRYWT.

DRYWT

DRYWT.

DRYWT.

DRYWT

O i l FBEXB22

PCBs ON SOLID






Date Sampled:E8082E8082E8082

E8082E8082E8082


UG/KG DRY WT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT


that it is not to be reproduced wholly or in part for advertising or orher purposes without approval from the laboratory.

U5DA-EPA-NIOSH Testing Food Sanitation Consulting Chemical and Microbiological Analyses and Research

NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid ft chemical matenals.air ft emissions anatytes

ACl


D

!QfS7WAr,FRRnAn STATECERTID.

ERIE, PA 16509 25-067,10

(814)825-8533 FAX (814)825-9254 C-PA-05


http://\vw\v. microbac.com E-Mail: [email protected]

21



DEMAXIMIS, INC.

MS. VALERIA A. RULE, P.E.

450 MONTBROOK LANE

K.NOXVILLE.TN 37919

Date ReportedDate Received 9/5/2007Order Number 0709-01502

Invoice No.Cust # 004229



TEST METHODANALYSIS

RESULT UNITS DATE TIME TECH ACCRED.

Q7 FBEXB20


.continuedAROCHLOR-1242, DRY WT. E8082

AROCHLOR-1248, DRY WT. E8082

AROCHLOR- 1254, DRYWT. E8082

AROCHLOR-1260, DRYWT. E8082

Time Sampled: 1 :39 pm

<111 MG/KG DRYWT 9/10/2007 11:14 OST

283 MG/KG DRYWT 9/10/2007 11:14 OST

<111 MG/KG DRYWT 9/10/2007 11:14 OST

<111 MG/KG DRYWT 9/10/2007 11:14 OST

DECACHLOROBIPHENYL E8082 %

TETRACHLORO-M-XYLENE E8082 %

SOLIDS, TOTAL A2540G 89.7 % 9/5/2007 11:14 OST

38 FBEXB20SN

Date Sampled: 9/4/2007 Time Sampled: 1:35 pmPCBs ON SOLID E8082



AROCHLOR- 1232, DRYWT. E8082




HROCHLOR-1260, DRY WT. E8082

<578 MG/KG DRYWT 9/11/2007 11:14 OST

<578 MG/KG DRYWT 9/11/2007 11:14 OST

<578 MG/KG DRYWT 9/11/2007 11:14 OST

<578 MG/KG DRYWT 9/11/2007 11:14 OST

851 MG/KG DRYWT 9/11/2007 11:14 OST

<578 MG/KG DRYWT 9/11/2007 11:14 OST

<578 MG/KG DRYWT 9/11/2007 11:14 OST

DECACHLOROBIPHENYL E8082 %

TETRACHLORO-M-XYLENE E8082 %

SOLIDS, TOTAL A2540G 86.5 % 9/5/2007 11:14 OST

9 FBEXDUP2

Date Sampled: 9/4/2007 Time Sampled:3CBs ON SOLID E8082

\ROCHLOR-1016, DRYWT. E8082

"iROCHLOR- 1221, DRYWT. E8082

i\ROCHLOR-1232, DRY WT. E8082

i\ROCHLOR-1242, DRY WT. E8082

^¥•?]nor•a K2kJ^ i that it is not to be reproduced wholly or in

<551 MG/KG DRYWT 9/11/2007 11:14 OST

<551 MG/KG DRYWT 9/11/2007 11:14 OST

<551 MG/KG DRYWT 9/11/2007 11:14 OST

<551 MG/KG DRYWT 9/11/2007 11:14 OST

ying documents, represent only the sample(s) analyzed and is rendered upon condition

part for advertising or other purposes without approval from the laboratory. MEMBER

iMBi -t USDA-EPA-NIOSH Testing Food Sanitation i_onbuii.iriy unemicai ana micronio'ogicai Analyses ana Kesearcn ^V^H^^ETT I

•MR rj NELAP accredited by PA, NYVisit our website to view our current NELAC accreditations for W^^« Ivarious drinking water, wastewater and solid & chemical materiais,air & emissions analytes



(814)825-8533 FAX (814)825-9254



Page 3 of 8




DEMAXIMIS , INC.MS. VALERIA A. RULE, P.E.

450 MONTBROOK LANE

KNOXVILLE,TN 37919


9/5/20070709-01502

004229



TESTANALYSIS


5 FBEXB18






DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

006 FBEXB19

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<581 MG/KG

<581 MG/KG

<581 MG/KG

<58i MG/KG

1,430 MG/KG

<581 MG/KG

<581 MG/KG

86.1 %

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

DRYWT

9/10/2007

9/10/2007

9/10/2007

9/10/2007

9/10/2007

9/10/2007

9/10/2007

9/5/2007

11:14

11:14

11:14

11:14

11:14

11:14

11:14

11:14

OST

OST

OST

OST

OST

OST

OST

OST

007 FBEXB20

PCBs ON SOLID




Date Sampled:E8082

E8082

E8082

E8082


<111 MG/KG DRYWT 9/10/2007 11:14 OST

<111 MG/KG DRYWT 9/10/2007 11:14 OST

<111 MG/KG DRYWT 9/10/2007 11:14 OST

The data and information on this, and other accompanying documents, represent only the samplefs) analyzed and is rendered upon condition



NELAP accredited by PA, NY Visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid & chemical materials,air & emissions analvtes

ACI



(814)825-8533 FAX (814)825-9254


http://www.microbnc.com E-Mail: [email protected]

Page 2 of 8





450 MONTBROOK LANE

KNOXVILLE.TN 37919


9/5/20070709-01502

004229




ANALYSIS


003 FBEXB16







DECACHLOROBIPHENYL


SOLIDS, TOTAL


E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


<563 MG/KG DRY WT 9/10/2007 11:14 OST

<563 MG/KG DRY WT 9/10/2007 11:14 OST

<563 MG/KG DRY WT 9/10/2007 11:14 OST

675 MG/KG DRY WT 9/10/2007 11:14 OST

<563 MG/KG DRY WT 9/10/2007 11:14 OST

<563 MG/KG DRY WT 9/10/2007 11:14 OST

88.8 % 9/5/2007 11:14 OST

004 FBEXB17

PCBs ON SOLID








DECACHLOROBIPHENYL


SOLIDS, TOTAL

Date Sampled:E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

E8082

A2540G


UG/KG DRYWT.

UG/KG DRYWT.

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

UG/KG DRYWT

005 FBEXB18

PCBs ON SOLID



Date Sampled:

E8082

E8082

E8082


UG/KG DRYWT

UG/KG DRYWT




NELAP accredited by PA, NY. Visit our website to view our current NELAC accreditations forvarious drinking water, wastewater and solid & chemical materials.air & emissions analytes

MEMBER

ACI

Microbac Laboratories, Inc.100 MARSHALL DRIVEWARRENDALE, PA 15086(724)772-0610 FAX (724) 772-1686MARK A. MATROZZA, MANAGING DIRECTOR

http://www. microbac.com

Page 1 of 1

State Laboratory Certification Numbers:PADEP: 02-257, NC: 42703, WVDEP: 215, 9951 CM K.Y: 90136


CERTIFICATE OF ANALYSIS

MICROBAC ERIE DIVISIONCHERI BROLASK11962 WAGER ROADERIE, PA 16509

Permit No.:Cust P.O.:

SUBJECT: 0708-2872/DeMaximis - Oil Sample for Analysis

Date Reported:Date Received:Order Number:Invoice No.:Cust #:Sample Date:Sample Time:

Sampler/Temp:

8/31/2007

0708-02667

M2968/29/20070:00

TEST METHOD RESULT UNITS DATE TECH

ooi 0708-2872

Collected 8/29/07

PCBs (Oil)

PCB-1016

PCB-1221

PCB-1232

PCB-1242

PCB-1248

PCB-1254

PCB-1260

SW-846 8082

<20,000

< 20,000

< 20,000

<20,000

1,140,000

< 20,000

<20,000

mg/Kg 09/07/07

mg/Kg 09/07/07

mg/Kg 09/07/07

mg/Kg 09/07/07

mg/Kg 09/07/07

mg/Kg 09/07/07

mg/Kg 09/07/07

TWCTWCTWCTWCTWCTWCTWC

Submitted By:

Mark A. Matrozza, Managing Director




MEMBER

TERESE To THOMAS SHORT/R5/USEPA/US@EPAVANDONSEL/R5/USEPA/US cc Schafer/R5/USEpA/us@EpA, Peter

09/07/2007 03:17 PM Felitti/R5/USEPA/US@EPAbcc

Subject Re: Fields Brook - Pure PCBs Q

Hi Tom,

New information from the PRPs. The oil is pure Therminol (a Monsanto heat transfer fluid)- basically purePCBs. 1,000,000 ppm.

The PRPs have tarped, sandbagged, tied down and tented the excavation in expectation of heavy windsand rain this weekend. They will have it staffed 24/7 until work resumes next week to try to make surenothing makes it to surface water.

I briefed Don Bruce over the phone and he tied in Mark Durno from Twinsburg - so they know what's goingon - just in case. I will be forwarding PRP contact information to the Twinsburg OSCs this afternoon (sothey have it if they need it).

Please let me know whether you'd like us to move forward with this under remedial or whether you'd likeme to coordinate with removal and have them pick up this portion of the project.

Thanks,Terese

Documents

ERIE DIVISION 1962 WAGER ROAD MARK MATROZZA , … · date timtech accrede . on fbex7402 continued solids, total date sampled: 8/30/2007 a2540g time sampled: 11:15 am 9/7/2007 10:56