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DIPA 2000 Particle Size & Shape Analyzer

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Page 1: DIPA 2000 Particle Size & Shape Analyzer

Particle Size & Shape

Analyzer

Page 2: DIPA 2000 Particle Size & Shape Analyzer

“Equivalent Sphere” Attitude

These diameters are fundamentally different for the same particle.The equivalent sphere diameters differ for any non-spherical material.Every PSA technique yields different results for non-spherical particles.

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Page 3: DIPA 2000 Particle Size & Shape Analyzer

DIPA-2000 Measuring ChannelsSingle Instrument ; Dual Measurement Channels

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Page 4: DIPA 2000 Particle Size & Shape Analyzer

DIPA-2000 Laser Channel

Main Advantages:Quick & Straight Forward

MeasurementHigh Resolution Detection CapabilitiesTime Domain Analysis, No “Pre-

Knowledge”

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Page 5: DIPA 2000 Particle Size & Shape Analyzer

The rotating laser beam scans single particles within its focus.

The diameter of the particle is directly correlated to the duration of the obscuration.

The measurement principle is a time interval, not an intensity measurement.

The time domain is independent of particles optical or physical properties.

DIPA-2000 Laser Channel A B C D E F

Ta Tb Tc Td Te TfTime

V

Scanning Laser

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Page 6: DIPA 2000 Particle Size & Shape Analyzer

From the duration of the obscuration (T), and the known rotation velocity of the laser beam (V), the particle diameter (D) can be calculated:

D = V · TIn relation to the high speed of the laser rotating laser, the particlesare stationary, thus will not effect particle size measurement.

No requirements for particles pre-knowledge of:1. Refractive index2. Temperature3. Viscosity variation4. Electrical conductivity5. Etc…

DIPA-2000 Laser ChannelSlide 8/43

Page 7: DIPA 2000 Particle Size & Shape Analyzer

Data is collected directly on each analyzed particle. Detection of minor fractions, high resolution. Correct measurement of particle size, not influenced by

physical or optical properties. Operation in Liquid, Dry and Aerosol mediums. No calibration/alignment required by user. Robust measurement, on-line indication for statistical

significance. Concentration measurement. FDA 21 CFR Part 11 S/W security compliance.

DIPA-2000 Laser ChannelSummery

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Page 8: DIPA 2000 Particle Size & Shape Analyzer

Single Instrument ; Dual Measurement Channels

DIPA-2000 Measuring Channels

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Page 9: DIPA 2000 Particle Size & Shape Analyzer

DIPA-2000 Video Channel

Main Advantages:Sample VisualizationDynamic Shape AnalysisAdvanced Particles Size and Shape

information

Page 10: DIPA 2000 Particle Size & Shape Analyzer

Dynamic Shape Analysis(DSA) Principle of Operation

Real time images of particles in motionare collected

Images are converted into a grid containing a collection of picture elements (pixels)

Each individual pixel has a value for brightness (grey level): 0 = Dark; 255 = White

All images are analyzed according to apre-defined set of Image Analysis characteristics

Measurement is finished when the analysis end conditions are met (# of particles/images, confidence level, time, etc)

420 µm

18 µm

Image Conversio

n

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Page 11: DIPA 2000 Particle Size & Shape Analyzer

DIPA-2000 DSA Main Features:

• Easy setup and measurement using software wizards

• Advanced pre-processing algorithms

• Size and Shape Filter/Grouping

• Automated Report Generation

• Storage of real raw date (un-processed images)

• Re-processing of raw data• Internal optical calibration

and verification tools available

• Interface with 3rd party hardware (Microscopy)

DIPA-2000 Video ChannelSlide 15/43

Page 12: DIPA 2000 Particle Size & Shape Analyzer

• For each individual particle, all size and shape parameters are determined.

• The DIPA-2000 Image Analysis S/W automates set-up and measurement.

• DIPA-2000 IA software includes many procedures such as:– Pre-Processing Procedures– Image Quality Filters– Region of Interest Determination– Out-Of-Focus Rejection– Morphology Operations– Grouping according to size/shape– Re-Processing of stored images

and movies– Manual Lens Calibration

(Microscopy)

DIPA-2000 Video ChannelSlide 16/43

Page 13: DIPA 2000 Particle Size & Shape Analyzer

Seeing is believing, visualize your sampled particles. Better and advanced characterization of materials. High resolution data (down to pixel size data). Detection and quantification of shape parameters. Validation technique for the Laser Channel or other

particle size methods. Detection capability of minor fractions for fine

particles or agglomerated materials. Quantification of material homogenity. Advanced tool for shape differences

characterisation. FDA 21 CFR Part 11 S/W security compliance.

DIPA-2000 Video ChannelSummery

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Page 14: DIPA 2000 Particle Size & Shape Analyzer

One System = Variety of Applications

“Adapting the technology to the application”, rather than - “adapting the application to the technology”

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Page 15: DIPA 2000 Particle Size & Shape Analyzer

Life Science

Heavy Industry

Food Products

Energy

Ceramics & Metals

Chemicals

Pharma/Bio-Tech

Environmental

Geology Soil, clay, sand, kaolin

Ocean water, tap water, waste water, membrane filtration, dust, flocculationPowders, suspensions, syrups, emulsions, pastes, micro-carriers, injectable solutions, collagen, microcapsules

Pesticides, dispersants, catalysts, resins, emulsions, preservatives

Alumina, silica, magnetic powders, tungsten, strontium, sintered products, stainless steel, cobaltCoal, fuels, slurries, shale-oil emulsions, fly ash

Emulsions, fine powders, beer, coffee, chocolate, flour, ground products, agglomerated crystals, peanut butter

Polymers, oil droplets, wear particles, calk, fillers, toners, pulp & paper, coatings, pigments, PVC, paintBacteria, smears, inhalation toxicology, cell research, algae growth, yeast, blood analysis

Some Global ApplicationsSlide 23/43

Page 16: DIPA 2000 Particle Size & Shape Analyzer

DIPA 2000 Particle Size & Shape AnalyzerElementary and Advanced S/W

Features

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Page 17: DIPA 2000 Particle Size & Shape Analyzer

SEEING IS

BELEIVING

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Page 27: DIPA 2000 Particle Size & Shape Analyzer

DIPA 2000 S/W FeaturesSummery

• Easy setup and measurement using software wizards

• Advanced pre-processing algorithmes• Size and Shape Grouping/Filtering• Automated report generator• Storage of real-time raw data (un-processed

images)• Re-processing of raw data (images & movie files)• Interface with 3rd party hardware (e.g.

Microscopy)• Manual calibration and verification tools avaible• Integrated laser and video software• Simultaneous laser and video results• FDA 21 CFR Part 11 S/W security compliance

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