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Martín Gascón Santiago de Compostela, December 10 th, 2010 1/34
Motivation Characterization Inbeam tests
Prototype of a new calorimeter for the studies of nuclear reactions with relativistic radioactive beams
Santiago de Compostela 10th. December, 2010
Martín Gascón
Martín Gascón Santiago de Compostela, December 10 th, 2010 2/34
Motivation Characterization Inbeam tests
MotivationMotivationFAIR, R3B, CALIFA, ProtoZero (CALIFA's prototype)
Characterization of CsI(Tl) crystals and photosensorsCharacterization of CsI(Tl) crystals and photosensorsPhotosensors
Benchtests on small and prototype crystals
Inbeam tests of the prototype Inbeam tests of the prototype and prototype simulationsand prototype simulationsResults of the proton beam test
Results of the gamma beam tests
ConclusionsConclusions
Martín Gascón Santiago de Compostela, December 10 th, 2010 3/34
Motivation Characterization Inbeam tests
FAIR: Facility for Antiproton Ion Research
New accelerator facility in Darmstadt (Germany)Antiprotons, stable and radioactiveion beams Primary intensity: (1012 ions/s)@ 230 GeV/u
Nuclear structure and Astrophysics with exotic nucleiAntiproton PhysicsRelativistic heavy ions collisionsAtomic and Plasma Physics
MotivationFAIR R3B CALIFA ProtoZeroFAIR
Scientific Program
FAIR
Martín Gascón Santiago de Compostela, December 10 th, 2010 4/34
Motivation Characterization Inbeam tests
R3B: Reactions with Relativistic Radioactive Beams
Calorimeter / gamma spectrometer Silicon arrays around target for recoils Large acceptance superconducting dipole High resolution neutron detectors ToF wall for chargedparticle id. High resolution magnetic spectrometer
MotivationFAIR R3B CALIFA ProtoZeroR3B
R3B experimental subjects
Detectors
Challenging research program including QFS, knockout, fragmentation, fission, ...
Nuclear structure far from stability Reactions of astrophysical interest Study of the EOS of asymmetric matter
Martín Gascón Santiago de Compostela, December 10 th, 2010 5/34
Motivation Characterization Inbeam tests
CALIFA requirements (R3B LoI, 2005) :
CALIFA: CALorimeter for InFlight emitted gAmmas
MotivationFAIR R3B CALIFA ProtoZeroCALIFA
Gamma sum energy
Gamma multiplicity
Gamma energy resolution
Calorimeter for high energy light charged particles Up to MeV in Lab system300
Good lightcharged particles energy resolution
(Esum)/<Esum> < 10%
(N)/<N> < 10 %
< 5 % E/E (gammas at 1 MeV)
Total absortion efficiency 80 % (up to ESRF = 5 MeV)
< 1% p/Ep (protons at 300 MeV)
H. Álvarez-Pol et al. Nucl. Inst. and Meth. B 266 (2008) 4616-4620
To fulfill all these requirements is a challenge that gives CALIFA its unique characteristics. This challenge is even greater if we take into account
the constraints imposed by experiments with relativistic ions in inverse kinematics.
Martín Gascón Santiago de Compostela, December 10 th, 2010 6/34
Motivation Characterization Inbeam tests
CALIFA: Geometry
Motivation
Gammas emitted by moving sources at relativistic energies suffer the relativistic Doppler Effect. Calculation of their energy in the Source Reference Frame (SRF) requires an
accurate measurement of both the Lab energy (LRF) and the emission polar angle.
A limited polar angle resolution would contribute to the uncertainty of the gamma energy in SRF
Doppler Effect Constraint
Doppler factor as a function of the polar
angle.
Angular distribution of gammas in the LRF
Detector design
The optimal polar angle granularity to guarantee the required energy resolution should be determined Totalabsorption efficiency requirement is determined by the
length of the scintillating material and dead volume (empty space and material as wrapping and support structures)
FAIR R3B CALIFA ProtoZeroCALIFA
Martín Gascón Santiago de Compostela, December 10 th, 2010 7/34
Motivation Characterization Inbeam tests
What scintillating material ?
Motivation
CsI(Tl) emission spectrumCsI(Tl)
Advantageswell known propertiesrelatively high density high light yield cheap to make, easy to handleslightly hygroscopicgood energy resolution with APDs
InconvenientLong scintillating decay time
NaI(Tl) CsI(Tl) CsI(Na) BGO LYSO PWO CsI (pure)
5.29 3.86 3.67 4.51 4.51 7.13 7.1 8.29 4.5163000 49000 39000 60000 45000 9000 32000 100 16800< 3% 3.5% 7% 6% 7.5% 10% 7.1% >10% 7.5%N/A N/A 3.8% 4.9% N/A 8.3% N/A N/A 4.3%
380350 310 fast
550 420 480 420 420 315430 415
25 25/213 620 fast 1000 630 300 41 6 35/6Hygroscopic yes yes yes slightly yes no no no slightlyCost (per cm3) $30 $30 $2 $5 $5 $9 N/A $2 $5
LaBr3 LaCl3
Density (g/cm3)
Light Yield (ph/MeV)E/E 662 keV (PMT)
E/E 662 keV (APD)
Peak(nm)
Fast Decay (ns)
FAIR R3B CALIFA ProtoZeroCALIFA
APD quantum efficiency
Martín Gascón Santiago de Compostela, December 10 th, 2010 8/34
Motivation Characterization Inbeam tests
CsI: what length?
Three different crystal sets were evaluated in simulations for the CALIFA calorimeter
Barrel specifications short: 9 12 cm medium: 1115 cm large: 1418 cm
Motivation
Conclusions The geometrical efficiency was higher than 80% for large and medium specifications The fullenergy peak efficiency decreased from 70% (0.5 MeV) to 50 % (10 MeV) Crystal Multiplicity goes from 2 crystals (0.5 MeV) to 7 (10 MeV) for the whole calorimeter. It can
reach 9 crystals in the Endcap, and it is limited to 4 crystals in the Barrel due to the Lorentz Boost Energy resolution contribution due to polar angle uncertainty is below 3%
Geometrical efficiency Several observables were studied to define the crystal geometry
FAIR R3B CALIFA ProtoZeroCALIFA
Martín Gascón Santiago de Compostela, December 10 th, 2010 9/34
Motivation Characterization Inbeam tests
ProtoZero: Design and construction
Crystal sample corresponding to ~ 90º polar angle
APDs tested in this prototype
15/16 bi frustumshaped CsI(Tl) crystals 15/16 LAAPDs (7x14 mm 2, 10x10 mm 2 an
d 10x10 2ch) 16 preamplifiers (Cremat, Mesytec)
ProtoZero
MotivationFAIR R3B CALIFA ProtoZeroProtoZero
Martín Gascón Santiago de Compostela, December 10 th, 2010 10/34
Motivation Characterization Inbeam tests
MotivationFAIR, R3B, CALIFA, ProtoZero (CALIFA's prototype)
Characterization of CsI(Tl) crystals and photosensorsCharacterization of CsI(Tl) crystals and photosensorsPhotosensors
Benchtests on small and prototype crystals
Inbeam tests of the prototype and prototype simulationsResults of the proton beam test
Results of the gamma beam tests
Characterization
Martín Gascón Santiago de Compostela, December 10 th, 2010 11/34
Motivation Characterization Inbeam tests
Test with small samples: APDs vs. PMTs
CsI(Tl) + APD CsI(Tl) + PMT
Crystal Length cm1 cm5 cm10XP1901
PMT XP1918
XP3102
7.0±0.1 8.4±0.1 12.8±0.16.1±0.1 7.4±0.1 10.7±0.19.1±0.1 9.9±0.1 16.5±0.2
ER at 662 keV for a 1 cm3 CsI(Tl) coupled to a S86641010 APD and to a Photonis XP1918 PMT for 8 s shaping time.
Characterization
Shaping Crystal Length time 1 cm 5 cm 10 cm
4.68±0.12 5.11±0.12 4.74±0.124.42±0.12 4.87±0.09 4.72±0.08
4 s8 s
Energy resolutions in % (FWHM) (at 662 keV) obtained for different PMTs and different crystal
lengths at 4 s shaping time
Best energy resolution values in % (FWHM) (at 662 keV), obtained for different crystal
sizes using a Hamamatsu S86641010 APD.
M. Gascón et al., IEEE Trans. Nuc. Sci 55 (2008) 1259-1262
Martín Gascón Santiago de Compostela, December 10 th, 2010 12/34
Motivation Characterization Inbeam tests
APD characterization
Procedure to compare different APD series and to disentangle the APD contribution to the energy resolution
Characterization
The APD contribution to the energy resolution was found to be 0.12% for the 10x10 APD. These LAAPDs were proven to work properly in a wide dynamic range
M. Gascón et al, IEEE Trans. Nuc. Sci 57 No. 3 (2010) 1465-1469
Martín Gascón Santiago de Compostela, December 10 th, 2010 13/34
Motivation Characterization Inbeam tests
APD characterization
Procedure to compare different APD series and to disentangle the APD contribution to the energy resolution
APD # A.A. Cap. LPR 1 10x10 std 406 5.2% 202 10x10 std 404 5.4% 223 10x10 std 410 5.3% 84 10x10 std 411 5.5% 75 7x14 std 332 7.2% 236 7x14 std 322 8.1% 237 7x14 std 332 8.7% 328 7x14 std 333 9.2% 399 7x14 low 491 7.5% 2410 7x14 low 484 8.0% 3011 7x14 low 493 8.2% 3112 7x14 low 492 9.8% 32
Cap=Capacitance
O.Vb ID(nA)
A.A.=active area (mm2)
O.Vb = Optimal bias voltage (Volts)LPR = Light pulse resolution @ 5.105 eh
Characterization
The best performance was found for the 10x10 Hamamatsu APDs
Martín Gascón Santiago de Compostela, December 10 th, 2010 14/34
Motivation Characterization Inbeam tests
APDs: Bias voltage and gain curves
Left: Energy resolution (Cs137) vs. bias voltage for a 5 cm long crystals coupled to Hamamatsu S86641010 APDs. Right: Typical gain curves of the S86641010 APD using 5 cm length CsI(Tl) crystals.
Conclusions
Gain variation smaller than 1% can only be achieved with bias
voltage variations below 350 mV
Relative gain variation due to bias voltage variation at optimal bias voltage for CsI(Tl) crystals coupled to S86641010 APDs
Characterization
Crystal length Gain variation (%/V)1 cm5 cm10 cm
2.84 ± 0.012.83 ± 0.012.83 ± 0.01
Martín Gascón Santiago de Compostela, December 10 th, 2010 15/34
Motivation Characterization Inbeam tests
APDs: Temperature drifts
(dM/dT)M1 = 2.8 %/ºCcompares well with the 2.5 %/ºC provided by Hamamatsu
Characterization
APD Gain Drift at RT
Mean Peak position and Temperature vs. time.
Total and gain drift corrected spectra for a 137Cs radioactive
source.
A PT1000 probe was placed near the APD to get the temperature information The detectors were cooled down using
LN2 vapor and warmed up by a heater
Experimental setup
Martín Gascón Santiago de Compostela, December 10 th, 2010 16/34
Motivation Characterization Inbeam tests
Test with prototype samples: crystal quality and optical coupling
Photograph of raw crystal samples from five providers. P1P5: Amcrys, Hilger Lanzhou, Saint Gobain, Scionix
Characterization
Crystal quality
Optical coupling For temporary bonds: optical grease, and optical pads. For permanent bonds: Scionix RTV 681 optical cement The result was found to be strongly dependent on details of the
contact, such as the amount of optical grease used, homogeneity or the presence of air bubbles
Optical cement and optical greases
The crystal quality depends on a set of factors such as transparency, surface treatment, polishing, and cutting edges. The samples with the best quality in the visual inspection did
not necessarily provide the best values for energy resolution and lightoutput
Martín Gascón Santiago de Compostela, December 10 th, 2010 17/34
Motivation Characterization Inbeam tests
Test with prototype samples: crystal wrapping
Averaged Lightpulse resolutions (FWHM) obtained using a LED with different 10x10 mm2 exit face crystals and different wrapping configurations, coupled to an XP5A08 PMT without optical grease. 1x,2x,3x,6x are the number of layers of 75 m Teflon tape
The ideal wrapping has not only to reflect the incident light but also to break up internal reflections and preferentially direct reflected light towards the photosensor. Best results for prototype crystals are
generally achieved with 2 layers of ESR (2x 65 m thickness)
Characterization
Conclusions
Setup for determining the optimal wrapping configuration for prototype crystals.
Wrapping configuration for prototype crystals
Wrapping L.P.R (%)
5.90
5.971x ESR + 1x TF 6.011x ESR + 2x TF 6.031x ESR + 3x TF 6.021x ESR + 6x TF 6.11
2x 65 m ESR
65 m ESR
Different wrapping materials: aluminized Mylar, ESR, LEF.
Martín Gascón Santiago de Compostela, December 10 th, 2010 18/34
Motivation Characterization Inbeam tests
Test with prototype samples: Light Output
The largest Light Output was found for crystals with the largest exit face.
Conclusions
Characterization
Energy resolution (FWHM) vs. photopeak channel for different samples, without optical grease between the crystal and the photomultiplier.
Setup used to compare the crystal light output
Tested crystals with 10x10 and 7x14 mm2 exit faces
Martín Gascón Santiago de Compostela, December 10 th, 2010 19/34
Motivation Characterization Inbeam tests
Test with prototype samples: Nonuniformity in light collection (N.U.)
Conclusions Important differences in lightcollection non
uniformity for each crystal, even for two samples coming from the same provider The E.R. can be bad for a good N.U. and vices
versa because the E.R. is measured only at the crystal entrance face
N.U. and energy resolution E/E (662 keV) for some samples tested in this workP: Provider S: Sample (S1 or S2)
Characterization
Light collection nonuniformity determination for P1S1 (best) and P5S2 (worst) samples.
M. Gascón et al., IEEE Trans. Nuc. Sci 56 (2009) 962-967.
sample N.U. (%) E.R. (%)P1-S1 1.1 9.3P1-S2 4.5 6.4P2-S1 2.2 5.9P3-S2 2.3 6.6P4-S1 1.8 6.5P4-S2 4.3 7.3P5-S2 10.4 7.4
Setup used for N.U. measurements
Martín Gascón Santiago de Compostela, December 10 th, 2010 20/34
Motivation Characterization Inbeam tests
Study of the energy resolution
Comments
Remarkably different performances were found among the measured samples, even for two samples coming from the same provider. The best energy resolution values obtained
were around 6% at 662 keV (5% at 1 MeV) which are close to the CALIFA requirements
Top: Experimental energy resolution as a function of the incident gamma energy.Bottom:Experimental spectra of the two detection systems P1S1 (red curve), and P2S1 (blue curve), in response to 662 keV rays. The energy resolution values obtained for the P2S1 sample are significantly better than P1S1
Characterization
Martín Gascón Santiago de Compostela, December 10 th, 2010 21/34
Motivation Characterization Inbeam tests
MotivationFAIR, R3B, CALIFA, ProtoZero (CALIFA's prototype)
Characterization of CsI(Tl) crystals and photosensorsPhotosensors
Benchtests on small and prototype crystals
Inbeam tests of the prototype and prototype simulationsInbeam tests of the prototype and prototype simulationsResults of the proton beam test
Results of the gamma beam tests
Inbeam tests
Martín Gascón Santiago de Compostela, December 10 th, 2010 22/34
Motivation Characterization Inbeam tests
The Svedberg Laboratory (Uppsala, Sweden)
10x20 mm2 exit face bifrustum shaped CsI(Tl) crystals, coupled to Hamamatsu 686710x20 APDs (2 channels) preamplifiers: 4 ch. Cremat CR110 mounted in a
common card in our laboratory crystal wrapping ESR (Enhanced Specular Reflector)
130 m thick per crystal
Proton beam energy 180 MeV A 2 mm thick Double Sided Silicon Strip
Detectors (DSSSDs) consisting of 32x32 perpendicular strips 25 mm thick copper and iron degraders for
calibration (protons at 92.7 and 120 MeV)
ProtoZero Experiment
180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUDInbeam tests
180 MeV proton beam at TSL
Martín Gascón Santiago de Compostela, December 10 th, 2010 23/34
Motivation Characterization Inbeam tests
Energy spectra
Comments
Energy resolutions are around 1%, which fulfills one of the main calorimeter requirements This values seem easily
achievable for protons at this energy. Beam was impinging in
the boundary between crystals #1 and #3 To the left of the peaks,
those events losing a certain energy can be observed
Spectra of incident 180 MeV protons obtained for each crystal of this prototype configuration
Inbeam tests180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD180 MeV proton beam at TSL
Martín Gascón Santiago de Compostela, December 10 th, 2010 24/34
Motivation Characterization Inbeam tests
Proton identification
Comments
Certain peak degradation energy
resolution ~3%
Events sharing the proton energy between crystals #1 and #3 produce a peak which is more than 1 MeV below the main peak
Conclusion
Correlation between Crystals #1 and #3. Addback between Crystals #1 and #3.
Left: Beam profile obtained with the DSSSDs, relative positions of all the detectors (#1 to #4), and selection of protons hitting A) the boundary between crystals B) region inside Crystal #3. Right: Spectra obtained for protons hitting in regions A, B and Total.
Inbeam tests180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD180 MeV proton beam at TSL
Martín Gascón Santiago de Compostela, December 10 th, 2010 25/34
Motivation Characterization Inbeam tests
R3BSim (GEANT4 and ROOT)
Wrapping
130 m per crystal
(2 ESR layers)
Peak degradation can be reduced using thinner crystal wrappingsProtons at 90, 120, 180 and 220 MeV, hitting close to the
boundary between 2 crystals (case B) wrapped with ESR 130 m thick (2 layers)
Inbeam tests
Conclusion
180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD180 MeV proton beam at TSL
The ProtoZero reconstructed energy spectrum for 180 MeV protons. The wrapping thicknesses ranges from 0 to 260 m.
Martín Gascón Santiago de Compostela, December 10 th, 2010 26/34
Motivation Characterization Inbeam tests
Centro de Microanálisis de Materiales (CMAM)
Protons
Wrapping 5 MV CockroftWalton
accelerator. Protons at 1 MeV The Teflon target (LiF)
was 30 mm in diameter, 5 mm thick
Inbeam tests180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD6.1 MeV gamma beam at CMAM
O. Tengblad. GSI Meeting. April 2009
CMAM
CsI(Tl) crystals + APDs (7x14, 10x10, 10x20) 4 ch. Cremat CR110 Mesytec MSCF16 amplifiers DAQ Midas (IEMCSIC)
ProtoZero
6.129 resonance1 5.618 single escape
5.1070.511
Ep (MeV) E (MeV)
19Fdoble escape
19F(p,)16O
Martín Gascón Santiago de Compostela, December 10 th, 2010 27/34
Motivation Characterization Inbeam tests
Protons
Wrapping
6.1 MeV gammarays produced at the target E.R = 2.8 % (FWHM) not so far
from 2.2 % (simulation)
Energy resolution
Inbeam tests
Energy reconstruction180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD6.1 MeV gamma beam at CMAM
Energy spectra of 6 crystals from this prototype configuration
Addback spectrum of 6 neighbor crystals
Martín Gascón Santiago de Compostela, December 10 th, 2010 28/34
Motivation Characterization Inbeam tests
Protons
Wrapping Energy range from 3 – 20 MeV 25 keV @ 10 MeV energy resolution photon flux is about 1000 ph/keV/s/cm2. Radiator target: 10 microns Au foil 64 scintillation fibres: 1x1mm2
Photon Tagger
2x 8 channels Mesytec preamplifiers (MSI8) Mesytec MSCF16 amplifiers 32 channel sensing ADC (CAEN V785) DAQ based on the MultiBranch System (MBS) A PT1000 temperature probe for monitoring
ProtoZero
NEPTUN Facility@SDALINAC TUD, Darmstadt, Germany
Inbeam tests180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD410 MeV gamma beam at TUD
Martín Gascón Santiago de Compostela, December 10 th, 2010 29/34
Motivation Characterization Inbeam tests
Calibration
Spectra obtained for a prototype configuration with 15 crystals using 137Cs and 60Co radioactive sources.
ProtoZero
Energy reconstruction
AddbackAddback energy spectrum for 60Co and 137Cs radioactive sources.
Inbeam tests180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD410 MeV gamma beam at TUD
Martín Gascón Santiago de Compostela, December 10 th, 2010 30/34
Motivation Characterization Inbeam tests
CalibrationWrapping
ProtoZero
Time Coincidences
The photon tagger has 64 pairs of fibers. Fibers give a signal after each electron hit. These signals are in time coincidence with the master trigger (MA) given by any prototype crystal
Inbeam tests180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD410 MeV gamma beam at TUD
Martín Gascón Santiago de Compostela, December 10 th, 2010 31/34
Motivation Characterization Inbeam tests
CalibrationWrapping
ProtoZero
410 MeV energy spectra
The higher the tagged energy, the lower the statistic due to a lower gamma yield at the radiator
Energy spectra of the reconstructed gammas after selection of several fibers at different tagged energies
Peak (MeV) E.R. (FWHM) 2.9........................ 4.9 % 4.0........................ 4.0 % 7.6........................ 3.4 % 8.6........................ 2.7 % 9.6........................ 2.6 % 10.3 ..................... 2.5 %
Inbeam tests180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD410 MeV gamma beam at TUD
Martín Gascón Santiago de Compostela, December 10 th, 2010 32/34
Motivation Characterization Inbeam tests
Calibration
Wrapping
ProtoZero
Comparison with simulations
Comparison for 4 MeV tagged gammas
Left: frontal view in the R3BSim program of the beam profile, together with the entrance position in the prototype for 1000 emitted gammas (depicted in red dots).Right: Beam Profile as tested in the R3BSim program.
Energy deposition (%) Multiplicity distribution
EX
PER
IME
NTA
LSI
MU
LA
TE
DInbeam tests
180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD
Mean Multiplicity Experimental: 2.32 Simulation: 2.45
410 MeV gamma beam at TUD
Martín Gascón Santiago de Compostela, December 10 th, 2010 33/34
Motivation Characterization Inbeam tests
Wrapping
Comparison with simulations
Experimental and simulated observables as a function of the tagged gamma energies.Comparison between simulation and experiment, addingback the energy deposited in the15 crystals, for three different tagged gamma energies.
Inbeam tests180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD
energy resolution full energy peak efficiency crystal multiplicity
410 MeV gamma beam at TUD
Martín Gascón Santiago de Compostela, December 10 th, 2010 34/34
Motivation Characterization Inbeam tests
The main parameters affecting the energy resolution have been systematically studied.
The 4.4% at 662 keV obtained with small samples coupled to 1 cm2 APD was better than those previously reported in literature.
The energy resolution for 13 cm crystals get worse since their light output is lower, however the values obtained for some of the APD-crystal assemblies were close to 5% @ 1 MeV, indicating that they are a suitable solution for the CALIFA Barrel.
Remarkably different performances were found among the measured samples, even for two samples coming from the same provider.
Prototype CsI(Tl) crystals + APDs were found to have a linear response for protons with energies between 90 and 180 MeV and for gammas between few keV and 10 MeV.
The obtained energy resolutions for protons fulfills the Calorimeter requirements.
The tests performed at TU Darmstadt showed the effectiveness of the addback procedure.
The simulation of these prototypes reproduced the experimental results with regard of the observables obtained in the CALIFA simulation and particularly in terms of energy deposition and crystal multiplicity distribution.
Conclusions
Martín Gascón Santiago de Compostela, December 10 th, 2010 35/34
Motivation Characterization Inbeam tests
Thank you for your attention
Martín Gascón Santiago de Compostela, December 10 th, 2010 36/34
Motivation Characterization Inbeam tests
Extra slides
Martín Gascón Santiago de Compostela, December 10 th, 2010 37/34
Motivation Characterization Inbeam tests
Test with prototype samples: LAAPD readout
Config. 1: single power suply and preamp.
Modest improvement in the energy resolution (from 6.7% to 6.5%)
E.R. depends on
Crystal quality Optical coupling Crystal wrapping Light output Temperature drifts
LAAPD readout Amplifier gain Shaping time Bias voltage NonUniformity
Config. 2: two power supply and 2 preamps.
Energy resolution as a function of the bias voltage. Config. 1 used a single power supply and a preamplifier; config. 2 used two independent voltage supplies and the currents were added in.
Conclusions
Characterization
Martín Gascón Santiago de Compostela, December 10 th, 2010 38/34
Motivation Characterization Inbeam tests
CalibrationWrapping
Spectra obtained for a prototype configuration with 15 crystals using Co56 radioactive source.
ProtoZero
Addback spectrum for Co56 radioactive source.
Inbeam tests
Energy reconstruction180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD410 MeV gamma beam at TUD
Martín Gascón Santiago de Compostela, December 10 th, 2010 39/34
Motivation Characterization Inbeam tests
Energy calibration
Correlation between neighbors A gain relation between #1 and #2 and between #3 and #4 allows calibration
The energy calibration was performed with protons at 92, 120 and 180 MeV ( 84, 117 and 173 MeV after DSSSD, Box)
Energy calibration
Inbeam tests
Correlation spectra obtained for neighbor crystals
180 MeV proton beam at TSL 6.1 MeV gamma beam at CMAM 410 MeV gamma beam at TUD180 MeV proton beam at TSL
Martín Gascón Santiago de Compostela, December 10 th, 2010 40/34
Motivation Characterization Inbeam tests
Prototype crystals characterization
Inbeam test with 6.1 MeV gamma beam at CMAMCsI(Tl) crystals + APDs have a linear response between 511 keV and 6.1 MeV,The reconstructed peak for 6.1 MeV gammas showed an E.R.= 2.8%, not so far from the 2.2% estimated by the simulation. Inbeam test with 410 MeV gamma beam at TUD DarmstadtThis test showed the effectiveness of the addback procedure in the range (0.510 MeV)The simulation reproduces the experimental results in terms of energy deposition and crystal multiplicity distribution
Inbeam tests with 180 MeV proton beam at TSL CsI(Tl) crystals + APDs have a linear response between 90 and 180 MeV E.R. = 1% (180 MeV) which fulfills Calorimeter requirements. Peak degradation can be solved using thinner wrapping.
Prototype test beams
Conclusions
Crystals with the largest exit face gave the largest light output. Important differences between lightcollection nonuniformity and energy resolution for each crystal, even for two samples from the same provider. The individual readout system for each of the two channels improved energy resolution, at the expense of greater complexity in both the electronics and the data analysis. The results obtained with some of the APDcrystal assemblies were close to 5% (FWHM) energy resolution for 1 MeV photons, indicating that they are a suitable solution for the CALIFA Barrel.
Martín Gascón Santiago de Compostela, December 10 th, 2010 41/34
Motivation Characterization Inbeam tests
Why CsI(Tl) + APD
Characterization
Estimated CsI(Tl) emission spectrum
CsI(Tl)
used in several experiments (Babar, Belle) cheap to make, easy
to handle, slightly hygroscopic High light yield
(~60000 ph/MeV) Good energy
resolution
Spectral response extends into long wavelengths. Ideal for CsI(Tl) crystals Higher quantum efficiency than
PMTs Higher gain than PIN Diodes Insensitive to magnetic fields
APDs
NaI(Tl) CsI(Tl) CsI(Na) BGO LYSO PWO CsI (pure)
5.29 3.86 3.67 4.51 4.51 7.13 7.1 8.29 4.5163000 49000 39000 60000 45000 9000 32000 100 16800< 3% 3.5% 7% 6% 7.5% 10% 7.1% >10% 7.5%N/A N/A 3.8% 4.9% N/A 8.3% N/A N/A 4.3%
380350 310 fast
550 420 480 420 420 315430 415
25 25/213 620 fast 1000 630 300 41 6 35/6yes yes yes slightly yes no no no slightly
Cost (per cm3) $30 $30 $2 $5 $5 $9 N/A $2 $5
LaBr3 LaBr3
Density (g/cm3)
Light Output (ph/MeV)E/E 662 keV (PMT)
E/E 662 keV (APD)
Peak(nm)
Fast Decay (ns)
Higroscopic
APD Quantum efficiency (%)
Martín Gascón Santiago de Compostela, December 10 th, 2010 42/34
Motivation Characterization Inbeam tests
Test with prototype samples: crystal wrapping
Averaged Lightpulse resolutions and energy resolution (FWHM) obtained using a LED with different 10x10 mm2 exit face crystals and different wrapping configurations, coupled to an XP5A08 PMT without optical grease. 1x,2x,3x,6x is the number of layers, and TF is Teflon tape
For small samples: four 75 mthick layers of Teflon tape covered by a 5 mthick layer of aluminized Mylar Best results for prototype crystals are generally achieved with 2 layers of ESR
E.R. depends on
Crystal quality Optical coupling Crystal wrapping Light output Temperature drifts
Amplifier gain Shaping time Bias voltage NonUniformity
Characterization
Best wrappings for small and prototype crystals
Setup for determining the optimal wrapping configuration for prototype crystals.
Wrapping configuration for prototype crystalsWrapping configuration for small crystals
Wrapping L.P.R (%) E.R. (%)2x ESR 5.90 15.441x ESR 5.97 15.80
1x ESR + 1x TF 6.01 16.281x ESR + 2x TF 6.03 15.721x ESR + 3x TF 6.02 15.581x ESR + 6x TF 6.11 16.60
Crystal wrapping E.R. (%)
Teflon + Aluminum foil 10.00 ± 0.098.68 ± 0.09
Teflon + Copper tape 8.41 ± 0.087.48 ± 0.08
Teflon tape (300 m) 25.95 ± 0.34
Teflon + Metalic adhesive tape
Teflon + Aluminized Mylar
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Motivation Characterization Inbeam tests
Test with prototype samples: Amplifier gain and shaping time
The best results were generally achieved when the amplifier gain was set to cover the full dynamic range of the MCA Shaping times between 4 and 8 s seemed to be a good compromise: they provided good energy resolution without incurring pileup effects.
E.R. depends on
Crystal quality Optical coupling Crystal wrapping Light output Temperature drifts
Amplifier gain Shaping time Bias voltage NonUniformity
Left: Energy resolution vs. amplifier gain for 4 s shaping time. Right: Energy resolution vs. shaping time for 1, 5 and 10 cm long crystals coupled to a S86641010 APD (4 s shaping time and 380 V bias voltage).
Conclusions
Conclusions
Characterization
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Motivation Characterization Inbeam tests
APDs: Bias voltage and gain curves
Left: Energy resolution vs. bias voltage, keeping the photopeak at a constant channel, for a 5 cm (top) and 13 cm long crystals (bottom) coupled to LAAPDs. Right: Typical gain curves of the S86641010 APD (top) and S86641010 2 channel APD (bottom) using CsI(Tl) crystals.
Conclusions
bias voltage variation below 0.35V can guarantee a gain variation smaller than 1%
Relative gain variation due to bias voltage variation for all crystals.
Characterization
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Motivation Characterization Inbeam tests
APD characterization
Procedure to compare different APD series and to disentangle the APD contribution to the energy resolution
APD # A.A. Cap. LPR 1 10x10 std 406 5.2% 202 10x10 std 404 5.4% 223 10x10 std 410 5.3% 84 10x10 std 411 5.5% 75 7x14 std 332 7.2% 236 7x14 std 322 8.1% 237 7x14 std 332 8.7% 328 7x14 std 333 9.2% 399 7x14 low 491 7.5% 2410 7x14 low 484 8.0% 3011 7x14 low 493 8.2% 3112 7x14 low 492 9.8% 32
Cap=Capacitance
O.Vb ID(nA)
A.A.=active area (mm2)
O.Vb = Optimal bias voltage (Volts)LPR = Light pulse resolution @ 5.105 eh
Characterization
Experimental setup for comparing different APD series
The APD contribution to the energy resolution was found to be 0.12% for the 10x10 APD.
The APD dark current can be obtained using a NHQ 225 ISEG power supply
The 10x10 Hamamatsu APD showed the best performances.
APD characterization