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Scientific Update February 2009

Zirconia Fundamentals

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Scientific Update February 2009 • Critical Factors for Success • Material Updates • Biological Issues All-ceramic products Material Update • e.max CAD/e.m ax Press – Lithium Disilicate Material Properties • Inlays • Onlays • Veneers • Thin Veneers (press) • Crowns • Anterior Bridges (press) Indications IPS e.max Press and CAD Clinical Studies

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Page 1: Zirconia Fundamentals

Scientific Update

February 2009

Page 2: Zirconia Fundamentals

Material Update

•e.max CAD/e.max Press– Lithium Disilicate

Page 3: Zirconia Fundamentals

Material Properties

Page 4: Zirconia Fundamentals

Indications

•Inlays•Onlays•Veneers •Thin Veneers (press)•Crowns•Anterior Bridges (press)

Page 5: Zirconia Fundamentals

IPS e.max Press and CADClinical Studies

Page 6: Zirconia Fundamentals

IPS e.max Press Crowns (3 to 5 years)

•Böning, Dresden, D 40 Crowns•Esquivel, San Antonio, USA 36 Crowns•Stappert, Freiburg, D 30 Crowns•Watson, London, USA 30 Crowns•Dumfahrt, Innsbruck, A 24 Crowns•Sorensen, Portland, USA 16 Crowns•Edelhoff, Aachen, D 121 Crowns

Page 7: Zirconia Fundamentals

IPS e.max Press Bridges (3 to 5 years)

•Böning, Dresden, D 14 •Anusavice, Gainesville, USA 30 •Kern, Kiel, D 37 •Sorensen, Portland, USA 56

Inlay-retained bridges•Kern, Kiel, D 45 •Göring, Zurich, CH 16

Adhesive bridges•Ries, Würzburg, D 80

Page 8: Zirconia Fundamentals

IPS e.max CAD - MO

Crowns (MO)• Mörmann, Zurich, CH (3year) 60 • Kelly, UConn, USA 51• Nathanson, Boston, USA 30• Sorensen, Portland, USA 20

Page 9: Zirconia Fundamentals

IPS e.max CAD LT Crowns

•Reich, Leipzig: e.max CAD LT for CEREC – 41 posterior crowns

•Beuer, München: e.max CAD LT for Everest – 30 crowns (mainly anterior)

•Bindl, Zürich: e.max CAD LT for CEREC – 30 crowns

•Fasbinder, Ann Arbor: e.max CAD LT for CEREC – 61 crowns

Page 10: Zirconia Fundamentals

IPS e.max Press and CADEsthetics

Page 11: Zirconia Fundamentals

IPS e.max Translucency Overview

e.max CAD

LT

e.max CAD

MO

e.max CAD

HT

Empress CAD

LT

Empress CAD

HT

Page 12: Zirconia Fundamentals
Page 13: Zirconia Fundamentals

•Higher edge strength vs. traditional glass ceramic materials (can be finished thinner without chipping)

•Low viscosity of heated ingot enables pressing to very thin dimension (minimal prep or no-prep veneers)

•Chameleon effect due to higher translucency

Page 14: Zirconia Fundamentals

•Please observe the following procedure for the fabrication of thin veneers:

– Apply the spacer to the preparation or tooth to be treated according to the veneer preparation guidelines

– For thin veneers without preparation, locate the restoration margins in the proximal area as well as along the gingival margin.

– Observe the minimum thickness of the veneer.– Sprue, invest, press, divest and remove the reaction layer according to the

stipulations – It is possible to apply IPS e.max Ceram Incisal or Transpa.– Conduct the Stain and Glaze firing with IPS e.max Ceram.– Thin veneers have to be adhesively cemented.

Page 15: Zirconia Fundamentals

Material Thickness RequirementsThe following material thicknesses must be observed to produce the desired tooth color and provide adequate strength:

Page 16: Zirconia Fundamentals

IPS e.max Press Thin Veneer

•IPS e.max Press can be used for the fabrication of very thin veneers (minimal Prep). If sufficient space is available, e.g. retrusion of a tooth, no preparation is required.

•The following minimum thicknesses for fabricating thin veneers have to be observed:

labial incisal

0.3 mm 0.4 mm

Page 17: Zirconia Fundamentals
Page 18: Zirconia Fundamentals

Factors affecting strength

•Crystallization procedure•Bulk of material•Bonding vs. cementation

Page 19: Zirconia Fundamentals

Effect of Heat Treatment on Strength of Dental Glass-Ceramic Discs

Page 20: Zirconia Fundamentals

Question asked

•What happens if the firing parameters of the standard crystallization program are changed?

Objective•To examine the effect on biaxial flexure strength by altering the heat treatment of the e.max CAD by changing the closing time, heating rate and long term cooling

Page 21: Zirconia Fundamentals

Common shortcuts

•Four groups were used for this study:– (1) Control – manufacturer’s instructions– (2) Rapid Closing - manufacturer’s instructions but the closing time is

reduced from 6 min to 18 s – (3) Increased Heating Rate - manufacturer’s instructions except the initial

heating rate is changed from 30ºC/min to 90ºC/min and – (4) No long term cooling - manufacturer’s instructions except no long term

cooling is used.

Page 22: Zirconia Fundamentals

Strength was studied•An ISO 6782 sized disc (1.2 mm in thickness and 15.5 mm in diameter) was scanned using the Cerec InLab (Sirona).

•Twenty specimens were milled for each group in four shades (five in each of A3, A3.5, B1 and BL2) using standard milling.

•The specimens were fired and glazed in one firing according to the firing parameters of each group in a P500 Programat oven (Ivoclar Vivadent).

•Specimens were tested using a universal testing machine (Instron Corporation) at a crosshead speed of 0.5 mm/min using a pin on three ball configuration.

Page 23: Zirconia Fundamentals

Effect of Treatments

Strength Versus Treatment

200.0220.0240.0260.0280.0300.0320.0340.0360.0380.0400.0

Control RapidClosing

IncreasedHeating

Rate

No LongTerm

Cooling

Page 24: Zirconia Fundamentals

Question asked How does cementation affect the failure load for e.max CAD and zirconia core restorations?

ObjectiveTo measure the fracture load of CAD/CAM lithium disilicate glass-ceramic crowns (e.maxCAD, Ivoclar Vivadent, Inc.) and zirconia core (Lava core, Lave Ceram 3M/ESPE) cemented either conventionally (Zinc Phosphate, Fleck’s) or adhesively (Multilink Automix, Ivoclar Vivadent, Inc.).

Page 25: Zirconia Fundamentals

Thickness and Cementation Groups

Four groups were used for this study:

(1) e.max CAD LT full contour and conventional cementation

(2) zirconia core/veneered and conventional cementation

(3) e.max CAD LT full contour and adhesive cementation

(4) zirconia core/veneered and adhesive cementation.

Page 26: Zirconia Fundamentals

Load to Failure was measured

Ten specimens were produced for each group. A standardized molar crown was scanned using the Cerec InLab (Sirona). Twenty crowns were designed with recommended dimensions for lithium-disilicate material. The specimens were fired and glazed according to the manufacturer’s instructions in a P500 Programat oven (Ivoclar Vivadent, Inc.). Twenty copings with proper support were milled in zirconia using the Lava system. These copings were layered in a matrix to full anatomy. The occlusal morphology was the same for all the crowns in the study. All crowns were cemented to composite (Heliomolar, Ivoclar Vivadent) preparations which were formed from the internal surface of each crown using either conventional cementation (Fleck’s Zinc Phosphate) or adhesive cementation (Multilink Automix) and stored in water for 24 h at 37°C. The crowns were loaded using a 15 mm diameter steel ball at a crosshead speed of 0.5 mm/min with an Instron Universal Testing machine.

Page 27: Zirconia Fundamentals

crown crunch test

0500

100015002000250030003500

MultilinkAutomix

Fleck'sCement

MultilinkAutomix

Fleck'sCement

lava zirconia lava zirconia e.max CAD e.max CAD

Mea

n br

eaki

ng lo

ad [N

]

Page 28: Zirconia Fundamentals

Zirconia Restorations

Page 29: Zirconia Fundamentals

Conclusion

Within this study, adhesive cementation increased the failure load of CAD/CAM crowns, though no statistical difference was found between the crown materials.

Page 30: Zirconia Fundamentals

Lithium Biocompatibility

Page 31: Zirconia Fundamentals
Page 32: Zirconia Fundamentals

Summary

•……..tended towards increasing cytotoxicity, however were less cytotoxic than several commonly used composites and comparable to several alloys and glass ionomers.

Page 33: Zirconia Fundamentals

Scientific Update

July 2008