WORK ORDER NUMBER: 17-03-0091 - BUR Replacement …burreplacementterminal.com/pdf/EFI-Attachment-C-WO-17-03-0091.pdf · WORK ORDER NUMBER: 17-03-0091 Analytical ... certifies that

WORK ORDER NUMBER: 17-03-0091

Analytical Report ForClient: Andersen Environmental

Client Project Name: Burbank Airport / 9836002041Attention: Brian Martasin

5261 West Imperial HighwayLos Angeles, CA 90045-6231

Approved for release on by:Stephen NowakProject Manager

AIR SOIL WATER MARINE CHEMISTRY

Eurofins Calscience, Inc. (Calscience) certifies that the test results provided in this report meet all NELAC requirements for parameters for which accreditation isrequired or available. Any exceptions to NELAC requirements are noted in the case narrative. The original report of subcontracted analyses, if any, is attached tothis report. The results in this report are limited to the sample(s) tested and any reproduction thereof must be made in its entirety. The client or recipient of thisreport is specifically prohibited from making material changes to said report and, to the extent that such changes are made, Calscience is not responsible, legally orotherwise. The client or recipient agrees to indemnify Calscience for any defense to any litigation which may arise.

04/07/2017

Supplemental Report 1

The original report has been revised toinclude the Level III deliverablespackage.

Page 1 of 335

mailto:[email protected]

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Contents

7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501

Client Project Name: Burbank Airport / 9836002041

Work Order Number: 17-03-0091

1 Work Order Narrative. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

2 Sample Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

3 Client Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53.1 EPA 8015B (M) Diesel and Motor Oil Ranges (Aqueous). . . . . . . . . . . . . . . . . . . . . 53.2 EPA 6010B/7470A CAC Title 22 Metals (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . 63.3 EPA 7470A Mercury (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83.4 EPA 8082 PCB Aroclors (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93.5 EPA 8270C SIM PAHs (Aqueous). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

4 Quality Control Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124.1 MS/MSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124.2 PDS/PDSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 144.3 LCS/LCSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

5 Sample Analysis Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

6 Glossary of Terms and Qualifiers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

7 Chain-of-Custody/Sample Receipt Form. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

8 Level III Data Package - Case Narrative. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

8.1 EPA 8015B ( M ) Diesel + Motor Oil ( Aqueous ). . . . . . . . . . . . . . . . . . . . . . . . . . . 28

8.2 EPA 6010B ICP Metals ( Aqueous ). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82

8.3 EPA 7470A Mercury ( Aqueous ). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 157

8.4 EPA 8082 PCB ( Aqueous ). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 196

8.5 EPA 8270C SIM PAH ( Aqueous ). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 257

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Condition Upon Receipt: Samples were received under Chain-of-Custody (COC) on 03/01/17. They were assigned to Work Order 17-03-0091. Unless otherwise noted on the Sample Receiving forms all samples were received in good condition and within the

recommended EPA temperature criteria for the methods noted on the COC. The COC and Sample Receiving Documents are

integral elements of the analytical report and are presented at the back of the report. Holding Times: All samples were analyzed within prescribed holding times (HT) and/or in accordance with the Calscience Sample Acceptance

Policy unless otherwise noted in the analytical report and/or comprehensive case narrative, if required. Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15

minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being

received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time. Quality Control: All quality control parameters (QC) were within established control limits except where noted in the QC summary forms or

described further within this report. Subcontractor Information: Unless otherwise noted below (or on the subcontract form), no samples were subcontracted. Additional Comments: Air - Sorbent-extracted air methods (EPA TO-4A, EPA TO-10, EPA TO-13A, EPA TO-17): Analytical results are converted from

mass/sample basis to mass/volume basis using client-supplied air volumes. Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC

results are always reported on a wet weight basis.

Work Order Narrative


Work Order: 17-03-0091 Page 1 of 1

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Sample Identification Lab Number Collection Date and Time Number ofContainers

Matrix

EB2-2017-03-01 17-03-0091-1 03/01/17 07:30 4 Aqueous

F-DU1-S-10-03 17-03-0091-2 03/01/17 07:56 1 Solid

F-DU1-S-10-08 17-03-0091-3 03/01/17 08:12 1 Solid

F-DU1-S-10-15 17-03-0091-4 03/01/17 08:20 1 Solid

Sample Summary


Client: Andersen Environmental

5261 West Imperial Highway

Los Angeles, CA 90045-6231

Work Order: 17-03-0091

Project Name: Burbank Airport / 9836002041

PO Number:

Date/TimeReceived:

03/01/17 17:25

Number ofContainers:

7

Attn: Brian Martasin

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Client Sample Number Lab SampleNumber

Date/TimeCollected

Matrix Instrument DatePrepared

Date/TimeAnalyzed

QC Batch ID

EB2-2017-03-01 17-03-0091-1-D 03/01/1707:30

Aqueous GC 45 03/03/17 03/04/1700:55

170303B04

Comment(s): - Motor Oil Range Organics (C17-C44) uses a Diesel Range Organics (C10-C28) standard for quantitation and quality control.

Parameter Result RL DF Qualifiers

TPH as Diesel ND 100 1.00

TPH as Motor Oil ND 100 1.00

Surrogate Rec. (%) Control Limits Qualifiers

n-Octacosane 96 68-140

Method Blank 099-14-355-9 N/A Aqueous GC 45 03/03/17 03/03/1721:42

170303B04

Comment(s): - Motor Oil Range Organics (C17-C44) uses a Diesel Range Organics (C10-C28) standard for quantitation and quality control.


TPH as Motor Oil ND 100 1.00

Analytical Report


Andersen Environmental



Date Received: 03/01/17


Preparation: EPA 3510C

Method: EPA 8015B (M)

Units: ug/L

Project: Burbank Airport / 9836002041 Page 1 of 1

RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.

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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

EB2-2017-03-01 17-03-0091-1-A 03/01/1707:30

Aqueous ICP 7300 03/03/17 03/07/1714:18

170303LA5


Antimony ND 0.0150 1.00

Arsenic ND 0.0100 1.00

Barium ND 0.0100 1.00

Beryllium ND 0.0100 1.00

Cadmium ND 0.0100 1.00

Chromium ND 0.0100 1.00

Cobalt ND 0.0100 1.00

Copper ND 0.0100 1.00

Lead ND 0.0100 1.00

Molybdenum ND 0.0100 1.00

Nickel ND 0.0100 1.00

Selenium ND 0.0150 1.00

Silver ND 0.00500 1.00

Thallium ND 0.0150 1.00

Vanadium ND 0.0100 1.00

Zinc ND 0.0100 1.00

Analytical Report







Preparation: EPA 3010A Total

Method: EPA 6010B

Units: mg/L



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

Method Blank 097-01-003-16353 N/A Aqueous ICP 7300 03/03/17 03/06/1712:15

170303LA5


Antimony ND 0.0150 1.00

Arsenic ND 0.0100 1.00

Barium ND 0.0100 1.00

Beryllium ND 0.0100 1.00

Cadmium ND 0.0100 1.00

Chromium ND 0.0100 1.00

Cobalt ND 0.0100 1.00

Copper ND 0.0100 1.00

Lead ND 0.0100 1.00

Molybdenum ND 0.0100 1.00

Nickel ND 0.0100 1.00

Selenium ND 0.0150 1.00

Silver ND 0.00500 1.00

Thallium ND 0.0150 1.00

Vanadium ND 0.0100 1.00

Zinc ND 0.0100 1.00

Analytical Report








Method: EPA 6010B

Units: mg/L



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

EB2-2017-03-01 17-03-0091-1-A 03/01/1707:30

Aqueous Mercury 07 03/03/17 03/06/1716:23

170303LA1


Mercury ND 0.000500 1.00

Method Blank 099-04-008-8139 N/A Aqueous Mercury 07 03/03/17 03/03/1715:53

170303LA1


Mercury ND 0.000500 1.00

Analytical Report








Method: EPA 7470A

Units: mg/L



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

EB2-2017-03-01 17-03-0091-1-B 03/01/1707:30

Aqueous GC 66 03/02/17 03/02/1718:08

170302L01


Aroclor-1016 ND 1.0 1.00

Aroclor-1221 ND 1.0 1.00

Aroclor-1232 ND 1.0 1.00

Aroclor-1242 ND 1.0 1.00

Aroclor-1248 ND 1.0 1.00

Aroclor-1254 ND 1.0 1.00

Aroclor-1260 ND 1.0 1.00

Aroclor-1262 ND 1.0 1.00

Aroclor-1268 ND 1.0 1.00


Decachlorobiphenyl 62 50-135

2,4,5,6-Tetrachloro-m-Xylene 76 50-135

Method Blank 099-12-533-1252 N/A Aqueous GC 66 03/02/17 03/02/1717:15

170302L01


Aroclor-1016 ND 1.0 1.00

Aroclor-1221 ND 1.0 1.00

Aroclor-1232 ND 1.0 1.00

Aroclor-1242 ND 1.0 1.00

Aroclor-1248 ND 1.0 1.00

Aroclor-1254 ND 1.0 1.00

Aroclor-1260 ND 1.0 1.00

Aroclor-1262 ND 1.0 1.00

Aroclor-1268 ND 1.0 1.00


Decachlorobiphenyl 80 50-135

2,4,5,6-Tetrachloro-m-Xylene 79 50-135

Analytical Report








Method: EPA 8082

Units: ug/L



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

EB2-2017-03-01 17-03-0091-1-C 03/01/1707:30

Aqueous GC/MS EEE 03/07/17 03/08/1711:33

170307L09


Naphthalene ND 0.20 1.00

2-Methylnaphthalene ND 0.20 1.00


Acenaphthylene ND 0.20 1.00

Acenaphthene ND 0.20 1.00

Fluorene ND 0.20 1.00

Phenanthrene ND 0.20 1.00

Anthracene ND 0.20 1.00

Fluoranthene ND 0.20 1.00

Pyrene ND 0.20 1.00

Benzo (a) Anthracene ND 0.20 1.00

Chrysene ND 0.20 1.00

Benzo (k) Fluoranthene ND 0.20 1.00

Benzo (b) Fluoranthene ND 0.20 1.00

Benzo (a) Pyrene ND 0.20 1.00

Indeno (1,2,3-c,d) Pyrene ND 0.20 1.00

Dibenz (a,h) Anthracene ND 0.20 1.00

Benzo (g,h,i) Perylene ND 0.20 1.00


Nitrobenzene-d5 93 28-139

2-Fluorobiphenyl 88 33-144

p-Terphenyl-d14 99 23-160

Analytical Report








Method: EPA 8270C SIM PAHs

Units: ug/L



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

Method Blank 099-06-008-954 N/A Aqueous GC/MS EEE 03/07/17 03/08/1710:32

170307L09


Naphthalene ND 0.20 1.00



Acenaphthylene ND 0.20 1.00

Acenaphthene ND 0.20 1.00

Fluorene ND 0.20 1.00

Phenanthrene ND 0.20 1.00

Anthracene ND 0.20 1.00

Fluoranthene ND 0.20 1.00

Pyrene ND 0.20 1.00

Benzo (a) Anthracene ND 0.20 1.00

Chrysene ND 0.20 1.00

Benzo (k) Fluoranthene ND 0.20 1.00

Benzo (b) Fluoranthene ND 0.20 1.00

Benzo (a) Pyrene ND 0.20 1.00

Indeno (1,2,3-c,d) Pyrene ND 0.20 1.00

Dibenz (a,h) Anthracene ND 0.20 1.00

Benzo (g,h,i) Perylene ND 0.20 1.00


Nitrobenzene-d5 95 28-139

2-Fluorobiphenyl 84 33-144

p-Terphenyl-d14 104 23-160

Analytical Report









Units: ug/L



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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number

17-02-2472-3 Sample Aqueous ICP 7300 03/03/17 03/06/17 12:43 170303SA5

17-02-2472-3 Matrix Spike Aqueous ICP 7300 03/03/17 03/06/17 12:45 170303SA5

17-02-2472-3 Matrix Spike Duplicate Aqueous ICP 7300 03/03/17 03/06/17 12:46 170303SA5

Parameter SampleConc.

SpikeAdded

MSConc.

MS%Rec.

MSDConc.

MSD%Rec.

%Rec. CL RPD RPD CL Qualifiers

Antimony ND 0.5000 0.5423 108 0.5474 109 72-132 1 0-10

Arsenic ND 0.5000 0.5671 113 0.5713 114 80-140 1 0-11

Barium 0.05187 0.5000 0.6065 111 0.6201 114 87-123 2 0-6

Beryllium ND 0.5000 0.5528 111 0.5631 113 89-119 2 0-8

Cadmium ND 0.5000 0.5229 105 0.5311 106 82-124 2 0-7

Chromium ND 0.5000 0.5413 108 0.5495 110 86-122 1 0-8

Cobalt ND 0.5000 0.5416 108 0.5403 108 83-125 0 0-7

Copper ND 0.5000 0.5321 106 0.5414 108 78-126 2 0-7

Lead ND 0.5000 0.5291 106 0.5282 106 84-120 0 0-7

Molybdenum ND 0.5000 0.5617 112 0.5617 112 78-126 0 0-7

Nickel ND 0.5000 0.5419 108 0.5439 109 84-120 0 0-7

Selenium ND 0.5000 0.5520 110 0.5622 112 79-127 2 0-9

Silver ND 0.2500 0.2564 103 0.2667 107 86-128 4 0-7

Thallium ND 0.5000 0.5573 111 0.5627 113 79-121 1 0-8

Vanadium ND 0.5000 0.5280 106 0.5393 108 88-118 2 0-7

Zinc 0.05225 0.5000 0.6224 114 0.8124 152 89-131 26 0-8 3,4

Quality Control - Spike/Spike Duplicate








Method: EPA 6010B


RPD: Relative Percent Difference. CL: Control Limits

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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number

17-02-2379-2 Sample Aqueous Mercury 07 03/03/17 03/03/17 15:57 170303SA1

17-02-2379-2 Matrix Spike Aqueous Mercury 07 03/03/17 03/03/17 16:00 170303SA1

17-02-2379-2 Matrix Spike Duplicate Aqueous Mercury 07 03/03/17 03/03/17 16:02 170303SA1

Parameter SampleConc.

SpikeAdded

MSConc.

MS%Rec.

MSDConc.

MSD%Rec.


Mercury ND 0.01000 0.009282 93 0.009305 93 75-120 0 0-20

Quality Control - Spike/Spike Duplicate








Method: EPA 7470A



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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed PDS/PDSD BatchNumber

17-02-2379-2 Sample Aqueous Mercury 07 03/03/17 00:00 03/03/17 15:57 170303SA1

17-02-2379-2 PDS Aqueous Mercury 07 03/03/17 00:00 03/03/17 16:04 170303SA1

Parameter Sample Conc. Spike Added PDS Conc. PDS %Rec. %Rec. CL Qualifiers

Mercury ND 0.01000 0.009276 93 75-125

Quality Control - PDS








Method: EPA 7470A



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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS/LCSD Batch Number

099-14-355-9 LCS Aqueous GC 45 03/03/17 03/03/17 22:03 170303B04

099-14-355-9 LCSD Aqueous GC 45 03/03/17 03/03/17 22:24 170303B04

Parameter Spike Added LCS Conc. LCS%Rec.

LCSD Conc. LCSD%Rec.


TPH as Diesel 4000 3869 97 3939 98 51-141 2 0-11

Quality Control - LCS/LCSD








Method: EPA 8015B (M)



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Total number of LCS compounds: 16

Total number of ME compounds: 0

Total number of ME compounds allowed: 1

LCS ME CL validation result: Pass

Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number

097-01-003-16353 LCS Aqueous ICP 7300 03/03/17 03/06/17 12:16 170303LA5

Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers

Antimony 0.5000 0.5199 104 80-120 73-127

Arsenic 0.5000 0.5260 105 80-120 73-127

Barium 0.5000 0.5743 115 80-120 73-127

Beryllium 0.5000 0.5170 103 80-120 73-127

Cadmium 0.5000 0.5326 107 80-120 73-127

Chromium 0.5000 0.5404 108 80-120 73-127

Cobalt 0.5000 0.5565 111 80-120 73-127

Copper 0.5000 0.5438 109 80-120 73-127

Lead 0.5000 0.5361 107 80-120 73-127

Molybdenum 0.5000 0.5354 107 80-120 73-127

Nickel 0.5000 0.5571 111 80-120 73-127

Selenium 0.5000 0.5373 107 80-120 73-127

Silver 0.2500 0.2605 104 80-120 73-127

Thallium 0.5000 0.5641 113 80-120 73-127

Vanadium 0.5000 0.5156 103 80-120 73-127

Zinc 0.5000 0.5669 113 80-120 73-127

Quality Control - LCS








Method: EPA 6010B



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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number

099-04-008-8139 LCS Aqueous Mercury 07 03/03/17 03/03/17 15:55 170303LA1

Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers

Mercury 0.01000 0.01015 102 80-120

Quality Control - LCS








Method: EPA 7470A



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099-12-533-1252 LCS Aqueous GC 66 03/02/17 03/02/17 17:33 170302L01

099-12-533-1252 LCSD Aqueous GC 66 03/02/17 03/02/17 17:51 170302L01

Parameter Spike Added LCS Conc. LCS%Rec.

LCSD Conc. LCSD%Rec.


Aroclor-1016 2.000 2.060 103 1.920 96 50-135 7 0-25

Aroclor-1260 2.000 1.940 97 1.820 91 50-135 6 0-25









Method: EPA 8082



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Total number of LCS compounds: 18

Total number of ME compounds: 0

Total number of ME compounds allowed: 1

LCS ME CL validation result: Pass


099-06-008-954 LCS Aqueous GC/MS EEE 03/07/17 03/08/17 10:52 170307L09

099-06-008-954 LCSD Aqueous GC/MS EEE 03/07/17 03/08/17 11:13 170307L09

Parameter SpikeAdded

LCS Conc. LCS%Rec.

LCSDConc.

LCSD%Rec.

%Rec. CL ME CL RPD RPD CL Qualifiers

Naphthalene 2.000 1.859 93 1.898 95 21-133 2-152 2 0-25

2-Methylnaphthalene 2.000 2.238 112 2.253 113 21-140 1-160 1 0-25

1-Methylnaphthalene 2.000 2.036 102 2.067 103 20-140 0-160 2 0-25

Acenaphthylene 2.000 1.714 86 1.734 87 33-145 14-164 1 0-25

Acenaphthene 2.000 1.769 88 1.756 88 55-121 44-132 1 0-25

Fluorene 2.000 1.798 90 1.754 88 59-121 49-131 2 0-25

Phenanthrene 2.000 1.904 95 1.893 95 54-120 43-131 1 0-25

Anthracene 2.000 1.971 99 1.974 99 27-133 9-151 0 0-25

Fluoranthene 2.000 2.028 101 2.037 102 26-137 8-156 0 0-25

Pyrene 2.000 1.939 97 1.872 94 45-129 31-143 3 0-25

Benzo (a) Anthracene 2.000 1.862 93 1.858 93 33-143 15-161 0 0-25

Chrysene 2.000 1.919 96 1.924 96 17-168 0-193 0 0-25

Benzo (k) Fluoranthene 2.000 1.956 98 2.049 102 24-159 2-182 5 0-25

Benzo (b) Fluoranthene 2.000 1.902 95 1.877 94 24-159 2-182 1 0-25

Benzo (a) Pyrene 2.000 1.978 99 1.949 97 17-163 0-187 1 0-25

Indeno (1,2,3-c,d) Pyrene 2.000 2.024 101 1.979 99 25-175 0-200 2 0-25

Dibenz (a,h) Anthracene 2.000 2.135 107 2.082 104 25-175 0-200 3 0-25

Benzo (g,h,i) Perylene 2.000 2.126 106 2.086 104 25-157 3-179 2 0-25












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Method Extraction Chemist ID Instrument Analytical Location

EPA 6010B EPA 3010A Total 935 ICP 7300 1

EPA 7470A EPA 7470A Total 868 Mercury 07 1

EPA 8015B (M) EPA 3510C 972 GC 45 1

EPA 8082 EPA 3510C 944 GC 66 1

EPA 8270C SIM PAHs EPA 3510C 907 GC/MS EEE 1

Sample Analysis Summary Report



Location 1: 7440 Lincoln Way, Garden Grove, CA 92841

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Qualifiers Definition

* See applicable analysis comment.

< Less than the indicated value.

> Greater than the indicated value.

1 Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sample data was reported without furtherclarification.

2 Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound wasin control and, therefore, the sample data was reported without further clarification.

3 Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. Theassociated LCS recovery was in control.

4 The MS/MSD RPD was out of control due to suspected matrix interference.

5 The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to suspected matrix interference.

6 Surrogate recovery below the acceptance limit.

7 Surrogate recovery above the acceptance limit.

B Analyte was present in the associated method blank.

BU Sample analyzed after holding time expired.

BV Sample received after holding time expired.

CI See case narrative.

E Concentration exceeds the calibration range.

ET Sample was extracted past end of recommended max. holding time.

HD The chromatographic pattern was inconsistent with the profile of the reference fuel standard.

HDH The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbonswere also present (or detected).

HDL The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but lighter hydrocarbons werealso present (or detected).

J Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value isestimated.

JA Analyte positively identified but quantitation is an estimate.

ME LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).

ND Parameter not detected at the indicated reporting limit.

Q Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spikeconcentration by a factor of four or greater.

SG The sample extract was subjected to Silica Gel treatment prior to analysis.

X % Recovery and/or RPD out-of-range.

Z Analyte presence was not confirmed by second column or GC/MS analysis.

Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results arereported on a wet weight basis.

Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes(40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of thestated holding time unless received at the laboratory within 15 minutes of the collection time.

A calculated total result (Example: Total Pesticides) is the summation of each component concentration and/or, if "J" flags are reported,estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zeroconcentrations.

Glossary of Terms and Qualifiers



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Case Narrative

Client Project Name: Burbank Airport / 9836002041 Work Order Number: 17-03-0091

Page 1 of 4

CONDITION UPON RECEIPT:

Eurofins Calscience, Inc. received (1) aqueous sample and (3) solid samples on March 1st, 2017. A total of (7) containers were received in good condition and at a temperature of 1.8°C, which was within the recommended temperature criteria of 0°C – 6°C.

Client Sample ID Lab Sample ID Date & Time Sampled Date & Time Received

EB2-2017-03-01 17-03-0091-1 03/01/17 07:30 03/01/17 17:25 F-DU1-S-10-03 17-03-0091-2 03/01/17 07:56 03/01/17 17:25 F-DU1-S-10-08 17-03-0091-3 03/01/17 08:12 03/01/17 17:25 F-DU1-S-10-15 17-03-0091-4 03/01/17 08:20 03/01/17 17:25

DATA SUMMARY

As per the chain of custody (COC), the sample was analyzed using one or more of the following methodologies:

EPA 6010B Title 22 Metals (Aqueous) EPA 7470A Mercury (Aqueous) EPA 8015B (M) Diesel and Motor Oil Ranges (Aqueous) EPA 8082 PCB Aroclors (Aqueous) EPA 8270C SIM PAHs (Aqueous)

The sample was analyzed within the suggested EPA holding time for the requested methods unless otherwise noted.

Sample results were reported in the RL format.

Any dilutions made to the sample(s) and/or QC will be noted in the following narrative. Reporting limits have been adjusted accordingly.

Any manual integration made to the data will be noted in the following narrative. The initial and amended chromatograms have been included in the data package.

All sample and instrument QC were within acceptance criteria, unless otherwise noted below.

EPA 6010B Title 22 Metals (Aqueous):

Sample -1 was analyzed for Metals by EPA 6010B. The sample was prepared on 03/03/17 and analyzed on 03/07/17 in batch #s 170303LA5 / 170303SA5 on ICP 7300.

Initial Calibration, Initial Calibration Verification, and Initial Calibration Blank:

All values were within acceptance criteria.


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Case Narrative


Page 2 of 4

Continuing Calibration Verification and Continuing Calibration Blank:


ICS A/AB:


Sample and QC:

The method blank was non-detect and the LCS was within acceptance criteria.

A non-client sample was used for the MS/MSD; refer to the MS/MSD summary form for further information.

EPA 7470A Mercury (Aqueous):

Sample -1 was analyzed for Mercury by EPA 7470A. The sample was prepared on 03/03/17 and analyzed on 03/06/17 in batch #s 170303LA1 / 170303SA1 on Mercury 07.

Initial Calibration, Initial Calibration Verification, and Initial Calibration Blank:


Continuing Calibration Verification and Continuing Calibration Blank:


Sample and QC:

The method blank was non-detect and the LCS was within acceptance criteria.

A non-client sample was used for the MS/MSD and PDS; refer to the MS/MSD and PDS summary forms for further information.

EPA 8015B (M) Diesel and Motor Oil Ranges (Aqueous):

Sample -1 was analyzed for Diesel and Motor Oil Ranges by EPA 8015B (M). The sample was prepared on 03/03/17 and analyzed on 03/04/17 in batch # 170303B04 on GC 45.

Initial Calibration and Initial Calibration Verification:

The initial calibration was performed on 12/02/16 on GC 45. The ICAL was within the 20% RSD acceptance criteria and the ICV was within the 30% D acceptance criteria.


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Case Narrative


Page 3 of 4

For the Diesel and Motor Oil Ranges, Diesel is used for the initial calibration and spiking standards. The surrogate recoveries for the samples and QC were calculated from the 5-point surrogate curve analyzed with the Diesel ICAL.

Continuing Calibration Verification:

All values were within the 20% D acceptance criteria.

Sample and QC:

The method blank was non-detect; the LCS/LCSD and all surrogate recoveries were within acceptance criteria.

EPA 8082 PCB Aroclors (Aqueous):

Sample -1 was analyzed for Polychlorinated Biphenyls Aroclors by EPA 8082. The sample was prepared and analyzed on 03/02/17 in batch # 170302L01 on GC 66.


The initial calibration was performed on 02/22/17 on GC 66. The ICAL was within the 20% RSD acceptance criteria and the ICV was within the 15% D acceptance criteria for Aroclors 1016 and 1260. Single point response factors were

generated for all other Aroclors.



Sample and QC:

The method blank was non-detect; the LCS/LCSD and all surrogate recoveries were within acceptance criteria.

EPA 8270C SIM PAHs (Aqueous):

Sample -1 was analyzed for Polynuclear Aromatic Hydrocarbons by EPA 8270C SIM. The sample was prepared on 03/07/17 and analyzed on 03/08/17 in batch # 170307L09 on GC/MS EEE.


The initial calibration was performed on 02/27/17 on GC/MS EEE. The ICAL was within the 15% RSD acceptance criteria and the ICV was within the 20% acceptance criteria.




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Case Narrative


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Tuning Standards:

All instrument tuning standards (DFTPP) were within acceptance criteria.

Sample and QC:

The method blank was non-detect; the LCS/LCSD, all surrogate and internal standard recoveries were within acceptance criteria.


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