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confidence security reliability efficiency productivity value quality flexibility control information accuracy Straight to the heart of the matter. The road to productivity had many bends. Now, the straight tube innovations found only in the OPTIMASS Coriolis mass flow meters provide the shortest path. Processes around the world benefit from their high accuracy, tight re- peatability, low pressure drop, wide flow range, and long-term reliability. Follow your heart. Let KROHNE OPTIMASS meters guide you straight to achieving more productivity. Visit www.krohne.com/northamerica for the straight story on OPTIMASS meters and many other products in productivity improvement applications, or call your local sales representative for details. Achieve More. Get Productive with OPTIMASS. 7000 - high performance 1000 - general purpose 2000 - the latest & largest meter, to 12 inch KROHNE, Inc., 7 Dearborn Road, Peabody, MA (USA) 01960 1-800-356-9464 [email protected] www.krohne.com/northamerica

Straight to the heart of the matter. - KROHNE Groupkrohne.com/fileadmin/content/media-lounge/PDF-US/Optimass...Straight to the heart of the matter. ... Solution: Installation of

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confi dence

security

reliability

effi ciency

productivity value

quality

fl exibility

control

information

accuracy

Straight to the heart of the matter.

The road to productivity had many bends. Now, the straight tube innovations found only in the OPTIMASS Coriolis mass flow meters provide the shortest path.

Processes around the world benefit from their high accuracy, tight re-peatability, low pressure drop, wide flow range, and long-term reliability.

Follow your heart. Let KROHNE OPTIMASS meters guide you straight to achieving more productivity.

Visit www.krohne.com/northamerica for the straight story on OPTIMASS meters and many other products in productivity improvement applications, or call your local sales representative for details.

Achieve More. Get Productive with OPTIMASS.

7000 - high performance

1000 - general purpose

2000 - the latest & largest meter, to 12 inch

KROHNE, Inc., 7 Dearborn Road, Peabody, MA (USA) 019601-800-356-9464 [email protected]

www.krohne.com/northamerica

Optimass Application Story

Application: Beer Brewing at Grolsch in Holland

When Grolsch built their new state of the art brewery at Enschede, they equipped it with KROHNE flowmeters, including OPTIMASS meters for the more demanding applications where there is high viscosity or no conductivity.

In the brewery applications this includes dosing liquid sugar and hops and for measuring carbon dioxide levels in the cold recovery system.

OPTIMASS is capable of high measurement accuracy of 0.1 % for fluids and 0.5% for gasses. Our mass flow meters can measure density and volume flow as well as calculating Brix or Plato with the concentration option.

Grolsch’s tests actually showed better than 0.1% accuracy when dosing 8 kg batches of hops

Observe the ice on the pipe above at right!

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.2

Optimass

Application Note

Brewing Beer with KROHNE - Optimass DECKER – Hop Extract Processing Plant

Customer: Decker Maschinenbau, 93358 Train

For a big Brewing Plant in Holland

Application In the brewing process, the hops are roasted in the pan. There are many different ways of doing this. So, too, with Hop extract processing.

The Optimass T10 measures exact dosing of the Hop extract into a heating chamber at 45°C in order to keep the amount used to the minimum required.This means the optimum cost control with Optimass. To ensure a clear operation and supervision, a galvanically separated output with PROFIBUS© PA is deployed.

Process Parameters: Product : Hop extract Flow Rate : 6 kg/min Viscosity : 20 Pa s Density : 1035 kg/m³ Temperature : 46 °C Pressure drop : 2,9 bar Meter type : OPTIMASS 10T

INDUSTRY: FOOD AND BEVERAGE COUNTRY: GERMANY METER: OPTIMASS T10

R. Schiller KROHNE Munich 28 May 2003

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.3

Optimass

Application Note

Why use Optimass?

Due to the very high viscosity and the subsequent need to reduce the pressure drop, it is necessary to choose a meter whose operating point lies in the lower range of the flow rate.

In this case Optimass shows a marked improvement over the competition.

Zero Stability

Various doses were checked against a certified scale. The following diagram shows how impressive the performance of the new Optimass was. The low flow cutoff was switched off during the tests.

Filling 8kg

7960

7980

8000

8020

8040

- kg

-

-0.06

-0.04

-0.02

0.00

0.02

0.04

0.06

- % -

OPTIMASS (kg) 8008 8018 7988 7987 8014

Scales (kg) 8010 8020 7990 7990 8010

deviation % -0.02 -0.02 -0.03 -0.04 0.05average % -0.01 -0.01 -0.01 -0.01 -0.01

Trial 1 Trial 2 Trial 3 Trial 4 Trial 5

The client is delighted with the results of the measurement tests and the plant has now been delivered to the enduser to be brought into operation.

R. Schiller KROHNE Munich 28 May 2003

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.4

Application Note

Optimass

INDUSTRY: BEVERAGE COUNTRY: COLOMBIA METER: OPTIMASS 80S

CERVECERÍA BAVARIA S.A. is a beer monopoly in Colombia which ranks number 10 of the largest breweries world wide. They have seven plants in Colombia, dominate the beer market in Ecuador and Panama, and produce more than 60% of beer consumed in Peru. Among their plants in Colombia, they have CERVECERÍA LEONA, one of the more modern plants in South America, built in 1994. Because BAVARIA is focused on increasing efficiency, they want to measure several points of the process to detect process loss. So at LEONA they instigated a pilot trial using mass flow meters for wort in kitchens as well as for bright beer after filtration.

Through local representative Control Engineering S.A., KROHNE beat E+H, ABB and Siemens (Danfoss) with the best technology; the lowest pressure drop on process and a reasonable price. But what really impressed LEONA was the wide flow range Optimass could handle, because production will be doubled over the next 5 years, and our meters could make the transition.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.5

2

Application: Beer

Process Parameters Bright beer after filters, Qty: 2 Flow rate: 1000 Hl/h Flow rate projected: 1500 Hl/hr Temperature: 0 °C Pressure: 2.4 bar Density: 1.00 … 1.07 kg/l Viscosity: 1.00 … 1.70 CP Wort after heat exchangers, Qty: 2 Flow rate: 800 Hl/h Flow rate projected: 1200 Hl/hr Temperature: 12 °C Pressure: 6 bar Density: 1.044 … 1.063 kg/l Viscosity: 1.50 … 1.74 CP Why KROHNE?

Straight tube with lower pressure drops No effects on accuracy from pipe vibration Lower installation requirements A wide measuring range

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.6

Application Note

Optimass

Tequila is the most popular drink in Mexico, and also a significant business for the producers, not only on the Mexican market but also internationally. The State of Jalisco is the only State in Mexico permitted to sow Agave and produce Tequila. Jalisco has many Tequila producers and one of the largest in sales is the Jose Cuervo brand. Jose Cuervo also exports Tequila by the 20-ton truckload. They have a filling station where they load the product into the trucks. Why KROHNE? Problem: Fiscal standards of accuracy for sales of alcohol Solution: Installation of reliable Optimass mass flow meters to ensure the accuracy of the invoiced quantity.

Process Conditions: Product: Tequila (alcohol) Pipeline: 2” Stainless Steel Temperature: 25 °C Pressure: 4 kg/cm2 Density: 0.95 Flow rate: 640 LPM Note: The meters have been installed in such a way that they will always be full. This is good engineering practice for this type of application.

Installation No.1: Suspended by two metal rods and two metal belts in a horizontal position from the top of the filling station. Optimass Type: S40 Tri-clamp connections, 120 VAC power supply Pulse output to a batch controller

INDUSTRY: FOOD & BEVERAGE COUNTRY: MEXICO METER: OPTIMASS S40

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.7

2

Application: Fiscal loading of Tequila

Installation No. 2: In a horizontal pipeline

Optimass Type: S40 Tri-clamp connections 120 VAC power supply, Pulse output to a batch controller

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.8

1STRAIGHT TALK

Application Story

Brix Measurement for Fruit Canning in the US

Application

Signature Fruit, based in Modesto, California, is the leading producer of long-life fruit products. Its product range includes peach, pear, apricot and other juices. Signature Fruit markets its products under the brand names Libby's® and Nature´s Orchard TM, as well as under customers' own labels for international and industrial food retail. The mass flowmeters are used during the initial mixing of the bulk syrup, which consists of canners corn syrup, high fructose, and sucrose concentrates to achieve the desired Brix in the concentrate, which is calculated by the control system’s PLC. In the second stage the syrup mix is diluted with water and poured into containers with the fruit.

Problem

Exceptional concentration measurement and avoidance of large pressure drops over a wide flow range

Solution

Why did the client choose KROHNE?

• Single straight tube give low pressure drop enabling reduction in size of meters ordered and resistance to blocking

• Good flow range and turndown enabled reduction in number of meters ordered

• Hygienic connectors available

• Excellent concentration measurement of Brix

Our thanks to Gordon Nickison of KROHNE Inc for this application

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.9

[email protected] www.krohne. 1/1

Chocolate consumption measurement Application 31, OPTIMASS

Customer

Pauly Biskuit, Dessau, Germany

Application Pauly Biscuits is producing Long Life bakery products on seven permanent baking lines and waffles on another seven production lines. In the coating section biscuit bars are double coated with chocolate. In order to measure the chocolate consumption and maintain a constant coating thickness two OPTIMASS T15 with heating jackets are installed, one at the dispensing point and one at the return flow. Process Parameters: Product : Chocolate coating Mass Flow : 1000 and 4000 kg/h Temperature : 45°C Viscosity : 1000 mPas Meter : MFS7000 – T15 with heating jacket

Problem

Accurate consumption measurement Solution

Why did the client choose KROHNE? • Precise Meter • Hygienic version • Excellent References

One of the Pauly Biscuit production lines

App

likat

ione

n

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.10

STRAIGHT TALK

Application Story – loading of milk in FranceCheese Producers sometime have to sell excess milk or buy in from other suppliers according to their production demands and quotas. They have various options available to measure this.

Application :To accurately record the quantity of milk loaded into the tanker trucks from the storage areas of the factory. As the milk is pushed through the pipes by water, density measurement is used to determine the cut-off point so only milk goes into the tankers.

Why did the customer choose KROHNE:The KROHNE sales team in France were able to use their experience to help the customer to choose Coriolis mass flowmeters instead of the weighbridge option, and to demonstrate to his customers that this was a reliable billing solution, without having to resort to custody transfer transactions.

Model chosen:The OPTIMASS 7000 has the technology. With its single straight tube, it is totally cleanable inline and approved for hygienic applications. The density measurement is used to limit the range of density between 1025 Kg/m3 and 1040 Kg/m3, allowing differentiation between the passage of the milk and the water.

Benefits to the customer: Simple daily operation; reduced investment cost with the meter installed online in the loading pipes, avoiding the need for civil engineering works to build a weighbridge.

Coriolis Mass Flow

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.11

Application Note

Optimass

Customer Unilever Bestfood Schweiz, Thayingen, Switzerland Application Unilever Best Foods, known as one of the world’s largest producer of food products, have automated their production line in Thayingen. 10-liter pouches of gourmet salad dressing for restaurants are filled automatically. The plant is designed as a double filling station, enabling two flowmeters to batch two different products into the same pouch, either simultaneously or sequentially, depending on the type of dressing. Each pouch can be filled within 7 seconds. For precise dosing the low flow cut off was taken out completely.

Problem: Accurate batching of high viscosity salad dressing at low flow rates Why KROHNE? Solution:

• High repeatability and accuracy

• DIN 11864-2 All welded design with EHEDG approval suitable for hygienic applications

• Lack of installation restrictions

• Self draining straight tube

• Good experience with KROHNE

INDUSTRY: FOOD COUNTRY: SWITZERLAND METER: OPTIMASS T 15

PDF created with pdfFactory trial version www.software-partners.co.ukCopyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.12

Salad Dressing CH

2

Left: On the production line, each Optimass meter is simply attached to the framework by means of clamps fastened around the meter body, something that would have been impossible with most previous designs of Coriolis mass flowmeters. Such an installation would have had a detrimental affect on the performance of the meter. This is now possible with the 7000 Series due to KROHNE’s patented ‘Adaptive Sensor Technology’ which intelligently ‘tunes’ each meter, independent of external forces and fluid density, to produce an inherently balanced instrument that remains stable in the most demanding processes.

Process Parameters Product: Salad Dressing Mass Flow: 1.2 kg/sec Nominal Pressure: 4 bar Density: 1.05 Viscosity: up to 100 cPs

The finished product

PDF created with pdfFactory trial version www.software-partners.co.ukCopyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.13

Application Note

Optimass

One of the UK’s leading speciality vegetable oil refineries is relying on the installation simplicity and accuracy of KROHNE’s revolutionary OPTIMASS Coriolis mass flowmeters to monitor the flow of their products into road tankers.

Application Vegetable oils with a variable loading temperature and a viscosity of between 8cp and 100cp, are pumped from storage tanks at an average mass flowrate of 60 tonnes per hour using centrifugal pumps. They are routed through two separate pipework systems, and pass through the flowmeters before reaching the loading points. The OPTIMASS meters send a pulse output to a batch controller to measure the mass of oil being pumped; when the totalised mass flow reaches a predetermined level the batch counter stops the pumps.

Above The OPTIMASS meters installed directly in a two metre high inverted u-bend to ensure there are no vapour inclusions within the meter during operation Why KROHNE? The refinery has built up a close relationship with KROHNE over the past decade after the flow and level company solved installation problems experienced with flowmeters. Problem: Installation restrictions and achieving batch process accuracy with Coriolis meters Solution: The innovative design of the 7000 Series, incorporating KROHNE’s

‘Adaptive Sensor Technology’ ensures total flexibility of installation plus superb accuracy and repeatability.

INDUSTRY: FOOD COUNTRY: UK METER: OPTIMASS T50

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.14

2

Process Parameters Product: Vegetable oils Mass Flow: 60 tonnes/hour Temperature: 20°C to 80°C Density: between 850 kg/M3 and 950 kg/m3 Viscosity: between 8 cp and 100 cp

Above: Our KROHNE Service Engineer checking the accuracy of reading after a tanker has been loaded with hard oil Customer Information Karlshamns are a Swedish vegetable oil refinery with the UK offices and refinery in Hull East Yorkshire. They are one of the largest suppliers of Vegetable oils in the UK, supplying both soft and hard oils such as Rapeseed oil, Coconut oil etc.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.15

Application Note

Optimass

This customer, Tovarna Sladkorja Ormoz, is a sugar producer in Slovenia. They use lime milk as a flocculent and require the concentration of lime milk to be constant. In order to achieve this they purchased an Optimass T 50 with the Baumé concentration option. Due to the abrasive nature of lime milk, transition pieces were installed. As the Optimass T 50 meter is measuring at the upper velocity limit (6 m/s) for abrasive applications, after three months' operation the KROHNE agents in Slovenia made a resistance check and removed the instrument to see if any damage on the transition piece or instrument had occurred. More than 47,000 tons of lime milk had passed through the instrument but there was no trace of wear, either on the transition piece or on the instrument. The customer was very satisfied with the measurement.

Why KROHNE? Problem: Accurate control of concentration and resistance to abrasion Solution: The Optimass Titanium meter with its accurate concentration measurement.

INDUSTRY: FOOD COUNTRY: SLOVENIA METER: T 50

Process Parameters Product: lime milk (Suspension of calcium hydroxide in water) Mass Flow: 0 - 50 T/h Flow direction: from down to up Temperature: up to 80°C Nominal Pressure: 6 barg Density: 1070 - 1200 kg/m3

Note the use of transition piece to protect the meter from abrasive process fluids

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.16

1STRAIGHT TALK

Application Story – Bio-Ethanol Production in US & CanadaFuel Ethanol (200 Proof) is a renewable, clean burning & high octane fuel that is better for the environment than gasoline. It is also bio-degradable and far less toxic than fossil fuels and can be used on its own (E100) or blended with gasoline (E10, E85 etc).

Ethanol can be produced from starch/sugar rich feed stocks such as grains/cereals (corn, wheat, rice etc) , potatoes, cassava, beet/sugar cane and today even from cellulosic biomass sources viz. wood chips, switch grass, corn stover's, municipal waste, recycled paper etc.

Of all these feed sources the Dry Grind/Milling process used for corn (or wheat) feed is the most popular in US & Canada. Typical OPTIMASS applications on a Dry Grind/Milling process (shown on right) include density measurement for slurry tanks , liquefaction mash, syrup draw , rectified & final proof measurements.

Liquefaction Mash(feed preparation for fermentors)

Slurry #1 Density ( Slurry Preparation)

Corn Slurry and syrup drawn from evaporators can be extremely nasty & viscous and will clog almost any bent tube designs - it is here that the single straight tube Optimass offers significant benefits.

Also lower pressure drop is a desirable feature as energy optimization is of utmost importance on these high energy intensive processes. It are for these reasons that Krohne is able to demonstrate value over our competitors.

Krohne Inc has over 60+ installation ( and 50 more on order) of OPTIMASS 7000 series (S25/S50 tubes) on the corn slurry/mash & syrup applications . Additionally on each of theseplants our 7000 series (S15 tubes) are installed on liquid ammonia feed lines that feed nutrients into the slurry tanks andfermentors.

Evaporator Syrup Draw

Our thanks to Hemant Narayan, Industry Specialist - Energy & Biofuels at KROHNE America IncFor additional details contact [email protected]

Combined Flow/Density measurement using our OPTIMASS 7000 series (S50 straight tube) on the evaporator syrup draw application (shown below) provides a high investment return by improving the overall dryer process efficiency downstream of the evaporators.

Ammonia Flow

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.17

[email protected]

App

licat

ion

stor

y

Production of Biodiesel

Application OPTIMASS 7000 T40 Custody Transfer

Customer GHP Biodiesel at Oranienburg near Berlin. The Oranienburg Transesterification plant, one of 4 they operate in Germany, was established in 2001. Application Transesterification of animal fats and used oils is done by the classical alkali – process with KOH as catalyst. It is dissolved in Methanol to form an approx. 12,5 % solution, which is added to the plant oil. Separation of Glycerin – phase and Methyl-Esters is done by gravity. The installation was tested against the custody transfer calibration verification equipment and the mass flow accuracy was 0,1 %. Volume flow also showed accuracy of better than 0,3 %. Process Parameters: Product : Organic oils and fats Mass Flow : 33000 kg/h and 16000 kg/h with batching of 2000 l Temperature : 31 °C Density : 0,872 kg/l Pressure : 6 bar

Problem Accurate measurement and batching to Custody Transfer standards Solution Why did the client choose KROHNE? • High accuracy and repeatability • Cost savings due to accurate batching • Approved for Custody Transfer

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.18

1STRAIGHT TALK

Biodiesel in Germany

The Biodiesel Production facility here has a capacity of 25,000 tons pa. This facility also has 12 Optimass DN 15 and DN 25 installed. The oils used for transesterification include rape oil, sunflower oil, and used cooking oils amongst others. Raw glycerine is produced as a byproduct and this can be used by biogas production facilties. There are no other waste products and the methanol used for extraction is recovered and reused.

The photo at right shows one of 4 Optimass T 80 Custody Transfer meters installed in the Tanker loading station at Biowerk Sohland in the Lausitz area of Germany. This is where the Biodiesel produced in the factory is loaded from the storage tanks into the distribution vehicles.

Following the establishment of Biowerk Sohland in 2002, another company, PPM Energie Germany GmbH, was established to build biodiesel plants like the existing installation for national and international customers with capacity between 8,000 and 50,000 t/a, with larger plants envisaged.Plants equipped with Optimass are now in Australia and Austria and 3 are being built for Hungary. They have already provided 6 plants in Germany.

Above and right: some more of the Optimass meters installed in the production facility

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.19

1STRAIGHT TALK

Biodiesel in Germany

The Biodiesel Production facility here has a capacity of 25,000 tons pa. This facility also has 12 Optimass DN 15 and DN 25 installed. The oils used for transesterification include rape oil, sunflower oil, and used cooking oils amongst others. Raw glycerine is produced as a byproduct and this can be used by biogas production facilties. There are no other waste products and the methanol used for extraction is recovered and reused.

The photo at right shows one of 4 Optimass T 80 Custody Transfer meters installed in the Tanker loading station at Biowerk Sohland in the Lausitz area of Germany. This is where the Biodiesel produced in the factory is loaded from the storage tanks into the distribution vehicles.

Following the establishment of Biowerk Sohland in 2002, another company, PPM Energie Germany GmbH, was established to build biodiesel plants like the existing installation for national and international customers with capacity between 8,000 and 50,000 t/a, with larger plants envisaged.Plants equipped with Optimass are now in Australia and Austria and 3 are being built for Hungary. They have already provided 6 plants in Germany.

Above and right: some more of the Optimass meters installed in the production facility

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.20

Our new Tantalum OPTIMASS 7300 A15 is now installed in a vitaminproduction facility at this multinational chemical, pharmaceutical and nutritional company in Switzerland.

Application: The Optimass 7300 C – A15 DN 25 PN 40 doses an aggressive fluid into a distillation column, where a vitamin is produced. The high flow velocity prevents deposition of the process medium on the inside of the tube.

Application Story – Chemical Industry in Switzerland

With thanks to Marc Madacs of Krohne Switzerland for this application note.

Technical data:Measuring range: 0-7000 Kg/hDensity: 0.881 Kg/lTemperature: 78°CPressure: 1.8 bar

Why KROHNE:The only Straight Tube Tantalum meter on the market!

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.21

Application Story Varnish Production at BASF Coatings AGBASF Coatings division develops, produces and markets a range of top quality innovative vehicle, car repair and industrial varnishes and coating materials for buildings and offers the corresponding coating processes. The Münster site is one of the biggest varnish plants in the world with a total area of 400,000 square meters.

In order to operate the mobile paddle mixers used in the colour grinding process without supervision over 36-48 hours BASF used a flowmeter to trigger a leakage alarm. This meter needed to fulfill high specifications in terms of accuracy. The properties of the media made things even more difficult. The raw materials for varnishes are high-viscosity media which are processed at a low flow rate. They have viscosities of 7000mPas and over, and are also shear thinning - their behavior changes with the flow rate. The DN 40 flowmeters also have to cope with high pigment contents. BASF Coatings did not want to risk any further pressure loss otherwise they would have to increase the performance of the pump. BASF Coatings thus opted for the OPTIMASS, a mass flowmeter which is virtually made for this application thanks to its straight-tube design.

The grinding system is designed for a flow rate of approx. 5000kg/h. Communication with the PLC takes place via the OPTIMASS's 4…20mA signal output. Every 90 seconds the PLC saves a flow measurement and compares it with the subsequent values. If there is a difference of 360kg/h, the system is automatically shut down. At present, further tests are underway to halve the leakage value.

• Less pressure loss• Less abrasion• Suitable even for large flow volumes• Wide measuring range• No risk of blockage

WhyKROHNE?

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.22

Application Story

Tanker loading using 6 OPTIMASS meters T 40 EEx in conjunction with batch controller Batching Master 100i ” from IBS-Control

DHC Solvent ChemieGmbH in Mülheim an derRuhr is a subsidiary of Ruhr Oel GmbH, a joint venture of Deutsche BP and Petróleos de Venezuela S.A. It is one of Europe‘s leading manufacturers of solvents and other speciality products from crude oil.The distillation unit is used to fractionate refinery feedstock to produce special boiling point products, white spirits, solvent naphtha and rolling-oils.

Process data:Flow: 50 t/hDensity: 0.850 kg/l Temperature: 18 °C.Viscosity 1 mPas

Our thanks to Dieter Timmerman of KROHNE Meßtechnik LGE West-Mitte for this application

(If you need information or advice on batch controllers, please contact Product Management)

Solvent loading stations in Germany

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.23

STRAIGHT TALK

Application Story – Chemical Industry in Switzerland

This chemical company in the Basel region used to dose the component products of the mixture one after another using a weigh scale. With the purchase of 2 Optimass T25s, 2 T40s and 2 x T80s they have greatly improved their mixing process enabling simultaneous dosing to save time and improve accuracy.

Above: the installed Optimass T25s

Left: one of the Optimass T80s with heating jacket

Below: the mixing unit w. remote converters

The Optimass Straight tube meters solved the problem of dosing highly viscous material with minimal pressure loss.

The accurate process information received from the customer enabled exact sizing which in turn enabled KAG to guarantee an accuracy of less than 1%.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.24

STRAIGHT TALK

Application Story - Chemical Dosing in Switzerland

11 x OPTIMASS 7300 F in sizes S10, S15, T15, T25 and T40

This Chemical Industry customer in the Basel area is using 11 OPTIMASS 7300F PROFIBUS PA meters for dosing various fluids in a mixing vessel.Previously the end products were consecutively dosed in the mixer using load cells. Now it is possible to dose multiple ingredients through a ring main into the mixer simultaneously.

Each product component has its own mass flowmeter. The new process method saves time and eliminates unnecessary measuring errors.

OPTIMASS 7000 with a single straight tube meter is ideal for dosing fluids with high viscosities.

Thanks to the exact process data supplied by the customer, we were able to fine tune the sizing and guarantee accuracy.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.25

STRAIGHT TALK

Application Story - Liquefied gas measurement in UK

The liquefied gas is distilled into several fractions which are used as active ingredients in pharmaceutical products. It was essential that F2 Chemicals found a way to measure the flow of the liquid reliably to ensure the consistent, high quality of its products. The measurement technology F2 Chemicals previously used to measure the flow of liquefied perfluorobutane and acetone did not provide the reliability which was critical for F2’s process.

Specialist chemical manufacturer F2 Chemicals Ltd has installed KROHNE’s OPTIMASS 8000 Coriolis mass flowmeter to improve the reliability of liquefied gas flow measurement at its plant in Lancashire.

Perfluorobutane and acetone are contained in 100 litre industrial cylinders and are charged into the distillation column and refluxed through the OPTIMASS Coriolis mass flowmeter at flow rates of between 40 and 200 kg/hour and at pressures of between 2 and 7 bar. The temperature of the liquefied gas varies between -5°C and +15°C. A 20 mA signal is taken from the OPTIMASS and fed into a DCS. The reading is manually monitored and the distillation process adjusted according to temperature.

Measurement reliability improved significantly since the KROHNE OPTIMASS 8000 Coriolis mass flowmeter was installed.

F2 Chemicals installed KROHNE’s OPTIMASS 8000 Coriolis mass flowmeter because of its ability to measure liquefied gas reliably and accurately at low temperatures. Its twin “u”shaped measuring tubes provide excellent signal-to-noise ratio and measurement turndown. This was important considering the low pressures of the gas being measured.

Coriolis Mass Flow

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.26

Application Story: Liquid Sulphur measurement in Russia

Ammofos plant in Cherepovets

Ammofos AG at Cherepovets is one of the leading Russian manufactures of phosphate fertilisers, and part of the chemical conglomerate JSC Fosagro AG The focus of the company is the production of sulphuric acid. Raw materials used in production are sulphur and pyrite.

OPTIMASS 7050 T25 mass flowmeters are used to measure the flow of molten sulphur with a temperature up to 145°C.

Problem: The temperature has to be kept above 130°C to prevent the sulphur from hardening and crystallising, and other measurement systems encountered problems.

Solution: The Optimass meter with its efficient heating jacket prevents the product solidifying. The great advantage of the single straight tube meter is its low pressure drop. The other advantage is that, if the product does solidify the straight tube is easy to clean out and restart the process.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.27

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Optimass Mass Flowmeters in Loading Systems

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Mass flowmeters of the Optimass family from KROHNE through their unique performance specifications are extensively used in various industrial applications for operating measurements and batching. However, this is far from being the only application area of these mass flowmeters. Growing prices on many kinds of products lead many plants and companies to look for effective methods of online monitoring of fluid operating flows, as well as measuring the quantities of product delivered to the buyer in business dealings.

Zoom Our customer, a major chemical plant, found an effective solution for a difficult task of hydrostabilized pyrolysis condensate loading into fuel tank trucks by using a straight-tube mass flowmeter Optimass 7000 along with the dedicated software. Flowmeter functionality, enabling simultaneous measurements of the actual product flow both in mass and volumetric units, its total mass, as well as density and temperature with all the obtained data displayed on the operator's panel, ensures that the product is delivered accurately,

Zoom

which makes the mass flowmeter indispensable in loading applications.

Page 1 of 1News : Optimass Mass Flowmeters in Loading Systems

02/10/2006http://www.krohne.ru/russia_en/news/data/news-Optimass-Mass-Flowmeters-in-Load...PDF created with pdfFactory trial version www.software-partners.co.ukCopyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.28

STRAIGHT TALK

Application Story Akzo Nobel UK

World leading producer of paints and coatings, Akzo Nobel Decorative Coatings, has installed four KROHNE OPTIMASS Coriolis Mass flowmeters at its manufacturing plant in Darwen, Lancashire to help accurately control product consistency and minimise production costs.

Accurately measuring the amount of chemicals added to Akzo Nobel’s Crown range of solvent-based paint products is essential to minimising costs and maintaining consistent product quality. The chemicals are contained in stainless steel storage vessels located 70 meters away from the production facility and are pumped at low pressure through the OPTIMASS flowmeters into mixing vessels where the paint is manufactured in batches.Signals from the instruments are fed into the production control system which controls the flow of the chemicals from the storage vessels to ensure that the correct amount is added.Previously Akzo Nobel measured the amount of chemical added to batches of paint using a load cell-based weighing system. However this did not provide sufficient measurement accuracy for the range of batch sizes.The OPTIMASS 7000 Series, with its single straight measuring tube, features a patented AST design which offers outstanding accuracy and stability when used on low flow rate applications.By installing our OPTIMASS meters, Akzo Nobel has automated the process and significantly improved measurement accuracy.

The installed meters are 2 x OPTIMASS 7000 T25s measuring Calcium and Lithium, 1 x 7000 T15 measuring Cobalt1 x 3000 S01 measuring silane monomer.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.29

Application Note

Optimass

Linz Oberflachen Technik in Gablitz in Austria have installed 36 Optimass 3000 Series S04 in their OEM equipment for paint and coatings mixing and dosing systems over the past 18 months. Application: Mixing and Dosing Systems for paint and coatings for up to 6 components. Why KROHNE? Problem: Accuracy and reliability required for low flows. Solution: The Optimass 3000 Series delivers the accuracy and reliability for trouble free running in the end user’s installation.

Process Parameters Product: Paint Waterbase and polyacrilate dispersals Mass Flow: 0.2 – 1.5 l/min Temperature: 18 – 27°C Nominal Pressure: 15 – 60 bar

INDUSTRY: PAINT MIXING OEM COUNTRY: AUSTRIA METER: 36 X OPTIMASS 3000 S04

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.30

STRAIGHT TALK

Application Story – Petrochemicals Manufacture in France

With thanks to Samuel MONNIER of Krohne France for this application note.

Application:This major petrochemicals manufacturing site for polypropylene, polyethylene, styrene, polystyrene, butadiene, and aromatics introduced mass flow measurement to measure and record the input of highly viscous polybutadene styrene into the manufacturing process. This input was not previously measured.

Process:Temperature: 30 ° C, Pressure: 8 bar, Density: 0.9 kg / l Viscosity: 7900 mPa.sMaximum flow rate: 13 T / H

The OPTIMASS 7300 S80 was used with the converter installed in the control room directly connected to the digital process controller. With the MFC300 it is possible to have up to 300 meters between converter and sensor

Why did the customer choose KROHNE?:A low pressure drop due to the single straight tube construction; quality advice on the setting up and installation of the sensor; assistance at the scheduled commissioning of the meter; and the bonus of an extended warranty for 2 additional years offered for the installation of this first device at this site.(Remember – you can always offer your customer a 3-year guarantee in exchange for the process details with the extended warranty card which they receive with the meter or fill in on the KROHNE website.)

Benefits to the customerImproved process installation, and control of consumption of process materials.Less than 0.5 Bar pressure drop in spite of the additional equipment in the process line and the extreme viscosity of the process fluid.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.31

STRAIGHT TALK

Application Story - PTFE production in England

TFE gas pipeline

1000 kg/h

PTFE Slurry

Water removal process

Polymerising Vessel

Water and Initiator 22 Bar

Asahi Glass Fluoropolymers UK Ltd installed four KROHNE OPTIMASS 7000 T10 flowmeters to measure heavy gas flow at its polytetrafluoroethylene (PTFE) manufacturing plant in Lancashire. Each OPTIMASS replaced 2 previous measuring devices for pressure and temperature.Tetrafluoroethylene (TFE) is a dense, almost liquid, heavy gas used in the production of PTFE.

The TFE gas is produced in a separate area of the factory and pumped into the PTFE manufacturing plant through a common pipeline 24 hours per day. The common gas feed is then split into four lines to produce different grades of PTFE, each of which is fitted with an OPTIMASS flowmeter.

Process ParametersMedium : TetrafluoroethyleneFlow Range : 0 ... 20 kg/minDensity : 144.8 kg/m3Viscosity : 0.0135 cPTemperature : 4 °CPressure : 24 bar

The OPTIMASS T10 meters measure the TFE gas into a polymerising vessel with great accuracy. The gas is then combined with water and initiators in the reactor to produce the PTFE slurry which then has the water removed to leave the end product.

Advantage for the customer:With the installation of these meters AGF improved the accuracy of gas measurement and eliminated the need for two measurement devices.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.32

1STRAIGHT TALK

Application Story – Waste Management in Canada

StS Waste Management in Ontario Canada produce equipment for the solidification and stabilization of liquid waste streams.They have the only technology on the market to transform used liquid drilling fluids into disposable, dumpable solids in minutes, eliminating the need for expensive liquid disposal fees.

A PitDry™ reagent chemically fixates heavy metal bearing wastes, stabilizes hydrocarbons and other organic and inorganic material while minimizing total solids volume. The equipment to process this incorporates an OPTIMASS T50 for batching and totalizing low flows of slurry.

Two views of the StS equipment incorporating the OPTIMASS 7000 T50

The apparatus is easily transportable and enables environmentally sound treatment and disposal of spent drilling fluids

Our thanks to Angelo Del Buono for this Application Story

Coriolis Mass Flow

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.33

STRAIGHT TALK

Application Story: Waste Disposal in FranceThe business of this company is the destruction of industrial waste by incineration. They specialise in the decontamination of equipment contaminated with PCBs and the destruction of halogenated products (compounds containing fluorine, chlorine, bromine or iodine. Application :Regulating the flow of all types of substance to the head of the furnace, in accordance with the corrosive nature of the fluids, which can also be mushy, crystallising, and containing large particles, all in a very hostile environment.

Models Selected:

OPTIMASS 7050 and 7300 H15: for its low pressure drop with viscous liquids. The single straight tube with constant diameter enables large particles to pass without clogging and the Hastelloy tube handles the corrosion issues for a wide range of substances.

OPTIMASS 8050 H25 high temperature meter: The heating jacket keeps the meter at a high temperature to avoid crystallization of the substances in the meter tube.

Why the customer chose KROHNE:A complete range of meters to cover the needs of this type of industry, such as single straight tube, Hastelloy appliances for corrosion issues, high reliability and good technical support, both before and after sales for equipment choice and commissioning.

Benefit for the customer:Low maintenance due to corrosion resistant materials, no clogging in the meter and reliable measurement.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.34

Application Note

Optimas

Sand Separation

INDUSTRY: MINING COUNTRY: SWEDEN METER: OPTIMASS T40

Råda Sand AB is a producer and supplier of fine sand to various industries including concrete, filtration manufacturer etc. To be able to get the fine sand out of the water, they have to add the right amount of flocculent chemicals to settle the sand. The mass concentration controls the whole process in a ratio with the volume flow. We supplied the customer with an Optimass MFM7050 T 40. Application: Flocculent Dosing Why KROHNE? Problem The customer required accurate dosing of the flocculent (inorganic coagulant) due to the high price of the flocculent and to improve efficiency. Solution The only equipment suitable for the customer was the Optimass due to its single straight tube, which is less susceptible to abrasion.

The fluid is very abrasive due to its sand content (<10%) so the cones on the inlet and outlet sections have to be narrow. The Optimass is used to measure the concentration of the sand mixture to provide an input to the controller which governs the ratio of flocculent addition to the mixture. Process Parameters Media: Sand/Clay slurry (<10% Sand >90% Water) Pressure: 2 barg Temperature: 15°C (Ambient) Flow capacity: 15000 l/h Sand content: 800 kg/h

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.35

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Above: more views of the Optimass T40 in operation

Schematic Diagram of Operation

Sand/Clay Slurry

Flocculent

DR21

2289

Volumetric flow

Gen.con

Belt filter press

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.36

Application Story

Salt Mining in AustriaShortly before its 25th Anniversary, Saline Austria in Ebenseemodernised its installation in order to optimise production processes and minimise environmental impact.

The brine tanks accumulate a slurry of chalk and gypsum at the bottom which has to be drawn off periodically. This led to a lot of the brine also being lost. However with the use of Optimass meters to measure the density, the valves can be closed as soon as pure brine is measured. The slurry density is around 1.3 kg/l and drops to 1.15 with pure brine.

The Adaptive Sensor Technology of Optimass removes the problem of external influences affecting measurement by using its own internal mass as a self compensating mechanism therefore responding quickly to changes in density.

Additionally a KROHNE Optimass is helping to improve the environmental impact as the waste water slurry from the process is no longer discharged into the Traunsee Lake but pumped back from Ebensee via a 20 km pipeline where it is forced into the salt caves of Bad Ischl which in turn displaces new brine. This is then returned by a separate pipeline. Here also, the KROHNE meter is being used for density control.

Application: Salt production

Why KROHNE?Problem: Loss of brine when slurry drawn offSolution:Prompt shut-off with Optimass density measurement

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.37

Application Note

Optimass

Paper Coating Plant produced by OEM customer, BVG for Paper Mill in Germany

Application: Discontinuous Paper Coating Our customer BVG in Greifenberg is an important Original Equipment Manufacturer (OEM) for the paper industry operating world wide. The installation of this extremely compact discontinuous coating kitchen was made by BVG’s Dr. Bauer at a paper mill in Germany. BVG have also developed innovative continuous coating plants for other customers with on line coating and on line satinage using our Coriolis meters. Problem The problem for the end user lay in the recipe for the coating colour. There were always bonding problems between the background and the coating. This could have been caused because the required level of dosing accuracy was not achieved with the previously used positive displacement meters. Getting accurate and responsive measurements of the highly viscous and dense products batched such as clay, latex, carbonate and dispersants was difficult. Solution

INDUSTRY: PULP AND PAPER COUNTRY: GERMANY METERS: 19 OPTIMASS T10, T15, T25, T40

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.38

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Changing to KROHNE Coriolis meters. This installation contains a total of 19 Optimass meters:

- 4 X MFM 7050 T10 - 4 X MFM 7050 T15 - 5 X MFM 7050 T25 - 6 X MFM 7050 T40

The Optimass meters are working very well. Some of these are connected in series, but there is absolutely no problem with this for Optimass, unlike earlier incarnations of Coriolis meters.

Process Parameters Size Medium Flow rate Pressure Density Viscocity T40 Setacarb (Calcium

carbonate, chalk), 20,000 l/h 3 bar 1,7 kg/l 500 mPas

T40 Hydragloss (Kaolin) 20,000 l/h, 3 bar 1,85kg/l 500 mPas T40 Hydracarb (chalk) 20,000 l/h 3 bar 1,7 kg/l 500 mPas T 25 Latex 10,000 l/hr 3 bar 1.02 kg/l 0,150 mPas T40 Acronal

(waterproofing) 10,000 l/h 3 bar 1,02

kg/l, 370 mPas

T40 Emsol K115 10,000 l/h 3 bar 1.02 kg/l 1.000 mPas T40

Finnfix (Binder) 5,000 l/h 3 bar 1,02 kg/l 750 mPas

T25 Acrosol 5,000 l/h 3 bar 1.08 kg/l 2000 mPas T25 Acrosol 1,000 l/h 3 bar 1.09 kg/l 2000 mPas T25 Poliviol (bonding,

glue) 1,000 l/h 3 bar 1.06 k/l 900 mPas

T10 Blankophor (optical brightener

1,000 l/h 3 bar 1.2 kg/l 50 mPas

T10 NaOH 50% 1,000 l/h 3 bar 1.52 kg/l 0.0800 mPas T15 Elastofix

(Waterproofing) 2,000 l/h 3 bar 1.1 kg/l 45 mPas

T25 ESTR200 (defoamer)

1,000 l/h 3 bar 0.86 kg/l 600 mPas

T15 Polysalz (dispersant) 1.000 l/h 3 bar 1.26 kg/l 450 mPas T10 X 2

colour 500 l/h 3 bar 1.00 kg/l 0.020 mPas

T15 Carrier Fluid 2,000 l/h 3 bar 1.40 kg/l 0.100 mPas T15 Spülmittel

(flushing medium) 2,000 l/h 3 bar 1.00 kg/l 0.500 mPas

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.39

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Our thanks to Peter Jüstel of KMT Süd for this application story

KROHNE Service Engineer, Robert Klur, setting up the meters

The view from behind

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.40

Application Stories

Density Measurement of Carbonate Slurry in the Paper Industry

The measurement of the density of Carbonate slurry has evolved considerably in the last few years in the paper industry and in particular at this customer in Finland.Initially the density was measured using Radiometric density meters and, combined with an Electromagnetic flowmeter, the mass flow was calculated. Here Berthold density meters and KROHNE IFM5110F Magnetic Flowmeters were used.Later on this measurement method was discontinued due to the ‘percieved’ dangers of Radiometric measurement and Single Straight Tube Coriolis meters were used to replace this technology. The process involves and evaporation process where the slurry is continuously circulated till the correct density is achieved in the evaporator. The Carbonate slurry is then pumped to a storage tank. A KROHNE 300 G+ was used for this process. In the initial production and mixing of the slurry and 800G+ was used. Further enhancement of the process was made using the Multi I/O option in the mass meters. This provided the plant engineers with more data with respect to the process, apart from density, eg temperature, mass flow etc.Later orders of mass flowmeters from KROHNE had the Profibus PA option which gave the plant engineers more flexibility in the control and monitoring of the plant.

New Evaporator

When it was decided to install a new evaporator the natural progression was to use the new Optimassmeters from KROHNE.

This project was started in October 2002 and fully commissioned by May 2003. Here an OptimassMFM7051 T40 with Profibus PA was used.

KROHNE Magnetic flowmeter Model IFM 5090 WITH Profibus PA was used for water addition to the process.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.41

Application Note

Optimass

INDUSTRY: PHARMACEUTICAL COUNTRY: CZECH REPUBLIC METER: Optimass T10

Sterile Water dosing application in the Pharmaceutical Industry MAAP s.r.o. is an OEM customer in the Czech Republic, manufacturing plant mainly for the Pharmaceutical Industry. The equipment below was produced for an end user in Austria. This is a sterile water batching application using flowmeter pulse output and a Siemens batch control system. The sterile water is then mixed with different additives, before filtration etc. and various pharmaceutical nutrient solutions are produced.

Application: Sterile water dosing Why KROHNE?

• Excellent performance/price ratio • Accurate dosing • Meets hygienic requirements • Suitable for Steam cleaning

Process Parameters Product: Sterile Water Mass Flow: Batch sizes of 1 to 10 litres Temperature: Operating temp 20°C with steam cleaning up to 130°C Nominal Pressure: 0.7 mPa

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.42

STRAIGHT TALK

Application Story

Applications in Denmark

This Pharmaceutical company in Denmark manufactures various enzymes used in the production of washing powder etc. The application pictured is the dosing of Sorbitol, Glycol and MPG into a continuous mixing of products for enzyme production.

Process Conditions

Temp. Density Viscosity Pressure

20° 1.036-1.037 g/ml 62 mPas 2,5 barg

20° 1.300 g/ml 180 mPas 2,5 barg

20° 1.258 g/ml 1410 mPAs 3 barg

The Optimass concentration measurement is used to measure solids before polymer dosing in a waste water treatment plant. The concentration of solids is approximately 5-7% and the waste water is both organic and non organic waste in the two lines.

Temperature range is 12-19 °C and a pressure of app. 3 barg.

Enzyme Production

Waste Water Treatment

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.43

Application Story

With thanks to Radmila Kompova of our KROHNE Ostrava office in the Czech Republic

Sterile Water dosing application in the Pharmaceutical Industry

Optimass T10 meters are used for a sterile water batching application using flowmeter pulse output and a Siemens batch control system.The sterile water is then mixed with different additives, before filtration etc. and various pharmaceutical nutrient solutions are produced.

Batch sizes of 1 to 10 litres

Operating temp 20°C with steam cleaning up to 130°C

MAAP s.r.o. is an OEM customer in the Czech Republic, manufacturing plant mainly for the Pharmaceutical Industry. This equipment was produced for an end user in Austria.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.44

STRAIGHT TALK

Our Application Story on Optimass 9000 meters was published in the June edition of Instrumentation magazine – in the middle of an article by ABB on selecting flowmeters!

A Texas asphalt facility has 6 x 9000 S100sinstalled for tanker loading.These meters have been supplied with steam heating jackets as well.

The Forgotten Meters? …. continued

The 9000 Series meter is suitable for all process temperatures above 230°C to 350°C (392 to 572°F). This is a great meter where heating is also required. It is always supplied with an insulation jacket for safety reasons.

We have had quite a bit of success on bitumen and carbon black applications (see PR at bottom of page).

Please go out and sell a few of these meters. If you need help, please contact Product Management.If you are having price problems, let us know as well. We will try to help.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.45

STRAIGHT TALK

Application Story – Optimass 2000 at Shell Canada

With thanks to Angelo DelBuono of KAI Canada for this application note

Process details

Media : GasolineTemperature : 15.0 CPressure : 3000 kPaDensity : 884.0 kg/m³Viscosity : 0.7 mPa.sFlow type : Volume flowFlow : 300 m³/h

Shell’s Sarnia Manufacturing Centre (SMC) in Ontario is also referred to as Shell’s Corunna Refinery. It is located on the St Clair river next to the US border and processes 72,000 barrels of crude oil per day. Shell Canada refines only low sulphur gasoline, which contains less than 150 parts-per-million sulphur.

Shell Canada Ltd purchased an OPTIMASS 2300F S150Custody Transfer version for use at the Sarnia site and on the right and above are pictures of the completed installation. This is our 3rd installed 2000 series meter, following the 2 meters installed in Kazakhstan last month.

above: The Shell Sarnia site

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.46

1STRAIGHT TALK

Application Story – Carbon Black Production in Europe

Meter: Optimass MFS9000 S25

Medium: FCC oil, or Etilen tar oilFlow range: 0-8000 kg/hTemperature: 230 CPressure: 23 bargDensity: 1,05..1,1 g/cm3 Viscosity (SUS99C) : 120-330

A carbon black producer in Europe has installed 5 of our high temperature Optimass 9000 meters to control the flow of oil at the reactors. Carbon black is used to improve the strength, durability and overall performance of a range of products including tyres and other mechanical rubber goods, as well as inks, paints, plastics and coatings

Our thanks to Frank Grunert of KLtd for this application note

Prior to purchase, our meters were tested against competitor’s meters and gave better results.

This company could rely on our local agents for good technical support and the high temperature meters provided the right options and accuracy at the right price.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.47

STRAIGHT TALK

Application Story – Carbon Black Production in Europe

Meter: Optimass MFS9000 S25

Medium: FCC oil, or Etilen tar oilFlow range: 0-8000 kg/hTemperature: 230 CPressure: 23 bargDensity: 1,05..1,1 g/cm3 Viscosity (SUS99C) : 120-330

A carbon black producer in Europe has installed 5 of our high temperature Optimass 9000 meters to control the flow of oil at the reactors. Carbon black is used to improve the strength, durability and overall performance of a range of products including tyres and other mechanical rubber goods, as well as inks, paints, plastics and coatings

Prior to purchase, our meters were tested against competitor’s meters and gave better results.

This company could rely on our local agents for good technical support and the high temperature meters provided the right options and accuracy at the right price.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.48

1STRAIGHT TALK

Application Story – 1st Optimass 2000s installed in Kazakhstan

With thanks to Yuriy Tuzhilov of Kanex Krohne Kazakhstan for this application

KazMunayGas is the state-owned oil and gas company of Kazakhstan. It was founded in 2002 by merging Kazakhoil and Oil and Gas Transportation.

KazMunaiGas Exploration Production (KMG EP) is a KazMunayGas -majority-owned oil and gas company producing crude oil, natural and associated gas from its hydrocarbon reserves on-shore in Kazakhstan. It was formed in March 2004 through the merger of JSC UzenMunaiGas (UMG) and JSC EmbaMunaiGas(EMG) and was the 2nd largest Kazakh oil producing company in 2007.

KMG EP is developing 46 fields in Western Kazakhstan, the largest being the Uzen field - in production since 1965 and accounting for more than 75% of reserves and 71% of 2007 production. This is where the first two Optimass 2000s shipped out from KLtd have been installed for tank oil metering.

Process DetailsPressure: 10-39 BarTemperature: 35˚C-55˚CFlow rates: 360-480 ton/hourViscosity: 40-150 cSt, Petroleum type: tank oil (with high

content of paraffin 70 %)

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.49

Application Note

Optimass

One of the biggest Shell petrochemical production facilities in Europe is at SHELL Berre (close to Marseille), Application: Truck loading The customer needs to load the exact quantity of SAP oil into the tanker to avoid any overloading. The trucks are then weighed on a weighbridge to get a custody transfer measurement of the mass. If there is an overload, the truck must come back to an offloading station, losing valuable operating time. If the tanker is not totally filled, then transportation costs increase.

The previous installation was less than ideal, and 7 larger meters were replaced with Optimass T 40 and T 50 meters without any pipeline modifications. This was a requirement, as Shell was not able to stop the loading stations in order to do the work. The measurement results were immediately excellent without any special adjustment or field calibration of the meter. For a 26 ton fill, the measurement accuracy improved to ±0.2% with Optimass from the previous ±0.8 to 2.5%.

INDUSTRY: OIL AND GAS COUNTRY: FRANCE METER: OPTIMASS 7000 T 40 & T50

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.50

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Application: Loading Station Why KROHNE? KROHNE France provided the support and convinced the customer that they could save money with the increased accuracy of the installation of Optimass. Problem: Unsatisfactory performance of existing meters. Solution: Improved accuracy meant more savings.

Process Parameters Product: SAP Oil Mass Flow: 40 – 60 t/h Temperature: 100 °C Viscosity: 83 -220 cSt Pressure: 3.9 – 6 bar Density: 920 – 1000 k/m3

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.51

STRAIGHT TALK

Application: Kerax produces a variety of different waxes to be used in making castings and as ingredients in products such as adhesives. Each formulation requires the blending of two or three types of wax plus a number of additives. The mechanical meter previously positioned on the input to the blending vessel was not able to provide the accuracy needed for Kerax’s increasingly stringent process control.

Application Story – Wax Production in UK

Problem:The wax flowing through the meter can vary in density from 0.8 to 1.0 kg/litre and in viscosity from 5.5 cP to 1,200 cP. It can be flowing at rates varying from 1.8 to 15 tonnes / hour with pressures from 1.4 bar to more than 4.1 bar at temperatures ranging from 20 to 120°C.

Solution: OPTIMASS 7300-T 50The installed OPTIMASS 7300 Coriolis mass flowmeter is capable of handling the wide variation in process conditions whilst still delivering accuracy of +/- 0.1 per cent.

UK wax manufacturer Kerax Limited has installed an OPTIMASS 7300 mass flowmeter to improve the accuracy of production processes at its plant in Chorley, Lancashire.

To maintain a consistent product temperature, the OPTIMASS meter is fitted with a heating jacket that can be fed with hot water or steam.

Coriolis Mass Flow

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.52

1STRAIGHT TALKWith thanks to Klaus Loetsch of KMT Freiburg for this application note

The Siemens gasification centre in Freiberg, Germany, is one of the most comprehensive gasification test facilities in the world. Its gasification reactor is rated at five MWth and can be adjusted to different feedstock conditions. The facility also includes a range of feedstock preparation systems and related gas cleaning process units.

For the examination of fouling in heat exchangers, a test rig was designed to gain experience when preheating process water up to 220°C. Thermo oil is used as a heating medium in the heat exchanger.Both the monitoring of temperature and a reliable monitoring of the volume flow are decisive factors for the evaluation.An OPTIMASS 9000 from KROHNE was installed to control the thermo oil volume flow. The mass flowmeter records the volume flow of the thermo oil at 230 °C and 10 barg. The maximal permissible temperature of the thermo oil is 300°C.

A test rig for large-scale, high-pressure feeding tests and further equipment for coal and slag analysis (e.g. fluidization and viscosity) complement the facilities. With this equipment, a broad range of test conditions can be simulated.

Optimass 9000 S25

Medium: Heating oilFlow rate:2500 kg/h Temperature: 260°CPressure:1-11 bar

Application Story – Siemens Gasification Test Rig

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.53

Application Story

ISPAT Nova Hut a.s. is one of the largest metallurgic plants in the Czech Republic. It is an integrated steelmaking concern with a metallurgical production and large engineering shops. The metallurgical production is of a mass character, the main products being welded and hot-rolled seamless steel pipes, long products and wire rod, hot rolled sheets and strips. The engineering production (e.g. steel mining supports) is geared for batch production. Their coking plant is the largest coke producer in the Czech Republic.

ISPAT Nova Hut has been using several hundreds of KROHNE magnetic inductive flowmeters and flow controllers (mainly on water measurements) and additionally ultrasonic flowmeters (on demineralised water and tar), level radar (blast furnace stock level, hydrochloric acid level measurement) and mass flowmeters (fuel oil, top gas and steel sludge measurement). All instruments have been subjected to demanding operating conditions.

In the blast furnace, during the pig iron production process, a lot of top gas is generated. The gas (with temperature 200 – 500°C) contains from 30 to 100 g/m3 of dust. The gas is cleaned with sprinkling water, which then flows into settling basins. Here the mud settles and then it is pumped first to thickeners and after thickening to a separator. For the process control it is necessary to know the density of the mud pumped from basins to thickeners and from thickeners to the separator.

The customer had been using nucleonic density meters for 10 years. These meters require special approvals and checks and a lot of maintenance. Moreover they could not be in operation without product flow. For this reason the customer decided to test 2 KROHNE mass flowmeters Corimass MFM 4085 G+ - 1500 G. After 6 months´testing, 8 pieces of Optimass T50 mass flowmeters were ordered.

Top gas mud density measurement in Nova hut a.s.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.54

Application Story

Burner control in Sweden

Ovako Steel at Hofors

Why KrohneNo maintenance necessaryLow pressure dropHigh accuracyOptimised burner controlExcellent support from Fagerberg Sweden

Steel is the world's leading producer of steel for rolling bearings and, in addition, the company has a strong position within the field of low alloy special steels. Their annual production capacity is 525 000 tonnes of special engineering steel. Ovako Steel's metallurgical facilities are located at Hofors, Sweden.

Optimass T 15 HJ

Medium: OilPressure: 4 bar.Temp: 80ºCDensity: 886 kg/m3Range: 0 - 4500 kg/h

Our Optimass 7050 15 T with heating jacket shown in the picture below is being used for burner control. We also have 24 of our low flow 7100 meters (now renamed 3000) being used in other applications in Ovako.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.55

STRAIGHT TALK

Application Story – Fuel Consumption in Norway

The basis of the system is a 6.5’’ TFT colour screen displaying the consumption based on different criteria, like time or distance travelled. The screen has a touch function and is easy to operate. There is an alarm function to show when the consumption is too high. The log function is in the screen and is saved in an USB-stick, which can be down loaded to a PC to keep a history of consumed fuel.The system is very flexible and can be extended where required to log the consumption with regard to number of revolutions, pitch or speed,

4 Optimass 1300 C S25 meters were purchased for fuel monitoring on ferries in Norway with very good results. The first installation is now saving about 1000 litre diesel per day, which is about 120.000 Euro p.a. The second pair have now been commissioned on another ferry and we expect more orders to be forthcoming.

The logging system is delivered by Bentzen Elektro. It uses 2 of our very precise OPTIMASS 1300C flow meters that measure the difference between input and output. One meter is on the input side of the fuel line and one on the return pipe. The difference measures the fuel consumption.

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.56

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Application StoryCzech Republic Custody Transfer

Process ParametersApplication: CT transfer of bulk Butane / Propane productsFlow Rate: Nominal flow rate of a 25 T is 34,500 kg/h, emptying at 14,000 kg/h(pressure drop 0,3 bar, velocity 15,4 m/s)Pressure: 7 to 12 barDensity: 560 kg/m3Temperature: Ambient (-30 to +35°C)

Why KROHNE? KROHNE Czech Republic is known for their customer support and client was confident that the solution proposed would do the job.

A T25 Optimass Meter was installed for Propane/Butane emptying of rail tankers with a capacity of approximately 42000 kg at BP in the Czech Republic. Accuracies of 0.2 to 0.3% were repeatedly achieved which included the uncertainty of the weighbridge used for the railcars. Resolutions of these weighbridges are typically in the tens of kilograms! This meter is installed as a Custody Transfer meter according to Czech Republic guidelines and directives.

All weather emptying from railway tanks using Optimass

Another Optimass T25 for Custody Transfer was subsequently installed at BP in Dysina near the city of Pilsen filling tank-trucks with propane/butane. The measurement error is approx. 30 kg per 10000 kg of the gas, but it also comprises the error of the recomputation as the tank-trucksare filled according to mass but the distribution to end users isperformed according to volume and the recomputation to mass is doneacc. to special tables.

Process ParametersApplication:CT transfer of bulk Butane / Propane productsFlow Rate: 12000 kg/hPressure: 6-8 barTemp: Ambient (-30 to +35°C)

The installation in Dysina

Our thanks to Radmilla Kompova of KROHNE CZ for this application story

Copyright KROHNE, inc. , 2009 OPTIMASS Applications Page No.57

Coriolis Mass Flow

Propane-butane measurement for the BP CZ company, used for filling from railway tanks under the environment conditions (outside), the instrument is „custody transfer“ acc. to the CZ directives, during the first filling the tank contained 41100 kg with the pressure of 5 bar, our Optimass measured by 120 kg minus, the customer was satisfied.

Custody transfer measurement of propane - butane

Applications Applications -- CTCT

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Coriolis Mass Flow

Applications Applications –– Oil & GasOil & Gas

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Coriolis Mass Flow

Applications Applications –– Oil & GasOil & Gas

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Coriolis Mass Flow

SHELL Berre (Marseille/France)Process ParametersProduct: SAP OilMass Flow: 40 – 60 t/h Temperature: 100 °CViscosity: 83 -220 cSt Pressure: 3.9 – 6 barDensity: 920 – 1000 k/m3

The customer needs to load the exact quantity of SAP oil into the tanker to avoid any overloading. The trucks are then weighed on a weighbridge to get a custodytransfer measurement. If there is an overload, the truck must come backto an offloading station, losing valuable operating time. If the tanker is not totally filled, then transportation costs increase.

Applications Applications –– Dosing and BatchingDosing and Batching

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Coriolis Mass Flow

Applications Applications –– Dosing and BatchingDosing and BatchingBenzine Benzine loading stations with OPTIMASS, Solvent loading stations with OPTIMASS, Solvent ChemieChemie, Germany, GermanyProcess data:

Flow: 50 t/hDensity: 0.850 kg/l Temperature: 18 °C.Viskosityt 1 mPas

Tanker loading with 6 OPTIMASS meters T 40 EEx in connection with the batch controller “Batchingmaster” from ibs-control

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Coriolis Mass Flow

Installation 2: in a horizontal pipeline

Applications Applications –– Food & BeverageFood & Beverage

Jose Cuervo Tequila - Filling Station in Mexico

Fiscal measurement with 2 x OPTIMASS S40 Connection: Tri ClampPower supply: 120 V ACOutput: pulse output to batch controller

Note:The meters have been installed in such a way that they will always be full. This is good engineering practice for this type of application.

Process Conditions:Product: Tequila (alcohol)Temperature: 25 °CPressure: 4 kg/cm2Density: 0.95 kg/lFlow rate: 640 l/min

Installation 1: Suspended by two metal rods and two metal belts in a horizontal position from the top of the filling station.

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