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8/9/2019 SODIUM CARBOXY METHYL CELLULOSE HIGH VISCOSITY (CMC-HV).pdf
1/9
Enquiry No
ate
tion Criteria
. .
OIL
GAS DEVELOPMENT COMPANY LIMITED
PROCUREMENT Dl'.PAR1]VlENT, ISLAMABAD
FOREIGN SECTION A
(To be completed, filled in, signed
and stamped by the principal)
,
ANNEXURE' A'
SODIUM CARBOXY METHYL CELLULOSE- HIGH VISCOSITY (CMC-HV)
PROC-F
A/ C B/W S/CH
EM
-12 84 /20
I;;
FULL
SCHEDULE OF REOUIREME~T
/
Unit Quantity Unit Price
Total
Price
(FOB) (FOB)
Unit Price Total Price
C F BYSEA C F BYSEA
Deviated From
Tender Spec, If Any
Description
120
OOlCY CARBOXY :VIETHYL CELLCLOSE- HIGH VISCOSITY (CY C- Metric
HV) Ton
1. B id b on d: -P ursuant to tender c lause #
2.2,
II A,
13
35.3.2,
bid es ) must be accom panied by an upfront bid bond in the form of pay ord er /
de mand draft or ba nk guarante e issu ed b y sc he duled bank of Pakistan or a br anch o f fo re ign bank operat ing i n P ak istan. for an amount of US D
5.000/= (US dollars five thousa nd only) or equivalent Pak Rupee s, wi th technical bid and valid for 150 d ays fr om the date of open in g of the
bids. The bank guarantee m ust be iss ue d in a cc or da nce w ith the form at as per Annexure-C of the tender docum ents.
2 . Term s and conditi ons:-Bidder s ar e advice to carefully read all the te rms and conditions of the Tend er Document available at OODCL web
site in the maste r te nde r document.
3 . S um mary rejec ti on cri te ri a: - The sum m ary rej ect ion cr iter ia at c lause
35
of th e tend er docum ent may also be exam ine d ca refully.
4 . An y bid not m ee ti ng the cr i te r ia spelled in th e clause
#35
shall be sum marily r eje cte d w itho ut any right of a pp ea l.
5. D el iv ery peri od of th e qu ote d p ro du ct should not be mor e than 90 days afte r open ing of Lette r of C red it (L C) .
.. .
8/9/2019 SODIUM CARBOXY METHYL CELLULOSE HIGH VISCOSITY (CMC-HV).pdf
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INDENT # WS MUD -365/12/2014
DATED 22.08.2014
TECHNICAL SPECIFICA TIONS SHEET OF
CARBOXY METHYL CELLULOSE - HIGH VISCOSITY
CMC(HV) is the technical grade, high viscosity, sodium carboxyl methyl cellulose (Na-CMC) used in the drillingfluids
rangingfrom fresh water to salt water (Containing up to 50,000 PPM Salt). CMC-(HV) also aids in rheologicalcontrol,filtration
control, formationof the filter cake, lubrication o f bit, suspension of cuttings and weighting materials. It is stable up to 300
of
(149C).
Each bidder of CMC-HV should invariably fill-in the table given below with exact value of these properties of their
quoted product.Onlyto write conforming to or OK will not be sufficient.
A)
TECHNICAL SPECIFICA TlONS
EXACT VALUE
SR.
PHYSICAL REQUIRED
OF THE OFFERED
NO. PROPERTIES
SPECIFICA TlONS
PRODUCT
01.
Light colored hygroscopic
Appearance
free flowing powder
02.
Moisture content
ASTM D 1439
8% Maximum
03.
Degree of Substitution
ASTM D 1439
0.75 Minimum
04.
pH of 1% Solution in distilled
water (25C)
7 - 10
05. Sieve Limit (%)
Retention on 16 mesh ASTM
1 Maximum
(1.18mm)
06.
Bulk Density (g/l) 550 Minimum
PERFORMANCE TESTING
-
AS PER API SECTION 10
SR.
REQUIRED
EXACT VALUE
NO. PERFORMANCE TEST
SPECIFICA TlONS
OF THE OFFERED
PRODUCT
1.
Viscometer
Dial In de-ionized Water 30 Minimum.
Reading at 600 rpm
40 g/L Salt water 30
Minimum.
API Spec. 13 A - 10
-
In
Saturated
Salt 30 Minimum.
water
Fluid Loss
10 ern, Maximum
Note: Detailed procedure for performance testing are enclosed at Annexure- AI
8/9/2019 SODIUM CARBOXY METHYL CELLULOSE HIGH VISCOSITY (CMC-HV).pdf
3/9
INDENT #
WS M UD -365/12/2014
C} NECESSARYDATA
DATED 22.08.2014
SR.NO.
DESCRIPTION
01 .
Name of Bidder
.
~.
Complete address, telephone,
,
02.
Email and fax numbers of
bidder
03.
Name of local agent
Complete address, telephone,
04.
Email and fax numbers of local
agent.
-
05.
Name of Manufacturer
Name of Authorized Signatory
06.
of Manufacturer
Complete address, telephone,
07.
e-mail and fax number of
manufacturer.
08.
Website of manufacturer
09. Brand Name of Product
10.
Country of origin
11.
Port of shipment
12.
Minimum shelf life of product
l.C-l[VT
c.
CMC-HVT
shall be
deemed to meet this
spccificu
tion
if
a composite sample representing no
r.icrc
thar
one day's production conforms to the phys ica1r equ ire
ments of Table 10.1, represents the producturoduced
and is controlled 'by the manufacturer.
TAJlLB 10.1
CMC-HVT PIIYSIC1-\L REQUrIlE1VillSTS
Requirem.ent
Sp
ecifi ca+io n
--------------.--.-.---
Solution Properties
Viscometer DiRI Reading at. 600
rprn
in Deionized Water 3n, minimum
in 40 glL Salt'Water
in Satur-ated Salt Water
Filtrate Volume
3 minimum '
10 crrr', maximum
._------
------
SOLUTION PROPERTIES'
10.2.
EquipInE'ut.
a. Thermometer: 32-220 l'F (0-10r: :to.5'C)
b. Balance:
precision of
ll.Olg
c. Mixer (e.g., Multimixer Model 9B
with 9n2~X
im-
.- pellers
or
equiva
lent
as shown in
rig.
2.1): Each spindle
will be fitted with a
single
sine-wave impeller approxi-
mat.ely one inch (25rnln) in diameter mounted flash side
up.
d. Mixer. Container: npproxirnate
dirncnsrions -
7 inches
(HIO
mm) deep, 313/16 inch
(97
mm) ll) top.
2-3/4inch (70
rom
ID bottom (e.g., Hamilton
BC :lc h
mixer cup No. Iv1l10-D,
0
equivalent)
e. Spatula
f. Container: glass or
plastic
with stopper or lid for
salt solutions
g. Motor-Driven
Direct Indicating Viscometer:
as
referenced in A.PI.RP 1313-1, 1st edition, June, 1990,
Par. 2.4
h. Deionized
(or
distilled) water
I. S eale . cnn t.air er:
about 5PO-clll'
j. Sodinm ch lorir.e: (CAS W/f;'7-1A
1< . 1000-crn'
01 metric:
flask
r ,
Defnamer
10
'I'irnars: two intervc l,
m.ichn ni
p-ecis[nn to 0.1 minute
11.
Filter press: ;-. referuncerl in A
edition,
JUDe,
199(;, Par. 3.:~
D,
Graduated
cylinders
(TDl:
Due
IUD 1 ern, and
OIl~ 500
5
Cl;;3
pH
meter:
pre iis ion of 0.1 pH il
q.
API Standard Svalual.ioll 112.5e C
r , Soclium
bicarb nate:
(CAS 1F14'b
lfUJ Procedure _.-
Deionized
'W~
a. Prepare a solulion ofCMC-HV'1'
(6.29 0.03 g L nfCMC-HVT to :J50 :'
water at a uniform rate over a tirne
iu
seconds while
stirring
on the
T1Lxer.
; ' ,TOTE: CMCHVT slial] be ac ded.
shalt to minimi.ze dlsting.
1,_ .1\1\;e1'stining ,5 :,::0.1 minutes,
from the mixer a.nd scr ape its sides
w
remove
or
dislodge
any CMC-HVT
container ,.'1115. Be sure
a n
C:'vlC-H
spatula is
iucorpora
ted
into t:h~ solut
r Replace the container on the rnix
stir. The container .riay
nr-ccl
t.o he
mixer and the sides scraped to
dislorlg
afler another 5 and; 0 minutes. Total
equal 20 :1:1 minutes.
d. Age the solution for up to 15 lie
covered container at room teruper atu
t:emperature
and
storage duratiou.
e. After
aging, sti r
the
solution 0
:to.l
minutes. .
L Pour the solution into the viscor
with the direct indicating
viscometer
a
t
the GOO
;:-jlln
rotor
speed setting
5 1 1 1 1 be recorded when a constant v
reached. The 600 r pm dial reading
solution
test
temperature of 77 2 F
lOJt Procedure -
40 gfL ::~ :J .lt 'YV
. a. Prepare a40 gll, salt
so~'j
tion
b
of dium ch.loridc t;: a
lOOO- :;'n>
vo
dilutmgwitli deionized water \
0
the
the flask. Mix .thorOl.:ghly.
8/9/2019 SODIUM CARBOXY METHYL CELLULOSE HIGH VISCOSITY (CMC-HV).pdf
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.:~~. ., :
Prepare a solution
o r
ClvIC-RVT. Add ;2.70 O.OJ
g o
0.03 g/L) of ClvIC-IIVT to as o :1;6 'cm
3
of the g e
the solution for up to 16 hours in a sealed r r
'\{.Jtedcontainer at room,tempp;rature, Record storage
:'/iperature aud storage duratiou.
,I
;t'Aft.e.r aging, stir the solution on the mixer for 5
minutes,
.Pour the solution into the
viscometer
cup provided
.the direct indicating viscometer. The dial r ea ding
e 600 rpm rotor speed setting of the viscometer
he recorded when a constant value at 600 rpiu is
ed. The 600 rpm dial reading shall be taken fit n
tion test temperature of
77 2'F (26
I'Cl.
I
5 Procedure - Sat:urai;ed Salt 'Vater Test
Prepare an ample vO ;lD1C of a saturated salt solu-
by
thoroughly rnixirig in a suitable corrtedn er t.o
4';
sodium chloride per 100
1 cm
3
of deionized
wa
t
er.
r solution to stand for approximately 1 hour.
t solution or filter it
into a stcragu
container.
,,,,-pare a solution of ClvIC-HVT,* Add :;: ,500.01
hs
0.03 gILl CMC-HVTl' to 350 5 cm
3
of saturn teci
, ater
at a uniform -rate over a time interval of
,~ 60 seconds while stirring on the rnixer ,
'~A.tter stirring 5 0.1 minutes, remove container
: 1 ft mixer and scrape its side~ with the spatul~l tc
:\odge any CMC~HVT adhering to the container
ls. Be sure any Clv.rC-H\'T clinging to the spatula is
orated into the solution.
Replace the container on mixer and continue to
The container may need to he removed from the
r and the sides scraped to dislodge any CII/,(C-HV']'
another 5 and 10 minutes, Total mixing time shall
120 1 minutes,
, Age the solution for up to 16 hours in a sealed OJ'
red container' at room temperat\lTe, Record storage
: erature and storage: duration.
..After aging, stir the' solution on thu mixer for 5
minutes.
-Irnmadiately pour the solution into the viscometer
,provided with the direct indicating viscometer. The
reading at the 600 rp~ rotor speed setting of the
,
::-:=-==-::-=~==.-=-::::::==.
.~.~=:~.-~-
viscornet .r shall he rccordnd when a constant value :
(00 rj1U1 S ruach cd. The (,00
11Tll
Iiul rea cling shall
talII3r t AL a solut
ion test tenu-errturo
of 77 :t2 F (
-:T'C)
I O,i~ Pr-. c c cl u r o - F i . l t r nt e Volurnc
a. Pr
c]
a
rs
flnample volume of
saturated salt so)
Lion by U oruughly mixing in n suit ab le eon tainer -1,0
,H i g sodum chloride per 100 l. CD,3 of d8icm,i7,ecl.wat.
:~Jlow Sf) ution t,l stand for approximately I
hot
Decant SI tution (11 filter
it into a s
toruge container.
h. Prer vr e a cl.ay-base suspension
by
adding 350 :
,,,1\3
of tlu saturat.ed salt solution tJ a mixer contain:
:\dcl 1.0 : 0,1 g of sodium bicarbor ate and stir on t
mixer for about one minute.
c.
Slow
y add
3:5.0 O.l g of API Etandarcl'Evaluat:i,
nasc CIa while stirring on the m.xer.
d. Afbe stirring 5 O.l mi.uute~ remove contain
.rorn mix
'1'
and scrape its sides with the spatula
Iislcdgc ( uy clay adhering to container walls. Be s u
:,11day c:l
ngi.llg- to
the spatula is ir corporat.ed into tl
suspenaic
e. .Repl: cc the container on the mixer and continue
sLir.
The ontainer rna
V
need
to
b: removed from tl
r.iixer
au
L the sides scra.pec\
to
dislodge
any
c lr
cling'iug t. the con tain er
walls
after
ancthvr
Ii.nud
J
min
nt.en. '
'ot.nl stirring t.ilne
a ft.er H:lding
Lh~1.:1 :1:1
:; 11l1
l:qllf\ 1 20 : t
rrrirrures .
r.
Add ~ 15
Q,OI
g
(9,01
O,03 g'Ll
of Cr.. rC -HVT
1
1
ne
SUSpCl
sion while
stini.ug all
the' mixer, udding at
i
.uiforru 1:
t~
over about
60
second
g. After sti rring 5 0.1 minutes, remove the contaiuc
from
the
n
.ixer and scrape its sides with th. spatula 1
cislodge
:1: ,)'
CMC-HVT adhering to container walls, B
sure
all
m:
.terial
clinging
to
the spatula
is incorporate
i
ito
the
si spensiou,
h. Rcplr ce the container on the
mixer
and continu
t ; -
stir. Th: container rnav need to be reruovcd from th
, ,'nixer and ~,hcsides scraped to
clislo-Ige
any CMC-FDi'
cii.nr,inf
tc
the
container 'walls after another 5 and 1
ltin;ll:c~~.
r ot.al sti~g time shall e~ual20 1.minute:
i.
Age tl e suspension for 2 hours 5 minutes in
sealed 0) covered con ta iner at room tcmpere ture
Record sto 'age tenipern ture.
, i After r ging, she the suspension on the mixer for,
il.l
minu-
es ,
lc. Imme Hately pour the CJ\l1:C-I'IVT-trcated suspen
sion into a filter press ce1l.-Before adding the suspen
sion, be, su e each part of the filter cell is dry and tha
all gaskets lienot distorted or worn. The tcmperatur
of the sus iensiori shall be 77
2T
(25 1 C), Pou:
tl ie suspen .ion to within about
1/2
inch (13 mrn) of tlu
top of the :e11. Complete assembly of the filter pres:
cell. Place the filter cell in' the frame and close thi
rnlief valvr 'I
J
lace a container under the drain tube,
8/9/2019 SODIUM CARBOXY METHYL CELLULOSE HIGH VISCOSITY (CMC-HV).pdf
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;:
~
:
~~
,
r
j
~,~~~~
: ~ I ~ t ~
: . : . p
:{~ fl
;i~~
~ ~ . I
I :. ~
J ~ j , '
{ t _
. l
nr;c ~
,I
I
,
Am.ric[nPat.rleu.D1 Institute
..-=~
====::::~== '
=====
,
------~
I:
1. Set one timer for 7.5 :to.l minutes and the second
timer for 30 O'.lminutes.Start both timers and adjust
pressure on th~ 'cell to 100
:1:5
psi
(690 35 leFft).
Both
of these steps shall be completed in less than 15
seconds. Pressure sha.Ilbe supplied by compress llair,
nitrogen or helium. .
rn, At 7.5 :to.1miuutes on the first timer, remo-.'e the
contai.ner and any
uillleriug
liquid
on
the drain tube
and
discar-d.
Place
a
dry 10 cm
3
graduated
cylinder
under the 'drain tube and continue collecting.filtTate1:0'
the end of the second' timer set at 30 minutes. Rf'lDOVe
the graclllat't d' cylinder and record thl~ volume
If
filtrate collected.
{
10.7 Calcti.lation - i~iltn.\tl'.Vohuue
Calculate the
filtr
at.e volume
If
the
ClvIC.
suspension as:
Filb'ate
vol., em ~ =: : x V,'
'~where: V,
volume
filt.rat.E
collected
and
30
minutes
Record ca