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Document ID: 227965

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Page 1

TETRA TECH INC.

Project # 520512.505

Bennett's Dump 4811-06

TETRA TECH INC.

Project # 520512.505

Bennett's Dump 4811-06

PCB's

June 8, 1992

Submitted By

PACE INCORPORATED9608 LOIRET BLVD.

LENEXA, KS. 66219-2406(913) 599-5665

FAX (913) 599-1750

GC SEMI-VOLATILES

DEFINITIONS

"' NARRATIVE

A case narrative includes an explanation of any problems encountered, both technicaland administrative, and the corrective action(s) taken.

RAW DATA

This section includes all Data entry forms, Chromatograms and Quantitation reports foreach sample.

PRIMARY

The primary analysis is the initial calibration and continuing calibration standardsdemonstrated under a set of predetermined Gas Chromatograph conditions.

CONFIRM

The confirm analysis is the initial calibration and continuing calibration standardsdemonstrated under a set of predetermined Gas Chromatograph conditions differentfrom the primary analysis for the verification of the tentative compounds.

I

BLANK

A blank sample is a volume of a clean reference matrix that is carried through the entireanalytical procedure to demonstrate that the analytical system is free fromcontamination by the compounds of interest. The blank is used to correct for possiblecontamination resulting from the preparation or processing of the sample.

* MS/MSD

Matrix Spike and Matrix Spike Duplicate: A prescribed mixture of compounds is spikedinto two aliquots of a sample, and analyzed by the appropriate method. The resultsobtained are used to evaluate the effects of the sample matrix.

LCS

Laboratory Control Sample: A mixture of target analytes at known concentrations isspiked into a clean reference matrix and analyzed by the appropriate method todemonstrate the analytical system is in control.twenty samples.

I N C O R P O R A T E D REPORT OF LABORATORY ANALYSISI H f A S S U R A N C E O F Q U A L I T Y

TETRA TECH

Project I 520512.505Client Reference - Bennett's Dump 4811-06

PROJECT NARRATIVE

Samples were analyzed by method 8080 for PCB evaluation. Sample 60 006289.7(HB2-1.5) and 60 006297.8 (HB4-0.5) contained Aroclor 1248 contamination. Theremaining samples did not contain PCB patterns for any of the Aroclors inquestion.

There were no complications in the extraction and analysis for this project.

Charles E. GirginGC Semivolatiles SupervisorJune 8, 1992

EET14-139/kez

9608 Loire! BoulevardLenexa, KS 66219TEL: 913-599-5665FAX: 9 1 3 5 9 9 1 7 5 9

Offices Serving: Minneapolis, MinnesotaTampa, FloridaIowa City, IowaSan Francisco, CaliforniaKansas City, MissouriLui Angeles, California

Charlotte, North CarolinaAsheville, North CarolinaNew York, New YorkPittsburgh, PennsylvaniaDenver, Colorado

An Equal Opportunity Employer

I REPORT OF LABORATORY ANALYSIS1 n I 1 S S U ' » » C I 01 0 u • I i I »

June 08, 1992

Ms. Michelle BeckmanTetra Tech Inc.10 East Cambridge CircleKansas City, KS 66103

RE: PACE Project No. 520512.505Client Reference: Bennett's Dump 4811-06

Dear Ms. Beckman:

Enclosed is the report of laboratory analyses for samples receivedMay 12, 1992.

If you have any questions concerning this report, please feel freeto contact us.

Sincerely,

Duane R. Boline, Ph.D.Director, Sampling and Analytical Services

Enclosures

9608 Lou el Boulevard

leneia, KS 66219

TEL: 913-5995665

FAX: 913 599-1759

Offices Serving: Minneapolis, Minnesota

Tampa, Florida

Iowa City, IowaSan Francisco. California

Kansas City, Missouri

Los Angeles, California

Charlotte, North Carolina

Asheville, North Carolina

New York, New York

Pittsburgh. PennsylvaniaDenver, Colorado


I REPORT OF LABORATORY ANALYSIS1 M I 1 S S U » « <r C I 01 0 U « I I 1 I

Tetra Tech Inc.10 East Cambridge Circle

Kansas City, KS 66103

Attn: Ms. Michelle Beckman

Client Reference: Bennett's Dump 4811-06

PACE Sample Number:Date Collected:Date Received:Client Sample ID:Parameter

ORGANIC ANALYSIS

PCBS IN SOLIDS/LIQUIDS/SOLVENTSAroclor 1016Aroclor 1221"v-oclor 1232

>*roclor 1242Aroclor 1248Aroclor 1254

Aroclor 1260Dibutylchlorendate (Surrogate)

June 08, 1992PACE Project Number: 520512505

Units

mg/kgmg/kgmg/kgmg/kgmg/kgmg/kg

mg/kg

60 006287005/11/9205/12/92HB1 - 2.5

MDL DATE ANALYZED

1.0

NDNDNDNDNDND

ND66

05/23/9205/23/9205/23/9205/23/9205/23/9205/23/92

05/23/9205/23/92

,DL Method Detection LimitND Not detected at or above the MDL.

9608 Loire! BoulevardLene.a. KS 66219TEL: 913 599-5665FAX: 913599-1759

Offices Serving: Minneapolis, MinnesotaTampa. FloridaIowa City, IowaSan Francisco, CaliforniaKansas City, MissouriLos Angeles, California

Charlotte, North CarolinaAsheville, North CarolinaNew York. New YorkPittsburgh, PennsylvaniaDenver, Colorado


IN C O " P O R » T ( D REPORT OF LABORATORY ANALYSISln| I S S U D I U C I 01 O u • I I I >

Ms. Michelle2

Beckman

-Client Reference: Bennett's Dump 4811-06

PACE Sample Number:Date Collected:Date Received:Client Sample ID:Parameter Units

ORGANIC ANALYSIS

PCBS IN SOLIDS/LIQUIDS/SOLVENTSAroclor 1016 mg/kgAroclor 1221 mg/kgAroclor 1232 mg/kgAroclor 1242 mg/kgAroclor 1248 mg/kg

oclor 1254 mg/kg

mg/kg

MDL


60 006289705/11/9205/12/92HB2 - 1.5

DATE ANALYZED


1.0

NDNDNDND1.2ND

ND69

05/23/9205/23/9205/23/9205/23/9205/23/9205/23/92

05/23/9205/23/92

MDL!D

Method Detection LimitNot detected at or above the MDL.

9608 loirei BoulevardLeneia. KS 66219TEL: 913-599 5665FAX: 913 599-1759

Offices Serving: Minneapolis, MinnesotaTampa, FloridaIowa City, IowaSan Francisco, CaliforniaKansas City, MissouriLos Angeles, California

Charlotte. North CarolinaAsheville, North CarolinaNew York, New YorkPittsburgh, PennsylvaniaDenver. Colorado


II N C D R P O R * T t 0 REPORT OF LABORATORY ANALYSIS1 HI * S S U » ' * CI 0> OU « M 1 I

Ms. Michelle Beckrnan'age 3t



ORGANIC ANALYSIS

PCBS IN SOLIDS/LIQUIDS/SOLVENTSAroclor 1016 mg/kgAroclor 1221 mg/kgAroclor 1232 mg/kgAroclor 1242 mg/kgAroclor 1248 mg/kg""odor 1254 mg/kg

mg/kg

MDL


1.0


60 006291905/11/9205/12/92HB3 - 0.5

DATE ANALYZED

NDNDNDNDNDND

ND67

05/23/9205/23/9205/23/9205/23/9205/23/9205/23/92

05/23/9205/23/92

MDL Method Detection LimitVD Not detected at or above the MDL.

9608 Loire) Boulevardlene.a, KS 66219TEL: 913-599-5665FAX: 913599-1759


Charlotte, North CarolinaAsheville, North CarolinaNew York, New YorkPittsburgh, PennsylvaniaDenver, Colorado


I T E D REPORT OF LABORATORY ANALYSIS1 HI » S $ U " l >.CI 01 OUM I

Michelle Beckman4



ORGANIC ANALYSIS

PCBS IN SOLIDS/LIQUIDS/SOLVENTSAroclor 1016 mg/kgAroclor 1221 mg/kgAroclor 1232 mg/kgAroclor 1242 mg/kgAroclor 1248 mg/kg•oclor 1254 mg/kg

mg/kg%

MDL

1.01.01.01.0


60 006292705/11/9205/12/92HB2 - 2

DATE ANALYZED


1.0

NDNDNDNDNDND

ND100

06/05/9206/05/9206/05/9206/05/9206/05/9206/05/92

06/05/9206/05/92

MDL Method Detection LimitD Not detected at or above the MDL.

9608 Loire! BoulevardLenexa, KS 66219TEL: 9 1 3 5 9 9 5 6 6 5FAX: 913599 1759

Offices Serving: Minneapolis, MinnesotaTampa. FloridaIowa City, IowaSan Francisco, CaliforniaKansas City, MissouriLos Angeles, California

Charlotte. North CarolinaAsheville. North CarolinaNew York, New YorkPittsburgh, PennsylvaniaDenver, Colorado


I N C O R P O R t T I O REPORT OF LABORATORY ANALYSISi H( t ssumi in 01 ou iuM

Ms. Michelle Beckrnan'age 5\



ORGANIC ANALYSIS

MDL


60 006294305/11/9205/12/92HB2 - 2.5

DATE ANALYZED

PCBS IN SOLIDS/LIQUIDS/SOLVENTSAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248"roclor 1254



mg/kg 1.0

NDNDNDNDNDND

ND93

06/05/9206/05/9206/05/9206/05/9206/05/9206/05/92

06/05/9206/05/92

MDLIDf

Method Detection LimitNot detected at or above the MDL.

9608 Loire! Boulevard

lenexa, KS 66219

TEL: 913-599-5665

FAX: 913599-1759

Offices Serving: Minneapolis, MinnesotaTimpa, Florida

Iowa City, IowaSan Francisco, Californii

Kansis City, Missouri

Los Angeles, California

Charlotte, North Carolina

AshevSle, North Carolina

New York. New YorkPittsburgh, Pennsylvania

Denver, Colorado


II N C O R P O H A T I D REPORT OF LABORATORY ANALYSISi HI jssuni. :i oi OUM 11 T

Ms. Michelle Beckman?age 6



ORGANIC ANALYSIS

MDL


60 006295105/11/9205/12/92HB5 - 0.5

DATE ANALYZED

PCBS IN SOLIDS/LIQUIDS/SOLVENTSAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248'"•odor 1254

Aroclor 1260Di butylchlorendate (Surrogate)


mg/kg

1.01.01.01.0

1.0

NDNONDNDNDND

ND64

05/23/9205/23/9205/23/9205/23/9205/23/9205/23/92

05/23/9205/23/92

MDL

fMethod Detection LimitNot detected at or above the MDL.

9608 Loire! BoulevardLene.a. KS 66219TEL: 913699-5665FAX: 913 599-1759


Charlotte, North CarolinaAshevSle, North CarolinaNew York, New YorkPittsburgh, PennsylvaniaDenver, Colorado


I N C O R P O R A T E D REPORT OF LABORATORY ANALYSIS1 Ml « i SU>•» t I 01 Oil • I I I »

Ms. Michelle Beckirian7


PACE Sample Number:Date Collected:Date Received:Client Sample ID:Parameter Units MDL

ORGANIC ANALYSIS

PCBS IN SOLIDS/LIQUIDS/SOLVENTSAroclor 1016 mg/kg 1.0Aroclor 1221 mg/kg 1.0Aroclor 1232 mg/kg 1.0Aroclor 1242 mg/kg 1.0Aroclor 1248 mg/kg 1.0Voclor 1254 mg/kg 1.0wAroclor 1260 mg/kg 1.0Di butyl chlorendate (Surrogate) %


60 006297805/11/9205/12/92HB4 - 0.5

DATE ANALYZED

NDNDNDND1.9ND

ND73

05/23/9205/23/9205/23/9205/23/9205/23/9205/23/92

05/23/9205/23/92

MDL

•fMethod Detection LimitNot detected at or above the MDL.

9608 Loiret BoulevardUneia. KS 66219TEL: 913-599 5665FAX: 913599 -1759


Charlotte, North CarolinaAsheville. North CarolinaNew York, New YoikPittsburgh, PennsylvaniaDenver, Colorado


REPORT OF LABORATORY ANALYSISOf OUi I M 1

Ms. Michelle Beck.rnan'age 8

"Client Reference: Bennett's Dump 4811-06


ORGANIC ANALYSIS

PCBS IN SOLIDS/LIQUIDS/SOLVENTSAroclor 1016 mg/kgAroclor 1221 mg/kgAroclor 1232 mg/kgAroclor 1242 mg/kgAroclor 1248 mg/kg"•odor 1254 mg/kg

mg/kg%

MDL


60 006298605/11/9205/12/92HB4 - 1.0

DATE ANALYZED

1.0

Aroclor 1260Di butyl chlorendate (Surrogate)

1.0

1.0

NDNONDNDNDND

ND100

06/05/9206/05/9206/05/9206/05/9206/05/9206/05/92

06/05/9206/05/92

MDL Method Detection LimitND Not detected at or above the MDL.

9608 Loire! BoulevardLeneia. KS 66219TEL: 9 1 3 5 9 9 5 6 6 5FAX: 913-599-1759

Offices Serving: Minneapolis, MinnesotaTampa, FloridaIowa Cily, IowaSin Francisco. CaliforniaKansas Cily, MissouriLos Angeles, California

Charlotte, North CarolinaAsheville. North CarolinaNew York, New YorkPittsburgh, PennsylvaniaDenver. Colorado


REPORT OF LABORATORY ANALYSIS1 H I t S S U K H C I 01 OU • I M T

Ms. Michelle Beckman°age 9

.Client Reference: Bennett's Dump 4811-06

PACE Sample Number:Date Collected:Date Received:Client Sample ID:Parameter Units MDL

ORGANIC ANALYSIS

PCBS IN SOLIDS/LIQUIDS/SOLVENTSAroclor 1016 mg/kg 1.0Aroclor 1221 mg/kg 1.0Aroclor 1232 mg/kg 1.0Aroclor 1242 mg/kg 1.0Aroclor 1248 mg/kg 1.0Aroclor 1254 mg/kg 1.0

*?Troclor 1260 mg/kg 1.0Dibutylchlorendate (Surrogate) %


60 006299405/11/9205/12/92HB6 - 0.5

DATE ANALYZED

NDNDNDNONDND

ND70

05/24/9205/24/9205/24/9205/24/9205/24/9205/24/92

05/24/9205/24/92

MDL Method Detection LimitND Not detected at or above the MDL.

lese data have been reviewed and are approved for release.

Neal R. HudsonManager, Organic Chemistry

9608 Loitel Boulevardleneia. KS 66219TEL: 913-599-5665FAX: 913-599-1759

Offices Serving: Minneapolis. MinnesotaTampa, FloridaIowa City, IowaSan Francisco, CaliforniaKansas City. MissouriLos Angeles, California

Charlotte, North CarolinaAsheville, North CarolinaNew York, New YorkPittsburgh, PennsylvaniaDenver. Colorado


I « C O H P O A A 7 ( D REPORT OF LABORATORY ANALYSISt«i »',su«">U 01 o u t u i r

Ms. Michelle Beckruan"'age 10

QUALITY CONTROL DATA June 08, 1992PACE Project Number: 520512505

-Client Reference: Bennett's Dump 4811-06

PCBS IN SOLIDS/LIQUIDS/SOLVENTSBatch: 60 13724

Samples: 60 0062870, 60 0062897, 60 0062919, 60 0062951, 60 006297860 0062994

METHOD BLANK:

ParameterAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248"roclor 1254


Unitsmg/kgmg/kgmg/kgmg/kgmg/kgmg/kg

mg/kg%

MDL1.01.01.01.01.01.0

1.0

MethodBlankNDNDNDNDNDND

ND69

SPIKE AND SPIKE DUPLICATE:

arameter""Aroclor 1242

Units MDL 60 0051089 Spikemg/kg 1.0 ND 4.0

SpikeSpike DuplRecv Recv RPD103% 88% 15%

LABORATORY CONTROL SAMPLE:

ParameterAroclor 1254

Unitsmg/kg

MDL1.0

ReferenceValue25

Recv100%

MDL Method Detection LimitRPD Relative Percent Difference

9608 loiret BoulevardUneia, KS 66219TEL: 913-599 5665FAX: 9135991759

Offices Serving: Minneapolis, MinnesotaTampa, FloridaIowa City. IowaSan Francisco, CaliforniaKansas City, MissouriUs Angeles. California

Charlotte. North CarolinaAsheville, North CarolinaNew York, New YorkPittsburgh, PennsylvaniaDenver, Colorado


II N C O f t H ' O N A T f D REPORT OF LABORATORY ANALYSISIHI « S S u > » ICl 01 O u » l II I

Ms. Michelle Beckman'age 11

QUALITY CONTROL DATA


PCBS IN SOLIDS/LIQUIDS/SOLVENTSBatch: 60 13960

Samples: 60 0062927, 60 0061943, 60 0062986


METHOD BLANK:

ParameterAroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254

1260Dibutylchlorendate (Surrogate)

Unitsmg/kgmg/kgmg/kgmg/kgmg/kgmg/kg

mg/kg%

MDL1.01.01.01.01.01.0

1.0

MethodBlankNDNONDNDNDND

ND100

SPIKE AND SPIKE DUPLICATE:

'arameterAroclor 1242

Units MDL 60 0073570 Spikemg/kg 1.0 ND 3.39

SpikeSpike DuplRecv Recv RPD127% 127% 0%

LABORATORY CONTROL SAMPLE:

ParameterAroclor 1254

Unitsmg/kg

MDL1.0

ReferenceValue Recv25 99%

LRPD

Method Detection LimitRelative Percent Difference

9608 Uiiel Boulevardlenexa. KS 66219TEL: 913 599 5665FAX: 913 599-1759

Offices Serving: Minneapolis, MinnesotaTampa, FloridaIowa City, IowaSin Francisco, CaliforniaKansas City, MissouriLos Angeles, California

Charlotte, North CarolinaAsheville. North CarolinaNew York. New YorkPittsburgh, PennsylvaniaDenver, Colorado


RAW DATA

This section includes all Data entry forms, Chromatograms andQuantitation reports for each sample.

*:*(> PM KANSAS REGION

Sample and Analysis Data Entry Form - Modified Sample(s)

Tetra Tech Inc. Client No : 501528Ms. Michelle Beckrnan : Client Contact

; Manager >/10 East Cambridge Circle •/ : AddressKansas City, KS. 66103

913-621-6041 : Telephone No913-621-6028 / : FAX No

MProject No: 520512.505 Due Date: 6/0/2/92 Client P.O. No:

Project Manager: M3-V Project Name: Bennett's Dump 4811-06Manager's Name: Judy Uellre-Ft-Project Type: A AnalyticalQC Level: A Report Style: dDesc: 920428100

Sample No: 60 006287.0 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB1 - 2.5Bottle Types: GN

w Comnt: Matrix: SOILAnalysis Abbr: Name:8080SPCBGC PCBS IN SOLIDS/LIQUIDS/SOLVENTS

Sample No: 60 006288.9 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4

4, Due Date: 5/29/92 Sample Desc: HB1 - 4.0Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:HOLD No analysis requested

Sample No: 60 006289.7 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB2 - 1.5Bottle. Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:8080SPCBGC PCBS IN SOLIDS/LIQUIDS/SOLUENTS

Sample No: 60 006290.0 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB3 - 1.0Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:HOLD No analysis requested

PACE, Inc. reserves the right to return all samples at its discretion.

4:26 PM KANSAS REGION


Tetra Tech Inc. Client No : 501528—: Ms. Michelle Beckman : Client ContactProject No: 520512.505 Due Date: 6/02/92 Client P.O. No:

Sample No: 60 006291.9 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB3 - 0.5Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:8080SPCBGC PCBS IN SOLIDS/LIQUIDS/SOLUENTS

Sample No: 60 006292.7 Collected Date: 5/11/92 Collected By: CLJLN1Lab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB2 - 2Bottle Types: GNCornnt: Matrix: SOILAnalysis Abbr: Name:HOLD No analysis requested

**Sample No: 60 006293.5 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB1 - 3.5Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:

11 HOLD No analysis requested

-Sample No: 60 006294.3 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB2 - 2.5Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:HOLD No analysis requested

'Sample No: 60 006295.1 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB5 - 0.5Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:8080SPCBGC PCBS IN SOLIDS/LIQUIDS/SOLUENTS

PACE, Inc. reserves the right to return all samples at its discretion.

. .. w t PftGE: 34:26 PM KANSAS REGION


Tetra Tech Inc. Client No : 501528Ms. Michelle Beckrnan : Client Contact

^Project No: 520512.505 Due Date: 6/02/92 Client P.O. No.

Sample No: 60 006296.0 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB5 - 1.0Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:HOLD No analysis requested

Sample No: 60 006297.8 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB4 - 0.5Bottle. Types : GNComnt: Matrix: SOILAnalysis Abbr: Name:8080SPCBGC PCBS IN SOLIDS/LIQUIDS/SOLVENTS

Sample No: 60 006298.6 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB4 - 1.0Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:

..). HOLD No analysis requested

Sample No: 60 006299.4 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB6 - 0.5Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:8080SPCBGC PCBS IN SOLIDS/LIQUIDS/SOLUENTS

e No: 60 006300.1 Collected Date: 5/11/92 Collected By: CLIENTLab Rec'd Date: 5/12/92 Checked-In By: MDT Priority: 4Due Date: 5/29/92 Sample Desc: HB6 - 1.0Bottle Types: GNComnt: Matrix: SOILAnalysis Abbr: Name:HOLD No analysis requested

PACE, Inc. reserves the. right to return all samples at its discretion.

PACE, INCORPORATEDSAMPLE CHANGE FORM

PROJECT NUMBER: 3"? 2. 3 1? CLIENT NAME:

SAMPLE NUMBER(S): An Oo(_ f, K Pi

ATTACHMENT 3

CHANGE: EXAMPLE NEW CLIENT FORM

///§//g

V v/

WHY: A/ - 7, - /.

MATRIX:

ANALYSIS:

TTD

REQUESTED BY: _,

INITIALED BY: _.

DATE CHANGED:

DATE: ~/'-

DATE:

OPERATOR:

PLEASE DELIVER IMMEDIATELY TO SAMPLE CHECK-IN.

CC: CHL - GC/MS Volatiles. MSR - Semi-Volatiles

CEG - GC VolatilesBJS - Inorganic ManagerNRH - Organic ManagerMSR - Organic Prep Lab

- other

(Initiator must circle manager(s) to be notified)

EET205/et

RECIPIENT'S COPY

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AR1016-012492SFLI-BLAWKAR1016-012492SFLAR1016-011692SFLAR1016-011692SPLARI221-012492SFLAR122S-011692SFLAR1221-011692SFLAR1232-012492SPLAR1232-011692SPLAR1232-011692SPLAR1242-011792SPLAR1242-011792SFLAR1242-050692SPLAR1248-012492SPLAR1243-011792SPLAR1248-011792SPLAR1254-0124923PLAR1254-011792SPLAR1254-011792SPLAR1260-012492SFLAR1260-011792SPLAR1260-011792SPLAR1262-012492SPLAR1242-0124923PL60006865860006S66660006067460006S6S2600068674IBLKAR1242-050692SPLar!262-012492ar!26S-012492ar!2i=-0!2492EDlar!262-012492splA?.12eO-031192SPLISLKAR1242-050692M3Li; 052192K8LK 052292LCS 05229260006S690

Sequence Sacple DescriptionsSatple Site Rack Vial Sacple ISTD Inj.Nutter Acount Acount Volume

250b

25blOOb250b25blOOb

250b25blOOb250b25blOOb250b25blOOb250b25blOOb250b25blOOb250b25blOOb

250b250825blOOb250b25Gb

250b

US *!FE

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AAAH

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1

1

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1

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1

1

1

1

1

1

1

1

11

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1

1

1

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1

1t

1

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1

1

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1

1

1

11

1

1

1

1

1

1

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11

1

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1

1

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14

1t

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111

1

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1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000l.OCC1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000

1.0001.0001.0001.0001.0001.0001.00.)1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000.000.000.000.000.000.000.000

2.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.000

Oil.Factor

1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0000.10010.0001.0001.0001.0001.0001.0001.0001.0001.0001.0000.1000.1000.1000.100

Mult Divisor

1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000

1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000i.OOO1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000« A /•. .*ii . VVV

1.0001.0001.0001.0001.0001.000

Addend

0.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000O.GOO0.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000O ft M :'\. vvv

InstFile

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OutputDevice

LPT1:.LPT1:.LFT1:,LPT1:.L?Tl:,iLPT1:.LPT1:,LPT1:.LPT1:,'LPT1:.1

LPT1:,:LPT!:,LPT1:,':LPT1:.LPT1:,!LPT1:.LPT1:,!LPT1:.LPT!:ilLPT1:.LPT1:..LFT1:.!LPT::,;LPT1:.;LPT1:,:LPT1:.;LPT1:,!LPT1:.:LPT1:,!LPTl:,iLPT1:,!LPT1:,;LPTl:,iLPT1:,!L?T!:,;LPT1:.'LFT1:.:LPT1:,!LF'Tl:.'LFT1:,:LPT1:,LLPTl-.,;LPT1:,.

46 60006871247 SC006S7044£ 60006S712

• 50 AR1242-050692\ 51 AR1242-0506923PL

52 HBU-05229253 LCS-05229254 60006287055 60006289756 60006291957 60006295158 60006297859 60006299460 60006725261 60006725262 I -BLANK63 AR1242-050682SFL64 AR1242-0506923PL65 60006370466 60006871267 60006725263 I-BLANK

* 69 AR1242-050692SFL70 AR1248-0111792SPL71 I-BLANK72 AR1242-050692SPL73 AR1242-050692SPL74 KBLK-052792

I 75 600068585* 76 I-BLANK- 77 AR1242-050692SPL

78 AP.1242-050693PL79 60006859580 AR1242-050692SPL81 I-BLANK82 AR1242-050692SPL33 AR1242-05C692SPL34 KBLK-052B92

IT 35 60007027036 500070270S7 60006353538 60006B53589 60006358590 I -PLANK91 i -BLANK92 ARl242-050i?23PL93 AR1242-05C692SPL949596579399

>. 100

250b250t

250b250b

250b250b

250b250b

250b250b

250&

250b250bPCS SOIL

250b250b

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5.7505.3305.700l.OCO1.0001.0001.0001.0005.2005.1305.7005.5305.2905.2005.4905.4901.0001.0001.0005.8305.7005.4901.000l.OCO1.0001.0001.0001.0001.0001.000l.COO1.0001.0001.0001.000l.OCOl.COOl.OCO1.0005.1605.1601.0001.0001.0001.0001.0001.000l.OCO1.000l.COO1.0001.000l.OCO1.0001.000

1.0001.0001.0001.0001.000l.OCO1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000l.COO1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000l.OOC1.0001.0001.0001.0001.000l.COC1.0001.0001.0001.000l.OCO

2.0002.0002.0002.UOO2.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.0002.000

10.0001.0001.0001.0001.0001.0000.1000.1000.1000.1000.1000.1000.1000.10010.0001.0001.0001.0001.0000.1000.1000.1001.0001.0001.0001.0001.000l.OCO0.1000.1001.0001.0001.0001.0001.0001.0001.0001.000C.I 001.0000.1000.5000.1000.0501.0001.0001.000l.OOC1.0001.0001.0001.0001.0001.0001.000

1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000l.OCO1.000l.OCO1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000l.OCO:.ooo1.0001.0001.0001.0001.0001.0001.0001.000i.CCO1.0001.0001.0001.0001.000

I.CCO1.000l.COOl.COOl.OCO1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000l.OCO1.0001.000l.OOC1.0001.000l.JOO1.0001.0001.000l.OOC1.0001.0001.000l.COO1.0001.0001.0001.0001.0001.0001.000l.OCO1.000l.COO1.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.0001.000i.OOO

o.occ0.000c.ooo0.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000 . COO0.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000c.ooo0.0000.000o.oco0.0000.0000.000c.ooo0.0000.0000.0000.0000.000o.oco

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LPTl:.;LPTl:, ILPTl:.1.LPTl:, ILPTl:,!LPTl:, ILPT1:,ILPTl:,!LPT1:,ILPTl:,1

LPTl:,LPTl:,!LPTl:,LPTl:,:LPTl:.LPTl:,1

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r i l e rt/riit r i l e n.e File Mode Kate Factor

4

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3it5b7S9101112131415Ifc17IS192021nn

2324252i27282930313233343536373S394041424344454S474349505152535455

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1AELC19lAELfcaO1AEL0611AEL0621AEL0631AEL0641AEL0651AEL0661AEL0671AEL0681AEL0691AEL0701AEL0711AEL0721AEL0731AEL0741AEL0751AEL0761AEL0771AEL0781AEL0791AEL0801AEL0811AEL0821AEL0831AEL0341AEL0851AELC361AELOS71AELOS81AELOS91AEL0901AEL0911AEL0921AEL0931AEL0941AEL0951AEL09&1AEL0971AEL0931AEL099iAELlOO

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1AEL059lAEi.060lAELCtl1AEL0621AEL0631AEL0641AEL0651AEL0661AEL0671AEL0681AEL0691AEL0701AEL0711AEL0721AEL0731AEL0741AEL0751AEL0761AEL0771AEL0781AEL0791AE10801AEL0811AEL0321AEL0831AEL0341AEL0851AEL0361AEL0871AEL0881AEL0891AEL090lAcLG9i1AEL0921AEL0931AEL0941AEL0951AEL0961AEL0971AEL0981AELO??1AEL100

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"in t i i i i t u c i eiPrep Date: Method:

Check: 20: 500: 5000: .0 500g + 20:

SSKfinr Project* Cfient-' Client I.D. Wet Wt. % Moist. Dry Wt.

/VC.Final y<$f.

-0

6,10

6.9-0

\;

Surrogates:

Matrix Spike:

Commsnts:

Analysts:

V)

Reviewed By: -9V)

T ^1I — I

Reagents

tftr :-

Date: Extract Location:

014

I N C O R P O H A T E OI N C t S S U I t l C E O f O U t H T T

Prep Date: Method:

I Baiarialance Checfc: 2g; 50g: 60 SOOg: ^DO .O SOOg + 2g:

PU * Cnentl.D. WetWt. % Moist. Dry Wt. Final Vp

5 i 1,0

\\

x\

\X

Surrogates: i^-Ot Itt/S

Matrix Spike: [

r ^^n

Comments:

Analysts: Reagents

0

A ,

Reviewed By: I Date: [_

N2 '031

1 „- — • 1

Extract Location:

oo

091

•

O

SUBSET ABBREVIATION: 8080SPCBGC SUBSET CATEGORY: 0

SUBSET NAME: PCBS IN SOLIDS/LIQUIDS/SOLVENTS

.DATE COLLECTED:\

DATE RECEIVED:

MATRIX:

DATE EXTRACTED/BY:

INITIAL VOLyk/7

FINAL VOL:

ANALYZED BY:

PARAMETER NAME

Aroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Voclor 1248

1254

05/11/92

05/12/92

SOIL

CLIENT

PROJECT

DATA RE'

ENTERED

f-JOt., SAMPLE 1

Qtr^lj SAMPLE 1

EVA

ABBREV.

PCB1016 SPCB1221 SPCB1232 SPCB1242 SPCB1248 SPCB1254 S


Tetra Tech Inc.

HB1 - 2.5

60 0062870

UNITS: mg/kgDATE:OIL: //->

MDL

1.01.0

PCB1260 S 1.0DBCSURR

DATE:DIL:INST:

FINALRESULTS

jjf)

COMMENTS:DATE: 05/15/92

MAY BE DUPLICATE COPY

J.i r t- . •_ •• '... xi-'. . :

iL. J il1 l-4l.iiul..i('-:"

i rii:-l r ' . n f i f ' r it.

.; (-!'..( "1 iJOc-l III p 1 ir_' I'

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K. •-..>} 1 I.I- 'L rioi i /1)

Lhai in'. • J

pen AM A!... Y

A ''I; iti'v Ranr.K-.:- 1 OGO

1 nter f ace Serial tt : 1248574035D e 1 ct y T i«i e : 0 . 0 < J m .1. i"i.End Time : 6'3.0<"' ruin.3 a m p 1 i n g R a t e : 1. . 0 0 0 O p 15 / r

:; e c

Data Acquisition Time: 5/23/92 1.8:45

Raw Data Hile : c:\270O\data\lAELG54.rawR e s LI ] t. F .11 e : r.: \ 2 7 O 0 \ d a t a \ i A E L 0 5 4 . r s t.Instrument 1-ile: c: \270v.' \data \1 lae .1 . J.HBP roc e s B F j. 1 e : c : \ 2 7 0 O \ cl a t a \ 11 a e I . p r cSample File : c : \2700 '^c.lata\ J. lael . smpSoautfnce File : c : \2700\c!at.i?i\.'i .lael . sen

.1 nj . '.'olL.ifieSample Amount

2 Mb /ML.5.20OC'

A r e a R e T e c t. : 0 . 0 0D i 1 u 11 o n F a c t o r : 0 .10

No15 e T h r e5noid: 61-lu Itiplier : 1. 0000

A r e a T h r e s h o 1 d :Divisor : 1.0000

B u n c h F a c t. o r :Adder : 0.OOOO

Instrument Conditions:Packed Column GC -

InstrumentColumnColumn LengthCarrier GasFlow RateTemperatureInjection Temp.Detector 1Ds tec to r tern pNotes

KSlli1 . 5XSP-2250/1 . 95/:SP-24016'x 2mm or, 100/120 SUPELCOPORTAR/ME 95/55 5 m 1 / m i n208250 CECD350 C

of Peaks Detected: 3

PRIMARY ANALYSIS

Peakt

i7

'•n

5

Ret Tios[sirs]

2.003"i 1°S3.4635.769

S.463

[uV]

S5220

691S12SO

PAC

Arts CcisporieTit

[uVtssc] Nase

9631692

6322231

9624

E. INC

BL

SVVBSBBSBE

. PCS REP OF.

Ex t rac t Uonc.nc/sL

6.40S16.601

3.9278.357

19.9S6

iT

Siljie LOuC.

eg /to

0.1230.319O.C760.1610.3S4

/ J. . 1JZ tSiv 1.A . 1 /b'Dt.

E 4S.36s 31 2453

5339 4517 /6

,> Group Re- port For : AR

Peak Ret Tite Peak Ht Areat [sin] [uV] [uVtsec]

1 2.612 0 02 3.311 0 03 4.250 0 0

0 0

1242

CoeponentNate

Arcl-1242 1

Arcl-1242 2Arcl-1242 3

ft CJ..'»0

BB 0.;»4

127.623

BL E x t r a c t Cone.ng/iL

VV 0.000

VV 0.000VV 0.000

0.000

i . . 0 V

0.009

2 .454

Siiiplt Cone.itg/kg

0.000

0.0000.000

0.000

Group Report For : AR1248

Peak Ret Tiae Peak Ht Area» fun] [uV] [uVtsec]

4 5.290 0 0* 5 7.760 0 0

7 ?.080 0 0

0 0

'C-Jroup Report For : AR

' Peak Ret Tite Peak Ht Area1 [ain] [uVJ [uVtsec]

6 8.301 0 03 11.918 0 0? 13.500 0 0

0 0

*

Group Report For : ARj

Peak Ret Tise Peak Ht Area* isinj [uV] [uVtsec]

10 15.160 0 011 17.200 0 012 19.400 0 0

0 0

CotponentNa*e

Arcl -1248 1Arcl-1248 2flrci-1246 3

1.254

ComponentNate

ft r r\ < ^ C » <m Cl iiJt'A

fircl 1254-2fircl-1254 3

.260

CosconentNaie

Ar:i-1260 1Arc!-1260 2Arel-1260 3

BL Ex t rac t Lone.no /si

VV 0.000VV 0.000VV 0.000

0.000

BL Extract Cone.rig/r:L

VV 0.000

VV 0.000VV 0.000

0.000

EL Ea t rac t Cone.ng/sL

VV 0.000VV 0.000VV O.GOO

0.000

Sacsle Cone.no /kg

0.0000.0000.000

0.000

Saiple Cone.ID /kg

0.0000.0000.000

0.000

Saeple Cone.«g/ko

0.0000.0000.000

0.000

Group Report For : SURROGATE

^'peak Ret Tise Peak Ht A rea

if [tin] [uV] [u'.'tssc]CuEporient

;<a«;e3L Ext ract Cone.

fiO/iiL

saspie Cone.35/1:0

w-ii isc

4413 65.526 1.260

.IMC. PCL< REPORT PAGE Mo,

r'l.L- l_r'r\LjniJ

iati'.e Nue : 600042570

Start Titc : C.OO i.inScale Factor: -1

Er.d 'ire : t'.OO tinFict yffset: 2* tV

Saioie »:

Date : 5/17/92 07 :52

Lc« fo;nt : 2*.C »V

Plot S c a l e : 30 iiV

F a c e 1 of :

Hioh Point : i4.4S »V

I

Ji

c

\ CO

•-•' nn

-

40

T. 5

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«t

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\ i i i i i ii iii ii ^__ _ j j _^

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< <-"5! <<! < < < < <COD

i0 10

i i j i i i t i I I ! I I I I i I I ! i; ' I ! I I ' I ii

I :

40 50 60

[ m i n ]

o>ooo0>to0710



1ATE COLLECTED: 05/11/92

DATE RECEIVED: 05/12/92

MATRIX: SOIL

DATE EXTRACTED/BY:

INITIAL VOL:/L/f J~< /3<\-J ff 1

FINAL VOL: o20Wj

ANALYZED BY: -&*) A

PARAMETER NAME

%r

Aroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248•'Voclor 1254


CLIENT NAME:

PROJECT NUMBER

DATA REVIEWED

ENTERED BY:

SAMPLE NAME:

SAMPLE NUMBER:

ABBREV. UNITS:

MDL

PCB1016 S 1.0PCB1221 S 1.0PCB1232 S 1.0PCB1242 S 1.0PCB1248 S 1.0PCB1254 S 1.0


Tetra Tech Inc.

: 520512505

BY: O C/1 / ^

.€*&

HB2 - 1.5

60 0062897

mg/kg clAzk-y-DATErVj/ DATE:

OIL: A'3 OIL:INST: /// INST:

A//)I/ /J/t-3.A//)

)/fo& y

FINALRESULTS

|

J/•3L3')

\/

9*?

COMMENTS: U<DATE: 05/15/92


'ciiuif-lp J £.' ! - : c : f i l » '

.1. niit. i'"Lifiit".-ri t.'s

.; ULI tobi.'iiifii J f.-r"' Rack /V ia l

T j. int-'; 11U Q V

'r.Slll

r'b i-i ;:»'(.:> _••<."•.

0 / 0

PCM HiMAi... v:;; i;:.

i/'D iii'v K'w-' 1 OOO

Interface Serial tt : 1248574035 Data Acquisition Time: 5/23/92 19:Delay TimeEnd TimeSampling Rate

Raw Data File-Result FileI n s t r u m e n t F i 1 eProcess FileSample Fil e3 e q u e i"i c e F i I e

I n j . Vo ] ume

i'--! Q 1 £ 'i-i1 1

Mul tip],'i f ' e 5 h O 1 d

0.00 mm.65 . 00 fiiin .1.0000 pts/sec

\2700\data\lAEL055.raw\27OO\data\lAEL055.rst

c

L.

\2700\data\ l lad. ins\2700\clata\llael . prc\ 2 7 O 0 \ d a t a Ml a e 1 . s n: p\ 2 7 0 -0 \ d a t a \ 1.1 a a-1 . s & q

2 MB/ML

1.0000

A f t; a R L-.1 j f C t

D i 1 u 11 o n !~ a c t o •

A r t; a T h i" e ~, h old :Divisor : 1.00OO

i. A f i c i" i ' a c. 1. o r ; 1Adder : 0.0000


k Instrument•jj|' Column

Co 1umn Leng t hCarrier GasFlow RateTemper a tu r eInjection Temp.Detector 1Detector tempNotes

KS1111.5XSP-2250/1 -95X3P-24016'x 2mm on 100/120 SLJPELCGPQRTAR/ME 95/55 5 m 1 / m i n

250 CECD350 C

Total Number of Peaks Detected: 21.

PRIMARY ANALYSIS

f: - - ' r" - 4> *

* [«B]

1 2.12 .6

!;E

93

05•» f\r- T0 .ICO

Ftdl. Ht Area

[Uv] [lJy>iE':J

253 3=63 '-

ivf 1 C

PACF.

CoftsoneritNa<:&

2494 A rc i -1242 103 Arc l -1242 2

4 .4:2 159 1723j 3.7 01 227 2361

, INC

DL

. PCS

Ext rac t

REPORT

no/eL

^1V

5iV

V

V

9

yi iV

V

19439

13

.5

^

w

t• 1

Os537539

.001

S.Q/;

0c0ou

Cone.Fi

.3EO•"*i '- ^

.175

.175

,2j3

6 5.794 3449 t.142 £•:?

10 e.565 7~6

11 7.7J3 11931 12 8.475 537

. 13 9.000 316• 14 10.990 137

15 11.347 17516 13.433 20717 17.065 9718 28.318 3019 29.971 4020 33.443 461621 62.405 9

12938

Group Report F

Feat Ret Tu,e Peat Ht* [ain] [uV]

• 1 i 1 (\ c '7

2 3.233 1573 4.2C1 1270

1490

.Group Report F

:'eak Rst Tiae Peak Ht* [sin] [uVJ

4 5.220 10205 7.703 11937 9.000 816

r """

Grouts Renort F

Peak Ret Tise Peak Ht* [tin] [uV]

s 3.301 08 11.347 1759 4 •* * f\ •• ••> "i 1

Ij.ilJ i07

<c!81693117990475:: Arcl-1243 21293834S16 A r c l - 1 2 4 3 3

68625608 Arc l 1254-29437 Arc l -1254 35273 Arcl-1260 220851798

450999 DEC2343

681722

or : AR1242

A r e a Coupcinerit[uVtsecj Kane

494 A rc l -1242 11503 Arcl-1242 2

19942 Arci-1242 3

21939

or : AR1243

Arsa CDBDonent[uVtsec] Kase

31806 fircl-1243 147522 Arel-1243 234816 Arcl-1248 3

114145

3r : AR 1254

Area Coiponent[uVlsec] Nate

0 A r c l 1254-15603 Arc ! 1254-2

VV

V »

VV

VV

VV

VV

VV

VB

FB

BB

BE

SB

B3

SB

BL

EB

VV

BV

EL

: M >V V

VV

VV

BL

VV

VB

*• -

15.9644 3 . 4 3 937.20460.39438.350o9.634

9.16511.69313.01710.971

0.4380.591

63.5480.138

537.340

Ex t rac t Cone.na/sL

J •? c.Qt . / w'U

3.97544.403

en « TIJO, 100

Ext rac t Cone.ng.'sL

53.03360.39469.634

139.066

Ex t rac t Cone.no/.L

0.00011.698t •* ^ 4 "7i j . i1 i. i

0.3110.8470.7251.1770.7481.3570.1790.2230.2540.2140.0090.0121.3360.003

10.475

Sanple Cone.ng/kg

0.0930.1750.866

1.133

iasole Cone.ED. 'kg

1.1311.1771.357

3,666 /

/$ - t'^trfr/fLt

Sctole Cone.»Q/kQ

0.0000.223A ™i r <0. J:>4

13045 24.715 A ,«.--nU . - f O i

vbroup Report For '. AR1260V'

Peak Rst Tie? Psak Ht Ext ract Cone.

It l!.leC 0 0 A r c l - l T o O 1 VV C.OOO11 ::.c-fc5 97 5:/; firci-i:to : ts 10.971i: ii.;ct o o ;rt i- i :6C :. ;; o.ooo

1 97 5273 10.971

Group Report For • SURROGATE

Peak Ret Ti»e Peat Ht Area Component BL Ex t rac t Conet [Bin] [uV] [uVJsec] Na*e ng/sL

13 33.443 4616 450999 DEC 6B 68.548

4616 450999 68.549

PACE, INC. PCB REPORT

0.0000.2140.000

0.214

Saoipie Cone.nq/kq

1.336

1.336

PAGE No. 2

t

Sdtc'.f liiit : 600Ce2:97: ::\:700\diiti\lfiELf.55.ri

S t a r t T:«e : 0.00 i:nScale Fac to r : -i

tn(! lite : fc'.OO n:nf'iot G i fse t : 24 tV

Sii&le t:Date : 5 / 2 7 / 9 2 C 7 : 5 5lot Point : 24.42 §VPlot Sca le : jO *V

Past 1 ct 1

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32.0-

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29

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.1 o * '"> 1 £; •"/ ••~- '""• -1 '"?• '— ' T ~J TM- Q i _£i i^J ^:>^ ^1^+ -i1-* -_/-;! •_•

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-i

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;i :—ii ii ,H! I! J31 i I

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28

f !;.•

oo



-JATE COLLECTED:

DATE RECEIVED:

MATRIX:

DATE EXTRACTED/BY:

INITIAL VOL:

FINAL VOL:

ANALYZED BY:

PARAMETER NAME

Aroclor 1016Aroclor 1221Aroclor 1232.Aroclor 1242Aroclor 1248,4n>clor 1254

Aroclor 1260

05/11/92

05/12/92

SOIL

5-l<yJ*M/->

g<»h

(Surrogate)

CLIENT NAME:

PROJECT NUMBER

DATA REVIEWED

ENTERED BY:

SAMPLE NAME:

SAMPLE NUMBER:

ABBREV. UNITS:

MDL



Tetra Tech Inc.

: 520512505

BY: C£6£/l-T/''

£Kfr

HB3 - 0.5

60 0062919

mg/kg s Lzk^DATE : /'7/^ ' DATE •OIL: /:? OIL:' FINALINSTy&T/// INST: RESULTS

///) /Jf)

jfa 7"? L

/7*y

COMMENTS: HIDATE: 05/15/92


MI 11 . f. i-f ir.'l 'i -i" :.

••..•r :.i *_•:.:• r :.

: i rl, i. I1 u.;l;C'l i H

i i 11. • . , : ' . :" i ; - i i .

r--'. ci (... k / V .1. ,:-i. i

Interface Se'ri a] 11 : J.24057'103^ Oat a Mtzquisi t i on Time: >j.' '23/92Delay Ti.m& : 0. >.>0 nil. n.End Time : 65.00 min.

Sampling Rate : 1. 0<" 00 p t •:;. / •:-: •!-c

Raw Data File? : c: \27OO\cici t.a \ 1AEL056 . rawResult File : c : \2700\clata \ 1AEL056 . rstInstrufiierit F iJo : c: -.2700\ci ato \ 1 lae 1 . insProcess F x 1 e : c: \2700\data\ l l .ael.prc:c:i ci ii'i pi I t? F" i. J. ei1 ! C : \ . :! / U'-..' d a t a \ .1 1 a & 1 . S> i'ii p

beouence f: j 1 c? : c : \27oO\dat.a\.l..l.ael . :~eq

.1. n_i . '-,'0 1 uniC:' " ...:' ! 'il-i .•' ML.Sample Amciunt : 5.7OOO

I'-.loi&e T!ire£holci: .->f'lu Itiplier : i . OOC>0

f-'irea Reject. : '.J „'...'OD i 1 '...t t .i. ci n F' a c t. o r ; C>. 10

Uivisor 1.0000i-i L.I i'i C h F 3 C t. O r : 1

1-1 d d e r ^ O . ''.'• •-.) '•..• i.'1

I n s t r u rn e n t C o n c:i 2. t. i D n s :Packed Column GC -

Instrument :KSlilColumn : 1 . 5/i.SP--22?0/l . 95X3P-2401Column Length : 6 ' >: 2 mm on 100/120 SUFELCOPGR"Carriei- Gas :AR/ME 95/5Flow F;ate : 55 ml/minTemperature :208Injection Temp.: 250 CDetector 1 :ECDDetector temo :35O CNotes i:

TotaI Mu.ffiber of F'eaks Detected: 3

PRIMARY ANALYST!

' A C- c.. 1 !'%J C . P C i R E F' U R T

'"ii'r, Rtt Tile Psil Ht Are3

•I [e ir i ] [ i i V j [ i iV!=5c]Ext rac t LOHC.

;

-,

^

1'

4

7

^._3

. Jii

.1=9. _,

.i'J:

,4c4

H• i !j.1 i C

,. §?*l

77

717C 7 •'•

i«^ • 1 n»^ J

-_j nr:;-l^ 1

C •-.' /

:S

3E_ r::;

SB

7

SJ

•:

•

.cl^

.936• ~ >•

.:•:'•;

.IIS

0c

(i

.0=74 CT

. : J/* — f:

, '-i ,

/• T n. V .• i

O . i a 4

a ::.i>: 4i.:s

5321-

*;•:;:: :•:

458"?

ts 67.394

120.692

1.162

2.117

. ' .- 'ruLip Report For : r-'iK'l ,'M'..'

Peak Ret Tite Peak Ht« [cm] [uV]

1 2.607 542 3.311 03 4.250 0

54

Area Component[uVlsec] Kane

423 Arc l -1242 10 ,'rcl-l?42 20 Arc l -1242 3

423

BL Ex t rac t Cone.ng/iL

BB 4.089

VV 0.000VV 0.000

4.089

Sample Cone.eg/kg

C.072

0.0000.000

0.072

G5roup Report. For : AR12/I3

Peak Ret T:*e Peak HtIf [«in] [uV]

4 5.290 0* 5 7.760 0

7 9.080 0

0

Area Component[ u V » 5 e e ] Ka»

0 Arcl-1248 10 Arcl-1248 20 fircl-1248 3

0

SL Ex t rac t Cone.na/uL

VV 0.000VV 0.000VV 0.000

0.000

SdJislE Cone.so /kg

0.0000.0000.000

0.000

•Group Report For : AR 1254[

Peak Ret Tiee Peak Htt {tin] [uV]

6 8.801 08 11.918 09 13.500 0

09

Group Report F

Peak Ret Tiss Peak Ht« [tin] [uV]

10 15.160 011 17.200 012 19.400 0

0

Group Report Fi

Peak Rst i lie Peak Ht# [sin] [uV]

Area Component[uVtsee] Naie

0 fircl 1254-10 Arc l 1254-20 Ar:i-1254 3

0

or : AR1260

Area Coinponent[u'.'Jsec] Kaae

0 Arcl-1260 10 Arei-1260 20 Arcl-1260 3

0

or : S U F; F; 0 G A T E

riftd COftpOHcrit

[ y V t s s c ] KafiS

BL Extract Cone.ng/iL

VV 0.000-VV 0.000VV 0.000

0.000

SL Ex t rac t Cone.ng/iL

VV 0.000VV 0.000VV 0.000

0.000

BL Ext rac t Cone.ng/sL

Sacple Cone.no/kg

0.0000.0000.000

0.000

Saaple Cone.ag /kg

0.0000.0000.000

0.000

Sample CMC.sg/kg

4S36 67.394 1.132

PACE, J i - J C . PCS hEPORT F'AGF I'-lo. 2

. \

Sit::t Kilt : cOOF:!el.i»e : ::\27001.d,»ti\lfitLC5i.rinSti't Tut : C . O O iir. Entf Ti*e : a ' .OO »:r,Scile Fictor: - • ? ! o t O f f s e t : 24 rV

t:Dite : 5/27/92 C7:57LO* Feint : 24.45 »VFist Scale: 30 »V

rioe 1 07 1

Hioh Point : J 4 . 4 5

I

50-

III 1 1COI

I1

45

ff\

f™"

.'•>'*-/

CLuT0)

40 — j

-1

Ji

Hi

_ I35-

i --iiii- j

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••-)l'

If

! i l l ii £M

i i i i i

I O i" O L>'_> U Cj O CJ O1 C£ '"''/y ccCi cci Cc; 'j; o; Qii -sj. <£-? <.-=i. < ^? <. •=!. ^

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I I I I I

201OI I i I ! !

t>0

; i rn e Ir ~\ii i---,-—, i t—-.s_ i > ! ' • l J

oOo>ts>

PACE



DATE COLLECTED:

DATE RECEIVED:

MATRIX: SOIL

DATE EXTRACTED/BY:

INITIAL VOL:

FINAL VOL:

ANALYZED BY:

PARAMETER NAME

Aroclor 1016Aroclor 1221Aroclor 1232.Aroclor 1242Yoclor 1248

r 1254

05/11/92

05/12/92


CLIENT NAME: Tetra Tech Inc.

PROJECT NUMBER: 520512505

DATA REVIEWED BY:

ENTERED BY:

SAMPLE NAME:

SAMPLE NUMBER: 60 0062927

HB2 - 2

ABBREV. UNITS: mg/kg

MDL


1.01.01.01.01.01.0


OIL: OIL:INST:

N/O

FINALRESULTS

A/0

0/Oo



' . - . • • ; • • .' ,.u: ( . - •;..-./ f ' .Loie! "I j rn-;

•, ] !i i J J-'1'1! ;-:.:"•'.'• -I -: O . OO / r u n .: ''! '~* . O'.'i (n . i I • .

~l. F ' . . ' iu - ; • • . , : ' • . • . : . • < . • • . ' ' \ v . ; . . . i ' : . . . • ' - . . i . M ! 4•....:..:. i .' . - • •. l:::(.:-l; !. F'> '!:.•; i. I: \ ,.''". 0 • ' • M !, •. 1 ,.i • .' .'! ,'. '1 -: - J.! : "

i- •.: -ii ! .'. J. (:i ; i. ;. •-.'.:! / '..".' '.. cl -..I '. 1.1 '•• i. •. -'.A i" • • » . ! ) I" C

• s > !•• : ; •- , .-. . '••.:,•".•'•'.:•<":• •J . . . - ' : , - , j l . . : • . ••I . . - . : ; ..!• .-i i-. i.-'1 ; ' • . - . ' :.'• . '•'' . ':'.•'. 7O'O''-. 'Vi i p"' '•- i. i i"ii'" ':: . :: ; •'.!

•!; . : ! i: : >:• !'!(-/ 'hi

i'-;m':'un t. : .^. .LfcjOv';' pi •. ; ' t. • . . ; C-' '\ (

' . ' ' • J (..' '•' i. i !fi r - I -C t

r":r •;.••.: : I"'." •, -; !'•'. :': (..I :

• i j. -,.• _>_ •;.;.;'• ; .( . OO'^'O

:. : : . \ ; \ : < _ - ! i i. ; . - i . - | ,! i .J. I .: :'.•'. : •:.. i

"* ! :• •.::!:•:..-I'M .- KSJ .1 j

PRIMARY ANALYSIS

Hie .-*iR ,Ht r ; V e i

43

a •••; ;-t it/ib * t i . * & h -

' :;.:!(• T:

•c-r.l Ret lift? F'sal. Mt•f [s;.'.-J [oV] tuVlsec ] Nene r.g/tL

:

7

2.612

4.22?

0(io

0oArc! -1242 1

Ar-l-'^T •:

VV

VV

0 . 300u.OOO.1 M.'id

0.000fi.V-A

0.000

0.000 0.000

ii. Pel Iu.f F'fci!, Hi[liVlsec]

Con:. Sift.pl5 Cone.

;.

r-

5.4306.4006.8008.024

000o

0 fircl-1245 10 Arc 1-1243 20 Arcl-!24S 30 Arc l -2243 T

VVWVVVV

0.000O.GOO0.0000.0 JO

0.0000.0000.000C.00-3

oup Report For : AR 12

• F;et Tiee feak Ht Arsa[*in] EuV] [uVlseci Baas

e.soi" 9JB

oo/.V

•l

0 flrcl0 Arc l

•"i

!25<-l

1 2 5 4 3

^V 0.000•:-i O . O O CVV 0.000

.-. ;-„•;,';

0 . O'.'(l

M OO-'i

:'': ,'"'f"!M

;') .Vi.1"!

LIP r":i-;:-!.:i; ';. F-or : AF'\..12.'.<•.')

Area C:

u, -c

_C« *'£'.'•'. ',

:'!3t S ' - i l t : 0 cwF'- r t : M-I.V."

CNICft

D oJfNI I

!•••toto

1

IOo

I I I I I I ICNTMCM COCO DO

C-J CM CM!

I I I I Il._l i I—I

cx_>o uo: 01 LL ctirr

CM-M-,,:--

1

i i iJ. t oi?) 1O <D

oj c,~ < -

(J CJCt

Io

aar

CM-d

c;CM

1

ioCM

I

Ocr

'T

Time [mfn]

i/~>

ro1

Al \--V

aCDo

ooo3>'N>a*•u)

PACE


NAME: PCBS IN SOLIDS/LIQUIDS/SOLVENTS

DATE COLLECTED:

DATE RECEIVED:

MATRIX:

DATE EXTRACTED/BY:INITIAL VOL:FINAL VOL:ANALYZED BY:

PARAMETER NAME

05/11/92

05/12/92

SOIL

'-V ML.

Aroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242roclor 1248

Aroclor 1254




DATA REVIEWED BY:_ /'"7 -/,

ENTERED BY:

SAMPLE NAME: HB2 - 2.5


ABBREV. UNITS: mg/kgDATEOIL:

MDL



OIL:INST:

FINALRESULTS



PRIMARY ANALYSIS

'.I'-' •'•. -'•''•' -

- 6 7 2 V - 5SJ.CK-

V' : •!(.-:.. '.. t i i ;• r i lv. i . . ' ' ' i . . ;

:;oi V"i? '-''it H\ -Vef Cccr : ' " . - r t[fir] !- jV] [aVI-ec] «=«e

'i' '.rf!i.'. Cone

(HI / (.3

2.4123.31!4.229

0 fire!-'242 !0 r fC i - i iS i I

0 Arcl-i2i? .'

vvVI1

o.cooO.MO

0.000

M. 000

C.fOO

i.i.- i - ; c ~ i • . • . ; ; . I i •> ; . M ! - . - . : • • • ; ; • (

Nirte n^ •'* L

J? CMC.

, .,,. ., ,, ;.,;.,"-, - ,,V ,; .V;.-;

^6.«50 0 Ofircl- i :«i- VV 0.000

R.OiM 0 0 ircl-ii'4t 4 VV 0.000

,, ,..

0.00?,'i ;'ii j

0.000

:•. -Jorc. c=*pjfr L-:-nc

0.000

Nafie

pls Ccf:c.

1S2CS

: :7. i53! - . £ £ •

0o0

0 irc;-12iO i0 Af i l - lZ iO 20 Arcl-1240 3

VVVV•!'•!

0 . 0000.0000.000

0.0000.0000.000

Ht ?rsc

] [tiVt:-:;Cone.

'-: 9

33

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fh-l

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..".'» r1!1 ' I I:!:t x-!n

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SUBSET NAMF: PCBS IN SOLIDS/LIQUIDS/SOLVENTS

—JATE COLLECTED: _

DATE RECEIVED:

MATRIX: SOIL

DATE EXTRACTED/BY:

INITIAL VOL:

FINAL VOL:

ANALYZED BY:

PARAMETER NAME

05/11/92

05/12/92

Aroclor 1016Aroclor 1221Aroclor 1232

fÂroclor 1242:; itroclor 1248-\roclor 1254




DATA REVIEWED BY:_

ENTERED BY: _

SAMPLE NAME: HB5 - 0.5


ABBREV. UNITS: mg/kg



O I L : /''J O I L :MDL INST:/^5/// INST:

FINALRESULTS



ri. 1.i.i dv

i (it it.!1 L.iiliC.'fit.

\ i-'iU I... O ;•)<'..! M i f ; 1 f;:r

K'iHC". k /' V i ii.!

:: i -S l l l:: PL A S

. i / i i

L,hi-ii ir it/ J MI'-.' K'i7-< r i ,rj £:••

interface Serial It : 1248574O35 Dsta Acquisition TimeDel a;/ Tifiie : 0.00 min.End Time : 65.00 rniri.Samplina Rate : 1.0000 pts/sec

Raw Datta File : c:\2700\data\lAEL057.rawResult File : c:\2700\da.ta\l.AEL057.r5tI nst r LUiien t Fi ] e : c : \270O\clat. a \llael . in s

c:\2 7 O 0 \ d a t a \ 1 1 a e 1 . p r cc : \ 2 7 < j O \ d a t a \ 1 1 a e i . 5 m pc:\2700\clata\llael.seq

Process FIT eSample FileSequence File

i n j . 'v'o 1 umeS a mpie Amount

2 MS/ML5.5800

r\ e j t.: C L

D j. 1 Li t i on F a c to r

N o a. E e T h r- e s h o id: t>Multiplier : 1.0000

Area Threshold :Divisor ; 1.0000

Bunch Factor: 1Adder : 0.OOOO

1nstrument Conditions:Packed Column GC -

InstrumentColumnColumn LengthCarrier GasFlow RateTemperatureInjection Temp.Detector 1Detector tempF- I „. j.. _ _r-j LJ T_ f

KSlll1. 57.3P-2250/1. 95/13P-24016'x 2mm on 100/120 SUPELCGPORTAR/ME 95/55 5 m 1 / m i. n208250 CECD350 C

"otal Number of Peaks Detected

PRIMARY ANALYST;

PACE. INC. PCS PEPORT

Psak Set Tise Peak Ht ArEi5 [s:r:j [liv] [i ivlEeC

Lciip Drier:' Ex t rac t CD.^sg/ig

T

3.••tV

-i

"

e

T

.202

.604

.4c3-!C?

• i ~!i T i /

£S

4=o/191223

5;351 firci-1242 1CC .'

7. r' ;'i

7S25

E?

BBit?3BB '

:.s4o y

.453 C

.S3? 0• i 1 0 C

.11?

.063

.Ob?

.159

.ico

:;BS 4355-. 110.187 1.975

LJI CLIP Report: 1 or : i-if\l. ,..'i .'"'V

/Peat Set Tine Peak Ht» [fiin] [uV]

1 2.604 46

2 3.311 03 4.250 0

46

Area Component[uVlm] Katie

351 A rc ! - 1242 10 Arcl-1242 2

0 Arcl-1242 3

351

&L E x t r a c t Cone.

ng/iiL

EB 3 .493

VV 0.000

VV 0.000

3.493

SatiDle Cone.«,g/kg

0.0630.000

0.000

0.063

Group Report For : AR 1.2-1 3

Peak Ret Tiiie Feat Ht1 [am] [uV]

4 5.290 05 7.7iO 0

*•* 7 9.080 0

0

x Group Report Fo

^ Peak Ret Tine Peak Ht_y * [tin] [uV]

6 3.801 08 11.918 0

9 13.500 0

0

Group Report Fo

Peak Ret Ties Peak Htf iiiin] [uV]

10 15.160 011 17.200 012 19.400 0

0

Group Report. Fo

> Peak Ret Tine Peat Ht* S [Bin] [uVj

Area Coiiiporient[uV lsec ] Nau,e

0 Arc l -1248 10 Ard-1243 20 Arc! -1248 3

0

r : AR 1254

Area Coaponent[uVlsec] Nans

0 Arc! 1254-10 Arc l 1254-2

0 Arci-1254 3

0

r : AR1260

Area CofiDonent[uv l sec j Naae

0 Arc!-12iO 10 Arc l -1260 20 Arcl-1260 3

0

r : iiUF-iRUiJA i ii

[uV tseC j Nifie

BL Extract Cone.

ng/BL

VV 0.000

VV 0.000

VV 0.000

0.000

BL Extract Cone.

fiQ/iL

VV 0.000

VV 0.000

VV 0.000

0.000

BL E s t ^ a c t Cone.

ng/*L

VV 0.000

VV 0.000

VV 0.000

0.000

BL E x t r a c t Cone.ng/sL

•>atto!e Coric.f i g / kg

0.000O.OGO0.000

0.000

Satple Cone.*g/kg

0.0000.000

0.000

0.000

Sample Cor.c.og/kg

0.0000.0000.000

O.OCv

SaBsIe Cone,rsg/ko

c. , l f>!C. t ' - 'L l- K t r - 'GK! p;'AGt:..

X•'f

ilefisle : C I \I;OC ; ' iij«ti\iAEi.C 11.Tin

'.o't Tue : 0.00 tin Ere hie : b ' . O O nr,:i:e Far ter : -1 Plot O f f s e t : 25 i:V

lot:ie I::«tt : 5 / 2 7 / 9 2 08:00LOU Point : ?4.66 *Vr io t s:«!e: oO *V

Page 1 of 1

r ich Poir.t : S.oj iV

Q

u i

OJVJ iTJ COI ll l i l

-J

40-

351

l j i»••

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: M i l I 11 I I I i I

! V *?~f ^fT ^ if-'. % <£ ?b! '•

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30 4O

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05


.SUBSET NAME: PCBS IN SOLIDS/LIQUIDS/SOLVENTS

•~-QATE COLLECTED: 05/11/92

"DATE RECEIVED: 05/12/92MATRIX: SOIL

DATE EXTRACTED/ BY:

INITIAL VOL:/, J/' £'M11 *> «)

FINAL VOL: -Q.c) /5

ANALYZED BY: &n fr

PARAMETER NAME

Aroclor 1016Aroclor 1221Aroclor 1232;Aroclor 1242"froclor 12484roclor 1254


CLIENT NAME:

PROJECT NUMBER

DATA REVIEWED

ENTERED BY:

SAMPLE NAME:

SAMPLE NUMBER:

ABBREV. UNITS:

MDL



Tetra Tech Inc.

: 520512505

BY: Mg&^-ifa^

&/wA- •

HB4 - 0.5

60 0062978

mg/kg -f/T A*DATE :V VX BATE:DIL: /;> DIL: FINALINST:&//y INST: RESULTS

A/0 A/9

/V /

W /-A/0 v

L ;71 V -7?'

//

^'/)

/

7'" ' ' 'L»



. ,C•'. '. sit'f'f; . i-r •=..

::.o.-nfj J C- NrXr.fe-

:]:••'.,il:j.. I C- Uuinl.n'.-1"

. j Pi tt :"L.l i l iC.- :r i 1.

Autu ' iai ' f ip .1 (..'I'

Rack .'Via ]

: l-'Cl.-: ANAL, v;..' ;:::1.1-1..

I-. 1") J11r'Ei AoB3.Ou

I J / 1 )

u.iT if "if..1 1

Interface Serial *l : 1.2 4 OS 7 4 03 5Del ay Tiine : 0 . 00 m in .End Time : fa5. GO mm.S a m p 1. i n g R ate : 1 . 0 0 0 O p t E / s e c

bat a Acquisition Time: 5/23,"-? 2 23:11

Raw Data File : c:V2700\data\IAEL053.rawResult File : c.:: \270O\data\lAEL058 . rstInstrufiient F"J.JD: c: \2700\data\llael .insP r o c e s s File : c : \ 2 7 0 0 \ d a t a \ 11. a & 1 . p r cSample File : c:\2700\ciata\llae.L.Bmp3« o u e n c e P' .1 1 e : r..: \ 2 7 O 0 \ d a t a \ 113 e ] . s t? q

Sample Amount

^•\ o i s e T h r e s h o 1 c-Multiplier

2 IMG/ML.5.2900

o

1.OOOO

A r e a R t? j e c tD11 u. 11 o n F a c t o r

A i" e? s 1 i i r e s h LJ 1 d 'Divisor : 1.0000

31.', i" i c h F a c t. o r : 1.Adder : 0., OOOO

Instrument ConditionsPacked Column GC -

Instruri ientCo1umnColumn LengthCarrier GasFlow RateTemperatureInjection T e m pDetector 1Detector tempNotes

KS1111. 5V.SP-2250/I . 95/'.SP-24016'x 2mm on 100/120 SUPELCOPORTAR/ME 95/55 5 m .1 / m i. n2OS250 CBCD350 C

i 5.1 N u m b e r of F:I e a k s D e t e c t e d : 1 D

PRIMARY ANALYSIS

Fi .'-! {-• r-f-IU/C. .

Peak Rft lite Peat Ht A rea Cuitporiefit

5 [ftifi] [uV] iL 'V ' Js fC ] Nafi

i 2.200 137 24:>,'•s " / i •! E •-. T • " • " . * . _ . ? 1 r .' 1 «.^ i .01.' ji C7C nr Li~ii**i i

3 3.471 95 126?4.203 7S 14EE3 Arc i -1242 3

^_^- 5.222 747 1^3i2 Arc i -124S 1

INC. PCS REPORT

BL Es t rsc t Cone. Essple Csr;:.ns/sl *o /kD

s3 i'.m O.;o7

iS 3.909 0.0-4

;••'; 5 . 407 0.102vv 2i.359 C . 4 9 S

VV 39.310 0 . 7 4 3

• , _ •;*».>

; e .572 552 13347

= 7.731 1S32 71970 ;r:;-1245 2

I;. 9.005 1156 67775 Arc ! - l I45 3

, 11 11.054 453 29227

12 11.325 450 20205 A rc i 1254-2

••, 13 13.453 415 "0520 Arc i -1254 3

-'' 14 17.049 140 5545 Arc i -1260 2

15 33.471 4901 4729S5 DEC

12603 755301

Group Report Far : AR1242

Peak Ret Tine Peak Ht Area CoBDunent

ft [sin] liiVJ [uVlse:] tiaae

1 2.617 52 393 Arcl-1242 1

2 3.311 0 0 Arc l -1242 2

3 4.203 754 145S3 A rc l -1242 3

S06 15281

Group Report For : AR124S

Peak Ret Tiie Peak Ht Area Couponed*.

« [sin] [uVJ [uVfse;] Nace

1 4 5.222 747 19362 Arcl-1248 1

-*"• 7.731 1882 71970 Arcl-1248 2

9.005 1156 67775 Arci-1248 3

3785 159107

Group Report For :: AR 1254

"-'eat Ret Ti«e Peak Ht Area Coiiporiertt

S^^sifi] [ii'.J] i i iVJsSC] Nass

a S.801 0 0 Arc ! 1254-1

3 11.S25 450 20205 Arc l 1254-2

9 13.453 415 20220 Arcl-1254 3

364 41025

roLiD Report For ; Ar\i2t>O

ik Ret Tins Peak Ht Area Coepor.ert

[sin] [uV] [uVJss:] !<aae

15.160 0 0 Arcl-1260 1

17.049 140 5545 Arc l -1260 2

S9.400 0 0 Ar;l-1260 3

.1.0/6

22.120

VV 26. 443VV 9S.7I6

VV ?9.36t

VV 30 .249

3C.059

VB 26.012

BB 15.854

9E 72 .775

cnc T-M.'.J. j/0

BL E x t r a c t Cone.

nc/*L

BB 3.909

VV 0.000

cV 26.359

3..M

SL Extract Cone.

na/il

VV 39.310

VV 93.726

VV 99,366

237.402

SL E x t r a c t Con:.

no. 'EL

VV 0.000

VV 30.059

V5 26.012

56.071

BL Extract Cone.

ng/eL

VV 0.000

28 15.S54

VV 0.000

0.177

0.41B

0.500

l.oas

l.c.75

0 .572

0.568

0.492

0.300

1.376

9.932

Saaple Cone.

iig/ko

0.074

0.000

0.498

0.572

Sa&ple Coric.

f ig , -kg

0.7«

/^Sii ~^ ^ -^ 1 . ^yv-W'

4.438

Saaoie Core.

E O / / Q

0.000

0.563

0.492

l.OcO

Saaoie Cone.

ng/kc

0.000

0.300

0.000

dr Di1 :.:< -v'r.' i jc.'t" t For : :•->( "- F-'. 'm 1 ' r

v Pe«l, ret TIM reat. Ht nrta Coiconerit BL E.-:tr«:t [or.:. Saitle Cor.c.

[ i jV] [uV lsec ] Na*e r,a/*L j .g/tg

•- 13 33.471 4901 472935 DEC &6 72.775 1.376

4901 47:985 72.775 i.37i

PAGE, INC. PCB FiEPORT PAGE I Jo. 2

tart THE : 0.00 tinciie Factor: -1

Er,d lite : 6'. 00Plot Offset: 2'. tV

Salt if »:

Gite : 5 /27/5" 0£:02Lo* Ftmt : 24 .72 iVF'lct Sca le : 30 tV

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PACE



DATE COLLECTED:

DATE RECEIVED:

MATRIX:

DATE EXTRACTED/BY:

INITIAL VOL:

FINAL VOL:

05/11/92 CLIENT 1

05/12/92 PROJECT

SOIL DATA RE1

/ A//:/\V W&Vv ENTERED/ '

.5~'5/?, /$T SAMPLE 1

?f?.6'Vw£-- SAMPLE 1

ANALYZED BY: M(.(Q'l —

* PARAMETER NAME

Aroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242

•' Aroclor 1248Aroclor 1254

ABBREV.



Tetra Tech Inc.

1.01.0


UNITS: mg/kg

MDLOIL: t:^ OIL:INST:/c<v/// INST:

FINALRESULTS

v



•;;. ;. 1 ; . • • ! ; . ; ' ' . ' ;• ' ! '

' • "> ,O ; ' . 1 1 . 1 1 .

- r"

' • i ' - i ' i - 1 : ' - , .•'. • •" ••• •'•! . • " ! ' . • • :j

i.:-- r

.. .X '.;!'::!':

' -J i i":' ! :

PRIMARY ANALYSIS

•.::',A '.''.'.il?

'It.' K'f| '(H ! f i.'f ; A r\.1 .',:•!.',.'

Kpl l i»e (•'*!

[ f f i n ] [ :.

2.6123.3114.22?

it Ht i

jVJ [tf

0f;

0

!irsf LoupC'rent

/ t ree] Nine

0 A r : l - l 2 < 2 i

0 Mrc!-12<' / 20 ftrcl-1242 3

i'-i

VVV'VV V

= 1; t r a c t U.fU.

ng/nl

0.000

0.000

0.000

Sa*;.'le Coiit .e g / k g

0.000ii . 000O.OvO

. . • • - • • • • . • • . • . r - l . • • • • - . . • ; :''ii'-:.l , ' : f ! i

Afi '.2S

[ r M f ] [ u V j [ u V J i e - : : ]

i-ci/ftL

a EI r. ) p f '" i^-rCl » ^.- i C wJ-i l . t

5.430

c.400i.SOOi>/5M

V

0

00

o

0 Ar;l-i2<5 i0 ^rc]-124S 20 Arc 1" 1248 30 Arci -1248 4

0

VVId 1t >

VVv'V

O.'JGO0.0000.0000.000

0.000

0.0000.0000.0000.000

O.OGO

« • - •: * r -, r f f" r, r - C i » r, J p f* ,-t r, -i-w *. .'» k ' Dk. I ut-'i. h * wCft p J C L-k,. i k •

• • • X . M . - r - r i . ( • : • • • t t ' . ' r- . . ' i >': .( . '

itr f-'?er. HI i ' f r C: rL £ > , t r r C i CoriC. :a»p]E ^0: C .

J i tp i f I: 1 of 1

CNCSJ

m in

•V-00

r-c

OCMI

riOJ

•»'mI

/.. -,/-..

\\

:s~r

1 1 1<TsCNCN".JTJ ^

CXTSIC^J

1 1 1t i i

OOOmv ce« <

i iiCOCO

OJCM

1 1| 1 i I

ooctcc

! 1Cf)_ ."•T ^T

1i. i

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'iCj O-J ^^ C^' CN ^^

1 *~I f

OOera:«

! ! ! ! ! 1 i 1 1

*— ioo:<.

1_j -

1 1 1_J 1 _J

O O O Oa: a: a tt< -

1 1 1 13 < toVO&•4k.



'-DATE COLLECTED:

DATE RECEIVED:

MATRIX:

DATE EXTRACTED/BY:

INITIAL VOL: Ajf

FINAL VOL:

ANALYZED BY:

PARAMETER NAME

Aroclor 1016Aroclor 1221Aroclor 1232Aroclor 1242troclor 1248Aroclor 1254


05/11/92

05/12/92

SOIL

CLIENT

PROJECT

DATA RE'

ENTERED

&ZO*f. SAMPLE 1

c20™A SAMPLE 1

r y#

ABBREV.


Tetra Tech Inc.

HB6 - 0.5

60 0062994

UNITS: mg/kg


MDL

1.01.01.01.01.01.0

OIL: /: JT DIL:I NST :/£J/// INST:

A/7)

FINALRESULTS

V?)

///

PCB1260 S 1.0DBCSURR -7/7*7



< i r i ;• i •:

f- i'\i;-inic." HI*--Ltd

I ni.it :~ unit/I. t.) Au too amp 1 er

i iwiC. i- / Via i

nh.-.nr ic- 1 A/D rr/v R^nae : 1OOO

I-' til AS 830'!'i..)/ '...•

Interface Serial tt : 1248^74035 Data Acquisition Time: 5/24/92 1.2:17De 1 ay T i me : 0 . OO m i n .End Time : 65.0O niin.Sampling .Rate : l.OOOO pts/sec

Raw Data File- : c:\2700\dsta\lAEL059.rawRe=SLtltFile : c:\27 0 0 \ data \ 1 A El I... 0 5 9 . r 5 1Instrument F.ile: c:\2700\data\llael.in5F-'rocess File : c : \27OO\dat.a \llael . prc3 a m p J e F 1 1 e : c : \ :! / (..) •'.) \ d a t. it. \ 1 1 a & i . s n > pSequence Fils i c : \2700\data\ 1 lae 1 . sirq

: 2 NG/riL.1. ri.i . vo j. LI Hie3 a m p 1 e A m o u n t

Noise Threshold: 6Multiplier : 1.0000

Area RejectD11 u 11. o n F a c t o r

A r e a T h r e ~. h o 1 d :Divisor : l.OOOO

Bunch FactorAdder : 0.0000


I n s t rumen t : K.S 111Column :1.5XSP-225Q/1.95:'.SP-24C1

'* Column Length :6'x 2rr\rri on 100/120 SLJPELCQF'GRTCarrier Gas :AR/ME 95/5Flow Rate : D5 ml/minTemperature : 203I n j e c t i on T em p . : 2 50 CDetector 1 :ECDDetector temp :35O CNotes s

.Total Nuuiber of Peaks Detected

PRIMARY ANALYSIS

PACE. INC. PCS REPORT

Peak ?,e: ";te Peak Ht Area Cuasonerit EL Ex t r ac t Cone.

1 2.201 295 iOsi Ev 22.263

/ 5 .4iS 173 4993 SB 12.354

Seicpie [one.so/kg

0.-2S

0 • i i /

0.14S.-•i •- •• nv . ^ v O

"••' "X3

) u' r o i .1 p Fs e p •'.'.• r t i:r o r : M R 1 ' -'i ,.'v,

Peat Ret Tine Peak Ht Area Component1 [tin] [uV] [uVlsec] Nai,e

1 2.623 101 1042 Arc l -1242 12 3.311 C 0 fircl-1242 2

3 4.250 0 0 Arcl-1242 3

101 1042

Group Report For : AR124£j

Peat Ret Tine Peak Ht Area CoffiDorient* [tin] [uV] [uV tsec ] iiane

4 5.290 0 0 Are l -1243 15 7.760 0 0 Arel-1243 2

* 7 9.080 0 0 Arcl-1243 3

0 0

Grouo Report For : AR 1254

1\ Peak Ret Ties Peak Ht Area Coeponentj \ [ein] [uV] [uVtsec] Nai,e

6 S.301 0 0 ftrcl 1254-18 11.913 0 0 Arcl 1254-25 13.500 0 0 Ar:l-1254 3

0 0

*broLio Repoi't For : AR1^6O

Peak ?.=t Tiiis Peak Ht Area Coaponent« [iifij [uV] [uVtse:] Na«e

10 15.160 0 0 Arcl-1260 1il 17.200 0 0 Arcl-1260 212 19.400 0 0 Arci-1260 3

0 0

3roup Report For : SURROGATE

vr:ecl Ret Tlfie Peak Ht ri'sS CoCpuHent

.1 * [ai.'i] [iiV] [ u V l s S C ] Ndifre

129.614


ng/iiL

FE 7 .632

VV 0.000

VV 0.000

7.632


ng/ftL

VV 0.000

VV 0.000

VV 0.000

0.000

6L Ex t rac t Cone.

ng/iL

VV 0.000

W 0.000

VV 0.000

0.000

£L Extract Cone.

ng/sL

VV 0.000

VV 0.000

VV 0.000

0.000

BL Ex t rac t Cone.

ng/eL

* t V- T V

2 .493

Saiple Cor;c.

oig/i.g

C.I 47

0.000

0.000

0.147

3*»p!& Core.

a Q / t c

0.000

0.000

0.000

0.000

oaipic LCTiC.

eg/kg

0.0000.0000.000

0.000

Saaple Cor.c.tQ/kg

0.0000.000O.COO

0.000

Sarpie Cone.isg/kg

1.340

PALE, JNC. F-'Cfc REPORT PAGE No...-<r\

• r

Siiple Sire : eOOC'i2:iFsieKm : cSlTOO'v3tirt "iSr : O.C-O t:rS:«!e Factor: -1 Plot Offset: IS iV

pie I:Cite : 5 / 2 7 / 9 2 08:05Lot< roif i t : K.S2 iVF l o t S c a l e : 30 *V

Fioe 1 GT 1

Hiah Point : 5J.82

•s en. . . } c

• O- Q.

o;

Qf^> Ki. fx

so-

II 1 1 1

li

45-JI

—i

n

lit h

20

-i i l I i II ill I i

rvj CMS} aoU- J. ^r O O Q

rr

I i i I i i i i

O CXJ CO O C: O <--• O

~~ î' <-=r. < <. ^ <! <;T" T"

10

OCD

i ' i i i i

me40

PRIMARY

The primary analysis is the initial calibration and continuing calibration standardsdemonstrated under a set of predetermined Gas Chromatograph conditions.

l»eiC

********** SUMMARY REPORT *********

1

File Nate

Iael014.!af4018.la<4024.Iaf4025.

AveracesIRSD

File Naee

Iael014.Iaf4018.idf4024.Iaf4025.

Averages2RSD

File Nate

Iael014.Iaf4018.Iaf4024.laf4C25.

Averaoss:F,SD

File IJ.ee

Iaf4018.Iaf4024.Iaf4025.

AveracesIRS3

::;ni-JT ]NL:J.NL-; ;::;

Sample Nase

AR1242-050692SPLAR1242-050692AR1242-050692AR1242-050692SPL

Saipie Mane

AR1242-050692SPLAR1242-050692AR1242-050692AR1242-0506923PL

Sasole riai*

AR1242-0506923PLAR1242-C50692AR1242-050692AR1242-050692SPL

Saeple Kaee

AR1242-050692AR1242-05069.2AR1242-050692SPL

A, :,F<

Date OfInjection

5/21/926/5/926/5/926/5/92

Date OfInjection

5/21/926/5/926/5/926/5/92

Dats Ofinjection

5/21/926/5/92i/5/926/5/92

Date OfInjection

3;.:l/9j6/5/92i/5/926/5/92

.! [.•! .i '. !.

Tue OfInjection

19:3110:1414:5315:39

Tiae OfInjection

19:3110:1414:5315:39

TIKB OfInjection

19:3110:14« * i C f

15:39

Tine OfInjection

19:ol10:1414:5315:39

> J F" F Ei: FA

Ret.Tite

2.622.622.622.63

2.620.14

Ret.Tue

3.323.323.333.33

3.320.19

Ret.TlfiB

4.244.264.264.27

4.260.25

Ret.Tue

oo. ; J

34.2234.2734.27

34.130.74

•LNCL -

Height

3227297529442904

30124.34

Heioht

4263431242364195

42511.15

Heioht

6396642064496357

65313.72

Height

O-Si

6750s350i860

71757.70

F ,,. HOC,,,',

Arcl-1242 1uij/L Reference

Satple Att Ratio

243.6247 1.0000271.8465 1.1158268.9624 1.1040265.2929 1.0309

262.4316 1.07724.89 4.89

Arcl-1242 2UQ/'L Reference

Saiiple fist Ratio

243.6678 l.COOO283.6025 1.163927S.6450 1.1435275.9379 1.1324

270.4633 1.11006.71 6.71

Arcl-1242 3uo/L Reference

Saeple Act Ratio

241.1106 1.0000239.6196 0.9938240.6847 0.9982237.2561 0.9840

239.667S 0.99400.72 0.72

Decuo/L Reference

Sasple Ait Ratio

lJ2.o444 1.0000140.6740 1.1498142.7713 1.1670142.9737 1.1636

137.1903 1.12'47.25 7.25

- F- I RS

ACT I DIFFRESPONSE

0.00-11.58-10.40-8.89

-7.72-63.18

ACT I DIFFRESPONSE

0.00-16.39-14.35-13.24

-11.00-67.71

ACT I DIFFRESPONSE

0.000.620.18l.eO

0.60119.60

ACT Z DIFFRESPONSE

0 . 00-14.98-16.70-16. Si

-12.14-67.03

1 ROW GAL 1 BRAT 1OI

REL I DIFFRESPONSE

0.0000-10.9499-9.8862-8.5154

-7.3379-6B.04

REL A DIFFRESPONSE „

0.0000-15.1477-13.3932-12.4210

-10.2405-67.57

REL I DIFFRESPONSE

0.00000.62030.17681.6115 **

0.6022119. E5

REL I DIFFRESPONSE

0 . OOOU-13.9379-15.4098-15.5507

-11.2246-ii.73

tc : '.'' ' 1'7

L c'« 1 i.5it.-r>

(:,'„.» ve ti

Calibration

Level

Nate

123

'. ' —

.'J.. 1 fi CÎ ; P J r

U,?:,

Curve = 158.

Observed

X-Value

2:.. oooooo100.000000

250.000000

. . j . ^ t . . u j1 J r"'~ • • ' " * • "

i j C. t 1 ! <fl t i..'!.i

• o t t.; r c; t- r h-. q 1 : 1. .1 n o F c- 1

134358 )X

Calculated

It-Value

31.663020

107.733192

246.239929

i *t

..;U,.;C. ^,;r ,.,

r.i ;. riofriiijj F ::I...!' ~ .1. .O

Delta JDiff.

-6.668020 -26.672

-7.733192 -7.733

3.760071 1.504

r h 'f i t :t -- For cod 1' r-Jo Wo. ~i.fj l'it in

Obierved

V- Value

1841.000000

6263.000000

14315.000000

' • ' - ' • '

hro-..igh t hog ) ,.-.-•: r::

Calculated

v-Value

1453.353837

5813.435547

14533.569844

i..ir :. Q:.:-I: . :."., ..! '../Qf j

Delta

337.641113

449.564453

-213.5E9344

ZDi f f .

21.0

7.1'

-1.5:

:«= : r- - • - -'- - ' - • • •

.- - .•:-...1.6-' C r s. :

Arcl-1016

jr.-

.AltJOUTll

;.'.-*«.-: . . . . . • - . ' I - me.-: i-i : /

I'.-.i:.r- i lir.tB W i t h C# 1 tit.'1 c-i 1 r-c.i 'v'ci 1 i.p-ir, For t.ac.h !"it.:'.'..-.' ve 111 : r i rs i - t OrtJ&r r'ol vTioriiJ j 1 i .1 t - r' orct-cl Ihrouqh t fir.- Or iq.i.n

i^lr-iciht. i riC] I' ,-i r. t r.i r --•• i . i * (No Ue:i qht.inq ) r' •-- '..'. "S''-:'^"'^

Cal ibrat ion Curve - (42.730598));LevelNaie

ii3

Observe!!It-Value

25.000000100.000000250.000000

CalculatedIt -Value

26.20530196.038223251.464188

Delta

-1.2053013.961777-1.464138

ZDiff.

-4.8213.962-0.586

ObservedY-Vilue

1277.0000004680.00000012254.000000

CalculatedY- Value

12*8.2650154873.06005912182.649414

Delta

58.734985-193.06005971.350586

ZDiff.

4.601-4.12:0.53:

Arci-1232

.Amount

Ci. r ve> 41

CalibrationLevelKane

127•J

1 : f- .\ r=',t i.Jr dor i1-Je.i otil. i ng F-'^c

Curve = (59. 365310 )HObserved Calculated

X-Value K-Value

25.000000 27.91:633100.000000 118.452019250.000000 242.323033

'<"..; j •/ 1 i ijfii ."i.

Ll.t,,- -

Delta

-2. 9. '1688

-18.452019

7.671967

M i I' J

i . 1.1

Miff.

-11.447

-18.452

3.069

t. - !~circ.t:-d 1

i l.io l\!& i q h t. j re

OtiervedV-Va lue

1657.0000007032.000000

14386.000000

hrouqh Ititv-q ) i ":' -•

CalculatedY-Value

14S4. 1452645936.581055

14841.452148

O r i. g a. r i

i.'.98:>IO.l.

Delta

172.8547361095.418945-455.452148

ZDif f .

10.43215.573-3.166

— -• ' f .

Ci'iilfif.crt Cur.e = •.S'.r-t'Sl-.-i!

Arcl-1242

-"EII

- 30W

AfflOlBtt

I.;. L i<->1.-.:> W i th C«lculitttr'.:J V^Jut - iH, f -or [-.<=. c h Fi t :!_. •'r vY.- 1! J. : F: i r <;:, 1 i.;r ;:!i-/i !•'O I , i ic.jnu ;:<.! r .1 t - Forc.e-c.l I ! HO'.M:.I i. t.t.i;;- Ui .1 Q i r>

t-JiV-i u! it v riu Fac tor - 1.0 i !JD W«?i.qht J fiu i i""' ••••• •). S-92o-l J

Ca!i6ration Curve - i j4.1j9317)>Level Observed Calculated Observed CalculatedNate K-Value X-Va lue Del ta ISiff. V-Va lue V -Va lue Leila iDiff.

1 2:i.OOOOOO 25.386589 -0.8365E/ -3.546 1402.000000 1353.982910 ifi. 017090 3.422 IOC.000000 36.79946? 13.200531 13.201 47C1.300000 5415.931641 -714.931641 -15.2053 250.000000 255.191544 -5.191544 -2.077 13821.000000 13539.829102 231.170898 2.034

J

:35

?5I-

VT*M

Arcl-1248?t :

tt

!i1

I!

1i

•.---I

/ ";

'

fl it-:

a 1. i it a W i t h C* 1 <::u I at<:-ii v'-sl '..'»:-r: f-or E-.ach Fit:Curve 111 : Fa. r? , J c Drdor ! o J :. noil, .1 s j Fjt - forced Ihrouqh the

Wt;irjht i no r .099GOTi

Calibrition Curve = («.148377iXLevel Observed CalcuiattdNa*e I-Vaiue It-Value

Observed CalculatedDelta IDiff. V-Vaiue i-Value Delta XDiff.

2J. 000000 24.519154 0.480846 1.923100.000000 102.06346? -2.063469 -2.064250.000000 249.222687 0.777313 0.311

1107.000000 1128.7094734608.000000 4514.83789111252.000000 11237.093750

-21.709473 -1.96193.162109 2.022-35.093750 -0.312

Arcl-1254

n

HSCO

.Amount

.-.. : "L: >.„..••'.>'.:.) \ DA 1 M '-. i -iRi 1'cs',1. SMf-"1

• i .- • . • • • • . : <! .1. : r ' a r s t. Or tfrr P:;-. j v i iOiT.:; * 1 Fit. ••• !:: or reci l inc/unh t Lf

W e i g h t i n g rec tor ::: .1 . * > i No l-Je .1 ghl iriCj ) r- •'•

Cihbration Curve = ( 4 4 . 2 4 6 4 9 4 ) K

['!: i o .11,

LevelKaf;E-

tAn

3

ObservedX-Value

25.000000100.000000250.000000

CalculatedH-Vilue

20.09199896.635623251.816559

Delta

4.908012f ? 1 / •••?•?J. Ji*IJ/ /

-1.816559

-.Diff.

19.6323.314-0.727

OsservedY-Value

889.0000004278.00000011142.000000

CalculatedY-Value

1106.1623544424.64941411061.624023

Delta

« • 7 • r i?c Ai.L I • lOi *)*"!

-146.64941430.375977

ZDiff.

n *1^"it.fiC

-3.42E0.721

*t:3*t:&c-if»p> -n-*

Ard-1260

•n

.L

m

i'v

Amount

fe o 11 w a r *.-• V f •- r & i o r.: 7-. _.' . o F.. • • iAh 1 O 1 to — 1-.11 1>J '•? ...'.'.--if 'i...

Se«iTipl*? Number

Goc-r a tor

Inst.r umeritAutoSamplerRack/Vial

£: MA

KS111PE AS83OG0/0

T i nit'Study

C ha

PCB ANALYSIS

A/D 1OOO

Interface Serial # : 1240574035 Data Acquisition Time: 5/21/92 10:43Delay TimeEnd TimeSampling Rate

Raw Data FileResult FileInstrument FileProcess FileSample FileS e q u e n c e F' i 1 e

I to . Volume,6'ample Amount

Noise ThresholdMultiplier

O.OC -nin.45.OO min.1.0000 pts/sec

\2700\clata\lAEL003.raw\27OO\data\1AE L 003 . r s t\ 2 7 O O \ d a t a \ 11 a e 1 . i n s\270O\data\llael.prc\27 OO\data\ARl016.smp\27OO\data\llael.seq

2 N6/ML1.0000

Area Reject : 0.OODilution Factor : 1.00

1.0000Area Threshold :Divisor : 1.0000

Bunch Factor: 1Adder : 0.0000

j


InstrumentColumnColumn LengthCarrier GasFlow RateTemperatureInjection Temp.Detector 1Detector tempNotes

KSlli1. 57.SP-2250/1. 957.SP-24016'x 2mm on 100/120 SUPELCOPGR"AR/ME 95/555 ml/min208

ECD35O C

Total Number of Peaks Detected: 14

PRIMARY ANALYSIS

PACE, INC

Peak

t

12

j 3s ^

5

Ret T:»e

[fiin]

2.1S32.3192.609

3.3003.607

Peak Kt

[uV]

333255530755369

Area Cosponent

[uVlsec] Naiie

2537

2iS«>

6641 Arc!-!016 1

3086 Arcl-1016 2

6003

BL

BVVVVBBVVV

. PCB REPORT

Extract Cone.

ntj/iL

20.158

Lt>.992

34.607

3A.52316.839

Sasple Con:.

UQ/100Ci2

20.158

14.992

34.607

34.523

16.38?

7 4.kT Kfc 7343 Arc;-ic:« 3£ j.^;< 3i; 3'ui 5.142 «45 9e55

o *.;;: 3tf 5i/s; i.!-1* ie4 'O3r: ::.cio 34 HIT3 30.473 57 2937

14 33.604 3543 336174 OK

TO65 416284

Group Reoort For : AR1O1S

ttti Bet TIM real HI Area Cotsoner.t.1 :»nj tiVj [tii'tse:] *«ite

• l.tifi 536 6641 Arcl-lOIe 1: 3.3W 755 SOob Ar:I-10it 2

r S'V* l"""i T343 i"'-'-1"-;- 3

;i<; ::o,;

Grouo Report For : SURROGATE

ffil Mt TIK Peat Kt Area Cotoc^Mt» fi:a} [sVJ [u VI sec] Sat*

4 33.604 3X3 336174 CiC

3503 336174

>"V 3C.07?17.532

vB :6.«4:&V 17.EU

Vfc 15.B?4

B» 0.151

F& 0.932

SB 57.019

36B.516

ii Eitrjct Cor.c.

nc/*L

ri. 34.»07V.' 34.523',",' "0 f,*9

?9.no

?- Extr jct Cwc.TiC/ki.

EB 57.01?

57.019

30.079

P.':;Zi.44117.616:5.i?4

0.551

0.932

57.019

3*6.516

Saeple Cor,c.

«•!»:•:

34.607

34.523-ft C7C

"•:»

Eatsle Cone.

ua/100:§2

57.019

57.019

PACE, INC. PCB REPORT PAGE No. 2

•"-t- '-.

e : c:\2700\dita\IAEt003.ra*Stirt THE : 0.00 mn End Iji.e : <5.00 tinScale Factor: -1 Plot O f f s e t : 26 *V

t: 2'bDate : 5/26/92 12:15Lo* Point : 27.59 iVriot Scale: 30 §V

Face 1 of :

Hioh Point : 57.59 tV

55 _

soI

40—

CM f"!^"*- COII I I I III II

-iI

CO

CO <JrrW (V

1—r -i—ri ' i—i—i—;—i—i—i—i—r

oCD

0i i i

10i i

Time [min]

icH^rt- V£-r&

'. . f f l i ^ ' . t- I.««."n<r

S-r-^r-lC- rJc-f.f-.eri i:.-(•• .:.'.or

• i rij.tr ufiiC-nt

a c ^ / V i a l

Stud .: :-/^<S- ^1' IT: IV: f-'CB AfJ^LVSIS

-MA

h £.1 1 1PE ASS7-O-'.-O/O

Interface Serial « : 124S574Or-5 Dc'-ta Acquisition Time: 5/21/92 11:35Delay Time : O.OO mm.End Time : 5.00 .T,ar, .Sampling Rate : l.OOOO pts/sec

Ffaw Data FileP:esuit File

: c : '•.270O\data\lAEL'X"1 . raw: c: \Z7-:-y.;j5.ta\ l£ELOO-t . rst

-.-jiit-ri t F i le - : c : vZ?!."""1 '-.data \ 1 lael . insProcess P i. I •=• : c : \T 7 1 / - .• -.as t f i ' . i iae 1 . p^cS^niDae Fi le- : c : 1\27'I"!'\de' ta \Ar i lOl S. B M I DS s-caence F L « e : c : \27-i1-.1 • c :% ta '• i 1 .--.e i . seq

Jr,j. Volume 2 NG/ML Area RejectDilution Factor

)Joise Threshold: 5Multiplier : 1.0000

Instrument Conditions:Packed Column GC —

InstrumentColumnColumn LengthCarrier GasFlow RateTemperatureInjection Temp.Detector 1Detector temo

Area Threshold :Divisor : l.OOOO

Bunch Factor: 1Adder : O.OOOO

KS1111.57.SP-2250/1.957.SF— 24016'x 2mm on 100/12O SUPELCOFCRTAR/ME 95/55 5 m 1 / m i n2 OS25O CECD7-50 C

~cte : I ;jt':T:a.er of Pear s de tec ted: IT-

PR I MARY ANALYSIS

rfil r|

t ;

:r

r

t:5j :«Vj [a

c.2-4 ;o.150 Ut

.ftv5 1E7C

.JM :«


;rti loiscrer.'. cL Extr«:t Cine. Sitcle Cor.c..-l«cj i«* r-a/H My!Wci2

TIT i; i ;:; i "toi> A «. » * « * A v 7 *•*•?

:•:« cV 2i.7i5 c.795

:!il £V -l.i;7 1.107

ôw* 1317S 4.223 436C? 4.B10 17E610 4.924 1196

. 11 5.252 1669' 12 6.186 1221\ 13 6.603 958? 14 7.296 132

15 33.652 6736

25093

. _I'3b316095927466 Arcl-1016 3162044212325089191771856

649010 DBC

927779

• V

vvvvvvvvvvvvVB66BB

119.257o0.246259.079106. i:571.20899.17072.5385c.9477.812

109.637

1144.144

119.257bO.246259.079106.12571.20899.17072.53856.9477,812

109.637

1144.144


Peak Ret lite Peak Htt [•in] [uV]

1 2.605 18702 3.300 26073 4.610 1786

6263

Mil*

Area ConponentiuVJsec) . Kane

20188 Arcl-1016 130894 Arcl-1016 227466 Arcl-1016 3

78548

BL

BEEVVV

[strict Cone.no/*L

111.533119.257106.125

336.914

Saople Cone.uo/100c»2

111.533119.257106.125

336.914

wGroup Report For : SURROGATE

Peak Ret Tiie Peak Htt [«n] [uV]

1 4 33.652 6736

-.J 4736

Area Coaponent[uVlsec] Na«

649010 DBC

649010

BL

BB

Extract Cone.ng/DL

109.637

109.637

Saiple Cone.ug/100c»2

109.637

109.637

PACE, PCB REPORT PAGE No. 2

Si.if -i:*.ir: -1EaC TJI« : «J.t;. i;r,Fict C f f w t : 13 tt

ii»ple I: 'OCt'i't • •./"<•,•?'' • ' • '?•r • i C • »''»«' i -. • • • • •

Lc. roir.t : 22.GO »V

?:c t Scile: 33 »V

Cr 1 C c f t« ei r t- v e r s J o PI :Scimp j e- Mr'me.-Sample NumberC) tit1 rat. or

" Instrument• 'AutoSamplerRack/Vial

AR101 ci- '..»!. 1 o'-rSF'250t)EMA

KS1.11PE ASS3000 / 0

"i 3 n.o?Study

C ha nri el

5/2t , /92 12:19PC& ANALV 3 IS

A/D iTi'v 1OOO

Interface Serial tt 1243374035 Data Acquisition Time: 5/21/92 1.2:32Delay TimeEnd TimeSampling Rate

Raw Data File-Result FileInstrument FileProcess FileSample FileSequence File

Inj . Volurnef S a m | j 1 e A m o u n t


0.00 min.45.00 min.l.OOOO pts/sec

c \ 2 7 0 0 \ d a t a \ 1A E L. 0 0 5 . r a wc \2700\data\lAEI_005. rstc \ 27OO\d a ta\llael.in5c \ 2 7 0 O \ d a t. a \ 11 a e 1 . p r cc. \ 2 7 0 0 v- d a t. a \ A R101 o . 5 m pc \ 2.7 0 0 \ d a t. a \ 11 a e 1 . s, e q

2 IMG/ML1.0000

1.OOOO

Area Reject : 0.00Dilution Factor : 1.00

Area ThresholdDivisor : l.OOOO



Instrument' Column

Column LengthCarrier GasFlow RateTemperatureInjection Temp.Detector 1Detector tempNotes

KS1111 . 57.SP-225Q/ 1 . 957.SP-24016'x 2mm on 100/120 SUPELCOPORTAR/ME 95/555 ml / m i n208250 CECD350 C


PRIMARY ANALYSIS

PACE. INC. PC3 REPORT

Peak Ret Tise* [tin]

1 2.1702 2.3293 2.6144 3.0585 3.309

Peak HttuV]

63S90942294515929

Area[uVlsec]

51t9744243544436463120

ComponentNate

Arcl-1016 1

Arc!-1016 2

3L

SVVVVEEVVV

Extract Cone.ng/fiL

33.03654.167252.25520.647271.267

Sasple Cane.UO/lOOcBi

33.03654.137252.25520.647

271. 2S7

.«»« -•••.••i

. .^ c »216;.J/»

172.'Bi:3'...u£ID.064

0.662

236.645170.732

90C Bil 0.662 0.6*215 :3.5£S ?> "at. ti V!.t?6 0.47t16 30.2:2 45 4113 VB 1.C63 1.C63J7 .472 4737 6475-; 3tC fcB 10S.653 30..4KIS 39.532 30 1212 26 C.472 0.4S2

4J475 1234108 2456.101 2454.101

3r DO p êr&O'" t r C'^ * f-ir' i '.l 1 O

?t*i net a«€ re«i ni Area Co4&ooef>t t-L Eitrict Cone. 5i§ole Cone.

• * , . • f-î f * C f * f , . ' * r - i ! * * • -» t * *»e t ^ e T i n c ej »*cH **» * Yj.'înri.i'ivlOi Ci •.j^.^Jk* »J. ... J

I I.r«r? JT!? callO lircl ~1 i6 •. * * ^7l. 26? «.i.«6?3 4.i21 4!57 t3a75 Arc i - iOls 3 W 247.014 247.014

14315 I75J31! 770.S36 77C.5v4


'*al tot TIM Pea rtt Area C«*c<>H«t 31 Extract Cone. Sawie Cone.Km ng/ti uj

SS 109.453

PACE. IliC. PCE REPORT PAGE SJo. 2

;teft ':tt : O.OC ur.Scale Factor: -1

End 7me : <5.00 urPlot O f fse t : 29 i;V

sitple I: 2MbCite : 5/24M2 12:20Lo« Foir.t : 29.2c ivFSot Scale: 30 nV

cf

High Point : 59.26 »V

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£ Ii — i0> 45 —

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J nsit rum*?n t>i*''A u t o 3 a ff i p 1 e r

Rack/Via l

;• o'r'...i::-oi3t •-.••:

Ur.'nEM A

KB.1.1 1PE AS33OO0 / 0

TimeStu.dy

Channel

: 5/26/92: PCD ANA

A/D riiV 1 OoO

Interface Serial tt : 1248574035 Data Acquisition Time: 5/21/92 14:05Delay TimeEnd TimeSampling Rate

Raw Data FileResult FileInstrument FileProcess FileSample FileSequence File

inj. VolumeSample Amount


0.00 man.45.00 rnin.l.OOOO pts/sec

\27OO\data\lAEL007.raw\27OO\data\lAEL007.rst\27OO\cât^^\ 1 lae 1 . ins\ 2.7 O 0 \ dataMlael . p r c.\27OO\data\AR122i.smp\2700\data\llael.seq

2 NG/ML1. (jOOO

1.0000

Area Reject : 0.00D i1u t ion Fa c to r : 1.00

Area Threshold :Divisor : 1.0000

£ LI n c h F a c t a r : 1Adder : 0.0000


Instrument :KS111, Column : 1. 57.SP-2250/1. 957.SP-24Q1- Column Length :6'x 2mm on 100/120 SUPELCQPQRT

Carrier Gas :AR/ME 95/5Flow Rate :55 ml/minTempered ture :208Injection Temp.:250 CDetector 1 :ECDDetector temp :350 CNotes :


PRIMARY ANALYSIS

PACE, INC,

rei

1

12345

i Ret Tics[tin]

1.9212.1752.3302.6193.325

Peak Ht[uV]

1204841065222t234

Area CoBponent[uVJsecj Kaae

oil4121S2iO256483706

BL

SVVVVVVVVB

. PCB REPORT

Extract Cone.ng/sL

10.81043.58295.35993.2009.527

Saiple Cone.UQ/!OOca2

10.81043.58295.35993.2009.527

«.:«*

14.813{•1

•s«

• jj

;.E;? :a :6i>:?.3i? 7 ICtO-.:i:- joo 7cn

3.7fc£ 6617 0(356:

113M 700538

is K.711t- :.7cart 1.625it ioa.:-s2

W6.6?c

K.711:./osi.&a

US.SB:

5(>6.696


Pea1

i^»<J

Bet Tiic Pea Ht Area CupcAcut[•i»] 1«V] (nVtsecl NIM

2.270 5 0 Arcl-ii I ]:.7w o o A.-ci-i: i :*.<w» o o sr:i-:: i 3

G 0

tl Eitract Cone.no/kl

'.".' O.O&O0.0000.000

f.OOO

Suple CMC.uo/100«2

C.OOO0.0000.000

C'.OOO

Srouo Report For : SURROGATE

Feat

4

Eet TIK Pea Ht Area CMoooeflt[•»] (iV] [iVlse;] ka*e

25.200 0 0 8K

0 0

3L £: tract Coot.r. .-ii.

W 0.000

0.000

13i«pie Cfiflc.uc/:05:§2

0.000

0.000

•—. ,ii j-^ r- T * I r^ *"• <"* C: C- C" *""« O O T *~' ^ f* C" * * ^r ACc. , 11JC. . r Cr» KErUK i r .~i£E. IMLJ , .1

.- Mi:2:-oi:s9:s?i.FileN.ee : c : \27W\f l i t i \ lStar t 7i« : O."0 e:n End T:«e : 45.00 »u<S:aie Factor: -1 Plot O f f s e t : 32 »V

S.tple »: lOObCite : i / :<i/<;2 12:1<L 01. Fcir.t : 31.77 »VPlo t Sciie: 30 »V

Fioe 1 cl 1

H ; g N Poin t : 61.77

60 —

ui Tin

cq

-"-•N-X='

»J

• 1

>— 1

(b(/)

CL!f\

<D

~1

50 —

i

A ^ •

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-ii.

"1*

35

1

/

I f11 I

C-j CNCM CM

i iOQ50

10 20

7me [rnin]40

i.-r ".

' > j o

Nun.be-r : 25Ob: f - / 1 t. -2 11:26

r.f-«» - *» . ^ | . - - ~ T ^ ^; r l_c- fr-i.ii-n_ i o I _>

r - i . t rnf j .E-nt . iV K'«nqe : 1000

Inter-face Serial * : 124857403.5Delay Time : 0.00 mm.End Time : 45.OO mm.Sampling Rate : l.OOOO pts/sec

r-icquisition Time: 5/21/92 14:52

Ran DataResul t Fi1 nst rumenProcess FSample Fi

Fiietille

le

Fi 1e

..

•e::•

Cc

•—

cc

\ ~2v-'• —

'» _

\ r

-Vf

f

/

"

OO\dl.-v '3

OO\d

I. It ' '-. j

•>»."' -d

ct

5

c1

i,

taN

tcl-.

to'-

ta'vt^- \

1AEL:,^CL

i 1 cie

"?<i2

•JOS .i .O

I . P'~

fc * . S

re File

Ir.j . Volume

c \2700\cet^Mlael .sec

ftejtctic-n Factor

*^Cii£e Threshold: 6Mult ipl ier : 1.0000

MI-£-^ ; nresi .0 j a :Divisor : 1.0000

i.:L'n-_t~i Fcj

Adder : O.OOOO


v InstrumentColumnColumn LengthCarrier GasFlo* RateTemperature

Detectorte^.o

KS1111. 5V.SP-2250/1.95:iSF'-24016'x 2mm on 100/120 SUPELCCPOR7AR/ME 5/55 5 .Ti 1 . iTt i T:

2OS250 C

350 C

PRIMARY ANALYSIS

-•ACE. INC. PC3 REPOR"

rfitt

rlit ht Ca.c.

.£.0

7718

10-E2

iV

221. vi4

•

E91C11

' « *>

•' 17-1415161718192021

4.:5ij • t »* .0**

4.963f.OJ?10.S9C11.9S313.59515.36817.70620.0962*. 36230.46733.74140.44843.319

'.*<!19?fc7547912E73;s41452297

7039359

7:7i:53?785lift<43154:23.967Is8&1819139126439207

67549210341402

V'v'VVV6EB6VVBBBBBBBBBBBBVV36BB8

2C6.80676.19125. MO20.80230.10749.03629.86518.48815.7580.7340.3601.564

114.1250.5640.142

Jot. 60676.19125.51070.30230.10749.03629.86518.43815.7580.7340.3601.564

114.1250.5640.142

18656 326396 1255.853 1255.653

Group Report For : AR122.1

F'eat Ret Tine Peak fit Area CoaiOonentuft

1

123

BL Ext ract Cone.[sin] [u'v'j [uVJszc ] f«a*e ng/isL

2.2702.7004.400

000

0 Arcl-1221 10 Arcl-1221 20 Arcl-1221 3

VVVVVV

0.0000.0000.000

SdhDle Cone.

uo/100c§2

0.0000.0000.000

0.000 0.000

' Group Report For : SURROGATE

Peak Ret Tiie1 [tin]

4 35.200

Peak Kt

0

0

Area[uVlsecj

0 DBC

0

ComponentWane

BL

VV

Extract Cunc.

0.000

0.000

Sdtpie CuHC.

UQ/100CB2

0.000

0.000

PACE, INC. PCB R5

Ute : 5/:6L:» fc.:r.t : ".W »V . F'cict : s3.50 •'•'

JI

SO—I

1 1 1 ii

•-. U-- -- -3- — — TN:

50—

~~ Ii

_t ,

_! 1ji ii *— \ -.fti . L I-CJ .i ti

:! &"' ' '—-i J^v V.rtJ*

i li 'i

-r-T

35-

CD

I E I

\ S**~*i • '

Sam pile NumberP-pr-r f' tor

1 netrumen t

l'5b

KS111PEE. AS330O

Stud;/

Channel A/D mV Range 1000

Interface Serial tt : 124S574O35Delay Time :: O.OO min.

Data Acquisition Time: 5/21/92 15:38

End TimeSampling Rate


I n j . v'o 1 urneSample Amount

ise ThresholdMultiplier

45.00 min.l.OOvO pts/sec

\270O\data\lAEL009.raw\270O\data\lAEL009.rst\27OO\data\llael.ins\27 OO\data\llael.prc\2700\data\AR1232.smp

c:\270O\data\llaei.seq

2 MG/ML1 .0000

61.0000

Area Reject : O.OODi1u t1an Fa c to r : 1.00


Bunch FactorAdder : O.OOOO

Instrument Conditions:Packed Column CSC -

InstrumentColumn

:KS111: 1 . 5XSP-2250/ 1 . 957.SP-2401

A Column Length :6'x 2mm on 100/120 SUPELCOPORTj Carrier Gas :AR/ME 95/5

:55 ml /min: 203

Flow RateTemperatureInjection Temp.:25O CDetector 1 :ECDDetector temp :350 CNotes :


PRIMARY ANALYSIS


Featt

!•5L.

.} 3f 4

5

Ret Tiee[sin]

0.2192.2032.3442.6223.32i

Peak HtIuV]

552753615S3263

Area[uV'tsec]

i7524733274ii973017

ComponentNate

Arcl-1232 1Arcl-1232 2

BL

SBBVVVvSEV

Extract Cone.nc/eiL

2.66913.31317.4482S.17524.S34

Saiple Con:.uo/100cs2

2.tt>9f "? T < 71J.OJ.O

17.44828.17524.834

^

; :.{ •.

* * •^3 * -

•O* 22.y.5 13.

16 2f.17 23.18 30.1? 33.

Gi'OuD

rfil Tit .

A

3 4.

GrouD

Pea Ret 1t [ua

'" < 33.

.S »*£•"•; re

II!- ":

7?v !?•151 ol016 53»S3 50217 27682 28303 76769 3352

6CC1

Keport For

;i* rf j* s»

til !el

219 430

1277

Report For

iw Pea Ht

1»01

!::

IC33!43e23622207ifib1338WO

4123315938 OK

356162

: AR123I'

Srsi .itsir.cr.tVise:] fc.ir

5181 3Srcl-1232 3

14395

: SURROGATE

Area Cotpwwt

t?Etrtr?•ttf

rtElfSoe

0B

rr

'.•V

SL] [aV] [iVIsec] Kue

76? 3352

I-S1

315938 iK

-iw-a

U

3.JC.

2.236

<.43o

3.1424.771

r.oiiI.£b20.477

0.5031.34S

59.172

203.737

Eilr«:t C&r.:.

r.g/*L

IS. 175-•^.Oji

77.674

Eitrict Cone..10 /tl

59.272

59.272

J..-OI

2.2334.43i

3.1424.791

3.C111.B620.477

D.5031.349

59.272

203.737

2<&ple Cone.

.1.fij4

77.674 ^

Eeisle Cone.ua/lCOcx2

5?. 272

59.272

r i^r? f c:r'(_irv I .— 1-101 f <

rl.e:««i.e : ;.; ... ,v\<.St.rt *i*e : C .OO i:rik i l t Fi- ; tcr : -1

Enti hre : < ' .CO nnr iot O f f s e t : 3A »V

ID* Point : 3<.2b »Vf' iot Sca le : 30 »V

High Point : 6A.26 *V

t

* o r«i •* iro LO in<N c»j *'ICN o«p r T-

r-j *$ ~? «V5 f^ r>i i 11 i ii. in

60

i

I

-II

(

0) 50—|

Wc0aw^ 45—J

- 1-i

40

4t1 ,+A/vJ i Jr-rn

-I»_j

•-->•:£H

r-r- .

Z5CMI

rr O•oI

r)•oi

A

,• »• 'i ;•*• •

j i~~l-~> CN

5S COO

"i i i i i i i i. r, , , , , , , , ,30O 10 0

! Ime Fminift. —j

40

' Instruct-, it : t Silli-.Litoiample-r : PE AS8T»• •

S;-'sc<^ /Viitl : 0/0P

Interface Serial * : 1248574-Delay TimeEnd TimeSampling Rate

Raw Data FileResult FileInstrument FileF-TC'Cc-is. FileSample FileSequence- File

L.harifit-1 : « fi/D mV Ranatr : 1 '_>O'

Acquisition Time: 5/21/92 16:25

Hultiplier

O. OO fT'in .45.00 mm.1.OOOO p ts/se c

c \270O^data\lAEL010.rawc \27OO\data\l«EL01O.rstc \27'!•'!•' clj ta'. 1 lae 1 . insc * 27->"'Vd.5t^ • 1 lêl . prcC \ 2 7'.'• •. ' '•- dci t.ci \i-iri 1 _J -•*.'. Sfiip

; •''<(- Are£< Reject•^ . * *. . _ ,- f~ _ .« * i n i_ j. i_i. i r & t

i-iTcci il". ("esncjicJ : -_^JL-i visor : 1. OC'OO


Instrument :<S111Column :1.5:'.SP-225O/1.957.SP-2401CoiuiTin Length :6'x 2mm on 10O/I20 SUPELCOPDRCarrier Gas :AR/ME 95/5Flow Rate : 55 ml/mmTemoerature :203Iroection Tern p.: 2 5O C

Ir=-tector 1 :ECDT-etectcr temp : 35"'1 C

: O.OO

ich Factor: 1Adder : O.OOOO

PRIMARY ANALYSIS


:fii r.t

i :Eerier C:

r.o/tl£i*::e Core.

j 3

TO*•::315

*

1011121314151617181920

4. =575.1966.2236.6427.7929.11813.64017.16720.09530.06333.81639.183

39651E39030753827338396342

693140

47771148369C45b60

2004877961260111523471639

667577 DEC1054

vvVB6VVB6VVBSBB9IBBBBBEB

i'J.OVi

29.71922.34717.59030.85015.9242.1872.2431.1130.743

122.5640.704

ii.bii

29.71922.34717.59030.85015.9242.1872.2431.1130.743

122.5640.704

16597 814131 676.526 676.526


Peak Ret Tine P1 [tin]

1 2.6272 3.3243 4.250

eak HtfuVJ [

20479631671

firea CoiponentuVlsec] Nine

21106 Arcl-1232 110998 Arcl-1232 222213 8ArcI-1232 3

BL

SBBVVV

Extract Cone.ng/ftL

98.93690.74495.786

Saftple Cone.ug/100ct2

98.93690.74495.736

4680 54318 285.465 235.465


Peak Ret Tiie Peak Ht Area Coiponent' f [iiin] [uV] [uVtsec] Kane

BL Extract Cone.ng/tL

Sacple Cone.ug/100c»2

4 33.316 6931

6931

667577 DEC

667577

BB 122.564

122.564

122.564

122.564

PACE, INC. PCS REFORT PAGE Wo. 2

Sti't *:•« : :.OC •:•lli'.t ?i:ttr: -1

End !;« : ;!.CC> *:r.rlct Sftstt: 31 *.

Lo» feint : 35.33 (?;&'. Hcile: 30 tV

"•.c = Feint : e5.33 §V

r

CN,CM

65 1

50-

• I I I III! I i

CD

I

03fj

I

45

,'_'f • •.»

_V

) f-1 * i ;"" i f~: I

bt<mple Number: -Jt-ODOpt? rater : EM A

I" L- £."• t-i I M M L_. I

AutoSamplerRack /vial

: K3111: PE ASS3UO: O / 0

Chan ri mV Range : 1OOO



Inj . Vol unie3 a in p 1 e A MI o u. n t

Noise Thresholdu.! tipl ier

0. GO mi.n.45.00 min.1.0000 pts/sec

\2700\dat.a\ 1AELO11. raw\2700\data\lAEI_011. rst\270O\dataMlaei.ins\270O\data\llael.prc\2700\data\AR1232.smp

c \ 2 7 0 0 \ d a t a Ml. a e 1 . s e q

2 MG/ML.1 . OOOO

61.0000

Area Reject : 0.GOD i \ a 11 CD n F a c t o r : .1.. 0 G

A r e a T h r e s h o 1 d :Divisor : 1.0000

B u n c h F a c Jc o r :Adder : O.OOOO


Instrument :KS111Column : 1. 57.SP-2250/1. 957.SP-2401Column Length :6'x 2mm on 100/120 SUPELCDPCRTCarrier Gas :AR/ME 95/5Flow Rate :55 ml/minTemperature :203Injection Temp.:250 CDetector 1 :ECDDetector temp :350 CNotes :

"otal Number of Peaks Detected:

PRIMARY ANALYSIS

PestS

12345

Ret Tisetain]

0.2491.9172.1S32.3412.i30

Peak Kt[uV]

4519473118365174

PACE

Area Component[uVJsec] Maes

8321407a3341512256539 Arcl-1232 1

E, INC

SL

EBBVVVVVVE

. PCS REPOR

Extract Cone.ng/iL

2.190.9.33337.77233.754250.033

T

Sasple Cone.uo/lCOei2

2.1909.38337.772S3. 7 54250.083

*J>1W t.o. en?V

. 1

Ij

^~v H

IS!&171819202122"3n25

•'^46.2316.650

7.7o3

9.145

10.625

12.021

13.523

17.312

20.08822.784

30.26533.60641.SS3

i'*9140711631S0187139

159191

49E73198

7522:i

«*3186626349

6656330486

7425083

8456t;293662

594/:*i

bToTSi OK

172

3«:72 1157543

Group Repor

•Hi

t

1

x 2"* 3

Set TIM Put

[•i>] I«V

2.630

3.3284.255

t f

Ht

]

517426914350

or i Aft 1 — -• —

Area CotKcefit

[uVtsec] K«M

56539 Arcl-1232 1

36067 Arcl-1232 262617 SArcl-1232 3

77.8fc5

W 80.674

W 66.68?So.070

i'5 49.953

tt 2.250

3B 9.117

tf 10.938

69 2.815it 1.539

K 0.543rb 1.727B3 124.176»S 0.371

1715.4:4

?l Extract Cone.

no/tL

Be 250. OS3SV 253.681

251.713

9i.276B3.674

66.639

OB. 0:0

49.953

2.2509.117

10.938

2.8151.539

0.5431.727

124.1760.371

1715.424

Suple Cone.

uq/100c*2 W

25C.033253.6S1251.713

12254 155222 755.476 755.476

Group Report Por : SURROGATE

rtal i»t I:K Peal >it Area Co*pwi«t t-trjci Cone

28i 33C i:4.176 124.176

PACE. IMC. PCB REPORT PAGE Ko. 2

Start T:te : 0.00 tinScale Factor : -1

Erid Ti»e : <'.00 tinPlot OUset: 37 tV

Lo* Point : 36.54 tVPlot Scale: 30 tV

Hich Point : at.54 tV

"> 14•AT""' (f-

65 —

_J—J

160 —

H

ir— i _

* E 55~

<L>* 00•? c; o so—

~ . Q. _J en

<Dor

i45 — j

J~1-1

tL

m* "I'

41

40 — |

1!!

(

ii

\i

i

i

,' J

ro £N SN •- 01 so r- i- aoi CM-TOf-ixn KI co LO r.o o ir> ^ o rv. .7^ DD or>J O .T*') 04T; CvJ N »-( Q r rrj r,' (~i cvi Q rH — '

5 1,-. .jV . - -»- * f%, -p, __ __ ^— v— n. i rv i M^l */ l *^*-^^Srr7 •* " *t.- l^* S? ^ ' ', J » t« i . Tmi it 1 1 ii i 1 1 i t i t i t i i t i i

A

/Ij ii )

i,, - MalifJM^^ft V VlA? 1 V J I L-Y- j- . — -T1 • --TrrT -r- -, ri r— i — rr— <" • •I'i/jj-^-r-i-rrr 5 1 > 'Ii:i

11 1 ri, 1

^•J^J "1K>OCNv-sTvi i-T— T— 11

1 i J

cx3 £' oQSV;*IJ CO<K CO Q

1 i ! ! j 1 ! i 1 j ! ! i 1 | 1 I i ! | ! ! 1 ! | 1 ! ! ! | 1 ! 1 ! i ! ! ! i i I 1 !' 10 20 ' 3O ! 40

r ~i3 i--vt i *—i I; i i i i i i I

il Cr itt r : _'L'b 3 LUU V

:i.t' UJJit-1'i I ' ! J *. 1 i

rr.pl e-r : f-E AS37.O >Vial : -./O

'Interface Serial * : 124257-1O7-5Dela/ Time :-.».OO îin .End Time : 45.00 mm.Sampling Rate : l.OOOO pts.sec

1 'X-..'

Date-. Acquisi t ion Time: 5.-'21.-'92 17:53

Raw Data File : cResult File : cInstrument F i le : cProcess r i l e : cSample File : c

riCr1 c 11 tr : c

\ ^7'';••'* '• da ta \ i AELO1 2 . r aw\27oO\data\ 1AEL'''12. rst\27 :JO'- Jata .i lael . ir ,s\27'X> ^ c J 5 t a \ i ^ a e ! - p r e'-. 27'!1':1' cJata'.r".." 1 2^2 . S.T.D

_ - - A . _ v * * _ _ * . — ^ _' ' ' J o t a - . i l s c r J . -=e-O

. r, .1 . '.C. i LI -V.,r

~-:«^.^ ] e- AIIT.C L-'.1"ri r e a f-. e j £• c tI • 3 ] LI 11 o ~i F f- c v o •"

"u I t i p l i e r.-«.'"5a : i :t"&5i i'_'j. u I

Divisor : 1.0O £ • 0 Adder-cri Factor:: O.OOOO

Instrument Conditions:^- — « _ w f* •» * — ^f^

.v Instrument :K31ilf Column : 1. 5XSP-2250/1.95'/lSP-240i

Column Lencth :6':: 2:Ti:Ti or. i-X1.-12'I> SLiFELCDPCRTCarrier Gas :AR/ME =5/5Flow Rate :55 ml/minTemperature :2OSInjection Temo.:250 CT-etector i :ECDDetector temo :750 C

PRIMARY ANALYSIS

I. PCB REPCR-

•ak ;.*: T:w ;«i Ht* !s:^] lav; Nate

Ezt rac t Lor.c. Siti'.E CjT.C.

C-S

>0

sV

22. o:?

:a.?53

.-

1011r

1 13v 14/15

16171819

5.2365.B543.211

6.6377.8209.089

13.63320.14321.848

33.783

™ * •»->.>.••

:os285234253151

5911734

3746

7707309757804752

10281612822835952

769

356993 DBC

VVVVVVVVVVVBBBBB63

BB

11.6357.1619.9678.1659.0265.2762.0661.7390.49B

55.608

11.6357.1819.9678.1659.0265.2762.0661.7390.498

55.608

8461 441246 268.032 268.032


Peat Ret Tine Pi» [iir,l |

1 2.6212 3.3113 4.252

?ak Ht[uV] [

384447827

Area CoeoonentuVtsec] Kajie

4361 firc!-l':42 14703 Arcl-1242 2

11090 Ard-1242 3

BL

BB6VVV

Extract Cone.riO/ilL

2S.953

25.5322S.913

Sacde Cone.uo/100:n2

23.95825.53228.913

1657 20154 83.403


Peak Ret Tise Peat h't Area Cowoiient* [tin] [uV] [uVtsec] Na«e

BL stract Ccnc.no/iL

Saiiple Cone.uo/100c«2

4 33.783 3746

3746

356993 DBC

356993

55.608

55.608 55.608

PACE, INC. PCS REPORT *AGE No.

C".3v end Tilt : i".i»v »:r.Fill i'Stt: -"S »V

LD« Foirt : !•'.?< tV::it :Cilt: 30 i'.'

I

«- Csi "JO(Cr>4OO 30 O

*~ \i i i Mit iiT i ~

55-

» i-

9- 50-

U

— EJ2C

ro

45 i!

gp

^;e L

| : ; : i i !40

Number : l-.-Ob: EMA

3 I LIU ,

lni.trunit-.-ntAutoSeimp.iler

.—s.Rack/Vial

KS1.11.PE AS8300O / 0

A/D rn'v 1OOO


Raw Data FileResult FileInstrument FileProcess FileSample FileSequencc- File

Inj. VolumeSample Amount

Noise Thresholdtiplier

0.00 min.45.OO min.l.OOOO pts/sec

\270O\data\1AEL013.raw\2700\data\lAEL013.rst\27OO\data\llael.ins\2700\data\llael.prc\27O0\dat a\AR1242.smp\27O0\data\llae1.s eq

2 NG/ML1.0000

1.0000


A r e a T n r e s h o 1 c! :Divisor : l.OOOO

Bunch Factor: 1Adder : O.OOOO


Instrument :KS111Column : 1. 5XSP-225O/1.957.SP-2401Column Length :6'x 2mm on 100/120 SUPELCOPQRTCarrier Gas :AR/ME 95/5

; Flow Rate :55 ml/minTemperature :20SInjection Temp.:250 CDetector 1 :ECDDetector temp :350 CNotes :

Total Number cf Peaks Detected: 24

PRIMARY ANALYSIS

Feak

*

12

; 345

Ret Ties[sin]

0.1382.199i jj£

2.6193.056

Peat Kt[uV]

49•T*!/

6451522313

PACE ,

Area Co*Bonent[uv'tssc] Nate

43047965S7319925 Arcl-1242 13404

INC

3L

E5EVvyVVvV

. PCS REPORT

Extract Core.

"?/EL

3.67032.20643.663114.892IS. ISO

Sasple Cone.ijg/100es;2

3.67032.20643.663114.39213. ISO

•

i

4

cj

t

7a

19202122;3

:;

*.e.« *'

i.:a!.£3t.2vt6.60

7.7:9. OS!

11.134

11.951

13.M3

17.2C419.91!28.77J

3J.(3!"."t

.:}.» .*ji»

11*1 l!5t*

:!•:•! «!IC3-as 504*

::!< :7S5i1014 22102

1315 o?3eZ1 3:; 49404

( •> . « *LiCTJO J Ôv * '

403 21260

259 10382

133 7556123 3644

1 31 74347 13!9

:;o: ::o&^ :K

i •

1 1

• V

\v;;.7t «

wVtf

V6

JD

B6

fStireKH

.•'..JO

T9.~;65:.tp;ls.3t?43.S49

35.450

'i.oTo

32.031

J2.69614.084

?.049

4.6651.320

0.460

0.700

111.390

-•-.-cc

-' -~ ' .3

52.60416.*6943.549

35.450* •" ***£.&' 0

32.031

12.670

14.084

5.04?

4.665

1.520

0.460

0.700111.390

9i9.S29

rtii iii *1K

» !t;a]

1 2.6192 3.3133 4.247

•til iit!«¥] [

15222*42

34i8

n.'Ei .;«;a.erit

liViScC] KiM

1??25 Arci-1242 1

2647? ftrcl-1242 2

51732 Arcl-1242 3

:l

iV»VW

i:lr«:t Lt:.:.

,i9/t

114. £52lie. 618121.262

e?/;oott:

114.8=:l!e.s5S

121.268

;J!2

3roup Reoort ror :

fri« lift TIM ?eii Ht Areit

Supie Cone.

7W3 111.370

'<C . FCE> REF'G?;T

r ;.th«lt ; L. '...YJ ,„

Start 7:«e : C.OO *ir(

Scale Fac to r : -1Er.d Ti*e : "..00 »rFlot DM set: 35 *V

L&» Foir.t : 38.44 tVriot Sciie: 30 *V

High Fou.t : ci.44 »V

65

i

-I

-i

50 —

T-iH',flri

i. . — — f~>

IT 'HI ii i niVi77 ' i "i i i i

40-I!/

i a

i i

I I I Ii I'M CN

| ^N CM

! Ill! ddd! .-"r'.V ,vi .r^-^ -;i

1 1 1 t f | { i t 1 1 1 1 i t 1 1 i ( 1 1 j ( i | 11 . . . i , . , . . , . . . , 1 , , , , , , , , , ,3 10 20

i

OCDc.

! ! ! ! | 1 ! ! !30

1 I ! ! 1 i 1 i Ij , . , , j 1 1 ,

40

l ime [ m i n ]

' ; - f.r _.(!,,<:••••„•.«-i'..i t<j3afj>!j I C-r"

-x '•' e1 C I - V 1 ei I

£1 ; : f.r.^r.i.e-1 : "

Interface Serial « : 12-19f- 7 4-' 7 S f'&tii Acquisit ion Time: 5/1:1/92 19:31

Del a/ lime : «.».«x« nan.End Time : «J5.OO ruin.

Sampling Rate : l.OOOO pts/se-c

?.-&** Data File : c:\27oONcJataMAELO14.rciWResult File : c : \.27<X»'-.cJata\ lAEL'i 14 . r&t" r 51 r uroen t File: ~ : '•> 2 ~-I'0v d <? t =• '•-' 1.-e-1 . i n s

File : c: . I'7'>~ • c^ t«'» 1 iêi . pfc€• r i le : i: - . •.••.' .1 t.^'• *~\~ 1 _ - t . _ . =.nip

rr Fi le : c: ' • I'"1'1'/ -d^t« v . 11 f*ei . seq

ire^ Reject : • : > . " • ; >.'ilution Factor : 1.00

:'•-• 1 tip! ler :

Instrument Conditions:Packed Column GC —

^ Instrument9 Co1umn

Eur.ch Factor: ir : O.OOOO

Carrier GasFlo»* RateTesr-peratursInjection Temp.

Detector iDetectc-" tempNotes

1. 5/1SP-225O/ 1. ?5:'.SP-240i6':: 2m:Ti on 1 •'•'!'.- 1 Iv 5UFELCOFG?\'TAft/ME =5/555 ml/.Tiin203250 C

ECO

PRIMARY ANALYSIS

iCE. INC. PCB riEFORT

ri -ct Estr«:» CM:'•'.•ti

Cone.

;j.5j5

i.tol

it.'/:o111213J<;is161718192021222324

4.9445.2806.2136.6437.7679.10411.12411.95213.56715.23917.20519.83323.08524.63133.750

•:•;?:«3722481869254215793334955271552521214040

8241

15007505604245538549100883562231561217381230777410125^9781512101929

800597 D&C

VVVBBVVVVVVBBVVBBVVBBBBBBBEBBB

43.60655.21473.60465.35188.63155.20911.64517.30413.4245.4328.8111.8030.5870.593

122.344

43.60635.21473.60465.35183.58155.20911.64517.30418.4245.4328.8111.8030.5370.593

122.344

41324 1400009 1552.877 1552.877

Group Report h-rer : AR 1.242

Peak ir*

123

let Tine PUinJ

2.6193.3164.243

eak HtluV] [

322742636896

Area ComponentuVlssc] Nase

30907 Arcl-1242 141075 Arcl-1242 280806 Arcl-1242 3

EL

SBESVB

Extract Cone.ng/sL

243.625243.668241.111

Saiple Cone.ug/100cii2

243.625243.668241.111

14336 152737 728.403

''Group Report For : SURROGATE

Peak Ret lice Peak Kt Area Cosponent* [tin] [uV] [uV'tsec] Nate

BL Extract Cone. Satple Cone.ug/100c*2

4 33.750 3241

3241

300597 DEC

300597

BB 122.344

122.344

122.344

122.344


::&t C f ' S t t : 13 ».Ls. fc.r.t : :-E.C*•li'. =:.le: j'J »'•

nlc^ "sift : ce.C? »V

* V*9 C

a:

ii i i 1 1 1 1 1

! I~~: I

1 I~! I

•Mj

5O

.l i! ! »' !"r i" f >i t i i i.' ,

i : i

O

^, 1

J

Ejafnp i e Numbr-r : 2 L .b('.):.':• r a t e r : r. ' .Mri

c-jtuay

JnsJ:. rumen it : KS111AutoSampler : RE ASS3OO

: 0/0

A A/D f< <* n q e? lUOi'.)

interface Serial tt : 12485740.35 Data Acquisition Time: 5/21/92 2O:17Delay Time-End TimeSampling Rate

Raw Data FileResult FileInstrument FileProcess FileSample FileSequence Fi1e

Inj. VolumeS a in pie A CM o u n t


0.00 min.45.0O min.1.0000 pts/sec

\270O\data\iAEL015.raw\27OO\data\lAEL015.rst\27OO\data\llael.ins\27OO\data\llael.prc

c \27OO\data\AR1248.smpc \ 2 7 O O \ d a taMlael . s e q

2 IMG/ML1. . 0000

61.0000

A r e a R eject : 0. 0 0D i 1 u t i o n Fa c t or : 1 .0 0


Bunch Factor: iAdder : 0.0000

;l


I n s t rumen t : K'3 i 11Column : 1. 57.SP-2250/1. 957.SP-2401Column Length :6'x 2mm on 100/120 SUPELCOPDRTCarrier Gas :AR/ME 95/5Flow Rate :55 ml/minTemperature :208Injection Temp.:250 CDetector 1 :ECDDetector temp :35O CNotes :


PRIMARY ANALYSIS

Peak

*.

•)

34J

Ret TiffiE[Bin]

0.2042.2142.3312.627J.30i

Peat. HI[uV]

i:8

2?2236

882;;2

PACE, INC.

fires Coiponent ?L[uVJsec] Kase

746 EB2423 BV2645 VV

907 V32iSi SB

PCS REPORT

Extract Cone.ng /iiL

3.549... 14.296

12.3844.624

13.762

Sexoie Cone.sg/U-

3.54914.29612.3844.624

13.762

.j i.V:j!6 II.53317 13.61518 15.2S7

'? If.9682C 24.503

22 33.750

7

56

120

08150

47364C

537514337

90981132

»B

Bit>VVBBEBE

7S.2S:

21.SS715.50725.777

E.S0716.7405.014

11.5260.660

54.C32

.

21. Sc

25.797

3.807Is.740

5.01411.G260.660

Group Re-port, i-or : rV-\ 1 _-1 ?*

*t»i rrl :i« :fii rtt V=i CMiC-r.fM rL I t t f i t t C&riC. Sstlir LOT.C.

t it:*] iii>i [-.liec] )>«n r^/ti t;,.c

c ^m c-j. .-,-c •i-^'c • B'I •'p 191 -"p %!. •l..T« J1^) iJC.J nK.^*C ; f> ^C.ôl ~C...D*

I T TI C£i *1IÔ •"•"**G ^ "•" "<e "**T ~C ^ff-*i.it& 556 i260t (iMi'B 2 r» i j . / t / »J . . -TI• V *^« "n* CCCl Ifi 'TIfl T "t ""• t*t ""> iTt^ ?.V9« JV' T0j4 mi.%C a v& ^^.OOC ...d«-C

•402 45537 76.7;4 7s.714


'til «itl TIM Pest Ht n-e. LMK'K.*. rl Estrict Cait. sitsle CwiC.i :*:n] iuV] -n'Visec: 5»< ''?.»L *?/l?

35i72i D=: BE 54.?32 54.C32

-ACE. If:". ?CE- F.EPCRT PAGE ?Jo. 2

't ".te : 0.00 tin'.e Filter: -1

tri list : <!.00 i:nPitt C f1<e» : 38 iV

lo. Fcir.t : 33.<I *VPlot 5:a!e: 30 tV

riicjri Point : 6S.<*

r-,

c

^/rtV '

c0Q_

s01

^

65 —

—1

60— j

-11

—

55 —

—

_

—

50 —

:— \i

45 — |

• j-

~f— i

— i40 — i

in I'IIHI iTT i ~ i i i i

si

-

i CL . *P

y"r

CM >oi i

OS

i i nr-, e [ rn I n ]

Nt.ffibc-r: IX'T ; n,i-Sturf . : I "CL- rifî-tL '•. i> 1 o

.' r.s. t» u/iiernt : "r.Sill«utoSampler- : PE HS

::» /Vial : o/O/

Interface Serial * : 1243574O35 L>c«te« Acquisition Time?: 5/21/92 2I:O4

Delay TimeEnd TimeSampling Rate


3 nj . Volt" Tie= cpfljp j e- i-iiiiGur. t

Multiplier

O. OO m i r,.45.OO nan.i.OOOO pts.'sec

c: \270O\da to X i AEL'M 6. rawc:\27OO\data1 1 AtL-Mo. r= tc : \27O«I^ c5 =11 .119it- i . i :•r-c : \27OO\data'- llael . prcc z'-. 271.•'.*'-. ci a t a' AKi ^^3. snipc: .27-:-:-\c;5t^' 1 l^c-1 .sec;

2 r;G MIi . •.">-•>.>

Cr

1.GCOO

D11 -i 11 on Facti-r

: O.OOOO

Instrument Conditions:acked Column GC -InstrumentCo1umnColumn Length^rrier Gas

ow RateTemperatureInjection Temo.Lstector IDetector temp

KS1111. 5XSP-2250 i . ?5::3r-240i6'x 2mm on i•:«?•/120 SUFELAR/ME 95/555 ml/mm"•"•

PRIMARY ANALYSIS

PACE. INC. PCS PEPCftT

r.tt T:ii ?fil rt A'*J si.

ij.ij

: T . r l i•-C

'

;:;

p

s 4.c,ri t'2i :.:;: •;::

ic 6. in M '211 S.e:i :.!04

1: 7.757 190513 9.093 il6314 11. He 24015 11.913 33516 13.554 35017 15.167 10613 17.175 255

19 20.014 «20 30.103 5221 33.718 702922 43.219 45

20635

Group Report F

Peak Ret Tise Peak Ktt [tin] [uVj

1 5.283 14322 7.757 19053 9.093 1163

4701

903S3977t AR124S 11136?Z123173290 AR124S 23E686 hR;:;a 31245512525161085293

1187014572535

6S2630 OBC1617

1005548

or : API 248

firea Component[uVisEc] Nane

39774 AR1248 173290 AR1248 233686 AR1248 3

151750

v *

VBBV• ir.v D

8VVVvvVB3VVBBB86SBBitBB

BL

BBBVVV

W 1 ..».

85.79362.62051.17933.35385.70017.71624.64325.7547.814

18.764

3.1910.767

104.3470.669

349.809

Extract Coneng/el

85.793S3. 35835.700

259.851

S5.7".62.62051.17988.35385.70017.71624.64325.754

7.81418.764

3.1910.767

104.3470.669

849,809

basple Cone.to/kg

35.793bS.35385.700

259.851


Peak Ret lite Peak HtS [sir;] luVJ

4 33.713 7029

7029

Area ComponentEuVlsec] Nsfie

i826SO DSC

6£2i30

•". .-*••. r r-r t-i u . ^

BL

J.r

r h i •"•* r-i r^ ""ti ! ••! i— . r i- o

Extract Coneng/tL

104.347

104.347

REF:'ORT

Sasple Cone.«g/kg

104.347

104.347

PAGE No. 2

; r- • ,:.?.*-e :-.-:•• r-r-i-

/Vial

Stud-.

1 ;. 1 i 1

h E «o0 / •->

Sr.ter-face Serial « : 1243574O35 Data Acquisition Ti.Te: 5/21/92 21:5ODelay TimeEnd TimeSampling Rate

Ra« Data FileResult FileI rstrufJier: t .-lieProcess File

r i <Ti p i e t-iiwOL." ri t

V'u ] 11 p 1 ier

0. OO IT, i n .4 5.OO min.1.OOOO pts/sec

'OONdata\1AELO17.raw\27O

\270

i'.dataMAEL.017.rst

1 .data .^.I.aej .prc

Dilution Factor : i.OO

.-if=ra Threshold :Divisor : 1.OOOO

r-uricn Factor: 1Adder : O.OOOO ^

Ir.stru:Tient Conditions:f'acked Columri GC -

•^ !nstru:Tierit9 Column

Column LengthCarrier Gas^lew RateTemoeratureInfection TecDetector i

6'x 2rri.-n en 10O/120 SUFELCCFORTAR/ME 95/555 (Tr 1 / iTi 1 n

21*3150 CECD

'- c-f -es^s Detectej: -7-

PRIMARY ANALYSTS

PACE. INC. PCB REPORT

I [1:1] *tVi 13. i

!.571

,V*V1±

::.42o

c

•* 9

.:. :o» »

) 12V, 13

J14

' :;""151617181920212223

*.&;y5.2E26.2006.6157.7489.037

11.20311.90213.54915.18517.20019.47024.79628.11430.11133.eSl

199348593333349354993474

84310301023212420626654

2587446

45337

2?t46H0226 fiRlI«S 1

S002575432

236744 AR124S 2140978 AR1243 3

5248646?4349939

S35118519286329161295

22053721046 OBC

176S723

1 V

VVvvvvvvvvvvvvvvvvVBBBBBBBBVVBSB

JO* . t*. J

104.763255.355201.423162.020254.572255.94462.10779.55775.39615.62330.9094.5760.982O.S013.326

110.542

2182.437

* • Q.MJCi .0^ J

104.763255.355203.423162.020254 .572255.94462.10779.55775.39615.62830.909

4.5760.9820.3013.826

110.542

2132.437

Group Report For : A R 12 48

Peal

VfA

23

\

Ret Tite[sin]

5.2327.7489.037

Peak Ht[uV]

435954893474

13821

Area CofiBorient[uVJsecJ tiase

140226 AR1248 1236744 AR1243 2140973 AR1248 3

517949

BL

BVBVSV

Extract Cone.no /'it.

255.355254.572255.944

765.871

Sarple Cone.eg /kg

255.355254.572255.944

765.871

li up Report For : SURROGATE

Peaki

4

*

Ret lice[•in]

33.631

r

Peak Ht[uV]

7446

7446

Area Cstpcnerit[uV.tsec] Nase

721046 DBC

721046

PACE,

BL

BB

INC. PCS

Extract Cane.ng/iL

110.542

110.542

REPORT PA

Sitp IE Cone.ig/fcg

110.542

110.542

GE No. 2

j'.ift !:»* : 0.0} §:r

f«:tir: -I rict £:iit: Ti »V

t

K; rjl?1 ~. ~« ~-i T-< f^

~~ iT i" i i 11 i 11 ic;i

-1

oQ.01

: if

: it

-J \. r

H!

! :• i

AI1 V

r ~i. .- .--. ; r~-. \L J

i line 9Sample- Number : 25taGrjcr;--.t.or : EM A

j . nst r Uiiiefit• AutoSampler

KSlliF£ A3 8 300

Channel : A A/D n>v o : lOGO

Interface Serial ft : 1248574035 Data Acquisition Time: 5/21/92 22:36Delay TimeEnd TimeSampling Rate

Raw Data FileResult FileInstrument File?Process FileSample FileSequence File

Inj. Volumeiaraple Amount

io;ê Thresholdiulîplier

0.00 mm.45.OO iJiin.1.0000 pts/sec

\2700\data\1AEL018.raw\2700\data\lAEL013.rst\2700\data\llael.ins\27OO\data\llael.prc\2 7 OO\data\AR1254.smp\ 2 7 O (..) \ ci a t a \ 11. a e 1 - s e q

2 NG/ML1.OOOO

A r e a R >5 j e c t : O . 0 0Dilution Factor : 1.00

£)

1.0000A r e a T h r e s h o 1 d iDivisor : 1.0000

Bunch Factor:Adder : 0.0000

nstrument Conditions:acked Column GC -InstrumentColumnColumn Length

GasRate

TemperatureInjection Temp.Detector 1Detector tempNotes

KS1111. 57.SP-2250/ 1. 957.SP-24016';: 2mm on 10O/120 SUPELCOPORTAR/ME 95/555 m l / m i n208250 CBCD350 C

tal Number of Peaks Detected: 20

PRII1ARY ANALYSIS

s.et T:se[sin]

5.1842.204? '??4.222- -,2?

Peak Ht[uV]

952491S962

236

Area[uVtsecJ

t!s240314176£9

4 .•"!•» 7VO J

PACE, INC.

Coaponent 31nS£&

i'3SVVBSBBV

PCB REPORT

Extract Cone.riQ/ri

i.e3S17.49713.22?4.333

la. 58?

SaSpie CoriC.

U9/100C62

4.63317.4?713.22?I 7?."1.-iv3

14.587

•*£<: A-

. *4 J

^L

•-**>'"

li

17

:a1520

ii'i i;;?.<•; ;56

24.765 37

30. U3 oO

33.471 3443

43.4S1 50

:!ii>s ire!-!:-!-; :

118*7

r&~'12:12023

350583 DBC245*

v-i :4.7i6sv 75.37-7

rV 14.700

i'i ::.3i4.:5 'J.5<9

're 0.839

?3 J.4.D73

bB C.732

H.7«0

22.3«4

0.543

0.839

M.073

0.733

JT-OUD Re&ort For : riP. 1254

rit

*

J

;*^

Jtt Til* :ril '-.'. irfi C

It:t3 J->: ;U''ISeC'

S.83« ;:4 11176 Arc!-:::.m 7:5 ::i:: ;.-c:-:• * c t^ t **j * c » * " • i t

'* ' """fi "• •

.•s:c-.r". rL £itri:t C&r.:. ;it:"jr L::.Si« r.:/t. uj/ii-ia:

;« : » :;.«: 2:.«:-;; I M 24.7IS :«.7!3'(•* -i, "C"**^ "C-*"*JtJ 11 .J..'fc/ &^.v^/

39738 73. «7

For : SURROGATE

•' ••**» Ti« rtik Ht Area LMMOKt 3L Eztrjct Cor.c.jji] fiiVj [uVIst:] Sjt? r.:/iL

33.»7J 3i*3 3fO!s3 SBC :3 ".C'72

7»i43 7K523 54.&7S

SM/:W«::'

5-.;;3

54.C75

FileNaie : c:\2700\data\lfiEL01S.ranStart Tite : C.OC nn End T;r,e : 45.00 tinScale Factor: -1 Plot Offset: 35 tV

Date : 5/26/92 13:14LOK Point : 39.28 »VPlot Scale: 30 tV

Hioh Point : i9.28 i.V

J t1

r'

j

•"-.. ~"

1 1

Q; 55 —A 00

* zo

?' a

jy 50—

—

H0 45_j

_ixn-^

? 'iS (

1i

^~1 fc

40

i i n i i i

icc^> — -"> •'"••

i i i i

r--

-o

A

--K-.

•i1I ii

0

f_\.Tr"

i i 1 1 i 1 1 1

' ' i ' ' ' ' |

10

O CJEC o:< <"1 ' 1 i i 1 i i 1 i 1 i 1 i i 1 ! T~

t 1 1 1 1 1 1 1 i f 1 1 I I I !

20 ' 2

oCOC5

i '( 1 i ! 1 i ! 1 1 1III | ! 1 1 1 j 1 1 1

;o ' 40lime [ rr i i n ]

Sample : FTL: A.UA.1.. Y Si:

fe t rument

y ' V l a 1

r\. D MI".' : 1OOOPE «S87-0o/o

Interface Serial * : 124857 07.5 Data f-.cqu.i BI tion Tin,e: r;./21 .-'92Delay Time : O.OO mm.End Time : 45.OO mm.Sampling Rate : l.OOOO pts/sec

Sa«* Data File : cResult File : c

File: c-rocess File?«iipje Fileleauerice Fiie

\27OO\data\lfiEL019. raw\27OO\d* t =• M AEL-M 9 . •- 5 1

\ 2 7OO \ ca a t a M 1 a e 1 -pre\27OOVda t =. . AR1 25-J . S.T-

i i Li t i o ;~t F a c t o t~

-oise Threultiplier : 1.0000

Are-S "!>.:-&•:•. riC-I d

C-i .'i = c-c- : 1 .- O.OOOO

nstrument Conditions:ac*ed Column 5C -InstrumentCD!umnZijlctAn Length" rrier Gas

_^^w Rate~e.7oeratij.reinjection Temp.

Detector temo:ores

rSllli.5::SP-22fo/i.?5::3P-2Ao:o'x 2mm on 10O/120 5UPELCCPORTAft/ME 95/5

250

tal Dumber of ?ea> s E-etec'=••-: IT

PRIMARY ANALYSIS

,.-**-. i".^-r~. j—iic-C- r,c.r Lj

".it ?*«« r.t Con:.

7?

...4U. H'T

9 6.635 1311C 7.592 ilC211 8.833 1430

1 12 V.567 413) 13 11.084 370^4 11.921 1530-15 13.537 164816 15.178 86817 17.161 80618 19.392 110219 22.752 5520 24.833 17521 27.754 9922 29.997 13623 33.S/0 7303

19527

Group Report f

Peat Ret Tine Peak Kt

^ ltin] [UV]1 8.833 14302 11.921 15303 13.537 1643

4608

794330254157254123 Arcl-1154 1107244399466482 Arcl-1254 277110 Arci-1254 34597541694676111702

111843BB311630

706325 DoC

1216433

or : AR125-I

Area Coftoanent[uVJsec] Natte

54123 Arcl-1254 1644S2 Arcl-1254 277110 Arcl-1254 3

197714

tl.6.1

•J'J i T t,» » ^C. / 0"r * t •?•? j'^ i». / jiBV 77.307

100.367VV 29.003VV 58.091VV 102.211VV 103.430VB 54.490BV 50.607VB 69.185SB 3.473SB 2.600:B 1.466ci. 2.764c.B 103.414

399.542

BL Extract Cone.nq/fiL

BV 100.367BV 102.2113V 103.430

306.009

14.62523.7lt12.73477.3C7100.36729.00358.091102.211103.43054.49050.60769.1353.4782.6001.4662.764

108.414

399.542

SatDJe Cone.uc/100ci2

100.367102.211103.430

306.009

-...Uip Report For s SURROGATE

:sak Set Ti«e Peat Kt* t»in] [uV]

4 33.670 7303

7303

Area Coirpsr.ent[aVIsecJ N'ase

706325 DBC

7D6325

EL Extract Coric.rl9/cl

SB 108.414

103.414

Sanple Cone.UQ/100Ci62

103.414

103.414

PACE, INC. PCS REPORT PAGE No. 2

l\t". '.a : 5. CO 1:1 t;rr.ot

i«t;.t i: ..-.-i.lite : S/2e/«2 ::.o» ?5:r.t : 35.Sifict sciit: 33 tV

t Fc:r=t sS. *V

r

'l>* &r -

,—v

t^ CNJ '•5 r-j-OT'-'iii i in ini I

—I

1I

1

55J

J I

50-

..I...':v.:..i-;."...i'..»---:v->

AI;! \

< <23

e [ rrs I n ]

i i40

Cicifnp) j fcr Nrtdife

Sample- NumberUc-tra t or

Instrument/rr?Sjf-t'-i toSamp 1 er

SyRack/Vial

rtKlJt.-4-ul

250bEN A

KS111PE AS330O0 / 0

i in it?Study

ilhanne 1 A

v* / *^ O / V J. _• . J

PCS ANALYSIS

A / D m V R & n q e 1OOO

Interface Serial tt : 1248574035 Data Acquisition Time: 5/22/92 .12:09Delay TimeEnd TimeSampling Rate

Fv'aw Data FileResult FileInstrument FileProcess FileSample File1

Sequence File

I n j . VolumeSample Amount

e ThresholdMultiplier

O.OO mini.45.00 mm.1. X>00 pts/sec

\270O\data\.rAEL020. raw\2700\d?ta\1AEL020.rst\27OO\d ata\11a e1.ins\27OO\data\llael.prc\27O0\d a t a\AR12 54.5 mp\2700\d a ta\11ae1.seq

2 MG/ML1.0000

61.0000

Area Reject : 0.00D i 1 u t. .1. o n Factor : 1 . 0 0

Area Threshold :Divisor : 1.OOOO



Instrument :KS111Column : 1. 5XSP-2250/1.957.SP-2401Column Length :6'x 2mm on 100/120 SUPELCOPORTCarrier Gas :AR/ME 95/5Flow Rate :55 ml/minTemperature :208Injection Temp.:250 CDetector 1 :ECDDetector temp :350 CNotes :

Total Number oi Peaks Detected:

PRIMARY ANALYSIS

s-.?'•T

Peaks

1•>345

Ret Tiae[ein]

2.C292.1922.3273. 3013.329

Peak Kt[uV]

£722315312351

Area[uVtsec]

i95142113221414i70

PACE, INC

Coeponent 8LNase

EVVVVBS3SV

. PCS REPORT

Extract Cone.^q/ftl

4.09415.44311.7593.i433.593

Satpie Cone.ug/lOOcrt

4.09415.44311.759S.44S3.5"S

i ;

1718152021

24

• cEV

i.542

13.53315.18117.134It.3*624.78S

lie*

372?

3?ol 18*624 fircl-1254 3132042

120254103035

141GE

70*5

v;vvw

vv

ES

r?

T5.S74

i-2.377

32.014

147.602

143.534141.754

178.572i.123;.5c>o

10-4.554

2!.574EC.543

^LIT-

22.014

147.t0224?.123248.534141.7!4

129.35517S.572

6.123

a.l"1M.554

:tii ?-Jt '.lit -tii H: Aret Ic*iOf.cflt rL Earict C:i [ita] io'/] [uVlitc] Kiu nc/cl uj/10Cc*2

2 ll.?32 372^ 165372 Arc!-1254 2 W 24?.123 24?.123; ;:.::: :H: is-?e24 Ar:;-::w: w 24E.5=4 -45.534

11252 494362 747.6?S 747.t>8

•Srcup Report For : SUPÔGATE

104. JS4

r-ACE, INC. PCS REPORT PAGE No. 2

Stirt Tiet : 0.00 tinSc«!t Fict&r: -1

Er.(! Tiw : 45.00Plot Offset: 3? iV

Cite : 5/2fc/92 13:19Low Point : 38.9& »VPlot Scale: 30 tV

High Point : bS.^S tV

>

'* c' Q.

<A<D

(T

i qr-J

MI

65 —

-1

1«J

55 —

50

i i i i i i i

-45_lij

~1 lii *

r , t.-t

SI!/ v (

eni

fc* A A7" " !\ A , Aj 1 (' 1 ' I / \

ii i\ A i i iW i I T \ / V VL*. .- •J-W-p/.-.r-.j-T—[-1-^ —"^ ^ "

40-

03

••»CM

I

> r.

7T

C-i

i

T Tin u~>CSi C-J

i Id dC*' !"'-'

oCOo

—i—i—i—i—i—!—i—i—i—i—i—ri ' ' ' ' i ' ' ' ' I '

10 20~i—i—i—i—r i—i—j—i—ri i i i i

Time [rnfn]

1 iTlt-

ANALYSIS

r.str urf.ent

ujtoSanip i&tcacl /Vial

: ^ c.l 1 1: f'E »i£3 .'••-.': O/«.>

i/I) niV Ran tie : 1OOO

Interface Serial # : l2-»S574O3f-Dela/ Time : O.OO miri.End Time : 45.00 tr.ir, .Sampling Rate : l.OOOO pts/sec

«cqui5itiori

Raw Data File : c:\27OO\data\lAEL02l.rawResult File : c : '• 27-'.1 • - ! • ' • - d« ta\ 1 A3"L v21 . rst1 nstf-imen t r i I e : c:\27-! '«' ' d.Htc- '» 1 1 £•£- ! . insF'rocess File : c : \27v.' -data'. 1 iael . oreSoflip ii •£- File : c : ' . 1? T'l •!• . cJ a t s \ ^F^ 1 2-i<!' . ~.n\ p

] r . j . Vc-1 •-•'«£• t 2 EiG. 'ooffipie i->(r.Gruri ; i . •-".''-'•-'

fc-i r \~ ci R tr j ^r C 1l

L'liution Factor

'«oise Thresriold: 6Multiplier : l.C-OOv

i-ires Threshold :Divisor : l.OOOO

£:u.~ich Factor: iAdder : O.OOOO


x Instrument9 Column

Column LengthCarrier GasFlow RateTemperatureI r. jection Temp.Detector lDefector temo

KSill1 . 5:'.SP-2250/ 1 . 9f.:-13P-24016'x 2mm on 1OO/120 SUPELCGPGRTAR/NE 95/555 ml /mm20S25O CECD350 C

r of Pesi s L-etectE-j: 1 c

PRIMARY ANALYSIS

Pr-i'_s;, !!<•_. F'CB F.'EPGRT

?tii :-r: Tile riii rt

* :i:.-.J :c»J

strict CORCr.s.'ti.

JI

.1.3

c5

.0

|iV 13

J44< cA j16

: s.ibs17.203n.44220.33321.30S2c.oc330.07333.63138.436

426220243543373347

347684

20563 Arcl-lleO 1iOOaO Arcl-1260 213172 trcl-1260 313-32374416229277

3317S1 CBC3298

v»VrrV

V«

rr36B6SBBB

t'^.i/i.21.86614.6473.267

1..325.45554.5901.324

.1.21.14..>.2.; .

c

54.i.:

/ »

347

73•Ji.

559024

5978 445420 186.157 186.157


Peai:t

123

set Ti«5t*in]

15.16617. 208li.442

Feat Ht[uV]

42622C" .. 7*.t .

fires Coftsorient[uVlsecj Nace

20863 fircl-12.0 110050 fir:l-12iO 213172 Ar:i-12sO 3

PL

BVt3EV

Extract Cone.ng/ttL

24.17421.S6614.647

Saapie Cone.ug/100cs2

24.17421.36614.647

359 44115


Peak Ret Tite Peak Ht Area Co.ponentI [tin] [uV] [uVtsec] Naiie

S 4 33.631 347i

347i

331781 DBC

331781

BL

EB

60.638

Extract Cone.

54.590

54.590

60.633

3aipie Cone.ug/100ca2

54.590

54.590

PACE, INC. PCS REPORT PAGE No. 2

C.-M t:t

r»;c i ct

tV

- let Q" :!:t stilt: 30 sV

(O**"> ' Z*

-•i x-tr

i i i i

i?O

5O—

•f*

•' i

o

i I i ;40

' " ' J

'.~j cl T: p : f- N

G [•;'••:•• at ort.l e I"

n«it •. r ume-n tH u t o S A in pierRack /Vial

nF< 12&<.••-Ol 1 792SPlOObEM A

KS111RE A38300

0 / 0

i i dieStudy

• 1 : A

: li/2c»/"-/2 J..:. :.: F'CB ANALYSIS

A/D mV Fvanue : J.OOO

Inter-face Serial tt : 1248574035 Data Acquisition Time: 5/22/92 01:42Delay TimeEnd TimeSampling Rate

Raw Data FileResult FileI n s t r • u rn a n t F i 1 eProcess FileSample FileSequence File

I r-.j . 'v'ol urneSample Amount


0.00 min.45.00 min.1.0000 pts/sec

\2700\data\lAEL022.raw\27OO\data\lAEL022.rst\270O\data\llael.ins\270O\data\llael.prcS 2 7 0 O \ d a t a \ A R12 6 O . s m p\2700\data\llael.sea

2 NG/I'1L1.OOOO

A r e a R e j e c t : 0 . 0 0D i1u t i on Factor : 1.00

61.0000




InstrumentColumnColumn LengthCarrier GasFlow RateTemperatureInjection Temp. :25O CDetector 1 :ECDDetector temp :35O CNotes :

KS1111 . 57.SP-2250/1 . 957.SP-24016'x 2mm on 100/120 SUPELCOPORTAR/ME 95/555 ml /min209

T'otal N'-ir.iber of Peaks Defected: 24

PRIMARY ANALYSIS

PACE. INC

Peakm

*

1

2

34

5

Ret lite[tin]

0.23i2.03?2.2032.3503.31S

F'safc Ht Area CmponentfiiV] [liVJsec] face

43 It?J2 4s2

193 1214122 113425 91

BL

SBSVV V

vsJE

. PCB REPORT

Extract Cone.ng/fiL

2.4392.951

10.9*2a.?301.433

Sample Cone.

u?/100ce2

2.43?2.951

•0.?426.9301.433

c ;. -ct * . -cC * -."* *^ *"t . 3 . ." . V J -•

i: i!*7: !:; i;**:-• •* • • « l ' i FT* ^£rt»4 * . * . V 4 9 .". J »^.**

. i: ::.:•: i:: «"5;; 13.437 l.'-e H'la

1' I5.isl !753 5S4j7 Arc!~l»oO 116 17.113 =55 53694 Srd-1260 217 19.354 1615 10M95 firti-l2eO 3

18 TG.bM 1199 :&3?3

19 22.935 51 94720 23. 4e? 76 196521 25.250 3«5 1897122 2^.9*4 1*45 I1759-:3 ::.»:: s"; c!:::s, ire.< -*-'a" **• i j- j--6

Ii*t! ir-3-''iis

îi fft :i» ?ri« Ht ftrej CctiOf.jrt

t it:n} [/*) JuVlje:] k<tT

: :5.!sl I7J8 S3437 Brcl-l2sv 12 !7.ilS 755 53494 fircl-l2iO 23 19.314 Iil5 100498 Ar:l-l260 3

4278 242523

oToUO Rerf.uiTt rCif i o--JriR<j-Jt-i • s.

:fii fit Tltt <E<t lit !<Tii IC-tSC&rT.t

cr '.-' •

r? :.::3rV " ••'•

B".' 5.3*0v V i 5 . * 5 7VV bJ.l^bVV ?6.395'."V 95.057VV 57.454

W 72.337

w 3.c;9VB 4.412

tfB 22.040rB Z2.73CJV 105.752Vtf I3.3i"?

t1. Eitfict 2tr.£.r.c/fcL

5V <!6.3?5

5V =5.057W 57.454

239.407

c. E.trtc: Zwc.

*...;i.i« j

• ••' • C

"* "4"

5.e40i5.45742.146

96.89575.05757.45472.337

3.049

4.61222.04022.738

1C5.75213.369

732. 227

C yi r. J g f jijv r B ^

00:100C(2

56.855?!.05757.;54

237.407

;iiUr tOi':.

105.75:

= r;CE, i:JC. PC5 FEPGRT FAGE No. 2

£ac:ie Kite : Hr.::sO-?lL7?:5PL

;ti't Tine : C.OC i:nS:c.;e "ictcr: -1

End lite : 4i.CC1 i.r,Plot Offset: 39 »V

=•15.e i: .vvjDate : 5/26/92 13:24LD* Pcir.t : 36.69 *VPlot Stile: 30 i.V

H i c h Poin t : 68.i? »V

c

5 O^ CL

CO

£

65 —

H60—I

55

50

45

III 1 1 1 II I I 1 1

~i o— !>Ji i > i i

4O

CO

I

V / \•-V--- '-•"

otpl'

i I I

O O QLD •£! LJ

CO0

0

1 1 ! 1 i 1 ! 1 I 1 ! J ! !

! i m e [ rn i n ]40

ie •i.=-t.!.,.-»

"iimer. t

/ Vial

Inter-face Serial *

t. r,-.r.r.el : 10'"'0

•atci Acquisition Tiroe: f-/22/*?2 02:29

Delay TimeEnd TineSampling Rate

ftaw Data FileResult FileZ r. E t r uf:'i€-r: t

r i » •^r'roce-ss File~>cifl!p » & r 1 4 e-

roce r i l e

*Joise Thrs-sr.oldMul tipl

O . OO fTiin.45. OO mm.

l.OOOO pts/sec

\27OO\data \1«ELO13. raw\270O\data\lAEL027-. rst• Z ~- '•'!> '• c!a *: > • 1 1 .^^ i . i f: B\Z7OO\da ta'\ 1 lael -p re\ to - • ' . . ' \ CJ c1 t. ct \ ?-if\ i ,^c '.• . ruTi

\27vv' -JatrrMlc-ei .sea

•-1 r e £« r-. &i . <.».•'.••-•

i . 00-X'

Ars-s ThresholdDi visor : 1 . O

Suncn Factor: 1


Instrument :KS111Column : i . 5V.5P-2250/ 1 .95:.SP-240lColumn Length :6'x 2mm on 1OO/120 SUPELCOPCRTCarrier Gas :AR/r:E =5/5Flo** Pate : 55 ml/mmTemperature :2O3Injection Temp.:25O Cdetector i :ECDDetector temo :350 Z

CT P'e&r 5 ^-r-t-^C^r-d: Z-i

PRIMARY ANALYSIi

PACE. INC. PCB REP3RT

?-Jt ":H rit Arei titract Car,:ns/*L

j j

5:10* *

12\ 13• it

15161718192021222324

5.1845.3057.9893.76611.18012.142 /13.453 J15. 163 J17.09919.33020.71423.40125.20326.54629.86633.59638.640

116156

9tl12s2

, :5i

2091283344312534417729904291746123041647526

• 2257

1614242322367335168331

122237116700231534 Arcl-1260 1145930 Arcl-1260 2264814 Arcl-1260 325258231982135766135603405290735935 DEC345416

r?S£BVVBBVVVvvvvvvvvVEEVVVVVvvvvVB

fc.67i8.86554.49471.60414.215113.599160.682251.311252.303252.058180.44325.870105.38519.30765.383123.83935.437

6.o798.66554.49471.fc0414.218

118.599160.692251.311252.303252.053180.44825.870105.38519.30765.386123.33935.437

40209 3052445 1785.335 1735.835


Ret Tioe Peak Ht[sin] [uVJ

Area[Msec]

CciiDDnentNate

Extract Cone. Sample Cone.uQ/100c«2

1 15.163 4431 231534 Arcl-1260 12 17.099 2534 145930 Arcl-1260 23 19.330 4177 264814 Arcl-1260 3

BVBVVV

251.311252.303252.053

251.311252.303252.058

11142 642278 755.672 755.672


Peat Ret Tise Peak Ht Area Cospone.T* Iain] [uV] [uVlsecj Nans

4 33.596 7386 735935 3B:

75=6 755935

t 3L Extract

JV 123

123

Cone.»L

.339

.339

Satple Cone.

123.339

123.339


'.&• Faint : ^.?' iV:::-t Btiit: 30 aV

\ Cf -

"S «

:I I i ii I i i

55-

Ji50

CO

iO

* <r~V. • l^v I

' ' - L : ' • " ' J

40

Sanole Namej.r«mpl e I Jumbo ri.) pt? rot. or

1 nst. rufiien t.-i1.11. o S a n I p 1 e? rRack/Vial

2*>bEtfA

KS111f-i- AS8300O / 0

I .1 meStudy

C, h an ;•)(/:• 1.

ANAL'r ;S !i 3

A /I) r:\ctnne 1000

Interface Serial tt : 1248574035 Data Acquisition Time: 1T./22/92Delay TimeEnd TimeSampling Rate

Raw Data FileResult FileI r 151. r LI m en t FileProcess FileSample FileSequence File

Inj. Volume3 a in p 1 e A m aunt

i.Ee ThresholdMultiplier

0.00 man.45.00 min.l.OOOO pts/sec

\270O\DATA\lAEL024.raw\27OO\data\1AEL024.rst\2700\data\llat:l .ins\27 00\d ata\llaei.prc\27 0 O \ cl a t. f.<. \AR1262. s m D\2700\data\llael.seq

1.0000

1.0000

Area Reject : O.OODilution Factor : 1.00


B u. n c h Factor ;Adder ; 0.0000


Instrument sKSlllColumn : 1. 57.SF-2250/1. 95XSP-2401Column Length :6'x 2mm on 100/120 SUPELCOPDRTCarrier Gas :AR/ME 95/5Flow Rate :55 ml/minTemperature :203Injection Temp.s250 CDetector 1 :ECDDetector temp :350 CNotes •;

Total Number OT Peaks Detected: 17

PRIMARY ANALYSIS

Peakat

,2345

F.et Tifte

[sin]

2.044

2.200

4.305

5.1355.7S3

Peat Ht

[aV]

2711121

25173

PACE

Arsa Coapensrit

[sA'tsec] Nsiss

204653903331

2393

. INC. PCS REPORT

3L

B3SSrB

BS93

Extract Cone.

ng/eL

1.979- §.2i9

1.524

1.86313.243

Satple Coric.

UQ/L

1.9798.2i?

C-tJ. Jif

.963

13.243

£ <:.:!.

V.' '.

;; :.^.

^ ; 5.* '.

;5 "9.16 ..3.17 38.

Group

real til '.* Ii:s

• »^ •

; 35.

;j* ;: :5:?s:;3 <: 15717:!!• :: :;;9':tJ: ;?* '»j;: A'dii::-:;?: :5 ;:?:333 1*5 &7S1jte oe 2'i~!'.

"SS *5e :5!63 Sr:! Hr2-I598 3549 337430 DBC719 254 19225 ftrt!-12i2 1

7139 SSiOBb

F>'eport Fcr : Aki2o2

iM ?ea» HI Area :su*»rt• Jevj [ jVlsec] !.«*

rv^1 J- v ^*rc l llw.~^cw w 0 nri.~4.b. .

vv.i5v.'cr?FtHi*

III

9BK

SL

* *.V

'••'

Tj.lel31.39615. 70S35.?;:

c c ^~J . J • *':.e<2

;.<i-;30.52252.69327.332

326.779

Earid C3r,c.r.o/tl

,. ,^..

.-.?:c-c.o:.c

37.16:3:.3?S15.70235.9*75.573?.6<2;.*o;

35.58252.69327.B02

326.779

3«§9!fr Core.U0/i-

^ ,.,

V • -V"*'

•i.c-::-

o.oco 0.530

oroup rt For : SURROGATE

?nl tit lite Peak Hi Area* I«:r,} [kV- [aVJsec]

3549 337*30 CSC

337430

Extract Cone. Sitple Cmc.

r«Cc.. : : JC. F'Cri REPOR

lu'.'.t Mt.t : ;..:

sti". Ti»e : 0.0

St'

1

65 1

1

-i60 — I

i , J

'| ]

<U 55 —t CO ,

'§ -1Q. -\'•ft —.Q 50_|i r

:|J j-1

t i' i45 .i*

; j— iil

-

~

40 —

i

»

i

1 it u

;;;"01iJ5;f!: . ,. r. *"t;! I!,-""--. .,..-, M« i -• i

0 em tr.d 1:iie : i'.CJ tin Lot. Psint : 3(i.2Ti iV Hioh foint : 6?. 29 i1,•i:t " f 'set : !? iiV - l e t :Ca \c \ 30 *V

--• c- c- --c o -x> f"i r^- o o -'-4f »— CIO D3 — -?" Cv — '' ' — ' ^1 ~~ ^^ CC' \~—O N^t-^ C ' ^ j -J ^ f- " X fi-\ LTJ j ' rr, f.-j 2C3•NJ W lf"jrt t T— ' • »— '7-j *>,' ^VJ -7-*J "-.J M l K^

*\\ ill 1 1 1 1 1 'l "l 1 'i '" l' i

A.• i• i

IS""! 1 '.

r\ tir _ ^ i V \ "*^ i-^ A IfcV ---'"" "•'T1""%._ -'"kS. _-_ ^ '"'""X. -^- -.-_ . \f^ '~ ''-9 » ^ \ "*^ -- ' . -r '

^-T'7 ! ^ l s r . i , , . , . - i . . . - - i

ci ! i i

1 J .^

s s §*~ ^ '7"^ 7-^ t* -j ^

iV ;v: (S , :

-cj ^ Q -5

! ! i 1 ( 1 i ! i : i i 1 I j i i '' i i ! i i ! j i 1 ! 1 j i ! 1 1 i i i 1 ! j I ! i: 10 ! 20 ' 30 ' 40

i i rn e [ rn i n ]

; T - ' .C - r.'-ê- : iv.'L>i:.-;.•: ..tor ; Lf'i-i

£tud>-

j .'i£.t:' u«*C-.'i t A. I? tiV Rr.nne : 1OOO

Ir.ter-face- Serial * : 12 4 85 7-1 M7. 5Delay Time : O.OO :rin.End Time : 4 5 . •-">•> rT.in .Sampling Rate : . OOO-:; ots/sec

i si t ion Time: S/22/9L:

Raw Data File : r:

] r-s t •- ^rêr-1 r i J ->r l OC'îi- ^ ••'" 1 t tr

\ 1 7 0 v \ d a t a \ i A £ L .' 2 ?,27*:-O-vdat5M"EL-: Tf.. rst

••.2 '."• :•'.• . dr- to '-. 11 jc-1 - =c-

2-i I u t j. c-- ;.?-. t

r e c t o r

ip 15« 11 v i = or : I. OOOG : O.OOOO

n51 r _uneri t Cc-ridi tions :acked Column 5C"-InstrumentColumnColumn LengthCarrier GasFlow Rate

' •=•."•• D

KSlil1. 5V.SF-2250/ 1. 95:.5P-24016'.-s 2mm on 100/120 3UPELE.GPGRAR/ME 95/555 ml / miri2O 325O C

PRIMARY ANALYSIS

rCB RtP

-ti« rf. .»f -rii -I

.' J1. . . *

c3

10^ 4

1

13^ :41516171819202122

1 . vil

:.=54£.'4:™ • C«. i

12.20013.A3S15.14217.18419.26720.63323.42125.21729.87033.57938.728

«»

IA:12513".

73;7;S

1311740

10161758131566190876181197

OCv

2-7;4:4;4AS73!420j i .. . "t649914C38153406136471 Arcll262 -1

5179',0400153047 Arcl 1262-2726100 DSC201614 Arcl-1262 3

I 4

; (

V::r8V1C >V V

vvf VvvV8BBBBBBBBfiB

* . .- -

1C. 54513.96314.17554.23759.2iO98.03554.93275.380130.5059.68441.975127.267113.090131.013

. . ,. . ,

IV. 5«5

13.96314.17554.23759.26098.03554.93275.380130.5059.68441.975127.267113.090131.013

19035 1511261 992.149 992.149


Peakt

I

124

Ret Tiaelein]

20.63329.87038.728

Peak HttuVj

175819081197

Area[uVlsec]

136471153047201614

LDisanentKaiie

Arcll262 -1Arcl 1262-2Arcl-1262 3

BL

BBBBBB

Extractog/i

130.127.131.

Cone.1

505267013

Saiole Cor.:.uo/L

130.505127.267131.013

4862 496132 388.7E5 338.785

'{Group Report For : SURROGATE

Peak Ret Ties Peak Ht Area4 [sin] [uV] [uVlsecJ ?>a*E

Ext rac t Cone.nq/flL

Sifiple Cone.

ug/L

33.579 7613

7618

726100 DSC

726100

113.090

113.090

113. 09C

113.090

-'ACE. INC. PCB REPORT PAGE No. 2

: ::-:*:.-.iiti-.:.ck::!.ri»: ..,& §;•• tr.l *.it : *!.-!• ti

'-. -'. ' let Z t ' s e t : i. i.

5::5/?: 11:5;

;;•. S:ilt: 30 iV

-IJ

*."". > X-

I'Tr cf>I . i I I i i

<%• n— C" '-I' •=*• Cv

i i ; 1 1W'l

I

-y 5.

r.T'-

f •

i i i • i

i^t rumen tpi u t o 3 <':? in p 1 e i'•: a c:.k/Vial

i a meStudy PC LI AN At. V 3 I 3

KSl 1 1.PL i~V;::;o3OO'..) / (D

A/D Kc<i:cie : 10OO


Raw Data FileResult FileI n s t r u m e n t. F i 1 eProcess File3 a. Tip. I e File:-j e q u e n c e File

.( l"i J . ' C) .:. L.i u'l':

Sample Amount

ThresholdMu. 1 tipl ier

0.00 min.65.0Q min.1.0 0 0 0 p t s / E e c

c \2700\da ta\1AEL033.raw\270O\da ta\1AEL033A.r s t\2700\clata\liaeJ. .ins\ 2 7 0 H) \ d a t a\il a e 1 -pre\2 70O\data\Arl262.smp\27OO\data\llae1.seq

1.0000

61.0000

i-i r £„• a R e j e c. t : >j . 0 0Dilution Factor : l.OO

Are a Thr eshoi d :Divisor : 1.OOOO

Bunch Factor: 1Adder : O.0000

Instrument Conditions:Packed Column 3C -

InstrumentColumnColumn LengthCarrier GasFlow RateTemperatureInjection Temp.Detector 1Detector tempNotes

KS1111. 5XSP-2250/1. 95'/.SP-240i6'x 2mm on 100/120 SUPELCOPORTAR/ME 95/555 ml/min203250 CECD35O C


PRIMARY ANALYSIS

Peak Ret Tue* tiin]

4 -•"• "• f-- 7

2 2.202

] 3 2.613

-. 4 3.331

.. 5 3.366

Peak Ht

[uV]

4926437

90

46

PACE ,

[u'vlsec] Naae

j.'2

4330527

693

I NiC .

BL

ts3VVBSB3V

PCS REPORT

Estract Cone.r:g/sL

3.6i219.565s.473i.6903.419

Satple Core.ug/L

3.66219.5656.4736. =903.419

t

:;.• *

i i j- *;5

1617:6;920;j

nj^.

=«

. . CV

s.i:4. - -« •

;:.«2:!.::i:7.2W1?.33220.76723.43925.539

26.6833C.C0833.71332.K3: 2.597M.983

»« *

35*• I.

. . •-

ii:i;3?5:37?18633-M*29

164210C<357553252167

15&

a;?;

Hessei~"

5321-7121:43£27'-

1152372599S1 Arcll2o2 -1283«5

1275568C831

35513C fcrcl 1262-2542374 DSC>6c7*. S ftrci***.si-. v

-• v.1 * ,•

l-J3w4

f f

.f^ ; •

»v;v.V

vvvE£VVf f

«WwVb

ra

rB

i. . . » J

;:-.!<£t ? « "

109.1621".793jl'i.-'O-

! 32. 271236.670

31.331121. S71

67.013233.539

79.G52237.260

6.3??OT. i4B

2l.C-«53'j.5-o.. £--

K'9.1i2177. 7?3102.3o3533. 27i236.67031.831

121.871

67.013238.53579.052

2'37.I60= .3n!

si.Wc

• >^r • • •

1x

*

2^.76730.0C3:i.sos

318935752167

11*<

Ji

^

8930

259731 Ar:11262 -1355130 ftrc! 12S2-2368929 ArcI-1262 3

984040

BE«

237.26C 137.2e

712.465 7-2.*6?

<;} rteoort For

HIiiic

Estr jct C»:.

-~'.--uc.. j TJu . r UB r-.'iir'Gf'T r'j-ioEI -*O. -i

)

: ::\27C'Oii«:a\lfiEL033.rii«Stirt T-.ce : C.OO tin £ni lite : bl.COS:ile Factor: -1 f'iot 31fset: 30 i.V

ali»lt t: .jvr

ite : 5/22/92 10:55SI Faint : I?.59 tViat Suit: 30 *V

Hi3H faint : 5*. 5? iv

r

CD(rt

CL

a:

&i5 ry

-J

—i

45 —

40—,

—:«

Ji'i^

30

cq CiOin <?2GI I I

c o .'•-1-

rn

. ;'. AMA A f i A M \

/ \/ \; W v / '• \i. ! / \

\ i \.

CMv

-I'l L.-wy^fl^-VT-

ir11

1!

i

i

jII i 1 ! i ! !

0

"-^r"!*-> — r I"H !' — •] — f •'t — j r~'4 • .-*rS. >•»_ J_^T-_ .-•"" ^^

.' ! 1 i' - • -N

:>; 1 , ID

^ ^ 7

. : iv 13 '-"?'^ ^ 0 <

1 ! 1 1 I 1 M | 1 1 M | i 1 1 ! | I 1 I 1 I 1 i 1 f j i ! 1 ! | II 1 1 j ! 1 1 1 j ; 1 ! i j 1 1 1 i j ,' ;10 ' 20 ' 30 ' 40 50 ! 60

~T : .-.. ... r .... • .. "i, ; f ; i & L r i , i n j

.'tic.-'

: , , 'r-l L-:I-— • ' • • <-.-. --*•

1 SI 1 1

-.1

i I lit I 1OOO

Interface Serial « : 12435T- 4-.'7-f- D^ta ricc|Liisi taon : 5/21'/v2 18:^:2Delay TimeEnd 1 inieSampl ing Rate-

Raw Data Fi leResult F i l e] n^trundent J-i

F- rocess F i l er>a.vif>; =• Fi: ~

ce Fi le

C>. <X> IT. i n .

1 . Ov'X1

C: \27O« >\DATAM AELO:-2. r,

• •dat^ \ ] .AELo72. ' -<'. un '.£> ' 1 i --ie- : . i ns

. Gi t ^ . 11 =••=• i - p r e

[.' i 1 u 11 on

rires T h r e s h o l d :Z-i . isor : 1 . 0-O'I'iJ Adder

h Factor: 1O.OOOO

t Conditions:ecJ Column GC -

Instrumenty Column

Column LengthCarrier GasFlow RateTemperatureInjection Temp.Deteeter i

i . 5'/.SP-225O/ 1.95:-:SP-24016'x 2mm on 1OO/120 SUPELCOPORTAR/ME 95/555 ml/mm2O825O CECD

PRIMARY ANALYSIS

F^CE. i:.;C. PCS REPOR"!

:Jii rrl "itr

* it::}

4415

rr;i-.. . i

I 4.245 !?15• 4.631 2357

10 4.9<8 162011 5.2S4 2373

1 12 6.220 1352••""•M3 fc.s40 1540

,'IH 7.768 ir7015 9. ICO 115416 11.115 23017 11.968 35818 13.554 374

19 15.263 12620 17.173 16421 19.658 4922 26.868 2823 30.015 5324 33.757 5352

34770

Group Report F

1 /Peak Ret Tise Peak Ht

t [tin] [uV]

1 2.621 24382 3.318 34233 4.245 5915

11781

Group Report F

Peak Ret Tine Psak HtS [sin] [ U V3

4 33.757 5352

^ 5S52

82078 ftr:l-1242 33612221690594o23S45132767£267:41813110661290616507

582266552643

6671330

561899 CBC

1117355

or : AR1242

Area Component

[uVtsec] Name

23749 Arcl-1242 133073 Arcl-1242 282078 Arcl-1242 3

143900

or : SURROGATE

Area Coftoorient[iiVtssc] Nace

5613" DEC

*""

V t

VV

vv< Mli i

VVvvvvV'BBVVVVV

VBEBBBBBBBSS

BL

BBBVVV

BL

SB

206.80833 .4685i.65551.95064 .74453.33563.33140.3508.024

12.53013.078

4.4055.7420.7260.4210.856

36.870

1315.290

Extract Cone.no/tiL

134.055195.940206.803

536.603

Extract Cone.ng/fti.

Sa.370

.*: 1 rT.A

03.31'J

2Ct.80cS3. 46556.655

22.95064 .74453.33568.38140.3508.024

12.53013.078

<.4055.7420.7260.4210.556

£6.870

1315.290

bdfiple Cone.

ug/L

184.055195.940206.803

536.303

Sacpie Cone.ug/L

36.370

S6.S70

r~i r-» , P~. r~ i~' *~* C' "i~ r"1 A r~-1— K I — •—«r ut( Kbr uK i r t-;cjn i^ltj . î

s»i:.t

c:i.* *:::•£:.J T•'let

.:s tV

T ^J-c-^tO !*> C~Itflllll II I I

HiI!

•:"> Cv

••"• inrr. . > «^

LT c Kî' i i

V4O

. •- , î i t- x~. i j^» jt _ • < • • - • I J

.:::<:* n>p 1 »-• Numb«:-rGn'fi-r at or

' Ins t.rument.•"*"S i:i u t cj S a m p 1 e r••^^ R a c k / V i a l

Mr\ll'-'4 I1'- '.''""-'CjV _

LHA

KS111PE ASS30OO / 0

Study: I-/,..://v.,: j..::-.•. PC LI ANALYSIS

A/ D mV .1.000


Raw Data FileResult FileInstrument File-Process FileSample FileSequence File

inj. Volumeb' a m pie A m o u n t


0.00 (Tiin.65.00 min.l.OoOO pts/sec

\27OO\data\lAELO39.\270OX d a ta\1AEL039.r51\2700\data\llael.ins\2700\data\llael.prc\27OO\data\ 11 ae>l . smp\2700\d-3ta\llael . seq

'Z N3/-''!L1.OOOO

Area Reject : 0.00D i 1 ut i o n Facto r : .1 . 0 0

61.0000

Area Threshold : 32Divisor : 1.0000

B u n c h F a c t o r : 1Adder : 0.0000


InstrumentColumnColumn LengthCarrier GasFlow RateTemperatureInjection Temp.Detector 1Detector teviDMotes

KS1111. 57.SP-2250/1. 957.SP-24016'x 2mm on 1OO/120 SUPELCOPORTAR/ME 95/555 ml/min208250 CECD350 C

Total Number rA Peaks Detected: 2.1

PRIMARY ANALYSIS

PACE, INC.

Peak Ret lite Peak Htit [tin]

i 2.1612 2.3123 2.5974 3.0435 3.2S9

iuV] [

45?t43

270?3533827

fires CoapcnentiiVJEec] Kate

37035t23

25372 Arcl-1242 i369544979 Arci-1242 2

BL

3VVVVEEVVv

PCB REPORT

Extract Cone.riQ/fil

34 . 307-, 4S.922204.52220.200218.772

Sanple Core.ita/V.;

34.30743.^22204.52220.200213.772

c i.^2 2~!1 <ic2e

14 11.666 *86 20040 Srcl 1254-217 13.471 <19 20018 ArcI-lIW 318 15.U2 3« 3ill f,rci-S2oC 1

:? 1M47 159 S53i :-:l-l2b<J 228 1».295 52 1182 Src.-1-Dv. -21 33.533 5952 578602 &BC

"M- 1273^2

• ^> I*'* *"*iT'f **rS"*" * r*" -*"* I " " '

" * ""iS "JT^T tiQT3 *r-?- '**i" "*

3 J.Tit MO* ?2276 Ar:l-l242 3

::?*o -£si27

Grouo Report For : AR1243

:nt ?-tt T:I* ?nl Ht Area CocKri?nti :*•:£] [cV] I'jVlitc; Xue

- :.237 273? 73S57 J-c:-12is :

: =:3 r*s :n;;; ;;;i-i:!! ':a-:l 24'47'

. rc.". "... "sc-i.-f"* f lir : i-'t- ' IZ^-J

:ril fit ";K -iii rtt A.-ci litc-or.Fr.t• ii:s} :tV] [-.Vt5%:] Kite

: :.;:: -i ; ;r: :-::-:

: ::.:•: *:5 :x :s ; r=- :M;

•« Jr.".?:?

TV lue.StB

VV 25.600

VV 26.201

Vt 5.30;

BB 15. £11

•S SS.3?4

1771. ef-i

I-L - i t^ ict Cert.rc/tL

?t 204. '2221E.772223. E?7

cL Estre:t Csnc.fiS.' 11

!«.<•:?• - ..B.-3-

-CT /•• '.3.'." . Ul'7

cL Ef t ract Cciic.

O.vCO

'%>• .-. ,^?5't.Kl

--

'6.312101.e!-7

3*:.°2e

114.1 £Sa.3:i5

25.60032.45526.201

5.W-1

15.811,.!j3

2E.394

.-.,. fti

EiS:;e C;.£.

223.397

ia:le C«c.

1^3. ?2;

10i.iE2

lo/is

:-.;;)

££!'

i- - - .

?-£vJjT* For : i-i

it *:ir :ee» -t*. ^rfri

1C 5.1CI 3s11 7.1:7 15i'i: 9.:?; 51

279

3el! fir:l-:leO 1 VtS536 fird-liiJ 2 EBHE: Rrd-i:60 3 P&

1 j v' 4. 1

5.001 5.001

15.611 iS.fll3. '3E 3.136

23.949 Z3.?;9


Peak Ret Tite Peak Htt [tin] [uV]

13 33.533 595::

5952

Area Cotponent BL

[uVlsecj Mace

573602 DSC EB

573602

Eiitract Cone. Satple Cone.ng/fiL ftg.'kg

83.394 63.394

83.394 88.394


sit;It

•:«r*. i-.u : . v. Er.i 'it* : t ' .C^ t:«?It! j '*ut: It •»

•. 5;:?;?: ::

: -

r ": "e.08 tV

40.

_ I -i.r:'-

— \

rs. JC• ^J. — T O O O

e s_ • ~i60

p J t-Dior a tor

Instr ument.Vi u t o S .-_• id p 1 e r

JK...K

F.MA

KB 11 1PE AS33000/0

T i iiie31 u c! • •

Channel

';.i/ L'.s/ 92 1O: 56rCB ANALYSIS

A/I) m'v

Interface Serial tt 124857403: Data Acquisition Time: 5/23/92 13:13Delay TimeEnd TimeSampling Rate


Inj. VolumeSample A mount

'Noise ThresholdMultiplier

O.OO mm.65.00 min.1.0000 pts/sec

\2700\data\lAEL049.raw\2700\data\1AEL049.rst\ 2 7 O O V data \ 11 a e 1 . i. n 5\2700\data\llael.prc\ 2 7 O 0 \ d a t a \ 11 a e 1 . s rr, p\2700\data\llael.seq

2 NG/ML1.0000

61.0000

Area Reject : O.OODilution Factor : 1.00

Are a 1hr es hold :Divisor t 1.0000

Eiunch Factor: 1Adder : 0.0000


Instrument :KSillCo lumn : 1. 57.SP-2250/1 - 957.SP-2401Column Length :6'x 2mm on 1OO/120 SUPELCOPORTCarrier Gas sAR/ME 95/5Flox-J Rate : 55 ml/minTemperature :208Injection Temp.:250 CDetector 1 :ECDDetector temp :350 CNotes :


PRIMARY ANALYSIS

PACE, INC

FsiiS

i

2345

:c. 7.re

[tin]

1.3862.1652.4442.6273.454

Peak Hi[uV]

1361309

5510S207

Area Component[ uv t seC j NaSe

75411323

252SO? Arcl-1242 1

2299

BL

BVVEEoS3EB

. PCS REPORT

Extract Cone.riO/*L

10.29793.8334.1353.140

11.S27

Saeole Cone.tg/kq

10.29798.S334.1353.140

11.327

«.::. ;:- *i«. tr c.o.e i.77« l.w 953* oc 24.?::5 e.*i2 tJ 75; fi 2.7?8

;i is.IES 3" I0c" rr *.:0!-; 11 i'.?l7 ilv O'flj [•» 12.3*4

x-^ :2 2t.»3i ;«: 22:4? ?& ;o.«2o:: ;:.?;t ::: ?5>>3 tic ts LSI/

i3W 80*92 122.123


?»L let TIM Pfii Ht Area Co»o»wt K. Eitract Cone.i [•!>] [«V] [uVlsec] **M ng/tL

: 3.3J1 <) o Arci-iN: 2 r; o.ooo; <.250 & 0 Arci-1241 3 '.'.' 0.000

I-K 50? E.Uy

3rou«o Report For : AR12-JS

Ftil Ktt lit* ?e*t Ht Area Coapcnefit :L Eitr.ct Cone.1 i«:«j [nV] [oVIstc] Ri«e ng/tL

* 5.2W 0 0 ;»r;l-!:«9 I W 0.000^ 5 7.7M 5 C Arel-:2«a 2 W C.OCC

7 f.MO 0 0 firci-12« 3 W C.OOO

0 0 0.000

Sroup Reoort Por : AR 12^-4

ffjl «t Tiw Ftil Kt Area Cc*&3«ef.t SL Eitr«:t Co-:.I ll.l', ;*.; [LtlSeC^ Sifrr TiO/tL

i ::.?;* i ^ ircl ;l:^-2 ;.' o.W'O? ;!.:*•; v 0 irc!-l2'< 3 W &.i'M

i j G.Ovu

Group Report r-or : AR12o'.'

:6 :i.lt* j ) r'c'i-I2ev 1 VV 0.000:; .1.1*1 -j i Arci-::-o * .v j.cco11 ll-tC* -J 0 Arcl-IIiO 3 W 0.000

2.793

1.617

?•- P3

Satple Cwc.

B '£,-

0.0000.000

£.1*0

£i*£.:e Cone.N/kc

O.OC-JC-.OOO0.000

C.OOO

3«i5ie Con:.M/ta

O.CC-0 ^

C-.OCO

i-.-iCO

K/L3

O.OvO

O.-JCO

0.000

o.:.., o.soo

Pe«k Ret Ti»e Pe«k Ht Area Cotpoiunt SL Extract Cone. Staple Cone.t [tin] [uV] [uVUec] N«*e nq/tL tg /kg

13 32.994 122

122

9500 DEC

9500

BB 1.817

1.617

1.617

1.817

PACE., INC. PCS REPORT PAGE No. 2

stir: ":« :S:.3t riittr:

ir-C T;tt : t'.OO t:Hot C?f«t : 25 iV

Lite : i-rs/72 K-:i6l.o» Fort : :!..1B »VFlat Suit: ;C »V

§V

55

II ™ LTi co •I * . • .— ~^— •<*«I . ^ .

HI II I II

1

H

: I

i f

oa

il

•I

-iH

40

» I t I ! I l l I I

r O ~ O

sime [ rrs

SampleSampleOper a tor

Instrument-'"TX A u t o S a m pier;'jRack/Vial

EHA

KS111PE ASa30O0/0

T i cii eStudy

Channel : A

: l' / xJ6 / v A: .1 i.i::..->: F'CB ANALYSIS

A/D fiiV Range : .LOuO

Interface SerialDelay TimeEnd TimeSampling Rate


In j olumeSample Amount

I Noise Thresholdhul tipl ier

tt : 12435740350.00 mm.65.00 rnin.1 .OOOO pt=5/sec

Data Acquisition Time: 5/23/92 14:19

\27OO\data\lAEL050.raw\2700\data\1AEL050.rst\2700 \ c.l a t a \ 3 1 a e 1 . i n s\27OO\data\llael.prc\27OO\c!at.a\ll£tel . smp\270O\data\llael.seq

2 NG/ML1.OOOO

61.OOOO


Area Threshold :Divisor : 1.OOOO

B u n c h F a c t o r : 1Adder : 0.0000


InstrumentCo1umnColumn Length

' Carrier GasFlow RateTemperatureInjection Te^mpDetector 1Detector tempNotes

: 1. 57.SP-2250/1.957.SP-2401:6'x 2mm on 1OO/120 SUPELCOPORT:AR/ME 95/5: 5 5 m 1 / m i n:203:250 C:ECD:350 C


PRIMARY ANALYSIS


Fed

*

1

2345

'i net Tide

[ein]

2.1602.309

2.5953.03S3.284

Peak Ht[uV]

441653

2S37250

3974

ArealliVUfC]

3S745523

2B542"V r. "•: ';i-i-i.*.

43915

ConponentNats

Arcl-1242 1

Arci-1242 2

BL

BVVVVEtv

VV

Extract Cone.ng/nL

33.300, 49.700214. 1S5

14.2S3227.124

3a*ple Cone.•g/fcg

33.30049.700

214. 1S514.2S3

227.124

;

. ;*'• 14

1516171829202122^ J

24

c •«

T.i?»

<».030

11.060

11.831

13.421

15.019

17.117

19.3SS

28.372

30.163

3:.4S5

44.177

ii2!3l!2«528543541884

236ISS2977

e4I** •**j

3345-)

21472

225SS ftr:!-:H6 I

45035 ftrci-l2;3 3

13879

15381 Arcl 1254-2

17848 Arcl-1254 3

3393 Arcl-1260 1

14120 Arcl-1260 2

14716 ;rc;-12i>0 3

951453?

622743 IsZ

1536

: 2233: 5

» »

'.'cii

WVd

3r

W

W

VB3VVB8VVBr£

SB

14C.023

77.309

; 09. 444

107.93019.06429.02826.2004.917

26.58319.3490.4321.33o

95.S300.&39

17«.W1

91. SSI

1C2.420

140.023

109.295

77.309

109.444

107.930

19.064

29.028

26.200

4.917

26.583

19.349

0.432

1.13&

95.HEO

0.639

;m.«i

Grot'p Report For : ARl2-t2

?fii(

12

^

Kct il«e

i««3

2.5953.2864.204

?i«l tit Area !c*p30cr.t al

luVj [iiVlsec] Kiie

283739746644

13455

Group Report For

?«1

*<rj

?et TIM:t:a]

5.233*.a?l

'•^

Feat stI*'! ;.

2493

::3!::H;

28542 Arcl-1242 1

43915 Arcl-1242 2

90133 Arc! -1242 3

162589

: AR1243

Area IO*X*K.'..Vliec] \*K

54964 Src;-i:-42 1£2S:5 vc:-i:;j 2«K:S ;r::-i:«s :•

K

v;w

a

•irTC

,'r

Vc

Eitr.ct Cone.ng/»L

214.185227.124232.300

673. oO?

Eitrict Cor.c.r.j.tL

140. C23109.444

Ivr .9^0

jdijir tone. ^^,•g/tic

214.185227.124232.3W

673.609

Sitsie Cs^c.ti/'ic

14C.C2310?. 444107.930 W

IS2337 357.397

i^roô Reoort For : A?

r**i êt 7;** rtil *it ^rei« * • - - * i „ •" ****"'• j 1^* j ViK

Ertrsct CMC. Sitde CST.:.

i s. »i; ;: ;;.o3I i"5? 13.421 41=

0 ir:Ilieel AT:!17343 ircl-

.1-4-1 k"? 0 .-*i--J ni -»^

-£!• -fl *f-.••• J «V iS.

:•?•) c.c-ocC2S ".0"3200 2i.:c-?

'

l-Eik *et I'tK r'EU HI

»

101112

i — - —

nffci LGipOneni tL

[tin] [uV] [uVlsecJ N»t

15.01917.11719.385

E4236188

3393 Arcl-1260 114129 Arcl-1260 214716 ftrcl-1260 3

VBBVVB

ts;r«c: Lone.ng/»L

4.91726.58319.349

o«*Bit tone.tg/kg

4.91726.53319.349

50.£ 50.£

Group Report For :

Peak Ret lite Peak Ht Area deponentI [§in] [uV] [uVlsec] Nate

BL Extract Cone.ng/iL

Satple Cone.ng/kg

13 33.485 6457

6457

622748 DBC

622748

95.880

95.830

95.880

95.830


O.OC- £no TIM?!ot

»vlot Stiie: ;0 »V

high Point : ;S.li

I *iiimii*Ti'i "i i i i i i i

•_/.' r-,

45-

4O 1

II

_ f

if

T o ^~i u"> -J: ± -Jjr^ CM ?si r>.

1 I

- • "

i_

f- • -il-^v^> y^S I . V~. : i^ I

' - L J

diOt Vwar il it- I

, t- r t, -i LJI i : .• . ... .'.'t. •..• j. .

AF.1242-O5O692SFL•sample NumberUi.jF-r ator

\I fi t . t. f Uf l i&r: t

"fy n t o S a HI p 1 e rF<:ack/Vial

250L

K.SJJ1PE A383000 / 0

T 3 meStud-/

Char.ni?! : A

1 1 :?.-1PCS ANALYSIS

A/D Ranat? : 1OOO

Inter-face Serial tt : 1248574035 Data Acquisition Time: 5/24/92 04:43Delay TimeEnd TimeSampling Rate

Raw Data FileF<esult FileInstrument Fi.l&Process FileSample FileSequence File

Inj. VolumeSample Amount


0.00 min.65.00 min.1.0000 pts/sec

\270O\data\lAEL063.raw\27OO\data\lAEL063.rst\ 2-7OO \ d a t a \ .1.1 ae 1 . i n s\2700\data\llael-pre\ 2 7 0 0 \ d a t a \ 11 a e 1 . s m pS27OO\data\llael.seq

2 NG/NL1.0000

Area Reject. : 0. OODilution Factor : 1.00

1.OOOOArea Threshold ;Divisor : 1.0000



Instrument :KS111Column : 1. 57.SF-2250/1. 957.SP-2401Column Length :6'x 2mm on 100/120 SUFELCDPORTCarrier Gas :AR/ME 95/5F1aw Rate :55 ml/minTemperature :20SInjection Ternp.:250 CDetector 1 :ECDDetector tetr.p :350 CNotes :


PRIMARY ANALYSIS

PACE, INC. PCS REPORT

Peak*

123i•t5

Ret Titie[sin]

0.214.159. ;-CS.595.033

Peak HttuV]

3i5407502934449

ArEc Cosoonent[uVlsec] Si&e

475iOi3t27232620 fircl-1242 14651

BL

B3BVVVVEEV

Estract Cone.riQ/fiL

2.71340.7615i.i3i221.47425.651

Sasole Cone.ttj/t.g

2.71340.7615i.s36221.47425.c5i

e «.2t* o5~«• *.!?: ;3*

:< t.iV lee

11 i.232 «3ln i«-12 a. lie j«6

\ 13 t.i:? CZ!1* 7.6?5 51615 ?.£lT li?l

16 11.025 45*17 11.836 56019 13.478 458

19 14.953 5920 17.048 20421 1«.269 6622 30.058 9723 33.«35 s*<"

«*::

Grouo Report P

ftil Sti TIM reit rt

1 !•!•] I.VJ

1 2.595 29342 3.285 41623 4.204 6S74

13970

Sroup Resort F

•til ttt TiK re*l -it

1 !»•} i.V]

4 5.232 3C:i7.6?5 2;'!.

7 S.C19 «5?i

""'

irouo Seport r

rfit iit T;K rtil r»

t inrj iu«)

e £.3?! 03 11. £3* j<05 :;.«TS :;E

?5ci)« fc'c'.-i:*: 3*3C*32?eii

7963* irc!-ll«o 1

5271657E23

1207&0 SrcI-:2*5 2

7c*e2 A':I-;2*S 32764525351 Arcl 1254-220918 ArcI-1254 3

2213 Arcl-1260 19523 Arcl-l26C 22575 fird-1260 33979

i<;;;2 EE:

1*2.57

,— . »— • , . p.' ' *.j • • f~fi • •. •. ^ — _

Area Cu:criKi'v

[.Vise;] *i«

32620 Arc!-!242 150833 Sr:l-!242 2936C6 Arcl-1242 3

1S2109

or : AR1243

Area CatsreeAt[uVtsec] Gue

79i36 Sr:i-i2«3 !12i37W hr;l-l2<3 27i*32 Ar:i-12*3 3

•°-"*

or : i-,?: 1254

;rei CuD«Ktr.tEuVUtcj Si«

o;r: ::!;-:253il ire 12S-22C'!3 -re -115* 3

2*0.337VV 106.066VV 12*. 396

loS.ota

135.0*1: 05. 2 73

125.564W 127.771

VV 30.475W 37.390W 23.771

VB 3.4<5J8 23.373(S o.767

?V 1.442

;-B ?5.768

:o;s.34i

sL Eitrjct Cont.no/in.

EE 221.474SV 237.917

2*0.337

679.723

rl. Eitr.ct L&.IC.

no/iL

'."V 165.006W 125.56*W 127.771

»le. ."v"

S. Estr.ct Coric.

ns/tL

W O.JPC-W 37.370

:E.:TI

2*0.337

lf j.0«6124.698

165.036135.041

1C5.278125.56*127.771

30.47537.39028.771

3.44523.I7B6.7671.4*2

55.763

2013.3V:

Siftbic COTiC.

U/LS ^^

221.474237.91724C.337

659.728

S«ii!e Cunc.

ti/io

U5.C06125.564127.771

-iC.^v

Hitc-le Ccnc.to.'ic

O.CC-0:?.;?o:S.;;1

66.161

10 14.953 59 2213 Srel-1260 111 17.04S 204 9523 Arc l -12 iO 212 19.269 66 2575 Arci-1260 3

V8rBit

3.44523.173

6.767

3.44523.173

6.767

323 14316 33.389 3.389


Peak Ret Tine Peak Ht Area Componentt [iin] [uV] [uVtsec] Ns*e

BL Extract Cone.no/fiL

Saiple Cone.c c / k o

13 33.485 6449

6449

643442 DBC

643442

VB 95.768

95.768

95.763

95.768

PACE, INC. PCB REPORT PAGE No.

kit* : irIX-Cl&o?:3?l.

e:f.:ii:&r: -I

tr.i T

f l c i t: I" •'.'

t. 2'

30 •'»'

ra;e 1 ct :

H:qn Foir.t : 5;.S3 tV

H — ***- "* *

T "lIBMIIlTl" I " l t i l l I I

I!-il

IIHI

40-

• !&.£

« « < < < < <

rrj'n J60

:>o-t t "til-::>e>Hip 1 t?

(.- ve-r&a.oii

:- Number

/ - _ I r: s t. r u m e r 11_.,. A u t D 5 a i; i p I c- r

'"*" Rack/Vial

EM A

KS1.11PE ASS30C0/0

i iriiebtudy

Charme-J : A

: 5/2e>/92 1.1 :37: PCft ANALYSIS

A/0 mV Ranqe? : 100O

Interface Serial tt : 1243574035 Data Acquisition Time: 5/24/92 05:5ODelay TimeEnd TimeSampling Rate

Raw Data FileResult FileInstrument FileProcess FileSample File3 e q u e n c e F i 1 e

I n j . Vol timeSample Amount


0.00 min.&5.0O min.I.OOOO pts/sec

\2700\da t.a \ J. AEL064 .raw\27OO\data\lAEL064.rst\2700\data\ 1 l.ae 1 . i.i"rB\27OO\data\llael.prc\270O\data\llael .snip

ta\llaej. . seq

cccccc.

o

1

\2700\27OO\ 2 7 1.) 0\27OO\270O\27OO

NG/ML0000

Area Reject : 0.OODilution Factor : 1.00

1.0000Area Threshold :Divisor : 1.0000



Instrument :KS111Column : 1. 57.SP-2250/1. 957.SP-2401

; Column Length :6'x 2mm on 100/120 SUPELCOPORTCarrier Gas :AR/ME 95/5F1ow Rate :5 5 m1/m i nTemperature :203Injection Temp.:250 CDetector 1 sECDDetector temp :350 CNotes :


PRIMARY ANALYSIS

Peak Ssi litet [*in]

1 2.1632 2.3063 2.5944 3.0365 3.235

Peat Ht[uV]

463653

2316263

3955

PACE .

Area Conporisnt[>jVl=ec] riaes

37:35163

2S723 Arci-1242 12143

44035 firci-1242 2

INC.

SL

sVVV'-.'EEVVV

PCB REPORT

Extract Cone.ng/«L

34.966- 49.305

212.59115.016

226.062

Saeple Ccnc.HC/^Q

34.96649.305

212.59115.016

226.062

t L ^"

I: s.552

15 11.C1916 11.K917 :3.449

IB 15.09219 17.06720 19.39621 30.047

fcii afl TlK* 7 > *

1 2.594

2 3.2S5

Group Re

feat Jet Tiw

5 :.8«?

r;ai if. TIM1 I::--

i i.331

• ::.i4?

:*0« 389951679 222C8

1315 33?771436 29137IW1 ."6I6S «rcl-;i<3 I1223 41765 Ar:!-1243 3279 12683406 14707 Arcl 1254-2375 15240 Ar:l-1254 3

78 2302 Arcl -1260 1

192 9865 Arcl-1260 261 2331 Arcl-1160 338 2180

6354 6H346 D8C

.r • 6 1 6 ilc. '50

S'^rt For : .-,R 1 ~ -• ...

reai nt Area Co4^*eriltuV] [uVlsec] Mate

2S16 2S728 Arcl-1242 13955 44035 Arcl-1242 26121 £9017 Arcl-1242 3

1329! 161780

port For : AR1Z43

Peak Ht Area !c*:-:«£ntiuVj NVIsec] Ka*e

2433 54574 Arcl-1142 !:«! 7fc2K ArcI-1245 2

SC-rt. For : AR I2^--?

rtii rt Area 2o*oo«crit:»»j it-Vised Sa:e

5 C Ar:l 154-1K-» 14707 ;r:i "s t-2375 :3;43 ;r:l- 154 3

51.16?W 102.167

«V 103.439Vi 76.708

VB 103.9095V 18.662V8 27.0915B 23.511BB 4.562

rB 21.856fci 6.240"D A "QrB v.j.-ot't 94.363

1754.124

EL Extract CoriC.na/«l

BE 212.591W 226.062W 227. <?SO

tL Eitr.ct CMC.n;/»L

VS 135.542vv ;o;.oioit 103.90?

•v £itrict Cone.

• » V* Wv

v': 17.091

fb 23. 511

-.- - row

?1.139102.167

135.542103.48?76.708

103.709

13.66227.CT123.5114.562

21.8566.2400.558

94.363

1754.124

212.551226.062217. ?30

£46.633

E«tple Cone.

13?. 542104. CIO

Saip'te Ccric.ta.'io

,;-2?23.511

Sm'.eFileN.ie : c:\2700\(!,itc\lfiE1LC64.rit,Start T:oe : 0.00 nn Enfl Tue : i'.OO nnScale Fictsr: -1 Plot O f f s e t : 25 *V

I:Lite : 5/26/92 11:37Lo« Point : 25.05 iVPlot scale: 30 iV

Fige 1 of 1

Hich Poir.t : 55.05 tV

L~! o^ r-*s- r^» o

-I0-

i inn 111 n ] i t i \ \ \ i

^X'f—c

o;\ CO

-••) C

iy* OCL

rt!Ll_

45-J

—

—

40 —

~~

1

35-J

-i

—i K

Mil I II I I I )

.T in CD 'ion;£>

I •. v' ;, . ' !. '. 'i o c^j co o o o o GI ,-•-• fvrv ri-'."v- .".-' ry ,••)-• .".- r.-'

i_>COO

I i i i i I i I i i i i i i I i i i i i i i rI I r I ! ; i i i 1 i i i i i j i i t I J I i

6 ' 10 : 20 30 40

i f m e [ m f n ]

-r-t.-r : Stucl-

.nar.nel : A. D (iiV Rsr.oc- : l»5i..-0

"r-:&c>. /Via l

Iriterface Serial ** : 12 Acquis i t ion Time-: f./27/?2 07:55

Delay TimeEnd TimeSampling Rate

Raw Data FileResult FileI nstr ..ii-=t-r.* Fi 1 i;Process FileSafiip J 5- F i l eSt-out--r.ee F i 1 5.

J nj .Cn3i_i~L t

Multiplier

>!'. O'"i m i n .4 5. OO IT. i r,.l.OOOO pts/sec

\27«»O' - de-tax lAELOfao.

> " > d a ta . i lael . prc

r-! t" •- £1 r- ii J •=• C (_

I1 i 1 -j 11 on Factor

o1.0000

S-anch r actor: 1•r : 0. OOOO

Instrument Condit_ons:cacted Column GC -

InstrumentCo 1 u.r.nColumn LengthCarrier Gas

Tea.peratureinjection Tr .3-". e - * o:" 1

KS1111. 5V.SF-225O/1. 95^3P-24016':: 2-r.fr: on iOO/HO b'JPELCC.F'CF.-AR/ME 95/555 ml .'rin2O3250 CECU350 C

PRIMARY ANALYSIS

:AC£. INC. PCB REP'jRT

f [t:s;

SI

rV

it

fi 3.842 2349 «.:s7 135

1C 4 . 4 ? ? 30?i! 5.027 64

•J-X 12 5.781 E20£/ 13 6.447 356

14 7.314 1915 8.452 6816 15.684 5617 18.105 6718 20.134 12119 24.632 51120 30.593 4921 33.305 335

6411

Group Rr-port V-

Peal Ret Tiae Peak Kt* [iinj [uV]

W1 2.623 1892 3.311 03 4.267 235

424

*

38203256 Arc l -1242 34515754

18704712125071493

1583640275358

418512369

32499 DBC

171015

or : AR1242

Area CC'tconent[uVisec] Naee

1352 Arci-1242 10 Arc!-1242 2

3256 fird-1242 3

4608

JV

VV

Ve

SSBVV6BBBBBBBFBB

BBBBBB

BL

EBVVVV

S.1953.226

1C. SI?3.354

13.07920.2990.8684.8333.1926.6637.275

30.3330.7244.975

331.386

Ext rac t Cone.no/sL

14.2630.0003.226

22.494

6.1958.226

• 10.8193.354

43.079•"\ nnn

0.8684.8383.1926.6637.275

30.8330.7244.975

-»n < TO 'JOl. JOO

Sacpie Cone.uo/L

14.2680.0008.226

22.494

;;J Group Report Fror : AR1243

Peak Ret ii§e Peak Kt* [tin] [uVJ

4 5.290 05 7.760 07 9.080 0

"^ 0

Group Report F

Peak Ret Tise Peak Ht1 [»in] [uV]

i 8.301 05 11.913 09 13.500 0

Area Coeponert[uVtsac] N'aie

0 Arcl-1243 10 Arcl-1243 20 Arci-1248 3

0

or : AR 1254

Area CoipDnsnt[uvtsec] Naie

0 Arcl 1254-10 Arcl 1254-20 Arcl -1254 3

SL

VVVVVV

EL

VVVVVV

Extract Cine.fiO/E!.

0.0000.0000.000

C.OOO

Extract Cone.no/it

0.0000.0000.000

SauDle Ccnc.U3/L

0.0000.0000.000

0.000

Eaepie Cone.ug/L

0.0000.0000.000

0.000 0.000

:. Group Report "or : AR1260

Peak Ret Tilts Peak Ht Area Coftsonent Extract CDHC.

'.. ui •-

c.wc0.036 i.C-OO

c.ooo o.oco

••c'C> Re-jjort For : Sli^F-rOO'iTE

rtil Stt Til* ffil Ht Area Cccpcwcntt

—« -'ICO «2fWVJ J *T • I .ffw

Fi. Ertrict Cone,no/kl

S««pie Ccnc.uq/L

-ACE. IMC. PCt; REPORT PAGE No. 2

• ; • ; ! • • N:-:::.. • . ,-,KJ .' V '

!.;-. ; ! ' .i!"'l-.' i i :>:,;

Se;-. ic: j I! ;: 11- U.< Ix'-10 31.", Dziiti ric;qu.:i E,J L.i c.-u 'I i mo: <•>/!:'•/Vl::i ay Time : •'!•.. OO m -i 0.<! Time : IT.. 00 n- ; ; - : .

Rate '.. 1.0000 tt!;;/^v.:'i:

;-,• Data FiJii- i •:: : \:-.->7-.--:-%.,:Jal.i;4\.-i r.i-'^C'.Ur'. r ;nv:-;.uJ. t l-"i li:- " c : M:/•:!••.> \^:UAt:'.i. \ irtKÎ •:.-•.'.;..!. i •=!-.:•'• "!;i I.UHF-! i I r .\ .1 ("T-f 1.1 ; •.»•:.'/'')•'..) \(..!c^'!.!'•( '. j J is i -'r ..].; '•.(•;.

i.vce^: !" .'. 11-- : c : \27'">-0\<j -.: '':a '•. ' .!. a ' * "? • . Pf"1:-.•:• . . : .• !<.:• F.i iu- ; ..-; \^70O1'.L:..rv ;i\.i 1 ,H-i-3 , Li-Kit..

r,-.«:-;:'•!(.•.,•:• •!-";. li.- ; i'i : \2''i.;iO\.Oi"; Ti';1-.!..).A!"'i .. t jc:

.. . V^lL'.jr.iL- ;. 2 MG.'- i i .';:ple Hiiioun t : L . 0000 D i 1 i..i t i. o r; Factor : 1 ,. 0 0

Thrtis-holc!; 6 Hrc'a "I hrtsi-sol'J t 31': ISi-incii F a c t o r s 1Itiplier i 1.0000 Divisor : i.OOOO Adder : 0.0000

•tt.inment Coctcii ti a: :-:"• ='ksd Cclumn GC --

'. s i. rumen t t KS i 1 i

I umn Length : 6 ' >: 2mm on iOO/J.20 oL.'r'tLCL'PUF^T

:-: 'i 'j'i-j Rate : tMi i::3/;iii:'i!"!:? ffi p G r a t u re r 2 O 8

PRIMARY ANALYSIS

P.4CE, JKC. l-'CLi REPORT

Rst Tise ?;;t. rt ^re; Cofttonstit [;L E^ t ' sc t Car-:, Ssitls C^rc,

533

?

,17 c c f - i271.647

;:.*.-.

• 1 - ••

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ift

i-i*: »:•-'«:•

2.t213.521*.257

:up Repc-r ',

:tt "Jf t f i :eik Ht[fin] to]

^.400 144i7.385 178•,881 0

322

.tp Report Fo

=t Ties Peak Htiiiftl [uV]

J4.217 i750

Area Cetpor-.eni IL E ••(';•:» Cor : . t-eftlt CMC.[uVlstc] Nace .".;.'fcL iV'-C

3^60 Arci-iriO ! VE S.703 9.7036riD A 'cJ- i240 2 SP !•:.:•:.? i2.::i

'> SrcI-1260 3 VV 0.000 0.000

17!»? 31.939 31.939

r : BURRDGATf-

Artc Cospsnent BL Ex t rsc t Cor:. SafoJe Cor-:.[uVlset] Na&e r;c/rL *:Q.;f;q

667468 5K BB »0.674 14J.67*

140. i?4

PACE, INC. PC.:!- REPOFV! PAGE !••!(:.. 2

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PRIMARY ANALYSIS

Ret Tifie Pesk r1:

2.218•2.37;• 2 . 6 o ?

-• . i r,•-' « C i 7

32.07537.SS;3.7Zi

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t i pi it;r : 1 .0000 D.i.vi r;or ; 1. 0000Du! it:! i Fc-.c t t < r

/r : 0 u OOOO

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:• i"! Bill: 1 - 5y.SP-225O/ .r. . 95/:3P-240: o ' x

•'v-ti^jeiraûriz :203i- i.iv't. 1 j or; "fr-!i>p . : 2SO t;•>^tf?::-l.or i ; E£CP• h- i el: t.C'!" t-^jtip : 'J-TiO C

PRIMARY ANALYSIS

'-'ACE, INC. PCB REPORT

El Ex t rac t "we.-

.••: '.''5

) 2Ê3

AC.TT. ' '

:i..t;f

c ft f ' c

•>•• M t

K-s-iJ

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• Ret Tioe Feat: Ft Area CMC went E ' t r e c t Cone.

10/ei.Sa«Dle Cone.

34.270 ^950 f?73:2 l-F.

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r--> r-i

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cxô oc_t <_/_;021:0: a:o. c:

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ocr roo

i i i t i j i i : i

Time [min]

• •'::•' .;:'ip I '..-I

,;«y ! i -liej c;.i -ti ;• .'i .'/ 3 til •/•'!•'•.

:: •.' . OO MI LI i .:: 'I!.. '.1O :-i in.

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i. • r" • «M tT-i t •_ :,'!;:.!!'»t:i j t.i.\''r. ;.-'•..! Co J. i.iiil:"i GC ~

• • "

PRIMARY ANALYSIS

l-ACE,, IMC. PCD REPORT

0.173M.S67/ l'..S42.3392.*28

:i i:1*;.j 372

f.-Ss 4i?i-7f-3 i2102.';4 •',.'•-••? ir,- i-'.?-'1 '•

S5 j,'i>.

5V 5. 00?v V ** • - 1 i "* *

1 1 ; i i .^ (• d».7 T C 'T • <1 / k

:-E ".:> 7'

o.I635.0094s.ri3i5 '•??

vAr, '.CT

i:.s:

?*t 7ii* rtit Ht

2.423

I'M*;.

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3

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f.tt Ti« rsti c:l:«»; i---:

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T i m e [ m i n ]

BLANK

A blank sample is a volume of a clean reference matrix that is carried through the entireanalytical procedure to demonstrate that the analytical system is free fromcontamination by the compounds of interest. The blank is used to correct for possiblecontamination resulting from the preparation or processing of the sample.

' '

Batch Code:

Prep Pate;

GC FORM C

Method Blank Results

Cl lent:

GC Method

Component MDL Units Results

Wo

-H

.:.:>>_•< ('i p J •'..• i J'_i:i. C

'....liver <:•: t orf-TF..1 j i

i 11.1 '.' C; ij," i fi i p J t1 r : r

r •; <ii c. k / V i. a J : u / 0

L'l iid if if:.-1 10 CO

Interlace SerialDelay TimeElnd TimeSampling Rate

Raw Data FileResult FileI n s t rumen t F :i. i eProcess File-Sam pie Flit-Sequence File

i nj .S 3. ni p 1 e A ffi o u. n t

Noise ThresholdMul tipl ler

4* : 1248S7Î035O.OO mm.65.00 min.1.0000

Data Acquisition Urne: 5/23/92 16:32

pts/sec

c:\27 O O \ d a t a M A E L 0 5 2. r a. wc: \2700\ciata\lAEL052. rstc.: \ 2 7 GO \ d a t a \ 1. J. ae 1 . i. n sc:: V 2 7 0 0 \ d a t a \ 11 <:< e 1 . p r cc : \ 2 7 CO \ data \ 1 J. a e 1 . s n> pc:\2700\dataVllasl.seq

2 NG/MLI.0000

1.0000

Area Reject : 0.00Dilution Factor : O.10


32 Bunch Factor: 1Adder s 0.0000


-, Instrument'if Co 1 umn

: Column LenqthCarrier GasFlow RateTemperatureInjection Temp.Detector 1Detector tsmpNotes

KS1111. 57.SP-2250/1.957.SP-2401i'x 2mm on 100/120 SIJPELCOFORTAR/ME 95/555 ml/ iT'i i n208250 CECD350 C


PRIMARY ANALYSIS

PACE. INC

Peak1

12

j 3

45

ftet THE[Bin]

2.0172.2022.S173.4575.753

Pssk Kt[uV] [i

421255049

141

Arsa Cseponent

iVIsec} N'a.'i5

320SSS333 Ard-1242 1

5562342

EL

25SBSB£3SB

. PCS REPORT

Estrsct Cone.ng/'fiL

3.1999.412

3.7903.9146.539

Socole Cone.

•g/kg

0.3200.941u.3790.3910.454

5:;3i

'} -••• -. j. ,-L '• 1 " D L II I f< C.: pO t t i •• C

-"" i Peak Ret lite Peat Ht,, , i [*in] [uV]

1 2.617 502 3.311 03 4.250 0

50

Group Report Fo

Peat Ret Tiee Peak Ht* [tin] [uVj

4 5.290 05 7.760 0

^7 9.080 0

0

•fr Group Report Fo

Peak Ret Tiie Peak Ht[Bin] [uV]

~ 6 8.801 0S 11.918 09 13.500 0

0

'i roup Report Foi

Peak Ret Tite Peak Ht* [tin] [uV]

10 15.160 011 17.200 012 19.400 0

0

:roup Report Foi

;afc Rst Tiee Feat Ht- [sir/] [uV]

459911

>r : AR1242

Area Component[uVJsec] Na*e

333 Arcl-1242 10 Arcl-1242 20 Arcl-1242 3

338

r : AR1.248

Area Component[aVIsec] Nase

0 Arcl-1243 10 Arci-1243 20 Arci-1248 3

0

r : AR 1254

Area Component[uVtsec] Kate

0 Are! 1254-10 fircl 1254-20 Ar:i-125i 3

0

r : AR126O

Area CoEponent[ uV tSECJ Ndfee

0 Ar:l-1260 10 Arci-1260 20 Arc 1-1 260 3

0

r : SURROGATE

Arts Consponent[iivlsecj Naze

"•"*

117.C'31

6L Ex t rac t Cone.ng/'AL

EB 3.790VV 0.000VV 0.000

3.790

cl Eitraet Cone.nq/sL

VV 0.000VV 0.000VV O.OGO

0.000

31 Extract Cone.ng/ftL

VV 0.000VV 0.000VV 0.000

0.000

BL Extract Cone.nc/al

VV 0.000VV 0.000VV 0.000

0.000

rl Ext ract Cone.iia/Bi.

6.SI4

11. ;c:

SiJiple Cone.*; /kg

0.3790.0000.000

0.379

Satole Ccnc.5,Q/kQ

0.000O.COO0.000

o.coo

Satple Cone.

•9 '4

0.0000.0000.000

0.000

Saftcle Cone.eg /kg

0.0000.0000.000

0.000

Sssple Cone.iO /KQ

<45e>01

PACE, 1I4U. PCT: RPPGRT PAGE No

stiri Tite : O.OC *jn End Ti»e : 6'.; i&t iiHsEt: lj

»:n

r o u e i U

Date : 5/27/?2 07:47Lo*. Foint : 2<.79 tVriot Scale: VJ «V

Hich Point : S.79 i.V

(U0c0a

O t--t ^

r r T

1II

50

—1

J

I

40-

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O C: O O O•y -z. a; a; a: oCQO

l ! I

1 rr i e

TTT I j f40 60

f m I n 1

GC FORM C

Method Blank Results

Batch Code: lfblrtyM}/fahvf>\ Client: . 7 j4-

(\f\lMatrix: i 7 1' —

Preo Date: [ fi 'T"'

Component

l 'f /7>V

]Nftr^-

'

MDL

GC Method: '

Units

-

^n:tf:f¥r.

Results

lOoD/'/

>

• - i .• ' V ' / 'V! ;; i •• O.(

'•yLifu!: Li'ritj !..!: i 6 ' x !::'(;•:<; i:.-l i'.•:•'•'v t.vr i^rAS • f,h/<:•'.'.". v l^ / r "

' -.• !-J ?••;?: 'hi.'1 i "-^ ••'. ? / 1; ?. i ;

PRIMARY ANALYSIS

'(' .«",/ CV Vn

:-«.:r ^' wn cue

.•->'• f i r t " ?

; ftft " jdc ftfil: Ht Ar fa Comôrivntffir;] tuV] luVlsec] Ndte

2.M2 0 0 Ar:M2« 13.331 0 (' ftrcH2« 2i.229 0 0 Ar:l-!242 3

0 0

-• f.ii T :rr r-r.fi Ht Ar-ra rc.aocr.ert

w " ""5.130 0 0 Arcl-1245 1£-.400 0 C Arcl-31'48. 2t.SOO 0 0 Arci-124S 3S.024 0 0 Arc!-12« 4

.!•>-4> RGDort For : AR 1254

; hst T i fc j ?ea>, Ht Ar=i Cosporert

r.iOi v 0 Arcl i:S4-!!1.>15 0 •• Ar:l 12:4-2".*£- 0 0 *r:l--254 3

'•. i •"•

• .::et Use Frili Ht Arri Ccs£-?r,?r:t

11.205 0 0 Arcl-1240 11 - ' r 7 •'. A ^ , . 1 : : ;'. •".

l^.Stl C 0 Arc - -12 iO J

b't i.21!v O.:;i'iL-L ; ';! .• "1 r.:".V

lit', 71"- ]ts -,<•

SL t'xlfrc.! Ccrir. Sefcpip Conr,nqVrL »q/(q

VV 0.000 0.000VV 0.000 0.000VV 0.000 0.000

0.000 0.000

sg/aL ft-j/i'.g

VV 0.000 0.000VV 0.000 0.000VV 0.000 0.000w o.ooc o.ooo

0.000 O.OOv

5L Extract Cc-n:. £«»[•]? Cone.RQ/iL ag .-'f.g

\V 0.000 O.C':(i

VV v.0-50 0.000

(:•.•':••:•'•• O .OOC

BL Ex t rac t C'-jric. 52<ple CcriC.

VV 0.000 0.000

VV 0.000 0.000

0.000

• ' In - '.c«r

PACE, INC. PUB RtPUm PAW- Hn. v

.-1

:r.i u-:

befp i f f :

L > ' f : -..•:.?:•, .L ; « F''.-:'i'. I I':

1 Of 1

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ocr>o

I i l l

Time [min]

LCS

Laboratory Control Sample: A mixture of target analytes at knownconcentrations is spiked into a clean reference matrix and analyzed bythe appropriate method to demonstrate the analytical system is incontrol.

GC FORM I

LABORATORY CONTROL SAMPLE

SPIKE RECOVERY

BATCH

WANG #

MATRIX

CLIENT

METHOD

PREP. DATE

/1 A-

O

%o a 83 3Seuf) J

COMPOUND SPIKEADDED

SPIKE PERCENTRECOVERY RECOVERY

_7.

_7.

_7.

_7.

7.

7.

7.

ANALYST

DATE

Sample

I n?rit.r urne-ril.

t--V_l1_Qc:af(ip 1 05 r"""

I-.;:. 111PC. ASS'.M.»0

o / o

A/1) fii'v R-'

Inter-face Serial tt : 1243574035 Dot;-'. Ac.quiBi ti.on Time: 5/23/92Delay TimeEnd TimeSampling Rate

Raw Data FileResult FileI. n s t r u m e n t F i 1 e-'ro c e s s FileSample File•.equence File

nj. Volume; c> iTi p 1 e A ;T; O U n t

j! Thresholdol ier

0 . 00 mm .65 . 00 ruin .l.OOOO ptfs/sec

c:\2700\data\lAEL053.rawcs \2700\datc-.\lAEL053. rstc : \ 2 7 0 0s^ d s. t a \ .1J a e.- i . in ~>c:\2700\data\liael-prec : \2700\dete x 1 lê 1 . =,ii!pc : \27OO\data\.l. lael .. seq

2 NG/ML1.0000

1.0000

Area Reject : 0.00Oil u. t i o n F a c tor : 0 . 10

Araa Threshold :Divisor : l.OOOO


net. rumen t Conditions:-•>. c k ea Column GC -Instrument :K3111Column : 1. 5XSP-2250/1 -95'/.3P-2401Column Length :&'x 2mm on 100/120 SUPELCOPQR"

-rier Gas rAR/'ME 95/5i^xbw Rate : 55 ml/minTemperature :203Injection Ternp.:250 CDetector 1 :ECDDetector temp :350 CNotes :

tr Number of Peaks Detected: 2'J

PRIMARY ANALYSIS

Ret Tise

."•»'« J

2.1932.6073.440

3. £31^02

Feat Ht

[aV]

12610599

41

1:1

<~t /\ f~- 1 — T K ;r-«r i-iLr. . j. i-Ji^ .

Arts Cojiporitrit SL

•uV lsec ] Ni£5

951 £3779 Arci-1242 1 BS

13;:6 BV1017 VV

31J7 Arc i -1242 3 VV

PCB REPORT

Extract Cone.

"?/aL

9.4927.939

5.642

2.144b.i74

Seipie Cone.

£? / tg

0.94?C.794

0.564

0.215G.ib7

T t.lj. '.l^l

10 e.567 5=4;. !1 7. ,28 2S55

' 11 6.767 3795

;; 9.4S3 12bO

s 14 10.997 2220

> 15 11.627 3699

16 13.445 3820

17 15.065 1973

13 17.035 1739

19 19.252 2136

20 24.665 373

21 27.548 267

22 29.668 359

23 33.435 4319

24 33.685 109

34100

Group Report F"

Peak Ret Tine Peak Ht

j \ [oin] [uV]

1 2.607 105

2 3.311 03 4.202 191

296

2<ls;>12107

117596

159179 A r c l 1254-1

34131116150

160815 Arc l 1254-2

134097 Arcl-1254 3

1060S6 Arcl-1260 1

85923 Arcl-1260 2

119329 Arcl-1260 3

25235

21286

30530

4120<7 DBC

7575

1674041

or : AR1242

Area Component

[uVtsec]' Nate

779 Arcl-1242 1

0 Arcl-1242 2

3137 Arci-1242 3

3915

v'V

v'v

vvvvvvVv

vvvvVBBV

VBBB

BVVBBBBB

BL

BBVV

6V

61.1 'I

27.101

139.766

171.006

106.285146.296

247.111

239.743

114.616

174.465

133.40832.114

3.9615.324

64.142

1.621

1961.577

Ext rac t Cone.

ng/ftL

7.939

0.0006.674

14.614

t.ti i2.711

13.977

27.10110.629

14.830

24.711

23.974

11.46217.447

13.341

3.211

0.396

0.532

6.4140.162

196.158

3a&p!e Cone.

Iiy/ko

0.794

0.0000.667

1.461


Peak Ret Tise Peak Ht

* [Bin] [uVj

4 5.290 0

5 7.760 0

/ 7 9.030 0

0

Area Coeponent

[uVtsec] Nate

0 Arcl-1248 10 Ard-1243 2

0 Arci-1243 3

0

BL

VVVvVV

Ext rac t Cone.ng/sL

0.000

0.000

0.000

0.000

Saiple Cone.iO/kQ

0.000

0.0000.000

0.000

Group Report For : AR 1254

Peak Ret Tiee Peak Ht

* [sirs] [uv]

a 3.767 3795

8 11.827 :.i99

9 13.445 3S20

\ 11313

Area Component

[uVl=ec] Nate

159179 Are! 1254-1

160£:5 Arc l 1254-2

134097 Arei-1254 3

504C91

BL

VVVVVV

Extract Cone.

ng/eL

271.006

247. Ill239.743

757.560

Sa«pie Cone.eg /kg

27.101

24.711

23.974

75.786 / ,,- „

1

\

I

'•

Inn]

-,.:ic

17.035< r i c "i

[ cV j

1"3173?:isi

5393

iu VI sec 3

K-SOBi A r c lS5923 A r c l

119329 Arc l

JHS7

.w».-,.CIIk

l.ate

-;ibi ;« •»> • \ n

"liDV i

-1260 3

:-L tx i f ic t Lone. Sdiplt Cent,no/f tL iig.;»Q

Vji 114.'.'V 174.vt> 133.

422.

616 11.462465 17.447408 13.341

489 42 .249


Peakf

13

Ret Tiie

Ciir.3

33.435

Peat Ht[uVJ

4319

Area[uVtsec]

412047 'M

CoiponentNaie

BL Extractng/B

rB 64.

Cone. Sa*ple Cone.L nQ/ lq

142 6.414

4319 412C47 64.142 6.414

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