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Two and Three Electrode Potentiostats. Three-Electrode Design. Sponsored By. Background Information Dr. Harnett’s lab needs up to 15 potentiostats that are: Inexpensive (less than $100 per unit) Easy to assemble by students OTS solutions range from $5K to $10K Theory of Use - PowerPoint PPT Presentation
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Background Information• Dr. Harnett’s lab needs up to 15
potentiostats that are:• Inexpensive (less than $100 per unit)• Easy to assemble by students
• OTS solutions range from $5K to $10K
Theory of UseA potentiostat is:• The electronic hardware required to
control a three electrode cell and run most electro-analytical experiments
• An electronic instrument that controls the voltage difference between a Working Electrode and a Reference Electrode.
• It measures the current flow between the Working and Counter Electrodes.
Design Methods• Two-Electrode Potentiostat• Previously developed by Capstone
group during Fall 2010• Follow-on project by Ben Williams• Firmware improvements• Hardware component revision
• Three-Electrode Potentiostat• Originally developed by University of
California Santa Barbara
Objectives• Improve existing Two-Electrode Potentiostat• Implement Three-Electrode Potentiostat• Test and compare results between designs
Two and Three Electrode Potentiostats
Sponsored By
Group Members: Kyle Bloomer, Luke Bennett, Josh Geiman
Three-Electrode Design
Cindy Harnett
DDMS
Two-Electrode Design
Arduino Development Board Daughter Card
DDMS
Experiment• Tested the current difference in four orange juice
samples caused by varying amounts of ascorbic acid• 0, 0.1, 0.2, and 0.3M of ascorbic acid in each
sample, respectively• Electrode usage• Counter: Platinum wire• Working: Pencil “lead”• Reference: Standard Ag/AgCl
Expected Results Two-Electrode Results
Three-Electrode Results
Conclusions and RecommendationsResults gathered from experiment do not coincide with expected results.• Possible contributing factors:• Reference electrode in poor condition• Possible firmware issues with measurement
execution• Possible errors in chemistry related procedures