22
Meso: Figs2 (Benjamina) – Exp1 29.06.2009

Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

  • View
    222

  • Download
    1

Embed Size (px)

Citation preview

Page 1: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

Meso: Figs2 (Benjamina) – Exp1

29.06.2009

Page 2: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

08:46 after 2 fill/flush cycles

Page 3: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

09:00 A spike at the end of the flush cycle followed by another one at the beginning of filling

Page 4: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

09:06 the following scan at the end of that fill

Page 5: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

09:16

Page 6: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

10:26 Filling via PC (20 mins in)

Page 7: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

11:26 12 minutes ALO

Page 8: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

37min ALO

Page 9: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

52min ALO

Page 10: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

57min ALO

Page 11: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

1 HALO

Page 12: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

12:22 Arcing!

Page 13: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

Reduced the upper size from 264 to 245nm

Page 14: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

12:37 Still arcing

Page 15: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

Reduced max size to 184nm

Page 16: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

3 HOLA

Page 17: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

4 HOLA

Page 18: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

5h13min ALO

Page 19: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

5h 24min ALO: injected 2ppb limonene

Page 20: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

6HALO, 40min after Limonene injection: nothing happened!

Page 21: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

30 min after second limonene injection

Page 22: Meso: Figs2 (Benjamina) – Exp1 29.06.2009. 08:46 after 2 fill/flush cycles

7h25min ALO: 1 h 24 mins after injection