ICP Test Report Certification Packet/media/files/littelfuse/technical... · Total Parts Raw Material Part Number Raw Material Description Page(s) 1 901-556 Cap base & plating 3-6

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: 5x20 Fuse Product #: 0477016.MXEP Issue Date: October 10, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (2011/65/EU – recast of EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts This document covers the 477P Fuse RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：.

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part

Number Raw Material Description Page(s) 1 901-556 Cap base & plating 3-6 2 C610 (909-449) Body Ceramic tube 7-35 3 311.7374.5000 Filler Sand 36-45 4 082xxx/ 0823xx-001 Wire - Cu99.9MSn 46-50

5 YTW102

(692539-002) Solder 51-56

6 C030204/ 934-077/ 934-071/ 934-078 Overcap - Cap Base & Plating 57-60

Form 585-047 Rev. A 2/21/06

Customer: Suzhou FuHong Electronjc InduslrialCo., Lld.

Addres!: NO.89 WEIDU ROAD, WANGTINGTOWN, XIANGCHENG DlsTRlCT, SUZHOU, CHINA

Report on ths submitred s.mplesald to be

S.mple name: CoppeJ,shell

Mod€h/

Item/LoiNo.:/

Metar lal : / ,

Buyer: / ,

Suppli€r: /

Samplo recaivsd d.te: Ocl. 08. 2012

Testins period: Ffom oct os, 20!€ 1o'O4r'10, 2012 . . ,,' \ l '

E9S!.s-Ecs!ed9!f

NO.: 4002R12100802+1 R02

As specified by dient, to determine ihe Lead, cadmlun,

accordance with Dircctive 2002/95/EC {RoHS).

AOV"BPFS,U

LiTingting, Maggie

Chemic€l Test Direcror

TEST REPORTDare: ocr.10, 2012

Mercury & Hexavalent Chrcmium content in the submitled sample in

Ylan Qi, lrickey

Ec!!!s-ee$9!.:Testing ltem Measunng instrumeni I\4QL

Lead (Pb) IEC 62321: 2008, s€ction 9 ICP€ES 2-'nglkg

Cadmium (cd) |EC62321: 2008, seclion I ICP-OES 2 mg/kg

[4ercury (Hg) lEc 62321 2008, seclron 7 tcP-oEs 2 mg/kg

Chromum (Cr\rl) IEC 62321 2008 Annex B 0.02m9/k9'

Ieqr 0.02 mg/kg reE|s to the MQL ofsample extfaction liquid

SsElcge!:-when tesled as speci{i€d the submitted sample complied with the requirements of commission Decision ol 18 Aug 2005

amending Directjve 2002/95/Ec noiilied under document 2005/618/Ec

ILS, PLEASE REFER TOTHE FOLLOWNG PAGE(S)***

signed lor and on behalfof

Shenzhen AOV Tesling Technology Co., Ltd, Kunshan Brcncn

caeateaaer: /blfil **n*"oor, We-r k] n ooo,',*or44.

SI tEN2HEN AOV Tf S I ING T€CHNOI ,O6Y CO. , I "TO.KUNSNAN BRANCTI /// \ Noll ne, J a,t 7tt) 9€'t'o

AOV'*F#S,[

NO.: 4002R121008024-1 R02

TEST REPORTOate :Od.10,2012

Content i|retb.r sulit€le). \ .

Cooling the vess€|, nlter;washed and

Rlled 10 the mark with distill€d wat€r.

The sample is digested in the

microwave oven following a specific

decomposrlon program

Test the sample solution and lhe 0.02

ng/kg standard solltion by uv-vls.F;;1.-

SH€NZH€N AOV TESTITIG lCCINOLOGY CO.,LTD.KUNSIIAN BSANCH( :

H o t l r n e'tL)0 700 8600

1. To Determiney'.ead, C€dmium Contenli (Metal subslrate)

I*redby (y'a04*

Add ihe digestion solulioni the

vessel is heated unlil the sampleWeigh ihe sample into

Add HrOruntilthe sample is clear

To Dete

Weigh ihe sample

Cooling the vessel, tiltei washed and

filled lothe maiK wilh dislilled water.Tested by lcP-oES

Chromium Contenl (boiling- wat€F €xtlaclion): ([4etal Eubstrate)

Remove lhe sample, and cool

the beak€r to room temperature,

and do the color reaction

Take the (50i5) cm,

sample in the beaker.Heat 50 mL of Olwater in

the be6ker to boiling for 1o

nov'Bpf,F,il

NO.: 4002R121008024-1R02

5. To oetemine Hexavalenl Chromium Contonl in_ .. -i\

: va'hu't'

TEST REPORTDaie: Ocl.10, 2012

colorless and colored chromate coating on metats: iPtating)

5.2 Boiling-wateF enradion

lfthe lest result is positive,

the sample is considered to

have hexavalent chmmium

Place 1-5

and the 0.02 mg/kg

Boiling- water- extraotionprocedu€ shall be used to

lflhee is interference or it is hard to decide

whetherlhe sample have lhe hexavalent

Remove the sample, and coolthe beaker lo room temperalure,and do lhe color reaction

sample in the beaker.Heat 50 mlof Dlwaier in the

beaker to boiling for 10 min

Test tne sample solution and lhe 0.02mg/kg standad solulion by UV-VIS.

Sample Delcriptlon:

Code Sample Descndion

1-1 Substrate

Plating

Te3t R63ulb:

Unit RoHS Limit

Lead (Pb) msfts 1000 N.D. 1 0

Cadmium (Cd) mg/K9 100 N.D. N.O.Merorry (Hg) ms/Kg 1000 N.D, N.D.

Chromium {Crl,ll) m9/kg 1000 Negative Negative

s8€NZh€N AOV T€SrtNG TECHNOlOSY CO,,tTD,TUNSHAI!ARANCH H ot l in e.100 700 B6a0

,.r

nov'F"Ff"qn

No.: A002R1210o602:L1 R02

neoatve.,-"The te8t is bas€d on lhe followins d!!{mplifi:

maybe cannot stand lor the physical lrdh 6t s€r

TEST REPORT

Coppershell

-The new RoHS dircclive 2011/6tEU, on Jul. 21, 2011 come into forc€, on Jan. 03, 2013lhe formal implementation, Direclive

2002r'95/EC ahall be repealed simultaneously.

Sp€cimens, which r€Slested lo detemine Lead, Cadmium and Mercury Content, have been dissolved completely,-mg/kg=ppm ,-N.D.=not

i",, ,,,,( The iested sample result is uncertain or

SH€NZII AOVTIST|n|G TECHNOIOCV CO.,ITD.KUNSHAN AFANCH H ot l in e400 /00 8600

Signature plidForQueslionPlease Qltwith SGSwww.tw.sal-om

rtlt[tll][]|lt

Test Report No.: CE/20't3l/13191 Dale 2013101121 Page: 1 of 29

CERAMTEC GMBHGESCHAFTSBEREICH IJULTIFUNKTIONSKEMMIK,LUITPOLDSTRABE'I5. 91207 LAUF

The following sample(s) was/werc submitted and identified by/on behatf of the client as:

Sample DesoriptionStyle/ltem No.Sample Receiving DateTesting Period

CERAMICc6102013t1tl42013t1tl4 10 2013tO1n1

Test Re3ult(s)

Conclusion

: Please lefer to next page(s).

: Based on the pedomed test6 on 6ubmitted 6amples, the test results of Cadmium, Lead,I\rercury, Hexavalent Chromium Cr(Vl), PBBS and PBDES comply with tho limits as set byRoHS Dircctive 201'1/65/EU Annex ll; recasting 2002/95/EC.

Efnrd fr. aod

Chqdcd frbot bry-Trlgd

tHl5";vtr^:,)n*$i"d h8 T.u:lM

I d!'€'' ledn'"Jg onr oi.-i"oiji.--," **o o n"c.ru rcele o1r{ o'd.r'"€.o*or

f';;il*-fl9#'i"15;; d;hd,"...bndd;cmsns. E-i '.r ' i ' 'r s.rd bndid roE. .1Yand{o1ouon! (

; -to;;'; ;;:' de. rdd a- i {d d s'***d $;i-.h'';l:*l;-*.":*:;;*|'!6;, .,1;TtydT PJ.;1ii:;;T*.iiift i;;5#;i"'":1'"p,;ilbe tme or E fleiEdm onry ad s

t";!i;y1;;*"*#:;;lim:r"r"*li:;.::ir*"'r;fff";ffij'i"""ffi'13il*:#ift'r-"-".ff'""1;",1#,;1""H{i;:i""'ri"rl,1;ii , : : : n r . l l i r i l l i

Test Report No. : CE/2013/13191 DaIe :2013101121 Page: 2ol 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNfiIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

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Test Result(s)

PART I{AME No.1 : CREAM CERAirlC

Test ltem(s) Unit Method MDLReault

LimitNo.t

Cadmium (Cd) mg/Kg with reference to lEc 62321: 2008 andperformed by ICP-AES.

2 n.d. '100

Lead (Pb) mdkg With reference to IEC 62321: 2008 andperformed by lCPiEs.

2 204 1000

Mercury (Hg) mg/Kg With reference to IEC 6232 1 : 2008 andperformed by ICP-AES.

2 n.d. 1000

Hexavalent Chromium cr(Vl) msyKg With reference to IEC 62321: 2008 andperfonned by UV-VIS.

2 n.d. 1000

BBP (Benzyl butyl phthalate) (CASNo. : 85-68-7)

With reference to EN 14372. Analysis,ras performed by GC/MS.

0.003 n.d.

DEHP (Di- (2-ethylhexyl)phthalate) (CAS No.: 117-81-7)

o/. With reference to EN 14372. Analysiswas perfomed by GC/MS.

0.003 n.d.

DIDP (Di-i6odecyl phthalate) (CASNo. : 26761 -4O0)

% With reference to EN 14372. Analysis,,,€s p€rformed by GC/|\4S.

0.01 n.d.

DINP (Di-isononyl phthalate) (CASNo.:28553-12-0)

o/o With reference to EN 14372. AnalysiswEs perfomed by GC/MS.

0.01 n.d.

DNOP (Di-n-octyl phthalate) (CASNo.: 117-84-0)

o/o With reference to EN 14372. Analysisw€s perfomed by Gc/Ms.

0.003 n.d.

DBP (Dibutyl phthalate) (CAS No.u-7+2\

% With feference to EN 14372. Analysiswas performed by GC/MS.

0.003 n.o.

Perf luotooctane sulf onates(PFOS-Acid, Metal Salt, Amide)

mg/kg With reference to US EPA 3550C;2007. Analysis was performed byLC/MS.

1 0 n_o.

PFOA (CAS No.; 33S7-1) mg/Kg With reference to Us EPA 355ocl2007. Analysi6 was pedomed byLC/MS.

1 0 n.d,

Polychlorinated Biphenyls (PCBS)(CAS No.r '133,S36-3)

mg/kg with referenc€ to us EPA 3540cmethod. Analysis was perfomed byGC/MS.

0.5 n.d.

Test Report No. I CE/2013/13191Oate | 2013101121Page :3o f29

CERAI,ITEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[/|IK,LUITPOLDSTMBE 15. 9'1207 LAUF

tl|||tt lttlul

Test ltem(s) Unit Method MDLR€6ult

LimitNo.'l

Polychlorinat€d Terphenyls(PCTs)

mS/kg With reference to US EPA 3540Cmethod. Analysis\ ras perfomed byGC/MS.

0.5 n . d .

Polychlorinat€d Naphthalene(PCNs)

mgKg Wth reference to US EPA 3540Cmethod. Analysis\ ras performed byGC/MS.

5 n.d.

Alkanes, C10-13, chloro (ShortChain Chlorinated Paraffins) (CASNo. : 85535-84-8)

mg/Kg With reference to US EPA 3540Cmethod. Analysis was performed byGC/l\rs.

'100 n.d.

PVC Analysis was performed by FTIR andFLAME Te6t.

Negative

Formaldehyde (CAS No.: 50{0-0) mg/Kg With reference to ISO 17226-1(2008).Analysis was performed by HPLC/DAD.

3 n.d.

Monomethyl dibromodiphenylmethane (DBBT)

mg/Kg With reference to uS EPA 8270Dmethod. Analysis was performed byGC/MS.

0.5 n.d.

Monomethyl dichlorodiphenylmethane (Ugilec121)

mg/Kg With refefence to US EPA 8270Dmethod. Analysis was performed byGC/MS.

0.5 n.d.

[4onomethyl tetrachlorodiphenylmethane (Ugilec141)

mg/kg With reference to US EPA 8270Dmethod. Analysis was performed byGC/rlts.

0.5 n.d.

HalogenHalogen-Fluodne (F) (CAs No.:14762444\

mg/Kg

Wilh €fe.ence to BS EN USA2:20O7.Analysis was p€rfomed by lC.

50 n.d.

Halogen-Chlorine (Cl) (CAS No.:22537-15-1)

mg/Kg 50 n . d .

Halogen-Bromine (Br) (CAS No.:1OO97-32-2)

mg/Kg 50 n.d.

Halogenlodine (l) (CAS No.:1436244-8)

mg/Kg 50 n.d.

Oryanic.tin compoundaTdbuvl Tin (TBT) mg/Kg With reference to DIN 38407-13.

Analysis was pertormed bY GC/FPD.0.03 n .d .

rriphenylTin (TphT) me/Kg 0.03 n.d.

TestReport No.:CE/201:r/13191 Date:2013t01t21 pase:4of2s

CERAI,TEC GI,BH |I]|||tt][tt rlGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

Test ltem(s) Unit method MDLResult

LimitNo.l

AabestosActinolite (CAS No.: 77536-66-4)

Wilh reference to EPA 600/R-93'/1 I 6method. Analysis was performed byStereo l\Iicroscope (SM), DispersionStaining Polarized Light Microscope(DS-PLlr) and X-ray DiffractionSpectrometef (XFID).

NegativeAmosite (CAS No.: 12172-73-5) o/o NegativeAnthophyllite (CAS No.: 77536-67-5)

% Negative

Chrysotjle (CAS No.: 12001-29-5) NegativeCrocidolite (CAS No.: 12OU-2a4\ ok NegaliveTremolile (CAS No.: 7753e68$) % Negative,zo1): 4-AMINODIPHENYL (CAS No.:92-67-1)

mg/Kg With reference to LFGB 82.02-2.Analysis uras performed by cC/lVS.

3 n.d,

BENZIDINE (CAS No.: 92-87- mg/Kg With feference to LFGB 82.02-2.Analysis was performed by GC/IVIS.

3 n.d.

3): 4.cHLORO-O-TOLUIDINE(CAS No.: 9569-2)

mg/Kg With reference to LFGB 82.02-2.Analysis u/as performed by GC/MS.

3 n.d.

4)r 2-NAPHTHYLAMINE (cASNo.r91-59-8)

mg/Kg With reference to LFGB 82.02-2.Analysis w€s performed by GC/MS.

3 n.d.

5): O-AMINOAZOTOLUENE (CASNo.:97-56-3)

mg/kg With reference to LFGB 82.02-2.Analysis was performed by GC/tu|S.

3 n .d .

6): 2-AMlNO.4-NITROTOLUENE(CAS No.: 99-55-8)

mgikg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

n.o.

7): P-CHLOROANILINE (CAS No.:10647-8)

mg/Kg With referenc€ to LFGB 82.02-2.Analysis wEs performed by GC/MS.

n.d.

8): 2,4-DIAMINOANISOLE (CASNo.:6'15-05-4)

m9Kg With reference to LFGB 82.02-2.Analysis was performed by GC/[,!S.

3 n.d.

9'):4,4-DIAMINODIPHENYLI\4ETHANE(CAS No.: 101-77-9)

mg/Kg With reference to LFGB 82.02-2.Analysis was performed by Gc/Ms.

3 n.d.

10): 3,3'-DICHLOROBENZIDINE(CAS No.: 91-9+1)

mg/Kg with reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

1 1)r 3,3'-DIMETHOXYBENzIDINE(cAS No.r 11$9&)

mgftg With roference to LFGB 82.02-2.Analysis w€s perfomed by GC/MS.

3 n.o,

'1 2): 3,3'-DII,iIETHYLBENZIDINE(CAS No.: 119-93-7)

m9Kg With reference to LFGB 82.02-2.Analy6is was performed by GC/lltS.

3 n.d.

fi ' ' !,"l;*'"*.;*.-".:;". ' ' ' ,.""""...].,";..":"'.s"*"...*"-':.."'"."."-, i l ; , .n i ' jn . i , .n t tomaroi - . "* . -d€o6|er ,ardcotro|3|oLeiii, iil.-niiniiv-iiiiiinnn-in,ii^?,aitd;*uBdlin6dthe;;^i i i i i i i"i,i ir,i*o' -ry-"*ri tr. -'borc ctihqrudm' Ir'l -tcomdars ea s!oo!oi,.i"*.i- m * os no a i r.' q*

" o o'qa'o* -0.'- nino;r'doe-44 n s do' -d -moin. ?erc!L("d P e0

li;fiii rii;" r;;a; tao: b's;t "abi"r.d*

oJ rhe @;;;;;i;;;;;i $ n@*i' "

*h*tu sa otundds mai be prcsdcd b '

, " , . , , , . : i l i i ; i l . r , qno*' t r"aFt i r i . l i . { rrr * f : rr}L s d ..::i-:-1' 9P !.ll!!.r.1

Test Report No. : CE/2013/13191 Dale:2013101121 Paqe | 5 of 29

CERAI\4TEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[IIK,LUITPOLDSTMBE 15, 91207 LAUF

Il]mttfittltl

Test ltem(s) Unit lrethod MDLR€ult

LimitNo.l

1 3): 3,3!DIMETFIYL-4,4-DIAIJINODIPHENYLMETHANE(CAS No.: 838-88-0)

mg/Kg With reference to LFGB 82.m-2.Analysis was performed by GC/lrS.

3 n.ct.

14)r P-CRESIDINE (2-IUETHOXY-s-METHYLANILINE) (CAS No. I120-71-8)

msasWith reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

'1 5): 4,4.-METI-IYLENE-BIS- (2-CHLOROANILINE) (CAS No.:101-144)

m!/(g With reference to LFGB 82.02-2.Analysis was performed by GC/MS_

3 n.d.

16): 4,4'-OXYDIANILINE (CASNo.r 101-80-4)

mg/Kg With reference to LFGB 82.02-2.Analysjs wEs p€rfomed by GC/MS-

3 n.d.

17): 4,4'-THIODIANILINE (CASNo.: 139€5-1)

mg/Kg With reference to LFGB 82.02-2.Analysis w€s perfomed by GC/MS.

3 n.d.

1E): O-TOLUIDINE (CAS No : 95-s34)

mg/Kg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

'1 9): 2,4-TOLUYLENEDIAMINE(CAS No.: 95-80-7)

mg/Kg With reference to LFGB 82.02-2.Analysis wa6 performed by GC/MS.

3 n . d .

20): 2,4,5-TRIMETHYLANILINE(CAS No.: 137-17-7)

mdkg With reference to LFGB 82.02-2.Analysis\ ras performed by co/l\rs.

3 n.d.

21): O-ANISIDINE (CAS No.:90-04-0)


3 n.d.

22): P-AMINOAZOBENZENE(CAS No.r 6M9-3)

mg/Kg With reference to LFGB 82.02-2.Analysis was perfomed by GC/MS.

3 n.d.

23): 2,4-XYLIDINE (CAS No.r95-68-1)

mg/kg With reference to LFGB 82.02-2.Analysis was performed by GC/IVS.

3 n.d.

24): 2,6-XYLIDINE (CAS No.: 87-62-7)


3 n.d.

CFC's (Chlorofl uorocarbons)Group IChlorofluorocabon-1 1 (CAS No.l75€9-4)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n .d .

Chlorof luorocarbon-1 2 (CAS No. :75-714]


n-d.

;ii; i;i;;; ; ,!,.i .d '; ri. c.-,;;' ',ti; b iL; &ne'ar condi om d;; ;;;;i i;; d;-tu:^a 3uh;ed b rem! ano co.o @ns h' rrqd. b;{.I d{w.{s.o- e.i ; ; d ; l a ' ' h " i j . ' i - * ' ; . d i $a fnn ' 3 . "dddh .F 'ha rme or i! 'meilerton onrv and -; ; ; ; - ; ; h : ; . ; n . d J , ' i . i ' . c ' o i d 0 a f ; i " ' d f u r 1 a " .

Nev tdiFi .ir r.iws / I -: .'. qi i ni {li3rrL

Test Report No. : CE/2013/13191 Date: 2013t01t21 Paoe : 6of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15. 91207 LAUF

rlfll tlt! ttt]l

lest ltem(s) Unit Me{hod MDL R€6ultLimitNo.1

Chlorof luorocarbon-1 13 (CAS No.:76-13-1)

mg/Kg With reference to US EPA 502 1method. Analysis was performed byGC/t S.

1 n.d.

Chlorcfluorocarbon-1 14 (CAS No.l7efi-2)


1 n.o.

Chlorotluorocarbon-l 15 (CAS No.:76-15-3)

msasWith reference to US EPA 5021method. Analysis was performed byGC/MS,

1 n . d .

Group lllChlorof luoroca6on-1 3 (CAS No.:75-72-9)

mg/kg With reference to US EPA 502 1method. Analysis wEs perfomed byGC/MS.

1 n.d-

Chlorof luoroca6on-'1 1 1 (CAS No.:354-56-3)


1 n.d-

Chlorofluoroc€rbon-'112 (CAS No.:76-12-O)

mlyKg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n . d .

Chlorof luorocarbon-2l 1 (CAS No.:422-78-8)

mgikg With reference to US EPA 5021method. Analysis was pertormed byGC/MS.

'I n.d.

Chlorof luorocarbon-21 2 (CAS No. :3182-%-1)

mg/Kg With refefence to US EPA 5021method. Analysis wEs performed byGC/MS.

1 n.d.

Chlorof luoocarbon-21 3 (CAS No.:2354{6-5)

mg/kg With reference to US EPA 5021method- Analysis was performed byGC/[rS.

1 n.d.

Chlorof luoroca6on-214 (CAS No.:29255-31-0)

mgKg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

Chlorof luorocarbon-215 (CAS No.:425943-2)

mgi Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

n .d .

. ! . .;

"'.i;-.. ; *d b' h6 cmou

,no b' e€dM c romar dnoments rd pd 6 hr3 and cot ions b' Lrecl;;;;tmh ;A;ii-6; md :.$-r,sr3ne . reo rE 'n r . ne f l ono -vdFowt i n ' h . 'mbo rca -s iF taon< 3 l ponqb f t v ' r o c iP "d t r sdo* *o , j " t ' o . i * - " " 0 a i r

" mo l imdmb- i 5doo - t ' a t b pno ' l de roo t l a o . i c

( omod i Mv r s ! o zao arasrca o's.ry o' r;sfr-ton ol I e d+n d

.-""'.,ii::lliiillr: r l Y"!:1t]:rt"pjrtrg:.11':11j'-

Test Report No.: CE/201313191 DaIe 2013101121 Paoe 7 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULIIFUNKTIONSKERA[TIK,LUITPOLDSTMBE 15, 91207 LAUF

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Test ltem(e) unit Method I'DLResult

LimitNo.l

Chlorof luoroc€6on-216 (CAS No.l661-97-2)

mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/tUS.

1 n.d.

Chlorof luoroca6on-217 (CAS No.:422-E&6)

mg/kg With referenc€ to US EPA 5021method. Analysis was performed byGC/t S.

1 n.d.

HCFCa(Hydrochlorofl uorocalbons)HCFC-21 (CAS No.: 75434) mg/Kg With reference to US EPA 5021

method. Analy6is was performed byGC/MS.

I n.o,

HCFC-22 (CAS No.: 75-45$) mg/Kg Wilh reference to US EPA 502'1method. Analysis was pertormed byGC/MS.

'I n.d.

HCFC-31 (CAS No.: 593-70-4) mg/Kg With reference to US EPA 5021method. Analysis u/as performed byGC/MS.

'I n.d.

HCFC-121 (CAS No.: 354-14-3) mg/Kg With refefence to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HCFC-122 (CAS No.: 354-21-2) m!/Kg With reference to uS EPA 5021method. Analysi6 was pedormed byGC/MS.

1 n.d.

HCFC-123 {CAS No.: 306-83-2) mg/Kg With refere.ce to US EPA 502 1method. Analysis was performed byGC/rVlS.

1 n.d.

HCFC-124 (CAS No.: 2837-89-0) mg/Kg With reference to US EPA 5021method. Analysis rvas performed byGC/tVS.

n.d.

HCFC-13'1 (CAS No.r 359-28.4) mg/Kg With reference to US EPA 5021method. Analysis was pedormed byGC/tVS.

n.d.

HCFC-132b (CAS No.: 1649-08-7)mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

-nn.'"iJ'""r

" **o

"iuie coma;";b,*

"iGa*eft codod'"s"1eor'sode' .s5i-ier-'-,nd rtro 5b

i J6 i i " oJ . i t i j a ' . i ' . n " , ' " ' , qa i 6 re - , ddod id ' b 'F3ad i , { do ' *La€ - . d t ?n &

rhermed b deiudio onl! d{sh F. aborc ens'n{rdo'' ' l;;;;" b; ;;-ii!i;,;. ilis i; ;'q;,r"";, iir" r*a;m;ry ay lmdb';d *sdon. ro@ery o, disddoi dr he 6n,ent o

Test Report No.: CE/2013/13191 Date:2013101121 Page: 8 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

rll |ltt][ttllll

Test liem(s) Unit Method MDLResult

LimitNo.'l

HCFC-133a (CAS No.: 75-88-7) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/t S.

n.cl.

HCFCI4lb (CAS No.: 1717-00€) mgKg With reference to US EPA 5021method. Anaiysis was performed byGC/MS.

I n.d.

HCFC-142b (CAS No.: 75-68-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n-d.

HCFC-221 (CAS No.: 422-264) mg/kg With reference to US EPA 502 1method. Analysis was performed byGC/l\rs.

1 n.d.

HCFC-222 (CAS No.r 422-49-1) mg/Kg With reference to US EPA 5021melhod. Analysis was performed byGC/MS.

1 n.d-

HCFC-223 (cAs No.: 422-526) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HCFC-224 (CAS No.: 422-54-8) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

HCFC-22sca (CAS No.: 422-56-0) mg/Kg With reference to US EPA 502'lmethod. Analysis u/as performed byGC/MS.

1 n.d.

HCFC-22scb (CAS No.i 507-55-1) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

HCFC-226 (CAS No.: 431-87-8) mg/Kg With reference to US EPA 502'1method. Analysis wes performed byGC/MS.

n.d.

HCFC-231 (CAS No.r 421-94-3) m9Kg With reference to tJS EPA 502'1method. Analysis was Performed bYGC/[iS.

't n.d.

HCFC-232 (CAS No.: 460-89-9) mg/Kg With reference to US EPA 502 1method. Analysis was Performed bYGC/MS.

1 n.d.

ow. m h's 3s B@. FF ul b ne 3

.;;.";;-", is ,rd b, h c-ps y sD.eq,o 6 Gr6rcdoj:i.,.*,pffii;F"1;f;*&,;:,#"r,,!;ri:\t,itr,:xi{.y;%1"iffT"1_i;j ?;:jli:i:",Sblecl lo rems and @ndhons ftr.,m. o. ar .* dstrnra,o, nd.inedd 'nu*"- "t:lll.lj;;1.;:t*"*;,f;:::*i;;fjl,,". if;ti* ilf,;'"-;le:'i:";i;; -?":ig:";',?lli0,:"ii

* * " " "a - , * ' - " - , - . J i i - a ; l ,mom.EF .do - -a ' 6 fdc r e . , & y l 1 a n 1 o n z e d " s d d , . - ' # i ; ; ; ; : ; ; i ; ; * : l i " ^ r ' r o b r o - d i b ' r e * d b r r l l e ' " ' { r o L h e b n

r\eift peicivft rs/:r";iii i ) i il i i 4firb

Test Report No- : CE/201313191 Date:2013101121 Paoe i gof 29

CERAMTEC GMBHGESCHAFTSBEREICH

rllllllat][ ttltMULTIFUNKTIONSKERAMIK,LUITPOLDSTRAEE 15. 91207 LAUF

Te6t ltem(a) Unit method MDL Re€ultLimit

No.1HCFC-233 (CAS No.: 7125-84-0) mg/Kg With reference to US EPA 5021

method. Analysis wa6 performed byGC/MS.

'I n.d.

HCFC-234 (CAS No.: 425-94-5) mg/Kg With reference to US EPA 5021method. Analysis was perlormed byGC/MS.

1 n.d.

HCFC-235 (CAS No.: 450-92-4) rnglkg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.

1 n . d .

HCFC-241 (CAS No.: 666-27-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n . d .

HCFC-242 (CAS No.r 46063-9) mgag With reference to US EPA 5021method. Analysi6 was performed byGC/MS.

1 n .d .

HCFC-243 (CAS No.: 460$9-5) mgKg With reference to US EPA 502 1melhod. Analysis was perfomed byGC/MS.

1 n.d-

HCFC-244 mg/Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

1 n .d .

HCFC-251 (CAS No.: 421-41-0) mg/Kg With reference to US EPA 502 1method. Analysis was pertormed byGC/MS.

1 n.d.

HCFC-252 {CAS No.: 819-00-1) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HCFC-253 (CAS No.: 460-35-5) mdkg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

HCFC-261 (CAS No.: 420-97-3) mg/Kg With reference to US EPA 5021method. Analysis w€s perfomed byGC/MS.

n.d.

HCFC-262 (CAS No.: 421-m-03) mdkg With reference to IJS EPA 5021method. Analysis was performed byGC/MS.

n.d.

I i B . I I l !anv5ub ] . db tGE la | cond lonso ' sed@prn iedowdca i ' ava iab |eon r€

qedb ams sr co-o m\!o' ehdd rinsdidon 'sEs ddd rhere n 6y io &r of b s eumd ; adv 3ad Lh be company s {indino! ar

Test Report No. : CE/201313191 Dale 2013t01t21 paoe | 10 of 29

CERAIVTEC G[/lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15. 91207 LAUF

rtrr lrt][ttt||l

Tegt ltem(s) unit Method MDL ResultLimitNo.1

HCFC-271 (CAS No.r 430-55-7) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

1 n .d .

HalonsHalon-1211 (CAS No.: 353-59-3) mg/Kg With reference to US EPA 5021

method. Analysis wEs performed byGC/MS.

1 n.d.Halon-1301 (CAS No.: 75-63-8) mg/Kg 1 n.d.Halon-2402 (CAS No.: 124-73-2) mg/Kg 1 n.d.CHCs (Chlorinate hydrocarbon)1, 1, 1,2-Tetrachloroelhane (CASNo.:630-206)

mg/Kg With reference to US EPA 5021melhod. Analysi6 w€s performed byGC/MS.

1 n.d.

'1 , 1 ,'1 -Trichloroethane (CAS No. :71-55€)

mdkg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

1 n . d .

'1, 1,2,2-Tetrachloroethane (CASNo.:79-34-5)

mgKg With reference to US EPA 5021method. Analysis wa6 perforned byGC/MS.

1 n . d .

1,1,2-Trichloroethane (CAS No.:79-00-s)

mg/Kg With reference to US EPA 5021method. Analysis $/as performed byGC/t\rs.

I n.d.

1,1-Dichloroethane (CAS No.: 7$34-3)

mgKg With reference to US EPA 5021method. Analysis was performed byGC/MS,

,| n .d .

't ,1-Dichloroethene (CAS No.: 75-354)


1 n.d.

1,1-Dichloropropene (CAS No.:5695&6)

mg/Kg With reference to US EPA 5021method- Analysis was performed byGC/tVS.

n.d.

1,2,3-Tichloropropane (CAS No.:96-184)

mdks With reference to US EPA 5021method. Analysis was pedormed byGC/tVlS.

n.d.

'1,2-Dichloroethane (CAS No.:107-06-2)

mgftg With reference to US EPA 5021method. Analysis was performed byGC/l\,!S.

n.d.

LN4r : i F (V r r iw in rn 1 . 1 ' n i l r i i f r : t { J

Test Report No. : CE/201 3/1 3 1 91 Dale : 2013t01t21 page : .l .1 of 29

CERAMTEC GMBHGESCTIAFTSBEREICH MULTIFUNKTIONSKERAI\4IK,LUITPOLDSTMBE .l 5, 91 207 LAUF

lfl tl|[ tllttl

Test lt€m(s) Unit Method i,DLRegult

LimitNo.l

1,2-Dichloroprcpane (CAS No.:78-87-5)

mg/kg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.

1 n.d.

'l,}Dichloropropane (CAS No. :142-2&9)-

mg/Kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.

1 n.o.

z,2-Dichloropropane (CAS No.:53+20-7',)

mg/Kg with reference to us EPA 5021method. Analysis wa6 performed byGC/MS.

I n.d.

Carbon tetrachloride (CAS No.i56-23-5)

mgikg Wath reference to US EPA 5021method. Analysis was pertormed byGC/MS.

1 n . d .

Chloroethane (CAS No.: 7$00-3) mg/Kg With reference to US EPA 502 1method. Analysis was porformed byGC/MS.

1 n.d.

Chlorofom {CAS No.: 67-66-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/[rS.

1 n.o.

Chloromethane (CAS No.: 74-87-3)

mg/Kg With reference to US EPA 5021method. Analysis wEs performed byGC/MS.

1 n.d.

cis-1,2-Dichloroethene (CAS No.:15G59-2)

mdkg With reference to uS EPA 5021method. Analysis\ ras pertormed byGC/MS.

1 n . d .

ci6-l,3-Dichloropropene (CAS No.l10061-01-5)

mg/Kg with reference to us EPA 502 1method. Analysis was performed byGC/MS,

1 n.d.

Hexachlorobutadiene (CAS No.i8768-3)


'I n-d.

Methylene Chloride (CAS No.: 75-09-2)

mg/kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

Tetrachloroethene (CAS No.: 127-184)

mgI(g With reference to uS EPA 5021method. Analysis was performed byGC/MS,

n.d.

s r lEk t repo ld - r t bs ' s

i ;T f t :k" ' ' ' , . " " " "* - , " . " . " " . " - ; - . " ' " " ' " : . . i " , ' i ' . "s . . *p**"" . i .a 'a-uu"" ' l .osdo!esbA-"e!o 'o 'i * i i " i

" an ' i n t ma r ; i e r c i . r i d . db -em, ' bco r ' . " r ' ' edonLOo@f t1Rd"ms { ' , o -

a1 eas , dco ,d tuo s r8Tseooai ; ; ; ; j b ; i i ; # ; i i " ; ; i ; ; . i " " " ; . ^ d ' * h . * , e ' ' d o . t r | ' 0 r ' a ' ' a d . gh " | - . d k FE ; \ ed on odv and w ,h i d he im so c rems nsMros ' L r v i b i s r r . l a d lF tum"d6;;;(-;;;;;;-;;;;6;i;;oi:a ;; ;;J;, . ;. :ie r,..obidd-.-d -n, oo@r1 d "o 0- re o! @o "oo;#ffi;:p;;;;,-,i;;;:d i;i,;: i;a;t ;iai,n-i;";i h" -"bd

"; r . : r i r ! r ' i ' i t - l r .

Test Report No.:CE/2013/13191 Dale 201310121 Paoe:12 ot 29

CERAMTEC GMBHGESCI-I,AFTSBEREICH

tl| |l lrtl]lIVULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

T€6r ltem(s) Unii method MDLResult

LimitNo.1

trans-1,2-Dichloroethene (CASNo. : 1 56-60-5)


'I n.d.

trans-1,3-Dichloropropene (CASNo.: 10061-02€)

mg/Kg With reference to US EPA 502'method. Analysis was performed byGC/MS.

1 n.d.

Trichloroethylene (CAS No.: 7$.01€)

mg/Kg With refefence to US EPA 5021method. Analysis was performed byGC/US.

'I n.o,

Sum of PBBS mg/Kg

With reference to lEc 62321: 2008 andoertormed bv GC/I\IS.

n.d. 1000lMonobromobiphenyl mg,iKg 5 n.d.Dibromobiphenyl mdkg 5 n .d .Tribromobiphenyl mg/kg 5 n.d.Tetrabromobiphenyl mg/Kg n.o,Pentabromobiphenyl mg/Kg n.d.Hexabromobiphenyl mg/Kg 5 n.d.

Heptabromobiphenyl mgKg 5 n .d .Octabromobiphenyl mg/kg 5 n.d.Nonabomobiphenyl mg/Kg n.d.Decabromobiphenyl mg/Kg 5 n . d .

Sum of PBOE5 mg/Kg n.d. 1000Monobromodiphenyl ether mg/Kg 5 n.d.

Dibromodiphenyl ether mgikg 5 n.d.

Tribromodiphenyl ether mg/Kg 5 n.d.Tetrabromodiphenyl ether mg/Kg 5 n.d.

Pentabromodiphenyl ether mg/Kg 5 n.d.

Hexabromodiphenyl ether mg/kg 5 n.d.

Heptabromodiphenyl ether mg/Kg 5 n.d.

Octabromodiphenyl ether mgKg 5 n.d.

Nonabromodiphenyl ether mg/Kg 5 n.o.

oecabromodiphenyl ether mg/Kg 5 n.d.

i . , ; j i t r : l e t . r \ i

Test Report No. I CE/2013/13191Dale | 2013101121Page : 13 ot 29

CERAMTEC GMBHGESCI-I,AFTSBEREICH iNULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15, 9.1207 LAUF

lm[llt rt]I

Not. :'1. mg/kg = ppm | 0.1wt% = loooppm2. n.d. = Not Detecled3. MDL = Method Detection Limit4. "-"= Not Regulated5. - = Qualitative analysis (No Unit)6. N€gative = Undet€ctable / Positive = DetectableT Testing range of asbestos qualitative analysis is from less than 0.1% to 1OO%. The judgment crjterion: asbestos fibers

being found is shown as "Positive'; asbeslos fibers not being found is shown as,'Negative..

PFOS Refe.ence Intormetion : POPS - (EU) 757m10Outlawing PFOS as substances or preparations in concentrations above O.OOl% (lOppm), in s€mi-finished products ofarticle6 or parts at a level above 0.1%(1000ppm), in textiles or other coated materials above 1pg/m,.

3liffJ*:"iT,:'?jil\"ri+iTi:?i,iii)i:;::ii:?i"T::i:rl'!{i'iili:r!':ti,li;'rflf'l"1-'e@rcd@d eed rtur Mhdrp

ii":l"H*;:;rls,:iixs'.9"r;i"'t*;:ffagfi"u;::"^'J:rffis#j:r,x*ir5'Lri!tr:"i3;xlf;,i:;-x'#;%1:"#il";: rd,rll,l'Ti"'4ri,:"-..r-o'in|;n,*..neo,-d .<-'.*"a,doids";, ti;o; tr: dMm{ F;dre 'edsI e (omLnr\ihdin$''iiiiilni.l *'r"i'*ro" on" a"o *ti".m rns or ce.' +.*"i ';q Fe.d",p".v"d"."po"'blv ' 'o r! LrPl' . t r ' ood ̂ " diliil;a; i."- d*o.ri+e

"e;fi;;l!;;;'.;-*o;;&;1.;i;;: 6;s;t ;iaianai,* .r h. -dei, (

Test Report No.:CEl2013l13191 DaIe:2013101121 Page: 14 of 29

CERA['TEC GI,lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE'15, 9'1207 LAUF

1 ) These samples were dissolved toblly by pretonditioning method according to belolt/ flow chart.( Cf' te€t method excluded )

Name of the person who made measurement Climbgleat YangName of the person in charge of measurement: Troy Chang

2)3)

SamDle Mderial DioestionAcid

S'teel, copper, aluminum, solder Aqua reqia, HNOr, HCl, HE HzO:

Glass HNOy'HF

Gold, platinum, palladium, ce€mic Aqua regia

Silver HN03

Plastic H,SO., H,O,, HNO3, HCI

Others Added appropriate reagent to totaldiOe6tion

Note- : (1) For non{netallic material, add alkaline digestion reagent and heat to 90'95f(2) For metallic material, add pure water and heat to bdling.

r ! { e * h p e . 4 f t t $ / i i : l i i i r d r i r : l i i 4 3 \ 1

Cutting / Preparation

Sample Measurement

Add appropriate amountof digestion reagent

Acid dige6tion by suitable aciddeoended on different samolematedal (as below table)

Microv/ave digestion withHN03/HCI/HF

Heat to appropriatetemperatuae to erdr€ct

1) Alkal iFusion2) HClto dissolve

Add d iphenyltarbazidefor color development

measute the absotbanceat 540 nm by UV-VIS

Test Report No. ICE/2013i/13191Dele :2013101121Page : 15 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 1 5. 91 207 LAUF

]tI|tt][tttutl

PFOA/PFOS analytical flow chart of Ultrasonic extraction (LC/MS) procedure

r Name of the person who made me€surement: Roman WongI Name ofthe person in chaqe of measurement Troy Chang

ffi um*m,1*ffit*'r,*ffi*#iHl*gl+rsirti*ffikNdrripd.tvlriw:i/li: ' n ] ': Iiriti33li

r+elo2)r4rD ||e6Orlr??1 ?1

Test Report No. : CE2013l'13'191 Date 201?,10121 Paoe: 16of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE 15, 91207 LAUF

lm[tr|| ||tt]t

Data

PCTS analytical flow chert

t Name ofthe petson who made measurement Barry T6engr Name ofthe per6on in charge of measurement: Troy Chang

. i r i { r i c f n r \ i

Test Report No. : CE/2013/13191 Dale : 2013101121 Page : 17 of 29

CEMMTEC GMBHGESCFI,AFTSBEREICH MULTIFUNKTIONSKERA[/lIK,LUITPOLDSTMBE 1 5, 91 207 LAUF

ll] ttJflllafll

PBB/PBDE analytical FLOW CHART

I Name ofthe person who made measurement Roman Wongr Name of the person in charge of measurement Troy Chang

First testing process -----'

Optional screen proce6s ....

Confirmation procegs -.>

[J-"'d;---l--------r-------[s-"-lrj--jr"t""t.-tl-T-

Screen analysis

Sample e)draction/Soxhlet method

Concentrate./DiluteExtEcted solution

Filter

Analysis by GC/lvlS

lssue Report

" " " " " " ' f " " " " " "

a;; . : : ' ' . <we p" 'ed owtd ars dbir oll, :T i ;e1d; : - . ;F ; l ;u . ; " ;o€ ; '6hr 'mdcordb4u i ;n rc : .oo . - . ' l dMa ' jdq |

" ' , , . . - ' * * . . " ' , , " , , " ;r i , i j t i i o is ; ; l *m, - rv - " - ' . ,n " . ,uo |cs '+n ' .d ;n i; a ; i i i i ' . i # a j g . * , g , ' r - ' g t : T o o ] g ! j l o B J n d e l ' 9 ? n % d f ' @ o - 4 k T i 3 d o (

u ' { i;:;; ;;;;r;;: : 'oeft | s 5d|" oo'arc"a -dib'

l i i i ,: r !l I {lii:rri

Test Report No. : CE/2013/13191 Dale:20131O1n1Page : 18 of 29

CERAI,TTEC GI,/lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15. 91207 LAUF

PCBe analytical flow chart

r Name ofthe person who made measurement Bafiy Tsengr Nameoftheperson incharge of measurcment: Troy Chang

Data

lll |ltt][ttlllt

M ti rhlsresr €Don rerer ont ro be tpdorMtbpembsondrE

rhsiftinmr'a €sid b! lh€ cmoanv eubEci ro 'ls Gne'arcndiions orseruie or ed o6'ldat a$ abeonie ms .M,@iditons lrhand ror € adrof, c romd dntum.nb e 6 e d 6 re' ms and C.d ton s lo' Ered msad.Cond( ons/rerm* Dotuft

d u'is. dion isues derned bere i tuv s Ihe companvs nnd'nqs ari heheo ib i n l e iwn1ono i vandw id i n l he ] im$o l c i e i 1sns1 rc i ons f ; nyTheco Inpas$ |e Iespon3b |ftnsdon rrom err"vnq ri h., adFioftJml' hEoodm"lrConprnJ diy iaLtdzeo arleu on

Test Report No. : CE/2013i13191Dale:2013101121Page : 19 of 29

CERAMTEC GMBHGESCHAFTSBEREICH [/|ULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 1 5, 91 207 LAUF

Chlorinated Paraffins analytical flow chart

r Name oflhe person who made measurement: Bary Tsengr Nam€ of the person in charge of measuremenl Troy Chang

Data

tl][ || t|:ll]I

a m o € ' : e e e d I i ' 6 r ? o o ' € o' , t . - I . t i ,

i i i i i . i . * . " * . * o " o e c o . o a ; ' ' o d b ' i c s t . | L d d ' o ' ' d . o l , o ' 3 e e * o A d e 3 s 9 J - l;; ;i; ;.;;; ;;;' ;r;. ;;;B &;ed b rems rm cdiGmb 0 Eranrcn( ooom.{ . ar "B {- "o_ .innn;iiri,h ,omnta;.; d :1d'do sr! d,,rd h.r,he ru or r 'n,ei!en, on oi v dnd dbinher+aorcrcn \'ran01"; ; ; ; ; ; ; ; ' ; " ^ n ; ; i ; ; i o i " * o o t a " . ' ' c . * . u " ' * . ' o , ' o o J m ' 6 i I o o J - e { o ' '( dmoa., hr ,rd bo zen ,n4no'

N€r tdFi.[r ri iwri / i i-: ' !: ]. ' i : . r {iLli! l i

Test Report No. : CE/2013/13191D?[e:2013101121Page:20 ol 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAIV]IK,LUITPOLDSTMBE 1 5. 91 207 LAUF

Analysis flow cha.t for determination of Asbe6tos

I Name ofthe person who made measuremenl: Victor KaoI Name of the person in charge of measurementt Wendy Wei

( Reie.ence method: EPA 600/R-93/l 16l

Sampling

Contai ning AsbestovPositive Not conhining Asbesto6/ N€gative

!]l[ttt ltt]l

" i t , 1rh6 do.irm.m E Lsusd s rha com"nd b . l . {on . r .mar o@merb . . ' iF - d re- 'dndco ld ro 's ro Fsa vdm(odor - " -3€Dor_ena

ndemnrca( on and 'LlNd d6 6su6rheriftdl6 d.iwi{on otrlv a qsi r;nrTh?com0anyssercspoi5br'ry'' 'o Lsc'en and'hsdocum.ndt r sdo hma . G ro a r i t e nConpaiy ay unauhdzad a lsrdion

k { 4 r t P ( r y r . e d / i . l : i . i 1 1 i t * j : t j r

Continue when probl€rnsarc encournefed withDS-PLM and/or for quality assurance pufposes

Asbestos identifc€lion by dispetsion stainingpola zed light micrcscope (DS-PLM)

Asbe€tos idenlifcation by X-faydiff raclion speclrometer (XRD)

Test Report No. : CEl2013i/13191 Date : 2013101121 Paae : 21 of 29

CERAI,iITEC GMBHGESCHAFTSBEREICH

!

I

Analytical flow chan of Organic-Tin content

Name ofthe person who made measurement: Ginny ChenName ofthe person in charge of measuremenl Troy Chang

It] tttI[ltr tMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

ui4s dheNs sbcd hs e$ 6 s,o!.n ,n h'' '6d rcpoi erer o'u.bri€ 3aT?fFr,!".i:i .iii:iif...;r':pd

**d b

"K1 i l ; "1 . , . " ; , , " . * . *# ; " , " . * ' " " ; ' * , . J , * * . '9 {ep ' ' coo ' " l "a ] ' .€ ,bPo1 'a;;.rii;etu .-d oie.- ',oFc6 krsmd hthE,o L] . i i i ' i " ' i n * l "nd6mnid lo ,a t '1 r$oo '9ae ' *nare6 ' : , i , i i "nnn.s i io ; { ' , i .Nsddd'r. t-n:

"i s l;* m. -rv,

" w

3'Ji;::i:,m^'tf:3.'illli'i*:?fJliP','€*":ii#l;iik"," '""doneid-" *vbfi;;;;ih;i6.1eiii"brih" ""

Test Report No.:CE201?'13191 Date:2013101121 Page: 22 of 29

CEMMTEC GIVBHGESCHAFTSBEREICH

rtl ltrt ttlllllMULTIFUNKTIONSKERAI/|IK,LUITPOLDSTRABE 15, 91207 LAUF

PCNS analytical flow chart

r Name ofthe person who made measurement: BarryTsengI Name of the person in charge of measurement; Troy Chang

Data

Test Report No.: CE/201313191 DaIe 2013101121 Paqe: 23 of 29

CERAMTEC GMBHGESCHAFTSBEREICH IVULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 15. 91207 LAUF

tn[lnl|l l|l]t]

Analytical flow chad of phthalate content

I Name of the person who made measufementr Roman Wongr Name of the pe6on in charge of measurement: Troy Chang

Data

' ' r i n l ! r i r r f t i3 r l ' i

Concentrate./Dilute Extracted solution

An€lysis was perfomed by GC/MS

Test Report No. : CE/2013/13191 Dale : 2013101121

CERAMTEC GMBHGESCIIAFTSBEREICH

Page:24 ol 29

91207 LAUFll| |l!] |lttl

I,IULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 1 5,

I

I

Formaldehyde analytical flow chart

Name of the pe6on who made measurement: Scott KuN€me of the person in charge of measurement: Troy Chang

I Test Method : US EPA 83154 ' ISO 17226-1 ]

Dala

Derived by DNPH ConcentrateJDilute Extractedsolution

Test Report No. :CE/2013 /13191Dale'.2013101121Page : 25 of 29

Analyais flow chart for determination of PVC In material

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAI,!IK.LUITPOLDSTMBE 1 5. 9'1 207 LAUF

||]tIltt][t [Il

I

I

Name ofthe person who made measurement: Ginny ChenName of the person in charge of measurement: Troy Chang

Sample analyzed by FTIR

Check wave-number of c-cl bonding

Test Report No. CE2013,/13191 Dale:2O1AO1121 Page : 26 of 29

CERAMTEC GMBHGESCHAFTSBEREICH

|ln[ t][tll]rMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

II

DBBT analytical flow chart

Name ofthe pe6on who made me€surement Roman WongName ofthe person in charge of measurement: Troy Chang

Dala

. i : r , i l r 1 i l i t - l j

Sample pretreatmenvseparation

Sample extraction by 6oxhlet method

Test Report No.:CEl2013/13191Dale: 2o13lo1nl Page 27 ot 29

CERAI.TTEC GI,/IBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAI/|IK,LUITPOLDSTRABE'1 5, 9'1 207 LAUF

Analytical flow chart of halogen content'1) Name of the oerson vt/t|o made measurement: Rita Chen2) Name of the person in charge of measurement: Troy Chang

||l ||tt]tI|tttll

9fj] iH*"", ';:* ' ' ,*.- '"], ' ' , ;;"...""*.l"i"".-".n.*,." ' '-"*"'.n-.*'."1' ; ; t i ; d f u .bmddmmmE' *oFdhh rsmdcodbn 'b ; ; i . nn . cDo6m{ | J# { , od 'ri,:"luri6'in

'rn,r Ardbs; ;jlnri'n dhatu-.in in i

" l " d* . " - , , " * i ' r . . , so - t "n .c i " . , ; ' ; ' : ;a ; . ; ; ; ' - ; - "F*br ' rv rb c* r id ' '<dc ' -c

r i in i i , " j r . * lo i rua i r " monoodm. . ' i ' doo .ne1rcomoanv try unau,tu'z& abad.,-q.ry * I'kh*- drb-tu;it;iFt€ne or th sdturud smawtu

i. ., + i _ri;\l

lFli33!1

Sample pretreatment / separation

Wdghting and putting sample in cell

Oxygen Bomb Cornbustion / Absorption

Dilution to fixed volume

Analysis was performed by lC

Test Report No. : CE/20'13/13191Dai'e : 2O13101n1 Page : 28 of 29

CERAMTEC GMBHGESCHAFTSBEREICH l/TULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 1 5, 91207 LAUF

Analytical flow chart ofvolatile organic compounds (VOCS)

I Name ofthe oe6on who made measurement : Chun WuI Name of the person in charge of measurernent : Shinjyh Chen

(Reference method : US EPA 5021)

lfl||tt][ttl||ll

Sample pretreatment

Take sample and put it intoheadspace glassware.

Analy6is was per{ormed by GCYlrs

Test Report No. : CE2013/13191D e: 2013101121Page : 29 of 29

cERAlilTEC GIVBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[/|IK,LUITPOLDSTRABE 15, 91207 LAUF

'The tested sample/ part is ma*ed by an arrow if ifs shown on lhe photo.'

'* End of Repod "

ll]t ttflll0llll

kNewr i t s i . i vL {$ i , : - : ' . ! r , d r i i i l i l f n r \ i

Test Report Number : TWNC00302922

Authorized by: On Behalf of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0302922* Page 1 of 10

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse, S.A. de C.V. Date : Mar 20, 2013 Blvd. Fausto Z. Martinez #1800

Col. Magisterio Seccion 38 C.P. 26070 Piedra Negras, Coahuila, Mexico

Sample Description:

One (1) group of submitted samples said to be : Part Description : Sand Part Number : 311.7374.5000 Date Sample Received : Mar 14, 2013 Date Test Started : Mar 14, 2013

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Number : TWNC00302922

Test Conducted

*THJ0302922* Page 2 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary: Result

Test Item Unit Test Method Sand podwer

RL

Heavy Metal

Cadmium (Cd) Content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Lead (Pb) Content ppm


ND 2

Mercury (Hg) Content ppm


ND 2

Chromium VI (Cr6+) Content ppm

With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer.

ND 1

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB)

ppm ND 5

Dibrominated Biphenyls (DiBB)

ppm ND 5

Tribrominated Biphenyls (TriBB)

ppm ND 5

Tetrabrominated Biphenyls (TetraBB)

ppm ND 5

Pentabrominated Biphenyls (PentaBB)

ppm ND 5

Hexabrominated Biphenyls (HexaBB)

ppm ND 5

Heptabrominated Biphenyls (HeptaBB)

ppm ND 5

Octabrominated Biphenyls (OctaBB)

ppm ND 5

Nonabrominated Biphenyls (NonaBB)

ppm ND 5

Decabrominated Biphenyl (DecaBB)

ppm

With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

ND 5


Test Conducted

*THJ0302922* Page 3 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Result

Test Item Unit Test Method Sand podwer

RL

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE)

ppm ND 5

Dibrominated Diphenyl Ethers (DiBDE)

ppm ND 5

Tribrominated Diphenyl Ethers (TriBDE)

ppm ND 5

Tetrabrominated Diphenyl Ethers (TetraBDE)

ppm ND 5

Pentabrominated Diphenyl Ethers (PentaBDE)

ppm ND 5

Hexabrominated Diphenyl Ethers (HexaBDE)

ppm ND 5

Heptabrominated Diphenyl Ethers (HeptaBDE)

ppm ND 5

Octabrominated Diphenyl Ethers (OctaBDE)

ppm ND 5

Nonabrominated Diphenyl Ethers (NonaBDE)

ppm ND 5

Decabrominated Diphenyl Ether (DecaBDE)

ppm

With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

ND 5

Halogen Content

Fluorine (F) ppm ND 50

Chlorine (Cl) ppm 154 50

Bromine (Br) ppm ND 50

Iodine (I) ppm

With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by Ion Chromatograph. ND 50

Remarks: ppm = parts per million based on weight of tested sample = mg/kg

ND = Not detected

RL = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Mar 14,2013 Test Period : Mar 14,2013 to Mar 19,2013


Test Conducted

*THJ0302922* Page 4 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅱ) Limit: RoHS Limit

Restricted Substances Limits

Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.


Test Conducted

*THJ0302922* Page 5 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by GC-MSD

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Make up with deionized water and add diphenyl-carbazide solution

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Negative *2

Substrate Plating

Weigh sample and add alkaline solution

Definite temp. extraction

Cool and filter the extract

Cr6+

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Confirm the tested samples are totally dissolved


Test Conducted

*THJ0302922* Page 6 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Remarks: *1: List of Appropriate Acid：

Material Acid Added for Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.


Test Conducted

*THJ0302922* Page 7 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Test for Halogen Content Reference Standard：EN 14582

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the bomb at room temperature

Transfer the absorbent into a volumetric flask


Sampling/grinding or cutting

Analyzed by ion chromatography


Test Conducted

*THJ0302922* Page 8 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Test For Phthalates Contents Reference Method: EN 14372: 2004



By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD


Test Conducted

*THJ0302922* Page 9 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.



By soxhlet extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MSD


Test Conducted

*THJ0302922* Page 10 of 10



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Photo

Test Report Number： SHAH00362261

Authorized by： For intertek testing services Ltd., Shanghai

Jacob Lin General Manager

Page 1 Of 5 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

Applicant： ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU Date： JAN 18, 2013 GMBH

GEWERBESTRASSE 87,D-98669 VEILSDORF, GERMANY

Sample Description： Two (2) pieces of submitted samples said to be ： (1)Substrate. (2)Plating. Item Name ： Wire With Plating. Item No. ： 101 -- 271.0 --- tin plated,copper wire,Cu,Sn --%. Country Of Origin ： Germany.

************************************************************************************************************************************************************ Tests Conducted：

As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************

To be continued


Tests Conducted





(A) Test result of RoHS Directive： Result Testing item (1)

Cadmium (Cd) content (mg/kg) ND Lead (Pb) content (mg/kg) 24 Mercury (Hg) content (mg/kg) ND Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2) ND

Result Testing item (2)

Cadmium (Cd) content (mg/kg) / Plating ND Lead (Pb) content (mg/kg) / Plating 21 Mercury (Hg) content (mg/kg) / Plating ND Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2) / Plating ND

Remark：mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter ND = not detected

(B) RoHS Requirement：

Restricted substances Limits Cadmium (Cd) 0.01% (100 mg/kg) Lead (Pb) 0.1% (1000 mg/kg) Mercury (Hg) 0.1% (1000 mg/kg) Chromium (VI) (Cr6+) 0.1% (1000 mg/kg)

The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.

(C) Test method： Testing item Testing method Reporting limit

Cadmium (Cd) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 mg/kg

Lead (Pb) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 mg/kg

Mercury (Hg) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 mg/kg

Chromium (VI) (Cr6+) content (for metal)

With reference to IEC 62321 Edition 1.0: 2008, by boiling water extraction and determined by UV-VIS Spectrophotometer.

0.02mg/kg with 50cm2

(in testing solution)

Date sample received：Jan.14, 2013 Testing period： Jan.14, 2013 To Jan.17, 2013

************************************************************************************************************************************************************ To be continued


Tests Conducted





(D) Measurement flowchart：

Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents Reference standard: IEC 62321 Edition 1.0: 2008

Remarks： *1: list of appropriate acid：

Material Acid added for digestion Polymers HNO3,HCL,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

************************************************************************************************************************************************************ To be continued


Weigh sample and for different material, digest

the sample with appropriate acid*1


Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp. Extraction

Make up with deionized waterand add diphenyl-carbazide

solution

Cr6+

Weigh sample and add organic

solvent

Soxhlet extractionor

Solvent extraction

Concentrate the extract and make up with organic

solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples

Boiling water extraction

Metal Polymers / electronics

Positive*2

Confirm the tested samples are totally

dissolved

No

Cool and filter the extract

Yes


Tests Conducted





************************************************************************************************************************************************************

To be continued


Tests Conducted





************************************************************************************************************************************************************

End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Test Report. No. SHAEC1317518847 Date: 06 Sep 2013 . Page 1 of 6.

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO., LTD .

XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE, CHINA

.

.

The following sample(s) was/were submitted and identified on behalf of the clients as : LEAD-FREE SOLDER

WIRE.

SGS Job No. : SP13-026309 - SH .

Model No. :. YTW102（692539-002）.

Composition : . Sn2.0CuRE.

Date of Sample Received : . 03 Sep 2013.

Testing Period : . 03 Sep 2013 - 06 Sep 2013 .

Test Requested : . Selected test(s) as requested by client. .

Please refer to next page(s). .

Please refer to next page(s). .

Test Method : .

Test Results : .

Based on the performed tests on submitted samples, the results of Lead,

Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB),

Polybrominated diphenyl ethers (PBDE) comply with the limits as set by RoHS

Directive 2011/65/EU Annex II; recasting 2002/95/EC. .

Conclusion :.

Signed for and on behalf of

SGS-CSTC Ltd. .

JJ Fan.

Approved Signatory .


Test Results : .

Test Part Description : .

Specimen No.. SGS Sample ID. Description.

1. SHA13-175188.040 Silvery metal wire .

Remarks :.

(1) 1 mg/kg = 1 ppm = 0.0001% .

(2) MDL = Method Detection Limit .

(3) ND = Not Detected ( < MDL ) .

(4) "-" = Not Regulated .

RoHS Directive 2011/65/EU.

Test Method : . (1) With reference to IEC 62321-5:2013, determination of Cadmium by ICP-OES.

(2) With reference to IEC 62321-5:2013, determination of Lead by ICP-OES.

(3) With reference to IEC 62321-4:2013, determination of Mercury by ICP-OES.

(4) With reference to IEC 62321:2008, determination of Hexavalent Chromium by spot test /

Colorimetric Method using UV-Vis.

(5) With reference to IEC 62321:2008, determination of PBBs and PBDEs by GC-MS. .

040.

Cadmium (Cd) . 100 mg/kg. 2 ND

Lead (Pb). 1000 mg/kg. 2 140

Mercury (Hg). 1000 mg/kg. 2 ND

Hexavalent Chromium (Cr(VI)) . - - ♢ Negative

Sum of PBBs. 1000 mg/kg. - ND

Monobromobiphenyl . - mg/kg. 5 ND

Dibromobiphenyl . - mg/kg. 5 ND

Tribromobiphenyl . - mg/kg. 5 ND

Tetrabromobiphenyl . - mg/kg. 5 ND

Pentabromobiphenyl . - mg/kg. 5 ND

Hexabromobiphenyl . - mg/kg. 5 ND

Heptabromobiphenyl . - mg/kg. 5 ND

Octabromobiphenyl . - mg/kg. 5 ND

Nonabromobiphenyl . - mg/kg. 5 ND

Decabromobiphenyl . - mg/kg. 5 ND

Sum of PBDEs. 1000 mg/kg. - ND

Monobromodiphenyl ether . - mg/kg. 5 ND

Test Item(s). Limit. Unit. MDL.


Test Item(s). Limit. Unit. MDL. 040.

Dibromodiphenyl ether . - mg/kg. 5 ND

Tribromodiphenyl ether . - mg/kg. 5 ND

Tetrabromodiphenyl ether . - mg/kg. 5 ND

Pentabromodiphenyl ether . - mg/kg. 5 ND

Hexabromodiphenyl ether . - mg/kg. 5 ND

Heptabromodiphenyl ether . - mg/kg. 5 ND

Octabromodiphenyl ether . - mg/kg. 5 ND

Nonabromodiphenyl ether . - mg/kg. 5 ND

Decabromodiphenyl ether . - mg/kg. 5 ND

Notes :.

(1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex II

(2) ◇Spot-test:

Negative = Absence of Cr(VI) coating, Positive = Presence of Cr(VI) coating;

(The tested sample should be further verified by boiling-water-extraction method if the spot test result

is Negative or cannot be confirmed.)

◇Boiling-water-extraction:

Negative = Absence of Cr(VI) coating

Positive = Presence of Cr(VI) coating; the detected concentration in boiling-water-extraction solution is

equal or greater than 0.02 mg/kg with 50 cm² sample surface area.

Information on storage conditions and production date of the tested sample is unavailable and thus

Cr(VI) results represent status of the sample at the time of testing. .

Halogen.

Test Method : . With reference to EN 14582: 2007, analysis was performed by Ion Chromatograph (IC). .

Test Item(s). Unit. MDL. 040.

Fluorine (F). mg/kg. 50 ND

Chlorine (Cl). mg/kg. 50 354

Bromine (Br). mg/kg. 50 ND

Iodine (I). mg/kg. 50 ND


ATTACHMENTS

RoHS Testing Flow Chart

1) Name of the person who made testing: Jan Shi/Star Wang/Shara Wang/Gary Xu 2) Name of the person in charge of testing: Jeff Zhang/George Xu/ Jessy Huang 3) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr

6+

and PBBs/PBDEs test method excluded)

Cr6+

Adding 1,5- diphenylcarbazide

for color development

UV-Vis

Nonmetallic material

Metallic material

Adding digestion reagent

DATA

A red color indicates the

presence of Cr6+

. If necessary, confirm with

UV-Vis.

Sample Preparation

Sample Measurement

PBBs/PBDEs

Sample solvent extraction

Concentration/ Dilution of extraction

solution

Filtration

GC/MS

DATA

ICP-OES

Solution

Filtration

Residue

1) Alkali Fusion / Dry Ashing

2) Acid to dissolve

Pb/Cd/Hg

Acid digestion with microwave/ hotplate

DATA

Heating to 90~95℃ for extraction

Filtration and pH adjustment

Boiling water extraction

Adding 1,5- diphenylcarbazide

for color development

Spot test Positive

Negative

DATA


Halogen Testing (oxygen bomb) Flow Chart

1) Name of the person who made testing: Sisily Yin

2) Name of the person in charge of testing: Linda Li

Sample cutting/preparation

Sample measurement

Combustion in oxygen bomb

Dissolved in an absorption

solution

Filtration

Analyzed by ion

chromatography. Double confirm

by other instruments, if

necessary

DATA


Sample photo: .

SHAEC1317518847

SHA13-175188.040 .

SGS authenticate the photo on original report only .

*** End of Report *** .

TEST REPORTNO. : 4002R1 30403070-2R02 oate: Apr08, 2013

Customer: Suzhou FuHong Electronic IndustrialCo., Ltd.Add'€gs: NO.89WEI DU RoAD, WANGTING ToVvN, XIANGCHENG DISTRICT, sUzHoU. cHINAReport on th€ submittad sample said to beSample name: r{Q copper shell

Page 1 of4

in the submitted samole in

itod€l:,

ItemrLot

uatertat;/ I iEuyer: / \Supptier: \,_--_./tlanufacturer: /

Samplo recelved dato;TeEtlng perlod; From Apr03,

Testinc Rsouested \

As specified by client, to determine the Lead, Cadaccordanca with Directive 20't1l65/EU (RoHS).

Tostinq m6thod:

I ( \ , l\ * , , ' zrohtra.-yelury'i

Conclusion:

Wlen tested as specified, the submitted sample complied with the requirements of Directive 2011/6S/EU (RoHS).

***FOR FURTHER DETAILS, PLEASE REFER TO THE FOLLOWNG PAGE(ST**-

Signed for and on behalf of

ShenzhenAOV Testing Technology Co., Ltd, Kunshan B.anch

,.r"Or.X"r, fr?ZLi lingting, Maggie

Chemical Tesl Director

n"ui","oov' ll/€j h i\Wang Wexin, Weikin

Technical Director

Hotl ine400 700 8600

IEC 62321: 2008, section 9

IEC 62321: 2008, seclion I

IEC 62321; 2008, section 7

IEC 62321: 2008, Annex BNots:-* 0.02 mg/kg refers to the MeL ofsample extraction tiouid.

+prou.oov44Yuan Qi, Mickey

Lab Manager

SHEIIZH€'{ AOV TESTIJ{G T€CHM)LOGY CO.,LTD.TU SfiAN SRAI{CHNo 8 inhech(o.d, Znonrnr Tq*n. Kurhrn Cd!, Jl'ng5u rrcvrnco, Chr.r

td. +46.512.56r0adb t.r {6.5t2-5510 aCog Hfis; /repr..ovr c€., po.t od! ?r9tOOlAl!€.t'on i6 dlnw^ l. lrre |!rm! ann.ondrton$ ofhr6doe€rt.ait

ngv"RF#;qt

NO.r A002R1 30403070-2R02

T63t Flow:

TEST REPORTDate:Apr08, 2013

Content (Metal substrate)

Page 2 ol 4

1. To Detemine

t o

Add the digestion solution; the

vessel is heated until the sample

has been dissolved

Add H2O2 untilthe sample is clear

Cooling the vessel, filter; washed and

filled to the mark with distilled water.

The sample is digested in the

microwave oven following a specific

decomposition program.

Add the digestion solution, close

the microwave vessel.

Cooling the vessel, filter; washed and

filled to the mark with distilled water.

Vveigh lhE sample

into a vessel.

Chromium Content (boiling- water- extraction): (Metal substrate)

Remove the sample, and cool

the beaker to room temperature,


Heat 50 mL of Dl water in the

beaker to boiling for 10 min

Test the sample solution and the 0.02

mg/kg standard solution by UV-VIS.

4. To Oelermino d, Calmium and Mercury Content (Plating)

SHENZHEII AOV TESTI'{G T€CHNOTOCY CO.,LTO.|(UI{SHAN EBAI{CHr|o ! xr.e@ R.rd, thdih ror^_ Xuh.nrn Cn'' Jir.Ors p.ov,rr.?, Ctm4

r.r. a.6-rr2.t6ior0oo FrF.66-5r2,srloato8 }|t|r: //*we..ovt.4n po.tcod! 2r$oo{Att.n!6n € d6*. lo Lne t.rbr.nd @ndrtrof,3 etunred ova.hnt,

Cooling, filtel washed and filled

to the mark with Dl water.

Tested by:

'sF#gt

NO.: A002R13040307e2R02

5 To D€termlPtl€xavalent chromium content in colodess and colored chromate coating on metals: (plating)

u'l"""ji_l"ll, WaI

SHENZHEI'I AOV TESTIT{G TECH'{OI.OGV CO.,LTD.KUT{SIIAI{ BRANCHtlo I Minlr|rn (o.d. Zh.!rlr' ro*n. t(!.rh.n Cdy, ,rq,r,/ p.!encr, Ctf.

lii .t6.tr2.t6t0t00O F.s.t6,Sr2.551OEr00 rnb://ire,.ort..sfl ft.icoda lri3oo{a||o.r1ont. diawnb lhe rern! and {ndit6tr5 pahts{t olonrdt)

TEST REPORTDate: Apr.08, 2013 Page 3 of 4

Hotl ine400 700 8600

lf the test result is positive,

the sample is considered tohave hexavalent chromium

sample solution

and the 0.02 mg4(g

standard solution

Boiling- water- extractionprocedure shall be used toverify the result

lf there is interference or it is hard to decide whetherthe sample have the hexavalent chromrum

Remove the sample, and coolthe beaker to room temperature,


Take the (5015) cm'zsample in the beaker.

Heat 50 ml of Dl water in thebeaker to boiling for 10 min

Test the sample solution and the 0.02mg4(g standard solution by UV-VIS.

Samplo Descriptlon:

Code Sample Description Code Sample DescriptionLead wire substrate Copper shell substrate

2-2 Lead wire Plating 24 Copper shell Plating

Teat Results:

Item Unit RoHS Limit Result

2-3Lead (Pb) mg/kS 1000 N.D. N.D. N.D. N.D.Cadmium (Cd) mg/kg 100 N.D, N.D, N.D. N.D.Mercury (Hg) m9I(g 1000 N.D. N.D. N.D. N.D,Chromium (CrVI) mg/kg 'r 000 Negative Negative Negative Negative

-specimens, which requested to determin. Lead, cadmium and Mercury content, have b€en dissorved compte.ry.-N.D.=not detecled(<MeL)

NO.: A0o2R 1 do4o307o-2R02

Noto:

-MQL=Melhod

-PThe test is based onmaybe cannot stand

-Photo is inctuded

TEST REPORTDete: Apr08, 2013 Page 4 of4

have Hexavalent Chromium by spot-test.boiling-water-extrac,tion method if the spot test rEautt ia uncerfain or

is a single layer and each part is unitorm. The test result

*End of Reporf**

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|^ri.nr,oo i. dr.r. to rh. r. rhr nd cond,hon6 p,nr.o cvarb;;

Hotline400 700 8600

( The

L€ad wir€ copper shelt

Documents

ICP Test Report Certification Packet/media/files/littelfuse/technical... · Total Parts Raw Material Part Number Raw Material Description Page(s) 1 901-556 Cap base & plating 3-6