ICP Test Report Certification Packet/media/files/littelfuse... · Form 585-047 Rev. A 1 2/21/06 2 Table 1: List of Raw Materials covered by this report . Parts P/N Raw Material Description

Form 585-047 Rev. A 1 2/21/06 1

ICP Test Report Certification Packet

Company Name: Littelfuse, Inc.

Product Type: Metal Oxide Varistors

Product Series: LA Series RoHS Compliant models

Issue Date: March 8, 2013

It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive

2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to

be used for unit parts, for packing/packaging materials, and for additives and

the like in the manufacturing processes.

In addition, it is hereby reported to you that the parts and sub-materials, the

materials to be used for unit parts, the packing/packaging materials, and the

additives and the like in the manufacturing processes, are all composed of the

following components.

Issued by:

< DGLF Environmental, Health & Safety Engineer >

(1) Parts, sub-materials and unit parts

This document covers the Surface Mount Varistors MHS/MLE/MLAxxxxNR

compliant series products manufactured by Littelfuse, Inc.

Please see Table 1 for raw materials used.

(2) The ICP data on all measurable substances

Please see appropriate pages as identified in Table 1

Remarks：

Form 585-047 Rev. A 1 2/21/06 2

Table 1: List of Raw Materials covered by this report

Parts P/N Raw Material Description Page

1 N/A Black disc, type including DD,DM,DP,DV,DH,HD,HH and HM 3-42

2 N/A Silver Paste 43-48

3 N/A Pb-free Solder Bar 49-57

4 N/A Tinned Copper Wire 58-70

5 N/A Epoxy, Red HF 71-76

Test Report Number: SZHH00699643

Authorized by: For Intertek Testing Services Shenzhen Ltd.

Ben N.L. Lin General Manager

Page 1 of 5 Intertek Testing Services Shenzhen Ltd.-TFH Division

7/F., ShekouTechnology Main Building, Industrial 7th Road,Shekou,Shenzhen, China Tel: (86-755) 2602 0111 Fax: (86-755) 2683 7118/9 Postcode: 518067

Attention is drawn to the terms and conditions printed overleaf.

Applicant: LITTELFUSE, INC Date: Jun 19, 2012 8755 WEST HIGGINS ROAD SUITE

500CHICAGO IL 60631 USA

Attn: KRISTEEN BACILA/ARSENIO CESISTA JR.

Sample Description:

One (1) submitted sample said to be DD black disc. Tested component: black solid material.

**************************************************************************************************************************************

Tests conducted:

As requested by the applicant, refer to attached page(s) for details. **************************************************************************************************************************************

Conclusion:

Tested Samples Standard Result Tested component of submitted sample

Restriction of the use of certain hazardous substance in electrical electronic and equipment (RoHS Direction 2002/95/EC and supersedure 2011/65/EU)

Pass

*********************************************************************************************************************************


Tests Conducted




RoHS Chemical Test (A) Test Result Summary:

Testing Item Result

Cadmium (Cd) Content (mg/kg) ND(<2) Lead (Pb) Content (mg/kg) ND(<2) Mercury (Hg) Content (mg/kg) ND(<2) Chromium (VI)(Cr6+) Content (mg/kg) 10 Polybrominated Biphenyls (PBBs)(mg/kg) Monobromobiphenyl (MonoBB) ND(<5) Dibromobiphenyl (DiBB) ND(<5) Tribromobiphenyl (TriBB) ND(<5) Tetrabromobiphenyl (TetraBB) ND(<5) Pentabromobiphenyl (PentaBB) ND(<5) Hexabromobiphenyl (HexaBB) ND(<5) Heptabromobiphenyl (HeptaBB) ND(<5) Octabromobiphenyl (OctaBB) ND(<5) Nonabromobiphenyl (NonaBB) ND(<5) Decabromobiphenyl (DecaBB) ND(<5) Polybrominated Diphenyl Ethers (PBDEs)(mg/kg) Monobromodiphenyl Ether (MonoBDE) ND(<5) Dibromodiphenyl Ether (DiBDE) ND(<5) Tribromodiphenyl Ether (TriBDE) ND(<5) Tetrabromodiphenyl Ether (TetraBDE) ND(<5) Pentabromodiphenyl Ether (PentaBDE) ND(<5) Hexabromodiphenyl Ether (HexaBDE) ND(<5) Heptabromodiphenyl Ether (HeptaBDE) ND(<5) Octabromodiphenyl Ether (OctaBDE) ND(<5) Nonabromodiphenyl Ether (NonaBDE) ND(<5) Decabromodiphenyl Ether (DecaBDE) ND(<5)

Chemist: Wang Haijun/Zeng Guoliang mg/kg = milligram per kilogram = ppm < = Less than

ND = Not detected *************************************************************************************************************************************


Tests Conducted




(B) RoHS Requirement:

Restricted Substances Limits Cadmium (Cd) 0.01% (100 mg/kg) Lead (Pb) 0.1% (1000 mg/kg) Mercury (Hg) 0.1% (1000 mg/kg) Chromium (VI) (Cr6+) 0.1% (1000 mg/kg) Polybrominated Biphenyls (PBBs) 0.1% (1000 mg/kg) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000 mg/kg)

The above limits were quoted from 2002/95/EC and supersedure 2011/65/EU for homogeneous material.

(C) Test Method:

Testing Item Testing Method Reporting Limit

Cadmium (Cd) Content With reference to IEC 62321 Edition 1.0:2008, by acid digestion and determined by ICP - OES 2 mg/kg

Lead (Pb) Content With reference to IEC 62321 Edition 1.0:2008, by acid digestion and determined by ICP - OES 2 mg/kg

Mercury (Hg) Content With reference to IEC 62321 Edition 1.0:2008, by acid digestion and determined by ICP - OES 2 mg/kg

Chromium (VI)(Cr6+) Content With reference to IEC 62321 Edition 1.0:2008, by alkaline digestion and determined by UV-VIS Spectrophotometer

1 mg/kg

Polybrominated Biphenyls (PBBs)& Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 Edition 1.0:2008, by solvent extraction and determined by GC/MS and further HPLC confirmation when necessary

5 mg/kg

Date sample received: Jun 09, 2012

Testing period: Jun 09, 2012 to Jun 16, 2012 (D) Measurement Flowchart:

1. Test for Cd/Pb Contents Totally dissolved

*************************************************************************************************************************************

Put weighed sample into a suitable vessel

Add suitable acid Digest sample in vessel

Transfer the digested solution into a volumetric flask

Made up with deionized water

Analyzed by ICP-OES


Tests Conducted




2. Test for Hg Content Totally dissolved

3. Test for Chromium (VI) (Cr6+) Content (Alkaline Digestion)

*************************************************************************************************************************************

Put weighed sample into a microwave digestion vessel

Concentrated nitric acid, fluoroboric acid and hydrogen peroxide were added

Digest sample in microwave digestion vessel



Analyzed by ICP-OES

Weigh sample in an Erlenmeyer flask

Add digestion solution and continue stirring while heating at 90~95℃

Adjust the pH of the solution to 7.5±0.5 and transfer the solution to a volumetric flask

Make up with deionized water

Adjust the pH of the solution to 2.0±0.5

Add diphenylcarbazide solution and make up with deionized water

Analyze the mixture by using UV-VIS Spectrophotometer with wavelength set at 540 nm


Tests Conducted




4. Test for PBBs/PBDEs Contents

*************************************************************************************************************************************

End of report

Weigh sample and place in a thimble

Extracted by Soxhlet extraction with organic solvent

Concentrate the extract

Transfer the extract into a volumetric flask

Make up with organic solvent

Analyze by GC/MS and further HPLC confirmation when necessary










Sample Description:

One (1) submitted sample said to be DM black disc. Tested component: black solid material.

**************************************************************************************************************************************

Tests conducted:

As requested by the applicant, refer to attached page(s) for details. ************************************************************************************************************************************** Conclusion:



Pass

*********************************************************************************************************************************


Tests Conducted





Testing Item Result



ND = Not detected *************************************************************************************************************************************


Tests Conducted







(C) Test Method:






1 mg/kg



5 mg/kg




*************************************************************************************************************************************





Analyzed by ICP-OES


Tests Conducted






*************************************************************************************************************************************






Analyzed by ICP-OES









Tests Conducted





*************************************************************************************************************************************

End of report
















Sample Description:

One (1) submitted sample said to be DP black disc. Tested component: black solid material.

**************************************************************************************************************************************

Tests conducted:




Pass

*********************************************************************************************************************************


Tests Conducted





Testing Item Result



ND = Not detected *************************************************************************************************************************************


Tests Conducted







(C) Test Method:






1 mg/kg



5 mg/kg




*************************************************************************************************************************************





Analyzed by ICP-OES


Tests Conducted






*************************************************************************************************************************************






Analyzed by ICP-OES









Tests Conducted





*************************************************************************************************************************************

End of report
















Sample Description:

One (1) submitted sample said to be DV black disc. Tested component: black solid material

**************************************************************************************************************************************

Tests conducted:




Pass

**************************************************************************************************************************************


Tests Conducted





Testing Item Result

Cadmium (Cd) Content (mg/kg) ND(<2) Lead (Pb) Content (mg/kg) ND(<2) Mercury (Hg) Content (mg/kg) ND(<2) Chromium (VI)(Cr6+) Content (mg/kg) ND(<1) Polybrominated Biphenyls (PBBs)(mg/kg) Monobromobiphenyl (MonoBB) ND(<5) Dibromobiphenyl (DiBB) ND(<5) Tribromobiphenyl (TriBB) ND(<5) Tetrabromobiphenyl (TetraBB) ND(<5) Pentabromobiphenyl (PentaBB) ND(<5) Hexabromobiphenyl (HexaBB) ND(<5) Heptabromobiphenyl (HeptaBB) ND(<5) Octabromobiphenyl (OctaBB) ND(<5) Nonabromobiphenyl (NonaBB) ND(<5) Decabromobiphenyl (DecaBB) ND(<5) Polybrominated Diphenyl Ethers (PBDEs)(mg/kg) Monobromodiphenyl Ether (MonoBDE) ND(<5) Dibromodiphenyl Ether (DiBDE) ND(<5) Tribromodiphenyl Ether (TriBDE) ND(<5) Tetrabromodiphenyl Ether (TetraBDE) ND(<5) Pentabromodiphenyl Ether (PentaBDE) ND(<5) Hexabromodiphenyl Ether (HexaBDE) ND(<5) Heptabromodiphenyl Ether (HeptaBDE) ND(<5) Octabromodiphenyl Ether (OctaBDE) ND(<5) Nonabromodiphenyl Ether (NonaBDE) ND(<5) Decabromodiphenyl Ether (DecaBDE) ND(<5)

Chemist: Wang Haijun/ Zeng Guoliang mg/kg = milligram per kilogram = ppm < = Less than ND = Not detected

*************************************************************************************************************************************


Tests Conducted







(C) Test Method:





Chromium (VI)(Cr6+) Content

With reference to IEC 62321 Edition 1.0:2008, by alkaline digestion and determined by UV-VIS Spectrophotometer

1 mg/kg


With reference to IEC 62321 Edition 1.0:2008, by solvent extraction and determined by GC/MS and further HPLC confirmation when necessary 5 mg/kg

Date sample received: Jun 09, 2012 Testing period: Jun 09, 2012 to Jun 14, 2012 (D) Measurement Flowchart:

1. Test for Cd/Pb Contents

Totally dissolved

*************************************************************************************************************************************





Analyzed by ICP-OES


Tests Conducted




2. Test for Hg Content

Totally dissolved


*************************************************************************************************************************************






Analyzed by ICP-OES









Tests Conducted





*************************************************************************************************************************************End of report
















Sample Description: One (1) submitted sample said to be DH black disc. Tested component: black solid material.

************************************************************************************************************************************** Tests conducted:




Pass

*********************************************************************************************************************************


Tests Conducted





Testing Item Result



ND = Not detected *************************************************************************************************************************************


Tests Conducted







(C) Test Method:






1 mg/kg



5 mg/kg




*************************************************************************************************************************************





Analyzed by ICP-OES


Tests Conducted






*************************************************************************************************************************************






Analyzed by ICP-OES









Tests Conducted





*************************************************************************************************************************************

End of report
















Sample Description: One (1) submitted sample said to be HD black disc. Tested component: black solid material.

************************************************************************************************************************************** Tests conducted:




Pass

*********************************************************************************************************************************


Tests Conducted





Testing Item Result



ND = Not detected *************************************************************************************************************************************


Tests Conducted







(C) Test Method:






1 mg/kg



5 mg/kg




*************************************************************************************************************************************





Analyzed by ICP-OES


Tests Conducted






*************************************************************************************************************************************






Analyzed by ICP-OES









Tests Conducted





*************************************************************************************************************************************

End of report
















Sample Description: One (1) submitted sample said to be HH black disc. Tested component: black solid material.

************************************************************************************************************************************** Tests conducted:




Pass

*********************************************************************************************************************************


Tests Conducted





Testing Item Result



ND = Not detected *************************************************************************************************************************************


Tests Conducted







(C) Test Method:






1 mg/kg



5 mg/kg




*************************************************************************************************************************************





Analyzed by ICP-OES


Tests Conducted






*************************************************************************************************************************************






Analyzed by ICP-OES









Tests Conducted





*************************************************************************************************************************************

End of report
















Sample Description:

One (1) submitted sample said to be HM black disc. Tested component: black solid material.

**************************************************************************************************************************************

Tests conducted:




Pass

*********************************************************************************************************************************


Tests Conducted





Testing Item Result



ND = Not detected *************************************************************************************************************************************


Tests Conducted







(C) Test Method:






1 mg/kg



5 mg/kg




*************************************************************************************************************************************





Analyzed by ICP-OES


Tests Conducted






*************************************************************************************************************************************






Analyzed by ICP-OES









Tests Conducted





*************************************************************************************************************************************

End of report







SGSTest Report

ANSON SOLDER & TIN PRUDUCTS ITADE LTDCHANG HONG RIDGE INDUSTRIAL PARK OAIL NANHAIGUANGDONG

This report is to supersede test repon CANAUTO1210273201

The lollowing sample(s) was/were subfiitled and idenlilied on behajf ot the applicant as Lead-free Soldor SnAgCu

SGS Job No.Date of Sample ReceivedTesting Period

Test Requested ;

Test Result(s) :

Summary :

Conclusion:

Signed lor and on b€half ofSGS-CSTC Ltd.

No.: CANAUTO1 21 0273203 A01 Date: 07 Aug 2012 Page I ofg

:SC4TR1207000558-1: 30 Jul 2012: 30 Jll 2012 - 03 Aug 2012

A: As requested by clienl, SVHC scleening is perlomed according to:(i) Specified substances in the Candidate Lisl ol Substances of Very High Concern (SVHC)lor aulho zation puuished by Eurcpean Chemicals Agency (ECHA) on and betore Jun 18,2012 r€garding R€gulation (EC) No 1907/2006 ooncerning lhe REACH.B: Selected lest (s) as requested byclient.

Pleas€ relgr to n€xt pag€(s).

A: According to the sp€cili€d scope and analytical tochniques,concantrations ol tested SVHC are < 0.1olo (Ww) in lhe PASSsubmatlod samDls.

B: Based on the perfomed tests on submitled samples, the resulls ol L€ad, Mercury,Cadmium, Hexavabm chromium complywlth the limits as set by RoHS Directive201 1 /65/EU Ann€x ll; recasting 2002/95/EC.

; im h 6n d.@d d. oily 6 6.ni!r.{r) brd

Approved Signatory

ny etr.d b berdtudb.d 3tr pdrdod't rrhM or '{q'no rus6! '! rtergn 4 6elE-JLl4!49!r

srdrdJir5lpdd&Ed.rbqb.F.bqolEerxr51(a t(c,o)lEq j F?6?0"111 - j:11":

Test Sample :

Samole Descriotion :

Sp€cimen No. SGS Samplo lD D6criptionI CAN12-102732.001 Silvery metal

A: SVHC

Rema* :(l) The chemical analysis of specili€d SVHC is perlormed by msans ot currently available analytical

techniques againstlhe lollowing SVHC relaled documents published by ECHA:http//echa.europa.er./wob/gu€sucandidalelist-tableThese lists are under evallalion by ECHA and may subiect to change in the lulure.

(2) Concerning article(s)iln accordanco wilh Regulation (EC) No 1907/2006, any EU producgr or importer ol articles shall nolilyECHA, in accordanco with paragraph 4 ol Article 7, il a substance meets the criloria in Arlicle 57 ancl isidentitied in accordance with Article 59(1) ot the Regulalion, if (a) the subslance in the Candidale Lisl ispresent in those arlicles in quantilies lotaling over one tonne per producer or imporier per year; and (b)the substance in the Candidate List is present in those arlicles above a concenlration of 0.1% weighl byweight (Ww).

Article 33 ot Rogulalion (EC) No 1907/2006 requires supplier of an arlicle conlainang a substancemeeting the oriteda in Article 57 and identilied in accordanoe wilh Article 59(1) in a concentration abo!80.1% weight by weight (w/w) shall provide the recipient ol the article wilh sufficienl infofmation, availableto lhe sutpler;to ataow safe use ol the anicle including, as a minimum, the name of that subslance in lhecandidate List.

SGS adools the interprelalion ol ECHA lor SVHC in anicle unless indicated otherwise. Oetail explanationis available at the following link:http://webslage.contribule.sgs.nevcoFreach/documents/ScS-CTS-SVHC'paperEN-1 1.pdl

(3) Concerning malerial(s):Tsst resulG in this r€pon are barsed on lhe tested sample, This reporl relers to lesling result ol lestedsample submitted as homogenous malerial(s). In case such malerial is being used to compose an article,the ;esutts indicated in thia.€port may not represent SVHC concentration in such article. ll this reportrefers to testing resull of co;posile matedal group by equal weight proportion, the material in eachcomposite tesl group may come lrom morelhan one anicb.

lJ the sample is a substanc,e or mixture, and n directly exports to EU' client has the obligalion to complywhh the supply chain communication obtigation under Adicle 31 of Regulation (EC) No 1907/2006 andihe conditidns ot Autho zation of substance of very high concem included in the Annex XIV of theBegLrlation (Ec) No. 1907/2006.

(4) Conceming substance and preparalion:' - lt a SVHCis tound over 0.1i. (;/yr) and/or lhe specific concenlration limil which is set in Regulalion {EC)No 1272/2008 and No 790/2009, client is suggested to prepare a Safely Data Sheet (SDs) against lhe

Test Report No.: CANAUTO1210273203 A01 Date:07 Aug 2012 Page 2 of9

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Test Report No.: CANAUTO1210273203 A01 Dale: 07 ArJg 2012 Page 3 of I

SVHC to comply with the supply chain communicalion obligaiion under Regulalion (EC) No 1907/2006,in which:- asubstance thal is classifigd as hazardous underlhe CLP Regulation (EC) No 127212008.

- a mixture that is classified as dangerous according Dangerous Preparalions Directive 1999/45/EC orclassified as hazardou6 und€r lhe CLP Regulalion (EC) No 127212008, when their concentalions are€qual to, or greater than, those delined in the Anicle 3(3) ot 1999/45/Ec or lhe lower values given in Part3 of Annex Vl of Regulation (EC) No. 12722008; or

- a mixlurc is not classilied as danq€rous under Directive 1999/,f5/EC, bul contains eilh€r:(a) a substance posing human heahh or environmental hazards in an individual concsnlralion ol > 1 7oby weight tor mixtures that are solid or liquids (i.e., non-gaseous mixlures) or > 0.2 % by volume forgaseous mxlures; or(b) a substance that is PBT, or vPvB in an individual concenlration ol > 0.1 % by w€ight lor maxlureslhat are solid or liquids (i.0., non-gaseous mixlu@s);or(c) a substanc€ on th€ SVHC candidate list (tor reasons oiher than those lisled above), in an individualconcenlraiion of > 0,1 % by weight for non-gaseous mixlurest or(d) a substance for which th€r€ are Europe-wide workplace exposure lamits.

(5) ll a SVHC is found over the reporling limit, client is suggosted to identily the component which contarnsthe SVHC and the exact concgntration ol lh€ SVHC by requesting lurthor quantitative analysis kom lhelaboraiory.

Test Method:

SGS In-House method- GZTC CHEM-TOP-092-01 , Analyzed by ICP-OES, UV-VIS.

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SGqTest Report No.: CANAUTO12l0273203 401 Date:07 Aug 2012 Page 4 of9

Test Result: (Substances in the Candldate Ligt ot SVHC)

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i6iiE;HiF.-'.-4-1ieli4l'-"-l:-b*-1x:-ij13*jfr.H;'ltrj^,T1H"",':,1ffiffiiffi'JLfil-";..;. ^** .'-o-""ft T.*#l[ffiur{*ffi181ffi A,Ee":1ffi*#"?$ililg':r.srn iudlrdi bn d.n'.d tu.ln r4Mio

Substance Name CAS No. EC NO. 001Concentration

t%l

RL(%)

Aluminosilicale Refractory Coramic Fibres '^ 650-017-00-8(lndex no.) ND 0.005

Ammonium dichromale' 7789-09-5 232-143" 1 ND 0.005

Arsenic acid' 7778-394 231-901-9 ND 0.005

Boric acid' 1004:'-35-311113-50-1

233-139-2234-343-4 ND 0.005

Calcium arsenatg' 7774-44-1 231-904-5 NO 0.005

Chromic acid,Oligomers of chrcmic acid and dichromic acid,Dichromic acid'

7738-94,5

13530-68-2

231-801-5

236-881-5NO 0.005

Chromium lrioxide' 1333-82-0 2t5-607-8 NO 0.005

Cobalt dichbnde' 7646-79,9 231-589-4 ND 0.005

Cobalt(ll) carbonate' 513.79'1 208.169-4 ND 0.005

Cobalt(ll) diacetate' 71-44-7 200-755-8 ND 0.005

Cobah(ll) dinilrate' 10141-05-6 233-402- l ND 0.005

Cobalt(ll) sulphate' r0t24.43-3 233-334-2 ND 0.005

Diarsenic pentaoxide' r303-28-2 2't5-116-9 ND 0.005

Diarsenic lfioxide' 1327-53-3 215-48t-4 NO 0.005

Diboron trioxide' 1303-86-2 215-125-8 NO 0.005

Dichromium lris(chromate)' 24613€9-6 246-356-2 ND 0.005

Disodium letratrorate, anhydrous'1300-9641330-43-412179-04-3

215-540-4 ND 0.005

Lead(ll) bis(methanesultonate)' 17570-76-2 401-750-5 ND 0.005

Lead chromate' 77fi-97-6 231-846-0 ND 0.005

. {iduedr'.loteEb6ftdql.rditrdo4u0n 5'0663 | ,q{rlry l91e0t5::: " j:39

No.: CANAUTOl210273203 A01 Date: 07 Aug 2012 Page 5 ot I

sGqTest Report

Subslance Namo CAS No. EC l{o. oolConcenlratlon

t%l

RL(%)

L€ad chromate molybdate sulphate red (C.1.Pigm€nl Red 104)'

12656-85-8 235,759-9 N D 0.005

Lead diazide, Lead azide' 13/2446-9 236-542-1 ND 0.005

Lead dipicrate' 64n-64-1 229-335-2 ND 0.005

Lead hydrogen arsenate' n8+40-9 232-064-2 ND 0.005

Lead styphnate' 15245-4+0 239-290-0 ND 0.005

Lead sullochrcmate yellow (C.1. Pigment Yollow34)',

134+37-2 215-693-7 NO 0.005

P6ntazinc chromate octahydroxide' 49663,84-5 256-418-0 ND 0.005

Potassium chrcmale' 7789-00-6 232-140-5 NO 0.005

Poiassium dichrcmate' 7778-50-9 231-906"6 ND 0.005

Potassum hydroxyoclaoxodizincalodichromate' 11103-86-9 23+329"8 ND 0.005

Sodium chromale' 7775-11-3 231-889-5 ND 0.005

Sodium dichromate'7789-12-O't0588-01-9 234-190-3 N D 0.005

Strontium chromate' 77a9-06-2 232-142-6 ND 0.005

Tetraboron disodium heplaoxide, hydrate' 1?267-73- l 235-541-3 ND 0.005

Tdlead daarsenate' 3687-31-8 222-979-5 ND 0.005

Zirconia Aluminosilicate Relractory CeramicFibres'^

650-017-00-8(lndex no-)

ND 0.005

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SGqTest Report

Notes:

No.: CANAUTO1 21 0273203 A01 Date:07 Aug 2012 Page 6 of9

(1)RL = Reporting Limit. All RL are based on homogenous malerialND = Not detected (ower than RL), ND is denoted on lhe SVHC substance.

(2) 'Th€ test r€sult is based on lhe calculation of selected element(s) / marke(s) and to lho worst-casesc€nado. For delail intormation, please refer to ihe SGS REACH w€bsito: lWJlgCb j$gIllgllghledLvgw.hbh-concom-anelhb-lnf ometbn-os.hlrn

Calculated concenlration ol diboron triorile, boic acid, disodium telraborate, anhydrous and tetraborondisodium heptaoxide, hydrato are based on the water extractive boon and sodium by ICP-OES.

RL = 0.005% is evaluated lorelement (i.e. cobalt, arsenic, load, sodium, chromium (Vl), silicon, aluminum,zirconium, boron, potassium, sirontium, zinc and calcium @spectively), excopt molybdenum RL=0.0005o/"

{3) ̂ On Jun 18, 2012, ECHA consolidat€d two entdes of aluminosilicate refraotory oeramic fibres and two oJzirconia aluminosilicate refractory ceramic libres in the Candidale Lisl of SVHC for aulhorization published inJan 201 0 and Deo 201 1 into one entry lor aluminosilicats relractory oelamic tibres and one lor zarconiaaluminosilicate refraclory ceramic fibres.

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Test Report No.: CANAUTO1210273203 A0l Dale: 07 Aug 2012 Page 7 ofg

B: RoHS Oirecllve ml1/65/EU

Test Method: With relerence to IEC 62321:2008(1) Delermination of Cadmium by ICP-OES.(2) Delermination of Lead by ICP-OES.(3) Delermination of Mercury by ICP-OES.(4) Determination of Hexavalent Chromium by spot t€sl / Colorimetric Method using uv-Vis.(5) Delermination of PBBS and PBDES by GC-MS.

Test llem(s):Cadmium(Cd)Lead (Pb)Mercury (Hg)Hexavalent Chromium (C(Vl))Sum ol PBBSMonobromobiphonylOibromobiphenylTdbromobiphenylTetrabromobiphenylPentabromobiphenylHetabromobiphenylHeptabromobiphenylOctabromotriphenylNonabromobiphenylDecabromobiphenylSum ol PBDESMonobromodiphenyl etherDibromodiphenyl etherTribromodiphenyl etherTelrabromodiphenyl etherPenlabromodiphenyl etherHerabromodiphenyl etherHeptabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl 6therDecabromodiphenyl ether

1000

1000

us!22

o

55555

5555

5

55555

5

5

!4i! u!!!100 mgftg1000 mg/t(g1000 mgrkg

9AND53ND

NegativeNDNDNDNDNDNONONDNONDNDNDNDNDN DN DNDNDNDNDNDND

m9n€msagmgkgmS/kSmsftsm94(gmgKgmg/kgrng/lqmS/kSmo/kSmS/kSmS/kSmg/kgmS/kSmS/kSms^smSil€mS/kSmsftgms4qmS/kS

M d k .lfu biirr @Mi.,&itd bLE.io cdld.E I' ErfuE oeudb rr !4J!9@!I41q!q!'l!hrn N.lwindrmDdnrlAqEl;; i_anui"r'o"aujd.n'dfte ^ryEa,dtueerdr6dd'dd;idd6

rffi .mm*'s"g"Esq'ls,m*}illfs,"gi:T.1ir.;lfil"ffi;:1';#*""'H"ii@;:;;k;u;;;;d;; 'fr;;;;;';;a;6riat;nddl.rrddd.sDr-'un.vibu,Dr.'rturrp* oituc@nv

. bDd tt.nd,o'. ' ' i . dnir d

axd!tu(Sdblht0#lEditEqrLirF.d.i{0t@oL s1(r6e} |(610)82159666 I F2q4205113 iw.6j!.M

SGSTest Report

Notes:(1) The maximum pormissible limit is quoled iiom directive 2011/65/EU, Annex ll(2)o spol-test:Negative = Absence of C.Vl coating, Positive = Presence ot CrVl coating;(The tested sample should be turther vedlied by boiling-wateFexiraclion melhod if the spot test resutt isNegativ€ or cannot be confirmed-). Boiling-watgrenraction:Negalive = Absenca of CrVlcoatingPosilive = Pr€sence ot CrVl coating;the detected concentration in boiling-water-extraction solution is equatorgreater than 0.02 mg/kg with 50 cm2 sample sur,ace area.For @rrosion prot€ction coatings on metals: Informalion on sto€ge condiiions and production date ol thet€st€d sample is unavailable and thus rosults ot C(Vl) repr€sgnt status ol the sample atthe time ol testing.

rllrdbro.ndtudh.d3.# ra.rd. r !!!ruEs@EsJlls!!&s5Ndd [email protected] cdth b E!fu

d iud!6i b;ddhdm.di.rryi.r..'dtud.di.irrrdrs htnffino@s& kdi.iixi. tbconFvt '1d14. nbdmdfritrfubin.'o,ntIedo.'r.'ry.rn.6hFyi*BFjatynbh.cbnljdd|!de!hmld{

No.: CANAUTO1 21 0273203 A01 Date: 07 Arjg ml 2 Page 8 of I

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: .N, {hlhdlddlhtorCrtuilrdiqL.Ffilrrartrron 516 t 0er)8215ss I (620)ta0l511t m.d 3!. M

Test Report

Sample photo:

No.: CANAUTOI 210273203 AOI Date: 07 Aug m12 Page I ofg

cANt2-102ru.00r

;;;fi ; ;j".i;*;rvi'o.-rrr.t*4.

SGS aulh€ntlcate lhe photo on o ginal rgport only*' End ol Repod -'

-Jl, hrlElrdoh slirs3 | 64e15556 | F?0)32t5113 frar$@

Analyzed for Undisclosed Recipient upon request of: Littelfuse Inc. 8755 West Higgins Road, Suite 500, Chicago IL 60631 USA

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Signature tidFor QuegionPlease with SGS

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,F{ff,#+Test Report S4(No.) : cE/2012182966 Erh(Dare) : 2012/08 /21 ag / .PaEe) : I o f I

t*t+.tEAAfEa6l,IMROIiG TECHNOLOGY @RPORATION

dbE *i9*t1r&1* E1r:'as*NO. 5, YOU 3F.D RD., YANGMEI CITI, TAO'I'IJAN COUNTY 326, TAIITJAN

ll|||tal||||ttllr!

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l [S* { r1(sanpte Descr i p t ion)

t t s4!t(sryle/I tem No. )

t l t? t E * (S ,6p lc Recc iv ins Data)

tll djh fll (re s t i n8 P€riod)

TrN PL^TED Nrc(EL CIoVERED coPPm SmX (€*rtr94.6.S,*)

s T N - ( 0 . 1 3 ) ( 0 , 4 5 ) ( 0 , { 5 { ) ( 0 , 5 ) ( 0 , 5 r l ) ( 0 , 5 7 4 ) ( 0 . 5 8 ) ( 0 . 6 ) ( 0 . 6 3 ) ( 0 . 6 3 5 )( 0 , 6 1 3 ) ( 0 , 6 4 5 ) ( 0 , 6 5 ) ( 0 . 7 ) ( 0 , 7 2 1 ) ( 0 , 7 6 ) ( 0 , 8 ) ( 0 . 8 1 3 ) ( r . 0 ) ( r . 0 2 4 ) ( r . 2 )( 1 , 2 9 ) ( 6 6 )

| 2012/08/20

| 2072/08/20 lO 2012/04/24

f i } i ** ( r . " t R€qle l ted) : ( t ) tni t t ,P i t t , iL l i t [ , * , * , ; t { lJt t r l*{ . (As sP.ci f icd by.r icn!, !ot € s r c a d E i u E , L € a d , v € . c u r y , C r ( V I ) c o n r e n l s i n t h € s u b n i t t € d s a o p l e . )

(2 , &* .EP )3F ' i l l iA t+r t (n) .An+n*8, n .$ . , ,4 .* f l$ , . (A"5 p e c i ! i e d b y c l i € n t , t o r € s t P F O A , P ! 9 s a n d H a L o s e n - F l u o r i n € ,C h l o r i n € . B r o o i n e , l o d i n e c o n t c n t r i n t h e s u b r i t ! € d s a n P l e . )

f tX,T-F (Pl .ase .efer to next pases) .

l f ,E-F-F (PI" , . . re fe. ro t rex i pases) .Nll l t i i ( r .6t x. tbod)jdl l**( I"" t R"""t tg)

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n{'d,+t€Test Report f iq(N..) , cE/2012/a2966 Srq(D,t .) ,

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*,e **ffi Nr'it-* 891 ='85fi,NO. 5, YOU 3RD RD., YANGVEI CITY, TAOWAN COI'I]AY 326, TAII{AN

*$*(T€st Re6ul t . )

j ttqr{n (PART NA.vE)No. r

2012/oa/24 F* lPzEe\ : 2 ot 3

tl]Llttll lllll

.EE&,4,l (6Tt,T) (22Ii) (SILVER COLORED VRTAL IXIRE (INCLUDING THEPLAIINC LAYER) (22 TYPES) )

Jat a(T.st t teos)

+1!(uri t )

' iatx( l |3 t lod)

t*odEticoml-)

*J((R.sul t )

N o . l

, i / Cadhiun (cd) ng/kg +*tE 6232r. 2oo8t*, /&rgt*6tt&?d'4t,bllfi,**; r tri tt'refer€nc€ to IEC 62321: 2008 andperforned 6y ICP-A!S.

,S / Lead (Pb) mt/kg +)grF[ 6232\. 2oo8ti], ,x,gAtsa.it *,f +**trt t*{,i*tri. / {irhre le r€ncc to IEC 62321: 2008 and

p.rforoed by ICP-,A'S.

2

;R / \ t€r.ury (Hs) as/kE +*rE 6x2r,2oo8t;*, r,. S,Ali6€*,.f +*ttrt*{,*,r|. / Nithre fe ren .e to IEC 62321: 2008 and

p€. fo .ned by ICP-AF,S.

2

ni l r& / Hexav ' t .n t chroniun cr(VI) ++rEi: 6232r. 2008l:. il, ,)\;ft,Y'+$i i l$ - / s i th reference to IEc

62321: 2008 and Per lorned bY

B o i l i n A v a t € r e x t r a c l i o n V e t h o d . #

+n+}t4& / Perrtuoroocranesu l lonates (PFIS_ACid , Vera l Sa l t

4*us EPA 3550c: 2oo?)rit, rt'&4a,f f r / {*&l i j f l . / { i th reretenc€to US EPA 3550C: 200?. Ana lYs is was

pe. fo rned by ta lvs . _

4f.+& (*) / PloA (cAs No.: 335-67-I )

+*us EP 3550c, 2oo1)r)L, v]litt-+a,? f f / f ; ** ,€t l . / f l i rh r€rer€nce

to I tS EPA 3550C: 2007. AnalYsis was

perforDed 6y rc/MS.

l 0

JliiAftl'Y: T.5 T':*'r':"0i1'l h: i,sr 5:n 'n; olvj:::

.' suorao .o ̂ .'.,u, ." .ton.-s ob *. *" -."' - 'i;; i-d';. D@

m p"oq- *"r.*'* *"iii/$v b*.r tr6 .i*t 't ae* hd -om{o @1r'-{ t 'dr F1'6 $' cortusrndinos d

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".'..' ' '-.i; '; ;:'fr rl" coitsts 're c$msiDi' '

i6 am ao estrt ! u u- ,,. ;; Ea." "*Md

nL dummr snrc F F'ogL€d'"'s",' " "'' *"'" ",.;;i;iii';;"n"o**''-t"*

{ N . v i ; r o ' i e L l r i } : r ; I " i

t ! - ' J r i !

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Test Report+*t+&.eDtrrF2'1,I@RONG TECHNOLOGY CORPOR,{TION

*t fr #.ttih fr' 4t &a f, E 1, :ra5 !tNO. 5, YOU 3RD RD., YANCVEI CITI, TAOWAN COUNTY 326, TAI\{AN

fr i i (Not.):l . n g / k t = p p n i 0 , l s t % = I 0 0 0 P P h

2 . n . d . : N o r o . r " " t . a ( , t l t * )

3. IDL = Vethod Deiect ion Lini t (r* jHi l l iePF/d)

4. -" = Nor Resurated (**x, t6ld)

5. **= eual i rat ive a.alysis (No uni!) .€, I{r}r t (*+1,!)

6 . # = a . P o s i t i v e n e a n s i h e t r e s e n c e o f C r V I o h l h € t e s t e d a r e a s

(Posi r ivei.a:; i{Ed{A:rl5'l;r'ilJ})b. Negat ive means ihe absence of CiVI o ' the tested areas

( Nega t i ve l,F i.l i{ E r&* {A irl I'l ^lllJt )

T h e d e t € c l e d c o n c e n | . a r j o n i n b o i l i n s s a i e r - e x t r , c t i o n s o l u t i o n i s e q u a l o r s r e a t e r l h , n o . 0 2 n a l k gni rh so cn2 resred a.eas. / ? tBiUtA>0.02 Dslks v i th s0 cn '1 ( tested areas)

?- tle6!rifi,4.*+{:tr'-*'*tr +xl3i ' *t+ I'ttrE+d*e*'F'ft i* f {Et{ +-*tl{ 6i }l (ahe sanpr"s

eas/ *ere ana ly2ed on beha l f o f rhe aPPl i 'ahr as mix ins sanPle in one resr ina Th€ above 'esu l ts

r a s / s e r e o n l y s i v € n a s t h e i n f o r n a l i t v v a l { e ' )

rtt E +{i(Uni t )

ri t{rti(u. thod)

t*{t;ib F{r(flDL)

g *

N o , l

l* / x. lorc.

6* (A) / Halosen-Fluorine (F) (cAs

N o . : I { 7 6 2 - 9 4 _ 8 )

t+Bs B\ r4s82,2ooz, $+nfr&,t l f i . / r l t th re ierence to BS EN1 1 5 8 2 : 2 0 0 7 . A n a l y s i s u a s p e r f o f m e d

by lc .

5 0

6* ( { , ) / } la togen-chlor ine (c l ) (cAS

N o . : 2 ? 5 3 7 _ 1 5 - l )

5 0

i* ( ; l ) i Harosen-Bronine (Br) (cAs

N o , | 1 0 0 9 7 _ 3 2 _ 2 )

5 0

6 * ( 4 t ) / H a t o s e i - I o d i n e ( I ) ( c A s

N o . : I 4 3 6 2 - 1 { - 8 )

5 0

fla+E+Test Report !14(No.) : cE/2012182e55 ES(Date) : 2a12/a8/24 F*. (Pase) . 4 or a

*++rtrftad a,r4TOORONG TECHNOI'CY CORPOMTION

dt El *it**f9frr* E1r:t65SNO. 5, YOU 3RD RD., YANGMEI CITY, TAOYUAN COUNTY 326, TAISAN

|r][!rttl[rtl]l

PF0s+*llR(R.f. ' . '". Inroroatio!) ' t i^,l l t lE*ti PoPs - (EU) 75712010pFs,*./t.i'!trf i.8'lf,f f{+&.!60.001%( l oppn) ' A+A.e ' fr.e{.4qt1+ q'4r+&.i&0. r%( 1000ppn) ' A}6$sC.Giit*f 44€€tuer'z '

( O u t l a , i n g P I o S a s s u h s r a b c e s o r p r e p a r a t i o n s i n c o n c e n t r a t i o t s a b o v e 0 . 0 0 1 % ( l 0 P p n ) , i n s e n i _ r i n i s h e d

p r o d { c t s o r a r t i c l e s o r p a r t E a t a l e v e l a b o v e 0 . 1 % ( l 0 0 0 P P n ) , i n t e x t i l e s o r o t h e r c o a t e d n a t e r i a l s

abov€ Us/nr. )

L , e o . . 2 e #

fla#+Test Report i E 6 ( N o - ) : c E / 2 0 1 2 l 8 2 9 6 6 E J q ( D a r e ) : 2 0 1 2 / o a / 2 4 F f ( P , s . ) , s . r 8

i++?tnf,)atE'taT@RO!iG TECHNOLOGY @RPOMTION

tt Ei f.tsf fr a, fr1* E lt :t65 !tNO. 5, YOU 3RD RD., YANCMEI CITY, TAOYIJAN COUNTY 326, TAI\T'AN

tl |ltt][trtrll

t

2)3)

Ai,tT t tft,{i n aif4} ' *s e- l,}8rl ' ( ^-fi t},ri{t ilrh rt ) / These samphs weredissoN€d tohrt by pE{orditioning method accodi.g |o below itolv chan. ( cf Esl mettlod excluded )iq'l^ I : *fll / N6me of lhs p€Bon wtlo made measusnent climbg€al Yang,lt{ I I ^ : ti*a / Name or lhe peBon in charge or measu€ment Trov Chang

6fF +t{ f r+ t{J t i l l / lcP4Es

*.sfif / samde Maieiar titLtitttt / Digestion acid

sel 6tffi almiNm.solderr,h. 4.t. tt, LA|t. tn+ /Adu.6ia. HNO.. HCl. hF. H,O,4{,!.*.* / HNOJHF

arld nlrito,m mllrdium samic

E--ri+. 4&. r* , H,so,. H:q.!!gdql,r^i*al: i4el|FNl /add€d appoFiatere€genl io total drgeston

Nob- : (1) lt r++ A.&l,li+/F ^*,1+fi ltri ' ,,tr4 9o_9s'c +lts / For non-retallic matedal add alkaline diq€slion Egent and h€stro s0-€5C.

tzl i+ r+tf ii+l, r.rt+ ' ,1" *4,i,;+xt / For n€lallic m.tedal add pu€ waler and heal lo boiling

t*. tft*t /Cuning Preparalion

'id.i*sft / samde Measuremenl

4.',/tfrlr,A'ldrft*.)klL tMicrouave dlgEslioo wilh HNO/HCI/HF

R* T |tl t{s il i't ( ,rb tr jli t 6t rt,tli tr{ &(r'-F l.i'i) /r'ald dig€slion by suilable acld dep€nded ondifered samDle maledal (as b€low hbl€)

,"*ailf,tr/l!tiiih4x{ / Hear to appropnate

&tBtAtt /AlkaliF$iontn*|l / HClto dissolw nlter digestale lhrelgh nler

,"\*a |ta /Add

,t* tt k-n LteLtjt^' tirj&s*na.'1|oM 6ta

ab6odan@ at sao m bYUV-VIS

fi{fi,*r+Test Report si4(No-) : CE/2012l82966s $ ( D , r . ) , 2 0 1 2 / 0 8 / 2 { E r h ( P " s e ) , 6 o r 8

**t+An{r}ArEaaTOORONG TElCHNOTOGY CORPOMTION

dbEi *iD&f crtrlf Elr:r*5fiNO. 5, YOU 3RD RD., IANGMEI CITY, TAOIUAN COUNTY 326, TAISIAN

an+rt(s)/Af,.+**al''*,8tr / PFoA./PFos analytical flowchartr inli{,l'F : it'rrly / Name ofthe person w'ro made measurem€nt RomanWong! tnjfih t ': iir#A / Name of the person in charge of measur€ment Troy Chang

r ; ; ; r ' : : ' ; . . ; . 'oaru -"p".

"*--, . " *"iE

i".i 'i,*i:iii6ni rc;,6-mr'e]'d 6'sr. md oifrms 'o Erdo1" Ddlmnts d w a\ d'iii'."i' niiiri" '*-'neu '{ u.s dd 's*'

".1*d h ;,i

iii d#d c;a;;o" or -" **. +e ,.6 "r.

'd,1's*d;;'. 'r;o rii @Fn! o' Fst c'ie 's b i crem at r ' doi J-€ ' d@i ' ! . i& ; i# l lo .^n"g . r io . , "g . t . -ag . ro ru-a . ' * . .6 ;o idomdr i , .eg ' * . rd

, ,' -i'-[iii'',i'p"; ;;i r'' *med ts Jn M' dnd oferde- -r; F prc5e'iec 'o tre tu b4 Fd"nr o'be rd

#SfiA.q / Sample pretr€atment

&*;A+t(*+Ir iSample extraclion by Ultrasonic extraclion

(&*f,:* Reference mehod: Us EPA 3550c)

o1&4aEftry*i-,;'fr4&i&. IAnalysis was pertormed by LC/MS

rfla*E+Test Report)i*+iteaaIEz:'1T@RONG TEC}INOI'GI CORPOMTION

dkEi *i*rifr .r&a* E*, :r55ftNO. 5, YOU 3RD RD., YANGM-EI CITY, TAOI1JAN coWTY 326, TAIIIAIi

f i€(No.) : cE/201?/82966 g lB(Da!e) : 2012/aa/24 F*.(Pase) . 7 or e

tl|||tttrffirllll

i *+fi'tl€f, / Analytical flow1) ,rl$,r'.F : t*.,9* /Nameof the person who2) ,.1 rl. I I A : it ** / Name of the person in

chart of halogen content

made measurement: Rita Chencharge of measurement: Troy Chang

o!- 1h ( 'r i reFn Rt' 6 t tolI smpk\s16tF Tnr' kd r"@n h d'

" -'"";

' s---;id;*;" "" '"' - -q'"" "Ds n@nHt s 'sud bv de conpany 3uhjed ro G 6i.d edo

.i"li ii'ii,k@"* rofu,i,**r. *br',i, Tsm. md cqd bn;:ii;i i oiLiiii* a ** *" "d"" '

.e .g" - ' . : , r ' " - . . . " . " , i ' , r , l - ;o |6 . fh [email protected] ' j , * *o rd, ,,,, ,,, ;iii i !{ l 6-;o-, -

iiiiffii .i;i --;;; ,& a-.m' "'

-. -;:;;;;;* t t;4;;"d r nw ;otutu'3 -aie

t&!"tt &l'lt>*. ISample pretreatrnenusepamtion

*:lA*t l*&&r\l l&{l f iWeighting and puting sample in cell

t'ilf EE AAtt /Dilution to fired volume

*+Eh&rrit tAnalysis ,a|as perlormed by lC

I

SGqx{a#+Test Report I t q ( N o . ) : c E / 2 0 1 2 / 8 2 9 6 6 E l h ( D a r e ) : 2 0 1 2 / o a / 2 t ! [ & ( P a 8 . ) : 8

" l 8

+*t+&EDtr&'taTooRONC TECIINOI.GY @RPOMTION

i,t Ei *rlf t 4tfi f E 1r:!&5tt,NO. 5. YOU 3RD RD.. YANGYEI CITY, TAOWAN @UNTY 326, TAIfrTN

- nA fr'f,*tlti ' la^l|Flft lt&&/*&. '(ThG l .s led darplc / par t is Darked bt ao. f fo ' i f i t 's shocn o! tbe photo.)

" le+ '*4. (E d of R€port ) ++

- h 5 E!. '6pol tt -o.rr r 'is *oo!:(3) BH rhBbqG@iddbctuN-:Jr n: t t - t . r '+ ' ' ' r; ; H ; ; ; * ; ; ' ; . c . @ r v . ! t ] d | o t r c f . ' | c o n d ' d ; o , s . @ F f u o v d b . i a v 6 | a d e o a q J 6 s d ' . , d 3 s G . - a . M s { s 6]i 'oinei;;mdo*s'9b]d6r.ff iadcfolFEi' i iei 'mcDdIffidw'{s6fu.dr

Fa'-- '**'de@ ".;;:av; ; ; ; . ; _ # ; ; ; - ! - d * d i " ' h . | l . " d c h d " " , . " ; ; ' i ; ' r * c d 4 ' ' ! * 4 d s b J i

;_;;d nm *c dib', "

*, te hn*doidM; nisd@ntdndbeiiiGHliiiii*ma&;;;o'i oo"r . d' r-m"

"t rc -'iini;;;F.;Abn,it*r = '",m' '14 oiende- ma b' oa*e

. -,.,-,,;lrll:,li: !l'l

82966

Documents

ICP Test Report Certification Packet/media/files/littelfuse... · Form 585-047 Rev. A 1 2/21/06 2 Table 1: List of Raw Materials covered by this report . Parts P/N Raw Material Description