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BITUMEN BROCHURE Royal Petro Energy BRIDGING THE GAP R

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BITUMEN BROCHURE

Royal Petro EnergyBRIDGING THE GAP

R

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OVERVIEWINTRODUCTION

2005Royal Industries FZ LLC

2011Royal Petro Energy FZC

THE GENESIS

A healthy economic scenario and a robust oil industry laid the ground for realizing Royal Petro Energy Group in 2005 in the United Arab Emirates, the way the founders envisaged it to be.Today, with its own fleet of tankers, Oil Terminals an efficient logistics network and tie-up with renowned refineries, Royal Petro Energy Group has steadily grown to be the pioneering player in oil space of Middle East and Africa, specializing in manufacturing,refining,distributing and trading of base oil, bitumen , lubricants and greases with focus on adequate supply chain management.

VISION STATEMENTTo be the top most solution provider in the Petro Energy Sector by up keeping the corporate responsibility towards the society and caring the nature.

ROYAL PETRO ENERGY GROUP OF COMPANIESThe growing energy needs can be met through effective collaborations powered by a better mix of different, sustainable energies.

At Royal Petro Energy, we’re exploring a broad mix of energies. We’re making our fuels and lubricants more advanced and more efficient than ever.

• Royal Petro Energy FZC• Royal Industries FZ LLC • Royal Lubricant and Grease Manufacturing LLC • Oil & Gas Enterprises FZC

Message of the chairman of the board of directors

Petrochemical plant and Transport line established at AL Ghail Industrial Area, RAK

Trading petroleum products, established at Hamriyah Free Zone- Sharjah- UAE

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2012 Royal Petro Energy Qatar LLC

2013 Royal Lubricant and Grease Manufacturing LLC

2014Oil and Gas Enterprises

THE ROYAL PHILOSOPHYROYAL PETRO ENERGY FZC believes that the protection of the environment, safety and health of its employees as well others involved in its operations is an integral part of its business and operations.

MISSION STATEMENTRoyal Petro Energy is committed to harness the value in every sphere of the energy chain for the existing and prospective clients through our integrated team effort by making the optimum utilization of all available resources in an ethical and socially responsible manner.

Tank FarmOil & Gas Enterprize FZC

Refinery

Refinery

Trading

Lubricant

Ro

ya

l Pe

tro

En

erg

y G

rou

p

Royal Industries FZ LLC(RI)

Royal Petro Energy FZC(RP)

Royal Lubricant and Grease (RGL)

Foundation stone laid for Petrochemical plant at Doha, Qatar

Manufacturing of all types of Lubricants, greases and specialty oil products established at Ajman, UAE

Tank farm with total 21 tanks with different capacity which can handle class I,class II and Class III petrochemical products at Hamriyah Free Zone- Sharjah- UAE

ISO 9001 certification for Design, Manufacturing and Supply of Lubricants and Grease

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ROYAL PETRO ENERGY FZCA leading player in oil space, specializing in Oil Trading, Oil Refining, Grease ,Manufacturing, Oil Storage Terminals, Diesel Trading, Bitumen Manufacturing.Shipping & LogisticsEstablished in the year 2005, Royal Petro Energy initially started as an oil trading company and with years of hard work and its commitment to perfection has now emerged as one of the leading organisations in the oil trading industry of Middle East Royal Petro Energy engaged in trading of Group I and Group II

Base Oil which is exported in bulk quantities to North East Asia, Africa, and the Middle East

and has a major share of the.market in UAE and India

BITUMEN GRADES

Penetration graded Bitumen complying with ASTM & AASHTO specification.

40/50, 60/70, 80/100

Cut backs(Medium & Rapid Curing) Bitumens full range as per ASTM & AASHTO specifications

MC30, MC70, MC250 & MC3000 and RC70, RC250 & RC3000

Anionic Emulsions(Rapid and Slow Settling) Bitumens full range as per ASTRM, AASHTO and B.S. Specifications

A140, RS1, RS2, SS1 ans SS1H

Cationic Emulsions(Rapid and Slow Settling) Bitumens full range as per ASTRM, AASHTO and B.S. Specifications

K140, K160, CRS1, CRS2, CSS1 and CSS1H

Polymer Modified Bitumen full range of PG grades complying with SuperPave MP1/SP1 and AASHTO M320

PG70-10 and PG76-10

OVERVIEW

Bitumen is produced from selected crude oils through a process of fractional distillation. The crude oil is heated to temperatures of between 300 and 350 degrees Celsius and fed into a distillation column allowing the lightest fractions of the crude to separate, through vaporization, from the heavier fractions, which remain liquid. The higher boiling point fractions are then drawn-off via a heat exchanger and enter a vacuum distillation column. This process produces a “short residue” that is used to manufacture several grades of bitumen. The pressure and temperature conditions within the vacuum process will determine the hardness of the short residue, and as such the grade of bitumen produced. The short residue may be further modified by ‘air blowing’ in which air is passed through the residue at temperatures of 250 – 300 degrees Celsius.

Penetration Grade DeterminationThe Penetration Test determines the hardness of Bitumen by measuring the depth (in tenths of a mm) to which a standard, and loaded needle will vertically penetrate in 5 seconds, a sample of Bitumen maintained at a temperature of 25°C. Hence the softer the bitumen, the greater will be its number of penetration units.

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SPECIFICATION UNIT 40/50 60/70 80/100 TEST METHOD

Specific Gravity at 25°C 1.01 - 1.06 1.01 - 1.06 1.00 - 1.05 ASTM D-70

Penetration at 25°C, 100 gm, 5 sec 0.1MM 40 - 50 60 - 70 80 - 100 ASTM D-5

Softening Point, Ring & Ball °C 52 - 60 49 - 56 45 - 52 ASTM D-36

Ductility at 25°C, after TFOT, Min CM 100.0 100.0 100.0 ASTM D-113

Loss on Heating, Max %Wt 0.2 0.2 0.5 ASTM D-6

Drop in Penetration after Heating, Max % 20.0 20.0 20.0 ASTM D-6 & ASTM D-5

Flash Point Cleveland open cup, Min °C 250.0 250.0 232.0 ASTM D-92

Solubility in CS2, Min %Wt 99.5 99.5 99.5 ASTM D-4

Organic Matter Solubility in CS2, Max %Wt 0.5 0.5 0.5 ASTM D-4

Spot Test Negative Negative Negative *A.A.S.H.O.O.T.102

TECHNICAL DATA SHEET

QualityAll Bitumen supplied is of the highest quality and fully compliant with ASTM and AASHTO, equivalent EN and BS International Standards and Test Methods. Third Party Inspection (SGS/GEOCHEM) for Quality Testing and Analysis certification are performed for all the supplies and certified for compliance with product specifications and International standards.

ApplicationsPenetration Grade Bitumen are used in various types of road application such as hot-mix asphalt (HMA) and surface treatment (single or multiple) for pavement base and surfaces and also some industrial applications. Additional processing of this type of Bitumen yields various grades of Bitumen products.

*American association of state highway officials

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PRODUCTS| FOR ASPHALT WORKS

Cutback Bitumen Cutback Bitumen (Liquid Bitumen) is Bitumen that is dissolved in a solvent . Typical solvents include Naptha, gasoline and kerosene, white spirit etc. The type of solvent controls the curing time while the amount determines the viscosity of the Cutback Bitumen.

The advantage Cutbacks have over Emulsions is a much higher residual Bitumen percent, typically over 80% compares with over 40-65% for Bitumen emulsions. The result is more Bitumen left on the roadway after curing, for the same volume of binder applied.

Cutback ClassificationCutbacks are divided into two classifications, Rapid-Curing (RC) and Medium-Curing (MC) depending on the solvent used. They are further defined by a number which indicates the minimum kinematic viscosity(fluidity) of the cutback.

CUT BACK SPECIFICATION UNIT MC30 MC70 MC250 MC3000 RC70 RC250 RC3000 TEST

Kinematic viscosoty at 60°C CST 30/60 70/140 250/500 3000/6000 70/140 250/500 3000/6000 D2170

Flash Point, Min °C 38 38 66 66 - 27 27 D1310

Residue from Distillation to 360°C, Min % Vol. 50 55 67 80 55 65 80 D402

Test on Residue from Distillation

Penetration at 25°C, 100g, 5 Sec CM 120/250 120/250 120/250 120/250 80/120 80/120 80/120 D5

Ductility at 25°C, Min CM 100.0 100.0 100.0 100.0 100.0 100.0 100.0 D113

Solubility in Trichloroethylene, Min % 99.0 99.0 99.0 99.0 99.0 99.0 99.0 D2042

Water, Max % Vol. 0.2 0.2 0.2 0.2 0.2 0.2 0.2 D95

SYSTEMSURFACE DRESSING

PRIME COATING

TACK COATING

SEMI-GROUTING/PENETRATION MACADAM

SLURRY SEALING

FOG SEALING/ MIST SPRAYING

DUST BINDING

Emulsion RS-3K SS-1K K1-40, RS-1K, RS-2K RS-3K SS-1K K1-40, SS-1K K1-40, SS1K

CutBack MC3000 MC30, MC70 MC3000

*Test method is based on ASTM standards.

Product required for various systems of road construction and maintenance

Do not act based on the above data, it is purely for information purposes only. The grade used for each system may vary based on application and country.

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Bitumen Emulsion Bitumen emulsions generally belong to the oil-in-water type of

emulsions where bitumen is dispersed in water with the aid of a small quantity of emulsifying agent. The agent stabilises the bitumen particles

under normal conditions of storage. Bitumen emulsions derive their main use in road construction and maintenance because of their safety, ease in

handling and excellent adhesion properties.

AdvantagesThe advantage of water based bitumen emulsion is that it allows bitumen, which is

semi-solid unless heated, to be handled and applied at low temperatures. Following application of an emulsion, it undergoes a ‘breaking’ or ‘setting’ process where the

bitumen droplets combine to deposit the bitumen on the paving aggregate as a film. By contrast, cutback bitumen contains a significant proportion of cutter (kerosene), to

reduce the viscosity of the bitumen and help coat the aggregates. The cutter must then evaporate before the bitumen is left behind as a film on the stone. This evaporation process

can take many months. If the cutter is still present when the final surfacing is applied, this can result in flushing of the pavement and resultant loss of surface texture and skid resistance.

BITUMEN EMULSION SPECIFICATIONTest on Residue Form Distillation

COUNTRY

Emulsion Type

D244 D244 D244 D244 D244 D244 D244 D5 D2042

Min Max Max -/+ Min/Max Min/Max Max Min/Max Min

Re

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by

Eva

po

rati

on

Sie

ve

Sto

rag

e s

tab

ility

at

1 D

ay

Pa

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Vis

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t 2

5 °

C

Vis

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ty a

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0 °

C

Oil

dis

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Pe

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tra

tio

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t 2

5 °

C,

100

g, 5

Se

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So

lub

ility

in C

2H

Cl 3

UK US MY SG

Tack - Coat 38% 0.10% 1% +ve 25 Max - 3 60-200 97.5 K1-40 RS-0K

Rapid Setting 50% 0.10% 1% +ve 20-50 - 3 60-200 97.5 RS-1K

Rapid Setting 57% 0.10% 1% +ve - - - - - K1-60

Rapid Setting 60% 0.10% 1% +ve - 20-100 3 60-200 97.5 CRS-1 RS-2K RS-2K

Rapid Setting 65% 0.10% 1% +ve - 100-400 3 60-200 97.5 CRS-2 RS-3K RS-3K

Rapid Setting 67% 0.10% 1% +ve - - - - - K1-70

Medium Setting 57% 0.10% 1% +ve - - - - - K2

Medium Setting 60% 0.10% 1% +ve - 50-450 20 60-200 97.5 MS-1K SM-K

Medium Setting 65% 0.10% 1% +ve - 50-450 12 60-200 97.5 CMS-2 MS-2K CM-K

Slow Setting 56% 0.10% 1% +ve - - - - - K3

Slow Setting 57% 0.10% 1% +ve 20-100 - - 60-200 97.5 CSS-1 SS-1K SS-K

UK- United Kingdom Standard | US- United States Standard | MY- Malaysia Standard | SG- Singapore Standard

Type & Grades of EmulsionsThe emulsion type refers to the nature of the mechanism used to stabilise the emulsion. Emulsions generally fall into either cationic or anionic types. The grade relates to the degree of mixing stability. Grades within each type can be modified with regard to the nature of the base bitumen and rate of ‘break’ or ‘set’ (deposition of bitumen droplets in contact with mineral aggregates) depending on the specific application requirement.

PackingStandard Seaworthy Exportable Packing in 200Kg New or Re-Conditioned Steel Drums/Platic Drums/1 Ton IBC Containers. 4 drums per pallet if Palletizing required.

If any special grades of emulsion required, contact our team

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SPECIFICATION UNIT 85/25 95/25 90/40 115/15 TEST METHOD

Specific Gravity at 25°C 1.01 - 1.05 1.01 - 1.05 1.01 - 1.05 10.1 - 1.05 ASTM D-70

Penetration at 25°C, 100 gm, 5 sec 0.1MM 20/30 20/30 35/45 10/20 ASTM D-5

Softening Point, Ring & Ball °C 80/90 90/100 85/95 110/120 ASTM D-36

Ductility at 25°C, after TFOT, Min CM 1.5 1.5 1.5 1.5 ASTM D-113

Loss on Heating, Max %Wt 0.2 0.2 0.2 0.2 ASTM D-6

Flash Point Cleveland open cup, Min °C 260 260 260 260 ASTM D-92

Solubility in CS2, Min %Wt 99 99 99 99 ASTM D-4

OXIDISED BITUMEN

OXIDIZED BITUMEN Industrial bitumens (or oxidized bitumens) are made by blowing air through hot paving grade bitumen.

The so-called blowing process results in harder bitumen that softens at a higher temperature than that at which paving grade bitumen softens. Industrial bitumens also have more rubber-like properties and their viscosities are much less affected by changes in temperature than is the case with paving grade bitumen. Hard bitumen under controlled temperature conditions is widely used as an anti-slip layer compound in the piling industry, for manufacture of roofing felts, the roofing and waterproofing industries, for sound dampening felts and under carriage sealant in the automotive industry, electric cable joint protection, joint filling compound, sealant compound and many others. Also used in sealing saw cuts and joints where expected movements are minimum.

Some of the major advantages of Oxidized Bitumen are that it is completely water resistant, highly flexible and durable. Further, it is chemically very stable. Oxidized bitumen is a very flexible compound that is not only chemically stable but also a very durable compound apart from being completely water resistant. Lastly, Oxidized Bitumen has some very prominent technical advantages that makes it a very sought after compound in various applications.

The most popular grades are; grades 95/25, 85/25, 90/40, and 115/15.

We are also capable of producing and supplying other grades of Oxidized Bitumen according to the specifications of individual clients.

Uses & ApplicationsOxidized Bitumen high softening temperatures qualify them as excellent sealant for prevention from bleeding in high temperature applications. Oxidized Bitumen is predominantly used in the piling industry as an anti slip compound for the manufacture of under carriage sealants in the automobile industry. It is also used as a sealant compound, as a joint filling compound apart from being used in the manufacture of roofing felts and sound dampening felts. Further, Oxidized Bitumen is used in the manufacture of bituminous marine mastic, which is required for the oil and gas pipeline joints. Some of the application of the oxidized bitumen are as follows• roofing and waterproofing industries• carpet-backing• corrosion protection• acoustic panels• manufacture of paints

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TANKER | BULK SUPPLY

Bitumen Tanker availability on some Global Markets is quite tight and insufficient vessels are available, however making use of our good network of ship owners, tanker operators and our integrated own shipping team will assist our clients to materialize bulk supplies. The company also has strong relationships with many refiners of bitumen both small and large throughout the world and is therefore able to offer a wide range of supply solutions.

Our shipping team ensures best freight rates for voyage charters or time charters and will assist our clients to meet their Bitumen requisitions. Bulk bitumen cargoes can be supplied in tankers ranging in size between 1,000 and 8,000 metric tons. We can supply on a Delivered ex-Ship, CIF, C&F or FOB basis depending on the customer’s needs. While most deliveries by tanker will be direct into a tank terminal, we can arrange for discharge into trucks if a terminal with pipeline connection to a jetty is not available.

Our quality assurance team will implement and engage appropriate quality control measures to maintain the quality of the bitumen shipped throughout the voyage so that our clients may receive quality bitumen at their destination terminals. In bulk shipments we appoint internationally reputed inspection company to carry out Bitumen quality inspections and certifications for the clients from point of loading to point of delivery.

Thanks to our wide range of contacts we endeavour to offer supply of bitumen complying with the client’s local specifications rather than delivering a generic grade. In order to support this service we can arrange testing and analysis of bitumen prior to conclusion of a contract in order to ensure that the product will meet customer requirements.

Factors affecting Ocean Freight RatesUnderstanding ocean freight rates and the ways and means of its applicability is important because if a shipper undertakes to transport the goods without proper knowledge, then he could end up making a huge loss. The following are the factors affecting ocean freight rates1. Intended destination: The destination is

a factor when calculating ocean freight rates. Longer the journey, the exorbitant the ocean shipping rates and vice-versa as mostly the Bitumen vessel after discharging returns empty to the source.

2. Service Charges: Any extra charge levied by port authorities like the security service charges also tends to affect the ocean freight rate

3. Season: During monsoon season thedemand for Bitumen is low and the vessel’s are ideal, hence the vessel owner or operator try to recover costing during the peak season.

4. Terminal Fees: The ocean freight also depends on the terminal fees to be paid while embarking the journey from a port and after reaching the intended destination.

5. Bunker Price: Rising fuel prices and the latest prevailing fuel rates will affect the freight charges

6. Vessel Capacity: If the shipper does not have enough goods to fill the vessel to

their optimum capacity, it will affect the freight charges by way of the shipper having to pay more in spite of lesser quantity

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PACKING |

POLYBAG/BITUBAGThe Bag is a self-stabilizing flexible container made of an outer plastic bag and an inner liner. The bag is designed to carry road paving or industrial bitumen, taking into account of the visco-elastic flow characteristics at (solid) storage and transport conditions. While filling the bags the bitumen is exactly cooled down to a temperature slightly higher than the softening point of the bitumen and lower than the melting point of the plastic material of the container.

It is suitable for packing in liquid condition at ideal product temperature. The inner liner bag is made of a meltable plastic film. Bag volume and shape are designed for maximum loading of normal seagoing standard containers and road trucks. This mode of packing allows economical supply of any volumes (from a few tons to hundreds of thousand tons) and reaching the end-consumer

Advantages: • reduction of logistics costs up to 40% • feasible and economical for any quantities (from several tons up to hundred thousands of tons)• “soft” bitumen grades (road paving bitumen) packed in flexible, easy-to-handle, plastic

container• applicable for all climatic corrditions• environmentally friendly (in comparison to metal drums): inner liner is melted together with the

bitumen, the outer plastic bag («2kg) is recyclable• high safety and stability during transport• long-term outdoor storage• can be transported by any means of conventional transportation (ships, containers, trucks,

railways etc.)• dimensions concur with international transportation standards

Storage & Handling RecommendationsFor normal operations storage temperature limits 1°C-50°C.

SPECIFICATION POLYBAG BITUBAG

Capacity

Filling quantity for Bitumen (net)

300Kg 1000Kg

Loading in 20Ft Container

Number of Bags 80 20

Quantity of Bitumen - Net Weight

= 24MT = 20MT

* The outer bag is made of PP Fabric and inner Liner is made of Polyethylene.* Storage under the roof: 12 Months

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PACKING | POLYBAG/BITUBAG | STEEL DRUMS | ISO CONTAINER/ BITUTAINER

ISO Container / Bitutainer These are essentially containers designed for shipment of bitumen in larger quantities and in containerized form. In certain locations, such as developing countries or in small islands where bulk bitumen receiving facilities do not exist supply of bitumen in an ocean tanker is not possible. The needs of customers in such locations can be met using ISO tank containers with a capacity of 20 MT. Supply in Containers usually requires the customer to commit to receiving bitumen on an on-going basis because of the need to set up facilities for the discharge of the containers. Typically tonnage might range from 20 MT - 500 MT per month depending on location and the customer’s needs. Projects which require large volumes in a short period can be accommodated using a combination of supply by tanker into bitumen containers, temporary storage in portable tanks or a bitumen barge for example. Again, our focus is on accommodating the customer’s needs in the most efficient manner. All containers meet all International Maritime rules, regulations and classifications and are certified by Lloyds or other internationally accepted certifying bodies for containers used in International Maritime Containerized Shipments. All Bitumen Containers supplied are highly isolated and ensure the quality of the Bitumen transported and or stored in them is maintained throughout the operations they are intended for.

FAQ on typical Bitutainers Q: Are Bitutainers supplied with heating and handling equipment included? A.No, Bitutainers are supplied with factory installed heater tubes but Burner Sets and other equipment is not included.

Q: What are the heating options?A.Three options; Direct Fire Diesel or LPG Burners, inserting electric elements into the direct fire heating tubes or by using Thermal Oil from an existing circuit. Direct Fire heating is the most popular option.

Q: How long does it take to heat a full Bitutainer? A.Typically it will take 10-11 hours to heat a full Bitutainer (using a 2001tr of diesel) from ambient (approx. 200C) to pumping temperate (approx. 1400C).

Q: Can 40ft Bitutainer be transported full? A.No, 40ft Bitutainers are for storage only. They are not designed or certified for transportation full of product.

Q: Do Bitutainers ship as standard containers? A.Yes, they are shipped as standard CSC plated containers

Q: Are Bitutainers suitable for all grades of Bitumen? A: Yes, Bitutainers are suitable for all grades of bitumen, PMBs and heavy fuel oils. The exception is Coal Tar due to the higher temperatures required for discharge and transfer.

HandlingAvoid contact with eyes, skin, clothing and foodstuffs. Wash thoroughly after handling. Launder contaminated clothing prior to use; use good personal hygiene. This product is a hazardous substance when heated above I00°C. Storage: Keep product away from ignition sources such as heat, sparks and flame. Extinguish pilot lights, cigarettes and turn off other sources of ignition prior to use and until all vapors has dissipated. Store in a cool, dry and well ventilated area. Keep containers closed at all times.

SPECIFICATION(STEEL DRUMS)

150KG 180KG

Plate Thickness

Body 0.6 ± 0.02mm 0.6 ± 0.02mm

Top and Bottom 0.6 ± 0.02mm 0.7 ± 0.02mm

Height 86 cm 98 cm

Diameter 50 cm 50 cm

Lid Hole Position Center

Lid Hole Diameter 10 ± 1 cm 10 ± 1 cm

Net Filling capacity 147 ± 3 kg 182 ± 3 kg

Gross Weight 156 ± 3 kg 192 ± 3 kg

Drum Tare Weight 8.2 ± 0.1 kg 9.5 ± 0.1 kg

Color Glossy Black

Loading in 20ft Container- With Pellet

Number of Drums 80 80

Bitumen net weight ≈12.00 MT ≈14.40 MT

Loading in 20ft Container- Without Pellet

Number of Drums 110 110

Bitumen net weight ≈16.50 MT ≈19.80 MT

*Drums supplied will be of good workmanship and are sufficiently leak proof when filled with hot Bitumen*DIN 1623 ST12 new cold rolled A grade steel

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ROYAL PETRO ENERGY’S GLOBAL PRESENCE

Hamriyah Free zoneSharjah , UAEPO Box : 52197

Email: [email protected]

• UAE• Bahrain• Kuwait• Oman• Qatar• Saudi Arabia• India• Africa• Pakistan• Bangladesh• Malaysia• Indonesia• Singapore• Nepal• China

A leading player in oil space, specializing in Oil Trading, Oil Refining, Grease Manufacturing, Oil Storage Terminals, Diesel Trading, Bitumen Manufacturing, Shipping & LogisticsEstablished in the year 2005, Royal Petro Energy initially started as an oil trading company and with years of hard work and its commitment to perfection has now emerged as one of the leading organizations in the oil trading industry of Middle East Royal Petro Energy engaged in trading of Group I and Group II Base Oil which is exported in bulk quantities to North East Asia, Africa, and the Middle East and has a major share of the market in UAE and India

ROYAL PETRO ENERGY FZCHAMRIYAH FREE ZONESHARJAH , UAEPO BOX : 52197EMAIL: [email protected]

ROYAL INDUSTRIES FZ LLCAL GHAIL INDUSTRIAL PARKRAS AL KHAIMAHUAEPO BOX : 86022EMAIL: [email protected]

ROYAL LUBRICANT AND GREASE MANUFACTURING LLC PO BOX : 2494TEL : +971 6 7481453FAX: +971 6 7481463EMAIL: [email protected]

OIL AND GAS ENTERPRISE FZCPO BOX 52763HAMRIYAH FREE ZONE, SHARJAHHAMRIYAH, SHARJAHUNITED ARAB EMIRATESEMAIL: [email protected]

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