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    Edwards Fiberglass, Inc.PO Box 1252 Sedalia, MO. 65301 Telephone Number 660-826-3915 Fax Number 660-827-2793

    TANK CATALOG

    THIS INFORMATION IS FOR MARKETING AND

    ENGINEERING PURPOSES ONLY. THE RECIPIENT HAS NO

    AUTHORITY TO FORWARD THIS DOCUMENT TO ANYONE

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    AUTHORITY TO FORWARD THIS DOCUMENT TO ANYONE

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    FIBERGLASS REINFORCED PLASTIC STORAGE TANKS

    1. SCOPE

    This section covers the furnishing of tanks fabricated of fiberglass reinforced plastic and intended forabove and belowground bulk storage of chemical solutions.

    This specification is not intended to be used in the fabrication of tanks intended for pressure and/orvacuum conditions or heating liquids above their flash points.

    When additional specifications are issued for special applications, they shall also be considered a part ofthis specification.

    2. GENERAL

    Tanks furnished under this section shall be fabricated and assembled in full conformity unless exceptionsare noted by Customer/Engineer. When additional specifications are issued for special application, theyshall also be considered a part of this specification as it pertains to the manufacturing of FRP tanks.

    3. SUBMITTALS

    Complete drawings and details covering the storage tank, connections and accessories shall be submitted forCustomer review and approval.

    The data shall include information on all tank fabrication, materials of construction, and data confirmingchemical resistance of the proposed resins to the intended tank contents.

    Drawings shall include a profile of the entire tank indicating the thickness, resin designation, reinforcement,and surfacing mat material of the structural and corrosion barrier layers.

    The drawings shall also indicate the sizes of all major tank components and/or accessories.

    4. OPERATION AND MAINTENANCE MANUALS

    The operation and maintenance manual shall include project information, certified copy of the tank drawing,copies of the tank certification label, quality control inspection report, and warranty.

    Data shall include handling and installation procedures, flange and tank repair procedures and accessory

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    518

    the specified positive and negative pressure not to exceed 14 in. of water when all tie down lugs areproperly secured, in accordance with the fabricators recommendations for flat-bottom tanks.

    Tanks meeting this specification are classified according to grade as follows:

    Grade 1: Tanks manufactured with a single generic type of thermoset resin throughout.

    Grade II: Tanks manufactured with different generic types of thermoset resin in the barrier and thestructural portion.

    7. GENERAL PRODUCTS AND ACCESSORIES

    STANDARD TANK INSIDE DIAMETER

    20 624 7

    28 8

    30 9

    36 10

    42 11

    48 12

    54 13

    60 1472 17.5

    TANKCONFIGURATIONS

    Cylindrical Dome Flat

    Horizontal Open w/Rim Flange Dome

    Rectangle Flat-Bonded Cone-30, 40& 60 Degree

    Above and Below Ground Flat-Bolted w/Rim Flange Internal/External Slopes

    TOP DESIGNS BOTTOM DESIGN

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    8. BASIC MATERIALS

    Resin: The resin used shall be a commercial-grade, corrosion-resistant thermoset that has either been evaluated ina laminate or has been determined by previous documented service to be acceptable for the service conditions.

    The resin shall contain no pigment, dyes, colorants, or filler, except as follows:

    a. A thixotropic agent that does not interfere with visual inspection of laminate quality, or with the requiredcorrosion resistance of the laminate, may be added for viscosity control.

    b. Resin pastes used to fill crevices before overlay

    c. Ultaviolet absorbers may be added to the exterior surface for improved weather resistance.

    d. Antimony compounds or other fire-retardant agents may be added for improved weather resistance

    Chopped Strand Mat: Chopped strand mat shall be constructed from chopped commercial-grade E-typeglass strands bonded together using a binder. The strands should be treated with a sizing that is chemicallycompatible with the resin used.

    Continuous Roving: Continuous roving shall be a commercial-grade of E-type glass fiber with a sizingthat is chemically compatible with the resin system used.

    Woven Roving: Woven roving shall be in accordance with ASTM D2150.

    Surfacing Mat: The reinforcement used for the inner surface shall be either a commercial-grade chemicalresistant glass surface mat or an organic-fiber surface mat. In environments that attack glass, the use of an

    Chemical compatibleResin

    Chopped Strand Type E Glass

    Continuous Roving Type E Glass

    Woven Roving 60 End-Type E Glass-24oz per sq. ydRoving for Filament Winding Type E Glass, continuous filament strand

    Fillers-By Request UV Protection and Fire Retardance

    Surfacing Mat C-veil or Nexus whichever is suitable for chemical

    Metal Customer Specified

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    All measurements in inches

    Nozzles 4 in and smaller shall be supported by a suitable gusseting technique, using plate gussets or conical

    gussets. Plate gussets, where needed, shall be evenly spaced around the nozzle and are to be added aftercomplete assembly by the nozzle on the shell. Larger nozzles, subject to superimposed mechanical forces,require special consideration.

    Manways installed in top heads may be of the flanged or nonflanged design, as agreed upon between thefabricator and purchaser.Vents: Tanks that discharge freely into the atmosphere must be provided in all Type I closed-top tanks.Minimum vent size shall be sufficient to handle the flow displacement of all combined inlet or outlet nozzleswithout creating any pressure above atmospheric, or any vacuum condition.

    Special vent sizing consideration should be given to the numerous operating situations that could otherwisecause a positive or a negative pressure in a closed tank. Since overfilling a closed tank with the vent on the topcan cause the tank to be over-pressured, a suitably sized overflow, properly located, or other appropriateprotection ma be req ired to pre ent o er press ri ing the tank

    Nozzle

    Inside

    Diameter

    Minimum

    Wall

    Thickness

    Minimum

    Flange

    Thickness

    Minimum

    Hub

    Thickness

    Minimum

    Hub

    Length

    1

    3/161/2

    1/421 1/2 3/16 1/2 1/4 2

    2 3/16 1/2 1/4 2

    3 3/16 1/2 1/4 24 3/16 1/2 1/4 2

    6 3/16 1/2 1/4 28 3/16 9/16 5/16 2 1/2

    10 3/16 11/16 3/8 2 3/4

    123

    /163

    /43

    /8 314 1/4 13/16 7/16 3 1/4

    16 1/4 7/8 7/16 3 1/218 1/4 15/16 1/2 3 1/420 1/4 1 1/2 4

    24 1/4 1 1/8 9/16 4 1/2

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    Structural Tank: The laminate comprising the structural tank (bottom, shell, top head) shall consist of acorrosion-resistant barrier comprised of an inner surface, interior layer, and a structural layer.

    Inner Surface: The inner surface exposed to the chemical environment shall consist of a resin rich layer 0.010to 0.020 in. thick, reinforced with a suitable chemical-resistant glass fiber surface mat or with an organic fibersurface mat.

    Interior Layer: The inner surface layer exposed to the corrosive environment shall be followed with a layercomposed of resin, reinforced only with non-continuous glass-fiber strands applied in a minimum of two pliesof chopped-strand mat. As an alternative, a minimum of two pass of chopped roving of minimum length of 0.5in. to a maximum length of 2.0 in. shall be applied uniformly. Each ply of mat or pass of chopped roving shallbe well-rolled prior to the application of additional reinforcement. The combined thickness of the inner surfaceand interior layer shall not be less than 0.10 in.

    Glass content of the inner liner and the interior layer combined shall be 27 +/- 5% by weight.

    The degree of cure of the laminate shall be such as to exhibit a Barcol hardness on the inner surface of at least90% of the resin manufacturers minimum specified hardness for the cured resin.

    Structural Layer:

    Filament Wound: Subsequent reinforcement shall be continuous-strand roving. The thickness of the filament-wound portion of the tank shell may be varied with tank height (tapered-wall construction). If additionallongitudinal strength is required, the use of other reinforcement such as woven fabric, chopped-strand mat, orchopped strands, may be interspersed in the winding to provide additional strength. Glass content of thisfilament-wound structural layer shall be 50 to 80% by weight.

    Contact-Molded Structural layer in Top and Bottom Heads: Subsequent reinforcement shall be comprised of1.5 oz/ft chopped-strand mat or equivalent weight of chopped roving, or shall be comprised of chopped-strandmat or chopped roving and such additional number of alternating plies of 24 oz/yd woven roving 18 oz/yd non-woven biaxial fabric to a thickness as required to meet the physical properties that are used for the design.Each successive ply or pass of reinforcement shall be well-rolled prior to the application of additionalreinforcement. Where woven roving is used, chopped-strand glass reinforcement shall be used as alternatingand final layers. All woven roving and surfacing mat shall be overlapped. Laps in subsequent layers shall be

    staggered at least 2.25 in. from laps in the preceding layer.

    When the outer surface of this structural layer is to be subject to spillage or a corrosive environment, a resin-rich layer, shall be applied over the final layer of reinforcement.

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    Fittings and Accessories: The surfaces of fittings, tank accessories, and the laminates required for theirinstallation that are exposed to the corrosive media shall be constructed in accordance with this specificationexcept for those fitting surfaces which are made by manufacturing processes other than contact molding.

    The cut edges of all laminates exposed to the chemical environment shall be sealed with a laminate. Whereshape, thickness, or other restrictions preclude covering the edges with laminate, such cut edges and any

    machined flange faces shall be at least coated with resin. In either case, the resin used shall be the same used inthe equipment laminate.

    Nozzle and Manway Installation: Flanged nozzles may be installed with the pipe stub flush inside the tankshell or projecting inside the tank.

    Nozzle Projection: The installed nozzle shall maintain a clearance of 3 in. between the back of the flange andthe exterior of the cutout opening reinforcement. In addition, this clearance shall not be less than the sheardistance required for proper installation of the nozzle.

    Cutout Reinforcement Laminate: When a vessel shell or head is cut in an area bearing hydrostatic pressure,the cutout shall be reinforced on a circular area concentric with the cutout.

    Cutout Reinforcement Diameter: The outer diameter of the cutout reinforcing laminate, shall not be less thantwo times the nominal nozzle diameter. For nozzles less than 6 in. in diameter, the minimum cutoutreinforcement diameter shall be the nominal nozzle size plus 6 in.

    Cutout Reinforcement Thickness: The thickness of the cutout reinforcement laminate for nozzles installed incylindrical shells or dished heads shall be determined by nozzle and tank size.

    When reinforcing materials are cut to facilitate placement around and installed nozzle, joints in successivereinforcing layers should be staggered to avoid overlapping and (on cylindrical shell installation) shall not beplaced so they are parallel the axis of the tank. The intent of this requirement is to avoid orienting joints inreinforcing layers perpendicular to the maximum load-bearing direction.

    Nozzle Installation Laminates: The all interior installation laminate placement is used only when the nozzlebeing installed has an integral conical gusset preventing application of an exterior laminate.

    Installation Laminate Thickness: The inside and outside installation thicknesses combined shall be at least asthick as the nozzle neck.

    Inside Installation Laminate Construction: The inside installation laminate shall be constructed using only

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    11. DIMENSIONS AND TOLERANCES

    Standard tank diameters are based on internal measurements with the tank in the vertical position.

    Tolerance on the inside diameter, including out-of-roundness, shall be +/- 1%.

    Shell taper shall be additive to the figure used for the tank diameter. Shell taper shall not exceed 1/2 degree perside.

    Tolerance on overall tank height shall be 1/2%, but shall not exceed +/- 1/2 in.

    Nozzle flange faces shall be perpendicular to the axis of the pipe and shall be flat within +/- 1/32 in. through 18in. nozzle size and 1/16 in. for large nozzle sizes.

    The standard orientation of flanges shall provide bolt holes straddling the normal centerlines of the tank. Bolt

    holes of flanges located on the tank top or bottom, shall straddle the principal centerline of the vessel or linesparallel to it.

    12. WORKMANSHIP, FINISH and APPEARANCE

    The minimum acceptable for workmanship and finish of the finished laminate shall conform to the requirementsspecified in Section 9 of Specification C 582.

    13. REQUIRMENTS

    Degree of Cure: Degree of cure of the laminate shall be found by determining the Barcol hardness.

    A useful technique to check the cure of a non-molded surface of a polyester resin is as follows: Rub a fewdrops of acetone on the laminate surface until it evaporates. If the surface becomes softened or tacky, it isindication of under cure.

    The use of organic reinforcing materials may reduce the Barcol readings without necessarily indicating undercure.

    Barcol hardness values may vary upon temperature.

    14. PRODUCT MARKING

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    OC SURFACING VEILSPRODUCT INFORMATION

    PRODUCT FAMILY INTRODUCTION

    OC Surfacing Veils

    are designed to give surface

    enhancement to composite

    laminates.They are designed to

    add reinforcement at the surface

    of a laminate and provide a

    smooth, resin-rich, durable

    surface.The surface layer is an

    aesthetic enhancement and a corrosion resistant barrier

    for the finished part.The wide range of products means

    that the user may select one that satisfies both process

    and end-use performance requirements.

    VEIL TYPES

    OC Surfacing Veils are available in two types, Dry Process

    C Veils and Wet Laid ECR Veils. Each is manufactured

    through a process that is suitable for many composite

    processes.

    OWENS CORNING C VEILS

    OC C Veils provide corrosion resistance and surfaceenhancements in many composite manufacturing

    processes. OC C Veils contain C Glass, which is a

    chemically resistant glass that withstands acid and alkaline

    OWENS CORNING ECR VEILS

    OC ECR Veils are uniform and can be used in a variety

    of composite manufacturing processes. OC ECR Veils

    are made with Advantex glass fiber reinforcements, which

    combine the electrical and mechanical properties of

    E Glass with the corrosion resistance of ECR glass.

    BINDERS

    OC Surfacing Veils are available with either high solubility

    or low solubility binders. Low solubility binders provide

    superior wet strength and resist fiber washing, yet maintain

    rapid wet-out. High solubility binders dissolve in styrene

    based resin systems and offer very fast wet-out and

    conformability to complex part curvatures as the binder

    is dissolved.All binders are compatible with polyester,

    vinylester and epoxy resins.

    GLOBAL QUALITY

    Owens Corning continues to meet ongoing customer

    demands for higher productivity, higher value products

    and excellent support. OC Surfacing Veils are high-quality

    products produced with a multi-regional process that helpsto ensure consistent products in many regions of the

    world while meeting performance and cost requirements.

    The Owens Corning worldwide technical and marketing

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    OC SURFACING VEILS

    OC SURFACING VEIL PRODUCTS (M524)THICKNESS BASIS WEIGHT STYRENE WIDTH STANDARD WIDTHS

    MILS CM G/M2 SOLUBILITY INCHES CM STOCKED IN NORTH AMERICA

    Wet Process Advantex Veils

    ECR25A 10 0.5 25 low 1.5 - 83 3.5 - 210 10" (25 cm), 39"(1m), 50" (127cm)

    ECR50A 19 1.0 50 low 1.5 - 83 3.5 - 210 39" (1 m)

    ECR70A 27 1.4 70 low 1.5 - 83 3.5 - 210 39" (1 m)

    ECR30S 12 0.6 30 high 2 - 83 5 - 210 39" (1 m)

    Dry Process "C Veils"C64 11 0.29 30 high 2 - 72 5 - 200 39.4" (1 m), 50" (127 cm)

    C33 12 0.32 33 low 2 - 72 5 - 200 39.4" (1 m), 50" (127 cm)

    OC SURFACING VEIL PRODUCT SELECTIONThickness

    OC Surfacing Veils are generally selected first based

    on thickness in the composite part.The standard forcorrosion resistance and surface enhancement is 10 mil

    (0.5 mm). Thicker veils are selected for enhanced surface

    print blocking or added corrosion protection through a

    thicker resin-rich surface layer. Generally the thinnest

    layer that gives sufficient surface properties is chosen.

    For closed molding and infusion process with higher glass

    content in the laminate, thicker veils are often required

    to mask the substrate reinforcements.

    Solubility and Binder Selection

    The selection of the appropriate binder is based on the

    composite process and matrix resin chemistry. For open

    Wet Process Advantex vs. Dry Process "C-Veil"

    OC C-Veils are a standard for the corrosion and open

    molding industries. The familiarity in handling these

    combined with a fiber architecture that allows easy wet-

    out, make these preferred products of many molders.The

    long fibers in OC C Veils can give more conformability in

    complex parts.Advantex OC ECR Veils are a newer

    product with advantages in some applications.The Wet

    Process used to produce these OC ECR Veils makes a

    product with very high small-area weight uniformity.

    The binders applied can give a high and uniform tensile

    strength to the OC ECR Veil for processes such as

    filament winding. Both OC Surfacing Veil product typesoffer excellent corrosion resistance.

    Owens Corning manufactures a very broad range of OC

    S f i V il d d h h bi d d

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    COMPOSITE POLYMERS DIVISION OF ASHLAND CHEMICAL CO. DIVISION OF ASHLAND

    INC.BOX 2219, COLUMBUS, OHIO 43216 (614) 790-3333

    TECHNICAL DATA

    AROPOL 7241T-15Isophthalic Polyester Resin

    MAY 1998

    CORROSION AND HEAT RESISTANT, ISOPHTHALIC POLYESTER RESIN

    DESCRIPTION: AROPOL 7241T-15 resin is a thixotropic, promoted, corrosion resistant,

    isophthalic polyester resin. The raw materials used in the manufacture

    of this resin are listed as acceptable in FDA regulation Title 21 CFR

    177.2420 for repeated use in contact with food, subject to the user'scompliance with the prescribed limitations of that regulation.

    PERFORMANCE: Excellent corrosion resistance

    High strength

    High heat deflection temperature

    MIL-R-7575C Grade A capability

    SUGGESTED USES: AROPOL 7241T-15 resin can be used for hand lay-up and spray-upapplications, such as, fabrication of fume hoods and ducts, tanks, pipe,

    storage tank repairs and linings in applications where corrosion

    resistance and FDA food applications resins are required.

    ALTERNATIVE PRODUCTS: AROPOL 7241 resin is the same base resin, however, it is not thixotropic

    and is unpromoted. AROPOL 7240T-15 resin is recommended for

    applications that require greater corrosion resistance. For improved high

    temperature/corrosion resistance, contact your Ashland Chemical

    technical service representative.

    TYPICAL * LIQUID PROPERTIES AT 77F (25C)

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    AROPOL 7241T-15 Resin (continued)Copyright 1998, Ashland Inc.

    TYPICAL * PERFORMANCE DATA

    (for guidance only)

    TYPICAL CURING CHARACTERISTICS AT 77F (25C):

    1.25% LUPERSOL1 DDM-9 Catalyst

    Gel Time, minutes 13

    Total Time, minutes 28

    Peak Exotherm, F 380

    Temperature LUPERSOL DDM-9 Catalyst Level, phr

    F 0.63 1.25 1.88

    60F 55 27 15

    70F 46 19 11

    80F 29 12 7

    90F 14 7 4.5

    TYPICAL* MECHANICAL PROPERTIES

    TYPICAL PHYSICAL PROPERTIES OF CURED CASTINGS2 AT 77F (25C):

    TEST VALUE TEST METHOD

    Barcol Hardness 45 ASTM D-2583

    Tensile Strength, psi 10,700 ASTM D-638

    Tensile Modulus, psi x 105 5.4 ASTM D-638

    Tensile Elongation, % 2.4 ASTM D-638

    Flexural Strength psi 19 000 ASTM D 790

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    AROPOL 7241T-15 Resin (continued)

    RECOMMENDED STORAGE:

    Drums - Store at temperatures below 80F. Storage life decreases with increasing storage temperature.

    Avoid exposure to heat sources such as direct sunlight or steam pipes. For thixed resins, mild agitation is

    recommended to address thixotrope settling after prolonged storage. Rotate stock.

    Bulk - See Ashland Chemicals Bulk Storage and Handling Manual for Polyesters and Vinyl Esters. A copy

    of this may be obtained from Ashland Chemicals Composite Polymers Division at (614) 790-3333.

    SHELF LIFE: This product has a limited shelf life. When stored in accordance with the above conditions,

    this product has a minimum shelf life of three months.

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    INTERPLASTIC CORPORATIONThermoset Resins Division

    2015 Northeast Broadway Street

    Minneapolis, Minnesota 55413-1775

    (651) 481-6860 Fax (612) 331-4235

    TECHNICAL DATA SHEET: CORVE8301CORVE8301 is a corrosion resistant, promoted, bisphenol A epichlorohydrin based, vinyl ester resin. Uses include tankrelining, pipe fabrication, tank construction, and applications where a promoted (for gel and cure with MEKP) vinyl ester resinis desired. CORVE8301 is manufactured from ingredients listed as acceptable in the FDA Code of Federal Regulation Title 21,CFR 177.2420. This resin may safely be used as a component of articles intended for single or repeated use in contact withfood as prescribed in the regulation. See CoREZYN Vinyl Ester Resins publication 4/02 A-006a for corrosionrecommendations and general information.

    FEATURES: BENEFITSHigh physical properties: Makes extremely tough compositesHighly versatile viscosity properties: Formulated for spray-up and hand lay-up needs

    Promoted resin system: For ease in field applications

    Outstanding corrosion resistance: Resists caustic and solvent with hydrolytic stability

    High heat distortion resistance: Maintains dimensional stability

    LIQUID PROPERTIES

    Viscosity, Brookfield Model LV #3 Spindle @ 60 rpm, 77F (25C), cps 425-575

    100 grams resin @ 77F (25C), catalyzed with 1.2% Hi-Point 90 by volume*

    Gel Time, min:sec 16:00-19:00

    Gel to Peak Exotherm Time, min:sec 9:00-15:00

    Peak Exotherm 325-360F (162-182C)

    Non-Volatile Content, % 53.5-56.5

    Specific Gravity 1.02-1.05

    TYPICAL PROPERTIES: Thickness 1/8 inch (3.2 mm) Casting 1/8 inch (3.2 mm) Laminate

    Construction Not applicable 4 Plies, 1.5 oz/ft2, 30% Glass Mat

    Flexural Strength, ASTM D790 19,000 psi 130 MPa 23,600 psi 163 MPa

    Flexural Modulus, ASTM D790 4.5 X 105 psi 3,100 MPa 12.0x105 psi 8,276 MPa

    Tensile Strength, ASTM D638 11,500 psi 80 MPa 16,000 psi 110 MPa

    Tensile Modulus, ASTM D638 5.0 X 105 psi 3,450 MPa 11.0x105 psi 7,586 MPaTensile Elongation, ASTM D638 5.0 % 5.0 %

    Barcol Hardness, 934-1 gauge, ASTM D2583 35 35

    Heat Distortion Temperature, ASTM D648 210 F 99 C

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    Composite Polymers Division of Ashland Specialty Chemical Co. Division of Ashland Inc.

    Box 2219, Columbus, Ohio 43216 (614) 790-3333

    TECHNICAL DATA

    HETRON

    922

    Epoxy Vinyl Ester Resin

    FEBRUARY 2001

    CORROSION RESISTANT, EPOXY VINYL ESTER RESIN

    DESCRIPTION: HETRON 922 resin is a low viscosity, unpromoted patented epoxy vinyl ester

    with F-Cat technology. The raw materials used in the manufacture of this resin

    are listed as acceptable in FDA regulation Title 21 CFR 177.2420 for repeated

    use in contact with food, subject to users compliance with the prescribedlimitations of that regulation.

    PERFORMANCE: Excellent corrosion resistance

    Excellent impact strength

    High tensile elongation

    Patented chemistry results:

    No foaming

    Exotherm control Industry-leading storage stability

    SUGGESTED USES: HETRON 922 resin can be used with hand lay-up, spray-up, and filament

    winding. It can also be used for flake glass and filled lining and coating

    compounds.

    ALTERNATIVE PRODUCTS: HETRON 922L epoxy vinyl ester resin has a lower viscosity. HETRON 942/35

    epoxy vinyl ester resin should be used when higher operating temperatures or

    greater resistance to organic solvents is needed. HETRON FR 992 vinyl ester

    resin provides flame retardancy.

    TYPICAL * LIQUID PROPERTIES AT 77F

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    HETRON 922 Resin (Page 2 of 4)

    TYPICAL * PERFORMANCE DATA

    (For Guidance Only)

    TYPICAL CURING CHARACTERISTICS AT 77F:

    SPI Gel T ime - 180F Bath, 2% LUPERCO1ATC Paste

    Gel Time, Minutes 12

    Total Time, Minutes 20

    Peak Exotherm, F 370

    MEKP Cure System

    Resin

    TemperatureDMA

    6% Cobalt

    NaphthenateCatalyst

    DELTA1

    X-9

    Catalyst

    LUPERSOL1

    DDM-9*

    Catalyst

    HI

    POINT3

    90

    Catalyst

    (F) (phr2) (phr) (phr) Gel Time, Minutes

    14 21 22

    24 31 2965

    0.15

    0.075

    0.05

    0.3 1.25

    40 40 40

    15 17 17

    21 23 2277

    0.075

    0.05

    0.025

    0.3 1.25

    33 35 36

    15 18 18

    22 24 2485

    0.075

    0.05

    0.025

    0.2 1.25

    37 40 40

    BPO / DMA Cure System

    Temperature

    (F)

    50% BPO Paste

    (phr)

    DMA

    (phr)

    Gel Time

    (minutes)0.7 17

    0.5 2465 2.0

    0.3 40

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    HETRON 922 Resin (Page 3 of 4)

    Effects of 8% Copper Naphthenate6

    Resin

    Temperature(F)

    6% Cobalt

    Naphthenate(phr)

    DMA(phr)

    DELTA X-9

    Catalyst(phr)

    8% Copper

    Napthenate(phr)

    Gel

    Time(minutes)

    Gel

    to Peak(minutes)

    Peak

    Exotherm(F)

    0 12 5 33565 0.3 0.15 1.25

    0.04 10 6 225

    0 16 8 32077 0.3 0.075 1.25

    0.04 17 10 215

    0 19 11 31585 0.3 0.04 1.25

    0.04 20 23 180

    0 22 15 31395 0.3 0.02 1.25

    0.04 29 28 120

    Effects of Copper Levels at 77F

    6% Cobalt

    Naphthenate

    (phr)

    DMA

    (phr)

    DELTA X-9

    Catalyst

    (phr)

    8% Copper

    Napthenate

    (phr)

    Gel

    Time

    (minutes)

    Gel

    to Peak

    (minutes)

    Peak

    Exotherm

    (F)

    0 16 9 320

    0.01 16 8 285

    0.02 16 11 280

    0.03 17 11 230

    0.3 0.075 1.25

    0.04 16 13 210

    CAUTION: Thoroughly mix promoters with resin before adding catalyst.

    TYPICAL* MECHANICAL PROPERTIES

    TYPICAL PHYSICAL PROPERTIES OF CURED CASTINGS

    7

    AT 77F:

    TEST VALUE TEST METHOD

    Barcol Hardness 30 ASTM D-2583

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    HETRON 922 Resin (Page 4 of 4)

    MASTER BATCH GUIDE

    6% Cobalt Naphthenate Quantity For:

    55-Gallon (450 lbs.) 5-Gallon (41 lbs.)

    0.2 13.5 fl.oz/400 cc 1.2 fl.oz/36 cc

    0.3 20.3 fl.oz/600 cc 1.8 fl.oz/54 cc

    0.4 27.9 fl.oz/800 cc 2.4 fl.oz/72 cc

    DMA Quantity For:

    55-Gallon (450 lbs.) 5-Gallon (41 lbs.)

    0.05 3.6 fl.oz/106 cc 0.32 fl.oz/9.5 cc

    0.10 7.2 fl.oz/212 cc 0.65 fl.oz/19.0 cc

    0.15 10.8 fl.oz/318 cc 0.97 fl.oz/28.6 cc

    8% Copper Naphthenate Quantity For:

    55-Gallon (450 lbs.) 5-Gallon (41 lbs.)

    0.02 1.0 fl.oz/40 cc 3 cc

    0.03 2.0 fl.oz/60 cc 5 cc

    0.04 3.0 fl.oz/80 cc 7 cc

    9% MEKP Quantity For:

    1 Quart 5 Lbs.

    1.25 0.39 fl.oz/11.4 cc 0.90 fl.oz/26.2 cc

    HANDLING: HETRON 922 resin contains ingredients which could be harmful if mishandled. Contact with skin and

    eyes should be avoided and necessary protective equipment and clothing should be worn.

    Ashland Specialty Chemical Company maintains Material Safety Data Sheets on all of its products. Material Safety

    Data Sheets contain health and safety information for your development of appropriate product handling procedures

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