36
FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA MANAGEMENT PLAN TULSA FUEL AND MANUFACTURING COLLINSVILLE, OKLAHOMA JUNE 2005 Prepared for Oklahoma Department of Environmental Quality Burns & McDonnell Project No. 36478 Burns & McDonnell Engineering Company Engineers-Architects-Consultants Kansas City, Missouri TFM-0000751

FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

  • Upload
    others

  • View
    6

  • Download
    0

Embed Size (px)

Citation preview

Page 1: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

FINAL

REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA MANAGEMENT PLAN

TULSA FUEL AND MANUFACTURING COLLINSVILLE, OKLAHOMA

JUNE 2005

Prepared for

Oklahoma

Department of Environmental Quality

Burns & McDonnell Project No. 36478 Burns & McDonnell Engineering Company

Engineers-Architects-Consultants Kansas City, Missouri

TFM-0000751

Page 2: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Table of Contents Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_TOC.doc TC-1 06/10/2005

TABLE OF CONTENTS

Page No. LIST OF TABLES.............................................................................................................................. TC-2 LIST OF ACRONYMS AND ABBREVIATIONS............................................................................ TC-3 1.0 INTRODUCTION........................................................................................................................1-1

1.1 Objective ............................................................................................................................1-1 1.2 Contact Information ...........................................................................................................1-1

2.0 DATABASE STANDARDS........................................................................................................2-1

2.1 Database Platform..............................................................................................................2-1 2.2 Normalization.....................................................................................................................2-1 2.3 Database Object Naming Conventions ..............................................................................2-2 2.4 Data Types .........................................................................................................................2-2

3.0 TABULAR DATA MANAGEMENT .........................................................................................3-1

3.1 Chemical Data....................................................................................................................3-1 3.2 Borehole Data ....................................................................................................................3-1

4.0 SPATIAL DATA MANAGEMENT............................................................................................4-1

4.1 Spatial Data Format ...........................................................................................................4-1 4.2 Feature Dataset Organization and Naming Conventions ...................................................4-1

5.0 SOURCE DATA HANDLING ....................................................................................................5-1 5.1 Adding Source Data to the Database .................................................................................5-1

5.1.1 Electronic Data......................................................................................................5-1 5.1.2 Hard Copy Data ....................................................................................................5-2

5.2 Archiving Source Data.......................................................................................................5-2 5.3 Metadata Collection ...........................................................................................................5-3

6.0 DATABASE SECURITY ............................................................................................................6-1

6.1 Security Against Unauthorized Use ...................................................................................6-1 6.2 Protection from Accidental Data Corruption .....................................................................6-1 6.3 Physical Safeguards ...........................................................................................................6-2

TABLES APPENDICES APPENDIX A - DAVES Data Dictionary APPENDIX B - FDGC Recommended Minimum Content

TFM-0000752

Page 3: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Table of Contents Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_TOC.doc TC-2 05/12/2005

LIST OF TABLES

Table No. Title

4-1 Feature Dataset and Feature Class Naming Standard

TFM-0000753

Page 4: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Table of Contents Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

LIST OF ACRONYMS AND ABBREVIATIONS

DMP_TOC.doc TC-3 06/10/2005

ASCII American Standard Code for Information Interchange BMcD Burns & McDonnell Engineering Company, Inc. CSDGM Content Standard for Digital Geospatial Metadata DAVES Data Analysis, Validation, and Evaluation System ESRI Environmental Systems Research Institute, Inc. FGDC Federal Geographic Data Committee FS Feasibility Study FTP File Transfer Protocol GIS Geographic Information System GPS Global Positioning System 1NF First Normal Format 2NF Second Normal Format 3NF Third Normal Format 4NF Fourth Normal Format ODEQ Oklahoma Department of Environmental Quality PID Photoionization Detector QA quality assurance QAPP Quality Assurance Project Plan QC quality control RI Remedial Investigation SQL Structured Query Language USEPA United States Environmental Protection Agency .xml Extensible Markup Language

* * * * *

TFM-0000754

Page 5: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Introduction Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_01.doc 1-1 06/10/2005

1.0 INTRODUCTION

Burns & McDonnell Engineering Company, Inc. (BMcD), under contract with the Oklahoma Department

of Central Services Construction and Properties Division on behalf of the Oklahoma Department of

Environmental Quality (DEQ), will conduct a remedial investigation (RI) and feasibility study (FS) at the

Tulsa Fuel and Manufacturing site in Collinsville, Oklahoma. The RI/FS is 100% federally funded

through a Cooperative Agreement between DEQ and the United States Environmental Protection Agency

(USEPA). In order to effectively manage and accurately report data collected during the RI/FS, a plan is

required that documents the intended processes, formats, and uses of attribute and spatial data. This

document is intended to satisfy subtask 1.1 of the Scope of Work for the Tulsa Fuels and Manufacturing

RI/FS, dated January 28, 2005.

1.1 OBJECTIVE The purpose of this document is to facilitate understanding of project data storing, handling, accessing,

and security between DEQ, BMcD, USEPA, and other participating parties.

1.2 CONTACT INFORMATION For assistance with database issues, contact the BMcD project manager or database administrator for this

project:

Tracy Cooley David Smith Project Manager Database Manager Burns & McDonnell Engineering Burns & McDonnell Engineering 9400 Ward Parkway 9400 Ward Parkway Kansas City, Missouri 64114 Kansas City, Missouri 64114 Ph. (816) 822-3369 Ph. (816) 822-4362 Oper. (816) 333-9400 Oper. (816) 333-9400 Fax (816) 822-3494 Fax (816) 822-3463 [email protected] [email protected]

* * * * *

TFM-0000755

Page 6: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Database Standards Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_02.doc 2-1 06/10/2005

2.0 DATABASE STANDARDS

Standards for data storage help ensure that data is effectively managed throughout the life of the project.

While some flexibility in data collection methods is warranted, attention to these data management

principles will prevent future problems caused by incompatible or incomplete data items, and will

facilitate exchanges of data between parties. This data management plan serves as the foundation for

agreement between parties on key data management issues.

2.1 DATABASE PLATFORM Because the tools needed to process information must have a common source data format, the Microsoft

Access 2000 base format will be used by BMcD to store and process data for delivery to DEQ. If a

specific data delivery format is different than Microsoft Access 2000, required by DEQ, that format will

be communicated to BMcD, and the database will be queried to organize the data in that fashion for the

purpose of making the electronic data delivery.

The database will contain Environmental Systems Research Institute, Inc. (ESRI) Personal Geodatabase

feature classes, and therefore will contain tables to support its use with ArcGIS version 9.x. Any tables

added to the database will be incorporated by using ArcCatalog to either build or import the table

structure. In order to allow the use and editing of data in ArcView, only simple feature classes will be

used, and relationships will not be explicitly defined in ArcGIS.

2.2 NORMALIZATION Normalization refers to database design considerations that eliminate redundant data and create data

dependencies consistent with the use of the data. Designations for four normalization levels have been

agreed upon by the database community. Normalization guidelines are cumulative – that is, data in each

normal form fulfills the requirements of lower-numbered forms. In other words, for a database to be in

second normal form (2NF), it must first fulfill all the criteria of a first normal form (1NF) database and

also satisfy the 2NF conditions. The four normal forms are generally defined as described below:

• First normal form (1NF) sets the very basic rules for an organized database:

- Eliminate duplicative columns from the same table.

- Create separate tables for each group of related data and identify each row with a unique column

or set of columns (the primary key).

• Second normal form (2NF) further addresses the concept of removing duplicative data:

TFM-0000756

Page 7: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Database Standards Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_02.doc 2-2 06/10/2005

- Remove subsets of data that apply to multiple rows of a table and place them in separate tables.

- Create relationships between these new tables and their predecessors through the use of foreign

keys.

• Third normal form (3NF) goes one large step further:

- Remove columns that are not dependent upon the primary key.

• Fourth normal form (4NF) has one requirement:

- A relation is in 4NF if it has no multi-valued dependencies.

Normalization of a database allows more efficient data storage, in terms of database size, and also can

help to improve data querying and processing. There is typically a cost for normalization, in terms of the

effort required to populate and maintain the database. The return on that investment is realized through

improved data organization and the ability to implement complex querying tools.

The Tulsa Fuel and Manufacturing RI/FS database will contain some instances of multiple data

relationships – e.g. information about a given sample is related to the chemical data for that sample and

also to the spatial (geographic location) information. It would be redundant to store sample information

in the sample location table and also in the lab data table. It makes more sense to remove such

information to a separate table and create relationships to the two other database objects. For this reason,

the database design should strive to achieve second normal form, taking advantage of these relationships

to reduce data redundancy.

2.3 DATABASE OBJECT NAMING CONVENTIONS Since the database will necessarily interact with multiple applications having required names for certain

tables, some of the table and field names are predetermined by the requirements of these applications.

2.4 DATA TYPES Data types for attribute data fields will follow these guidelines:

• Numerical data used for calculations or ordered sorting will use a numerical datatype – either

long integer or floating point (double precision) decimal data types are preferred.

• Date and time data will use a date/time data type.

• Text or character data fields will not exceed 255 characters.

TFM-0000757

Page 8: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Database Standards Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_02.doc 2-3 06/10/2005

• True/False or Yes/No data fields will use a Boolean data type – text fields should not be used to

store Boolean information.

• Spatial data will be stored as ArcGIS spatial objects. In addition to the binary data field that

holds the feature geometry, this requires an ObjectID field that is managed by ArcGIS alone, and

is created when the feature class is originally built in ArcCatalog.

* * * * *

TFM-0000758

Page 9: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Tabular Data Management Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_03.doc 3-1 06/10/2005

3.0 TABULAR DATA MANAGEMENT

Two major categories of tabular (attribute) data will be delivered under this contract; chemical data for

samples, and data collected during subsurface exploration, such as lithology and instrument readings may

be added. Spatial data, such as sample and borehole locations, will be discussed in the next section.

3.1 CHEMICAL DATA Analytical results for samples will be divided into two categories – analyses performed by a third-party

laboratory, and analyses performed in the field. Results for samples analyzed by a laboratory will be

delivered in electronic and hard-copy formats. After the hard copy has been validated by BMcD, the

corresponding electronic data will be added to the database using a custom import mechanism based on

structured query language (SQL) statements. Results for samples analyzed in the field will be delivered

to BMcD by the field crew in hard copy format and added to the database by hand. Data entry forms exist

for field analyses, and they will be used by the data entry personnel as applicable. The data entry

operations may also involve some stepwise processes such as using Microsoft Excel to collect and

organize the data prior to adding to the database.

3.2 BOREHOLE DATA Lithologic data will be recorded by the field geologist on a standard drilling log. Results of instrument

readings such as photoionization detector (PID) readings will be recorded on the drilling log. These data

items may be added to the database in tabular form if necessary to produce finished products such as

maps or tables.

* * * * *

TFM-0000759

Page 10: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Spatial Data Management Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_04.doc 4-1 06/10/2005

4.0 SPATIAL DATA MANAGEMENT

Spatial data will be used to produce report figures and other map exhibits, and may also be used for

calculations based on areas, distances, and other spatial analyses. Coordinate information for borehole

locations will be the primary data that is collected during this project cycle, but other data may be

collected or created for the purpose of providing base map information.

4.1 SPATIAL DATA FORMAT All spatial data will be ultimately stored in the database as ESRI feature classes. For this reason, the

project database will be created using ArcCatalog, which adds certain tables to manage spatial

information. Borehole locations will be provided by a surveyor, or collected using a global positioning

system (GPS) unit. Coordinate data will be delivered and stored using unprojected (latitude/longitude)

coordinates with North American Datum 1983 as the horizontal reference, or using the following

projected coordinate system:

Albers Conical Equal Area

Standard Parallel 1: 29.5 degrees

Standard Parallel 2: 45.5 degrees

Longitude of Central Meridian: -96 degrees

Latitude of Origin: 23 degrees

False Easting: 0

False Northing: 0

Distance Units: Meters

Horizontal Datum: North American Datum 1983

Ellipsoid: GRS1980

All other site data will, as necessary, be projected or converted to one of these coordinate systems.

The ESRI Personal Geodatabase will contain only simple geometry and tabular data. No complex

polygons, relationship classes, or network geometries should be used in the project database, since they

are not editable using ArcView.

4.2 FEATURE DATASET ORGANIZATION AND NAMING CONVENTIONS The feature dataset and feature class names in Table 4-1 should be used where applicable. Feature dataset

names, shown as bold section headers in the table, should be used for feature classes that belong in that

TFM-0000760

Page 11: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Spatial Data Management Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_04.doc 4-2 06/10/2005

dataset. Discriminators and suffices may be used to uniquely identify feature classes with similar content,

and should be separated from the feature class name by an underscore character. Dates may also be used

to identify periodic or date-specific data. In such instances, the date format YYYYMMDD should be

used (e.g. gwcont_20040101 for groundwater contours based on elevations collected January 1, 2004). In

cases where the data covers a range of dates, the date formats YYYYMMM (e.g. “2004JAN”) or

YYYYQQ (e.g. “2004Q1”) are alternative means of representing the date.

Where feature classes are added to that database that do not have an explicit naming convention as

described below, deviations from this naming convention may occur. The primary intention is to utilize

meaningful names that effectively identify discrete information. Also, where features used by a specific

third-party application must be identified with a specific table name, it is acceptable to deviate from this

naming standard.

* * * * *

TFM-0000761

Page 12: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Source Data Handling Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_05.doc 5-1 06/10/2005

5.0 SOURCE DATA HANDLING

The data processing event most likely to incur errors in the database is conversion and appending of

source data to the database. By controlling the processing of source data, confidence in the accuracy of

the data and calculations derived from the database will accrue. This section addresses data provided in

electronic format and hard copy.

5.1 ADDING SOURCE DATA TO THE DATABASE The database will be appended by several means – some of which are performed using third-party

applications, and others that require more direct handling of the data. In general, automated means should

be used to add data whenever possible. For example, SQL statements should be used for data

manipulation instead of cut-and-paste type transactions. The following subsections address specific

anticipated data transactions.

5.1.1 Electronic Data

Data provided in electronic format may be received by electronic transmission (e.g. File Transfer Protocol

[FTP], e-mail), or delivered on compact disc or other optical or magnetic media. Automated data loading

mechanisms are preferred, at minimum the database administrator should execute SQL statements to

transfer data. Any SQL statements used should be saved in the database so that the data process history is

fully recorded.

The preferred means for delivery of laboratory results data is the Data Analysis, Validation, and

Evaluation System (DAVES) database format. DAVES is a Visual Basic application developed by

BMcD that uses a Microsoft Access database to store and report chemical data. The DAVES database

standard consists of four tables to be populated by the laboratory, the relationships between these four

tables, and a list of analytical parameter names that must be adhered to in reporting the results. A data

dictionary is included in this document as Appendix A.

Because it greatly reduces the labor-intensive data processing activities, BMcD offers assistance to

laboratories in preparing a DAVES-compliant data delivery. A package of information, and empty

database, and a data format verification tool are distributed to laboratories, and personal technical support

is available to help resolve problems. When necessary, data is sometimes delivered by a laboratory in a

format different from the DAVES standard. When this occurs, it is preferable the date be delivered as a

flat-file spreadsheet or American Standard Code for Information Interchange (ASCII) file. Submittals in

TFM-0000762

Page 13: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Source Data Handling Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_05.doc 5-2 06/10/2005

this format take more effort to load and validate. The most important consideration is that the content of

the data delivery is consistent and accurate.

5.1.2 Hard Copy Data

A certain amount of hard-copy data is anticipated, especially for drilling logs and other field observations.

Data from such sources should, when practical, be entered through a user interface that performs some

elementary verification of the data. Monitoring well drilling log data, for example, should be entered

using the gINT user interface, which will help enforce referential integrity rules and perform some

consistency checks. When data must be entered directly into database tables, more stringent quality

control procedures are indicated.

Some electronic forms for data entry for environmental projects are available for use. These forms allow

the proper entry of field-collected sample results, water level depths, data validation qualifiers, and other

typical hand-entered data. These forms are part of the master database, and will be used whenever

applicable.

5.2 ARCHIVING SOURCE DATA Electronic source data delivered on physical media will be archived by transferring the data to a specific

location on the BMcD file server and changing the attributes on the file to “Read Only” for all users. The

physical media will then be stored with all other project materials until completion of the project. After

completion, all project materials will be collected and sent to long-term storage for a period not less than

ten years. All project-related materials are property of DEQ, and may be transferred to them for storage

at any time prior to the ten year time frame.

Electronic source data delivered independently of any physical media (such as data delivered through

BMcD’s FTP system) will be stored on the file server in the same fashion. A physical media copy of the

data will not be created, except the copy created on backup servers by the standard file backup process at

BMcD.

Hard copy source data will be stored with all other project materials until completion of the project. If a

hard copy is to be used in the evaluation or processing of data, it will be requested from the project

manager, who will create a duplicate or photocopy of the original and return the original to file. After

completion of the project, all project materials will be collected and sent to long-term storage for a period

not less than ten years. All project-related materials are property of DEQ, and may be transferred to them

for storage at any time prior to the ten year time frame.

TFM-0000763

Page 14: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Source Data Handling Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_05.doc 5-3 06/10/2005

5.3 METADATA COLLECTION A database is of limited use without understanding the limitations inherent in the data itself due to its

source. Metadata is data that describes the content, quality and condition and other characteristics of

database data, and may include source, reliability, spatial reference, date, and point of contact

information. There are several ways to document metadata. One increasingly common way for file-

based data such as shapefiles or data tables is to include metadata as an Extensible Markup Language

(.xml) file that accompanies the dataset. In an ESRI Personal Geodatabase, tables are built into the

database format to house the metadata references and make them accessible to the user through

ArcCatalog or other ESRI applications. Since ArcCatalog is the primary tool being used to build the

database, using it for metadata creation is consistent with the overall approach.

The Federal Geographic Data Committee (FGDC) is widely considered the authority on metadata

standards, and has provided guidance to the Geographic Information System (GIS) community for several

years on issues related to metadata. Their guideline for “mandatory” metadata information, Content

Standard for Digital Geospatial Metadata (CSDGM) is often used as the standard for minimum content.

Because all spatial data shares certain fundamental properties, alternatives to the FGDC minimum content

would simply be additions to or deletions from this list based on the intended use of the metadata

information and the general characteristics of the data. The complete CSDGM is included in this

document as Appendix B.

* * * * *

TFM-0000764

Page 15: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Database Security Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_06.doc 6-1 06/10/2005

6.0 DATABASE SECURITY

The issue of security has several facets, each with different protection measures. Protection from

inappropriate or unauthorized use, protection from accidental corruption, and physical safeguards against

fire or natural disaster are the three main considerations for databases. This section addresses these issues

and the means by which risk can be mitigated.

6.1 SECURITY AGAINST UNAUTHORIZED USE Unauthorized use of data is one of the greatest challenges facing database administrators in the

information age. Chief among the concerns associated with unauthorized use, especially for government

databases, is the possibility of information being used to threaten national security. Typically, an official

classification of such data would serve to indicate specific handling procedures that mitigate such risk.

The data being collected for this project is not subject to any official classification, and can therefore be

assumed to carry little or no security risk. Since the data being collected will ultimately become public

record, there is little reason to be overly concerned with damages resulting from unauthorized use.

Protection against unauthorized use of proprietary business info is a similar concern, which can be

mitigated through proper access restrictions. BMcD implements network security to prevent access to its

automated information systems by unauthorized persons. This level of security is sufficient for storing

project information on internal file servers.

Certain data is available to clients and contractors through a separate FTP server, which does permit some

anonymous logins. Such information must be deliberately placed on the FTP server by a BMcD

employee or a partner client or contractor. To assure the greatest level of security for this project within

current BMcD operating procedures, a separate FTP access point should be established that requires a

named user login. This will serve as a repository for data deliveries and exchanges as appropriate. Only

project personnel will be provided access to this FTP site.

6.2 PROTECTION FROM ACCIDENTAL DATA CORRUPTION Most database corruptions are caused by unfamiliarity with the database and the tools used to create and

maintain it, and are not malicious or intentional. The best protection against this type of data loss is to

prevent access to the database. There are different levels of prevention available. The most basic is to

prevent access to the project files, which can be easily accomplished by a network administrator. Next,

access to the files can be designated as “Read Only” access for all personnel except those directly

involved in building and maintaining the database. Another level of protection can be attained by setting

TFM-0000765

Page 16: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Database Security Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_06.doc 6-2 06/10/2005

up security information in Microsoft Access to mark individual objects, or the entire database, such that

they cannot be altered by anybody except certain named personnel. This requires that each user be given

a login, and that each database object be assigned to an owner. As a last-chance provision in the security

plan, network backups will prevent the loss of a significant amount of data. BMcD currently performs

incremental backups, which copy to tape any file that has changed since the previous backup, every

working day at noon. Additionally, a backup of the server content is performed nightly on each server.

These tapes are kept for a month, and weekly backup sets are drawn from those to be retained for a year.

Securing individual database objects is cumbersome to work around, and often causes problems for third-

party applications attempting to access the data. Additionally, it is an administrative burden, and can

cause difficulty in sharing the database with other parties. Although these problems can be resolved,

there is always a cost associated with administration. Most unintentional corruption can be prevented

with education of the users and control of the process. For instance, using data entry forms vice manual

entry into tables presents opportunity to verify that the data being added meets formatting and referential

integrity requirements.

The best approach in this circumstance is to restrict network access to the database to all personnel, and to

designate certain users who will build and maintain the database. Those users will have the ability to

append, modify, and delete records from the database. Other users will be granted “Read Only” access to

the database. The BMcD project manager will determine which users need full access to the database.

This approach, in concert with the daily backups, will mitigate unintentional data loss.

6.3 PHYSICAL SAFEGUARDS The final consideration with respect to database security is the accidental loss of data due to damage to

the server equipment that prevents recovery of the information. Fire, flood, earthquake, tornado, and

other potential causes for natural disaster pose some threat to electronic information. In order to mitigate

that threat, BMcD has undertaken several preventative measures. Chief among these is the physical

separation of the server machines into controlled access areas, redundant cooling systems, fire protection,

and uninterruptible power supplies, and daily data backup operations. The network servers are kept in an

isolated room constructed from fire-resistant materials, and protected with a dry extinguisher system. The

power supply system is augmented with DC power converters and backup generators so that data can be

safely stored in the event of a power loss. This room is in the lowest floor of the building in order to

further protect the machines. In addition, backups are stored off-site so that if the servers themselves

were critically affected, the data recovery would be almost complete.

* * * * *

TFM-0000766

Page 17: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

TABLES

TFM-0000767

Page 18: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

K:\ENV\OKLAHOMA DEPARTMENT OF ENVIRONMENTAL QUALITY\Site\36478\Deliver\RI_FS Data Mgmt Plan\Final\Tables\Table4_1.doc Page 1 of 3

Table 4-1

Feature Dataset and Feature Class Naming Standard Remedial Investigation/Feasibility Study

Tulsa Fuel and Manufacturing - Collinsville, Oklahoma Feature Dataset Name Feature Description Feature Class Name Discriminators Suffices Boundaries

24K, 100K Boundaries bound 24, 100 Census Blocks, Groups, Tracts census grp, blk, trct City Boundaries city County Boundaries cnty ok, <county name> Legislative Districts legdis hos, sen, cong ok, us Native American Resevations natamer Parcels parcel Parks park city, state Public Land Survey System plss 24, 100 State Boundries state mo, ks, us School Districts school Townships twp Voting Districts vote Watershed Districts wtrshd Zip codes zip

Elevation

Digital Elevation Models dem 24K, 100K Groundwater Contours gwcont (geologic unit abbr.) 20040101 (date) Hypsography (Contours) topo indx, intr Isoconcentration Countours isocont (analyte name) 20040101 (date)

Environmental

Wells well piez, bor, mw, temp Contour cont gw,pce,tce,dce,ctet,be

ddate of sampling,interval

Survey Locations surdata series,location date of survey Roads rds access Buildings bldgs current,former River river Sewerline sewline current,former Boundary bound site,property,reservatio owner Tributaries trib id Landfills landfill cap,bed,was (type) beg, six, fin (stage) / (date) Ditch ditch Utilities util storm, sewer, gas,

bl

Airstrip airstrip use ( ilit i l)

TFM-0000768

Page 19: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

K:\ENV\OKLAHOMA DEPARTMENT OF ENVIRONMENTAL QUALITY\Site\36478\Deliver\RI_FS Data Mgmt Plan\Final\Tables\Table4_1.doc Page 2 of 3

Table 4-1 Feature Dataset and Feature Class Naming Standard

Remedial Investigation/Feasibility Study Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

Feature Dataset Name Feature Description Feature Class Name Discriminators Suffices Corral corral Fence fence Railroads rr ownership Landfills landfill cap,bed,was (type) beg, six, fin (stage) / (date) NPDES npdes

Threatened and Endangered Species te plant, animal sensitivity

Lithology

Cross Section Line Map xsmap date Cross Sections xsect geol, anal (type) date Geology geol surface unit name Soil (SSURGO / STATSGO) soil ssurgo, statsgo

Stormwater Cross Sections xsect Flow Paths flpaths Overbanks banks Channel Centerline raschnl Bridge Decks brgdecks Mannings n values mannings

**Prefix** If used the prefix shold correspond to the identification codes setup for the projects sub-watersheds (Wears Creek cross sections would be wc_xsect)

Culverts culvert Surface Tins _tin wears_, clear_ Surface Grids _g wears_, clear_ Filled Grid _fill wears_, clear_ Flow Acumulation Grid _acc wears_, clear_ Flow Direction Grid _dir wears_, clear_ Watershed Boundaries sheds FEMA Flood Plain fema

Floodplain fp_ exst(existing) ult(ultimate) 100,500,<shed id>

Utilities

Corridor corr 20 (width) v37, z15 (version #) Right-of-Ways row 20 (width) Route rt 0101 (month-day) v37, z15 (version #) Substations sub wps, bmc (source) Transmission Lines tran wps, bmc (source) Utilities util storm, sewer, gas,

bl

TFM-0000769

Page 20: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

K:\ENV\OKLAHOMA DEPARTMENT OF ENVIRONMENTAL QUALITY\Site\36478\Deliver\RI_FS Data Mgmt Plan\Final\Tables\Table4_1.doc Page 3 of 3

Table 4-1 Feature Dataset and Feature Class Naming Standard

Remedial Investigation/Feasibility Study Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

Feature Dataset Name Feature Description Feature Class Name Discriminators Suffices Water Lakes hydro_ lakes General watersheds hy_unit ok, state Rivers / Streams hydro major, minor Wetlands wetland nwi, dnr, state

TFM-0000770

Page 21: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

APPENDIX A

DAVES Data Dictionary

TFM-0000771

Page 22: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-1 06/10/2005

DAVES MASTER PARAMETER LIST

The following parameter names are approved for use with the DAVES application. Although adherence to the DAVES standard is not explicitly required for completion of this contract, this list will form the basis for consistent parameter naming in the database.

ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER BTEX 1,2-Dichloroethane FMET Bismuth, Dissolved 7440-69-9BTEX Benzene FMET Boron, Dissolved 7440-42-8 BTEX BTEX (total) FMET Cadmium, Dissolved 7440-43-9 BTEX Ethyl Benzene FMET Calcium, Dissolved 7440-70-2 BTEX Toluene FMET Cesium, Dissolved 7440-46-2 BTEX Xylene FMET Chromium, Dissolved 7440-47-3 BTEX Xylenes (total) 1330-20-7 FMET Chromium, Hexavalent

DIOXINS 1,2,3,4,6,7,8,9-OCDD 3268-87-9 FMET Cobalt, Dissolved 7440-48-4 DIOXINS 1,2,3,4,6,7,8,9-OCDF 39001-02-0 FMET Copper, Dissolved 7440-50-8 DIOXINS 1,2,3,4,6,7,8-HpCDD 35822-46-9 FMET Gold, Dissolved 7440-57-5 DIOXINS 1,2,3,4,6,7,8-HpCDF 67562-39-4 FMET Iridium, Dissolved 7439-88-5 DIOXINS 1,2,3,4,7,8,9-HpCDF 55673-89-7 FMET Iron, Dissolved 7439-89-6 DIOXINS 1,2,3,4,7,8-HxCDD 39227-28-6 FMET Lead, Dissolved 7439-92-1 DIOXINS 1,2,3,4,7,8-HxCDF 70648-26-9 FMET Lithium, Dissolved 7439-93-2 DIOXINS 1,2,3,6,7,8-HxCDD 57653-85-7 FMET Magnesium, Dissolved 7439-95-4 DIOXINS 1,2,3,6,7,8-HxCDF 57117-44-9 FMET Manganese, Dissolved 7439-96-5 DIOXINS 1,2,3,7,8,9-HxCDD 19408-74-3 FMET Mercury, Dissolved 7439-97-6 DIOXINS 1,2,3,7,8,9-HxCDF 72918-21-9 FMET Molybdenum, Dissolved 7439-98-7 DIOXINS 1,2,3,7,8-PeCDD 40321-76-4 FMET Nickel, Dissolved 7440-02-0 DIOXINS 1,2,3,7,8-PeCDF 57117-41-6 FMET Osmium, Dissolved 7440-04-2 DIOXINS 2,3,4,6,7,8-HxCDF 60851-34-5 FMET Palladium, Dissolved 7440-05-3 DIOXINS 2,3,4,7,8-PeCDF 57117-31-4 FMET Phosphorus, Dissolved 7723-14-0 DIOXINS 2,3,7,8-TCDD 17460-01-6 FMET Platinum, Dissolved 7440-06-4 DIOXINS 2,3,7,8-TCDF 51207-31-9 FMET Potassium, Dissolved 7440-09-7 DIOXINS Total HpCDD 37871-00-4 FMET Rhenium, Dissolved 7440-15-5 DIOXINS Total HpCDF 38998-75-3 FMET Rhodium, Dissolved 7440-16-6 DIOXINS Total HxCDD 34465-46-8 FMET Ruthenium, Dissolved DIOXINS Total HxCDF 55684-94-1 FMET Selenium, Dissolved 7782-49-2 DIOXINS Total PeCDD 36088-22-9 FMET Silver, Dissolved 7440-22-4 DIOXINS Total PeCDF 30402-15-4 FMET Sodium, Dissolved 7440-23-5 DIOXINS Total TCDD 41903-57-5 FMET Strontium, Dissolved 7440-24-6 DIOXINS Total TCDF 55722-27-5 FMET Thallium, Dissolved 7440-28-0 EXPLO 1,3,5-Trinitrobenzene FMET Thorium, Dissolved 7440-29-1 EXPLO 1,3-Dinitrobenzene FMET Tin, Dissolved 7440-31-5 EXPLO 2,4,6-Trinitrotoluene FMET Titanium, Dissolved 7440-32-6 EXPLO 2,4-Dinitrotoluene FMET Vanadium, Dissolved 7440-62-2 EXPLO 2,6-Dinitrotoluene FMET Zinc, Dissolved 7440-66-6 EXPLO 2-Am-Dinitrotoluene FPCB PCB-1016 12674-11-2EXPLO 2-Nitrotoluene FPCB PCB-1221 11104-28-2EXPLO 3-Nitrotoluene FPCB PCB-1232 11141-16-5EXPLO 4-Am-Dinitrotoluene FPCB PCB-1242 53469-21-9EXPLO 4-Nitrotoluene FPCB PCB-1248 12672-29-6EXPLO Guanidine nitrate FPCB PCB-1254 11097-69-1EXPLO HMX FPCB PCB-1260 11096-82-5EXPLO Nitrobenzene HAZWASTE Corrosivity (pH) EXPLO Nitrocellulose HAZWASTE Corrosivity Toward Steel EXPLO Nitroglycerin HAZWASTE Ignitability EXPLO Nitroguanidine HAZWASTE Oil and Grease EXPLO RDX HAZWASTE Paint Filter Test

TFM-0000772

Page 23: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-2 06/10/2005

ANALYSIS TYPE

PARAMETER NAME CAS NUMBER

ANALYSIS TYPE

PARAMETER NAME CAS NUMBER

EXPLO s-Triazine, Hexahydro-1,3,5-Trinitro HAZWASTE Reactive Cyanide EXPLO Tetryl HAZWASTE Reactive Sulfide FMET Aluminum, Dissolved 7429-90-5 HAZWASTE Reactivity FMET Antimony, Dissolved 7440-36-0 HERB 2,4,5-T 93-76-5 FMET Arsenic, Dissolved 7440-38-2 HERB 2,4,5-TP (Silvex) 93-72-1 FMET Barium, Dissolved 7440-39-3 HERB 2,4-D 94-75-7 FMET Beryllium, Dissolved 7440-41-7 HERB 2,4-DB 107-92-6 HERB Atrazine 1912-24-9 METAL Chromium, Hexavalent HERB Dalapon 75-99-0 METAL Chromium, Total 7440-47-3 HERB Dicamba 1918-00-9 METAL Cobalt, Total 7440-48-4 HERB Dichlorprop 120-36-5 METAL Copper, Total 7440-50-8 HERB Dinoseb 88-85-7 METAL Cyanide, Total HERB MCPA 94-74-6 METAL Gold, Total 7440-57-5 HERB MCPP 7085-19-0 METAL Iridium, Total 7439-88-5

HERBSURR 2,4-Dichlorophenylacetic acid METAL Iron, Total 7439-89-6 INORG Amenable Cyanide METAL Lead, Total 7439-92-1 INORG Ammonia 7664-41-7 METAL Lithium, Total 7439-93-2 INORG Boron 7440-42-8 METAL Magnesium, Total 7439-95-4 INORG Bromide METAL Manganese, Total 7439-96-5 INORG Carbon Dioxide 124-38-9 METAL Mercury, Total 7439-97-6 INORG Cation Exchange Capacity METAL Molybdenum, Total 7439-98-7 INORG Chloride METAL Nickel, Total 7440-02-0 INORG Chlorine METAL Osmium, Total 7440-04-2 INORG Chlorine Dioxide METAL Palladium, Total 7440-05-3 INORG Chlorine, Total Residual METAL Phosphorus, Total 7723-14-0 INORG Chromium, Trivalent METAL Platinum, Total 7440-06-4 INORG Cyanide, Amenable METAL Potassium, Total 7440-09-7 INORG Cyanide, Total METAL Rhenium, Total 7440-15-5 INORG Fluoride METAL Rhodium, Total 7440-16-6 INORG Iodide METAL Ruthenium, Total INORG Iodine 7553-56-2 METAL Selenium, Total 7782-49-2 INORG Moisture (Oven) METAL Silica (SiO2), Total INORG Nitrate METAL Silver, Total 7440-22-4 INORG Nitrate-Nitrite METAL Sodium, Total 7440-23-5 INORG Nitrate/Nitrite as N METAL Strontium, Total 7440-24-6 INORG Nitrite METAL Thallium, Total 7440-28-0 INORG Nitrogen, Ammonia METAL Thorium, Total 7440-29-1 INORG Nitrogen, Total Kjeldahl METAL Tin, Total 7440-31-5 INORG Oil and Grease METAL Titanium, Total 7440-32-6 INORG Orthophosphate METAL Vanadium, Total 7440-62-2 INORG Oxygen, Dissolved 7782-44-7 METAL Zinc, Total 7440-66-6 INORG Phosphorus, Total 7723-14-0 MISC Organic Lead INORG Radium 228 7440-14-4 MISC Radium 228, LLD INORG Radium 228, LLD MISC Radium 228, total INORG Radium 228, total MISC Radium 228, total, error, +/- INORG Radium 228, total, error, +/- MISC Static Water Level INORG Silica MISC TCLP Cyanide INORG Silica, Dissolved MISC Well Depth INORG Sulfate PAH 1-Methylnaphthalene 90-12-0 INORG Sulfide PAH 1-Methylphenanthrene 832-69-9 INORG Sulfite PAH 2,3,5-Trimethylnaphthalene 2245-38-7 INORG Total Organic Carbon PAH 2,6-Dimethylnaphthalene 581-42-0 INORG Total Solids PAH 2-Methylnaphthalene 91-57-6 METAL Aluminum, Total 7429-90-5 PAH Acenaphthene 83-32-9 METAL Antimony, Total 7440-36-0 PAH Acenaphthylene 208-96-8

TFM-0000773

Page 24: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-3 06/10/2005

ANALYSIS TYPE

PARAMETER NAME CAS NUMBER

ANALYSIS TYPE

PARAMETER NAME CAS NUMBER

METAL Arsenic, Total 7440-38-2 PAH Anthracene 120-12-7METAL Barium, Total 7440-39-3 PAH Benzo(a)anthracene 56-55-3 METAL Beryllium, Total 7440-41-7 PAH Benzo(a)pyrene 50-32-8 METAL Bismuth, Total 7440-69-9 PAH Benzo(b)fluoranthene 205-99-2 METAL Boron, Total 7440-42-8 PAH Benzo(e)pyrene 192-97-2 METAL Cadmium, Total 7440-43-9 PAH Benzo(g,h,i)perylene 191-24-2 METAL Calcium, Total 7440-70-2 PAH Benzo(k)fluoranthene 207-08-9 METAL Cesium, Total 7440-46-2 PAH Biphenyl 92-52-4

PAH Carcinogenic PAHs PEST cis-Permethrin 52645-53-1PAH Chrysene 218-01-9 PEST Coumaphos 56-72-4 PAH Dibenz(a,h)anthracene 53-70-3 PEST Cycloate PAH Dibenzothiophene 132-65-0 PEST DCPA 1861-32-1 PAH Fluoranthene 206-44-0 PEST delta-BHC 319-86-8 PAH Fluorene 86-73-7 PEST Demeton, -O and -S 8065-48-3 PAH Indeno(1,2,3-cd)pyrene 193-39-5 PEST Demeton-O PAH Naphthalene 91-20-3 PEST Demeton-S PAH Perylene 198-55-0 PEST Diazinon 333-41-5 PAH Phenanthrene 85-01-8 PEST Dichlorvos 62-73-7 PAH Pyrene 129-00-0 PEST Dieldrin 60-57-1 PAH Total PAHs PEST Dimethoate 60-51-5 PCB Aroclor-1016 12674-11-2 PEST Diphenamid 957-51-7 PCB Aroclor-1221 11104-28-2 PEST Disulfoton 298-04-4 PCB Aroclor-1232 11141-16-5 PEST Disulfoton sulfone PCB Aroclor-1242 53469-21-9 PEST Disulfoton sulfoxide PCB Aroclor-1248 12672-29-6 PEST Endosulfan I 959-98-8 PCB Aroclor-1254 11097-69-1 PEST Endosulfan II 33213-65-9PCB Aroclor-1260 11096-82-5 PEST Endosulfan sulfate 1031-07-8 PCB Total PCBs PEST Endrin 72-20-8

PEST 4,4'-DDD 72-54-8 PEST Endrin aldehyde 7421-36-3 PEST 4,4'-DDD/Endo II 72-54-8 PEST Endrin ketone 53494-70-5PEST 4,4'-DDE 72-55-9 PEST EPN 2104-64-5 PEST 4,4'-DDT 50-29-3 PEST EPTC 759-94-4 PEST Alachlor 15972-60-8 PEST Ethoprop 13194-48-4PEST Aldrin 309-00-2 PEST Ethylene dibromide PEST alpha-BHC 319-84-6 PEST Etridiazole PEST alpha-Chlordane 5103-71-9 PEST ETU PEST Ametryn 834-12-8 PEST Fenamiphos 22224-92-6PEST Aroclor-1016 12674-11-2 PEST Fenarimol 60168-88-9PEST Aroclor-1221 11104-28-2 PEST Fensulfonthion 115-90-2 PEST Aroclor-1232 11141-16-5 PEST Fensulfothion PEST Aroclor-1242 53469-21-9 PEST Fenthion 55-38-9 PEST Aroclor-1248 12672-29-6 PEST Fluridone PEST Aroclor-1254 11097-69-1 PEST gamma-BHC (Lindane) 58-89-9 PEST Aroclor-1260 11096-82-5 PEST gamma-Chlordane 5103-74-2 PEST Atraton PEST Heptachlor 76-44-8 PEST Atrazine 1912-24-9 PEST Heptachlor Epoxide 1024-57-3 PEST Azinphos-methyl 86-50-0 PEST Hexachlorobenzene 118-74-1 PEST beta-BHC 319-85-7 PEST Hexachlorocyclopentadiene 77-47-4 PEST Bolstar (Sulprofos) 35400-43-2 PEST Hexazinone 51235-04-2PEST Bromacil 314-40-9 PEST Malathion 121-75-5 PEST Butachlor 23184-66-9 PEST Merphos PEST Butylate 2008-41-5 PEST Methoxychlor 72-43-5 PEST Carbaryl (Sevin) PEST Methyl paraoxon PEST Carboxin 5234-68-4 PEST Metolachlor 51218-45-2PEST Chlordane 57-74-9 PEST Metribuzin 21087-64-9

TFM-0000774

Page 25: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-4 06/10/2005

ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER PEST Chlordane (technical) 57-74-9 PEST Mevinphos 7786-34-7PEST Chlordane-alpha 5103-71-9 PEST MGK 264 PEST Chlordane-gamma 5103-74-2 PEST Molinate PEST Chlorneb PEST Monocrotophos 6923-22-4 PEST Chlorobenzilate(a) 510-15-6 PEST Naled 300-76-5 PEST Chloropropham 101-21-3 PEST Napropamide 15299-99-7PEST Chlorothalonil 1897-45-6 PEST Norflurazon 27314-13-2PEST Chlorpyrifos 2921-88-2 PEST Parathion, ethyl PEST cis-Nonachlor PEST Parathion, methyl 298-00-0 PEST Pebulate 1114-71-2 SVOC 1,4-Phenylenediamine PEST Phorate 298-02-2 SVOC 1-Acetyl-2-thiourea PEST Prometon 1610-18-0 SVOC 1-Chloronaphthalene PEST Prometryn 7287-19-6 SVOC 1-Naphthylamine PEST Pronamid 23950-58-5 SVOC 2,2',3',4,6-Pentachlorobiphenyl PEST Propachlor 1918-16-7 SVOC 2,2',3,3',4,4',6- PEST Propazine 139-40-2 SVOC 2,2',3,3',4,5',6,6'-

O

PEST Ronnel 299-84-3 SVOC 2,2',4,4',5,6'-Hexachlorobiphenyl PEST Simazine 122-34-9 SVOC 2,2',4,4'-Tetrachlorobiphenyl PEST Simetryne 1014-70-6 SVOC 2,2'-OXYBIS(1-

C O O O )

PEST Stirofos 22248-79-9 SVOC 2,3,4,6-Tetrachlorophenol 58-90-2 PEST Stirofos (Tetrachloroviniphos) 22248-79-9 SVOC 2,3-Dichlorobiphenyl PEST Sulfotep 3689-24-5 SVOC 2,4,5-Trichlorobiphenol PEST Tebuthiuron 34014-18-1 SVOC 2,4,5-Trichlorophenol 95-95-4 PEST TEPP 107-49-3 SVOC 2,4,5-Trimethylaniline PEST Terbacil 5902-51-2 SVOC 2,4,6-Trichlorophenol 88-06-2 PEST Terbufos 13071-79-9 SVOC 2,4-Diaminotoluene PEST Terbutryn SVOC 2,4-Dichlorophenol 120-83-2 PEST Tetrachlorvinphos (Stirophos) SVOC 2,4-Dimethylphenol 105-67-9 PEST Tokuthion (Protothiofos) SVOC 2,4-Dinitrobenzene PEST Toxaphene 8001-35-2 SVOC 2,4-Dinitrophenol 51-28-5 PEST trans-Nonachlor SVOC 2,4-Dinitrotoluene 121-14-2 PEST trans-Permethrin 52645-53-1 SVOC 2,6-Dichlorophenol PEST Triademefon SVOC 2,6-Dinitrotoluene 606-20-2 PEST Trichloronate SVOC 2-Acetylaminofluorene PEST Tricycloazole SVOC 2-Aminoanthraquinone PEST Trifluralin 1582-09-8 SVOC 2-Chlorobiphenyl PEST Vernolate 1929-77-7 SVOC 2-Chloronaphthalene 91-58-7

PESTSURR Abate SVOC 2-Chlorophenol 95-57-8 PESTSURR Decachlorobiphenyl SVOC 2-Cyclohexyl-4,6-dinitrophenol PESTSURR Ethion SVOC 2-Methyl-1-propanol PESTSURR Tetrachloro-m-xylene SVOC 2-Methyl-4,6-dinitrophenol

PHYS CEC SVOC 2-Methylnaphthalene 91-57-6 PHYS Clay/Colloids (< 0.005 mm) SVOC 2-Methylphenol 95-48-7 PHYS Gravel & Coarse Sand (> 2.00 mm) SVOC 2-Naphthylamine PHYS Liquid Limit SVOC 2-Nitroaniline 88-74-4 PHYS Medium & Fine Sand (0.075 to 2.00

) SVOC 2-Nitrophenol 88-75-5

PHYS Moisture SVOC 2-Picoline 109-06-8 PHYS Percent Retained on #40 Sieve SVOC 3,3'-Dichlorobenzene 106-46-7 PHYS pH SVOC 3,3'-Dichlorobenzidine 91-94-1 PHYS Plastic Limit SVOC 3,3'-Dimethoxybenzidine PHYS Plasticity Index SVOC 3,3'-Dimethylbenzidine PHYS Silt (0.005 to 0.075 mm) SVOC 3,3-Dimethylbenzidine

TFM-0000775

Page 26: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-5 06/10/2005

ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER PHYS Total Solids SVOC 3-(Chloromethyl)pyridine SVOC 0,0,0-Triethyl Phosphorothioate 126-68-1 SVOC 3-Methylcholanthrene 56-49-5 SVOC 1,2,4,5-Tetrachlorobenzene 95-94-3 SVOC 3-Methylphenol SVOC 1,2,4-Trichlorobenzene 120-82-1 SVOC 3-Nitroaniline 99-09-2 SVOC 1,2-Dichlorobenzene 95-50-1 SVOC 4,4'-DDD 72-54-8 SVOC 1,2-Dinitrobenzene SVOC 4,4'-DDE 72-55-9 SVOC 1,2-Diphenylhydrazine SVOC 4,4'-DDT 50-29-3 SVOC 1,3,5-Trinitrobenzene 99-35-4 SVOC 4,4'-Methylenebis(2-chloraniline) 101-14-4 SVOC 1,3-Dichlorobenzene 541-73-1 SVOC 4,4'-Oxydianiline SVOC 1,3-Dinitrobenzene SVOC 4,6-Dinitro-2-methylphenol 534-52-1 SVOC 1,4-Dichlorobenzene 106-46-7 SVOC 4-Aminobiphenyl SVOC 1,4-Dinitrobenzene SVOC 4-Bromophenyl-phenyl ether 101-55-3 SVOC 1,4-Naphthoquinone SVOC 4-Chloro-3-methylphenol 59-50-7 SVOC 4-Chloroaniline 106-46-8 SVOC Carbaryl 63-25-2 SVOC 4-Chlorophenyl-phenyl ether 7005-72-3 SVOC Carbazole 86-74-8 SVOC 4-Methylphenol 106-44-5 SVOC Carbofuran 1563-66-2 SVOC 4-Nitroaniline 100-01-6 SVOC Carbophenonthion 786-19-6 SVOC 4-Nitrobiphenyl SVOC Chlordane 57-74-9 SVOC 4-Nitrophenol 100-02-7 SVOC Chlordane (trans-Nonachlor) SVOC 5,5-Diphenylhydantoin SVOC Chlordane-alpha 5103-71-9 SVOC 5-Chloro-2-methylaniline SVOC Chlordane-gamma 5103-74-2 SVOC 5-Nitro-o-anisidine SVOC Chlorfenvinphos 470-90-6 SVOC 5-Nitro-o-toluidine SVOC Chlorobenzilate 510-15-6 SVOC 5-Nitroacenaphthene SVOC Chlorofenvinphos SVOC 7,12-Dimethylbenz(a)anthracene SVOC Chrysene 218-01-9 SVOC 7,12-Dimethylbenzo(a)anthracene SVOC Coumaphos 56-72-4 SVOC Acenaphthene 83-32-9 SVOC Crotoxyphos 7700-17-6 SVOC Acenaphthylene 208-96-8 SVOC delta-BHC 319-86-8 SVOC Acetophenone 98-86-2 SVOC Demeton-O SVOC Alachlor 15972-60-8 SVOC Demeton-S SVOC Aldrin 309-00-2 SVOC Di(2-ethylhexyl)adipate SVOC alpha,alpha-Dimethylphenethylamine SVOC Di(2-ethylhexyl)phthalate SVOC alpha,alpha-Dimethyophenethylamine SVOC Di-n-butyl phthalate SVOC alpha-BHC 319-84-6 SVOC Di-n-butylphthalate 84-74-2 SVOC Aminoazobenzene 60-09-3 SVOC Di-n-octyl phthalate 117-84-0 SVOC Anilazine 101-05-3 SVOC Di-n-octylphthalate SVOC Aniline 62-53-3 SVOC Diallate (cis or trans) 2303-16-4 SVOC Anthracene 120-12-7 SVOC Dibenz(a,h)acridine SVOC Aramite 140-57-8 SVOC Dibenzo(a,e)pyrene SVOC Aroclor-1016 12674-11-2 SVOC Dibenzo(a,h)anthracene 53-70-3 SVOC Aroclor-1221 11104-28-2 SVOC Dibenzo(a,j)acridine SVOC Aroclor-1232 11141-16-5 SVOC Dibenzofuran 132-64-9 SVOC Aroclor-1242 53469-21-9 SVOC Dichlone 117-80-6 SVOC Aroclor-1248 12672-29-6 SVOC Dichlorobenzenes SVOC Aroclor-1254 11097-69-1 SVOC Dichlorovos SVOC Aroclor-1260 11096-82-5 SVOC Dicrotophos 141-66-2 SVOC Atrazine 1912-24-9 SVOC Dieldrin 60-57-1 SVOC Azinphos-methyl 86-50-0 SVOC Diethyl phthalate 84-66-2 SVOC Barban 101-27-9 SVOC Diethyl sulfate 64-67-5 SVOC Benzidine 92-87-5 SVOC Diethylstilbestrol 56-53-1 SVOC Benzo(a)anthracene 56-55-3 SVOC Diethylstillbestrol 56-53-1 SVOC Benzo(a)perylene SVOC Dimethoate 60-51-5 SVOC Benzo(a)pyrene 50-32-8 SVOC Dimethyl phthalate 131-11-3 SVOC Benzo(b)and/or(k)fluoranthene SVOC Dimethylphthalate 131-11-3

TFM-0000776

Page 27: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-6 06/10/2005

ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER SVOC Benzo(b)fluoranthene 205-99-2 SVOC Dinocap 39300-45-3SVOC Benzo(g,h,i)perylene 191-24-2 SVOC Dinoseb 88-85-7 SVOC Benzo(k)fluoranthene 207-08-9 SVOC Diphenylamine 122-39-4 SVOC Benzoic Acid 65-85-0 SVOC Disulfoton 298-04-4 SVOC Benzyl alcohol 100-51-6 SVOC Endosulfan I 959-98-8 SVOC Benzyl butyl phthalate SVOC Endosulfan II 33213-65-9SVOC beta-BHC 319-85-7 SVOC Endosulfan sulfate 1031-07-8 SVOC Bis(2-chloroethoxy)methane 111-91-1 SVOC Endrin 72-20-8 SVOC Bis(2-chloroethyl)ether 111-44-4 SVOC Endrin aldehyde 7421-36-3 SVOC Bis(2-Chloroisopropyl)ether 108-60-1 SVOC Endrin ketone 53494-70-5SVOC Bis(2-ethylhexyl)phthalate 117-81-7 SVOC EPN 2104-64-5 SVOC Bromoxynil 1689-84-5 SVOC Ethion 563-12-2 SVOC Butylbenzylphthalate 85-68-7 SVOC Ethyl carbamate SVOC Captafol 2425-06-1 SVOC Ethyl methanesulfonate 62-50-0 SVOC Captan 133-06-2 SVOC Famphur 52-85-7 SVOC Fensulfothion 115-90-2 SVOC p-Benzoquinone SVOC Fenthion 55-38-9 SVOC p-Cresidine SVOC Fluchloralin 33245-39-5 SVOC p-Dimethylaminoazobenzene 60-11-7 SVOC Fluoranthene 206-44-0 SVOC Parathion 56-38-2 SVOC Fluorene 86-73-7 SVOC Pentachlorobenzene 608-93-5 SVOC gamma-BHC (Lindane) 58-89-9 SVOC Pentachloronitrobenzene 82-68-8 SVOC Heptachlor 76-44-8 SVOC Pentachlorophenol 87-86-5 SVOC Heptachlor epoxide 1024-57-3 SVOC Phenacetin SVOC Hexachlorobenzene 118-74-1 SVOC Phenancetin 62-44-2 SVOC Hexachlorobutadiene 87-68-3 SVOC Phenanthrene 85-01-8 SVOC Hexachlorocyclopentadiene 77-47-4 SVOC Phenobarbital 50-06-6 SVOC Hexachloroethane 67-72-1 SVOC Phenol 108-95-2 SVOC Hexachlorophene 70-30-4 SVOC Phorate 298-02-2 SVOC Hexachloropropene SVOC Phosalone 2310-17-0 SVOC Hexamethylphosphoramide SVOC Phosmet 732-11-6 SVOC Hydroquinone 123-31-9 SVOC Phosphamidon 13171-21-6SVOC Indene SVOC Phthalic anhydride 85-44-9 SVOC Indeno(1,2,3-cd)pyrene 193-39-5 SVOC Piperonyl sulfoxide SVOC Isodrin SVOC Pronamide 23950-58-5SVOC Isophorone 78-59-1 SVOC Propylthiouracil SVOC Isosafrole 120-58-1 SVOC Pyrene 129-00-0 SVOC Kepone SVOC Pyridine 110-86-1 SVOC Leptophos 21609-90-5 SVOC Quinoline SVOC Malathion 121-75-5 SVOC Resorcinol 108-46-3 SVOC Maleic anhydride 108-31-6 SVOC Safrole 94-59-7 SVOC Mestranol 72-33-3 SVOC Simazine 122-34-9 SVOC Methapyrilene 91-80-5 SVOC Strychnine 57-24-9 SVOC Methoxychlor 72-43-5 SVOC Sulfallate SVOC Methyapyrilene SVOC Terbufos 13071-79-9SVOC Methyl methanensulfonate 66-27-3 SVOC Tetrachlorvinphos (Stirophos) SVOC Methyl parathion 298-00-0 SVOC Tetraethyl pyrophosphate 107-49-3 SVOC Methylchrysene SVOC Thionazine 297-97-2 SVOC Methylphenols SVOC Thiophenol (Benzenthiol) SVOC Mevinphos 7786-34-7 SVOC Toluene diisocyanate 584-84-9 SVOC Mexacarbate 315-18-4 SVOC Total Petroleum Hydrocarbon SVOC Mirex 2385-85-5 SVOC Toxaphene 8001-35-2 SVOC Monocrotophos 6923-22-4 SVOC Tri-p-tolyl phosphate SVOC N-Nitrophenol SVOC Trifluralin 1582-09-8 SVOC N-Nitroso-di-n-propylamine 621-64-7 SVOC Trimethyl phosphate

TFM-0000777

Page 28: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-7 06/10/2005

ANALYSIS TYPE

PARAMETER NAME CAS NUMBER

ANALYSIS TYPE

PARAMETER NAME CAS NUMBER

SVOC N-Nitrosodibutylamine 924-16-3 SVOC Tris(2,3- 126-72-7SVOC N-Nitrosodiethylamine 55-18-5 SVOCSURR 2,4,6-Tribromophenol SVOC N-Nitrosodimethylamine 62-75-9 SVOCSURR 2-Fluorobiphenyl SVOC N-Nitrosodiphenylamine 156-10-5 SVOCSURR 2-Fluorophenol SVOC N-Nitrosomethylethylamine SVOCSURR Nitrobenzene-d5 SVOC N-Nitrosomorpholine 59-89-2 SVOCSURR p-Terphenyl SVOC N-Nitrosopiperidine SVOCSURR Phenol-d5 SVOC N-Nitrosopyrrolidine 930-55-2 SVOCSURR Terphenyl-d14 SVOC Naled 300-76-5 SVOCTIC (3S,4R,5R,6R)-4,5-

(

SVOC Naphthalene 91-20-3 SVOCTIC (Z)14-Tricosenyl formate SVOC Nicotine 54-11-5 SVOCTIC 06.92 Undecane SVOC Nitrobenzene 98-95-3 SVOCTIC 08.22 Dodecane SVOC Nitrofen 1836-75-5 SVOCTIC 09.08 Unknown cyclic SVOC Nitroquinoline-1-oxide SVOCTIC 09.24 Unknown cyclic SVOC o-Anisidine SVOCTIC 09.45 Tridecane SVOC o-Toluidine SVOCTIC 09.53 Unknown cyclic SVOC Octamethyl pyrophosphoramide SVOCTIC 09.96 Unknown cyclic

SVOCTIC 1,1,2,2-Tetrachloroethane SVOCTIC 25.06 Unknown carbonyl SVOCTIC 1,1,2-Trichloroethane SVOCTIC 25.07 Unknown carbonyl SVOCTIC 1,16-Hexadecanediol SVOCTIC 25.19 Unknown alkane SVOCTIC 1,2-Benzenedicarboxylic acid, mono SVOCTIC 25.22 Unknown steroid SVOCTIC 1-Decene SVOCTIC 25.41 1H-Cycloprop[e]azulene, SVOCTIC 1-Dodecanol SVOCTIC 25.42 Unknown alkane SVOCTIC 1-Eicosanol SVOCTIC 25.43 Unknown alkane SVOCTIC 1-Heptadecanol SVOCTIC 25.46 Benzo[b]triphenylene SVOCTIC 1-Octadecanol SVOCTIC 25.50 .gamma.-Sitosterol SVOCTIC 1-Tridecanol SVOCTIC 25.51 .gamma.-Sitosterol SVOCTIC 10.18 Unknown cyclic hydrocarbon SVOCTIC 25.52 .gamma.-Sitosterol SVOCTIC 10.39 1-Decene SVOCTIC 25.58 Hexadecyloxirane SVOCTIC 10.60 Tetradecane SVOCTIC 25.71 Hexadecyloxirane SVOCTIC 11.69 Unknown cyclic hydrocarbon SVOCTIC 25.72 Heneicosane SVOCTIC 11.82 Unknown cyclic hydrocarbon SVOCTIC 25.73 Eicosane, 10-methyl- SVOCTIC 11.92 Unknown cyclic hydrocarbon SVOCTIC 25.81 Cyclohexane, 1,2,4,5- SVOCTIC 12.90 Unknown cyclic hydrocarbon SVOCTIC 25.92 2-Dodecen-1-yl(-

)

SVOCTIC 13.04 Unknown cyclic hydrocarbon SVOCTIC 25.92 Dicholesteryl succinate SVOCTIC 13.43 Unknown cyclic hydrocarbon SVOCTIC 25.92 Hexatriacontane SVOCTIC 14.92 Unknown cyclic hydrocarbon SVOCTIC 25.92 Trilostane SVOCTIC 15.69 4H-

C f SVOCTIC 25.95 Unknown hydrocarbon

SVOCTIC 16.33 Unknown hydrocarbon SVOCTIC 26.04 Hexatriacontane SVOCTIC 16.83 Unknown hydrocarbon SVOCTIC 26.20 Unknown steroid SVOCTIC 17-Pentatriacontene SVOCTIC 26.25 Ledol SVOCTIC 19.04 Unknown steroid SVOCTIC 26.34 Octadecane SVOCTIC 19.13 cis-7-Tetradecen-1-ol SVOCTIC 26.39 Unknown alkane SVOCTIC 19.16 Unknown steroid SVOCTIC 26.45 Unknown hydrocarbon SVOCTIC 19.22 Unknown steroid SVOCTIC 26.52 Unknown steroid SVOCTIC 1H-3a,7-Methanoazulene, octahydro- SVOCTIC 26.62 Stigmastenone SVOCTIC 1H-Cycloprop[e]azulene, 1a,2,3,4,4 SVOCTIC 26.64 Stigmast-4-en-3-one SVOCTIC 1H-Cycloprop[e]azulene, decahydro- SVOCTIC 26.65 14-Octadecenal

TFM-0000778

Page 29: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-8 06/10/2005

ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER SVOCTIC 2-Dodecen-1-yl(-)succinic anhydrid SVOCTIC 26.66 Pregn-4-ene-3,20-dione, SVOCTIC 21.07 Hexatriacontane SVOCTIC 26.71 Unknown alkane SVOCTIC 21.07 Hexatriacontane SVOCTIC 26.71 Unknown alkane SVOCTIC 21.94 Pentadecanal- SVOCTIC 26.75 Unknown steroid SVOCTIC 22.44 Heptadecane SVOCTIC 26.78 Ergost-5-en-3-ol,

( )

SVOCTIC 22.95 Benz[e]acephenanthrylene SVOCTIC 26.88 D-Friedoolean-14-ene, 3- SVOCTIC 23.15 Hexadecyloxirane SVOCTIC 26.88 Hexadecyloxirane SVOCTIC 23.19 Pentadecanal- SVOCTIC 26.99 Hexatriacontane SVOCTIC 23.28 Eicosane SVOCTIC 26.99 Nonadecane SVOCTIC 23.48 1-Docosene SVOCTIC 27.01 Hexadecylcloxirane SVOCTIC 23.67 Heneicosane SVOCTIC 27.17 Unknown steroid SVOCTIC 23.68 Tetracosane SVOCTIC 27.22 Hexatriacontane SVOCTIC 24.00 Unknown alkane SVOCTIC 27.38 .gamma.-Sitosterol SVOCTIC 24.10 Unknown alkane SVOCTIC 27.38 .gamma.-Sitosterol SVOCTIC 24.14 1-Hexacosanal SVOCTIC 27.39 .gamma.-Sitosterol SVOCTIC 24.32 Hexadecyloxirane SVOCTIC 27.44 1,2:3,4-Dibenzpyrene SVOCTIC 24.50 Eicosane SVOCTIC 27.58 [3,4:9,10]Dibenzpyrene SVOCTIC 24.50 Heneicosane SVOCTIC 27.68 Unknown steroid SVOCTIC 24.50 Nonadecane SVOCTIC 27.91 Cyclopropa[d]naphthalen-

( )

SVOCTIC 24.51 Unknown hydrocarbon SVOCTIC 27.91 Phenanthro[9,10-b]furan SVOCTIC 24.55 Cyclohexadecane SVOCTIC 27.95 Unknown steroid SVOCTIC 24.68 Hexatriacontane SVOCTIC 28.11 Unknown cyclic SVOCTIC 24.68 Hexatriacontane SVOCTIC 28.27 1H-Cycloprop[e]azulene, SVOCTIC 24.69 Hexatriacontane SVOCTIC 28.30 Coronene SVOCTIC 24.80 Hexatriacontane SVOCTIC 28.41 Stigmast-4-en-3-one SVOCTIC 3,5-Cyclohexadiene-1,2-dione, 3,4, SVOCTIC Dodecanol SVOCTIC 3-Hexadecene, (Z)- SVOCTIC Dotriacontane SVOCTIC 4H-Cyclopenta[def]phenanthrene SVOCTIC Eicosane SVOCTIC 5(1H)-Azulenone, 2,4,6,7,8,8a-hexa SVOCTIC Eicosane SVOCTIC 6-Octadecenoic acid, methyl ester, SVOCTIC Eicosene SVOCTIC 7-Oxabicyclo[4.1.0]heptane, 1-meth SVOCTIC Elcosane SVOCTIC 9-Hexadecenoic acid SVOCTIC Ergost-5-en-3-ol, (3.beta.)- SVOCTIC 9-Octadecenoic acid (Z)-, octadecy SVOCTIC Ethanone, 1,1'-(6-hydroxy-2,5- SVOCTIC Aldrin SVOCTIC Ethenylmethylbenzene SVOCTIC Aldrin-R SVOCTIC Ethyl acetate SVOCTIC Amino-pteridinone SVOCTIC Glaucic acid SVOCTIC Androst-4-en-3-one, 17-hydroxy-, ( SVOCTIC Heneicosane SVOCTIC As-Indacene SVOCTIC Heptacosane SVOCTIC Benz[e]acephenanthrylene SVOCTIC Heptacosane SVOCTIC Benzo[b]naphtho[2,3-d]furan SVOCTIC Heptacosane SVOCTIC Benzo[e]acenaphthrylene SVOCTIC Heptadecane SVOCTIC Benzo[e]acephenanthyrlene SVOCTIC Heptadecane SVOCTIC Benzocycloheptene SVOCTIC Hexacosanal SVOCTIC Benzocycloheptene SVOCTIC Hexadecane SVOCTIC Benzofluorene isomer SVOCTIC Hexadecanoic acid SVOCTIC Benzofluorene isomer (1) SVOCTIC Hexadecenoic acid SVOCTIC Benzoic acid, 1-methylethyl ester SVOCTIC Hexadecyloxirane SVOCTIC bis-ethylhexyl ester hexanedioic SVOCTIC Hexahydroindenone SVOCTIC bis-ethylhexyl ester hexanedioic a SVOCTIC Indane SVOCTIC Bromodecahydropentanediol SVOCTIC Indene SVOCTIC Bromodecahydropentanediol SVOCTIC Methoxyfriedooleanene

TFM-0000779

Page 30: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-9 06/10/2005

ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER SVOCTIC Bromoethanol SVOCTIC Methylethenylcyclohexane SVOCTIC Butyl hexadecanoate SVOCTIC Methyloctadecane SVOCTIC Butyl octadecanoate SVOCTIC Methyloxabicycloheptane SVOCTIC Butyldocosane SVOCTIC Methyloxabicycloheptane SVOCTIC Chlorocyclohexanol SVOCTIC Naphthalene, 1,2,3,5,6,7,8,8a- SVOCTIC Cholesta-3,5-diene SVOCTIC Nonacosane SVOCTIC Cyclodecane SVOCTIC Nonadecane SVOCTIC Cyclododecane SVOCTIC Nonadecanol SVOCTIC Cyclohexenone SVOCTIC Octacosane SVOCTIC Cycloprop[e]azulene SVOCTIC Octadecanal SVOCTIC Cyclopropa[a]naphthalene SVOCTIC Octadecanamide SVOCTIC Cyclopropane, 1,1-dimethyl-2-(2-me SVOCTIC Octadecane SVOCTIC Cyclopropane, nonyl- SVOCTIC Octadecenamide SVOCTIC Cyclotetradecane SVOCTIC Octahydro-azulene SVOCTIC D-Friedoolean-14-ene, 3-methoxy-, SVOCTIC Octahydroazulene SVOCTIC D-Norandrostan-16-one, (5.alpha.)- SVOCTIC Octahydronaphthalene SVOCTIC Decahydromethylnaphthalene SVOCTIC Octahydroxyoctylbenzidine SVOCTIC Decahydronaphthalenecarboxylic acid SVOCTIC Oleic Acid SVOCTIC Decene SVOCTIC Pentadecanal SVOCTIC Dichlorobenzidine SVOCTIC Pentatriacontane SVOCTIC Dichlorocyclohexane SVOCTIC Pentatriacontane SVOCTIC Dimethoxylanthracene SVOCTIC Phenanthro[9,10-b]furan SVOCTIC Dimethoxymethylnaphthalenol SVOCTIC Pregn-4-ene-3,20-dione,

(

SVOCTIC Dimethylbenzeneethanol SVOCTIC Sitosterol SVOCTIC Dimethylheptadiene SVOCTIC Stigmastenone SVOCTIC Dimethylisopropyl SVOCTIC Stigmastenone SVOCTIC Dimethylmethylenecyclohexane SVOCTIC Sulfur SVOCTIC Dinitrobenzenamine SVOCTIC Tetracosane SVOCTIC Dioctadecylesterphosphonicacid SVOCTIC Tetracosane SVOCTIC Docosane SVOCTIC Tetradecanol SVOCTIC Tetradecyloxirane TCLPSVOC 1,4-Dichlorobenzene SVOCTIC Tetramethyl-butenone TCLPSVOC 2,4,5-Trichlorophenol 95-95-4 SVOCTIC Tetramethylhexadecane TCLPSVOC 2,4,6-Trichlorophenol 88-06-2 SVOCTIC Tetratriacontane TCLPSVOC 2,4-Dinitrotoluene 121-14-2 SVOCTIC Thiophene, 3,4-dichlorotetrahydro- TCLPSVOC Cresol (total) 1319-77-3 SVOCTIC Triacontane TCLPSVOC Hexachlorobenzene 118-74-1 SVOCTIC Tribromobenzenamine TCLPSVOC Hexachlorobutadiene SVOCTIC Tricosane TCLPSVOC Hexachloroethane 67-72-1 SVOCTIC Tricyclo[3.3.1.13,7]decane-2,6-dio TCLPSVOL m & p-Cresol SVOCTIC Tricycloundecene TCLPSVOC m-Cresol 108-39-4 SVOCTIC Trimethyltricycloundecenol TCLPSVOC Nitrobenzene 98-95-3 SVOCTIC Tritetracontane TCLPSVOC o-Cresol 95-48-7 SVOCTIC Unknown acid TCLPSVOC p-Cresol 106-44-5 SVOCTIC Unknown acid ester TCLPSVOC Pentachlorophenol 87-86-5 SVOCTIC Unknown alcohol TCLPSVOC Pyridine 110-86-1 SVOCTIC Unknown alkane TCLPVOC 1,1-Dichloroethene 75-35-4 SVOCTIC Unknown alkane (1) TCLPVOC 1,2-Dichloroethane 107-06-2 SVOCTIC Unknown alkane (2) TCLPVOC 1,4-Dichlorobenzene 106-46-7 SVOCTIC Unknown alkane (3) TCLPVOC Benzene 74-43-2 SVOCTIC Unknown alkene TCLPVOC Carbon Tetrachloride 56-23-5 SVOCTIC Unknown amide TCLPVOC Chlorobenzene 108-90-7 SVOCTIC Unknown amide (1) TCLPVOC Chloroform 67-66-3 SVOCTIC Unknown aromatic TCLPVOC Methyl ethyl ketone

TFM-0000780

Page 31: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-10 06/10/2005

ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER SVOCTIC Unknown cyclic hydrocarbon TCLPVOC Tetrachloroethylene 127-18-4SVOCTIC Unknown cyclic hydrocarbon TCLPVOC Trichloroethylene 79-01-6 SVOCTIC Unknown cyclic hydrocarbon (1) TCLPVOC Vinyl Chloride 75-01-4 SVOCTIC Unknown cyclic hydrocarbon (2) TPH #2 Fuel Oil SVOCTIC Unknown cyclic hydrocarbon (3) TPH #6 Fuel Oil C12-C24 SVOCTIC Unknown cyclic hydrocarbon (4) TPH Benzene SVOCTIC Unknown cyclic hydrocarbon (5) TPH C16 to C36 SVOCTIC Unknown cyclic hydrocarbon (6) TPH C18 to C36 SVOCTIC Unknown cyclic hydrocarbon (7) TPH Calculated as Diesel SVOCTIC Unknown cyclic hydrocarbon (8) TPH Calculated as Gasoline SVOCTIC Unknown hydrocarbon TPH Calculated as Kerosene SVOCTIC Unknown hydrocarbons (oil) TPH Calculated as Motor Oil SVOCTIC Unknown steroid TPH Diesel C10-C22 SVOCTIC Unknown unsaturated hydrocarbon TPH Ethyl benzene

TCLPHERB 2,4,5-TP (Silvex) 93-72-1 TPH Extractable Total Petroleum TCLPHERB 2,4-D 94-75-7 TPH JP-4 C6-C14 TCLPMET Arsenic 7440-38-2 TPH Kerosene C9-C18 TCLPMET Barium 7440-39-3 TPH Miscellaneous C10-C14 TCLPMET Cadmium 7440-43-9 TPH Miscellaneous C10-C16 TCLPMET Chromium 7440-47-3 TPH Miscellaneous C12-C28 TCLPMET Lead 7439-92-1 TPH Miscellaneous C14-C20 TCLPMET Mercury 7439-97-6 TPH Miscellaneous C14-C24 TCLPMET Selenium 7782-49-2 TPH Miscellaneous C14-C28 TCLPMET Silver 7440-22-4 TPH Miscellaneous C16-C22 TCLPPEST Aldrin TPH Miscellaneous C16-C28 TCLPPEST Chlordane 57-74-9 TPH Miscellaneous C18-C20 TCLPPEST Dieldrin TPH Miscellaneous C18-C24 TCLPPEST Endrin 72-20-8 TPH Miscellaneous C18-C28 TCLPPEST Heptachlor 76-44-8 TPH Miscellaneous C20-C22 TCLPPEST Heptachlor epoxide 1024-57-3 TPH Miscellaneous C20-C28 TCLPPEST Lindane (gamma-BHC) 58-89-9 TPH Miscellaneous C24-C28 TCLPPEST Methoxychlor 72-43-5 TPH Miscellaneous C7-C12 TCLPPEST Toxaphene 8001-35-2 TPH Miscellaneous C7-C16

TPH Miscellaneous C7-C18 VOC 2-Butanone 78-93-3 TPH Miscellaneous C7-C8 VOC 2-Chloroethanol TPH Miscellaneous C8 VOC 2-Chloroethylvinyl Ether 110-75-8 TPH Miscellaneous C8-C10 VOC 2-Chlorotoluene TPH Miscellaneous C8-C16 VOC 2-Hexanone 591-78-6 TPH Miscellaneous C8-C18 VOC 2-Hydroxypropionitrile TPH Miscellaneous C8-C9 VOC 2-Hydroxypropolionitrile TPH Miscellaneous C9-C18 VOC 2-Picoline 109-06-8 TPH Naphtha C6-C12 VOC 3-Chloropropionitrile TPH Toluene VOC 4-Chlorotoluene TPH Total Petroleum Hydrocarbons VOC 4-Methyl-2-Pentanone 108-10-1 TPH TPH as Diesel VOC Acetone 67-64-1 TPH TPH as Gasoline VOC Acetonitrile 75-05-8 TPH TPH as JP4 VOC Acrolein 107-02-8 TPH TPH as JP5 VOC Acrylonitrile 107-13-1 TPH TPH as Kerosene VOC Allyl alcohol 107-18-6 TPH TPH as Medium Petroleum Distillates VOC Allyl chloride 107-05-1 TPH TPH as Mineral Spirits VOC b-Propiolactone TPH TPH as Naptha VOC Benzene 74-43-2 TPH Varsol VOC Benzyl chloride 100-44-7 TPH Volatile Total Petroleum Hydrocarbons VOC Beta-Propiolactone

TFM-0000781

Page 32: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-11 06/10/2005

ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER TPH Xylenes VOC Bromoacetone 598-31-2

TPHSURR 1,3-Dichlorobenzene VOC Bromobenzene 108-86-1 TPHSURR 2-Chlorotoluene VOC Bromochloromethane TPHSURR Naphthalene VOC Bromodichloromethane 75-27-4 TPHSURR o-terphenyl VOC Bromoform 75-25-2 TPHSURR p-terphenyl VOC Bromomethane 74-83-9

VOC 1,1,1,2-Tetrachloroethane VOC BTEX (total) VOC 1,1,1,2-

/C VOC Carbon Disulfide 75-15-0

VOC 1,1,1-Trichloroethane 71-55-6 VOC Carbon Tetrachloride 56-23-5 VOC 1,1,2,2-Tetrachloroethane 79-34-5 VOC Chlorobenzene 108-90-7 VOC 1,1,2-Trichloroethane 79-00-5 VOC Chlorodibromomethane VOC 1,1-Dichloroethane 75-34-3 VOC Chloroethane 75-00-3 VOC 1,1-Dichloroethene 75-35-4 VOC Chloroform 67-66-3 VOC 1,1-Dichloropropene VOC Chloroprene VOC 1,2,3,4-Diepoxybutane VOC cis-1,2-Dichloroethene VOC 1,2,3-Trichlorobenzene VOC cis-1,3-Dichloropropene 10061-01-5VOC 1,2,3-Trichloropropane VOC cis-1,4-Dichloro-2-butene VOC 1,2,4-Trichlorobenzene VOC Dibromochloromethane 124-48-1 VOC 1,2,4-Trimethylbenzene 95-63-6 VOC Dibromoethane VOC 1,2-Dibromo-3-chloropropane 96-12-8 VOC Dibromomethane VOC 1,2-Dibromoethane VOC Dibromomethane/1,2- VOC 1,2-Dichlorobenzene 95-50-1 VOC Dichlorodifluoromethane 75-71-8 VOC 1,2-Dichloroethane 107-06-2 VOC Dichlorotetrafluoroethane VOC 1,2-Dichloroethene 540-59-0 VOC Diethyl Ether VOC 1,2-Dichloroethene (total) 540-59-0 VOC Epichlorohydrin 106-89-8 VOC 1,2-Dichloroethene(total) VOC Ethane VOC 1,2-Dichloropropane 78-87-5 VOC Ethanol 64-17-5 VOC 1,3,5-Trimethylbenzene 108-67-8 VOC Ethene VOC 1,3-Dichloro-2-propanol VOC Ethyl methacrylate VOC 1,3-Dichlorobenzene 541-73-1 VOC Ethylbenzene 100-41-4 VOC 1,3-Dichloropropane VOC Ethylene oxide 75-21-8 VOC 1,4-Dichloro-2-butene VOC Hexachlorobutadiene VOC 1,4-Dichlorobenzene 106-46-7 VOC Iodomethane VOC 1,4-Dioxane 123-91-1 VOC Isobutyl alcohol 78-83-1 VOC 2,2-Dichloropropane VOC Isopropyl alcohol VOC Isopropylbenzene VOCTIC 09.30 Trimethylbenzene VOC m,p-Xylene VOCTIC Dihydromethylindene VOC m-Xylene VOCTIC Dimethylheptane VOC Malononitrile 109-77-3 VOCTIC Ethyl acetate VOC Methacrylonitrile 126-98-7 VOCTIC Ethyldimethylbenzene VOC Methane VOCTIC Fluorotrimethylsilane VOC Methyl bromide 74-83-9 VOCTIC Isopropyl alcohol VOC Methyl chloride 74-87-3 VOCTIC Methyldecane VOC Methyl iodide 74-88-4 VOCTIC Methylindan VOC Methyl isobutyl ketone (MIBK) VOCTIC Octahydromethanoindene VOC Methyl methacrylate VOCTIC Propane VOC Methyl-tert-Butyl Ether VOCTIC Propenylbenzene VOC Methylene Bromide 74-95-3 VOCTIC Tetraethylbenzene VOC Methylene Chloride 75-09-2 VOCTIC Tetrahydronaphthalene VOC n-Butylbenzene 104-51-8 VOCTIC Trimethylsilanol VOC n-Propylamine 107-10-8 VOCTIC Trimethylsilanol VOC n-Propylbenzene 103-65-1 WQUAL Alkalinity VOC Naphthalene 91-20-3 WQUAL Ammonia

TFM-0000782

Page 33: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix A Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixA.doc A-12 06/10/2005

ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER ANALYSIS

TYPE PARAMETER NAME CAS

NUMBER VOC o-Xylene WQUAL Ammonia (N) VOC p-Isopropyltoluene WQUAL Ammonia (N) VOC p-Xylene WQUAL Ammonium Nitrate VOC Pentachloroethane 76-01-7 WQUAL Bi-Carbonate Alkalinity VOC Propargyl alcohol 107-19-7 WQUAL Biological Oxygen Demand VOC Propionitrile 107-12-0 WQUAL BOD VOC Pyridine 110-86-1 WQUAL Calcium Cyanide VOC sec-Butylbenzene 135-98-8 WQUAL Carbonate Alkalinity VOC Styrene 100-42-5 WQUAL Chemical Oxygen Demand VOC tert-Butylbenzene 98-06-6 WQUAL Chloride VOC Tetrachloroethene 127-18-4 WQUAL Cyanide VOC Toluene 108-88-3 WQUAL Fluoride VOC Total Petroleum Hydrocarbon WQUAL Hardness as CaCO3 VOC Total VOCs WQUAL Inorganic Chloride VOC trans-1,2-Dichloroethene WQUAL Nitrate VOC trans-1,3-Dichloropropene 10061-02-6 WQUAL Nitrate/Nitrite VOC trans-1,4-Dichloro-2-butene WQUAL Nitrate/Nitrite as N VOC Tribomomethane WQUAL Nitrite VOC Trichloroethene 79-01-6 WQUAL Nitrite as Nitrogen VOC Trichlorofluoromethane 79-01-6 WQUAL pH VOC Trichloromethane WQUAL Settleable Solids VOC Trichlorotrifluoroethane WQUAL Specific Conductivity VOC Vinyl acetate 108-05-4 WQUAL Sulfate VOC Vinyl Chloride 75-01-4 WQUAL Sulfate, Turbid VOC Xylene(m ,p ) 1330-20-7 WQUAL Temperature VOC Xylenes (total) 1330-20-7 WQUAL Total Dissolved Solids

VOCSURR 1,2-Dichloroethane-d4 WQUAL Total Hardness VOCSURR 4-Bromofluorobenzene WQUAL Total Organic Carbon VOCSURR Bromofluorobenzene WQUAL Total Organic Halogen VOCSURR cis-1,2-Dichloroethene WQUAL Total Phosphorous VOCSURR Dibromofluoromethane WQUAL Total Solids VOCSURR Naphthalene WQUAL Total Suspended Solids VOCSURR p-Chlorotoluene WQUAL Zinc Phosphate VOCSURR Toluene-d8

VOCTIC 06.83 Methylnaphthalene VOCTIC 07.97 Methylnaphthalene VOCTIC 08.88 Trimethylbenzene VOCTIC 08.94 Trimethylbenzene

TFM-0000783

Page 34: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

APPENDIX B

FDGC Recommended Minimum Content

TFM-0000784

Page 35: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix B Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixB.doc B-1 06/10/2005

APPENDIX B - FGDC Recommended Minimum Metadata Content (Source: FGDC Online Clearinghouse http://www.fgdc.gov/clearinghouse/metadataesystem/mes_description.html ) There is abundant interest in exactly what elements need to be filled in in order to build minimal but compliant FGDC-style metadata as produced by the Metadata Entry System. These are a few more than the mandatory list but constitute a minimal adequate set for general "catalog" use. Here is a list of those elements, valid for Version 1.0 of the Content Standard for Digital Geospatial Metadata: Repeating "Profile" Elements The following elements are collected once for a given metadata entry person and are embedded in every subsequent metadata entry they make, saving data entry time for this information.

• Metadata organization: • Metadata contact position/person: • Address type: • Address: • City: • State or province: • Postal code: • Country: • Phone: • Fax: • E-mail address

Metadata Elements for Each Entry General Identification Information

• Identity of this entry (for future update): • Originator: • Publication date (YYYYMMDD): • Title of data set: • Edition: • Presentation Form: • Publication place: • Publisher: • Online linkage (URL): • Abstract: • Purpose: • Supplemental Information: • Beginning date: (YYYYMMDD):

TFM-0000785

Page 36: FINAL REMEDIAL INVESTIGATION/FEASIBILITY STUDY DATA

Data Management Plan Appendix B Tulsa Fuel and Manufacturing - Collinsville, Oklahoma

DMP_AppendixB.doc B-2 06/10/2005

• Ending date: (YYYYMMDD): • Currentness reference: • Progress: • Intended data set maintenance and update frequency: • West bounding coordinate (-DDD.XXX): • East bounding coordinate (-DDD.XXX): • North bounding coordinate (DD.XXX): • South bounding coordinate (DD.XXX): • Theme keywords: • Theme Reference: • Place keywords: • Place Reference: • Limits on data accessibility: • Limits on use of data: • Browse graphic URL: • Browse graphic caption: • Browse graphic file type: • Spatial data type: (vector, raster, point)

Distribution Information

• Distribution organization: • Distribution contact position/person: • Address type: • Address: • City: • State or province: • Postal code: • Country: • Phone: • Fax: • E-mail: • Dataset name as known by Distributor: • Liability held by distributor: • Date of last metadata entry or update (YYYYMMDD):

TFM-0000786