Dioxins & Furans emission measurements June 2016 at ...4.1 Measuring results Dioxins & Furans In table 4.1 the emission results for dioxins & furans are given at actual O 2 vol. %

UAB “Bureau Veritas Lit”

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www.bureauveritas.lt

Dioxins & Furans emission measurements

June 2016

at Fortum Klaipeda

KW3 B.V.

Report number: KW3-20160049R02

UAB Fortum Klaipeda, Kretainis str. 3,

Lithuania Relatie nummer.: 96


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Summary

On 27 of June 2016, KW3 B.V. performed emission measurements at the main stack of a waste incineration plant

on the location of Fortum UAB, Lithuania.

The purpose of the emission measurements was to determine the emission of Dioxins & Furans in the flue gas of

the main stack.

The measurements were performed in accordance with the EN ISO 17020 and EN 15259. The specific standards for each component are described in chapter 2. The sample was analysed under EN ISO 17025.

Table 0.1 Emission dioxins & furans

Installation measurement Dioxins & Furans

Concentratie in ng/Nm3 at 11 % O2

Waste incineration plant 1 < 0.004

The average concentration for the sum of dioxins & furans is below the ELV of 0.1 ng/Nm3 at 11 vol. % O2.

The sample period was at 6 hours and at least 4 m3 of flue gas was led through the XAD cartouche.

Homogeneity tests

Profile measurements have been performed in 2013 and the flue gas at the sampling location is homogeneous.

See report: 7019303r01; 2013.


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Mailing list

1. Client (Digital)

2. KW3 B.V. archive (1x)

Colophon

Project leader : A. van Meekeren

Author : A. van Meekeren

Quality check calculations and report : M. Noortman

Measurement engineers on-site : B. Oudmaijer

: A. van Meekeren

Client

Name : UAB Fortum

Address : Kretainio street 3, LT-94103, Klaipeda Lithuania


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TABLE OF CONTENTS

1 INTRODUCTION ............................................................................................................................ 5

1.1 Introduction ........................................................................................................................ 5

2 MEASURING AND SAMPLING SYSTEM ..................................................................................... 6

2.1 Discontinuous measuring system (KW3) ........................................................................ 6

2.2 Quality KW3 B.V. ................................................................................................................ 6

3 Measuring program ...................................................................................................................... 7

3.1 General................................................................................................................................ 7

3.2 Emission program ............................................................................................................. 7

3.3 Description measuring area ............................................................................................. 7

4 results of measurements ............................................................................................................. 9

4.1 Measuring results Dioxins & Furans ............................................................................... 9

5 Uncertainty of measurements KW3 .......................................................................................... 10

5.1 Measuring uncertainty KW3 B.V. ................................................................................... 10

Appendix ............................................................................................................................................. 11

Appendix 1 Schematic of the gas sampling and analysing systems SRM ........................ 11

Appendix 2 Emission results ................................................................................................. 12

Appendix 3 Laboratory results .............................................................................................. 14

Appendix 4 Overview waste incineration plant ..................................................................... 17

Appendix 5 Accreditation certificate KW3 B.V. ..................................................................... 18


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1 INTRODUCTION

1.1 Introduction

On 27 of June 2016, KW3 B.V. performed emission measurements at the main stack of a waste incineration plant

on the location of Fortum UAB, Lithuania.

The purpose of the emission measurements was to determine the emission of Dioxins & Furans in the flue gas of

the main stack.

The measurements were performed in accordance with the EN ISO 17020 and EN 15259. The specific standards

for each component are described in chapter 2. The sample was analysed under EN ISO 17025.

In chapter 2 and 3 a description of the measurement system and the measurement program is presented. In

chapter 4 the results and the calculations of the tests are presented. The accuracy of the results is discussed in

chapter 5.


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2 MEASURING AND SAMPLING SYSTEM

2.1 Discontinuous measuring system (KW3)

Dioxins/ Furans

The dioxins & furans sampling were performed using the so-called condensation method. Via a cooled glass

measuring probe an isokinetic part stream from the waste gases was sucked through a XAD-2 cartridge. The

concentration of 17 PCDDs and PCDFs is then determined in a laboratory through high resolution mass

spectrometry gas chromatography.

The sampling is conducted in accordance with EN 1948-1. A schematic representation of the sampling system is

shown in appendix 1, figure 1.

Humidity flue gas

During the measurements flue gas is led through cooled glass bottles (impingers) to collect the water from the

flue gas. Before the measurement the impingers are weighted and after each measurement the impingers are

weighted again. Together with the exact known volume led through the impingers the humidity is calculated.

A schematic representation of the sampling system is shown in appendix 1, figure 2.

The sampling is conducted in accordance with the following European standards:

Table 2.1 EN standards

Component European standard/ method

Dioxins & Furans EN 1948-1

H2O EN 14790:2006

Volume flow ISO 10780

Emission sampling EN 15259:2007

2.2 Quality KW3 B.V.

KW3 B.V. is certified to perform emission measurements according to EN ISO/IEC 17020 (type A)/ ISO 9001 by

the Dutch council of Accreditation (no I304).

KW3 B.V. is certified for measuring NO, NO2, NOx, O2, CO, CO2, SO2, CxHy, dust, Hg, heavy metals (particle-

bound and volatile), gas velocity, gas temperature, gas humidity, flow, HCl, HF, NH3, H2S, CL2, formaldehyde,

dioxins & furans (PCDD/PCDF’s and PAH’s).

All project leaders and field engineers are in possession of a VCA certificate on level “ Safety for Operational

Supervisors Netherlands”.

All used equipment is electrical certified according to EN 1010, EN 50110 and EN 3140.

All inspectors on site are trained in performing emission measurements.


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3 MEASURING PROGRAM

3.1 General

The purpose of the measurement was to determine the emission concentration of Dioxins & Furans in the flue gas

of the waste incineration plant.

The plant is from UAB Fortum Klaipeda and has a capacity of 255000 tons waste per year. The incinerator is

designed for thermal destruction of solid waste. Herewith the boiler is used to produce steam for generating

electricity.

Before the flue gas is emitted to the air several treatment procedures are involved:

- Injection of NH3 for reducing NOx; - Injection of lime and charcoal; - Further treatment in a condenser.

See appendix 3 for an overview of the waste incineration plant.

3.2 Emission program

In table 3.1 the measuring program is presented.

Table 3.1 Emission measuring program component date measurements period

Dioxins & Furans 27-6-2016 1 11:56 – 17:56

3.3 Description measuring area

Table 3.2 Description measuring area

Parameters position measuring surface

Criteria

Placement stack at measuring surface vertical horizontal / vertical

distance after disturbance compliant > 5 x Dn.

distance straight duct after measuring surface compliant > 2 x Dn.

distance till outlet stack compliant > 5 x Dn.

Parameters for flow criteria Criteria

Minimum velocity compliant > 5 m/s en < 50 m/s

Direction flue gas compliant < 15º tov lengte-as

Fluctuations per point in flue gas compliant < 24 Pa

Dynamic and static pressure compliant P > 5 Pa

Distribution velocity in measuring surface compliant average velocity per ax < 5% of total average

Deviation temperature compliant < 5% of average

Parameters for dust criteria Criteria

Minimum velocity compliant > 2 m/s

Direction flue gas compliant < 15º tov lengte-as

Ratio highest and lowest velocity compliant Vmax / Vmin < 3


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The measuring surface is placed in the vertical duct. Access to the measuring ports via stairs. The measuring

surface is at the same level as the AMS at 20 meters height.

Table 3.3 Result homogeneity test (report 7019303r01: 2013)

NOx O2 SO2

flue gas Homogene Homogene Homogene

test value (ELV /average concentration) 70 mg/Nm3 21 vol% 750 mg/Nm3

required uncertainty 10 % 6 % 20.0 %

7 mg/Nm3 1.3 vol% 150 mg/Nm3

required sample type point point point

representative measuring point any point any point any point


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4 RESULTS OF MEASUREMENTS

4.1 Measuring results Dioxins & Furans

In table 4.1 the emission results for dioxins & furans are given at actual O2 vol. % and at 11 vol. % O2. In

appendix 2 an extended overview is given of the emission measurements.

Table 4.1 Emission measuring results

Concentrations at actual O2 vol% at 11 vol% O2

2,3,7,8 Tetra CDD (filter) ng/mn3 0.000 0.000

1,2,3,7,8 Penta CDD (Filter) ng/mn3 0.001 0.001

1,2,3,4,7,8 Hexa CDD (Filter) ng/mn3 < 0.001 < 0.001

1,2,3,6,7,8 HexaCDD (filter) ng/mn3 0.007 0.005

1,2,3,7,8,9 Hexa CDD (Filter) ng/mn3 0.002 0.002

1,2,3,4,6,7,8-Hepta CDD (filter) ng/mn3 0.066 0.045

Octa CDD (filter) ng/mn3 0.087 0.060

2,3,7,8-Tetrachloordibenzofuraan (filter) ng/mn3 0.009 0.006

1,2,3,7,8 Penta CDF (Filter) ng/mn3 0.003 0.002

2,3,4,7,8-Penta CDF (filter) ng/mn3 0.003 0.002

1,2,3,4,7,8 Hexa CDF (Filter) ng/mn3 0.001 0.001

1,2,3,6,7,8 Hexa CDF (Filter) ng/mn3 < 0.001 < 0.001


2,3,4,6,7,8 - Hexa CDF (filter) ng/mn3 < 0.001 < 0.001

1,2,3,4,7,8,9 -Hepta CDF (filter) ng/mn3 0.003 0.002

1,2,3,4,6,7,8 Hepta CDF (Filter) ng/mn3 < 0.001 < 0.000

Octa CDF (Filter) ng/mn3 < 0.006 < 0.004

TEQ volgens NATO/CCMS (filter) incl. <nd componenten ng/mn3 < 0.006 < 0.004

Measured O2 in flue gas [vol %] 6.52


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5 UNCERTAINTY OF MEASUREMENTS KW3

5.1 Measuring uncertainty KW3 B.V.

In the presentation of the emission components, which are sampled and analysed, several sources of errors can be

determined. Those are adding up to the inaccuracy of the measurement.

The measurement uncertainty indicates the uncertainty of a measured value. Each carried out measurement has a

certain degree of uncertainty. There’s a working method developed within the VKL (Dutch association of quality

air measurements) to determine the measurement uncertainties per component. The measurement uncertainty is

presented as a 95% confidence interval.

Table 5.1 Measuring uncertainty KW3

General

Company KW3

Project name Emission at UAB Fortum Klaipeda

Project number 20160049

location Stack waste incineration plant

Measurement performed by BO & AvM

Calculations performed by AvM

Debiet eenheid resultaat meetonzekerheid

[absoluut] [%]

Snelheid rookgas m/s 16.57 1.42 8.6

Debiet Nm3/h 152460 15617 10.2

Continue meting eenheid resultaat meetonzekerheid

[absoluut] [%]

O2 vol.% 6.5 0.24 3.7

Discontinue meting fase eenheid resultaat meetonzekerheid

[absoluut] [%]

PCDD/F totaal ng T.E.Q/Nm3 0.006 0.001 20.4


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APPENDIX

Appendix 1 Schematic of the gas sampling and analysing systems SRM

Figure 1 Overview Dioxins & Furans sampling system.

Figure 2 Overview H2O sampling system.


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Appendix 2 Emission results

Company UAB Fortum Equipment KW3-134

Emission source stack

Date 27-Jun-16

Component Dioxins & Furanes

Software version Software versie 5.10 (juni 2016)

Measurement 1

Measuring date 27-Jun-16

Measurement period from [hour] 11:56

til [hour] 17:56

Measuring time [min] 06:00

Atmospheric pressure [mbar] 1012

Diameter duct [m] 2.4

Surface duct [m2] 4.52

S-pitot factor [-] 0.809

Measuring points per ax [-] 8

Static pressure flue gas [mbar] -1.4

Temperature flue gas [°C] 147

Velocity flue gas (S-pitot) wet [m/s] 16.6

Flue gas flow at process conditions wet [m3/h] 269900

Flue gas flow at standard conditions dry [Nm3/h] 143159

Aspirated volume gasmeter dry [m3] 7.103

Temperature gas meter [°C] 24

pressure gas meter [mbar] 0.0

Aspirated volume gasmeter dry [Nm3] 6.520

Humidity flue gas dry [g/Nm3] 178.6

Humidity flue gas [vol.%] 21.4

Mass flow water [kg/h] 25561

Nozzle diameter [cm] 0.65

Bepaling van isokinetiek

Sampling time [sec.] 21600

Flow through nozzle dry [Nm3/s] 0.00030

dry [m3/s] 0.00047

wet [m3/s] 0.00056

Surface nozzle [m2] 3.32E-05

Velocity nozzle wet [m/s] 17.02

Isokinetiek factor [-] 1.03

Absorptiematriaal [-] XAD-2

Cartouchenummer [-] 0.0

Measured O2 in flue gas [vol %] 6.52


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Concentrations at actual O2 vol% 11 vol% O2

2,3,7,8 Tetra CDD (filter) ng/mn3 0.0005 0.0003

1,2,3,7,8 Penta CDD (Filter) ng/mn3 0.001 0.001

1,2,3,4,7,8 Hexa CDD (Filter) ng/mn3 < 0.001 < 0.001

1,2,3,6,7,8 HexaCDD (filter) ng/mn3 0.007 0.005

1,2,3,7,8,9 Hexa CDD (Filter) ng/mn3 0.002 0.002

1,2,3,4,6,7,8-Hepta CDD (filter) ng/mn3 0.066 0.045

Octa CDD (filter) ng/mn3 0.087 0.060

2,3,7,8-Tetrachloordibenzofuraan (filter) ng/mn3 0.009 0.006

1,2,3,7,8 Penta CDF (Filter) ng/mn3 0.003 0.002

2,3,4,7,8-Penta CDF (filter) ng/mn3 0.003 0.002

1,2,3,4,7,8 Hexa CDF (Filter) ng/mn3 0.001 0.001



2,3,4,6,7,8 - Hexa CDF (filter) ng/mn3 < 0.001 < 0.001

1,2,3,4,7,8,9 -Hepta CDF (filter) ng/mn3 0.003 0.002

1,2,3,4,6,7,8 Hepta CDF (Filter) ng/mn3 < 0.001 < 0.000

Octa CDF (Filter) ng/mn3 < 0.006 < 0.004

TEQ volgens NATO/CCMS (filter) incl. <nd componenten ng/mn3 < 0.006 < 0.004

TEQ volgens NATO/CCMS Upper bound (filter) excl. < ng/mn3 0.005 0.004


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Appendix 3 Laboratory results


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Appendix 4 Overview waste incineration plant


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Appendix 5 Accreditation certificate KW3 B.V.

Napájadlá 17, 040 12 KošiceIČO:31684165 tel. : 055/6411211, e-mail : [email protected]

RESULT OF THE ANALYSIS No. 5117/2016

Page : 1 / 3EKO-TERM SERVIS s.r.o.Napájadlá 11/2743040 12 Košice

Name saple : PUF 1 + filter + rinse + condensate Place of sampling : UAB "Fortum Klaipeda", Lithuania, Waste incineration plant Colecion of samples:EKO TERM -SERVIS s.r.o,Košice Date of service: 18.11.2016Sampling method: STN EN 1948-1 Date of colection : 7.11.2016Sampel charecteristic : emisie Termination date : 1.12.16

The analysis results are to the subject matter of the analysis and not replace any other documents.Without written approval of the testing laboratory this certificate may by reproduced as a whole only.

Results of testsParameter Unit Sample No. 16010000 Method

Value suma PCDD/F ng TEQ/sample 0,9668 A STN EN 1948-3:2006

Sample analysed : Ing. E. Jusková

A/N : acredited / not acredited

uncertainty U K=2 (95% probability)

Note on sampling: Sampling is not covered by this Protocol

Košice, dated: 1.12.2016

Head chemist: Ing. Eva Jusková

Autorized: ............................. Ing. Eva Jusková

Head manager of the laboratory

IČO : 31 684 165 P 12

Page No.2 / 3Protocol No. 5117/2016 Sample No.: 16010000

Order No : 1980/16

Partial results: Page No: 2/3

I-TEF Contcent.PCDD/F ng/sample. Contcent. PCDD/F ngTEQ/sample .

2378TCDD 1 0,019 0,0190

12378PeCDD 0,5 0,161 0,08065

123478HxCDD 0,1 0,595 0,0595

123678HxCDD 0,1 1,863 0,1863

123789HxCDD 0,1 0,912 0,09122

1234678HpCDD 0,01 15,810 0,15810

OCDD 0,001 12,260 0,012260

Suma PCDD 31,6206 0,607

2378TCDF 0,1 <0,004 <0,0004

12378PeCDF 0,05 0,125 0,006255

23478PeCDF 0,5 0,074 0,03675

123478HxCDF 0,1 0,406 0,04062

123678HxCDF 0,1 0,627 0,06273

234678HxCDF 0,1 1,416 0,1416

123789HxCDF 0,1 0,361 0,03613

1234678HpCDF 0,01 3,456 0,0346

1234789HpCDF 0,01 <0,010 <0,0001

OCDF 0,001 1,207 0,001207

Suma PCDF 7,6718 0,3598

Suma PCDD/F 39,2924 0,9668

Limit of quantification - shown in the table as the value of <

EQ value is given by the sum of the values of the concentrations of individual PCDD / F by multiplying the I-TEF

If the concentration of the wage determination is to TEQ values calculated LOD

Values of I-TEFpro PCDD / F used by Ministry of Environment Decree 410/2012 Coll

Disclaimer:

Chemical analysis was performed according to the IPP 464 (EN 1948 2.3)

The main difference IPP 464 - type mass detector triple qadrupol

The method was validated under the accreditation criteria.

Page No:2/3 2:

IČO : 31 684 165 P 12


Order No : 1980/16

For validation of the method under the following parameters:

- Expanded uncertainty: 30%

The volume of the sample after concentrating 100 µl

Injection: 2 ml

13C12 standad Typ Extraction

%

2378TCDD Extraction 101

12378PeCDD Extraction 112

123478HxCDD Extraction 114


1234678HpCDD Extraction 98

OCDD Extraction 98

2378TCDF Extraction 105

23478PeCDF Extraction 110

123478HxCDF Extraction 98



1234678HpCDF Extraction 95

OCDF Extraction 88

12378PeCDF Sampling 101

123789HxCDF Sampling 113

1234789HpCDF Sampling 87

The Annex is an integral part of the relevant protocol

It may be reproduced only with this Protocol

Prepared by: Ing. Eva Jusková Ing. Eva Jusková

Chemist Supervisor: Ing. Eva Jusková Head manager of the laboratory

IČO : 31 684 165 P 12




Name saple : PUF 2 Place of sampling : UAB "Fortum Klaipeda", Lithuania, Waste incineration plant Colecion of samples:EKO TERM -SERVIS s.r.o,Košice Date of service: 18.11.2016Sampling method: STN EN 1948-1 Date of colection : 7.11.2016Sampel charecteristic : emisie Termination date : 1.12.16



Value suma PCDD/F ng TEQ/sample <0,008 A STN EN 1948-3:2006









IČO : 31 684 165 P 12


Order No : 1980/16



2378TCDD 1 <0,004 <0,0040

12378PeCDD 0,5 <0,010 <0,005

123478HxCDD 0,1 <0,010 <0,0010

123678HxCDD 0,1 <0,010 <0,001

123789HxCDD 0,1 <0,010 <0,001

1234678HpCDD 0,01 <0,010 <0,00010

OCDD 0,001 <0,020 <0,000020

Suma PCDD <0,0280 <0,0028

2378TCDF 0,1 <0,004 <0,0004

12378PeCDF 0,05 <0,010 <0,0005

23478PeCDF 0,5 <0,010 <0,005

123478HxCDF 0,1 <0,010 <0,001

123678HxCDF 0,1 <0,010 <0,001

234678HxCDF 0,1 <0,010 <0,001

123789HxCDF 0,1 <0,010 <0,001

1234678HpCDF 0,01 <0,010 <0,0001

1234789HpCDF 0,01 <0,010 <0,0001

OCDF 0,001 <0,020 <0,000020

Suma PCDF <0,0520 <0,0052

Suma PCDD/F <0,0800 <0,008





Disclaimer:




Page No:2/3 2:

IČO : 31 684 165 P 12


Order No : 1980/16




Injection: 2 ml


%






OCDD Extraction 100







OCDF Extraction 89

12378PeCDF Sampling <1

123789HxCDF Sampling <1

1234789HpCDF Sampling <1





IČO : 31 684 165 P 12




Name saple : filter + rinse blank Place of sampling : UAB "Fortum Klaipeda", Lithuania, Waste incineration plant Colecion of samples:EKO TERM -SERVIS s.r.o,Košice Date of service: 18.11.2016Sampling method: STN EN 1948-1 Date of colection : 7.11.2016Sampel charecteristic : emisie Termination date : 1.12.16



Value suma PCDD/F ng TEQ/sample <0,008 A STN EN 1948-3:2006









IČO : 31 684 165 P 12


Order No : 1980/16



2378TCDD 1 <0,004 <0,0040

12378PeCDD 0,5 <0,010 <0,005

123478HxCDD 0,1 <0,010 <0,0010

123678HxCDD 0,1 <0,010 <0,001

123789HxCDD 0,1 <0,010 <0,001

1234678HpCDD 0,01 <0,010 <0,00010

OCDD 0,001 <0,020 <0,000020

Suma PCDD <0,0280 <0,0028

2378TCDF 0,1 <0,004 <0,0004

12378PeCDF 0,05 <0,010 <0,0005

23478PeCDF 0,5 <0,010 <0,005

123478HxCDF 0,1 <0,010 <0,001

123678HxCDF 0,1 <0,010 <0,001

234678HxCDF 0,1 <0,010 <0,001

123789HxCDF 0,1 <0,010 <0,001

1234678HpCDF 0,01 <0,010 <0,0001

1234789HpCDF 0,01 <0,010 <0,0001

OCDF 0,001 <0,020 <0,000020

Suma PCDF <0,0520 <0,0052

Suma PCDD/F <0,0800 <0,008





Disclaimer:




Page No:2/3 2:

IČO : 31 684 165 P 12


Order No : 1980/16




Injection: 2 ml


%






OCDD Extraction 89







OCDF Extraction 79

12378PeCDF Sampling 91

123789HxCDF Sampling 100

1234789HpCDF Sampling 70





IČO : 31 684 165 P 12

Documents

Dioxins & Furans emission measurements June 2016 at ...4.1 Measuring results Dioxins & Furans In table 4.1 the emission results for dioxins & furans are given at actual O 2 vol. %