CORPORATE OFFICES Maine, Massachusetts,Secure Site semspub.epa.gov/work/01/6862.pdf · CORPORATE OFFICES Maine, Massachusetts, New Hampshire, Connecticut Illinois, Florid, a Operational

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Operational offices throughout the US

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Jit eiJuly 27 2000 mdash

Mr Ed HathawayUSEPA Region IMaine Vermont and Connecticut Superfund SectionMailcode HBT1 Congress StreetBoston MA 02114

Subject Saco Municipal LandfillSpring 2000 Sampling Report

Dear Ed

This letter serves to convey the results of the spring 2000 sampling event This sampling was completedas described in our letter to you dated April 4 2000

Sample Collection and Analysis

Woodard amp Curran collected surface water and sediment samples from 1 1 locations on June 5 2000 Allsamples were analyzed at Katahdin Analytical Services for total arsenic iron and manganese accordingto Method 60102007 Sediment samples were also analyzed for total residual solids The results ofanalysis are provided as Attachment 1

Woodard amp Curran collected groundwater samples from 29 locations during the period May 30 throughJune 2 2000 All samples were analyzed at Katahdin Analytical Services for total arsenic iron andmanganese according to Method 60102007 Three samples (MW-95-4RD MW-95-1S and MW-13)were also submitted for volatile organic analysis (VOA) according to SW-846 Method 8260 The resultsof analysis are provided as Attachment 2

All samples were collected in pre-cleaned and pre-preserved sample jars provided by the laboratory Thesamples were kept on ice and delivered to the laboratory on the day of collection

Data Quality

The quality control results associated with analytical data for groundwater surface water and sedimentsamples collected on May 30 through June 5 2000 at the Saco Municipal Landfill were reviewed todetermine data quality Samples were segregated into the following sample delivery groups (SDGs)WQ-1540 WQ-1550 WQ-1571 WQ-1589 and WQ-1598 Data validation using established USEPAguidelines to determine data qualification was not completed

The laboratory Katahdin Analytical Services provided a QC level II analytical package A QC level IIanalytical package includes laboratory control sample results duplicate results matrix spike results andmethod and preparation blank results Raw analytical data calibration data and instrument performanceresults were not provided The following observations were made during the data review

41 Hutchins Drive i Portland Maine 04102 i 207-774-2112 i 207-774-6635 (Fax) i 1-800-426-4262 i wwwwoodardcurrancom

O95093Fall 1 999samplingreportcoverletter

WOODARD ampCURRAN L i rvnopt inr) Snence bull Opdegiations

Mr Ed Hathaway January 7 2000 Page 2

Metals Surface WaterSediments Surface water and sediment samples were collected from Sandy Brook on June 5 2000 All samples were analyzed for arsenic iron and manganese within EPA required holding times (6 months) Laboratory control samples had percent recoveries that were within acceptance limits for all target elements Duplicate surface water and sediment samples were collected at SWSD-103 and SWSD-52 The duplicate surface water samples compared well with relative percent difference (RPD) values below the EPA maximum of 30 For the sediment samples duplicate results for SD-103 were below the EPA maximum of 50 for all target elements However for the duplicate samples collected at SD-52 the RPD exceeded the EPA maximum for all target elements indicating that concentrations were not evenly dispersed throughout the matrix Matrix spike results for the surface water sample SW-103 was in compliance for all target elements For the sediment sample SD-103 non shycompliant matrix spike results were observed for iron and manganese Non-compliant matrix spike results were obtained due to spike concentrations added to the sample which were very low compared with the native concentrations already measured in the sample The spiked concentrations added to the sample were swallowed up by the high concentrations already present in the sample Preparation blanks were non-detect for target elements with the exception of trace levels of iron detected in one blank The iron detection in the blank had no effect on reported sample concentrations since sample concentrations were much greater than the associated action level

Metals Groundwater Groundwater samples were collected at Saco Landfill from May 30 to June 2 2000 All samples were analyzed within the EPA holding time limit of 6 months Laboratory control sample recoveries were acceptable for all target elements Duplicate results were collected at MW-95shy7S MW-95-1S and MW-95-8S Results for all duplicates compared well with RPDs below 30 for all elements in every pair Matrix spike results were acceptable for all elements indicating that matrix interferences were not likely Trace levels of iron at 0004 mgL were detected in preparation blanks Using the 5X rule (USEPA 1988) an action level of 002 mgL would have been established As a result reported concentrations of iron for MW-93-3 and MW-97-16S would have been qualified as non-detect during the validation process

VOAs Groundwater Three groundwater samples MW-95-1S MW-95-4RD and MW-13 were analyzed for VOAs using USEPA 8260 All samples were analyzed with EPA holding time limit of 14 days Laboratory control recoveries were acceptable for all target VOAs A field duplicate sample was collected at MW-95-1S The RPD between results was acceptable for all compounds except chloromethane (2 ugL in sample vs 25 ugL in duplicate) Matrix spike analysis was performed on MW-95-1S Matrix spike recoveries were below the minimum EPA acceptance limit of 60 for the majority of the target VOAs indicating possible matrix interference The matrix spike duplicate recoveries were in control for all VOAs so the interference indicated by the initial matrix spike results was not confirmed The method blank and trip blank each had methylene chloride detections of I MgL The blank data indicate that positive detections of methylene chloride in samples may be representative of laboratory contamination

O 95093Fall 1999samplmgreportcover letter

WOODARDampCURRAN f bullT j i i f -e rmq bull Science bull Ope rat ions

Findings

Results of groundwater surface water and sediment sampling conducted in MayJune 2000 are generally consistent with previous results

Surface water results from the May sampling event are shown on Table 1 with results from previous sampling events These results indicate that concentrations of arsenic in samples collected 300 to 500 feet downstream from the confluence of Sandy Brook and Big Ledge Brook (SW-98 and SW-103) are at concentrations similar to background

Sediment results are shown on Table 2 with results from previous sampling events Results from the May sampling event are consistent with historical concentration ranges Concentrations at the excavated seep location (SD-13) remain an order of magnitude below the pre-excavation concentrations Arsenic concentrations in sediment decrease downstream from the confluence of Sandy Brook and Big Ledge Brook Manganese and iron concentrations decrease downstream from the confluence with the exception of SD-103 where concentrations increase

Groundwater results from three wells at the foot of Landfill 4 (Table 3) illustrate the trends in groundwater concentrations Results from the November 1999 sampling are at or within historical concentrations

Please call me if you have questions or concerns on the enclosed report

Sincerely

WOODARD amp CURRAN INC

Tom Eschner PG Project Manager

cc W Harper (MEDEP) 1 copy R Michaud (City of Saco) 1 copy

File (Project 9509306)

O95093Fall 1999samplingreportcover letter

Table 1

Surface Water Analytical Data for Total Arsenic Manganese and Iron Saco Municipal Landfill

Saco Maine

RESULT Arsenic Manganese Iron LOCATION DATE TYPE (ugL) (ugL) (ugL)

Area 2

SW-7 111795 Primary 28 U 934 596 SW-7 51696 Primary 3 U 329 239 SW-7 111996 Primary 3 U 219 315 SW-7 62498 Primary 8 U 1880 SW-7(t) 10198 Primary ND 3050 SW-7 61099 Primary lt 5 1620 1320 SW-7 111999 Primary lt 5 708 366 SW-7 6500 Primary lt 5 418 380 SW-8 111795 Primary 28 U 779 582 SW-8 71797 Primary 67 U 3620 SW-8 62498 Primary 8 U 665 SW-9 111795 Primary 28 U 956 611 SW-9 111795 Duplicate 1 28 U 102 632 SW-9 51696 Primary 3 U 868 805 SW-9 111996 Primary 21 U 656 548 SW-9 111996 Duplicate 1 21 U 676 557 SW-9 71797 Primary 6 U 2680 SW-9 62498 Primary 8 U 792 SW-9 61099 Primary lt 5 73 790 SW-9 111999 Primary lt 5 374 392 SW-10 111795 Primary 28 U 972 619 SW-4 111795 Primary 28 U 804 575 SW-4 71797 Primary 46 U 2020 SW-4 71797 Duplicate 1 69 U 2650 SW-4 62498 Primary 8 U 839

Areas 3 and 4

SW-21 51696 Primary 138 3530 15500 SW-21 51696 Duplicate 1 136 3500 15400 SW-21 111996 Primary 21 U 835 772 SW-21 (t) 10198 Primary ND 43 SW-21 61099 Primary lt 5 88 806 SW-21 61099 Primary 34 875 4110 SW-21 111999 Primary lt 5 338 388 SW-21 6500 Primary lt 5 485 730 SW-52 111999 Primary 16 515 1900 SW-52 6500 Primary 30 816 3980 SW-52 6500 Duplicate 1 28 799 3640 SW-6A 62498 Primary 12 2130 SW-13 111795 Primary 87 J 342 1570

WOODARD CURRAN (95093 036) Spring 2000 Sampling Program 72700

Table 1

Surface Water Analytical Data for Total Arsenic Manganese and Iron

LOCATION

SW-13 SW-13 SW-13(t) SW-13 SW-13 SW-13 SW-13 SW-13 SW-37 SW-37 SW-37 SW-5 SW-34 SW-34 SW-34 (t) SW-34 SW-34 SW-34 SW-31 SW-31 SW-31 SW-15 SW-15 SW-15(t) SW-15 SW-15 SW-15 SW-69 SW-69 (t) SW-69 SW-69 SW-69 SW-73 SW-75 SW-78 SW-78 SW-83 SW-84 SW-86 SW-20 SW-93 SW-98 SW-98

111996 62498 10198 61099 61099

111999 111999

6500 61099

111999 6500

111795 62498 62498 10198 61099

111999 6500

61099 111999

6500 111795 111996 10198 61099

111999 6500

62498 10198 61099

111999 6500

111999 61099 61099 61099 61099

111999 61099

111795 111999 111999

Saco Municipal Landfill Saco Maine

RESULT Arsenic TYPE (ugL)

Primary 108 Primary 14 Primary 14 Primary 36

Duplicate 1 34 Primary 17

Duplicate 1 17 Primary 27 Primary 39 Primary 15 Primary 25 Primary 109 Primary 10

Duplicate 1 12 Primary 10 Primary 22 Primary 14 Primary 21 Primary 14 Primary 8 Primary 12 Primary 42 J Primary 122 Primary ND Primary 13 Primary 5 J Primary lt 5 Primary 11 Primary 8 Primary 12 Primary 6 J Primary 9 Primary 6 J Primary 12 Primary 11

Duplicate 1 12 Primary 11 Primary lt 5 Primary 11 Primary 28 U Primary lt 5 Primary 6 J Primary 9

Manganese (ugL)

1940 1300 1280 668 671 913

1350 704 938 239

448 1150 634 788 816 427 670 151 381

299 769 274 118

244 762 352 509 367 772 778 756 787 387 794 89

374 288 474

Iron (ugL)

12000 2370

3980 3850 2010 2010 3120 4990 1890 3370 1750 1760 1720

2450 1760 2870 1350 827 153 863

1260 601 410

1100 684

1160 652

1150 1050 1020 1020 669

1020 677 621 658

WOODARD CURRAN (95093 036) Spnng 2000 Sampling Program 72700

Table 1

Saco Maine

SW-103 111999 Primary lt 5 359 599 SW-103 111999 Duplicate 1 lt 5 375 630 SW-103 6500 Primary 7 J 458 1060 SW-103 6500 Duplicate 1 9 499 1120

Notes Sampling locations are presented in upstream to downstream order SW-6A - new location across from SW-13 J = estimated U = not detected at indicated reporting limit t = total arsenic analysis lt = element was detected but at a concentration less than the indicated value

Table 2 Sediment Analytical Data for Total Arsenic Iron and Manganese

Saceo Municipal Landfill Saco Maine

Location Sample Date Sample Type Arsenic (mgKg)

Iron (mgKg)

Manganese (mgKg)

Areas 3 and 4 SD-13 11171995 Primary 2250J 318000J 1660J SD-13 05161996 Primary 413 22400 184 SD-13 11191996 Primary 87 9350 92 SD-13 07171997 Primary 115 28800 NA SD-13 06241998 Primary 71 15700B NA SD-13 06101999 Primary 38 9710 122 SD-13 06101999 Duplicate 30 10900 137 SD-13 11191999 Primary 985 36200 508 SD-13 11191999 Duplicate 105 39000 551 SD-13 06052000 Primary 194 8990 146 SD-15 11171995 Primary 422J 16000J 464J SD-15 05161996 Primary 84 29000 NA SD-15 11191996 Primary 261 17200 305 SD-15 06101999 Primary 8 10400 163 SD-15 11191999 Primary 142 7340 122 SD-15 06052000 Primary 4 4500 593 SD-21 05161996 Primary 292 8090 102 SD-21 11191996 Primary 988 11500 214 SD-21 06241998 Primary 86 10000B NA SD-21 06101999 Primary 8 9170 221 SD-21 11191999 Primary 68 10300 162 SD-21 06052000 Primary 196 14700 269 SD-31 07161996 Primary 815 13700 NA SD-31 06101999 Primary 78 14700 973 SD-31 11191999 Primary 175 30900 1420 SD-31 06052000 Primary 773 14300 1020 SD-34 07161996 Primary 196 21500 NA SD-34 06241998 Primary 140 30000B NA SD-34 06241998 Duplicate 120 27500B NA SD-34 06101999 Primary 82 25400 324 SD-34 11191999 Primary 604 9920 109 SD-34 06052000 Primary 242 43300 639 SD-37 07161996 Primary 109 12000 NA SD-37 06101999 Primary 108 22400 734 SD-37 11191999 Primary 579 12200 242 SD-37 06052000 Primary 434 11500 969 SD-52 07161996 Primary 126 9410 NA SD-52 06101999 Primary 56 16300 417 SD-52 11191999 Primary 298 10400 851 SD-52 06052000 Primary 61 33300 286 SD-53 6500 Duplicate 242 11700 161 SD-69 04041997 Primary 70 6640 NA SD-69 06241998 Primary 61 4580B NA SD-69 06101999 Primary 18 7020 255 SD-69 11191999 Primary 183 6380 338 SD-69 06052000 Primary 357 10600 395 SD-73 06101999 Primary 19 9730 308 SD-73 11191999 Primary 173 8130 464 SD-84 06101999 Primary 28 7690 579 SD-84 11191999 Primary 168^ 5650 405 SD-93 11191999 Primary 144 5080 270 SD-98 11191999 Primary 124 5360 262 SD-98 06052000 Primary 269 12300 481 SD-103 11191999 Primary 11 14400 576 SD-103 11191999 Duplicate 10 17800 557 SD-103 06052000 Primary 172 6450 415 SD-103 06052000 Duplicate 172 7090 511

J = estimated NA = not analyzed

B = estimated

Table2sedxls 72700

Location

Area 2 SD-7 SD-7 SD-7 SD-7 SD-7 SD-7 SD-7 SD-9 SD-9 SD-9 SD-9 SD-9 SD-9 SD-9 SD-9

Sample Date

11171995 05161996 11191996 06241998 06101999 11191999 06052000 11171995 11171995 05161996 05161996 11191996 06241998 06101999 11191999

Sample Type

Primary Primary Primary Primary Primary Primary Primary Primary

Duplicate Primary

Duplicate Primary Primary Primary Primary

Arsenic (mgKg)

45 2 1

5 1 5 45

22J 22J 35 47 34 45

Iron (mgKg)

10500J 9420 9410

10100B 21600 5760 12300 4700J 5160 8740

10900 9080

10300B 6040

Manganese (mgKg)

329J 137 139 NA

1500 255 217

76 3J 91 8J

230 305 221 NA

277 202

Table2sed xls 72700

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Waterway Extent of Landfill Cap Capped Area

Figure 1 Spring 2000 Sampling Program

Groundwater Sampling Saco Municipal Landfill

Saco Maine

WDOMRDampCURRAN _i ^_^_mdash VBl Engineering bull Setone OplaquoraMoltM

95093raquoipfs2000fg 1 pff

SEEP AREA

BASE MAP SEE DETAIL AREA TO THE LEFT

NOTE FOR CLARITY OF PRESENTATION NOT ALL SAMPLING LOCATIONS ARE SHOWN LOCATIONS IN THE SERIES SD-73 TO SD-10J ARE AT 125 FOOT INTERVALS

SD-17 SEDIMENT SAMPLING LOCATION

LANDFILL PERIMETER

SEEP AREA

GROUNDWATER FLOW TO SEEP AREA

DESBY TE 1 DRBY PFF | CKBY TE SACO MUNICIPAL LANDFILL SACO MAINE

SPRING 2000 SAMPLING PROGRAM FIGURE 2

SURFACE WATER AND SEDIMENT SAMPLING LOCATIONS SCALE NTS JOB NO 9509306 DATE JULY 2000 SHEET fs2000fig2

WOODARDampCURRAN Engineering bull Science bull Operations

ATTACHMENT 1

REPORT OF ANALYSIS

SURFACE WATER AND SEDIMENT

rCatahdin I I C A I S K R V I C E S

July 7 2000

Mr Tom Eschner Woodard amp Curran 41 Hutchins Drive Portland ME 04102

RE Katahdin Lab Number WQ1598 Project ID SACO LANDFILL Project Manager Ms Andrea J Colby Sample Receipt Date June 6 2000

Dear Mr Eschner

Please find enclosed the following information

Electronic Data Deliverable (EDD) for the work order mentioned above

Due to an error in the Data Management department the EDD for this work order was not submitted with the hardcopy report We apologize for any inconvenience our error may have caused you

Should you have any questions or comments concerning this Report of Analysis please do not hesitate to contact the project manager listed above This cover letter is an integral part of the ROA

We appreciate your continued use of our laboratory and look forward to working with you in the future The following signature indicates technical review and acceptance of the data

Sincerely

KATAHDIN ANALYTICAL SERVICES

i CM (A poundX- L- 0 7 0 7 0 0

Authorized Signa Date Signature

MO ( oiuuv Riud Nn i 210Xc Road No 5 Portsmouth NH 1)3801 I l l Box -raquo c s t h n i u k Ml Tel 6lt 4 1 - S Fix 601 - t^3Vi6 ki iltr x i 2 d ) ( i iv (2 i r i ~~

Katahdin

June 22 2000

Mr Tom Eschner Woodard amp Curran 41 Hutchins Dr Portland ME 04102

RE Katahdin Lab Number WQ1598

Project ID SACO LF Project Manager Ms Andrea J Colby Sample Receipt Date(s) 6500

Dear Mr Eschner

Report of Analysis

Quality Control Data Summary

Chain of Custody (COC)

Confirmation

A copy of the Chain of Custody is included in the paginated report The original COC is attached as an addendum to this report

Sincerely

13OOAuthorized Signature Date

340 Counrv Road No S X^tRuJo i Portsmouth NH 05801 PO Box ~20 W e s t b r o o k MtCMraquo8 r oOl -ltM Strade FJX (60) -ttf-M lc1 (2(T) 8~M 2-tOO rax i2in trade=gt-4t)24

Katahdin Analytical Services 0000001

Katahdin A L S E R V I C E S

Lab Number WQ-1598-1

CLIENT TCM ESCHNER Report Date 062200

Wbodard amp Curran PO No 9509303

41 Hutchins Dr Project SAOO LF

Portland ME 04102

REPORT OF ANALYTICAL RESULTS Page 1 of 39

SAMPLE DESCRIPTION MATRIX SAMPLED BY SAMPLED DATE RECEIVED

SW-103 Aqueous DDINSMORE 060500 060500

PARAMETER RESULT UNITS DF PQL METHOD ANALYZED BY NOTES

Arsenic Total JO 007 mgL 10 0008 6010200 7 061400 EM 12 Iron Total 1 06 mgL 10 002 6010200 7 061400 EM 1 Manganese Total 0458 mgL 10 00050 6010200 7 061400 EM 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sample-specific reporting limits Sample-specific limits are indicated by results annotated with lt values

(1) Sample Preparation on 061200 by DCP using 3010 (2) J flag denotes an estimated value The analyte was detected in the sample at a concentration

greater than the measured detection limit but less than the laboratorys Practical Quantitation Level

062200

LJOmrcajc(dw) QF12ICWO

3-10 Counry Road No 5 210 West Road No 5 Portsmouth NH03SO

PO Box 720 Wtstbrook ME CH09S hirp kraquo ihdinhb ^ Tel (603) 431 V~~ Fax 605) 436 3^56

Tel (20^) 8^a 2400 Fix (207) gt 4029

Katahdin A N A L Y T I i S E R V I C E S

CLIENT TOM ESCHNER Report Date 062200

Woodard amp Curran PO No 9509303

41 Hutchins Dr Project SACO LF

Portland ME 04102

SW-103 DUP Aqueous DDINSMORE 060500 060500

Arsenic Total 0009 mgL 1 0 0008 6010200 7 061400 EM 1 Iron Total 112 trgL 10 002 6010200 7 061400 EM 1

Manganese Total 0499 mgL 1 0 00050 6010200 7 061400 EM 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sample-

specific reporting limits Sample-specific limits are indicated by results annotated with lt values

(1) Sample Preparation on 061200 by DCP using 3010

062200

340 Counrv Road No 5 2IO^ocRoadNo 5 Ponsmoutli NH0380I PO Box 20 Wcstbrook Mh 04098 Tel (603) 431 5V7 Fax (GOV ^3j 3356 Tel CO) S1 2400 Fax (20) 75 402J

Lab Number WQ-1598-3 CLIENT TOM ESCHNER Report Date 062200

Portland ME 04102

Arsenic Total 0009 mgL 1 0 0008 6010200 7 061400 EM 1

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

Manganese Total 0474 ngL 1 0 00050 6010200 7 061400 EM 1

(1) Sartple Preparation on 061200 by DCP using 3010

062200

LJOmrcajc (dw) QF12ICWO

310 County Road No 5 210 Vest Road No 5 Portsmouth NH03801 P O Bolt 20 Wfstbrook ME 04098

Imp k inlidmljb tlt-n Id (603) A3 Smdash Fax (603( 436-33iu Tel I2CT) 84 2400 Fai (207) 775 4029

41 Hutchins Dr Project SAGO LF

Portland ME 04102

Arsenic Total 0 009 mgL 10 0008 6010200 7 061400 EM 1

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

Manganese Total 0 509 mgL 10 00050 6010200 7 061400 EM 1

062200

340 County Road No 5 iOltXntRradNo 5 Poramouih NH03301 P O Box 720 Wcstbrook ME 0409S Td (603 431-5 Fij I60ii 43fr33Vgt Tel (20) 874 2400 Fix (207) 775-4029

Lab Number WD-1598-5

41 Hutchins Dr Project SACO IF

Portland ME 04102

MATRIX SAMPLED BY SAMPLED DATE RECEIVED SAMPLE DESCRIPTION

Arsenic Total lt0005 mgL 10 0008 6010200 7 061400 EM 1

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

Manganese Total 0118 mgL 10 00050 6010200 7 061400 EM 1

specific reporting limits Sanple-specific limits are indicated by results annotated with lt values

(1) Sanple Preparation on 061200 by DCP using 3010

062200

MO County Road No 5 210 Wot Road No 5 Portsmouth NH 03801

PO Box 720 Wcsibnok ME 0409S liar- k i t j i d i n l j b i T i Tel (603) 431-5777 Fix (603) 436-33

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

Arsenic Total 0012 mgL 10 0008 6010200 7 061400 EM 1 Iron Total 153 mgL 10 002 6010200 7 061400 EM 1 Manganese Total 0670 mgL 10 00050 6010200 7 061400 EM 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sanpleshy

062200

340 County Road No 5 2 IOWcnRo-dNo 5 Portsmouth NH 03801 PO Boraquo ~20 V t c s i b r o o k ME 04098 Tel 603) H31 i~ Fax f03gt 436 3356 Tel (207)8-4 2nOO Fax 20-) 775 4029

CLIENT TOM ESCHNER

Wbodard amp Curran

41 Hutchins Dr Portland ME 04102

Report Date 062200

PO No 9509303

Project SAOO LF

Arsenic Total 0021 mgL 10 0008 6010200 7 061400 EM 1

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

340 County Roid No 5 210 WestRoidNo 5 Poromouih NH 03801 PO Box720 Wcubrool ME 04098

Imp k j r ihdmlalgt i Tel (603 431-5~77 Flaquo (603gt 436-3356 Tel C07) S4-3400 FJJ 207) 75-4029

Lab Nun-ber WQ-1598-8

Portland ME 04102

SW-37 Aqueous DDINSM3RE 060500 060500

Arsenic Total 0 025 mgL 1 0 0008 6010200 7 061600 EM 1

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

P O Box 720 Wes tb rook ME 0109S 2IOXe[Rpoundj(JNo 5 Portsmouth NH 03801 Tel (207 874-2400 Fax (207) 75 4029 k l M l u l l let 1603) laquo1 57 ri iGOti 41ft-33iigt

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

340 County Road No 5 210 West Road No 5 Portsmouth NH 03801 P O Box 720 Wcstbrook ME 04093

Hup i kiMidmlab Tel (603)431 gt~7~ Fa (601) tW-3156 Tel (20^)8742400 Fax (207)^75-4029

CLIENT TOM ESCHNER Report Date OS2200

Portland ME 04102

SW-52 Aqueous DDINSMDRE 060500 060500

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

340 Coum Road No 5 210 West Road No 5 Portsmouth Nil 03801 P O Box 720 V c s c b r o o k ME 04098

Imp k i t i l u l m l i b Td (603) 131 5V7 Fix (603) 436 3356 Tel 0) S~4 2400 fn HC~ 775-4029

Woodard amp Curran PO Mb 9509303

Portland ME 04102

Arsenic Total 0028 mgL 1 0 0008 6010200 7 061600 EM 1 Iron Total 364 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

340 County Road No 5 210 Wat Road No 5 Portsmouth NH 03801 P O Box 720 Wcstbrook ME 04098 Tel (603 43 57-7 Fax (603) 436-3356

Tel- (2ltT) 8712400 Fix (207) 775 402V

Katahdin S E R V I C E S

Portland ME 04102

SW-21 Aqueous DDTNSMORE 060500 060500

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

specific reporting limits Sample-specific limits are indicated by results annotated with lt values (1) Sample Preparation on 061200 by DCP using 3010

062200

LJOmrcajc(dw)

QF12ICWO

3-10 Councy Road No 5 P O Box 720 Ccs ibrcok ME 04098 2 I O Vest Road o 1 fWmuuch NH 03801 Tci (20gt 3-4-2400 Fix f 2 lt T ) 775-4029 http kau idtnljb Tel (603 -i3l smdash- f j (603 436-3556

Portland ME 04102

Arsenic Total lt0 005 mgL 1 0 0008 6010200 7 061600 EM 1 Iron Total 038 mgL 1 0 002 6010200 7 061600 EM 1 Manganese Total 0418 mgL 1 0 00050 6010200 7 061600 EM 1

062200

340 County Road No 5 210WlaquotRoidNo 5 Poramouth NH 03801 P O Box 720 Westbtook ME 04098 Id 1603 431 57~7 Fax (603) 436 3^6 Tel (20) 84-24(W Fax (2ltTJ 75-4029

Lab Nurrter WQ-1598-14

Portland ME 04102

SD-103 Solid DDTNSMORE 060500 060500

Arsenic Total 172 08 6010200 EM mgKgdrywt 10 7 060900 1

Iron Total 6450 2 6010200 KD mgKgdrywt 10 7 061000 1 Manganese Total 415 mgKgdrywt 1 0 050 6010200 7 060900 EM 1

062200

LJOmrcajc(dw) QF08ICSO

340 Councy Road No 5 2IOesIRoadNo 5 Portsmouth NH 03801

P O Box 720 Wcstbrook ME 04098 h t t p k Tel [6tB (31 5~7 Fax (603) 436-3356 Tel (207) 874-2400 Fax (20~) 75-4029

Portland ME 04102

SD-103 Solid DDINSMORE 060500 060500

Solids-Total Residue (TS) 77 wt 10 010 CLPCIP SOW 060800 OF

(1) Sample Preparation on 060700 by JF

LJOmsmajc(dw)

QF07TSS3

340 County Road No 5 210 Vat Road No 5 Poromouih NH 03801

PO Bot 720 bulliXcstbrook ME (H098 Tel (6011 431 5T~ Fax (COD 4-56-3156 Tel (207) 874 2tOO Fix (207) -75-4029

062200

Woodard amp Curran PO No 9509303 41 Hutchins Dr Project SAGO LF Portland ME 04102

SD-103 DUP Solid DDINSMDRE 060500 060500

Arsenic Total 172 mgKgdrywt 10 08 60102007 060900 EM 1

Iron Total 7090 mgKgdrywt 10 2 60102007 061000 KD 1

Manganese Total 511 mgKgdrywt 10 050 60102007 060900 EM 1

PQL (Practical Ojuantitation Level) represents laboratory reporting limits and may not reflect sample-specific reporting limits Sample-specific limits are indicated by results annotated with lt values

062200

LJOmrcaj c(dw) QF08ICSO

3ltiO Counry Road No 5 2IOXctRoadNo 51ommouthNH 03801 T O Box 720 WcMhrook ME 0409S Til (603) 431-57mdash Fax (603) 436-3356

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

SD-103 DUP Solid DDINSMORE 060500 060500

Solids-Total Residue (TS) 75 wt 10 010 CLPCIP SOW 060800 JF

062200

LJOmsmajc(dw)

QF07TSS3

340 Counry Road No 5 2IOVCatRoadNo 5 Portsmouth NH 03801 P O Box 720 VXcwbrook ME 0409$

hnrgt kirilidmljlxur Tel (603)431-5777 Put (603gt 436-3356 Tel (20~) 84 2400 --t (20- 775-102

Wbodard amp Curran PO No 9509303 41 Hutchins Dr Project SACO LF Portland ME 04102

SAMPLE DESCRIPTIOSI MATRIX SAMPLED BY SAMPLED DATE RECEIVED

062200

340 Councy Road No 5 P O Box 720 VCes tbrook ME 0409S Tel (207) 874 2400 FAX (207) 75 W2V

210 West Road No 5 Poramouih NH 03801 Tc (603) 431 V1 fa (603) 43lti 3356

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

340 County Roid No 5 2 IOUlaquocRoadNo 5 Poromoutli NH03SOI P O Box 720 Vlaquoibrook Mk 0098 rd (G03mi V7 Fix 603 43igt335lt I r t p lt k i - i h d i i i l j l gt i i m Tel (20) 874 2400 Fax (20) 75 ltfC29

062200

Portland ME 04102

SD-69 Solid DDINSMDRE 060500 060500

Arsenic Total 357 mgKgdrywt 1 0 08 60102007 060900 EM 1

Iron Total 10600 mgKgdrywt 1 0 2 60102007 061000 KD 1

Manganese Total 395 mgKgdrywt 1 0 050 60102007 060900 EM 1

specific reporting limits Sample-specific lirrdts are indicated by results annotated with lt values

062200

340 Councv Road No 5 210VCcsRoid Vo 5 Portsmouth NH 03801

PO Bolt 720 Wotlrook ME 04098 Iif liiMhdin Tel (603)43 T~gt1 Flaquo (603 4363356

Tel (207l 8~42400 Fax (207) 775-4029

Woodard amp Curran PO No 9509303 41 Hutchins Dr Project SACO LF

Portland ME 04102

PQL (Practical Cuantitation Level) represents laboratory reporting limits and may not reflect sample-

specific reporting limits Sample-specific limits are indicated by results annotated with lt values (1) Sanple Preparation on 060700 by JF

062200

LJOmsmajc (dw)

QF07TSS3

3^0 Courtv Road No 5 210 West Road No 5 Pornmouch NH 03801 P O Box ^20 Wcstbrook ME 04098

kinhdiii Trl (601i 431 ^77 Fax (603) 136 3356 Tel i 2T) S-A 2400 Fn UltTi T 4029

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

340 Counry Road No 5 2IO West Road No 5 Pornmoudi NH 0380I PO Box 720 Wcstbiook ME 0-t098

ht tp Tel (603) 43-5777 FJJ- (603) 436-3356 Tel- (20~) S4-2400 Fa- (207) 7~5 t02y

Portland ME 04102

Solids-Total Residue (TS) 80 wt 10 010 CLPCIP SOW 060800 J

LJOmsmajc(dw) QF07TSS3

340 County Road No 5 210Wc3tRoil Mo 5 Porcnoudi NH 03801 PO Box ^20 Xcs tb rook ME 04098

Imp k j r ihdmbh Icl (603) 43 S~ F^ (601 4i 1355 Tel (207)8^2400 Fix (2(Tgt 5 4029

062200

Wbodard amp Curran PO No 9509303 41 Hutchins Dr Project SAOO LF Portland ME 04102

SAMPLE DESCRIPTICN MATRIX SAMPLED BY SAMPLED DATE RECEIVED

Manganese Total 1020 trgKgdrywt 10 050 6010200 7 060900 EM 1

062200

340 County Road No 5 210 Xcst Road No 5 Pornmouth NH0380I

PO Box 720 Woibroolc Mb 04098 Tel (603) 431 5777 Fi (603) 436-33S6 Tel (207) 874 2400 Falt pi)-) 5 4029

Portland ME 04102

specific reporting limits Sample-specific limits are indicated by results annotated with lt values (1) Sample Preparation on 060700 by JF

062200

LJOmsmajc (dw)

QF07TSS3

WO County Road No 5 P 0 Box -20 Wcsibrock ME 04093 Tel CO) 8-2400 Fax (207) 775-402ltgt

210VC=stRoidNo 5 Portsmouth NH 03801 Td (601)431-5~77 Fix 6051436-335(5

CLIENT TCM ESCHNER Woodard amp Curran 41 Hutchins Dr Portland ME 04102

Lab Number WQ-1598-20 Report Date 062200 PO No 9509303 Project SAGO LF

Arsenic Total 242 mgKgdrywt 10 08 6010200 7 060900 EM 1 Iron Total 43300 mgKgdrywt 10 2 6010200 7 061000 KD 1 Manganese Total 639 mgKgdrywt 10 050 6010200 7 060900 EM 1

062200

MO County Road No 5 20 Wai Road No 5 Portsmouth NH 03801

Tel (20^1 S~t 2400 l a x (2Q-) 775 4029 kjtihdnl Id (003)431 577- Fix (C0gt) 43fgt W6 PO Bo -20 NX-brook ME 04098

Katahdin A N A L Y T I C A L S E R V I C E S

Wocdard amp Curran PO No 9509303 41 Hutchins Dr Project SAOO LF

Portland ME 04102

Solids-Total Residue (TS) 28 wt 10 010 CLPCIP SOW 060800 OF 1

PQL (Practical Q iantitation Level) represents laboratory reporting limits and may not reflect sanpleshy

062200

340 County Road No 5 210 WK Road No 5 Poramouih NH 03S01 P O Box 720 Wes tb rook ME 04098

hup Tel (207)874-2400 Fax-(2071 775-4029 Tel-(6031 431-577 Fa (603M36-3356

Woodard amp Curran PO No 9509303 41 Hutchins Dr Project SAGO LF

Portland ME 04102

Arsenic Total 434 mgKgdrywt 1 0 08 6010200 7 060900 EM 1

Iron Total 11500 mgKgdrywt 1 0 2 6010200 7 061000 KD 1

Manganese Total 969 mgKgdrywt 1 0 050 6010200 7 060900 EM 1

(1) Sarrple Preparation on 060800 by DCP using 3050

062200

2IOWtscKoadNo 5 Portsmouth NH 03S01 Tel (207) 874-2400 Fax (207) 7754029 Ttl (603i 41lo7-7 FJ (603)436-3356 P O Box 720 Xestbrook ME 04098

41 Hutchins Dr Project SACO LF Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

3lttO Counrv Road No 5 210 Wcsi Road No 5 Portsmouth NH 0380 P O Boraquo 720 Wcstbrook Mh 04098

n r p lorihdinlih Tel (6031 431 57^7 Fax (603) 43ltS 3356 Tel (207) 84 2400 Fax 20T 775 4029

Woodard amp Curran PO No 9509303 41 Hutchins Dr Project SACO LF Portland ME 04102

062200

340 County Road No 5 210 West Road No 5 Portsmouth NH 03301 P O Box 720 Wcstb took ME 0409S

Imp kTfjhHinih M rr Tel ltgt03)431 577 Fix (603)436-3356 Tel (2071 S~4-2400 Fas (207) 775-4029

SD-13 Solid DDTWSMDRE 060500 060500

Solids -Total Residue (TS) 79 wt 10 010 CLPCIP SOW 060800 OF

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sanpleshyspecific reporting limits Sample-specific limits are indicated by results annotated with lt values

LJOmsmajc (dw)

QF07TSS3

210 West Road Mo 5 Pornnoudi NH0380I Tel lt20~) 874-2400 Fax CO7 775-4029 Tel (603 431-5-7 Fu (603 436-3356 P O Box 720 Wcsibro i l t ME 04098

062200

R3PORT OF ANALYTICAL RESULTS Page 32 of 39

SD-52 Solid DDINSM3RE 060500 060500

PARAMETER RESULT UNITS DF PQL ME7THOD ANALYZED BY NOTES

Arsenic Total 610 mgKgdrywt 20 08 60102007 061000 KD 1

Iron Total 333CO mgKgdrywt 20 2 60102007 061000 KD 1

specific reporting limits Sample-specific limits are indicated by results annotated with ltbull values (1) Sample Preparation on 060800 by DCP using 3050

062200

P O Box 720 Wcstbrook ME 0409S 210raquolaquocRoadNo 5 Portsmouth NH0380I Tel ( 207 )8742400 Fa 207)7754029 Tel (fi03) 431 5V7~ Fu (603) 436-335o

lab Number WQ-1598-23 CLIENT TOM ESCHNER Report Date 062200

062200

LJOmsmajc (dw) QF07TSS3

340 County Roid No 5 210 West Roid No 5 Portsmouth NH 03801 PO Box 720 Wcstbrook ME 04098 Tel (rgt03l 431 17trade Fw (603) 436-3356 Tel (207)3742400 Fix (207)-75 4029

rCatahdin S E R V I C E S

Lab Number WQ-1598-24 CLIENT TCM ESCHNER Report Date 062200

Manganese Total 161 TngKgdrywt 10 050 60102007 060900 EM 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sairpleshy

062200

MOCounrytWNo 5 P O Box 20 Wcsrbrook- ME 04098 Tel (207 S4-2400 Fax [207 775-4029 S l i p k j M l d m l i t i K

210 West Road No 5 Porumouih NH 03S01 Tel (603) 43-ltbull fix (603)436-3356

Wbodard amp Curran PO Mb 9509303 41 Hutchins Dr Project SACO LF Portland ME 04102

Solids-Total Residue (TS) 77 wt 10 010 CLPCTP SOW 060800 JF

062200

540 County Road No 5 210 Wat Road No 5 Portsmouth NH03SO PO Box 720 W c s t b r o o k M E C raquo O V 8 Icl (603)431 57^7 FJA 603) laquoul356 Tel (20) 84 2400 Fax i20~) ^54029

Katahdi S E R V I C E S

Iron Total 14700 trgKgdrywt 1 0 2 6010200 7 061000 KD 1

062200

340 Counrv Road No 5 210 West Road No 5 Pommouth NH 03801 P O Box 720 Wcstbrook ME 04098 Icl (603)431-5777 Fax (603M36-3356 Tel (20~gt 874-2400 Fix (207) 775-4029

Portland ME 04102

(1) Sample Preparation on 060700 by OF

062200

340 Councy Road No 5 210 West Road No 5 PonsmouchNH 03301 P O Box 720 Wesibrook ME 04098 Tel (603431-^7^7 Flaquo (603)436-3356 Tel (207) 874-2400 Fax 20~) 7^5--1029

Lab Nurrber WQ-1598-26

Portland ME 04102

Arsenic Total 4 5 mgKgdrywt 10 08 6010200 7 060900 EM 1

062200

LJOmrcajc(dw)

QF08ICSO

P O Box 720 W c s i b r o u k ME 04098 210 Wat Road No 5 Portsmouth NH 03801 T (2078--4-2400 Fix (207)7-^-4029 hep i Tel (603 43MT77 Flaquo (603) 436-3356

41 Hutchins Dr Project - SAOO LF

Portland ME 04102

Solids-Total Residue (TS) 78 wt 10 010 CLPCIP SO- 060800 JF

062200

LJOmsmajc (dw)

QF07TSS3

340 County Road No 5 210 Xest Road No 5 PoromouoS NH 03801

P O Box 720 Wcs tb rook Mt 0409S hrrp Tel 1603) 431 5777 FU (603) 436-3356 Td (2071874-2400 Fax (20^1^540-

iKatahdini^^^Bmyiiumn PREPARATION BLANK REPORT

Sample ID PBWQF121CWO Batch IDQF12ICWO

Element Name Result Units Flag PQL File

ALUMINUM 002 mgL U 010 BQF13A ANTIMONY 0002 mgL U 0008 AQF14A ARSENIC 0002 mgL U 0008 AQF14A BARIUM 00017 mgL J 00050 BQF13A BERYLLIUM 0001 mgL J 00050 BQF13A BORON 0007 mgL U 0100 BQF13A CADMIUM 00003 mgL U 00100 AQF14A CALCIUM 002 mgL U 005 BQF13A CHROMIUM 0004 mgL U 0015 BQFI3A COBALT 0003 mgL U 0030 BQF13A COPPER 0002 mgL U 0025 BQF13A IRON 0014 mgL J 0025 BQF13A LEAD 0001 mgL U 0005 AQF14A MAGNESIUM 001 mgL U 005 BQF13A MANGANESE 0001 mgL U 0005 BQF13A MOLYBDENUM 0002 mgL J 0100 AQF14A NICKEL 001 mgL U 004 BQF13A POTASSIUM 04 mgL J 10 BQF13A SELENIUM 0003 mgL U 0010 AQF14A SILICON 008 mgL J 020 BQF13A SILVER 0003 mgL U 0015 BQF13A SODIUM 002 mgL J 010 BQF13A THALLIUM 0008 mgL J 0015 AQF14A TITANIUM 00004 mgL U 00150 AQFI4A VANADIUM 0004 mgL U 0025 BQF13A ZINC 0002 mgL U 0025 BQF13A

U The analyte was not detected in the sample at a level greater than the instrument detection limit

J The analyte was detected in the sample at a concentration greater than the instrument detection limit but

less than the laboratorys Practical Quantitation Level

H The analyte was detected in the sample at a concentration greater than the laboratorys acceptance limit

bull Katahdin A N -v I v T I r A J SE k C L S 1

LABORATORY CONTROL SAMPLE REPORT

Sample ID LCSWQF12ICWO Batch ID QF12ICWO

Element Name True Value Result Units Recovery() Flag Limits () File

ALUMINUM 200 200 mgL 1000 80 120 BQFI3A

ANTIMONY 0500 0491 mgL 982 80 120 AQF14A

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BERYLLIUM 00500 00551 mgL 1102 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

CHROMIUM 0200 0226 mgL 1130 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

MAGNESIUM 500 515 mgL 1030 80 120 BQF13A

MANGANESE 0500 0561 mgL 1122 80 120 BQF13A

MOLYBDENUM 0300 0307 mgL 1023 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

POTASSIUM 250 264 mgL 1056 80 120 BQF13A

SELENIUM 200 193 mgL 965 80 120 AQF14A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

THALLIUM 200 209 mgL 1045 80 120 AQF14A

TITANIUM 100 104 mgL 1040 80 120 AQF14A

VANADIUM 0500 0542 mgL 1084 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

H Laboratory control sample recovery is greater than the laboratorys acceptance limit

Laboratory control sample recovery is less than the laboratorys acceptance limit

AAAKatahdin A N A L Y T I C A L ilaquogt L| ^^^^BH^HHHHBI^^H

PREPARATION BLANK REPORT

Sample ID PBSQF08ICSO Batch ID QF08ICSO

ALUMINUM 2 mgkgdrywt U 100 BQF09A ANTIMONY 02 mgkgdrywt U 0800 AQF09A

ARSENIC 02 mgkgdrywt U 0800 AQF09A BARIUM 005 mgkgdrywt U 0500 BQF09A BERYLLIUM 006 mgkgdrywt U 0500 BQF09A

BORON 07 mgkgdrywt U 100 BQF09A

CADMIUM 003 mgkgdrywt U 100 AQF09A

CALCIUM 2 mgkgdrywt U 500 BQF09A CHROMIUM 04 mgkgdrywt U 150 BQF09A COBALT 007 mgkgdrywt U 300 AQF09A

COPPER 02 mgkgdrywt U 250 BQF09A

IRON 16 mgkgdrywt J 250 BQF09A

LEAD 01 mgkgdrywt U 0500 AQF09A MAGNESIUM 3 mgkgdrywt J 500 BQF09A MANGANESE 01 mgkgdrywt U 0500 BQF09A

MOLYBDENUM 01 mgkgdrywt U 100 AQF09A

NICKEL 1 mgkgdrywt U 400 BQF09A

POTASSIUM 30 mgkgdrywt U 100 BQF09A

SELENIUM 03 mgkgdrywt U 100 AQF09A

SILICON 9 mgkgdrywt J 200 BQF09A

SILVER 03 mgkgdrywt U 150 BQF09A

SODIUM 4 mgkgdrywt J 100 BQF09A

THALLIUM 03 mgkgdrywt U 150 AQF09A

VANADIUM 05 mgkgdrywt J 250 BQF09A

ZINC 05 mgkgdrywt J 250 BQF09A

-KatahdinOBBBBD LABORATORY CONTROL SAMPLE REPORT

Sample ID LCSSQF08ICSO Batch ID QF08ICSO

Element Name True Value Result Units Recovery() Flag Limits (mgkgdrywt) File

ALUMINUM 4800 4690 mgkgdrywt 977 3040 6560 BQF09A ANTIMONY 498 431 mgkgdrywt 865 136 103 AQF09A ARSENIC 532 563 mgkgdrywt 1058 383 682 AQF09A BARIUM 112 126 mgkgdrywt 1 125 860 137 BQF09A BERYLLIUM 683 808 mgkgdrywt 1183 535 831 BQF09A BORON 819 916 mgkgdrywt 1118 818 161 BQF09A CADMIUM 151 148 mgkgdrywt 980 116 185 AQF09A CALCIUM 1320 1390 mgkgdrywt 1053 986 1650 BQF09A CHROMIUM 994 112 mgkgdrywt 1127 766 122 BQF09A COBALT 604 618 mgkgdrywt 1023 480 728 AQF09A COPPER 592 647 mgkgdrywt 1093 485 700 BQF09A IRON 9880 9780 mgkgdrywt 990 5050 14700 BQF09A LEAD 978 108 mgkgdrywt 1104 745 121 AQF09A MAGNESIUM 1220 1210 mgkgdrywt 992 983 1460 BQF09A MANGANESE 218 239 mgkgdrywt 1096 176 260 BQF09A MOLYBDENUM 107 118 mgkgdrywt 1 103 820 132 AQF09A NICKEL 633 67 mgkgdrywt 1058 495 770 BQF09A

POTASSIUM 2100 2250 mgkgdrywt 1071 1640 2560 BQF09A SELENIUM 143 144 mgkgdrywt 1007 106 180 AQF09A

SILICON 647 802 mgkgdrywt 1240 363 931 BQF09A SILVER 107 125 mgkgdrywt 1168 800 135 BQF09A

SODIUM 545 472 mgkgdrywt 866 370 721 BQF09A

THALLIUM 103 100 mgkgdrywt 971 587 146 AQF09A

VANADIUM 702 818 mgkgdrywt 1165 479 924 BQF09A

ZINC 123 129 mgkgdrywt 1049 947 150 BQF09A

L Laboratory control sample recovery is less than the laboratorys acceptance limit

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140 County RiMii No 5 PO Box 720 CHAIN of CUSTODY WeMbrook ME 04092 Tel (207) 874-2400 Fax (207) 775-4029 PLEASE PRINT IN PEN Page of

Client Contact -rr Phone Fax

(Zen ) Address -f ^ _ Clty state

Purchase Order Pro Katahdin Quote

Bill (if different than above) Address

Sampler (Print Sign) Copies To

LAB USE ONLY WORK ORDER It

KATAHDIN PROJECT MANAGER Hit Fill Rlt

ANALYSIS AND CONTAINER TYPE PRESERVATIVES

Fill Filt Filt Filt Filt Filt Filt O Y a N O Y O N O Y a N O Y O N O Y a N O Y O N O Y O N a Y O N l O Y O N OYON

REMARKSshy

SHIPPING INFO a FEDEX D UPS O CLIENT

AIRBILL NO

TEMPC O TEMP BLANK CD INTACT O NOT INTACT it-Sample Description Date Time

colld Matrix No of Cntrs

Sdgt 102)

SD-9B Moo HOC

ui-lS Ml-5 5D-(5 tygoo 16

Sco-3gt-( 2r5

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^Iwco (gtltlt$ ^J5 (^5co F2W5

SDshyCOMMENTS CAS-C

mdash fielinotusiisd By (Signature) Date Time Received By (Signature) Relinquished By (Signature) Date Time Received By (Signature)

Relinquished By (Signature) Date Time ReceiveltTBy (Signature) Relinquished By (Signature Date Time Received By (Signature)

13MSOURCE IMC TT 207)7823311 i^M ON-OF CSTOY

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

O 95093Fall 1999samphngreportcover letter

Katahdin I I c A I S K R V I C K S

June 282000

Project ID SACO LF Project Manager Ms Andrea J Colby Sample Receipt Date(s)shy 53000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

i i r rMcirux Lrug-urU Ofr18OO Authorized Signature Date

WO C ounn Roid laquo S 210 VW Road o 5 Portsmouth NH 01801 P C ) Box 20 XXes tb rook MF 04098 lei i601) 411 i- Fax (601) -16 Il if i rd i 2 o ~ gt s~4 2-iiio FJX (2ltrgt ~~s-iii1)

TECHNICAL NARRATIVE

For work order WQ1540 results for analyses performed according to EPA 60102007 have been reported to client-specified levels These levels are indicated in the results field of the analytical report

340 Count) Road No 5 210 Wat Road No JPortsmouth NH 03801 P O Box 720 Wcstbrook ME 04098 Tel (207) 8^4 2400 Fax (2(F ~gt 4029

Imp lor ihdinUh turn Tel (603) 4M-5777 Fax (603i 436-33

Portland ME 04102

MW-95-6S Aqueous DDINSMORE 053000 053000

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

MO County Road No 5 5 ftgtrrsmouth NH 03801 P O Box 720 Wcstbrook Mb 04098 Tel (207) 8T4-2400 [bulllaquo (207) 75 4029

h[tp Til (603M3I-57- Fraquox (603) 436 3356

Portland ME 04102

MW-93-3 Aqueous DDINSMORE 053000 053000

Arsenic Total lt0 005 mgL 1 0 0008 60102007 060900 EM 1

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

Manganese Total lt00050 mgL 10 00050 60102007 060900 EM 1

PQL (Practical Cuantitation Level) represents laboratory reporting limits and may not reflect sample-specific reporting limits Sample-specific limits are indicated by results annotated with lt values

062800

340 Councy Roid No 5 210 West Road No 5 Ponimouih NH 03801 PO Box 720 Wcscbrook ME 04098 Tel (207) 874 2400 Fix (207) 775-4029

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

MW-95-6R Aqueous DDINSMORE 053000 053000

Arsenic Total lt0005 tngL 1 0 0008 60102007 060900 EM 1 Iron Total 005 mgL 1 0 002 60102007 061000 KD 1

Manganese Total lt00050 mgL 1 0 00050 60102007 060900 EM 1

PQL (Practical Cuantitation Level) represents laboratory reporting limits and may not reflect sanpleshy

specific reporting limits Sartple-specific limits are indicated by results annotated with lt values (1) Sanple Preparation on 060800 by DCP using 3010

062800

340 Countv RoaJ Mu 5 210 West Road No 5 Poramouth NH 03801 P O Box 720 Wts ibrook ME 04098 Tel (207) 84 2400 f-ix (20) 775-4029

hrcp Td (603) 43l-577 fin (603) 4^6-33

Arsenic Total lt0 005 mgL 10 0008 6010200 7 060900 EM 1 Iron Total 0 05 mgL 10 002 6010200 7 061000 KD 1

062800

340 County Road No 5 210 West Roid No 5 rbrtsmouth NH 03801 PO Box 720 Wcstbrook Mt 04098 Tel (207) 874-2400 F-JJI 120) 75 4029

htp ka Tel (603)431-5777 Fix (603)436-3356

MW-95-7SDUP Aqueous DDINSMORE 053000 053000

Arsenic Total lt0 005 mgL 1 0 0008 6010200 7 060900 EM 1

Iron Total 006 mgL 1 0 002 6010200 7 061000 KD 1 Manganese Total 0188 mgL I0 00050 6010200 7 060900 EM 1

POL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sample-

062800

LJOmrcajcdw)

QF08ICWO

540 County Road No 5 210 Wot Road No 5 Poromouth NH 03801 [gt O Box 720 Wcstbcook ME 04098 Tel 2(T1 8~4-2400 Fix (20) 75 4029

h t t p lorahdmlj l on Tel (603) 431 5777 Fix (603) 436 3356

Portland ME 04102

Arsenic Total lt0005 mgL 1 0 0008 6010200 7 060900 EM 1

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

MO County Road No 5 210 War Rond No 5 Poirsmouch NH 05801 PO Box 720 Wcsbrook ME 04098 Tel (207) 84 2400 Fix (20) 77J-4029

ht rp k i r ahdmlah corr Tel (605) 431-5777 Fix (603) 436-3356

Katahdin A L S E R V

Woodard amp Curran PO Mb 95093 41 Hutchins Dr Project SACO LF Portland ME 04102

Arsenic Total lt0005 mgL 10 0008 6010200 7 060900 EM 1 Iron Total 011 mgL 10 002 6010200 7 061000 KD 1 Manganese Total 00218 mgL 10 00050 6010200 7 060900 EM 1

PQL (Practical Qjoantitation Level) represents laboratory reporting limits and may not reflect sample-specific reporting limits Sample-specific limits are indicated by results annotated with lt values

062800

LJOmrcajcdw) QF08ICWO

MO County Road No 5 210 Wot Road No 5 Poremourh NH038C1 PO Box 720 Wtstbcoolt ME 04098 Tel (2CP) 8T4 2400 fin (20) T) 4029

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Arsenic Total 0103 mgL 10 0008 60102007 060900 EM 1

Iron Total 457 mgL 10 002 60102007 061000 KD 1

Manganese Total 693 mgL 10 00050 60102007 060900 EM 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sample-specific reporting limits Sarrple-specific limits are indicated by results annotated with lt values

062800

340 County Road No 5 210 Wot Roid No 5 Portsmouth NH 03801 P O Box 720 VCcstbrook ME 04098 hrtp Td lt603gt4I-V Fix (603) 6-3356 Tel (207) 874-2400 FJJC (20~) 775-4029

41 Hutchins Dr Project SAOO LF Portland ME 04102

Iron Total 1 90 mgL 1 0 0025 6010200 7 062300 EM 1 Manganese Total 0 171 mgL 1 0 00050 6010200 7 062200 EM 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sarrpleshy

specific reporting limits Sanple-specific limits are indicated by results annotated with lt values (1) Sanple Preparation on 061400 by DCP using 3010

062800

340 County Road No 5 210Wot Road No 5 Ponsmouth NH 03SOI P O Boi 720 Westhfoolc ME 04098 Tel (207) 874-2400 Pix (207) 775-4029

hrp kjrahdmljb torp Tel (603 431-5777 Fix (603) 436-3356

Katahdin IB^^BBBBBi PREPARATION BLANK REPORT

Sample ID PBWQF08ICWO Batch ID QF08ICWO

ALUMINUM 002 mgL U 010 BQF09A

ANTIMONY 0002 mgL U 0008 AQF09A

ARSENIC 0002 mgL U 0008 AQF09A

BARIUM 00005 mgL U 00050 BQF09A

BERYLLIUM 00006 mgL U 00050 BQF09A

BORON 0007 mgL U 0100 BQF09A

CADMIUM 00003 mgL U 00100 AQF09A

CALCIUM 002 mgL U 005 BQF09A

CHROMIUM 0004 mgL U 0015 BQF09A

COBALT 00007 mgL U 00300 AQF09A

COPPER 0002 mgL U 0025 BQF09A

IRON 0004 mgL J 0025 BQF09A

LEAD 0001 mgL U 0005 AQF09A

MAGNESIUM 003 mgL J 005 BQF09A

MANGANESE 0001 mgL U 0005 BQF09A

MOLYBDENUM 0001 mgL U 0100 AQF09A

NICKpoundL 001 mgL U 004 BQF09A

POTASSIUM 03 mgL U 10 BQF09A

SELENIUM 0003 mgL U 0010 AQF09A

SILICON 002 mgL U 020 BQF09A

SILVER 0003 mgL U 0015 BQF09A

SODIUM 002 mgL J 010 BQF09A

STRONTIUM 000008 mgL J 0100 AQF09A

THALLIUM 0003 mgL U 0015 AQF09A

TITANIUM 00004 mgL U 00150 AQF09A

VANADIUM 0004 mgL U 0025 BQF09A

ZINC 0002 mgL U 0025 BQF09A

Katahdinmgomj^mu LABORATORY CONTROL SAMPLE REPORT

ALUMINUM 200 201 mgL 1005 80 120 BQF15A

ANTIMONY 0500 0452 mgL 90 4 80 120 AQF22A

ARSENIC 200 1 84 mgL 92 0 80 120 AQF22A BARIUM 200 2 14 mgL 1070 80 120 BQF15A

BERYLLIUM 00500 00475 mgL 95 0 80 120 AQF22A

BORON 0500 0566 mgL 1132 80 120 BQF15A CADMIUM 0050 0052 mgL 104 0 80 120 BQF15A

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

CHROMIUM 0200 0 195 mgL 97 5 80 120 AQF22A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

MANGANESE 0500 0543 mgL 108 6 80 120 BQF15A

MOLYBDENUM 0300 0286 mgL 95 3 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

POTASSIUM 250 264 mgL 105 6 80 120 BQF15A

SELENIUM 200 1 77 mgL 88 5 80 120 AQF22A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

STRONTIUM 0500 0505 mgL 101 0 80 120 AQF22A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

TITANIUM 1 00 0986 mgL 98 6 80 120 AQF22A

VANADIUM 0500 0538 mgL 107 6 80 120 BQF15A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

Laboratory control sample recovery is less than the laboratory s acceptance limit

VAKatahdi gmymggg LABORATORY CONTROL SAMPLE REPORT

Element Name True Value Result Units Recovery() Flag Limits I[) File

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

MAGNESIUM 500 5 13 mgL 102 6 80 120 BQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

THALLIUM 200 1 93 mgL 96 5 80 120 AQF09A

TITANIUM 1 00 1 06 mgL 1060 80 120 AQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

I aboratory control sample recovery is less than the laboratorys acceptance limit

kKatahdin HUyUIBBBB PREPARATION BLANK REPORT

ALUMINUM 002 mgL U 010 BQF~15A

BERYLLIUM 00003 mgL J 00050 AQF22A

BORON 0013 mgL J 0 100 BQF15A

CADMIUM 0003 mgL U 0010 BQF15A

CHROMIUM 00007 mgL U 00150 AQF22A

LEAD 0003 mgL J 0005 AQF22A

NICKEL 001 mgL U 004 BQF15A

POTASSIUM 03 mgL U 1 0 BQF15A

STRONTIUM 000007 mgL U 0 100 AQF22A

TIN 0002 mgL U 0 100 AQF22A

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34U County Road No 5 PO Box 720 CHAIN of CUSTODY Westbrook ME 04092 Tel (207) 874-2400 Fax (207) 775-4029 PLEASE PRINT IN PEN Page of

Client Contact Fax Phone

Address Cty State ZipCode ^ QHQ7

Purchase Order Proj Name No ^~ C QCgtQ3 Katahdin Quote

Copies To Sampler (Print Sign) T^ ^ J^JKVjttlc^^ Z^ ^^^L^

WORK ORDER bull^ bullbullH ANALYSIS AM) CONTAIN KIMK

LAB USE ONLY frj^ fT Ylt3

KATAHDIN PROJECT MANAGER Filt Filt Filt Filt Filt Filt Filt Filt Filt Filt OYON OY3N OYDN DYON OYON OY3N OYON UYDN OYDN DYDN

REMARKS

3C -J SHIPPING INFO O FED EX O UPS O CLIENT

AIRBILL NO

TEMPdegC O TEMP BLANK LJ INTACT LJ NOT INTACT

Date Time No of Sample Description Matrix colld Cntrs

Mu-95-lt^ 53calt)453o ngtiltlaquoi i i Hui-93-3 S^cxyioSo i Kui-95-^-R 53Dctit2o i i |VuJ-96-7S 53qbci2i5 i M -95-i7S Dup 5^o9^(2iS i I

53cwi3[5 Kui -97-145 i I MW-97-I^S 5ôcl3H5 i i Mu3-93-5 53ccxy IM45 i i ^û3957^ oiôjoctî^ iI

OMMENTS

^Relwiq~CijsJaed By (Signature) Date Time Received By (Signature) Relinquished By (Signature) Date Time Received By (Signature)

Relinquished By (Signature) Date Time Received By (Signature) Relinquished By (Signature) Date Time Received By (Signature)

MSOURCE INC tt (207)782-3311 M raquo CHN-OF-CSTOY

Kata^9mJKiaTytical Services 0000017

Katahdin A i s K R v I C E S

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Authorized Signature Date

340 Counrv Road No 5 210 esr Road No 5 Portsmouth NH 01801 P O Box 720 Wes tbrook ME 04098 Tel i6in -ill V F-i I 6 n raquo -t^6-3^ltgt Tel i2(T) 8~4-HOO FJlt (2CTI 5-4029

KATAHDIN ANALYTICAL SERVICES Summary of Report Notes

Report Note Note Text

B flag denotes detection of this analyte in the laboratory method blank analyzed concurrently with the sample

J flag denotes an estimated value less than the Laboratorys Practical Quantitation Level

Portland ME 04102

Arsenic Total 0 143 mgL 10 0008 6010200 7 061200 EM 1 Iron Total 31 1 mgL 1 0 002 6010200 7 061200 EM 1 Manganese Total 29 6 mgL 5 0 0005 6010200 7 061300 KD 1

062100

340 County Ro^d No 5 210 WOT ROK No 5 Portsmouih NH 03801

P O Box 70 W c s t b r o o k Mh 0409S f u r k i M h d i n l i b i n Tel 603 43 5~ l-ix (6031 436-3356 Tel (207) Si 2100 hx CO ~5-401)

Wbodard amp Curran PO No 9509303 41 Hutchins Dr Project SACO LF

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

340 Couni) Road No 5 210 West Road No 5 Portsmouth NH 038QI P O Box 720 VCcsrbrook Mt 0409S Tel (603)431-5777 Fax (603) bull36-3356 h u p Tel (20) S4 2400 Fax CO7 T5-trgt29

Portland ME 04102

MW-97-17R Aqueous DDTNSMORE 060100 060100

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

3ltiO County Roid No 5 210 Wat Road No 5 Poromouth NH 03S01 P O Box 20 Wtubrook ME 0-iOyS Tel (60J) 431-5- Fix 603) 436-3356 Tel f2ltT) 8-4 2400 Fax (2ir) 7~V4029

Arsenic Total 0 112 mgL 1 0 0008 6010200 7 061200 EM 1 Iron Total 323 mgL 1 0 002 6010200 7 061200 EM 1 Manganese Total 116 mgL 5 0 0005 6010200 7 061300 KD 1

062100

340 Countv Roid No 5 210 West Road No 5 1ortsmouih NH 0)801

P O Box 20 Wcjtbrook ME 04098 Ittrp k luhdnlljb torn Tel (603)431 T-^ Fax I f iO ) 436 13 Tel (20^) 84 2lOO Fax (207) 775 4029

Portland ME 04102

MW-97-14S2 Aqueous DDINSMORE 060100 060100

Arsenic Total 0 141 mgL 1 0 0008 6010200 7 061200 EM 1 Iron Total 23 9 mgL 1 0 002 6010200 7 061200 EM 1 Manganese Total 2 81 mgL 1 0 00050 6010200 7 061200 EM 1

062100

LTOmrcajc(dw) QF10ICWO

340 Counry Roid No 5 210 VCai Road No 5 Pommouch NH 03801 P O Box 720 Webrook MF 04098

htrp kjtilidii)Lb c Tel (603 131-5T7 Fix 1603) 43633^6 Tel 207i 874 2400 Fax W] 775-4029

Katahdin C A L S E R V I C E S

Wbodard amp Curran PO Mb 9509303 41 Hutchins Dr Project SAGO LF Portland ME 04102

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

540 Counry Road No 5 210 Wot Road No 5 Portsmouth NH 03801 P O Box 720 Wcjibiook Mfc D- lOVS Tel (603)43M7 FM (603 436-3356 Tel (20) 8T4 2400 Fax (20) -|09

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

Manganese Total 157 mgL 50 0005 6010200 7 061300 KD 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sarnpleshy

062100

LJOmrcajc(dw)

QF10ICWO

MO Councv Road No 5 210 West Road No 5 Portsmouth NH 03801

P O Bo in Wcnt-rook Mfc 04098 Id IIII ttl ltCgt Tel (603)4315777 Fax (603) 436 335d

Tel (2(T) 84 2400 FII (207) 77i-4029

KATAHDIN ANALYTICAL SERVICES REPORT OF ANALYTICAL RESULTS

Client TOM ESCHNER Lab Number WQ1571-7

Woodard amp Curran SDG WQ1571

41 Hutchms Dr Report Date 61600

Proj ID

PO No 9509303

Portland ME 041 02 Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

Sample Description Matrix Sampled Date Recd Date Ext Date Extd By Ext Method Analyst

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Compound Result Units DF PQL PQL

DICHLORODIFLUOROMETHANE lt2 ugL 10 2 2

CHLOROMETHANE 2 ugL 10 2 2

VINYL CHLORIDE lt2 ugL 10 2 2

BROMOMETHANE lt2 ugL 10 2 2

CHLOROETHANE lt2 ugL 10 2 2

TRICHLOROFLUOROMETHANE lt2 ugL 10 2 2

11-DICHLOROETHENE lt1 ugL 1 0 1 1

METHYLENE CHLORIDE lt1 ugL 10 1 1

12-DICHLOROETHENE (TRANS) lt1 ugL 10 1 1

11-DICHLOROETHANE lt1 ugL 10 1 1

12-DICHLOROETHENE (CIS) lt1 ugL 10 1 1

22-DICHLOROPROPANE lt1 ugL 10 1 1

BROMOCHLOROMETHANE lt1 ugL 10 1 1

CHLOROFORM lt1 ugL 10 1 1

111 -TRICHLOROETHANE lt1 ugL 10 1 1

1 2-DICHLOROETHANE lt1 ugL 10 1 1

11-DICHLOROPROPENE lt1 ugL 10 1 1

CARBON TETRACHLORIDE lt1 ugL 10 1 1

BENZENE lt1 ugL 10 1 1

1 2-DICHLOROPROPANE lt1 ugL 10 1 1

TRICHLOROETHENE lt1 ugL 10 1 1

CIS-1 3-DICHLOROPROPENE lt1 ugL 10 1 1

DIBROMOMETHANE lt1 ugL 10 1 1

BROMODICHLOROMETHANE lt1 ugL 10 1 1

TOLUENE lt1 ugL 10 1 1

TRANS-1 3-DICHLOROPROPENE lt1 ugL 10 1 1

1 1 2-TRICHLOROETHANE lt1 ugL 10 1 1

DIBROMOCHLOROMETHANE lt1 ugL 10 1 1

TETRACHLOROETHENE lt1 ugL 10 1 1

1 2-DIBROMOETHANE lt1 ugL 10 1 1

CHLOROBENZENE lt1 ugL 10 1 1

111 2-TETRACHLOROETHANE lt1 ugL 1 0 1 1

Report Notes

Client- TOM ESCHNER Lab Number WQ1571-7

PONo 9509303

Portland ME 04102 Project SACO LF

Solids- NA Proj ID-Method EPA 8260

Date Analyzed 6500

Sample Description Matrix Sampled Date Recd Date Ext Date ExfdBy Ext Method Analyst

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

ETHYLBENZENE lt1 ugL 1 0 1 1

M+P-XYLENE lt1 ugL 1 0 1 1

BROMOFORM lt1 ugL 1 0 1 1

O-XYLENE lt1 ugL 1 0 1 1

STYRENE lt1 ugL 1 0 1 1

1 23-TRICHLOROPROPANE lt1 ugL 1 0 1 1

ISOPROPYLBENZENE lt1 ugL 1 0 1 1

BROMOBENZENE lt1 ugL 1 0 1 1

2-CHLOROTOLUENE lt1 ugL 1 0 1 1

N-PROPYLBENZENE lt1 ugL 1 0 1 1

135-TRIMETHYLBENZENE lt1 ugL 10 1 1

TERT-BUTYLBENZENE lt1 ugL 1 0 1 1

124-TRIMETHYLBENZENE lt1 ugL 1 0 1 1

SEC-BUTYLBENZENE lt1 ugL 1 0 1 1

1 3-DICHLOROBENZENE lt1 ugL 1 0 1 1

P-ISOPROPYLTOLUENE lt1 ugL 1 0 1 1

14-DICHLOROBENZENE lt1 ugL 1 0 1 1

12-DICHLOROBENZENE lt1 ugL 10 1 1

N-BUTYLBENZENE lt1 ugL 10 1 1

1 2-DIBROMO-3-CHLOROPROPAN lt1 ugL 1 0 1 1

1 24-TRICHLOROBENZENE lt1 ugL 10 1 1

NAPHTHALENE lt1 ugL 10 1 1

HEXACHLOROBUTADIENE lt1 ugL 10 1 1

DIBROMOFLUOROMETHANE 112 1 0 TOLUENE-D8 111 1 0 P-BROMOFLUOROBENZENE 94 1 0 1 2-DICHLOROETHANE-D4 108 1 0

Report Notes-

Arsenic Total 0 368 tngL 1 0 0008 6010200 7 061200 EM 1 Iron Total 115 mgL 1 0 002 6010200 7 061200 EM 1 Manganese Total 15 4 mgL 5 0 0005 6010200 7 061300 KD 1

062100

340 Counry Road No 5 210 Wot Road No 5 Portsmouth NH 03801 P O Boraquo 720 WcS Ibrook ME 04093

hrp LjttlidmUh nun Tel (603)431-5^77 Fix (603) 436-3356 Tel (2071874-2400 Fix l2fT) 775-4029

Client TOM ESCHNER Lab Number WQ1571-8 Woodard amp Curran SDG WQ1571

41 Hutchins Dr Report Date 61600

Proj ID

PO No 95093 03

Portland ME 04102 Project SACO LF Solids NA

Method EPA 8260 Date Analyzed 6500

Sample Description Matrix Sampled Date Recd Date Ext Date Exfd By Ext Method Analyst

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

DICHLORODIFLUOROMETHANE lt2 ugL 1 0 2 2

CHLOROMETHANE 25 ugL 1 0 2 2

VINYL CHLORIDE lt2 ugL 1 0 2 2

BROMOMETHANE lt2 ugL 1 0 2 2

CHLOROETHANE J1 ugL 1 0 2 2

TRICHLOROFLUOROMETHANE lt2 ugL 1 0 2 2

METHYLENE CHLORIDE lt1 ugL 1 0 1 1

12-DICHLOROETHENE (TRANS) lt1 ugL 1 0 1 1

11-DICHLOROETHANE lt1 ugL 1 0 1 1

12-DICHLOROETHENE (CIS) lt1 ugL 1 0 1 1

22-DICHLOROPROPANE lt1 ugL 1 0 1 1

BROMOCHLOROMETHANE lt1 ugL 1 0 1 1

CHLOROFORM lt1 ugL 1 0 1 1

111-TRICHLOROETHANE lt1 ugL 1 0 1 1

11-DICHLOROPROPENE lt1 ugL 1 0 1 1

CARBON TETRACHLORIDE lt1 ugL 1 0 1 1 BENZENE lt1 ugL 1 0 1 1

CIS-1 3-DICHLOROPROPENE lt1 ugL 1 0 1 1

BROMODICHLOROMETHANE lt1 ugL 1 0 1 1

TOLUENE lt1 ugL 1 0 1 1

1 3-DICHLOROPROPANE lt1 ugL 1 0 1 1

DIBROMOCHLOROMETHANE lt1 ugL 1 0 1 1

TETRACHLOROETHENE lt1 ugL 1 0 1 1

12-DIBROMOETHANE lt1 ugL 1 0 1 1

CHLOROBEN2ENE lt1 ugL 1 0 1 1

1 1 1 2-TETRACHLOROETHANE lt1 ugL 1 0 1 1

Report Notes-

Woodard amp Curran SDG WQ1571 41 Hutchms Dr Report Date 61600

PO No 9509303

Method EPA 8260 Proj ID

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method Compound Result Units OF PQL PQL

ETHYLBENZENE lt1 ugL 10 1 1

M+P-XYLENE lt1 ugL 10 1 1 BROMOFORM lt1 ugL 10 1 1 0-XYLENE lt1 ugL 10 1 1 STYRENE lt1 ugL 10 1 1

1 1 22-TETRACHLOROETHANE lt1 ugL 1 0 1 1

123-TRICHLOROPROPANE lt1 ugL 10 1 1

ISOPROPYLBENZENE lt1 ugL 10 1 1

BROMOBENZENE lt1 ugL 10 1 1

2-CHLOROTOLUENE lt1 ugL 10 1 1

N-PROPYLBENZENE lt1 ugL 10 1 1

TERT-BUTYLBENZENE lt1 ugL 10 1 1

1 3-DICHLOROBENZENE lt1 ugL 10 1 1

P-ISOPROPYLTOLUENE lt1 ugL 1 0 1 1 14-DICHLOROBENZENE lt1 ugL 10 1 1

DIBROMOFLUOROMETHANE 106 1 0 TOLUENE-D8 110 10 P-BROMOFLUOROBENZENE 93 10

12-DIBROMO-3-CHLOROPROPAN lt1 ugL 10 1 1

124-TRICHLOROBENZENE lt1 ugL 10 1 1

12-DICHLOROETHANE-D4 106 10

Report Notes

MW-95-4RD Aqueous DDINSMORE 060100 060100

Iron Total 396 mgL 1 0 002 6010200 7 061200 EM 1 Manganese Total 219 mgL 1 0 00050 6010200 7 061200 EM 1

062100

LJOmrcaj c(dw) QF10ICWO

340 County Roid No 5 210 West Road No 5 Portsmouth NH 03301 P O Box 720 W c s t b r o o k ME 04098

I m p lt k u ihdmlit - Tel i603) 4310777 Fax (603)4363356 Tel 120 84 2400 Fax ltltT) 7^5-4025

PO No 9509303

Portland

Proj ID

ME 04102 Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

CHLOROMETHANE lt2 ugL 10 2 2

CHLOROETHANE 29 ugL 10 2 2

11-DICHLOROETHENE lt1 ugL 10 1 1

METHYLENE CHLORIDE B1 ugL 10 1 1

11-DICHLOROETHANE JOS ugL 10 1 1

12-DICHLOROETHENE (CIS) J05 ugL 10 1 1

11 1-TRICHLOROETHANE lt1 ugL 10 1 1

12-DICHLOROETHANE 1 ugL 10 1 1

CARBON TETRACHLORIDE lt1 ugL 1 0 1 1

BENZENE 14 ugL 10 1 1

TOLUENE J08 ugL 10 1 1

12-DIBROMOETHANE lt1 ugL 10 1 1

CHLOROBENZENE 12 ugL 10 1 1

111 2-TETRACHLOROETHANE lt1 ugL 10 1 1

Report Notes B J

kKatahdin KATAHDIN ANALYTICAL SERVICES I N A I Y M C A L S E R V I C E S REPORT OF ANALYTICAL RESULTS

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

ETHYLBENZENE 2 ugL 10 1 1

M+P-XYLENE 3 ugL 10 1 1

BROMOFORM lt1 ugL 10 1 1

0-XYLENE JO 8 ugL 10 1 1

STYRENE lt1 ugL 10 1 1

1 1 22-TETRACHLOROETHANE lt1 ugL 10 1 1

DIBROMOFLUOROMETHANE 110 10

TOLUENE-D8 111 10

P-BROMOFLUOROBENZENE 95 10

1 23-TRICHLOROPROPANE lt1 ugL 10 1 1

ISOPROPYLBENZENE 4 ugL 10 1 1

N-PROPYLBENZENE 2 ugL 10 1 1

1 35-TRIMETHYLBENZENE 1 ugL 10 1 1

SEC-BUTYLBENZENE lt1 ugL 10 1 1

P-ISOPROPYLTOLUENE JO 6 ugL 10 1 1 1 4-DICHLOROBENZENE 6 ugL 10 1 1

1 2-DICHLOROBENZENE 5 ugL 10 1 1

N-BUTYLBENZENE JO 8 ugL 1 0 1 1

NAPHTHALENE 14 ugL 1 0 1 1

1 2-DICHLOROETHANE-D4 110 10

Report Notes B J

Portland ME 04102

MW-13 Aqueous DDINSMORE 060100 060100

Arsenic Total 0 042 mgL 10 0008 60102007 061200 EM 1

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

MO Courm Roid No 5 210Wlaquo[Rxudo 5 Portsmouth N~H03SOI PO Box 20 Wjs ibrook ME 04098 Tel (603M3l-577 Fix 603436-3356 knhdulib Tel (20 7 gt8 7 4-2400 FAX (207)^5 4029

Proj ID

PO No 95093 03

Portland ME 041 02 Project SACO LF Solids NA

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

11-DICHLOROETHANE 40 ugL 1 0 1 1

1 1 1-TRICHLOROETHANE lt1 ugL 1 0 1 1

12-DICHLOROETHANE J06 ugL 10 1 1

CIS-13-DICHLOROPROPENE lt1 ugL 10 1 1

TOLUENE 5 ugL 10 1 1

112-TRICHLOROETHANE lt1 ugL 10 1 1

Report Notes

AAAKatahdini KATAHDIN ANALYTICAL SERVICES

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

Sample Description Matrix

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

1 1 22-TETRACHLOROETHANE

123-TRICHLOROPROPANE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

135-TRIMETHYLBENZENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

1 2-DIBROMO-3-CHLOROPROPAN

1 24-TRICHLOROBENZENE NAPHTHALENE

HEXACHLOROBUTADIENE

1 23-TRICHLOROBENZENE

DIBROMOFLUOROMETHANE

TOLUENE-D8

P-BROMOFLUOROBENZENE

1 2-DICHLOROETHANE-D4

REPORT OF ANALYTICAL RESULTS

Lab Number WQ1571-10

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

Sampled Date Recd Date Ext Date Extd By Ext Method Analyst

6100 6100 6500 BEG 5030 BEG

Sample Method

Result Units DF PQL PQL

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Client TOM ESCHNER Lab Number WQ1571-11 Woodard amp Curran SDG WQ1571 41 Hutchins Dr Report Date 61600

Proj ID

PO No 95093 03 Portland ME 041 02 Project SACO LF

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method Compound Result Units DF PQL PQL

DICHLORODIFLUOROMETHANE lt2 ugL 1 0 2 2 CHLOROMETHANE lt2 ugL 10 2 2 VINYL CHLORIDE lt2 ugL 1 0 2 2 BROMOMETHANE lt2 ugL 1 0 2 2 CHLOROETHANE lt2 ugL 1 0 2 2 TRICHLOROFLUOROMETHANE lt2 ugL 1 0 2 2 11-DICHLOROETHENE lt1 ugL 1 0 1 1

METHYLENE CHLORIDE 81 ugL 1 0 1 1 12-DICHLOROETHENE (TRANS) lt1 ugL 1 0 1 1 11-DICHLOROETHANE lt1 ugL 1 0 1 1 12-DICHLOROETHENE (CIS) lt1 ugL 1 0 1 1

BROMOCHLOROMETHANE lt1 ugL 1 0 1 1 CHLOROFORM lt1 ugL 1 0 1 1

111 -TRICHLOROETHANE lt1 ugL 1 0 1 1

1 2-DICHLOROETHANE lt1 ugL 1 0 1 1

11-DICHLOROPROPENE lt1 ugL 1 0 1 1 CARBON TETRACHLORIDE lt1 ugL 1 0 1 1 BENZENE lt1 ugL 1 0 1

1 2-DICHLOROPROPANE lt1 ugL 10 1 TRICHLOROETHENE lt1 ugL 1 0 1 CIS-1 3-DICHLOROPROPENE lt1 ugL 10 1

DIBROMOMETHANE lt1 ugL 10 1 BROMODICHLOROMETHANE lt1 ugL 1 0 1 TOLUENE lt1 ugL 1 0 1 TRANS-1 3-DICHLOROPROPENE lt1 ugL 1 0 1 1 1 1 2-TRICHLOROETHANE lt1 ugL 1 0 1 1 13-DICHLOROPROPANE lt1 ugL 1 0 1 1 DIBROMOCHLOROMETHANE lt1 ugL 1 0 1 1 TETRACHLOROETHENE lt1 ugL 1 0 1 1

CHLOROBENZENE lt1 ugL 1 0 1 1

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

M+P-XYLENE lt1 ugL 10 1 1

0-XYLENE lt1 ugL 1 0 1 1

1 35-TRIMETHYLBENZENE lt1 ugL 10 1 1

N-BUTYLBENZENE lt1 ugL 1 0 1 1

1 24-TRICHLOROBENZENE lt1 ugL 1 0 1 1

NAPHTHALENE lt1 ugL 1 0 1 1

HEXACHLOROBUTADIENE lt1 ugL 1 0 1 1

TOLUENE-D8 109 10

Report Notes B

Katahdin muuLmi^mi]PREPARATION BLANK REPORT

Sample ID PBWQF10ICWO Batch IDQF10ICWO

ALUMINUM 002 mgL J 010 AQF12A

ARSENIC 0002 mgL U 0008 AQF12A BARIUM 00003 mgL u 00050 AQF12A BERYLLIUM 00002 mgL J 00050 AQF12A BORON 0002 mgL J 0100 AQF12A CADMIUM 00003 mgL u 00100 AQF12A CALCIUM 0006 mgL u 0050 AQF12A

CHROMIUM 00007 mgL u 00150 AQF12A

COBALT 00007 mgL u 00300 AQF12A

COPPER 0002 mgL u 0025 AQF12A

IRON 002 mgL u 002 AQF12A

LEAD 0001 mgL u 0005 AQF12A MAGNESIUM 0006 mgL u 0050 AQF12A

MANGANESE 00002 mgL u 00050 AQF12A

MOLYBDENUM 0001 mgL u 0100 AQF12A

NICKEL 0001 mgL u 0040 AQF12A

SELENIUM 0003 mgL u 0010 AQF12A

SILVER 0001 mgL u 0015 AQF12A

STRONTIUM 000007 mgL u 0100 AQF12A

THALLIUM 0003 mgL u 0015 AQF12A

TIN 0002 mgL u 0100 AQFI2A

TITANIUM 00004 mgL u 00150 AQF12A

VANADIUM 00009 mgL u 00250 AQF12A

ZINC 00014 mgL J 00250 AQF12A

less than the laboratorys Practical Quantitation Level H The analyte was detected in the sample at a concentration greater than the laboratorys acceptance limit

Katahdin BBDBBS fl LABORATORY CONTROL SAMPLE REPORT

ALUMINUM 200 176 mgL 880 80 120 AQF12A

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BERYLLIUM 00500 00530 mgL 1060 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

CHROMIUM 0200 0216 mgL 1080 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

MAGNESIUM 500 525 mgL 1050 80 120 AQF12A

MANGANESE 0500 0518 mgL 1036 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

STRONTIUM 0500 0530 mgL 1060 80 120 AQF12A

THALLIUM 200 212 mgL 1060 80 120 AQFI2A

TIN 0500 0556 mgL 1112 80 120 AQF12A

VANADIUM 0500 0519 mgL 1038 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

VOLATILE ORGANICS METHOD BLANK SUMMARY

VBLKF05B Lab Name Katahdin Analytical Services SDG No WQ1571

Lab File ID F5632 Lab Sample ID VBLKF05B

Date Analyzed 060500 Time Analyzed 11 31

GC Column RTX-624 ID 018 (mm) Heated Purge (YN) N

Instrument ID 5972-F

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES LCSS MS AND MSDS

Client Lab Lab Date Time Sample ID Sample ID Data File Injected Injected

LCSF05A LCSF05A F5630 6500 9 39 00 AM MW-95-1S WQ1571-7 F5640 6500 51100PM

MW-95-1SDUP WQ1571-8 F5641 6500 5 50 00 PM MW-9amp4RD WQ1571-9 F5642 6500 6 28 00 PM

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

Client TOM ESCHNER Lab Number VBLKF05B

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

VBLKF05B AQ - 6500 BEG 5030 BEG

Sample Method

METHYLENE CHLORIDE 1 ugL 10 1 1

Report Notes

Client TOM ESCHNER Lab Number VBLKF05B Woodard amp Curran SDG WQ1571 41 Hutchms Or Report Date 61600

PO No 95093 03 Portland ME 04102 Project SACO LF

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

VBLKF05B AQ - - 6500 BEG 5030 BEG

M+P-XYLENE lt1 ugL 10 1 1 BROMOFORM lt1 ugL 10 1 1 O-XYLENE lt1 ugL 10 1 1 STYRENE lt1 ugL 1 0 1 1 1 1 22-TETRACHLOROETHANE lt1 ugL 1 0 1 1 1 23-TRICHLOROPROPANE lt1 ugL 1 0 1 1

DIBROMOFLUOROMETHANE 98 1 0

P-BROMOFLUOROBENZENE 94 1 0

ISOPROPYLBENZENE lt1 ugL 1 0 1 1 BROMOBENZENE lt1 ugL 1 0 1 1 2-CHLOROTOLUENE lt1 ugL 1 0 1 1 N-PROPYLBENZENE lt1 ugL 1 0 1 1 4-CHLOROTOLUENE lt1 ugL 1 0 1 1 135-TRIMETHYLBENZENE lt1 ugL 10 1 1 TERT-BUTYLBENZENE lt1 ugL 1 0 1 1 1 24-TRIMETHYLBENZENE lt1 ugL 1 0 1 1 SEC-BUTYLBENZENE lt1 ugL 1 0 1 1 1 3-DICHLOROBENZENE lt1 ugL 1 0 1 1 P-ISOPROPYLTOLUENE lt1 ugL 1 0 1 1 1 4-DICHLOROBENZENE lt1 ugL 1 0 1 1 1 2-DICHLOROBENZENE lt1 ugL 1 0 1 1 N-BUTYLBENZENE lt1 ugL 1 0 1 1

12-DIBROMO-3-CHLOROPROPAN lt1 ugL 1 0 1 1 1 24-TRICHLOROBENZENE lt1 ugL 1 0 1 1 NAPHTHALENE lt1 ugL 10 1 1 HEXACHLOROBUTADIENE lt1 ugL 10 1 1 1 23-TRICHLOROBENZENE lt1 ugL 1 0 1 1

TOLUENE-D8 108 10

Report Notes

Katahdin Analytical Services 8260 LCS Recovery Sheet

Lab File F5630 Sample ID LCSF05A Date Run 6500

Anahst BEG Time Injected 93900 AM Matrix AQ

Spike Amt Result Compound Name (ugL) Rec () Limits () (gD

1112-TETRACHLOROETHANE 50 554 in 60-140

111-TRICHLOROETHANE 50 523 105 60-140

1 I 22-TETRACHLOROETHANE 50 482 96 60 140

I 12-TRICHLOROETHANE 50 488 98 60-140

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

1 1 -DICHLOROPROPENE 50 496 99 60-140

123-TRlCHLOROBENZENE 50 48 5 97 60-140

1 23-TRICHLOROPROPANE 50 364 73 60-140

1 24-TRlCHLOROBENZENE 50 524 105 60 140

1 24-TRlM ETHYLBENZENE 50 582 116 60 140

l2-DIBROIO-3-CHLOROPROPANE 50 386 77 60-140

12-DIBROMOETHANE 50 422 84 60-140

1 2-DICHLOROBENZENE 50 539 108 60 140

U-DICHLOROETHANE 50 499 100 60-140

12-DICHLOROETHENE~(CIS) 50 552 110 60-140

1 2-DlCHLOROETHENE (TRANS) 50 ~~ 559 112 60 140

12-DICHLOROPROPANE 50 494 99 60-140

13 5-TRIM ETHYLBENZENE 50 567 113 60-140

1 3-DICHLOROBENZENE 50 543 109 60-140

1 3-D1CHLOROPROPANE 50 sTyen ~~ 104 60-140 ~

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

4-METHYL-2-PENTANONE 50 425 85 60-140 j

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOCHLOROMETHANE 50 45 8 ~ 92 60-140

BROMODICHLOROMETHANE 50 51 2 102 60-140

BROMOFORM 50 576 115 60-140

BROMOMETHANE 50~ 479 96 60 140

CARBON TETRACHLOR1DE 50 580 116 60-140

CHLOROBENZENE 50 533 106 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

CHLOROMETHANE 50 485 97 60-140

CIS-13 DICHLOROPROPENE 50 539 108 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

Compound Name D1BROMOCHLOROMETHANE

D1BROMOMETHANE

D1CHLORODIFLUOROM ETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

P ISOPROPYLTOLUENE ~

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRANS I 3 D1CHLOROPROPENE

TRICHLOROETHENE

TRICHLOROFLUOROM ETHANE

VINYL CHLORIDE

Katahdin Analytical Services

8260 LCS Recovery Sheet

Sample ID LCSF05A Date Run 6500

Time Injected- 93900 AM Matrix AQ

Spike Amt Result (ugL) (ugL) Rec ()

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

4A EPA SAMPLE NO VOLATILE ORGANICS METHOD BLANK SUMMARY

VBLKF07D Lab Name Katahdin Analytical Services SDG No WQ1571

Lab File ID F5679 Lab Sample ID VBLKF07D

Date Analyzed 060700 Time Analyzed 1824

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

AAAKarahdin ^H KATAHDIN ANALYTICAL SERVICES A N A I Y I 1 C A L SFKVICKS^^^^g REPORT OF ANALYTICAL RESULTS

Client TOM ESCHNER Lab Number VBLKF07D

41 Hutchms Dr Report Date 61600 PO No 95093 03

Portland ME 04102 Project SACO LF Solids NA Proj ID Method EPA 8260 Date Analyzed 6700

VBLKF07D AQ - 6700 BEG 5030 BEG

Sample Method

Compound Result Units DF POL PQL

CHLOROMETHANE lt2 ugL 1 0 2 2

CHLOROETHANE lt2 ugL 1 0 2 2

METHYLENE CHLORIDE 2 ugL 1 0 1 1

1 2-DICHLOROETHENE (TRANS) lt1 ugL 1 0 1 1

1 2-DICHLOROETHENE (CIS) lt1 ugL 1 0 1 1

1 11-TRICHLOROETHANE lt1 ugL 1 0 1 1

1 1 -DICHLOROPROPENE lt1 ugL 1 0 1 1

BENZENE lt1 ugL 1 0 1 1

TRICHLOROETHENE lt1 ugL 1 0 1 1

DIBROMOMETHANE lt1 ugL 1 0 1 1

BROMOOICHLOROMETHANE lt1 ugL 1 0 1 1

TRANS-1 3-DICHLOROPROPENE lt1 ugL 1 0 1 1

Report Notes

Client TOM ESCHNER Lab Number VBLKF07D Woodard amp Curran SDG WQ1571

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

VBLKF07D AQ - - 6700 BEG 5030 BEG

Sample Method

2 CHLOROTOLUENE lt1 ugL 1 0 1 1

1 35-TRIMETHYLBENZENE lt1 ugL 1 0 1 1

TERT BUTYL8ENZENE lt1 ugL 1 0 1 1

SEC BUTYLBENZENE lt1 ugL 1 0 1 1

12 DICHLOROBENZENE lt1 ugL 1 0 1 1

12-DIBROMO 3 CHLOROPROPAN lt1 ugL 1 0 1 1

DIBROMOFLUOROMETHANE 101 1 0 TOLUENE D8 104 1 0 P-BROMOFLUOROBENZENE 93 1 0 12-DICHLOROETHANE D4 98 10

Report Notes

Lab File F5676

Analyst BEM

Compound Name 111 2-TETRACHLOROETHANE

Ul-TRICHLOROETHANE

1 1 2-TRlCHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

1 1 -D1CHLOROPROPENE

123-TRICHLOROBENZENE

1 23-TRlCHLOROPROPANE

1 24-TRlCHLOROBENZENE

1 24-TRlMETHYLBENZENE

1 2-DIBROMO-3-CHLOROPROPANE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

12-D1CHLOROETHENE (CIS)

12-DICHLOROETHENE (TRANS)

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

4-M ETHYL-2-PENTANONE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMODICHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CARBON TETRACHLORIDE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

CIS-I3-DICHLOROPROPENE

Sample ID LCSF07B Date Run 6700

Time Injected 35700 PM Matrix AQ

Spike Amt Result (ugL) (ugL) Rec () Limits ()

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Time Injected 35700 PM

Date Run 6700

Matrix AQ

Compound Name

Dl BROMOCHLOROM ETHANE

DIBROMOM ETHANE

DICHLORODIFLUOROMETHANE ETHYLBE^NZENE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

NAPHTHALENE O-XYLENE

P-ISOPROPYLTOLUENE

SEC-BUTYLBENZENE STYRENE

TERT-BUTYLBENZENE

TETRACHLOROETHENE TETRAHYDROFURAN

TOLUENE

TRANS- 13 DICHLOROPROPENE TR1CHLOROETHENE

TR1CHLOROFLUOROM ETHANE VINYL CHLORIDE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

VBLKF08B Lab Name Katahdin Analytical Services SDGNoshy WQ1571

GC Columnshy RTX-624 ID 018 (mm) Heated Purge (YN) N

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES LCSS MS AND MSDS bull

LCSF08A LCSF08A F5695 6800 7 55 00 AM MW-95-1SMSD WQ1571-7MSD F5700 6800 11 4800AM

FORM IV VGA Page 1

vKatahdi KATAHDIN ANALYTICAL SERVICES A N A I V f i C A L REPORT OF ANALYTICAL RESULTS

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

12-DICHLOROETHANE lt1 ugL 10 1

11-DICHLOROPROPENE lt1 ugL 10 1

CARBON TETRACHLORIDE lt1 ugL 10 1

BENZENE lt1 ugL 10 1

12-DICHLOROPROPANE lt1 ugL 10 1

TRICHLOROETHENE lt1 ugL 10 1

TRANS-13-DICHLOROPROPENE lt1 ugL 10 1 1

Report Notes

MMBiiitH KATAHDIN ANALYTICAL SERVICES A N A L Y T I C A L S F K V 1 C fcT^^^^^^^B REPORT OF ANALYTICAL RESULTS

41 Hutchins Dr Report Date 61600 PO No 9509303

Date Analyzed 6800

Sample Method

O-XYLENE lt1 ugL 10 1 1

TOLUENE-D8 106 10

P-BROMOFLUOROBENZENE 91 deg 10

4-CHLOROTOLUENE bull=1 ugL 10 1 1

P-ISOPROPYLTOLUENE lt1 ugL 10 1 1

1 2-DIBROMO-3-CHLOROPROPAN lt1 ugL 10 1 1

HEXACHLOROBUTADIENE lt1 ugU 10 1 1

Report Notes

Analyst BEM Time Injected 75500 AM Matrix AQ

Spike Amt Result Compound Name (ugL) (ugL) Rec () Limits () 12 TETRACHLOROETHANE 50 533 106 60-140

1-TRICHLOROETHANE 50 59 1 118 60-140 ~~ 102~~ 7~22-TETRACHLOROETHANE 50 51 3 60 140

2-TRlCHLOROETHANE 50 542 108 60-140

-DICHLOROETHANE 587 117 60-140

T^DICHLOROETHENE ~ 50 656 131 60 140

-DICHLOROPROPENE 50 462 92 60-140

23-TRICHLOROBENZENE 50 50 I 100 60-140

23-TRJCHLOROPROPANE 50 392 78 60-140

1 24-TRJCHLOROBENZENE 50~ 52 1 104 60-140

I 24-TRIMETHYLBENZENE 50 590 118 1 60-140

1 2-DI BROMO-3-CHLOROPROPANE 50 448 90 1 60 140

1 2-DlBROMOETHANE 50 51 0 102 60-140

12-DICHLOROBENZENE 50 562 112 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

12 DICHLOROETHENE (CIS) 50 584 117 60 140

12-DICHLOROETHENE (TRANS) 50 62 4 125 i 60-140

1 2-DICHLOROPROPANE 50 51 8 104 60-140

1 35-TRIMETHYLBENZENE 50 577 115 60-140

1 3-DICHLOROPROPANE 50 ^ 542 108 60-140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

4-CHLOROTOLUENE 50 570 114 i 60 140

4-METHYL 2 PENTANONE 50 539 108 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOBENZENE 50 540 108 60-140

BROMOCHLOROMETHANE [ 50 ssT Tl6 f~ 60-140

BROMODICHLOROM ETHANE 54 1 108 60 140 L 50 WoMOFORM 50 572 114 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CARBON TETRACHLORIDE 50 603 120 60 140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

CHLOROM ETHANE 50 535 107 60-140

CIS-13-DICHLOROPROPENE 50 564 113 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Time Injected 75500 AM

Date Run 6800

Matrix AQ

Compound Name Spike Amt

(ugL) Result

(ugL) Rec () DIBROMOCHLOROMETHANE 50 550 no DIBROMOMETHANE 50 524 105

DICHLORODIFLUOROM ETHANE 50 590 118 ETHYLBENZENE L 50 600 120

HEXACHLOROBUTADIENE 1 50 41 3 83

ISOPROPYLBENZENE 1 50 562 112

M+P-XYLENE 1 100 118 118 METHYLENE CHLORIDE 50 446 89

N BUTYLBENZENE 50 582 116

WROPYLBENZENE 50 574 115 NAPHTHALENE 1 so 51 7 103

6-XYLENE 5deg 638 128

P-ISOPROPYLTOLUENE 50 ~ 595 119

SEC-BUTYLBENZENE 50 61 5 123

LSTYRENE 50 625 125

TERT-BUTYLBENZENE 50 606 121

TETRACHLOROETHENE 50 535 107

TETRAHYDROFURAN 50 786 ~157

TOLUENE SF mdash ~gt1 IM~

TRANS- 1 3-DICHLOROPROPENE 50 567 113

TRICHLOROETHENE 50 545 109

TRICHLOROFLUOROM ETHANE 1 50 658 132

VINYL CHLORIDE i 50 61 6 123

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

Sample File Name Date Acquired Time inj Analyst Matrix Method

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

MSSpk MSDSpk MS MSD MS MSD Recovery RPD Native Amount Amount Result Result REC REC Limits RPD Limit

CompounCompoundd NamNamee (ugL(ugL)) (ugL(ugL)) (ugL(ugL)) (ugL(ugL)) (ugL(ugL)) (()) () () () ()

2-CHLOROTOLUENE 0 50 50 163 586 ~ T 32 117 60-140 f 110 20 i

BROMOCHLOROMETHANE 0 50 50 214 62~2 j 43 124 60-140 ~ [ 98 20

UT-TRIMETHYLBENZENE 0 50 50 147 611 bull29 60-140 I 120 20

13-DICHLOROBENZENE 0 50 50 155 587 bull31 117 60-140 120 20

0 50 50 234 576 bull47 115 60-140 bull84 20 - 1 tl 4-DICHLOROBENZENE 0 50 50 152 571 bull30 114 60-140 bull120 20

1 2-DICHLOROETHENE(TRANS) 0 50 50 172 652 34 130 60-140 bull120 20 1

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

I2-D1CHLOROETHENE (CIS) 0 50 50 171 636 34 127 60-140 bull120 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

4-CHLOROTOLUENE 0 50 50 162 595 32 119 60-140 bull110 20 j

4-METHYL-2-PENTANONE 0 50 50 494 610 99 122 60-140 21 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

I I I 2-TETRACHLOROETHANE 0 50 r 50 170 580 bull34 116 60-140 bull110 20

22-DICHLOROPROPANE 0 50 50 140 630 ~ 28 126 60-140 | I30 20

1 23-TRICHLOROPROPANE 0 50 50 32 1 326 64 65 60-140 15 20 i

111-TRICHLOROETHANE 0 i 50 50 160 662 32 132 60-140 raquoI20 20

1122-TETRACHLOROETHANE 0 50 50 376 618 75 124 60-140 bull49 20

1 1 2-TRICHLOROETHANE 0 50 50 246 608 49 122 60-140 85 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

11-DICHLOROETHENE 0 50 50 165 666 r laquo33 133 60-140 120 20

1 2-DICHLOROPROPANE 0 50 50 178 567 bull36 113 60-140 bull100 20 1 7 1TRIPHI ORDRFN7FNF r 0 50 50 147 546 29 109 60-140 bull120 20

BROMODICHLOROMETHANE 0 50 50 187 590 bull37 118 60-140 bull100 20 j

1 24-TRICHLOROBENZENE 0 f~ 50 50 123 555 bull24 1 1 1 60-140 I30 20

1 24-TRIMETHYLBENZENE 0 50 50 147 614 29 j 123 60-140 bull120 20 I2-D1BROMO-3-CHLOROPROPANE 0 50 50 467 452 93 90 60-140 r 20 1 12-DIBROMOETHANE 0 50 50 294 505 bull59 60-140 53 20 |

12-DICHLOROBENZENE 0 50 50 176 593 bull35 118 60-140 bull110 20 12-DICHLOROETHANE 0 50 50 221 580 44 116 60-140 bull90 20

1 1 -DICHLOROPROPENE 0 50 50 130 472 26 94 60-140 bullno TERT-BUTYLBENZENE I 0 50 50 150 598 [ 30 120 60-140 bull120 20

BROMOBENZENE 0 50 50 181 577 36 60-140 IOO 20 _ _ 5

N-PROPYLBENZENE 0 50 50 154 575 31 115 60-140 I20~T 20

NAPHTHALENE 0 50 50 282 598 i 56 120 60-140 bull72 20 O-XYLENE 0 50 50 146 638 29 128 60-140 bull120 20

P-ISOPROPYLTOLUENE 50^ 50 128 S9S 26 120 60-140 bull130 20 1 -

METHYLENE CHLORIDE 0 50 50 149 480 30 96 60-140 bull100 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TETRACHLOROETHENE 0 50 50 133 531 27 06 60-140 120 20 laquo40 20TETRAHYDROFURAN 0 50~ 50 735 49~2 ] 147 98 60-140

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

RPD =[(ms res - msd res) (ms ibulles + msc1 res)2] 100 Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

MS Spk MSD Spk MS MSD MS MSD Recovery RPD Native Amount Amount Result Result REC REC Limits RPD Limit

Compound Name (ugL) (ugL) (ugL) (ugL) (ugL) () () () () () r2i9 ~ TRANS-U-D1CHLOROPROPENE 0 50 50 557 44 1 1 1 60-140 87 20

TRICHLOROETHENE 0 50 50 150 556 1 bull30 111 60-140 bull120 20

TRICHLOROFLUOROMETHANE 0 50 50 167 700 bull33 140 60-140 bull120 20 ISEC-BUTYLBENZENE 0 50 50 142 596 bull28 119 60-140 bull120 20 CIS-13-DICHLOROPROPENE 0 50 50 190 547 bull38 109 60-140 97 20

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

BROMOM ETHANE 0 50 50 145 564 bull29 113 60-140 laquo I 2 0 20 CARBON TETRACHLORIDE 0 50 50 164 629 bull33 60-140 bull120 20

CHLOROBENZENE 0 50 r 50 164 581 raquo33 116 60-130 110 20

CHLOROETHANE 0800 50 50 148 555 28 109 60-140 bull120 20

N-BUTYLBENZENE 50 50 122 591 bull24 | 118 60-140 bull130 20 L deg CHLOROMETHANE 235 50 50 161 950 28 bull185 60-140 140 20

VFNYL CHLORIDE 0 5deg 50 155 635 31 127 60-140 I20 20 I

DIBROMOCHLOROM ETHANE 0 50 50 226 595 bull45 119 60-140 90 20

DIBROMOM ETHANE 0 50 50 248 572 raquo50 114 60-140 79 20

DICHLOROD1FLUOROMETHANE 0 50 50 161 593 32 119 60-140 1 I O 20

ETHYLBENZENE 0 50 50 228 604 46 121 60-140 bull90 20

HEXACHLOROBUTADI ENE 0 50 50 828 403 bull16 81 60-140 bull130 20 ~20~

1SOPROPYLBENZENE 50 50 155 568 bull31 114 60-140 bull110 o CHLOROFORM 0 50 50 167 610 bull33 122 60-140 1 I O 20

RPD =[(ms res - msd res) (ms res + msd res)2] 100 Out of Limits

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Client Contact Phone FaxT^VA

vAJCX)CjCc fo ampbull C LJ VC~i t F^C^^OI ( 2c7)77q-ZZ Address ^J City state -- Zip Code S~Y~i ] C^7 Mix-T-ri^ltc JV FOT- U A M Purchase Order Pro] Name No ^-gtx- C C-tgt^O Vgt Katahdin Quote

Sampler (Print Sign) j S x - I mdash T lt- gti bullpoundgt vj (AI V Copies To

ANALYSIS AND CONTAINERTYPELAB USE ONLY WORKORDER JjQ^ - bull PRESERVATIVES

KATAHDIN PROJECT MANAGER Filt Filt Filt Filt Filt Filt Filt Filt Filt Filt OYON OYON OYON OYON OYON OYON OYON OYON OYON OYON

REMARKS

SHIPPING INFO O FED EX O UPS O CLIENT

AIRBILL NO

TEMP-C O TEMP BLANK O INTACT D NOT INTACT li|| Date Time No ofSample Description Matrix

colld Cntrs

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(VU)- 95-HR (sioo^3O I 1 |Yi6O-Q5-^Rb fcraquooc |5Do i a I MUgt13 fclOC((c730 ^

COMMENTS

Relinquished By (Sigrature) Date Time Received By (S gnajure) Relinquished By (Signature) Date Time Received By(Signature)

^JlW-^mdashlt faA-CD TCfevVraquoVlvi Af i bull Relinquished By- (Signature) Date Time Receive^JBy (Signature) Relinquished By (Signature) Date Time Received By (Signature)

ORMSOUFtCE INC TT (207) 782-3311 OHM CHN-OF-CSTDY

ORIGINAL Katahdin Analytical Services 0000043

Katahdin

June 162000

Mr Tom Eschner Woodard amp Curran 41 HutchinsDr Portland ME 04102

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Ka Ofe (no Authorized Signature Date

mi l mum R o i J N u - 2IOf[ RoidNo ltgt Portsmouth NHOVtOl I l l B gt 2(1 i M b r m i k M l ( gt 4 lt gt 1 gt S | id i2ir x 4 2-raquoilaquoi 11 i2nshy mdash- 4 gt gt

TECHNICAL NARRATIVE

3iO C ounty Road No 5 210 Wei Road No 5 PonsrMu1) NH 03801 Igt O Bo720 NXcstbrook ME 04093 Tel lt2ltTi 874-2400 Fax (207) 77i-4029

Imp k Tel (603 431-5777 Fax 603 436-3356

Vfcodard amp Curran PO No 9509303

WIC raquobull REPORT OF ANALYTICAL RESULTS Page 1 of 7

MW-95-5R Aqueous DDINSTORE 060200 060200

Iron Total 012 tngL 10 002 6010200 7 061200 EM 1

061600

340 County Road No 5 210 West Road No 5 Portsmouth NH 03801 PO Box 720 Wcsibrook ME 04098 http karahdmlab com Tel (603)431-5777 Fax (603)436-3356 Tel (207) 874 2400 Fax (20) 775 4029

Portland ME 04102

WICtt gt REPORT OF ANALYTICAL RESULTS Page 2 of 7

MW-95-4SA Aqueous DDINSMDRE 060200 060200

Iron Total 312 tngL 10 002 60102007 061200 EM 1

061600

LJOmrcajc(dw)

QF10ICWO

340 County Road No 5 210 Wlaquot Road No 5 Portsmouth NH 03801 PO Box 720 Wcstbroolt ME 04098 hup kacahdmlab com Tel (603)431 577 Fix (603) 436-3356 Tel (207)874-2400 Fax (207)7754029

Katahdin L S E R V I C E S

Portland ME 04102

MW-95-4SB Aqueous DDINSMORE 060200 060200

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

340CounryRoadNo 5 2IOlaquocst Roid No 5 Portsmouth NH 03801 PO Box 720 Wcstbrook ME 04098 hup katahdinlab com Tel 603)431 5777 Fax (6031 436-3356 Tel- (207) 874-2400 Fix (207) 775-4029

Portland ME 04102

WIC gt REPORT OF ANALYTICAL RESULTS Page 4 of 7

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

LJOtnrcajc (dw) QF10ICWO

340 Counrv Road No 5 PO Box 720 Wlaquobiook ME 04093 hitp kacahdmlab com

2 I O W laquo t RojdMo 5 PonsTiouth NH 03801 Tel (03) 43 i 5-77 Fax (603)436-3356

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

MR-97-13S2 Aqueous DDINSMORE 060200 060200

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

Manganese Total 0 778 mgL 1 0 00050 6010200 7 061200 EM 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sample-specific reporting limits Sanple-specific limits are indicated by results annotated with lt values

061600

340 County Road No 5 2 10 West Road No 5 Portsmouth NH 03801 PO Box 720 Wlaquotbroolc ME 04098 hup katahdmlab com Tel (603)431 57^7 FJX (603 436-3356 Tel (207) 874-2400 Fax (207) 7^5-4029

CLIENT TOM ESCHNER Report Date 061600 Woodard amp Curran PO No 9509303

Portland ME 04102

WICtf gtbull REPORT OF ANALYTICAL RESULTS Page 6 of 7

Arsenic Total 0880 mgL 1 0 0008 6010200 7 061200 EM 1 Iron Total 82 1 rngL 1 0 002 6010200 7 061200 EM 1 Manganese Total 128 mgL 1 0 00050 6010200 7 061200 EM 1

061600

340 County Road No 5 210 West Road No 5 Pommouih NH 03801 PO Bot 20 Wesibrook ME 04098 hc(p kaiahdmlab com Tel (603)431-5777 Fax (603)436-3356 Tel (207)874-2400 Fax (207) 775 4029

CLIENT TOM ESCHNER

Wocdard amp Curran 41 Hutchins Dr Portland ME 04102

Lab Number WQ-1589-7 Report Date 061600

PO No 9509303 Project SACO LF

EB-1 Aqueous DDINSMDRE 060200 060200

Arsenic Total lt0005 mgL 10 0008 60102007 061200 EM 1

Iron Total lt002 mgL 10 002 60102007 061200 EM 1

061600

340 County Road No 5 210 West Road No 3 Porumouth NH 03801 PO Box 720 Wcstbrook ME 04098 h(tp Vkjcihctinlib com Tel (603) 431-5777 Fix (603) 43Cgt-33S6 Tel (207) 8~4-2400 Fix 1207) 775-4029

rCatahdinimHybiBitiiiui PREPARATION BLANK REPORT

ALUMINUM 002 mgL J 010 AQF12A ANTIMONY 0002 mgL U 0008 AQF12A

BARIUM 00003 mgL u 00050 AQF12A

BERYLLIUM 00002 mgL J 00050 AQF12A BORON 0002 mgL J 0100 AQF12A CADMIUM 00003 mgL u 00100 AQF12A CALCIUM 0006 mgL u 0050 AQF12A CHROMIUM 00007 mgL u 00150 AQF12A COBALT 00007 mgL u 00300 AQF12A COPPER 0002 mgL u 0025 AQF12A IRON 002 mgL u 002 AQF12A LEAD 0001 mgL u 0005 AQF12A MAGNESIUM 0006 mgL u 0050 AQF12A MANGANESE 00002 mgL u 00050 AQF12A MOLYBDENUM 0001 mgL u 0100 AQF12A NICKEL 0001 mgL u 0040 AQF12A SELENIUM 0003 mgL u 0010 AQF12A SILVER 0001 mgL u 0015 AQF12A STRONTIUM 000007 mgL u 0100 AQF12A THALLIUM 0003 mgL u 0015 AQF12A TIN 0002 mgL u 0100 AQF12A TITANRJM 00004 mgL u 00150 AQF12A VANADIUM 00009 mgL u 00250 AQF12A ZINC 00014 mgL J 00250 AQF12A

Sample ID LCSWQF10ICWO Batch ED QF10ICWO

ALUMINUM 200 176 mgL 880 80 120 AQF12A ANTIMONY 0500 0512 mgL 1024 80 120 AQF12A ARSENIC 200 211 mgL 1055 80 120 AQF12A BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A TITANIUM 100 104 mgL 1040 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

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340 County Road Mo 5 CHAIN of CUSTODY PO Box 720 Westbrook ME 04092 Tel (207) 874-2400 Fax(207)775-4029 PLEASE PRINT IN PEN Page of

Client Contact ^0 Phone Fax

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VNAIVSIS AND CONTAINER TYPE LAB USE ONLY WORK ORDER ^Qi^g^ bull PRESERVATIVES

KATAHDIN PROJECT MANAGER Filt Filt Filt Filt Filt Filt Filt Filt Filt Filt QYON OYON OYON OYON OYON OYON OYON OYON OYON OYON

REMARKS

SHIPPING INFO D FED EX O UPS D CLIENT lt

lt -J AIRBILL NO s TEMPdegC O TEMP BLANK D INTACT 3 NOT INTACT 1

- ltN Date Time No of Sample Description Matrix colld Cntrs -lt

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COMMENTS

^ flelinquishedBy (Signature) Date Time Received By (Signature) Relinquished By (Signature) Date T ime Received By (Signature)

tTuAJl^ prft^amp-r~l^P qfeamp 1530 ^^^lt^^

OHMSOUnCEINC laquo (207)782-3311 -OHM t CHN-OF-CSTDV

Services 0000013

rCatahdin I I c A I S K R V I C ES

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

t(o f 00 Authorized Signature Date

lt-)(K ouim R jj No S 210 NXoi Road No i Portsmouth NHO801 I O Box ~raquo i s t h r o i k M l (MI )S 7el i6l)^gt 4M 5^^ hn 60l 4V n j- illjuil lh tn IJ Uin x~ i l-nraquo H (2ir gt icij i

TECHNICAL NARRATIVE

340 Coimcv Road No 5 210 Wat Road No 5 Portsmouth NH 0380] PO Bo 20 Wesibrool ME 04098 Tel (207) 8H 24PO Fax (207 775-4029

Imp Lar ihdmlib com Tel (603) 431-5777 Fix (603) 436-3356

Lab Number WQ-1550-1 CLIENT TOM ESCHNER Report Date 061S00

Arsenic Total 0183 mgL 10 0008 60102007 061000 KD 1 Iron Total 003 mgL 10 002 60102007 061000 KD 1 Manganese Total 0219 mgL 10 00050 60102007 060900 EM 1

061600

LJOmrcajc(dw) QF07ICW2

340 County Road No 5 210 West Road No 5 Portsmouth NH 03801 PO Box 720 Wcstbrook ME 04098 Td (603) 431-5777 Fax (603) 436-3356 htrp karahdmlab com Tel- (207) 874-2400 Fax (207) 775-4029

Lab Number H3-1550-2 CLIENT TOM ESCHNER Report Date 061600

Wbodard amp Curran PO No 9509303 41 Hutchins Dr Project SAGO LF Portland ME 04102

Arsenic Total lt0005 mgL 10 0008 60102007 061000 KD 1 Iron Total 028 mgL 10 002 60102007 061000 KD 1 Manganese Total 00091 mgL 10 00050 60102007 060900 EM 1

061600

340CoiuityRoidNo 5 210 Wot Read No 5 Portsmouth NH 03801 P O Box 720 Wcstbrook ME 04098 hirp katahdmlab com Td (603) 431-5777 Fa (603) 436-3356 Tel (207) 874-2400 Flaquo (207) 775-4029

Wbodard amp Curran PO No 9509303 41 Hutchins Dr Project SAQO LF

Portland ME 04102

MW-95-8SDUP Aqueous DDINSMORE OS3100 053100

Arsenic Total lt0005 trgL 10 0008 60102007 061000 KD 1

Iron Total 026 mgL 10 002 60102007 061000 KD 1

Manganese Total 00091 itgL 10 00050 60102007 060900 EM 1

PQL (Practical Quantitation Level) represents laboratory reporting limits and may not reflect sarrpleshyspecific reporting limits Sample-specific limits are indicated by results annotated with lt values

061600

340 County Road No 5 210 Wlaquo Road No 5 Portsmouth NH 03801 PO Box 720 Wcstbrook ME 04098 Tel (603) 431-5777 fir (603) 436-3356 htrpkjtahdinlab com Tel (207) 874-2400 Fax (207) 775-4029

Lab Number WQ-1550-4 CLIENT TDM ESCHNER Report Date 061600

Arsenic Total lt0 005 mgL 1 0 0008 6010200 7 061000 KD 1 Iron Total 0 18 mgL 1 0 002 6010200 7 061000 KD 1 Manganese Total 0 0058 mgL 10 00050 6010200 7 060900 EM 1

061600

LJOmrcaj c(dw) QF07ICW2

340 Counry Road No 5 210 Wet Road No 5 Portsmouth NH 03801 PO Box 720 Wcstbrook ME 04098 Tel (603) 431-5777 Fax- (603) 436-3356 hcrpkatahdmlab com Tel (207) 874-2400 fix (207) 775-4029

Portland ME 04102

MW-95-9S Aqueous DDTNSMORE 053100 053100

Arsenic Total lt0005 mgL 10 0008 60102007 061000 KD 1

Iron Total 030 tngL 10 002 60102007 061000 KD 1

061600

LJDmrcajc (dw) QF07ICW2

340 County Road No 5 210 West Road No 5 Portsmouth NH 03801 PO Box 720 Westbrook ME 04098 Tel (603) 431-5777 Fa (603) 436-3356 hupkauhdgtnlab com Tel (207) 874-2400 FM (207) 775-4029

Woodard amp Curran PO No 9509303 41 Hutchins Dr Project SACO LF Portland MB 04102

Arsenic Total 0111 mgL 10 0008 6010200 7 061000 KD 1 Iron Total 196 mgL 10 002 6010200 7 061000 KD 1 Manganese Total 670 tngL 10 00050 6010200 7 060900 EM 1

061600

340 County Road No 5 210WestRoadNo 5 PoramoiuhNH 03801 PO Box 720 Wtsibrook ME 04098 hrrpkarahdinlabcoin Td (603) 431-5777 Fax (603) 436-3356 Tel (207) 874-2400 Fax (207) 775-4029

Wcodard amp Curran PO No 9509303 41 Hutchins Dr Project SACO LF Portland ME 04102

MW-97-14S1 Aqueous DDTNSMORE 053100 053100

Arsenic Total 0181 mgL 10 0008 60102007 061000 KD 1 Iron Total 155 tngL 10 002 60102007 061000 KD 1 Manganese Total 140 mgL 10 00050 60102007 060900 EM 1

061600

340 County Road No 5 210 West Road No 5 Poromouch NH 03801 P O Box 720 Westbroolc ME 04098 Tel (603) 431-5777 Fix (603) 436-3356 Tel (207) 874 2400 Fax (207) 775-4029

hlrp kacahdmlab com

iKatahdin A N M V T I C M sEsis~m^mm^g^mgm^mgm

Sample ID PBWQF07ICW2 Batch ID QF07ICW2

BARIUM 00020 mgL J 00050 BQF08A

COBALT 0003 mgL U 0030 BQF08A

COPPER 0002 mgL U 0025 AQF09A

IRON 0003 mgL U 0025 BQF08A

NICKEL 002 mgL J 004 BQF08A

STRONTIUM 000007 mgL U 0100 AQF09A

U The anaJyte was not delected in the sample at a level greater than the instrument detection limit

Katahdin A N A L Y T I C A L ^ TT^jfjff^fffffffffffgfffgfffff

Sample ED LCSWQF07ICW2 Batch ID QF07ICW2

Element Name True Value Result Units Recovery() Flag Limits() File

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

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340 County Road No 5 PO Box 720 CHAIN of CUSTODY Katahdin Westbrook ME 04091 Tel (207) 874-2400 Fax (207) 775-4029 PLEASE PRINT IN PEN Page of

Client

Address

Purchase Order

Bill (if different than above)

REMARKS

SHIPPING INFO D FED EX

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

City State ZpCode 04I02 Proj Katahdin Quote

Address

Filt Fill Filt Filt Filt Filt Filt 3YON OYON OYONOYON OYON OYONOYON OYON OYON OYON

O UPS O CLIENT

O INTACT O NOT INTACT

Date Time No of Matrix colld Cntrs

-J Relinquished By (Signature) Date Time Received By (Sanakjre) Relinquished By (Signature) Date Time Received By (Signature)

Relinquished By (Signature) Date Time Received By (S gnature) Relinquished By (Signature) Date Time Received By (Signature)

5RMSOURCE INC laquo 207) 782-3311 gtRM raquo CHN-OF-CSTDr

barcode 6862

barcodetext SDMS Doc ID 6862

WOODARD ampCURRAN L i rvnopt inr) Snence bull Opdegiations

Metals Surface WaterSediments Surface water and sediment samples were collected from Sandy Brook on June 5 2000 All samples were analyzed for arsenic iron and manganese within EPA required holding times (6 months) Laboratory control samples had percent recoveries that were within acceptance limits for all target elements Duplicate surface water and sediment samples were collected at SWSD-103 and SWSD-52 The duplicate surface water samples compared well with relative percent difference (RPD) values below the EPA maximum of 30 For the sediment samples duplicate results for SD-103 were below the EPA maximum of 50 for all target elements However for the duplicate samples collected at SD-52 the RPD exceeded the EPA maximum for all target elements indicating that concentrations were not evenly dispersed throughout the matrix Matrix spike results for the surface water sample SW-103 was in compliance for all target elements For the sediment sample SD-103 non shycompliant matrix spike results were observed for iron and manganese Non-compliant matrix spike results were obtained due to spike concentrations added to the sample which were very low compared with the native concentrations already measured in the sample The spiked concentrations added to the sample were swallowed up by the high concentrations already present in the sample Preparation blanks were non-detect for target elements with the exception of trace levels of iron detected in one blank The iron detection in the blank had no effect on reported sample concentrations since sample concentrations were much greater than the associated action level

Metals Groundwater Groundwater samples were collected at Saco Landfill from May 30 to June 2 2000 All samples were analyzed within the EPA holding time limit of 6 months Laboratory control sample recoveries were acceptable for all target elements Duplicate results were collected at MW-95shy7S MW-95-1S and MW-95-8S Results for all duplicates compared well with RPDs below 30 for all elements in every pair Matrix spike results were acceptable for all elements indicating that matrix interferences were not likely Trace levels of iron at 0004 mgL were detected in preparation blanks Using the 5X rule (USEPA 1988) an action level of 002 mgL would have been established As a result reported concentrations of iron for MW-93-3 and MW-97-16S would have been qualified as non-detect during the validation process

VOAs Groundwater Three groundwater samples MW-95-1S MW-95-4RD and MW-13 were analyzed for VOAs using USEPA 8260 All samples were analyzed with EPA holding time limit of 14 days Laboratory control recoveries were acceptable for all target VOAs A field duplicate sample was collected at MW-95-1S The RPD between results was acceptable for all compounds except chloromethane (2 ugL in sample vs 25 ugL in duplicate) Matrix spike analysis was performed on MW-95-1S Matrix spike recoveries were below the minimum EPA acceptance limit of 60 for the majority of the target VOAs indicating possible matrix interference The matrix spike duplicate recoveries were in control for all VOAs so the interference indicated by the initial matrix spike results was not confirmed The method blank and trip blank each had methylene chloride detections of I MgL The blank data indicate that positive detections of methylene chloride in samples may be representative of laboratory contamination

O 95093Fall 1999samplmgreportcover letter

Findings

Sincerely

Table 1

Saco Maine

Area 2

Areas 3 and 4

Table 1

LOCATION

111996 62498 10198 61099 61099

111999 111999

6500 61099

111999 6500

111795 62498 62498 10198 61099

111999 6500

61099 111999

6500 111795 111996 10198 61099

111999 6500

62498 10198 61099

111999 6500

111999 61099 61099 61099 61099

111999 61099

111795 111999 111999

Manganese (ugL)

1940 1300 1280 668 671 913

1350 704 938 239

448 1150 634 788 816 427 670 151 381

299 769 274 118

244 762 352 509 367 772 778 756 787 387 794 89

374 288 474

Iron (ugL)

12000 2370

3980 3850 2010 2010 3120 4990 1890 3370 1750 1760 1720

2450 1760 2870 1350 827 153 863

1260 601 410

1100 684

1160 652

1150 1050 1020 1020 669

1020 677 621 658

Table 1

Saco Maine

Iron (mgKg)

Manganese (mgKg)

B = estimated

Table2sedxls 72700

Location

Sample Date

11171995 05161996 11191996 06241998 06101999 11191999 06052000 11171995 11171995 05161996 05161996 11191996 06241998 06101999 11191999

Sample Type

Duplicate Primary

Arsenic (mgKg)

45 2 1

5 1 5 45

22J 22J 35 47 34 45

Iron (mgKg)

10500J 9420 9410

10100B 21600 5760 12300 4700J 5160 8740

10900 9080

10300B 6040

Manganese (mgKg)

329J 137 139 NA

1500 255 217

76 3J 91 8J

230 305 221 NA

277 202

Table2sed xls 72700

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Saco Maine

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

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REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

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131 i5 1 - 1 1 i i 8 1 g pound w

If i a

m laquogt r- z z

REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

Al 0 1 UJo

3 a u_ LL ~~~

Q3t gt

j iUJ 5sr LU rshy

1 Q o gt_

JJ gt ^ CO

o m ^ m

a a a a a

a a a a O L_

(O deg

UJ _l a o a

REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

V) | UJ

6- o a5 KI

Q O^ y_= (S

a cc ||s^| s

a g n|

5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

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bulli s s i

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bulloII raquo

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SI CQ ^

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Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

Findings

Sincerely

Table 1

Saco Maine

Area 2

Areas 3 and 4

Table 1

LOCATION

111996 62498 10198 61099 61099

111999 111999

6500 61099

111999 6500

111795 62498 62498 10198 61099

111999 6500

61099 111999

6500 111795 111996 10198 61099

111999 6500

62498 10198 61099

111999 6500

111999 61099 61099 61099 61099

111999 61099

111795 111999 111999

Manganese (ugL)

1940 1300 1280 668 671 913

1350 704 938 239

448 1150 634 788 816 427 670 151 381

299 769 274 118

244 762 352 509 367 772 778 756 787 387 794 89

374 288 474

Iron (ugL)

12000 2370

3980 3850 2010 2010 3120 4990 1890 3370 1750 1760 1720

2450 1760 2870 1350 827 153 863

1260 601 410

1100 684

1160 652

1150 1050 1020 1020 669

1020 677 621 658

Table 1

Saco Maine

Iron (mgKg)

Manganese (mgKg)

B = estimated

Table2sedxls 72700

Location

Sample Date

11171995 05161996 11191996 06241998 06101999 11191999 06052000 11171995 11171995 05161996 05161996 11191996 06241998 06101999 11191999

Sample Type

Duplicate Primary

Arsenic (mgKg)

45 2 1

5 1 5 45

22J 22J 35 47 34 45

Iron (mgKg)

10500J 9420 9410

10100B 21600 5760 12300 4700J 5160 8740

10900 9080

10300B 6040

Manganese (mgKg)

329J 137 139 NA

1500 255 217

76 3J 91 8J

230 305 221 NA

277 202

Table2sed xls 72700

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ii ^ in n g Q

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= o J -3 -3 -3 j LL en v

in o u

mdash Q

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magt i

Q_ 5 I i5

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panlaquo

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CQ1shy

Saco Maine

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

ltu ca

-2laquo=a 3a

laquo S

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^ o -H S u A

bullshy 2 bull= 73

pound=shy

M a OO

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bulld trade

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bullo S

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pound Qo O ci

o lt II fc ^

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UJ ltD ra

rv ^ u

g fe a a a B a an 1

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dditio

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secta n

REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

laquo C UJ 1t

CO UJ 4gt

0 ui g 1v 0

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Q o UJ m

jUJ 8 o

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00 ^ P ^

131 i5 1 - 1 1 i i 8 1 g pound w

If i a

m laquogt r- z z

REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

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REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

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6- o a5 KI

Q O^ y_= (S

a cc ||s^| s

a g n|

5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

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Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

Table 1

Saco Maine

Area 2

Areas 3 and 4

Table 1

LOCATION

111996 62498 10198 61099 61099

111999 111999

6500 61099

111999 6500

111795 62498 62498 10198 61099

111999 6500

61099 111999

6500 111795 111996 10198 61099

111999 6500

62498 10198 61099

111999 6500

111999 61099 61099 61099 61099

111999 61099

111795 111999 111999

Manganese (ugL)

1940 1300 1280 668 671 913

1350 704 938 239

448 1150 634 788 816 427 670 151 381

299 769 274 118

244 762 352 509 367 772 778 756 787 387 794 89

374 288 474

Iron (ugL)

12000 2370

3980 3850 2010 2010 3120 4990 1890 3370 1750 1760 1720

2450 1760 2870 1350 827 153 863

1260 601 410

1100 684

1160 652

1150 1050 1020 1020 669

1020 677 621 658

Table 1

Saco Maine

Iron (mgKg)

Manganese (mgKg)

B = estimated

Table2sedxls 72700

Location

Sample Date

11171995 05161996 11191996 06241998 06101999 11191999 06052000 11171995 11171995 05161996 05161996 11191996 06241998 06101999 11191999

Sample Type

Duplicate Primary

Arsenic (mgKg)

45 2 1

5 1 5 45

22J 22J 35 47 34 45

Iron (mgKg)

10500J 9420 9410

10100B 21600 5760 12300 4700J 5160 8740

10900 9080

10300B 6040

Manganese (mgKg)

329J 137 139 NA

1500 255 217

76 3J 91 8J

230 305 221 NA

277 202

Table2sed xls 72700

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in CO E^

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10 cfi Q 1

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in01 Si E

S 5 Q poundif

ii ^ in n g Q

agtlaquo 7 v S

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= o J -3 -3 -3 j LL en v

in o u

mdash Q

J2 CJ Cl in J in

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magt i

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panlaquo

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CQ1shy

Saco Maine

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

ltu ca

-2laquo=a 3a

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REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

laquo C UJ 1t

CO UJ 4gt

0 ui g 1v 0

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jUJ 8 o

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00 ^ P ^

131 i5 1 - 1 1 i i 8 1 g pound w

If i a

m laquogt r- z z

REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

Al 0 1 UJo

3 a u_ LL ~~~

Q3t gt

j iUJ 5sr LU rshy

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a a a a O L_

(O deg

UJ _l a o a

REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

V) | UJ

6- o a5 KI

Q O^ y_= (S

a cc ||s^| s

a g n|

5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

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bulloII raquo

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SI CQ ^

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Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

Table 1

LOCATION

111996 62498 10198 61099 61099

111999 111999

6500 61099

111999 6500

111795 62498 62498 10198 61099

111999 6500

61099 111999

6500 111795 111996 10198 61099

111999 6500

62498 10198 61099

111999 6500

111999 61099 61099 61099 61099

111999 61099

111795 111999 111999

Manganese (ugL)

1940 1300 1280 668 671 913

1350 704 938 239

448 1150 634 788 816 427 670 151 381

299 769 274 118

244 762 352 509 367 772 778 756 787 387 794 89

374 288 474

Iron (ugL)

12000 2370

3980 3850 2010 2010 3120 4990 1890 3370 1750 1760 1720

2450 1760 2870 1350 827 153 863

1260 601 410

1100 684

1160 652

1150 1050 1020 1020 669

1020 677 621 658

Table 1

Saco Maine

Iron (mgKg)

Manganese (mgKg)

B = estimated

Table2sedxls 72700

Location

Sample Date

11171995 05161996 11191996 06241998 06101999 11191999 06052000 11171995 11171995 05161996 05161996 11191996 06241998 06101999 11191999

Sample Type

Duplicate Primary

Arsenic (mgKg)

45 2 1

5 1 5 45

22J 22J 35 47 34 45

Iron (mgKg)

10500J 9420 9410

10100B 21600 5760 12300 4700J 5160 8740

10900 9080

10300B 6040

Manganese (mgKg)

329J 137 139 NA

1500 255 217

76 3J 91 8J

230 305 221 NA

277 202

Table2sed xls 72700

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in CO E^

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in01 Si E

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ii ^ in n g Q

agtlaquo 7 v S

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= o J -3 -3 -3 j LL en v

in o u

mdash Q

J2 CJ Cl in J in

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magt i

Q_ 5 I i5

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panlaquo

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CQ1shy

Saco Maine

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

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REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

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CO UJ 4gt

0 ui g 1v 0

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00 ^ P ^

131 i5 1 - 1 1 i i 8 1 g pound w

If i a

m laquogt r- z z

REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

Al 0 1 UJo

3 a u_ LL ~~~

Q3t gt

j iUJ 5sr LU rshy

1 Q o gt_

JJ gt ^ CO

o m ^ m

a a a a a

a a a a O L_

(O deg

UJ _l a o a

REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

V) | UJ

6- o a5 KI

Q O^ y_= (S

a cc ||s^| s

a g n|

5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

pound asgt 3

bulli s s i

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f= CK r~J ( XMI

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bull ^ v y

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f_fl o

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bulloII raquo

dditio

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SI CQ ^

k If r

Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

Table 1

Saco Maine

Iron (mgKg)

Manganese (mgKg)

B = estimated

Table2sedxls 72700

Location

Sample Date

11171995 05161996 11191996 06241998 06101999 11191999 06052000 11171995 11171995 05161996 05161996 11191996 06241998 06101999 11191999

Sample Type

Duplicate Primary

Arsenic (mgKg)

45 2 1

5 1 5 45

22J 22J 35 47 34 45

Iron (mgKg)

10500J 9420 9410

10100B 21600 5760 12300 4700J 5160 8740

10900 9080

10300B 6040

Manganese (mgKg)

329J 137 139 NA

1500 255 217

76 3J 91 8J

230 305 221 NA

277 202

Table2sed xls 72700

in en S E

rr CD en 5I

en ^mdash n gt

in CO E^

0shyc 5

n rl 0

10 cfi Q 1

z pound 2 O

in01 Si E

S 5 Q poundif

ii ^ in n g Q

agtlaquo 7 v S

SO) o ^gt - Q

= o J -3 -3 -3 j LL en v

in o u

mdash Q

J2 CJ Cl in J in

in S CO

magt i

Q_ 5 I i5

m S S c

panlaquo

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CQ1shy

Saco Maine

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

ltu ca

-2laquo=a 3a

laquo S

s ^ ^ ^ so _ bull o 00 O 00

^ o -H S u A

bullshy 2 bull= 73

pound=shy

M a OO

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bulld trade

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bullo S

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pound Qo O ci

o lt II fc ^

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UJ ltD ra

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dditio

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REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

laquo C UJ 1t

CO UJ 4gt

0 ui g 1v 0

C eurof

II h~ ws i

Q o UJ m

jUJ 8 o

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00 ^ P ^

131 i5 1 - 1 1 i i 8 1 g pound w

If i a

m laquogt r- z z

REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

Al 0 1 UJo

3 a u_ LL ~~~

Q3t gt

j iUJ 5sr LU rshy

1 Q o gt_

JJ gt ^ CO

o m ^ m

a a a a a

a a a a O L_

(O deg

UJ _l a o a

REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

V) | UJ

6- o a5 KI

Q O^ y_= (S

a cc ||s^| s

a g n|

5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

pound asgt 3

bulli s s i

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Slaquo

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P C O 1 9

vgt OT 2 cv V CC v^

j fa 2 k U- Ushy

5 |CO 3 O O

NilsOL

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f= CK r~J ( XMI

2 1 88 O

UJ O O bull

o en w z LU o IJL

bull ^ v y

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f_fl o

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bulloII raquo

dditio

~ c poundbull1

SI CQ ^

k If r

Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

Iron (mgKg)

Manganese (mgKg)

B = estimated

Table2sedxls 72700

Location

Sample Date

11171995 05161996 11191996 06241998 06101999 11191999 06052000 11171995 11171995 05161996 05161996 11191996 06241998 06101999 11191999

Sample Type

Duplicate Primary

Arsenic (mgKg)

45 2 1

5 1 5 45

22J 22J 35 47 34 45

Iron (mgKg)

10500J 9420 9410

10100B 21600 5760 12300 4700J 5160 8740

10900 9080

10300B 6040

Manganese (mgKg)

329J 137 139 NA

1500 255 217

76 3J 91 8J

230 305 221 NA

277 202

Table2sed xls 72700

in en S E

rr CD en 5I

en ^mdash n gt

in CO E^

0shyc 5

n rl 0

10 cfi Q 1

z pound 2 O

in01 Si E

S 5 Q poundif

ii ^ in n g Q

agtlaquo 7 v S

SO) o ^gt - Q

= o J -3 -3 -3 j LL en v

in o u

mdash Q

J2 CJ Cl in J in

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magt i

Q_ 5 I i5

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panlaquo

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CQ1shy

Saco Maine

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

ltu ca

-2laquo=a 3a

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^ o -H S u A

bullshy 2 bull= 73

pound=shy

M a OO

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I ca 4gt

2 e H 4gt

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bulld trade

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a S gtgt A

bullo S

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_ampgtbull

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pound Qo O ci

o lt II fc ^

o o o lt5 w ^ a

UJ ltD ra

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g fe a a a B a an 1

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dditio

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REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

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CO UJ 4gt

0 ui g 1v 0

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II h~ ws i

Q o UJ m

jUJ 8 o

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I ^ ce

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mdash ui

I a 0 c_ c~ S

3 (_) f j ^ ^ Oi t S w S

00 ^ P ^

131 i5 1 - 1 1 i i 8 1 g pound w

If i a

m laquogt r- z z

REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

Al 0 1 UJo

3 a u_ LL ~~~

Q3t gt

j iUJ 5sr LU rshy

1 Q o gt_

JJ gt ^ CO

o m ^ m

a a a a a

a a a a O L_

(O deg

UJ _l a o a

REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

V) | UJ

6- o a5 KI

Q O^ y_= (S

a cc ||s^| s

a g n|

5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

pound asgt 3

bulli s s i

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S bull -

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Slaquo

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laquoi ^ lt n S

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mdashbullbull vo o

X ex bull5 a

g-L6 ID 1

P C O 1 9

vgt OT 2 cv V CC v^

j fa 2 k U- Ushy

5 |CO 3 O O

NilsOL

I ttill

Ill CO tr CC Lu lt-

f= CK r~J ( XMI

2 1 88 O

UJ O O bull

o en w z LU o IJL

bull ^ v y

^ LU X

O cv q pound S ii

f_fl o

O H l U 0 deg ^ ^ - ^ ^

il 5 0

5 tv S ^

I amp 1S o

s Jf g

bulloII raquo

dditio

~ c poundbull1

SI CQ ^

k If r

Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

Location

Sample Date

11171995 05161996 11191996 06241998 06101999 11191999 06052000 11171995 11171995 05161996 05161996 11191996 06241998 06101999 11191999

Sample Type

Duplicate Primary

Arsenic (mgKg)

45 2 1

5 1 5 45

22J 22J 35 47 34 45

Iron (mgKg)

10500J 9420 9410

10100B 21600 5760 12300 4700J 5160 8740

10900 9080

10300B 6040

Manganese (mgKg)

329J 137 139 NA

1500 255 217

76 3J 91 8J

230 305 221 NA

277 202

Table2sed xls 72700

in en S E

rr CD en 5I

en ^mdash n gt

in CO E^

0shyc 5

n rl 0

10 cfi Q 1

z pound 2 O

in01 Si E

S 5 Q poundif

ii ^ in n g Q

agtlaquo 7 v S

SO) o ^gt - Q

= o J -3 -3 -3 j LL en v

in o u

mdash Q

J2 CJ Cl in J in

in S CO

magt i

Q_ 5 I i5

m S S c

panlaquo

iN agt CD

| O ui

c Qgt HI

CQ1shy

Saco Maine

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

ltu ca

-2laquo=a 3a

laquo S

s ^ ^ ^ so _ bull o 00 O 00

^ o -H S u A

bullshy 2 bull= 73

pound=shy

M a OO

S 13 a -o

ob ab ab S E E

O oo O o gtn O ^

8 O ra

-o u C5

bullo pound sect

s bullo

I ca 4gt

2 e H 4gt

ibullo bulla u c V

bulld trade

11 1 1

^ Vbullo 5 3 O lt)

a S gtgt A

bullo S

o xP 0^ r^j m ogt

_ampgtbull

I ^ lt u oo oo

r~ r^ 00 ltN 00

laquo o

3 oR c

jjS S3

rr rr m r-

C _ IIlaquobull u

8 I b l2 o I

(N mdash ltN mdash

111 2H -s

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mdash ^_ bullz 2Q

^5 | |J

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Q O gt- _i o C

OO a 0

--1 Q- o ow a a a _i _i | |

pound Qo O ci

o lt II fc ^

o o o lt5 w ^ a

UJ ltD ra

rv ^ u

g fe a a a B a an 1

o tff raquo laquo^

LJJ pound Ss

dditio

s Ul M Sa pound

jut R v 0 or

4laquoC

figt 9Z

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secta n

REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

laquo C UJ 1t

CO UJ 4gt

0 ui g 1v 0

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II h~ ws i

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00 ^ P ^

131 i5 1 - 1 1 i i 8 1 g pound w

If i a

m laquogt r- z z

REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

Al 0 1 UJo

3 a u_ LL ~~~

Q3t gt

j iUJ 5sr LU rshy

1 Q o gt_

JJ gt ^ CO

o m ^ m

a a a a a

a a a a O L_

(O deg

UJ _l a o a

REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

V) | UJ

6- o a5 KI

Q O^ y_= (S

a cc ||s^| s

a g n|

5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

pound asgt 3

bulli s s i

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Slaquo

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laquoi ^ lt n S

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g-L6 ID 1

P C O 1 9

vgt OT 2 cv V CC v^

j fa 2 k U- Ushy

5 |CO 3 O O

NilsOL

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f= CK r~J ( XMI

2 1 88 O

UJ O O bull

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bull ^ v y

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f_fl o

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bulloII raquo

dditio

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SI CQ ^

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Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

in en S E

rr CD en 5I

en ^mdash n gt

in CO E^

0shyc 5

n rl 0

10 cfi Q 1

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in01 Si E

S 5 Q poundif

ii ^ in n g Q

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mdash Q

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CQ1shy

Saco Maine

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

ltu ca

-2laquo=a 3a

laquo S

s ^ ^ ^ so _ bull o 00 O 00

^ o -H S u A

bullshy 2 bull= 73

pound=shy

M a OO

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_ampgtbull

I ^ lt u oo oo

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dditio

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REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

laquo C UJ 1t

CO UJ 4gt

0 ui g 1v 0

C eurof

II h~ ws i

Q o UJ m

jUJ 8 o

J Tgt gti a

o 9 TJ -I

val w(

^23 si t

v V ^ if h- E-S z

I ^ ce

O c~ lt ^ iD ^_ O ~o 0) 19 uj y0 M o

mdash ui

I a 0 c_ c~ S

3 (_) f j ^ ^ Oi t S w S

00 ^ P ^

131 i5 1 - 1 1 i i 8 1 g pound w

If i a

m laquogt r- z z

REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

Al 0 1 UJo

3 a u_ LL ~~~

Q3t gt

j iUJ 5sr LU rshy

1 Q o gt_

JJ gt ^ CO

o m ^ m

a a a a a

a a a a O L_

(O deg

UJ _l a o a

REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

V) | UJ

6- o a5 KI

Q O^ y_= (S

a cc ||s^| s

a g n|

5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

pound asgt 3

bulli s s i

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os mdash

S bull -

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Slaquo

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laquoi ^ lt n S

OS r-1 cs

mdashbullbull vo o

X ex bull5 a

g-L6 ID 1

P C O 1 9

vgt OT 2 cv V CC v^

j fa 2 k U- Ushy

5 |CO 3 O O

NilsOL

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Ill CO tr CC Lu lt-

f= CK r~J ( XMI

2 1 88 O

UJ O O bull

o en w z LU o IJL

bull ^ v y

^ LU X

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f_fl o

O H l U 0 deg ^ ^ - ^ ^

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5 tv S ^

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bulloII raquo

dditio

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SI CQ ^

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Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

Saco Maine

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

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UJ ltD ra

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REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

laquo C UJ 1t

CO UJ 4gt

0 ui g 1v 0

C eurof

II h~ ws i

Q o UJ m

jUJ 8 o

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mdash ui

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3 (_) f j ^ ^ Oi t S w S

00 ^ P ^

131 i5 1 - 1 1 i i 8 1 g pound w

If i a

m laquogt r- z z

REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

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3 a u_ LL ~~~

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j iUJ 5sr LU rshy

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(O deg

UJ _l a o a

REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

V) | UJ

6- o a5 KI

Q O^ y_= (S

a cc ||s^| s

a g n|

5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

pound asgt 3

bulli s s i

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Slaquo

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laquoi ^ lt n S

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g-L6 ID 1

P C O 1 9

vgt OT 2 cv V CC v^

j fa 2 k U- Ushy

5 |CO 3 O O

NilsOL

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Ill CO tr CC Lu lt-

f= CK r~J ( XMI

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UJ O O bull

o en w z LU o IJL

bull ^ v y

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f_fl o

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bulloII raquo

dditio

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SI CQ ^

k If r

Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

SEEP AREA

LANDFILL PERIMETER

SEEP AREA

ATTACHMENT 1

REPORT OF ANALYSIS

July 7 2000

Dear Mr Eschner

Sincerely

i CM (A poundX- L- 0 7 0 7 0 0

Katahdin

June 22 2000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062200

Tel (20^) 8^a 2400 Fix (207) gt 4029

Portland ME 04102

062200

Portland ME 04102

Iron Total 109 ngL 1 0 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 1 16 mgL 10 002 6010200 7 061400 EM 1

062200

Portland ME 04102

Iron Total 041 mgL 10 002 6010200 7 061400 EM 1

062200

Tel-(207) 874-2400 Fx (2071775-4029

Portland MB 04102

062200

CLIENT TOM ESCHNER

Wbodard amp Curran

Report Date 062200

PO No 9509303

Project SAOO LF

Iron Total 287 mgL 10 002 6010200 7 061400 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

Iron Total 3 37 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 12 mgL 1 0 002 6010200 7 061600 EM 1

062200

Portland ME 04102

Iron Total 3 98 mgL 1 0 002 6010200 7 061600 EM 1

062200

LJOmrcajc (dw)

QF12ICWO

Portland ME 04102

062200

LJOmrcajc(dw)

QF12ICWO

Tel- (2ltT) 8712400 Fix (207) 775 402V

Portland ME 04102

Iron Total 073 mgL 10 002 6010200 7 061600 EM 1

062200

LJOmrcajc(dw)

QF12ICWO

Portland ME 04102

062200

Portland ME 04102

062200

Portland ME 04102

LJOmsmajc(dw)

QF07TSS3

062200

Tel (207) 874-2400 FM 1207) 7gt-4029

Portland ME 04102

062200

LJOmsmajc(dw)

QF07TSS3

062200

Portland ME 04102

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Tel (207l 8~42400 Fax (207) 775-4029

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

062200

LJOmsmajc (dw)

QF07TSS3

062200

Portland ME 04102

062200

Portland ME 04102

062200

LJOmrcajc(dw)

QF08ICSO

Portland ME 04102

062200

LJOmsmajc (dw)

QF07TSS3

ARSENIC 200 200 mgL 1000 80 120 AQF14A

BARIUM 200 215 mgL 1075 80 120 BQF13A

BORON 0500 0552 mgL 1104 80 120 BQF13A

CADMIUM 00500 00556 mgL 1112 80 120 AQF14A

CALCIUM 250 237 mgL 948 80 120 BQF13A

COBALT 0500 0560 mgL 1120 80 120 BQF13A

COPPER 0250 0267 mgL 1068 80 120 BQF13A

IRON 100 102 mgL 1020 80 120 BQF13A

LEAD 0500 0531 mgL 1062 80 120 AQF14A

NICKEL 050 055 mgL 1100 80 120 BQF13A

SILICON 523 562 mgL 1075 80 120 BQF13A

SILVER 0050 0054 mgL 1080 80 120 BQF13A

SODIUM 750 738 mgL 984 80 120 BQF13A

ZINC 0500 0523 mgL 1046 80 120 BQF13A

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REMARKSshy

AIRBILL NO

Sdgt 102)

SD-9B Moo HOC

Sco-3gt-( 2r5

I13o f i f t J

SDshyCOMMENTS CAS-C

Services 0000048

ATTACHMENT 2

REPORT OF ANALYSIS

GROUNDWATER

June 282000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Portland ME 04102

Iron Total 500 mgL 1 0 002 6010200 7 061000 KD 1

062800

Portland ME 04102

Iron Total 0 02 mgL 1 0 002 60102007 061000 KD 1

062800

hrrp k Tel (603) 431-5777 Fix (603) 436-3356

062800

hrcp Td (603) 43l-577 fin (603) 4^6-33

062800

htp ka Tel (603)431-5777 Fix (603)436-3356

062800

LJOmrcajcdw)

QF08ICWO

Portland ME 04102

Iron Total 002 mgL 1 0 002 6010200 7 061000 KD 1

062800

hrcp k Tel (603) 431 5~ Fix (603) 4 556

Iron Total 457 mgL 10 002 60102007 061000 KD 1

062800

CALCIUM 250 229 mgL 91 6 80 120 BQF15A

COBALT 0500 0492 mgL 98 4 80 120 AQF22A

COPPER 0250 0263 mgL 1052 80 120 BQF15A

IRON 1 00 0968 mgL 96 8 80 120 BQF15A

LEAD 0500 0495 mgL 99 0 80 120 AQF22A

NICKEL 050 054 mgL 108 0 80 120 BQF15A

SILVER 0050 0053 mgL 1060 80 120 BQF15A

SODIUM 750 770 mgL 1027 80 120 BQF15A

TIN 0500 0481 mgL 96 2 80 120 AQF22A

ZINC 0500 0519 mgL 103 8 80 120 BQF15A

ARSENIC 200 1 94 mgL 97 0 80 120 AQF09A

BARIUM 200 2 16 mgL 1080 80 120 BQF09A

BORON 0500 0570 mgL 1 14 0 80 120 BQF09A

CADMIUM 00500 00520 mgL 1040 80 120 AQF09A

CALCIUM 250 2 4 1 mgL 96 4 80 120 BQF09A

COBALT 0500 0506 mgL 101 2 80 120 AQF09A

COPPER 0250 0261 mgL 1044 80 120 BQF09A

IRON 1 00 0994 mgL 99 4 80 120 BQF09A

LEAD 0500 0508 mgL 101 6 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF09A

SILICON 523 568 mgL 1086 80 120 BQF09A

SILVER 0050 0053 mgL 106 0 80 120 BQF09A

SODIUM 750 757 mgL 1009 80 120 BQF09A

ZINC 0500 0537 mgL 107 4 80 120 BQF09A

5 amp1 S i J

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REMARKS

AIRBILL NO

OMMENTS

June 212000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

Portland ME 04102

062100

Portland ME 04102

Iron Total 85 9 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 578 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

062100

Iron Total 336 mgL 1 0 002 6010200 7 061200 EM 1

062100

Portland ME 04102

Iron Total 111 mgL 10 002 6010200 7 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Tel (2(T) 84 2400 FII (207) 77i-4029

Proj ID

PO No 9509303

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

PONo 9509303

Date Analyzed 6500

MW-95-1S AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

062100

Proj ID

PO No 95093 03

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes-

PO No 9509303

Date Analyzed 6500

MW-95-1SDUP AQ 6100 6100 6500 BEG 5030 BEG

Report Notes

062100

PO No 9509303

Portland

Proj ID

Solids NA

Method EPA 8260

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes B J

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

MW-95-4RD AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 111 10

Report Notes B J

Portland ME 04102

Iron Total 115 mgL 10 002 60102007 061200 EM 1

062100

LJOmrcajc(dw)

QF10ICWO

Proj ID

PO No 95093 03

MW-13 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

Report Notes

Client TOM ESCHNER

Woodard amp Curran

41 Hutchins Dr

Portland ME 04102

Proj ID

MW-13 AQ

Compound

ETHYLBENZENE

M+P-XYLENE

BROMOFORM

O-XYLENE

STYRENE

ISOPROPYLBENZENE

BROMOBENZENE

2-CHLOROTOLUENE

N-PROPYLBENZENE

4-CHLOROTOLUENE

TERT-BUTYLBENZENE

SEC-BUTYLBENZENE

1 3-DICHLOROBENZENE

P-ISOPROPYLTOLUENE

1 4-DICHLOROBENZENE

1 2-DICHLOROBENZENE

N-BUTYLBENZENE

HEXACHLOROBUTADIENE

TOLUENE-D8

SDG WQ1571

Report Date 61600

PO No 9509303

Project SACO LF

Solids NA

Method EPA 8260

Date Analyzed 6500

6100 6100 6500 BEG 5030 BEG

Sample Method

JO 6 ugL 10 1 1

3 ugL 1 0 1 1

lt1 ugL 1 0 1 1

3 ugL 1 0 1 1

lt1 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

J07 ugL 10 1 1

lt1 ugL 1 0 1 1

lt1 ugL 10 1 1

1 ugL 10 1 1

lt1 ugL 10 1 1

6 ugL 10 1 1

lt1 ugL 10 1 1

19 ugL 10 1 1

lt1 ugL 10 1 1

J08 ugL 10 1 1

lt1 ugL 10 1 1

J09 ugL 10 1 1

lt1 ugL 10 1 1

9 ugL 10 1 1

lt1 ugL 10 1 1

110 10

111 10

108 10

Report Notes

Proj ID

Solids NA

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Report Notes B

PO No 95093 03

Solids NA

Date Analyzed 6500

TB-1 AQ 6100 6100 6500 BEG 5030 BEG

Sample Method

TOLUENE-D8 109 10

Report Notes B

ARSENIC 200 211 mgL 1055 80 120 AQF12A

BARIUM 200 208 mgL 1040 80 120 AQF12A

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQFI5A

SILVER 0050 0049 mgL 980 80 120 AQF12A

TIN 0500 0556 mgL 1112 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQFI2A

4A EPA SAMPLE NO

MW-13 WQ1571-10 F5643 6500 7 06 00 PM

TB-1 WQ1571-11 F5644 6500 7 44 00 PM

FORM IV VOA Page 1

PO No 9509303

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

Sample Method

Report Notes

Solids NA

Method EPA 8260

Proj ID

Date Analyzed 6500

TOLUENE-D8 108 10

Report Notes

1 1 -DICHLOROETHANE 50 525 105 60 140

1 1-DICHLOROETHENE 50 577 115 60-140

12-DIBROMOETHANE 50 422 84 60-140

12-BUTANONE 50 384 77 60-140

2-CHLOROTOLUENE 50 528 106 60-140

2-HEXANONE 50 333 66 60-140

4-CHLOROTOLUENE 50 546 109 60-140

ACETONE 50 21 9 44 60-140

BENZENE 50 528 106 60-140

BROMOBENZENE 50 537 107 60-140 1

BROMOFORM 50 576 115 60-140

CHLOROETHANE 50 50 1 100 60 140

CHLOROFORM 50 488 98 60-140

Out of Limits 1

Lab File F5630

Analyst- BEG

D1BROMOMETHANE

ETHYLBENZENE

HEXACHLOROBUTADIENE

1SOPROPYLBENZENE

(M+PXYLENE

METHYLENE CHLORIDE

N BUTYLBENZENE

N PROPYLBENZENE

NAPHTHALENE

O XYLENE

SEC BUTYLBENZENE

STYRENE

TERT BUTYLBENZENE

[TETRACHLOROETHENE

(TETRA HYDROFURAN

TOLUENE

TRICHLOROETHENE

VINYL CHLORIDE

50 528 106

50 450 90

50 49 1 98

50 542 108 L

50 475 95

50 53 2 106

100 108 108

50 292 58

50 585 117

50 ~ 532 ~ 106

50 45 7 91

50 61 1 122

575 115

50 568 114

50 582 116

50 568 114

50 579 116

50 51 4 103

50 543 108

50 504 101

~ 537 106

50 558 112

50 51 0 102

Limits () 60 140

60 140

60 140 |

60 140

Out of Limits

LCSF07B LCSF07B F5676 6700 3 57 00 PM

MW-95-1SMS WQ1571-7MS F5692 6800 2 38 00 AM

FORM IV VOA Page 1

Sample Method

Report Notes

PO No bull 95093 03

Solids NA Proj ID

Method EPA 8260

Date Analyzed 6700

Sample Method

Report Notes

Lab File F5676

Analyst BEM

Ul-TRICHLOROETHANE

1 1 -DICHLOROETHANE

1 1 -D1CHLOROETHENE

12-DIBROMOETHANE

12-DICHLOROBENZENE

12-DICHLOROETHANE

1 2-DICHLOROPROPANE

13-DlCHLOROBENZENE

1 3-DlCHLOROPROPANE

14-DICHLOROBENZENE

22-DICHLOROPROPANE

2-BUTANONE

2-CHLOROTOLUENE

2-HEXANONE

4-CHLOROTOLUENE

ACETONE

BENZENE

BROMOBENZENE

BROMOCHLOROMETHANE

BROMOFORM

BROMOM ETHANE

CHLOROBENZENE

CHLOROETHANE

CHLOROFORM

CHLOROM ETHANE

50 511 102 60-140

50 537 107 60-140 99 50 495 60-140

50 53^4 107 60-140

50 sTs 108 60-140

50 596 119 60-140

50 442 88 60-140

50 488 98 60-140 75 50 373 60-140

50 498 100 60-140

50 ~5amp9 114 60-140

50 418 84 60-140

50 533 106 60-140

50 482 96 60-140

50 548 no 60-140

50 568 114 60-140

50 506 101 60-140

50 564 113 60-140

50 543 108 60-140 103

50 516 ^ 60-140

50 524 105 60-140

50 530 106 60-140

50 447 89 60-140

50 541 108 60-140

50 386 77 60-140

50 545 109 60-140

50 506 101 60-140

50 222 bull44 60-140

50 518 104 60-140

50 536 107 60-140

50 554 I I I 60-140 r _ bdquo_ _

512 102 60-140

50 528 106 60-140

50 495 99 60-140

50 531 106 60-140

50 546 109 60-140

50 487 97 60-140

50 498 100 60-140

50 472 94 60-140

50 554 I I I 60-140

Out of Limits

Lab File F5676

Analvst BEM

Sample ID LCSF07B

Date Run 6700

Matrix AQ

Compound Name

DIBROMOM ETHANE

HEXACHLOROBUTADIENE

ISOPROPYLBENZENE

M+P-XYLENE

METHYLENE CHLORIDE

N-BUTYLBENZENE

N-PROPYLBENZENE

P-ISOPROPYLTOLUENE

TERT-BUTYLBENZENE

TOLUENE

Spike Amt (ugL)

Result JugL)

559 554

Rec () Limits () 105 60-140

102 60 140

103 60-140

112 60 140

79 60-140

110 60-140

112 60-140

86 60-140

112 ~ 60 140

111 60-140

107 60-140

119 60 140

114 60-140

116 60-140

115 60 140

118 60-140

105 60-140

138 60-140

_M2_~ 60-140

108 60-140

102 60-140

115 60-140

106 60-140

Out of Limits

4A EPA SAMPLE NO

FORM IV VGA Page 1

Proj ID

9509303

Solids NA

Method EPA 8260

Date Analyzed 6800

Sample Method

Report Notes

Date Analyzed 6800

Sample Method

TOLUENE-D8 106 10

Report Notes

1 2-DlBROMOETHANE 50 51 0 102 60-140

1 2-DlCHLOROETHAN E 50 51 3 102 60 140

2-BUTANONE 50 493 98 60-140

2 CHLOROTOLUENE 50 562 112 60-140

2-HEXANONE 50 440 88 60-140

ACETONE 50 23 1 bull46 | 60-140

BENZENE 50 535 107 1 60-140

BROMOM ETHANE 50 ~55 2 110 60-140

CHLOROBENZENE ~ 50 555 111 60-140

CHLOROETHANE 50 51 1 102 60-140

CHLOROFORM 50 542 108 60-140

Out of Limits 1

Lab File F5695

Analyst BEM

Sample ID LCSF08A

Date Run 6800

Matrix AQ

(ugL) Result

LSTYRENE 50 625 125

Limits () 60-140

60-140

60 140

60-140

60 140

60-140

Out of Limits

MSMSD Report

WQ1571-7 F5640 6500 5I1OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

2-BUTANONE 0 50 50 475 554 95 I I I 60-140 15 20

2-HEXANONE 0 50 50 418 500 84 100 60-140 18 20

ACETONE 0 50 50 250 292 50 58 60-140 15 20

BENZENE 50 50 163 547 ~ 33 109 60-140 20

11-DICHLOROETHANE 0 50 50 176 653 35 130 60^140 120 20

STYRENE 0 50 50 159 631 32 i 126 60-140 bull120 20

M+P-XYLENE 0 100 100 303 F l9 30 119 60-140 bull120 20

TOLUENE 0 50 50 166 605 33 121 60-140 bull110 20

MSMSD Report

WQ1571-7 F5640 6500 511OOPM BEG AQ 8260_99

WQ1571-7MS F5692 6800 23800 AM BEM AQ 8260_99

WQ1571-7MSD F5700 6800 114800 AM BEM AQ 8260_99

BROMOFORM 0 50 50 257 644 bull51 129 60-140 86 20

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REMARKS

AIRBILL NO

colld Cntrs

COMMENTS

Katahdin

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

Imp k Tel (603 431-5777 Fax 603 436-3356

061600

Portland ME 04102

061600

LJOmrcajc(dw)

QF10ICWO

Portland ME 04102

Iron Total 15 7 mgL 1 0 002 6010200 7 061200 EM 1

061600

Portland ME 04102

Iron Total 780 mgL 10 002 60102007 061200 EM 1

061600

Tel (207)8^4-2400 Fix (207) 775 4029

Portland ME 04102

Iron Total 56 7 mgL 10 002 6010200 7 061200 EM 1

061600

Portland ME 04102

061600

CLIENT TOM ESCHNER

061600

BORON 0500 0525 mgL 1050 80 120 AQF12A

CADMIUM 00500 00573 mgL 1 146 80 120 AQF12A

CALCIUM 250 252 mgL 1008 80 120 AQF12A

COBALT 0500 0553 mgL 1106 80 120 AQF12A

COPPER 0250 0250 mgL 1000 80 120 AQF12A

IRON 100 110 mgL 1100 80 120 AQF12A

LEAD 0500 0555 mgL 1110 80 120 AQF12A

NICKEL 050 052 mgL 1040 80 120 BQF15A

SILVER 0050 0049 mgL 980 80 120 AQF12A

ZINC 0500 0528 mgL 1056 80 120 AQF12A

bullg 0 UJ

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6- o a5 KI

Q O^ y_= (S

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5 sect o J c

H pound to -5

f 8 | ^^

REMARKS

E8-I oe^i^^s T

COMMENTS

Services 0000013

June 162000

Dear Mr Eschner

Report of Analysis

Confirmation

Sincerely

TECHNICAL NARRATIVE

061600

Portland ME 04102

Iron Total 026 mgL 10 002 60102007 061000 KD 1

061600

Portland ME 04102

061600

hlrp kacahdmlab com

ARSENIC 200 209 mgL 1045 80 120 AQF10A

BARIUM 200 217 mgL 1085 80 120 BQF08A

BORON 0500 0578 mgL 1156 80 120 BQF08A

CADMIUM 0050 0055 mgL 1 100 80 120 BQF08A

CALCIUM 250 235 mgL 940 80 120 BQF08A

COBALT 0500 0563 mgL 1 126 80 120 BQF08A

COPPER 0250 0242 mgL 968 80 120 AQF09A

IRON 100 0972 mgL 972 80 120 BQF08A

LEAD 0500 0515 mgL 1030 80 120 AQF09A

NICKEL 050 054 mgL 1080 80 120 BQF08A

SILICON 523 572 mgL 1094 80 120 BQF08A

SILVER 0050 0052 mgL 1040 80 120 BQF08A

SODIUM 750 782 mgL 1043 80 120 BQF08A

TIN 0500 0540 mgL 1080 80 120 AQF10A

ZINC 0500 0527 mgL 1054 80 120 BQF08A

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Client

Address

Purchase Order

REMARKS

AIRBILL NO

TEMPC O TEMP BLANK

Sample Description

AltO-95-1 IS

COMMENTS

Contact Phone Fax

Address

O UPS O CLIENT

barcode 6862

Documents

CORPORATE OFFICES Maine, Massachusetts,Secure Site semspub.epa.gov/work/01/6862.pdf · CORPORATE OFFICES Maine, Massachusetts, New Hampshire, Connecticut Illinois, Florid, a Operational