8
27 Motion & Control No. 8 (May 2000) 1. Introduction Many of the rolling bearings produced today are made of AISI 52100 high-carbon chromium bearing steel (equivalent to SUJ2). Over the long, nearly 100-year history of AISI 52100, its main components have scarcely been modified. During this same period, a great deal of research has been conducted on such topics as bearing service life, bearing life evaluation technology, differences between types of premature bearing failures (e.g., failures due to surface- and subsurface-originated fatigue), 1) and material factors that can affect these types of premature bearing failures. 2) Based on the results of this research, improvements were made to steelmaking processes that resulted in higher purity of AISI 52100. 3) The results of studies and the types of premature bearing failures experienced in the field, however, indicate that AISI 52100 is not necessarily the ideal steel for rolling bearings. In response, we analyzed many premature bearing failures with a view to developing a material that would ensure longer bearing service life. In the course of developing this material, we focused not only performance factors like life, but also ease of production. This report gives background on and then describes the characteristics of NSJ2 bearing steel, a new steel with longer life and better performance than AISI 52100. 2. Research on In-Service Bearing Failures Fatigue failure of rolling bearings in service can be broadly classified into two types: subsurface-originated fatigue and surface-originated fatigue. In subsurface- originated fatigue, a crack initiates below the surface of the bearing raceway at a defect such as a non-metallic inclusion, often in the region of maximum shear stress. This type of fatigue is often associated with good lubrication. In surface-originated fatigue, a crack is initiated at a defect such as a scratch or indentation in the bearing raceway caused by foreign debris. This type of fatigue is associated with poor lubrication. In both surface and subsurface fatigue, the cracks propagate under the influence of cyclic stress until flaking of the bearing raceway occurs. These types of fatigue can be analyzed using X-ray diffraction (Figs. 1 and 2). 4)–6) For many years, NSK has used this technology to generate a vast amount of data on Development of NSJ2 Bearing Steel Nobuaki Mitamura NSK-RHP European Technology Centre Yasuo Murakami Research and Development Center ABSTRACT Using special fatigue analysis techniques, NSK has investigated numerous premature bearing failures in a variety of applications. Analysis revealed that in the majority of cases premature bearing failure was from surface-originated fatigue. NSK therefore developed a new steel, NSJ2, which has better resistance to surface-originated fatigue than conventional bearing steels. As a result, bearings made of NSJ2 steel are less prone to premature failure. The development of this new bearing steel involved the optimization of alloying additions to give improved resistance to surface-originated fatigue without adversely affecting other important steel properties such as wear resistance and dimensional stability. Consideration was also given to the ease with which bearings could be manufactured in the new steel. Fig. 1 Fatigue analysis of typical subsurface-originated fatigue Fig. 2 Fatigue analysis of typical surface-originated fatigue *The fatigue index is calculated based on changes in the half-value width of martensite and in retained austenite content. 2.5 2 1.5 1 0.5 0 0 0.2 0.4 0.6 0.8 1 Distance below surface, mm Fatigue index* 2.5 2 1.5 1 0.5 0 0 0.2 0.4 0.6 0.8 1 Distance below surface, mm Fatigue index*

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27 Motion & Control No. 8 (May 2000)

1. Introduction

Many of the rolling bearings produced today are made ofAISI 52100 high-carbon chromium bearing steel(equivalent to SUJ2). Over the long, nearly 100-yearhistory of AISI 52100, its main components have scarcelybeen modified. During this same period, a great deal ofresearch has been conducted on such topics as bearingservice life, bearing life evaluation technology, differencesbetween types of premature bearing failures (e.g., failuresdue to surface- and subsurface-originated fatigue),1) andmaterial factors that can affect these types of prematurebearing failures.2) Based on the results of this research,improvements were made to steelmaking processes thatresulted in higher purity of AISI 52100.3) The results ofstudies and the types of premature bearing failuresexperienced in the field, however, indicate that AISI 52100is not necessarily the ideal steel for rolling bearings. Inresponse, we analyzed many premature bearing failureswith a view to developing a material that would ensurelonger bearing service life. In the course of developing thismaterial, we focused not only performance factors like life,but also ease of production. This report gives backgroundon and then describes the characteristics of NSJ2 bearing

steel, a new steel with longer life and better performancethan AISI 52100.

2. Research on In-Service BearingFailures

Fatigue failure of rolling bearings in service can bebroadly classified into two types: subsurface-originatedfatigue and surface-originated fatigue. In subsurface-originated fatigue, a crack initiates below the surface ofthe bearing raceway at a defect such as a non-metallicinclusion, often in the region of maximum shear stress.This type of fatigue is often associated with goodlubrication. In surface-originated fatigue, a crack isinitiated at a defect such as a scratch or indentation in thebearing raceway caused by foreign debris. This type offatigue is associated with poor lubrication. In both surfaceand subsurface fatigue, the cracks propagate under theinfluence of cyclic stress until flaking of the bearingraceway occurs.

These types of fatigue can be analyzed using X-raydiffraction (Figs. 1 and 2).4)–6) For many years, NSK hasused this technology to generate a vast amount of data on

Development of NSJ2 Bearing SteelNobuaki MitamuraNSK-RHP European Technology CentreYasuo MurakamiResearch and Development Center

ABSTRACTUsing special fatigue analysis techniques, NSK has investigated numerous premature bearing failures in a variety of

applications. Analysis revealed that in the majority of cases premature bearing failure was from surface-originated fatigue.NSK therefore developed a new steel, NSJ2, which has better resistance to surface-originated fatigue than conventional

bearing steels. As a result, bearings made of NSJ2 steel are less prone to premature failure.The development of this new bearing steel involved the optimization of alloying additions to give improved resistance to

surface-originated fatigue without adversely affecting other important steel properties such as wear resistance anddimensional stability. Consideration was also given to the ease with which bearings could be manufactured in the new steel.

Fig. 1 Fatigue analysis of typical subsurface-originated fatigue Fig. 2 Fatigue analysis of typical surface-originated fatigue

*The fatigue index is calculated based on changes in the half-value width of martensite and in retained austenite content.

2.5

2

1.5

1

0.5

00 0.2 0.4 0.6 0.8 1

Distance below surface, mm

Fat

igue

inde

x*

2.5

2

1.5

1

0.5

00 0.2 0.4 0.6 0.8 1

Distance below surface, mm

Fat

igue

inde

x*

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the fatigue of bearings in service. From this data, it wasfound that in applications where fatigue was the maincause of premature bearing failure, the most common typewas surface-originated, usually due to poor lubricationconditions.

Fig. 3 shows the results of a bearing life test that wascarried out under good lubrication conditions (filteredelastrohydrodynamic lubrication). Microscopic observationof the bearings after testing showed those with a short lifehad an arrowhead-like trace of flaking originating from amicroscopic dent (Photo 1). This highlights the difficulty ofcompletely preventing surface-originated fatigue fromleading to premature bearing failure.

Fig. 4 shows the results of bearing life tests carried out

under various lubricating conditions. The bearings testedunder good lubricating conditions exhibited flaking fromsubsurface-originated fatigue and their life was muchlonger than the theoretical life. This is probablyattributable to recent advances in steel mill technologyresulting in greatly improved steel cleanliness and thealmost total elimination of harmful non-metallic inclusionsfrom which flaking originates. By contrast, the bearingstested under poor lubricating conditions exhibited flakingfrom surface-originated fatigue. Under these conditions,the life was as short as one twenty-fifth of the theoreticallife.

The above results show that in the case of subsurface-originated fatigue, bearings can achieve their theoretical

Motion & Control No. 8 (May 2000) 28

99.9

99

90

50

10

5

11 10 102 103 104

Life, h

Cum

ulat

ive

failu

re p

roba

bilit

y, %

Surface-originated failure

Subsurface-originated failure

: Test suspended (no failure)

Test conditions: P/C: 0.71 Speed: 3 900 rpm Lubrication: Oil bath

Fig. 3 Surface- and subsurface-originated failures in fatigue life test results of 6206 deep groove ball bearings

99.999

90

50

10

5

10.01 0.1 1 10 100

Contaminated with foreign particles of hardness 870 Hv and average size 100 µm

Contaminated with foreign particles of hardness 510 Hv and average size 100 µm

Contaminated with foreign particles of hardness 370 Hv and average size 100 µm

Contaminated with foreign particles of hardness 1200 Hv and average size 25 µm

Clean, no foreign particles

Lubrication conditions P/C N (rpm)

A 0.32 3 000

0.32 3 000

0.32 3 000

0.32 3 000

0.71 3 900

B

C

D

E

Life ratio (Actual life/Calculated L10 life)

Cum

ulat

ive

failu

re p

roba

bilit

y, %

All bearings were lubricated by the oil bath method

AB

C

D

E

Fig. 4 Fatigue life test results of 6206 bearings under various lubricating conditions

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29 Motion & Control No. 8 (May 2000)

life, while in the case of surface-originated fatigue bearinglife is often much shorter than the theoretical life. In orderto improve bearing reliability in the market, it isnecessary to develop a bearing steel with increasedresistance to surface-originated fatigue.

3. Concept of New Bearing Steel

To develop a new steel with improved resistance tosurface-originated fatigue and thereby improve the life ofbearings operating under poor lubricating conditions,research was conducted on material factors and alloys.7)

In relation to material factors it was found that greaterretained austenite content in the surface of the materialimproves resistance to surface-originated fatigue as shownin Fig. 5. Further studies on the relationship betweenmaterial factors and bearing life under contaminatedlubrication conditions revealed that increasing the amountof retained austenite was possibly the most effective wayof suppressing premature failure from surface-originatedfatigue. Fig. 6 shows the results of life tests carried out onbearings made from steel containing varying percentagesof retained austenite. The results of the tests show that asthe hardness of the foreign particles increases, bearing lifedecreases. However, the decrease becomes less pronouncedas the amount of retained austenite increases.

Although high retained austenite content improvesbearing life under surface-originated fatigue, it reducesthe dimensional stability of the bearing. Therefore in thedevelopment of a bearing steel resistant to surface-originated fatigue, consideration was given to thedimensional stability of the bearing.

4. Alloy Design

For the purpose of developing a new bearing steel, anumber of steels with various compositions were studiedto determine the effect of different alloys on performance.

4.1 Improvement in surface-originated fatigue life

Increasing the amount of retained austenite improvesresistance to surface-originated fatigue. In alloy design,therefore, steel compositions were formulated that wouldresult in levels of retained austenite above those found instandard heat-treated AISI 52100.

Figs. 7 to 10 show the relation between the mainalloying elements and the retained austenite content afterhardening and tempering. All these steels were heat-treated in the same way as AISI 52100.(1) C content

Fig. 7 shows the relation between carbon content andretained austenite. Under normal heat treatmentconditions, the amount of retained austenite is closelyrelated to the carbon content: the higher the carboncontent, the higher the retained austenite content.However, when the carbon content is in excess of 0.7%, theretained austenite content increases only slightly.(2) Si content

Fig. 8 shows the relation between Si content andretained austenite. Si has little effect on the level ofretained austenite.(3) Mn and Cr contents

Photo 1 Surface condition of prematurely failed bearing

10

120 25 30 35 40

Amount of retained austenite, %

L 10

life,

106

cyc

les

Fig. 5 Relationship between L10 life and the amount of retainedaustenite under contaminated lubrication

1 000

100

10

0Clean Contaminated

(Particlehardness = 510 Hv)

Contaminated(Particlehardness = 870 Hv)

L 10

life,

105

cyc

les

γR = 35%

γR = 22%

γR = 10%

Fig. 6 Relationship between retained austenite content (γR),hardness of foreign particles and surface-originated fatigue life

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The effects of Mn and Cr content on retained austeniteare shown in Figs. 9 and 10, respectively. The higher theMn content, the higher the retained austenite. Conversely,the higher the Cr content, the lower the retained austenite.

Figs. 11 to 14 show the relation between the alloyelements and bearing life under contaminated lubricationconditions, i.e., surface-originated fatigue. The bearingswere tested on a flat-washer type test rig under thefollowing conditions:

Pmax = 4 900 MPaN = 3 000 cpmContaminants:

- Hardness: Hv 540- Size: 74 - 147 µm- Quantity: 300 ppm

The retained austenite content was nearly a constantwhen the carbon content was higher than 0.7%, whilebearing life was nearly constant when the carbon contentwas higher than 0.8%. This indicates that a carbon contentof greater than 0.8% is necessary to obtain good bearing life.

Si showed little effect on the retained austenite content,but as the Si content increased so did the bearing life. Asto the effect of Mn and Cr on bearing life, the addition ofMn resulted in a higher retained austenite content andimproved bearing life, while the addition of Cr led to alower retained austenite content and a reduction inbearing life.

From these findings it was concluded that increased inC, Mn and Si content lengthens bearing life while,conversely, increased Cr content reduces bearing life.

4.2 Dimensional stabilityGenerally, the longer a bearing is either used or stored

the more likely it is to undergo dimensional change due tothe decomposition of its retained austenite. The degree ofdimensional change depends on the amount of retainedaustenite that decomposes; the larger the amount ofretained austenite that decomposes, the greater thedimensional change. On the other hand, high levels ofretained austenite can be very beneficial to bearing life

30

25

20

15

10

5

00 0.3 0.6 0.9 1.2

Am

ount

of r

etai

ned

aust

enite

, %

Manganese content, %

Levels of other alloys:C: 0.8-0.85%Si: 0.2-0.3%Cr: 0.9-1.1%

Fig. 9 Relationship between the amount of retained austenite andmanganese content

Motion & Control No. 8 (May 2000) 30

30

25

20

15

10

5

00.4 0.6 0.8 1 1.2

Am

ount

of r

etai

ned

aust

enite

, %

Carbon content, %

Levels of other alloys:Si: 0.2-0.3%Mn: 0.6-0.8%Cr: 0.9-1.1%

Fig. 7 Relationship between the amount of retained austenite andcarbon content

30

25

20

15

10

5

00 0.3 0.6 0.9 1.2 1.5 1.8

Am

ount

of r

etai

ned

aust

enite

, %

Chrome content, %

Levels of other alloys:C: 0.8-0.85%Si: 0.2-0.3%Mn: 0.6-0.8%

Fig. 10 Relationship between the amount of retained austenite andchrome content

30

25

20

15

10

5

00 0.2 0.4 0.6 0.8 1

Am

ount

of r

etai

ned

aust

enite

, %

Silicon content, %

Levels of other alloys:C: 0.8-0.85%Mn: 0.6-0.8%Cr: 0.9-1.1%

Fig. 8 Relationship between the amount of retained austenite andsilicon content

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31 Motion & Control No. 8 (May 2000)

characteristics associated with surface-originated fatigue,as discussed earlier.

Although the amount of dimensional change isproportional to the retained austenite content, what isimportant is the decomposition rate of the retainedaustenite. In other words, dimensional change may notoccur if the retained austenite does not decompose underthe bearing operating conditions including especially theoperating temperature. Si significantly affects the retainedaustenite decomposition rate. Fig. 15 shows the differentdecomposition rates of retained austenite in two steelswith different Si content. As shown in the figure, thedecomposition of retained austenite is retarded byincreasing the Si content. In addition, an increase in the Sicontent also increases the resistance to softening duringtempering and therefore maintains the hardness of thebearing when operated at high temperatures. Based onthese findings, NSK developed NSJ2 steel with higher Sicontent, a lower rate of retained austenite decomposition

and better heat resistance than AISI 52100 (Fig. 16).

4.3 Surface hardnessThe analysis results shown in Figs. 7 to 14 indicate that

the amount of retained austenite affects bearing lifecharacteristics associated with surface-originated fatigue.On the other hand, bearing surface hardness must also bea consideration from the point of view of wear andindentation resistance.

The precipitation of carbides affects surface hardness.To increase the precipitation of carbides, carbideconstituents such as C and Cr must be added to steel. Thismeans that, in spite of the fact that the addition of Crreduces the retained austenite content and degradesbearing life associated with surface-originated fatigue, aconsiderable amount of Cr must be added to developsufficient surface hardness.

Levels of other alloys:

Si: 0.2—0.3%

Mn: 0.6—0.8%

Cr: 0.9—1.1%

L 10

life,

105 c

ycle

s

1

0.4 0.6 0.8

Carbon content, %

1 1.2

10

100

Fig. 11 Relationship between L10 life and carbon content underdebris-contaminated lubrication

Levels of other alloys:

C: 0.8—0.85%

Mn: 0.6—0.8%

Cr: 0.9—1.1%

0 0.5 1

Silicon content, %

10

100

L 10

life,

105 c

ycle

s

1

Fig. 12 Relationship between L10 life and silicon content underdebris-contaminated lubrication

10 0.3 0.6 0.9 1.2 1.5

Manganese content, %

10

100

Levels of other alloys:

C: 0.8—0.85%

Si: 0.2—0.3%

Cr: 0.9—1.1%L 10

life,

105 c

ycle

s

Fig. 13 Relationship between L10 life and manganese content underdebris-contaminated lubrication

10 0.3 0.6 0.9 1.2 1.5 1.8

Chrome content, %

10

100

Levels of other alloys:

C: 0.8—0.85%

Si: 0.2—0.3%

Mn: 0.6—0.8%L 10

life,

105 c

ycle

s

Fig. 14 Relationship between L10 life and chrome content underdebris-contaminated lubrication

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Motion & Control No. 8 (May 2000) 32

4.4 ProductivityAs part of developing a new bearing steel, it is not only

necessary to consider the functional requirements asdescribed in the previous sections but also the feasibility ofmanufacturing bearings in the steel. From this viewpoint,manufacturing-related properties like machinability, cold-workability, hardenability and grindability wereexamined.

5. Performance Evaluation ofNSJ2 Bearing Steel

Based on the extensive research summarized in theforegoing, the composition of NSJ2 bearing steel wasdetermined. Test bearings were manufactured andevaluated in a number of tests.

5.1 Life testsFigs. 17, 18 and 19 show the results of life tests. The

results in Fig. 17 show that the life characteristics of the

NSJ2 bearings are similar to AISI 52100 bearings underclean lubrication conditions (i.e., subsurface-originatedfatigue). However, as shown in Figs. 18 and 19, the NSJ2bearings performed better than the AISI 52100 bearingsunder contaminated lubrication conditions (i.e., surface-originated fatigue).

5.2 Dimensional stability testFig. 20 shows the change in the dimensions of bearings

at 100°C and 120°C. The NSJ2 bearings demonstratedbetter dimensional stability than the AISI 52100 bearings.This indicates that NSJ2 bearings have better dimensionalstability than AISI 52100 bearings over the typicaloperating temperature range. This is because the retainedaustenite decomposes more slowly in the NSJ2 steel thanin the AISI 52100 steel.

5.3 Wear and seizure resistance testFig. 21 shows the results of a Sawin wear resistance

test. The results indicate that NSJ2 has similar wear andseizure resistance to AISI 52100.

15

12

9

6

3

0

Time, h

Am

ount

of r

etai

ned

aust

enite

, %

0 5 000 10 000 15 000 20 000

Si = 0.25%

Si = 0.50%

Fig. 15 Influence of silicon content on the retained austenitedecomposition rate at 120°C

Har

dnes

s, H

RC

56

57

58

59

60

61

62

63

160 180 200 220 240 260 280 300

Tempering temperature, °C (× 2h)

AISI 52100

NSJ2

Fig. 16 Tempering resistance of NSJ2 and AISI 52100

Test conditions:P/C: 0.71Speed: 3 900 rpmLubrication: Clean

Life, h

Cum

ulat

ive

failu

re p

roba

bilit

y, %

10 102 103 1041

5

10

50

90

9999.9

AISI 52100

NSJ2

Steel

NSJ2

AISI 52100

Number of tests

24

53

Occurrencesof flaking

7

15

Test suspended after 1 000 hours

Fig. 17 Fatigue life under clean lubrication conditions of 6206 bearings made of NSJ2 and AISI 52100

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33 Motion & Control No. 8 (May 2000)

The results of the evaluation tests show that NSJ2 steelhas greater resistance to surface-originated fatigue thanexisting AISI 52100 bearing steel. This is due to NSJ2’shigh level of retained austenite, which is achieved bycareful control of its composition. This high level ofretained austenite, however, compromises the dimensionalstability of the bearing. Furthermore, the lower content ofCr, while necessary to ensure a high level of retainedaustenite, has an adverse effect on wear and seizureproperties. To overcome these problems, silicon content isincreased and Cr content is optimized. As a result, NSJ2has similar dimensional stability and wear resistance toAISI 52100.

6. Conclusion

NSK has developed a new bearing steel, NSJ2, thatimproves the service life of bearings by minimizingpremature failures. NSJ2 was developed based on theunderstanding that the majority of in-service prematurebearing failures are due to surface-originated fatigue. Thecomposition of NSJ2 is designed to promote higherretained austenite content, which improves bearing lifeunder surface-originated fatigue. In testing, bearingsmade of NSJ2 demonstrated longer life than bearingsmade of AISI 52100 steel.

Life, h

Cum

ulat

ive

failu

re p

roba

bilit

y, %

1 101 1021

5

10

50

90

99

99.9

NSJ2

AISI 52100

Test conditions:P/C: 0.43Speed: 4 000 rpmLubrication: ContaminatedDebris: Hardness: 870 Hv

Diameter: 74-147 µmQuantity: 150 ppm

Fig. 19 Fatigue life under contaminated lubrication conditions of L44649/610 tapered roller bearings made of NSJ2 and AISI 52100

Life, h

Cum

ulat

ive

failu

re p

roba

bilit

y, %

1 10 102 1031

5

10

50

90

99

99.9

Test conditions:P/C: 0.32Speed: 3 000 rpmLubrication: ContaminatedDebris Hardness: 540 Hv

Diameter: 74–147 µmQuantity: 1000 ppm

AISI 52100

NSJ2

: Test suspended (no failure)

Fig. 18 Fatigue life under contaminated lubrication conditions of 6206 bearings made of NSJ2 and AISI 52100

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Motion & Control No. 8 (May 2000) 34

References:1) K. Furumura, S. Shirota and K. Hirakawa, “The Surface-

initiated and Subsurface-initiated Rolling Contact Fatigue,”NSK Bearing Journal No. 636 (1977) 1-10.

2) K. Furumura, Y. Murakami and T. Abe, “The Development ofBearing Steels for Long Life Rolling Bearings under CleanLubrication and Contaminated Condition,” NSK TechnicalJournal No. 656 (1993) 15-21.

3) T. Abe, H. Narai and K. Furumura, “EP Steel (A Superlong-Life, High Reliability Bearing Steel),” NSK Technical JournalNo. 652 (1992) 1-8.

4) K. Furumura, S. Shirota and A. Fujii, “Fatigue Analysis ofRolling Bearings (Part 1) - Analysis of Surface FatigueDamage (1) -,” NSK Bearing Journal No.643 (1982) 1-10.

5) K. Furumura, S. Shirota and A. Fujii, “Fatigue Analysis ofRolling Bearings (Part 2) - Analysis of Surface FatigueDamage (2) -,” NSK Bearing Journal No.644 (1984) 1-6.

6) K. Furumura, S. Shirota and A. Fujii, “Fatigue Analysis ofRolling Bearings (Part 3) - Analysis of Subsurface-FatigueDamage (1) -,” NSK Technical Journal No.646 (1986) 18-25.

7) Y. Murakami, N. Mitamura and K. Furumura, “Long LifeSuper TF & Hi-TF Bearings under Severe LubricationConditions,” NSK Technical Journal No. 652 (1992) 9-16.

AISI 52100 (120°C test)E

xpan

sion

rat

e, 1

0-3%

0

1

2

3

4

5

6

7

8

9

10

100 1 000 10 000 100 000

Time, h

NSJ2 (120°C test)

NSJ2 (100°C test)

AISI 52100 (100°C test)

Fig. 20 Dimensional stability of outside diameter of 6206 bearings made of NSJ2 and AISI 52100

Rel

ativ

e w

ear

amou

nt, 1

0-8m

m3 /N

mm

0

1

2

3

4

0 1 2 3 4Sliding speed, m/sec

Sawin wear testLoad: 36.1 NSliding distance: 1 000 mLubricant: None Seizure limit

NSJ2

AISI 52100

Fig. 21 Comparison of wear resistance of NSJ2 and AISI 52100l

Nobuaki Mitamura

Yasuo Murakami