20
CERTIFICATE OF ANALYSIS AND QUALITY Product Surge Acute Nootropic SKU SURGE Barcode 866033000222 Formula 2 Date 1 May 2019 Label

CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

  • Upload
    others

  • View
    1

  • Download
    0

Embed Size (px)

Citation preview

Page 1: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

CERTIFICATE OF ANALYSIS AND QUALITY

Product Surge Acute Nootropic

SKU SURGE

Barcode 866033000222

Formula 2

Date 1 May 2019

Label

Page 2: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

Certifications

Good Manufacturing Practice (GMP) Certificate

Capsule Certificate of Analysis from Supplier

Capsule Certificate of Analysis from Manufacturing

Capsule Identity Test Results (FTIR) from Manufacturing

Combined Ingredients Certificate of Analysis from Manufacturing

Caffeine Anhydrous Certificate of Analysis from Supplier

Caffeine Anhydrous Certificate of Analysis from Manufacturing

Caffeine Anhydrous Identity Test Results (FTIR) from Manufacturing

Caffeine Anhydrous Potency Test Results (HPLC) from Manufacturing

L Theanine Certificate of Analysis from Supplier

L Theanine Certificate of Analysis from Manufacturing

L Theanine Identity Test Results (FTIR) from Manufacturing

L Theanine Potency Test Results (HPLC) from Manufacturing

Panax Ginseng Certificate of Analysis from Supplier

Panax Ginseng Certificate of Analysis from Manufacturing

Panax Ginseng Identity Test Results (FTIR) from Manufacturing

Panax Ginseng Identity Test Results (HPTLC) from Manufacturing

Panax Ginseng Potency Test Results (HPLC) from Manufacturing

Page 3: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from
Page 4: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from
Page 5: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from
Page 6: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

ColorFile

7194-10786 CPS Capsule HPM

C 0 Orange 14486.0

Path

C:\Users\Israel\Docum

ents\Bruker\OPUS_7.5.18\D

ata\MEAS

Spectrum Type

Query Spectrum

5001000

15002000

25003000

3500W

avenumber cm

-1

0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35Absorbance Units

Search Library4/1/2019 3:27:11 PM

Page 1 of 1

Page 7: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

Certificate of AnalysisSample Information

CTLA ID:Date Received:Sample Name:Lot Number:Customer:

74854/16/201950145 THR Surge191007Origin Nutraceutical

Analysis SpecificationMethod ResultMDL UnitsRapid Complete Micro

ReportUSP <2021> 200Total Plate Count 100 cfu/g

ReportBAM CH.4 <10Total Coliforms 10 cfu/g

ReportUSP <2022> NegativeE. Coli

ReportUSP <2022> NegativeSalmonella

ReportUSP <2022> NegativeStaph. aureus

ReportAOAC 997.02 <10Rapid Yeast and Mold 10 cfu/g

1077 S 1675 W, OREM, UT 84058

Quality Manager

Page 1 of 1

Specifications provided by the Customer. Results with an asterisk (*) denote Specifications should be reviewed by the Customer.This Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entireproduct from which it was taken. These results are provided for the benefit of the Customer. MDL = Machine Detection Limit.

Page 8: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

Certificate of AnalysisSample Information

CTLA ID:

Date Received:

Sample Name:

Lot Number:

Customer:

7651

4/24/2019

50145 THR SURGE

191007

Origin Nutraceutical

Analysis SpecificationMethod ResultMDL UnitsHeavy Metals

ReportUSP <2232> 0.008Arsenic .001 ppm

ReportUSP <2232> <0.001Cadmium .001 ppm

ReportUSP <2232> 0.012Lead .001 ppm

ReportUSP <2232> <0.001Mercury .001 ppm

1077 S 1675 W, OREM, UT 84058

Quality Manager

Page 1 of 0

Specifications provided by the Customer. Results with an asterisk (*) denote Specifications should be reviewed by the Customer.

This Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire

product from which it was taken. These results are provided for the benefit of the Customer. MDL = Machine Detection Limit.

Page 9: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from
Page 10: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from
Page 11: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

ColorH

it Quality

966

Compound nam

e

Caffeine Anhydrous 1031807716 Standard 1

CAS Num

berM

olecular formula

Molecular w

eight

ColorFile

6025-10109 DRM

Caffeine Anhdrous (Kosher) 12892.1

Path

C:\Users\Israel\Docum

ents\Bruker\OPUS_7.5.18\D

ata\MEAS

Spectrum Type

Query Spectrum

Product Num

ber

Entry No.

Library name

Library description

Copyright

Caffeine Anhydrous 1031807716 Standard 1

86EQUIN

OX N

UTRACEUTICAL.S01

Equinox Nutraceutical M

aterials Only

User library

5001000

15002000

25003000

3500W

avenumber cm

-1

0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40Absorbance Units

Search Library3/25/2019 4:54:04 PM

Page 1 of 1

Page 12: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

Certificate of AnalysisSample Information

CTLA ID:Date Received:Sample Name:Lot Number:Customer:

70833/25/201910109 Caffeine12892Origin Nutraceutical

Analysis SpecificationMethod ResultMDL UnitsCaffeine ReportHPLC 101.66 %

1077 S 1675 W, OREM, UT 84058

Quality Manager

Page 1 of 0

Specifications provided by the Customer. Results with an asterisk (*) denote Specifications should be reviewed by the Customer.This Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entireproduct from which it was taken. These results are provided for the benefit of the Customer. MDL = Machine Detection Limit.

Page 13: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from
Page 14: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

Certificate of AnalysisSample Information

CTLA ID:

Date Received:

Sample Name:

Lot Number:

Customer:

7198

3/28/2019

10310 L- Theanine

14487

Origin Nutraceutical

Analysis SpecificationMethod ResultMDL UnitsID, Rapid Complete Micro Combo

ReportFTIR >95%ID

ReportUSP <2021> <100Total Plate Count 100 cfu/g

ReportBAM CH.4 <10Total Coliforms 10 cfu/g

ReportUSP <2022> NegativeE. Coli

ReportUSP <2022> NegativeSalmonella

ReportUSP <2022> NegativeStaph. aureus

ReportAOAC 997.02 <10Rapid Yeast and Mold 10 cfu/g

L-Theanine ReportHPLC 98.980.006 %

FTIR Spectra ReportFTIR (attached)

1077 S 1675 W, OREM, UT 84058

Quality Manager

Page 1 of 1

Specifications provided by the Customer. Results with an asterisk (*) denote Specifications should be reviewed by the Customer.This Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entireproduct from which it was taken. These results are provided for the benefit of the Customer. MDL = Machine Detection Limit.

Page 15: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

ColorH

it Quality

962

Compound nam

e

10310 L-Theanine 63011 Standard 1

CAS Num

berM

olecular formula

Molecular w

eight

ColorFile

7198-10310 DRM

L-Theanine 14487.0

Path

C:\Users\Israel\Docum

ents\Bruker\OPUS_7.5.18\D

ata\MEAS

Spectrum Type

Query Spectrum

Product Num

ber

Entry No.

Library name

Library description

Copyright

10310 L-Theanine 63011 Standard 1

293

ORIGIN

STAND

ARDS LIBRARY.S01

Library for Origin N

utra Materials

Origin N

utraceutical Materials O

nly

5001000

15002000

25003000

3500W

avenumber cm

-1

0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7Absorbance Units

Search Library4/4/2019 3:55:28 PM

Page 1 of 1

Page 16: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

4.03%

Page 17: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from
Page 18: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from
Page 19: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from

Certificate of Analysis: 10139 Panax ginseng (61880/20160420) High Performance Thin-Layer Chromatography with Photo-Documentation

1 2

Certificate Issued To: Origin Nutraceutical 1077 So 1675 West Orem, Utah 84058 USA

Company Name: Origin Nutraceutical Title: 10139 Panax ginseng Plant Part: root, leaf, stem Sample Received: 9/12/2016 Sample Description: Clear Whirl-Pak Form of Botanical: powdered extract Appearance: off-white fine powder Lot: (61880/20160420) Æ Lane 5(2µl) Sample: EA25616ON1_1 Latin Name: Panax ginseng C.A. Mey [Araliaceae] Reference Sample: Lane 2(2µl) (VE15305SWH) Panax pseudoginseng Wall. Var. notoginseng (root); Lane 3(2µl) (VE20508AHP4) Panax

pseudoginseng Wall. Var. notoginseng (root); Lane 6(2µl) (EA13805SWH) Panax ginseng (root); Lane 7(2µl) (EA08305SWH) Panax ginseng (leaf); Lane 8(2µl) (LA14609CRB1) Panax quinquefolius (root); Lane 9(2µl) (F12015AHP3) Astragalus membranaceus (root); held at Alkemist Labs, Costa Mesa, CA.

Analyst: J. Nguyen, N. Hoang, P. Fast, S. Kabbaj, K. Tran 74400 Sample Prep: 0.3g+3mL 70% grain EtOH sonicate/heat @~50° C ~ 1/2 hr Stationary Phase: Silica gel 60, F254, HPTLC plates Mobile Phase: chloroform: ethyl acetate: CH3OH: water [3/8/4.4/1.8] Detection: (1) 10% Ethanolic H2SO4 Æ 120° C 10 min Æ visible light

(2) 10% Ethanolic H2SO4 Æ 120° C 10 min Æ UV 365 nm Reference Std: Lane 1(1µl) Ginsenoside F11 (00007270-210, CHR), Methanol (55162, VWR), Ginsenoside Rf (00007216-601, CHR)

~0.1% Reference Source: Method Developed by Alkemist Labs IDT-SOP-72-01 Comments & Conclusions: Lane 5 is the test sample 10139 Panax ginseng (61880/20160420). Lanes 2, 3, 6, 7, 8, 9 are the reference samples used for comparison. This test sample, 10139 Panax ginseng (61880/20160420), is consistent with the chromatographic profile of the reference sample of Panax ginseng C.A. Mey [Araliaceae] used above. This test sample, 10139 Panax ginseng (61880/20160420) has characteristics of an extract derived from Panax ginseng C.A. Mey [Araliaceae] leaf and Panax sp. root. NOTE: The above conclusion may be a function of the natural variance found in botanicals &/or the extraction process used to create specific extracts. The growing and drying conditions, age, seasonal variations, geographic location, extraction solvents, etc. all play a role in the phytochemical fingerprint of botanicals as well as their extracts; hence, chromatographic variations are expected.

Examined, Reviewed & Authorized by: Sidney Sudberg, CSO, Alkemist Labs Report Date: 9/13/2016 Note: Any unidentified lanes in the above chromatograms are confidential and may represent internal studies or other test samples not related to 61880/20160420. This report applies to the sample investigated and is not necessarily indicative of the quality or condition of apparently identical or similar products. This report is for the exclusive use of the party who requested the report and not for public dissemination or use by third parties, including for promotional purposes, without the prior written permission of Alkemist Labs, Inc. This report provides technical results for a specific sample and the report shall not be altered, modified, supplemented or abstracted in any manner. Any violation of these conditions renders the report and its results void. © 2016 Alkemist Labs, Inc. All Rights Reserved

Work performed at: Alkemist Labs 1260 Logan Ave B2 Costa Mesa, CA 92626 714-754-HERB (4372) 714-668-9972 (FAX) [email protected] www.alkemist.com

Digitally signed by Sidney Sudberg DN: cn=Sidney Sudberg, o=Alkemist Laboratories, ou, [email protected], c=US Date: 2016.09.13 16:54:17 -07'00'

Page 20: CERTIFICATE OF ANALYSIS AND QUALITYThis Certificate of Analysis represents data for the sample submitted and does not constitute a guarantee of quality for the entire product from