Certificate Of Analysis · Certificate Of Analysis Analysis Start Date Customer Tracy Watson Avara Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Glare Parameter

Customer Tracy Watson Avara Sharlnon Pharmaceutical Sevices Shannon Industrial Estate Shannon Clam

Certificate Of Analysis Job Number: 17-35181 b u e N u m b e r : 1 Report Date: 14 November 2017

Site: Not Applicable PO Number: 4560436720 Date Samples Received: 0111 112U-17

Please find attached the results for the samples received at our laboratory on 01/13/2017.

Should you have any queries regarding the report or require any further services, we would be happy to diseuss your requirements. For additional information about the company please lag-on to our website at the above address.

Thank yau far choosing City Analysts Limited. We look forward to assisting you again..

Authorised By; Authorised Date: 14 November 201 7

Sham Reynolds Laboratory Manager

Ndas: R@sulh relate only to the itams testad. Information on methods of analyds and pe~omance characteristics i5 available on request. Any opinfans or interpretations indioated are outside the scope of uur fNAB accreditation. This fqsi ppcifi shall ~ l ~ f be rq~p$ljc+g exmpt in full or with written approval of City .. Analysts . Limited.

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EPA Export 16-03-2018:03:33:18

Customer Tracy Wakon

Methanol < 1uu.00

k Ethanol iaum L n-propanol < lQU,OO

Certificate Of Analysis

ugll UQ/l

ug/l -

Avara Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Clat%?

t

*

i

Site: Not Applicable

Sample Descrlption: ESOP 02/11/2517

Sample Type: Effluent [Final]

Lab Reference Number: 376475

- n-pentanal s: 1 a0,ao ugh

USA

- n-heptanol s: t oo.oa Srgll

Methyl Acetate e 100.00 ugA

n-hexanal += m o a

Site I Method Ref

sis3aom

IS0 1702

City Analysts Lifted, Pipm Hou&0 Road, Ringsend, Dublin 4.

t

Date of Sampling: 0 I I I t121117

Date Sample Received: Oi/l1/20~7

PV Value Analysis Parameter Result Units (Drinking

Start Date Water Only)

0911 1 /XI 7 Alkalinity CaC03 572.662 msn

06/11/2017 Copper e a.mo msn Cyclhexane 1-170 mgll

OlJllS2017 BOD5 31 mg/lO2

FOG

1 . 1 - 1 n-butanol I r 1 M O O I uan I - I

NOM: PV Value Is the parametric value, laken from European Cornmunitias, (Drlnklng Water) Regufahs, 201 4. S.I. No. 122 of 2U14 and relatee only to drlnking wter samples. For queries on results, please conlac! us wiffih ma weeks af the report date to ensure that we can acoornmtxiate your query as samples emnot be stored i*OiV3lY. NAC 8, RTC- Na abbnomal change and amptable to custnrners. TVC -Totar vlabIe count Site D = Analped at Ci& Analysts Dublin. Sk $ at City Analysts Shamon

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EPA Export 16-03-2018:03:33:18


Analysis Start Date

Customer Tracy Watson Avara Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Glare

Parameter ResuIt Units

Ethyl Acetate c 100.00 U#ll

nPrnpyl Acetate T lOO.0t) US11 iso-Prapyl Acetate < 100.00 ugll

Slte: Not Applicable

SampJe Description: ESO2 0211 1/2017

Sample Type: Effluent (Final)


L

* *

Site I Method Ref.

t

*

*

*

MlBK < 1OO.OQ ugll -

THF 1oa.m ug/l - r: l a m w g t ten Butyl Abohol

1

"U

'U f

*U

Date of Sampling: OllllW017

Uate Sample Received; Qlll Id01 7

- Butyric acid < 10,000 mg/l

Iso-valeric Acid -z f 0.000 mg/l

Valeric acid < TO.DO0 mgll

Caproic Acid *. 10.000 mgll

PV Value (Drinking

Water Only]

I c I - I < 25.80 t uall I - I 1 . 1 - 1 &Butanone 1 c 100.00 I U d l I - I

I udl 1 - I r; 100.00 1 . 1 - 1 Isobutanol I

I *U- I - I Acetic Add I f0.000 I I - I I * u I - I Prmianic acid I <10.000 I mall I - I I * u I - I Iso-buMic Acid I < 10.000 I mall I - I

#= INAB Accredited, U = UKAS Accredited, * =Subcontracted

Nbk: PVVdue [S the parametric value, taken from European hrnmnitias, (Drlnklng Walsr) Regutatkxls, 20'14,5,1, No. 122 of 8014 and relates only lo drinking wafef samples. FW queries on results, pkam contact us within two weeks of the report date to ensure that we ean accommodate your query as samples cannot be stored Indefinitely. NAG d ATC - Nu abnormal change and acceptable to customws. TVG - Total viable munl Site D = Analysed at CUy Andyak Dublin. S b S = Analysed at Ciy Anarets Shannon

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EPA Export 16-03-2018:03:33:18

Customer Tracy Watson

Site I Analysis Parameter Result Methad Ref. Start Date


PV Value Unit5 (Drinking

Water Only)

Avara Shannon Pharmacleutical Sevices Shannon Industrial Estate ShatlnQtI Clare

*U

*U

Site Not Applicable

Sample Description: €SO2 02/11/2017



1 ,BOichloroathane < 3.00 - I ,2-0ichloropropane sm ugll

I

N A B ACCREDITED

TESTING - City Analysts Limlted, Ptgeon House Road, Ringsend, Dublin 4.

Fax: [Or ) 61 3 SO08 Tal: fol] $13 6003

01 /I 1 /'2017 Date of Sampling:

Date Sampie Received: 07/11/2017

I " L I I - I Hepfanolc Acid I < 12.000 I m d l I - I

I 1 ,l-crichloroethane I .= 1.00 I I - I t .l-Dtchloraethene I i i.00 I u Q / l I - I

I * U I - l 1 ,l-Dtbhloropropene I i 1.00 I Wfi I - I

I 'U I- I ~

1,2,4-Trimethylbenzene - 1 < 2.00 I w/l I - I

I * u I - I 1 ,PDibromaetbane I < 2.00 I ua/l I - I 1 ' 1 - 1 1.2-Dichlorobmzsne I < 4.00 I l l w l I - I

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EPA Export 16-03-2018:03:33:18

Customer Tracy W atsan

Site I Method Ref.


PV Value AnaIysb Parameter Result Units (Drinking

Start Date Water OnlyJ

Avara Shannon PharmaceUtical Sevices Shannon Industrial Estate Shannon Clare

site: Not Applicable

Sample Description: €sa3 02lli12017



ACCREQtlEU

TESTING

Date of Sampling: 0 1 I f 14201 7

Date Sample Received: OllI1/2017

l0.no t ua(l 1 - 1 1 . 1 - 1 1,3,5-Tri~hlorabenzene I

I - L U l - l 2-Chloroto bene

I * u I - I 6Ghlarotoluene r: 2.00 I Wfl I - I

Benzene I < 1,uo I U411 I - I

~

Bromoform I Bramomethane I c 2.00

I * U l - l Carbon Dlsulphide I 1.00

I I 1 1 I ugn "w ChIoro benzene .= 4.00 I # = INAE Accredlfed, U = UYAS Accredited, * = Subcontracted

Nom: PV Value Is the parmetic value, Taken from European Oommunities, (Drtnkirag Water) Reguhtims, 2p14. S.I. No. 122 of 2014 and relata only lo drlnking water samples. Far queries on reaulls, please c n n w us wlthin two weeks af the report date to ensure that we can accommodate your queq as samples cannot ba m t e d indefinitely. NAG a A X - No abnormal change and acceptable fo Gustomem. TVC - Totat viabb count Stta 0 = Analysed at ciiAflaIy6k D&lh. SikS = Anzdysed at City Analysfs Shannon

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EPA Export 16-03-2018:03:33:18

A

Certificate Of Analysis Customer Tracy Watson Avara Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Clare


Sample OescrtpKort: ES02 0211 1/2017



Report Reference: 17.351 Vi

Report Version: 1

Date of Sampling: 01/11/2Q17

Date Sample Received: 01/11 /2017

# = INAB Aocredited, U = UKAAS Accredited, * = Subcontracted

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EPA Export 16-03-2018:03:33:18



Avara Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Glare


Sample Descrfption: EbO2 02/1 WO17



ACCREOR€D

TESTING

Report Reference: 17-35181

Repofl Version: 1

Date of Sampling: 0-111 I m i 7

Pate Sample ReceIveU: 01ll112017

Parameter

#= IMAB Accredited, U I UKAS Accredited, * = Subconwackd

Nota: PV Vahm is We parametricvalue, Wen from European Gomrnunlties, {Drinking Water) Regulations, 201 4. XI. No. 122 OF 2014 and mlabs only to drinking watm sanlpk. For guerbes on masuks, please contact us W'thfn two weeks d Ihe repoft dab to ensure that we can accomrndale your query as samples cannot be stored indefinitely. NAG B AT0 - No &nmmal change and awe&&[@ to C U S ~ C I ~ ~ O ~ S . TVC -Total viable count Sit8 0 = Analysed al City Analysts Oublin. Slle 3 t: Analysed at City Analysts Shannon

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EPA Export 16-03-2018:03:33:18

TeILab Q

Certificate No: L117fI838 Date Redd: DYI1/2017

hsuc Date: OB12r2017 Our Rep ws-44316

€EKTlFICATE OF ANALYSIS Page 1 of 2

Project Description: Analysis of Aqueous SmpIe

Attention: I1 Company: Addre@:

Lab m: 142050

Project Summary: One $ample ws analysed for a i w g e ofdetemn~nmds. Please see page 2 krresdts. Tams 8t Cmditiow and methods used ai= outlined in the attached appendix.

No. of Pages:

Mr, Peter O’Byrne QiteIity Manager

Ms Breds Moore Technical Manager

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EPA Export 16-03-2018:03:33:18

Page 2 of 2

Sample ID

Determ inand Lab It)

Nitrate as N nla

Tellab ES 02

0111112017

242050

4 . 5 6 (note I)

ANALYSIS OF AQUEOUS SAMPLE.

Date Sampled: O l / l ID017 Date Received: 0Y.t 1/2017 Date Analysis Commenced: 05/72/2017 Our Ref: WS-44316 Certificate No: U1 7/1838

Note I: LOD raised due to sample matrix interference.

Results expressed as mgd (ppm) unless stated otherwise

** INAB Accredited Pests ++ = Subcontracted Tests nla = Non-INAB Awredited Tests

The above results relate only to the sample tested This report should not be regenerated except in full and with the consent of T.E. Laboratotjes Ltd.

T.E. Laboratories

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EPA Export 16-03-2018:03:33:18


IS0 1702: .

I N A B hCCREOlTEO

Avara Shannon Pharmaceutical Sevices Shannon Industrial Esfate Shannon Clare

Certificate Of Analysis Job Number; 17'3541 3 lssue Number: 5 Report Date; -14 November 2037

Site: Not Applicable PO Number: 4500436720 Date Samples Received: 08/11 E201 7

Ptease find attaehed the results for the samples received at our laboratory on 08/11/2017,

Should you have any queries raqarding the report or require any further services, we would he happy to discuss your requirements. Far additional information about the company please log-on to our website at the above address.

Thank you far choosing City Analysts Limited. We look forward to assisting you again.


Notes: Results relate only to the items tested. Information on methods of analysts and petformane characterlstlcs Is avaifable on request. Any opinions or interpretatiaDs Sndicated are out.side the scope of our ]NAB aecredltation. This test report shall nat be reproduced except in full or wjth written approval of City Analysts Limited.

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EPA Export 16-03-2018:03:33:18


Slta I Method Ref.

SISIQOZW

Customer Tracy Watson Amra Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Clare

PV Value Analysis Parameter Result Unit5 [Drinking

Start Date Water Only)

O&/11/2017 BOD5 22 mg/J 02

Site: Not Applicabls

Sample Description: ESQ2 OW1 1117


Lab Referenm Numberr 3771 15

Gi!y Analysts Limited, Pigeon House Road, Ringsend. Dublin 4.

Date of Sempting; 08/11 /SO1 7

Date Sample Received: OBI1 1/2017

#- NAB Accrdltedx U = UKAS Accredited, * =Subcontracted

NOW PV Value Is lhe paramehlc value, faken from European Communities, (Drinking Water) RegukUons, 2014.S.l. No. 122 of 2014 and relates only to drfnklng water samples. Fbr qUBfie& on results, please contact us w.&in twa m k s of the report date to enare that we m accbrnmodale your query as samples cailna he stered Indefinitely. NAG & ATC - No abnormal ohange and ac~eptable to ~uskmtm~. TVC - Tqtal Ibiabte munt Site 0 = hnalysed at City Analysts Dublin. 'Site S = Analysed at City AnaptS Shannon

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EPA Export 16-03-2018:03:33:18

T,E. LABORATORIES T I I T E D 7iTading us

TeILab b LoughmartinBusiness Park, TSlow, CQ. Carlow

Phone: 05941 52881 Pax: 059-9152886

CERTIFICATE OF ANALYSIS Page1 of 2

Project Description: I Attention: ll Cornpnny: Address:

Certificate No:

Analysis oFAqueous Gample

Ms. Tracy Watson 142291

IssueDate: 11112~2017 Our Ref: WS-443 62 ll Pr6ject Summary; One sample was analysed for a range of determinands.

Pfease see page 2 for results. T m s & Conditions and methods used are autiined in the Efttaehed appendix.

No. of Pages:

Mr. Pder O'Byrne Quality Manager

Results page 2 plus 4 page a p p m d ~

& Bredr Moors Technical Manager

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EPA Export 16-03-2018:03:33:18

Page 2 Qf 2

Determinand

Nitrate a5 N

Tellab 4b Sample ID ES 02

0813 112077

Lab ID 142291

nla 4.56 (note I)


Date Sampled: 09/11/2017 Date Received: 1011 11201 7 Date Analysis Commenced: 08M212017 Our Ref: WS-44362 Certificate No: L/'l7/1906

~.

Nate 1 : LOD raised due to sample matrix interference.

Results expressed as mg/l (ppm) unless stated otherwise

** = INAB Accredited Tests ++ = Subcontracted Tests nla = Non-INAB Accredited Tests

The above results relate only to the sample tested This report should not be regenerated except in full and with the conaent of T.E. Laboratories Lid.

T.E. Laboratories

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EPA Export 16-03-2018:03:33:18

TESTING

Customer Tracy Watson Avara Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Clare

Certificate Of Analysis Job Number: 17-35754 Issue Number: 1 Report Date: 23 November 201 7

Site: Not Applicable PO Number: 4500436720 Date Samples Received: 1 5/1 i /2O17

PIease find attached the results for rhe samples received at our laboratory on 1541 1R017,

Should you have any queries regarding the report or require any further services, we would be happy to discuss your requirements. For additional information about the company please Iog-on to our website at the above address.

Thank you for choosing City Analysts Limited. We look forward to assisting you again.

Authorised By: Authorised bate: 23 November 2017


Notes: Resutts relate only to the items teefed. Information an methods of analysis and performance characteristics Is available on request. Any opinions or interpretations indicated are outside the s ~ o p e of our INAB accredltation. Thls teest report shall not be reproduced except in full or with written approval of City Analysts Limited.

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EPA Export 16-03-2018:03:33:19


Site / Analysis Parameter Result Unfts

S/S1003# 1511 Il2Oif BOD6 7 mg/lO2

Method Ref. Stat? Date


PV Value (Drinking

Water Only)

Avara Shannon PharrnmiWA Sevices Shannon Industrial Estate Shannon Clare


Sample Descrlption: ES02 15/11/2017

Sample Type: Effluent (Final}

Report Reference: 174571 4

Repm Yersfon: 3

Date of Sampling; 15/11/2017

Date Sample Received: 1511 1 BO1 7

# - INA& Accredited, U UKAS Accredited, * = Subcnnlracted

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EPA Export 16-03-2018:03:33:19

TeILab

Company: Address:

Cottifieate No:

Laughartin Business Park, TuUaw, Co. Carlow Yhme: 059-9152881 Fax: 0594152886

CERTIFICATE OF ANALYSIS Page 1 of 2

Prqject Description: I/ Atten tiorr:

Analysis of Aqu~ous Sample

Ms. Tracy Watson Lab IJX 142519

W17/1956

Issue Date: 15/12/2017 Our Rpf: WS-44416 n Project S~mmary: One sample was analysed for a m p of determinaads.

P h s e see page 2 for results, Terms & Condit i~n~ and methods used me a u t h d in the attached appendix

Results page 2 plus 4 page appendix

Ms Brcda Moore Technical Manrger

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EPA Export 16-03-2018:03:33:19

Page 2 of 2

Sample ID

Determinand Lab ID

Nitrate as N *if

Tellab 4 ES 02

15/17/2017

142519

<0.56 (note A )


Date Sampled: 16/11/2017 Date Received: A7/11/2017 Date Analysis Commenced: 13/12/2017 Our Ref: WS-44416 Certificate No: Ll-l JI1856

Note 7: LQD raised due to sample matrix interference.

Results expressed as mgll (ppm) unless stated otherwise


The above results relate only to the sample tested This report should not be regenerated except in full and with the consent of T.E. Laboratories Ltd.

T.E. Laboratories

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EPA Export 16-03-2018:03:33:19

Customer Tracy Watson A w a Shannon Pharmaceutical Sevices Shannan Industrial Estate Shannon Glare

IS0 I702

City Analysis Limited, Pipon House Road, Wings;8nd, Dublin 4.

Certificate Of Analysis Job Number; 17-35944 Issue Number: 1 Reporf Date: 28 November 261 7

Site: No1 Applicable PO Number: 4500436720 Date Samples Received; 22/1t120 17

Please find attached the results for the samples received at our laboratory on 2211 1/201?.

Should yau have any queries regarding the report or require any furZher seruice~, we would be happy to discuss your requirements. For additional informath about the company please log-on to our website at the above address.

Thank you for choosing City Anarysts Limited. We look forward to assisting you again.

Authorised By:

Caitlin Quinn Deputy Quality Manager

Authorised Date: 28 November 201 7

Notes:

Rewlts relate only to the Hams tested, lnformaticrn on methods of analysts and performance characteristics is available Any opinions or interpl'etations Indicated are outside the scope of our INAB accreditation. This test report shall hot be reproduced emept In full or with written approval of Glty Analysts Limited.

request,

Page 1 of2 Template: 1146 Ravislon: 016

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EPA Export 16-03-2018:03:33:19

Custorney Tracy Watson

Site I Analysis Par am et er RSi i l t Method Ref. Starl Rate

SfGI O O M 22/11/ZD17 BOD5 50


PV Value Units (Drinking

Water Only)

mQA02

Avara Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Clare


Sample Descrtption: ESU2 22/11/2017



1 :\'

Report Reference: 17-35944

Report Verdcn: 1

Date of Sarnplio$j: 22/11/21117

Date Sample Received: 22/11/2017

#- INAB Acmadited, U = UKAS Accredited, + = Subcontracted

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EPA Export 16-03-2018:03:33:19

TESTING

Company: Addnsr:

Certificate No:

TeILab Ca

CERTIFICATE OF ANALYSE3 Page 1 of 2

roject lh.wiptim: Analysis of Aqueous Sample

Ms, Tracy Watsan Lab ID:

AvaraMmufiicturing Ireland Ltd., Date SampSd: 2211 U22017 Shannon Industrial Mate> Shafinon, CO, Clare.

LJ17m70 DrteRec’d: 2411 1/2013

ssue Date: 13/12RDI 7 our Ref: w3-44452

Project Summary: Ode sample was analyyed for a mgs: o f determinands. please s w page 2 forresults. Terms iEk Conditions and methods used are outlined in the attached appendix.

MO, of Paw:

Mr. Peter O’Bytnc Quality Mwnagcr


MsBreda Moore Tothnical Manager

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EPA Export 16-03-2018:03:33:19

Page 2 ~f 2

Determinand

Nitrate as N

Tellab 4 Sample ID ES 02

2211112017

Lab ID 142699

x* <0,56 (note j)


-

Note I: LOD raised due to sample matrix interference.

Resutts expressed as mgll (ppm) unless stated otherwise


The above results relate only to the sample tested This report should not be regenerated except in full and with the consent of T.E. Laboratories Ltd.

T.E. Laboratories

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EPA Export 16-03-2018:03:33:19

Customer Tracy Wabon Avara Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Clare

Certificate Of Analysis Job Numbet; 17-363-17 Issue Number: 1

Report Date: 6 December 2017

SZte: Not Applicable PO Number: 4500436720 Date Samples Received: 29J111-2017

Please find attached the results for the samples received at our laboratory on 29/11/2017.

Should you have any queries regarding the report or require any further services, we would be happy to discuss your requirements. Far additional informatton about the company please Iog-on ta our website at the above address.

Thahk you for choosing City Analysts Limited, We Icmk forward fa assisting YQU again.

Authorised By: Authorised Date: 6 December 2017

SRane Reynolds Laboratory Manager

Notes: Results relate only to the items tested. Information on methods of analysis and performance characteristics is available on request. Any aplnlans or inlerpretaffms indicated are outside the scope of our INAB accredltation, This test report shall not be reproduced except In full or with written approval of City Analysts Limited.

Page 1 cif 2

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EPA Export 16-03-2018:03:33:19


Site I Method Ref.

S/S1003#


PV Value Analysis Parameter Result unit5 [Drinking

Stat7 Date Water Only)

29/11!2Q17 BO05 16 mall 02

Avara Shannon Pharmacautieal Sevices Shannon Industrial Estate Shannon Clare

Site: Not Appltcable

Sample Descdption: tS02 29/11/2U-i7

Sample Type: Effluent {Final)


R e p o ~ Reference: 17-361 17

Mpovt Verslan:l

Date of Sampling: 2911 iJ2017

Date Sample Received: 29f1112017

#= INAE Amrediled, U = UKAS Abcredited, ' = Subcontracted

IrlQta: PV Wue is tha paramwk gab@, taken ffum European Communities, (Drinking W-r) Regulallons, POI$. 6.1. No* 122 of 2014 and relab only to drinking water samples. For quaries an w~~lts, plea% conk& us within two weeks of the report date b ensure that we cm accommodate your quam as smpks m n o t be starad tndaflnilaiy. MAC & ATC - No abnnnal change and acceptable hs customers. TVC -Total vlable count Site D = AnalyM at Cify Analysts Dublin. Site S = Analped at City Analysts Shannon

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EPA Export 16-03-2018:03:33:19

TelLab 4b

CERTTFICATE QF ANALYSIS Page 1 of 1

Project Description: Analysis afdqtreous Sample

Attention;

COmpRny: Address:

Laughmattin Business Park, Tullow, CO, Carlow Phone: 0594152881 Fax; 0594152886

Ms. Tracy W a r n

ACCnEllllL”

TESTING

3 4294x4

Avare Manufacturing Imland Ltd., Data Sampled: 29/1 U2017 Shannon Industrial Estate, Shannon, CO, Clnte,

Prqjecf Summary:

Mr, Peter O’fEymc Quality Manager

One sample was analysed for a range of determinands. Please see pa& 2 Far resub. Teum & Conditions and methods used are outlined in the attached appendix.


Ms 3reda Moorc Technical Manager

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Page 2 of 2

Sample tD

Determinand Lab ID

Nitrate as N **

Tellab db ES 02

29/11/2017

142903

4 . 5 6 (note ?}


Date Sampled: 29/11/2017 Date Received: 04/12/2017 Date Analysis Commenced: 22/12/2017 Our Ref: WS-44494 Certificate No: U1 7/2039

Note 1: LOD raised due to sample matrix interference.

Results expressed as mg/l (ppm) unless stated otherwise

** = INAB Accredited Tests ++ = Subcontracted Tests nla = Non-lNA3 Accredited Tests

Tbe above results relate only to the sample tested This report should not be regenerated except in full and with the consent of T,E. Laboratories Ltd.

T.E. Laboratories

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Documents

Certificate Of Analysis · Certificate Of Analysis Analysis Start Date Customer Tracy Watson Avara Shannon Pharmaceutical Sevices Shannon Industrial Estate Shannon Glare Parameter