10064

001542

HfcUtUN t>

'- 27 *ZS'fl 26 J

*Relinquished by: Received by: Relinquished by: (Sfantwr*) Oete / Time

Relinquished by: iSi /Time Received by: fStffr-ityn}

Received for Laboratory by: Date /Time

Otetfteoa^rt^^ Fitld fit*s

Remarks

we6-7419

001543

Organics Analysis Data Sheet

Sample Number

Laboratory Name:udb Sample 10 No:Sample Matrix: —

Case No:

so/IData Release Authorized By:

QC Report No:Contract No: .Date Sample Received:

CASNumber

Volatile CompoundsConcentration: O>owJ/ MediumData Estmeted/Prepamd: -$/*£&

u^/l or ug/Kg{Clrela One} CASNumber74-87-374.83-975-01 -475-00-375-09-267*64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-37 1 -5S -656-23-5108 -OS -475-27-4

CnlorometharteSromomethaneVinyl ChlorideChloroethaneMethyfene ChlorideAcetoneCarbon Oiuulfide1. 1-Oichloroethene1. 1'0ichloro«theneTrans-1. 2-DichloroetheneChloroform1, 2-Dichlcroethane2-Butanone1 . 1 , 1 -TrichloroethaneCarbon TetrachlondeViny! AcetateBromodicMoromethane

ug/ler ug/Kg{Circle One)[79-34-S78-87-510061-02-679-01-6124.48-179-00-571-43-210081 -01 -5110-75-875-25-2591 -78-6108-10-1127 - 18 -4108-88-3tOa-90-7100-41 -4tOO-42-5

1 , 1 .2 , 2-Tetr3Chforo*thanef, 2-DtchlorQDi'opaneTrans-1. 3-OichloroprooenflTnchloroetheneOibromty;hlororne thane1 , 1 . 2-Trichloro«thaneBenzenec is-1, 3-Oichforopropene2-Chloroethylvinvletherflromo/orm2-Hexanone4-Me(hvl-2-PentarofieTetrachloroctheneTolueneChtor&ttenzeneSthylbenzeneStvreneTotal Xyienes

Data fl«oofit«g Qualifier*for rapoiing r*tgtt» to EPA. lh« fallowing r«suftj dualitiesAddiliomi flags or foomotvi •Kglatnino rtfsultt i/« ancourigad Hosv«v«/.d*(iniKon of «tch Hat] must b*

H th« /Mult i* a valu* gr«at«r than or equal to ih*r*pon

Indfccates eofnoaund wst tnatyifld 'or but not <fet»c!*d.ft«pon Uvt mmimum datacuan iimii (of th« ume»l« withtft* U (* 8 . J0*J) Euud on n*caKury eoncaniriiton/dtlutton •C1ton». fTttt« i« IVM n«c»turtty tha miitum«ntd*[«ctwrt limit | The footnote should *«d: U-Comaound wai *rul-/t*d for but «M d4tcct*d. Th«nuinftar <• tt»* minimum itiamabl* detection limit for

IndteatH an tinmatad v*!ti» this flag i« uud «ith«rt;l raioons* naaiumvd

oc wh«n m* nu*a coooval dau tftdie*!** ih* o/*Mne«o! • eomoownd that n»«ti lh« td«ntifl£atian «rtttru butth* mult m lit* itun the «tMei(«d deiKttan limit but

This Mag *oOti*l to tM«tcid« oarsmatan wfiara theidtfMiliuiiion ha> bMn eonlirm«j by GC/MS Sff^lieomponam (MiiictdasSIO ng/u| m m* flncl anracimould t« condrmad Ely QC/M3

This Hag it uwd wn«n tit« matyta it tound »n tH« stankID wail *t a umplc. H indieai«* tM«nblt/t)rebat)i«blank contamination and wam> the dii« ut«r to ukt

action.

Oihar**icnb«d and iueh d4Ur<otion •meh*d to fht dataaummarv ttmnn.

001 1/85

001544

LaboratoryNOJ

: SPEC7R1XCMP. .

ORSANICS ANALYSIS DATA SHEET(Tags 2)

Concent rat ionsSEMIVOLAT1LE COHPOUNDS______ 8PC Cleanup

Bate Analyzed*Factors

Percent Mo i s tu r e ) (Decanted )CAS108-95-2 Pheno l . . * , . . . . . . 380. UI I 1 - 44 -4 b i3 <2 -Ch i o r o e t h y l ) E t h e r . 380. U95-57-8 2-Chlaropheno l . . . . . . 380. U541-73-1 1 ,3-Dich lorobenzene . . . 380. U1 0 6 - 4 6 - 7 1 ,4 -D i c h l a r a b e n z e n e . . . 380, U1 00 -5 1 -6 Benzy l Alcoho l . . . . . . 380. U95-50- 1 1 ,2-D i c h l o r oo e n z e n e . . . 380. U95-48-7 2-Kethylphenol . . . . . . 380. U39638-32-9 b i s (2 -Cb l a r o i s o p r o p y l ) E t h e r 380. UK - - 4 4 - 5 4~Hethy lphenaI . . . . . . 360. U6^ 64-7 N -N i t r o s o -O i - n -P r a p y l am i n e 380. U67-72- 1 Hexach loroethane . . . . . 380. U98-95-3 N i t r o b e n z e n e . . . . . . . 380. U78-59 - 1 F s o p bo r o n e . . . . . . . . 380. U83-75-5 2 -M i t r o p h e n a l . . . . . . 380 , U105-67-9 2,4-DUethy lphena l . . . . 380. U65-85-0 Ben za i c Ac i d . . . . . . . 1900 . U1 1 1 - 9 1 - 1 b i s ( 2 - C h 1 o r o e t h o x y )Me t h a n e 380. U1 2 0 - 8 3 - 2 2 ,4 -D i c h l a r o p h e n o l . . . . 380 . U1 20 -82 - 1 1 ,2 ,4-Tr i c b l a r o b e n z e n e , . 380. U9 1 -20 -3 Naphthalene . . . . . . . 380. U1 0 6 - 4 7 - 8 4-Ch l o r oar. i l i ne . . . . . 380 . U8 7 - 6 8 - 3 H e x a c h l o r o b u t a d i e n e . . . 380. U59-50-7 4-Chloro~3-Methy lpheno l . 380. U9 1 -57 -6 2-Hethy lnaphtha lene , . , 380, U7 7 - 4 7 - 4 Hexa ch l o r o c y c l o p e n t ad i e n e 380. U88-06-2 2 ,4 ,6 -T r i c h l o r o p h e n o l . . 380. U95-95-4 2 ,4 ,5-Tr i c h l o r a p h e n o l . . 1900. U91 -58-7 2-Ch lo ronaph t ha l e n e . . . 380. U8 8 - 7 4 - 4 2 -N i t r o a n i l i n e . . . . . . 1 900 . U1 3 1 - 1 1 - 3 D i e e t h y l Ph t ha l a t e . . . . 300. U20B-96-8 Acenaphthy l ene . . . . . . 380. U79-09-2 3-Nitroan i l ine , , . . , . 1900. U

MoFunnel Extraction TesVea

CAS Number93-32-951-28-S100-02-7132-64-91 2 1 - 1 4 - 2606-20-284-66-27005-72-386-73-7100- 10 -6534-52- 186-30-6101 -55-31 1 8 - 7 4 - 187-86-585-01-8120 - 12 -78 4 - 7 4 - 22 0 6 - 4 4 - 012* » -00-085-68-79 1 - 9 4 - 156-55- j1 1 7 - 8 1 - 72 18 -0 1 -91 1 7 - 8 4 - 0205-99-2207-08-950-32-8193 -39 -553-70-319 1 -24-2

Aeenaphthene . . . . . . .2,4-Din i t r oph e no l . . . .D ib en zo f uran . . . . . . .2 ,4-O i n i t roto luene . . . .2,6-Din i t r o t o I u e n e . . . .Diethy lphtha la te . . . . .4-Chl or ophenyl-phenyl etherFluorene . . . . , . . . *4-Ni t roan i 1 i n e . . . . . .4 (6-D i n i t r o ~2-Me t h y l pheno lN-Ni trosodiphenylamine (1 )4-Broflophenyl-phenyl etherHexa c h l o r o b e n z e n e . . . .Pen t a c h l o r o p h e no l . . . .Phenanthrene . . . . . . .Anthracene , , . . . , . .Oi- n -Bu t y l p h t h a l a t e . . .F l u o r a n t h e n e . . . . . . .Pyrene . . . . . . . . . .Buty lbenzy lphtha l ate . , .3 , 3 ' - D i c h i o r o b e n z i d i n e . .B e n 2 0 ( a ) An t h r a c e n e . . . .b i s (2 'Ethy l h exy l )PhthaUteChrysene . . . . . . . . .D i - n -Oc t y l Ph t ha l a t e . . .B e n z o ( b ) F l u o r a n t h e n e , . ,BenzodOFlua ran t h en e . . .Benzo (a )Pyrer te . . . . . .I n d e r , o ( l ,2 ,3 - c d )Py r e n e . .Dibsnz (a ,h) Anthracene , .Benzo (g , h ,i )Peryleria . . .

......ttfl/jfg380.

1900.1900.380.380.380.380.380.380.

1 900 .1900 .380.380.380,

1 9 0 0 .380.380.380.380 .380.380.770 .38C .380.380.380 .380 .380.380.380.380.380.

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

(1) - Cannot be separated from d ipheny lamineForm I

000014

001545

,-,«,•*No

Organics Analysis Data Sheat{Page 3) O.C, No.

Pesticide PCSs

Cone 'OHPar-cent Moisture {decanted*

Cleanup DVts?unn«f Sxtracttcn C Ye*Liquid - Liquid Extraction CV«$

CAS u$ lorug 'KgNurvieiA' (Orel* One)3'3 3-i 53-9-35-3 ' § -3«-3So 39-57S-44-33C9-DC-:lC2- i-5"-3953-98-36C-5T - :7; 55*972-20-33 3 : ' 3 - = 5 -57:-5^-3r : 3 - - o7 - aSC :9-37 2 - J 3 - 5^^«£0^."A 3«J *" 4 *™ - ^

S T . 7 4 - 98001 -35 :t2674-M-21 1 ' 0 4 . 2 9 - 2* • ;4^ . ' 5 - 5«1i«3 " -9^ ^** - — -a- *7

• ; 5 " *2 - i9 -3• r C 9 * - c 9 - '' -C96 -3: 5

Ais-a 3*-c3*:a-8^CDe^a-3'-C-ja-"'-ta'3>-C L-^ea-'e'-estac^to^JiiC"**•*«3tai*"O'1 Eooiitie5^dosu»*an i>«M3rm^ 4 -00€Sncrsn5"*(30Sv>' '3n :id 4-000t'-dosui'a^ Su"a:s4 4 .00*Met^oitvc^torS"form <e:on«C^io^da^cTo»ao^«neArocioi-- -O 15Aroclo'-^ 22 'Arocio'-1232i ' ^C lOr- : 24:-i-'DC!Or * 248A-lC'.Gf ' 2 5 4A'oc-o ' * 25C

V( y Voluf«* o* SJtt-ac : in(<c:«d (uOV€ = Volume of wa:e' 9*trac:e< j iml)

V( »a' sa — u-e s*trac:«c! (g)

: lull

or w.

001546

•- -.. . •. ., . rr a « r --,— ^J - _ •. • I * • t« — " — — -J _;

SAMPLE FD321

•5C

Orga n i c * An a l y s i s Data 33p * c t r i x Corpo ra t i o n

159 ANALYST. TTO

Page 5CASE NO. : 3296

DATAF1LE: EU01002C04B. TENTATIVELV IDENTIFIED COMPOUNDS

CA3 4 SEMI VOLATILE COMPOUND NAMES

/$£-2/~y fiC&TlC /?£/£> /"/Wff3*M4£7#V£*UNKNOWN .00ESH7 MATCH_ _. . . . . _ _ . mumm SPECTRA

jy'Qjj-. >«3 3 •- — '• '• j .y..»— y.f*. — . . , - . ,*Ki.M, r, ter, . . . . , , _.

^ -~ y UNKNOWN. OOESN7 MATCHANY UDHW SPECTRA

SCANtt

^7S£ 272322336348355422

PURITY AMOUNT

UG/I?9^/ 270O J

55COO J^^" 540 J

<7<3 / 720 J9<!)/ 300 J

530 w

eu • . 3 l u e - A I i R e s p o n s e f a c t o r is a s s umed

001547

SPECTRIX

SEMIVQLATILE SOIL REPORT

DC ft 5296-14

AMPLE ID.F .ENAMECLIENT0ATECALIB

SCAN*532763

1063131 117671995373332

1203650957

1397

FD321EU01Q02C04EPA

INJECTED 01/24/86 13 : 10 :003TD DATE 1/17/86

CI30CI40CISOCI60CI70CI73CS50C343CSS5CS20CS25CS3O

SeWVOLATtLE COMPOUNDS1,4-B1CHLOI«3BENZEND-D4 ## IS! *#NAPHTHALENE-08 *#- IS2 *«ACENAPHTHENE-D10 *» I S3 **PHENANTHRENE-D10 ** IS4 **CHRYSENE-D12 ** IS9 ##PERYLENE-D12 ** IS6 **2-FLUQROPHENOL ** SU1 #*PHENQL-D5 #* 8U2 **2, 4,6-TRIBRQHOPHENdL ** SUS **NITROBENZENE-DS *# 8U3 »«2-FLUUQROBIPHENYL ** SU4 #*TERPHENYL-D14 #* SU6 *»

M/ff13213616418S2402641 1299330

82172244

INST ID.ANALYST

5 ICOTTQ

VERIFIED BY *>fffyCGRR. FACTOR

AMOUNT1560156O156O1560156O1360

5238684054

148

UG/KGUQ/KOU6/KGUG/KGue/KeUG/KS%7.X7.XX

111111001000

39.00

RRT. 000. 000.000. 000. 000. 000. 676. 964. 132. 852. 900. 904

AREA914c

3000*1275 i2356^12381602889

1277263619

21301823

tcift•-c

001548

(3) Regional Office:Sampling Personnel:

, .(Phone)Sampling Date: . % -/ ;* - ' r

, ..jgtn) (End)

For each sample collected ipeeffy numberof containers used and mark volume leveloneaehbotUe. * -

Wat0r(Extractahle)Water(VGA)

Number ofContainers ApproximateTotel VolumeSanrole Condition^- "on Kocaipt («.g.f broken, n^ice, Chain-of -Curtody, etc.)

© Shipping Information

Name of Carrier

Date Shipped:

Airbill ftumber® Sample Description__ Surf ace Water__ Ground Water__ Leachate

Soil/Sediment(ExtractalDle)Soil/SedimentCVOA)Other

Mixed MediaSample Location

f A*~n«f.'rt' t_ / Solids

Other (specify)

Special Handling Instructions:(e.g., safety precautions, hazardous nature)

LABOgEYFOR REPUBN 10.8110

001549

Laboratory Mama:Lab Sampt* » No:

Matrix; ~~—

Organic* Analysis Data Sheet(Pagel)

Caw NO.

Sample Number

Data fW»sa* Authorized By:

OC Report No:Contract No:Date Sample Received:

CASNumber

Volatile Compound*

Dam Analyred:Gone/Oil factorPercent Moisture:Percent Moisture (Decanted):

ug/lorug/Kg(Clreto One74-87-374-83-07S-01-47S-00-379-09-287-84-176-15-07S-3S-478-34-3156-60-567-66-3107-06-27S-93-371-S5-656-23-5108-05-475-27-4

CMorometHartft8romrjmetn*n«Vinyl CHforitfeGhtoroethaneMethyferte ChlorideAcetoneCarbon Oisulfida1 , 1 -Oiehloro«ih«n01. 1 -OtehloroethaneTrans'1. 2-OicHtoro«thanaChloroform1. 2-Diehloroethane2-8utanone1 . 1 , 1 -TnchlofMthant*Carbon TetrachlondeVinyl AcetateBromodichlorom«thane

CASNumber7d-34-S78-87-510061-02-679-01-6124-48-17S-00-S71-43-21 0081 -01 -S110-7S-875-25-2591-78-6108-10-1127- 18-4108-88-3108-90-7100-41-4100-42-5f

ug/l or ug/Kg(Clret* Qua)

1, 1. 2, 2-T«raeh[of«etri3na1, 2'OichloropropaneTrana-1. 3-OichloropropeneTrie hloroat handOibromochloromathane1, 1. 2-Trichforo«thart0Benzenecis-1. 3-0ichfordpr60ene2-ChloroflthylvinylctherBromoform2-Hexanone4'Methy[-2-PentanoneTetrachloroetheneTolueneChlorobenzeneElhylbenzeneStyreneTotal Xylanas

Oata Rvponing Oualificn^or rvoarting r*iufl* to E^A, (h* following rMufti <|ual)fi«n ar« tnwf.ArfdiikWijI Higs or footnarat explaining iwsults v* •neoufCgKl- Hov«w»r, th*difinrtton o< ueh fl«g must h« «0J<eit.

VahM 8 th* re<utt i* a valu* graa»r than or ao,u*l to th«<bit«ction taut. r*o0rt th* vat(M

U bfdiejilH compound vnt anltVMd for but not dataet**.fUDort ih* minimum daiceiior) limit for th* umpf* %wih

C

. ffhM f* rtol n*e«uri th* inttmmcnt.} Th* tootnof* thould r**d: U-

GomjMxmd WMI am Vud for but not dttaeud. Th*number tt fh* mtntmum atfct-wbt* d«t«ctton timit for

IndtcatM an titlmaud v*lu# Thia lUfl it ut*d arthcrMrfi«ii Mtimaimo • a9Tte«n!r*tlon for MntllivctyidtntifMd eompoundi wh«r* a 1:1 r**oons*i»«Mumador wtan tfw m*u C0*nf«4 dila indicatM lh« ort»«*y:«ef a compound that m**u th* nttnttftcation criteria butlh* r*tu)t i* Itu than Ih* tpMifM tfMKtnan iirmi bui0nui*r than wo (• g,. 1QJ)

Thu flag ipcliM to p*itieid« paramatdrs wfw« ih*idcnirffcation hit b*«n corrftrmad by GC/MS. Singl*eemponafit p*iticid«i2:10 ng/ul in Ih* (incl txtraefihould b* c«nf(rm*d by QC/MS.

This fl«g it u**d when th* an*M* I* found in th* MiniH wad ft a umpt*. ft iruttui** noHibla/pfobfibicblank eoritamiiatidn tnd warns th* data uMr to t*k*IpprotXiat* action.

Othar «o*eif « flag* and feotnotas may b* r*quir*d topropvrty define in* rasufu. S ut*d, thay must b* fully0>Mrib*d and lueh d**crip(iort atlKhod to th* datasummary report.

001550

Laboratory Name: SPECTf l i yNo:

ORSANtCS ANALYSIS DATA SHEET(Page 2)

3 Nutsber |t FD322 Ii—__________j

3EMIVOLAT1LE COMPOUNDSeertcentratfoni LQKSate Extracted/Prepared:Bats Analyzed iConc/Di l Factors _Percent Hoisture: (Decan ted * _GAS Number108-95-2 Phenol . . , . . . . . . , 4 2 0U 1 -44-4 b i s (2-Ch l o r o e t h y l > E t h e r ! 42095-57-8 2-Ch lo roph eno l . . . . . . 4 3 05 4 1 - 7 3 - 1 1 ,3 -D i c h l o r o b e n z e r > e . . , 420106-46 -7 l ,4-Di c h l o r ob«nz e n e . . . 4 2 01 0 0 - 5 1 - 6 Benzy l Al coho l . . , . . , 4 2 095-50- 1 i ,2 -D i c h l o r o b e n z e r i s . . . 4 2 095-48-7 2-Methy lpheno l . . . . . , 42039638-32-9 b i s (2 -Ch l o r o i s o p r o p y l ) E t h e r 420K -44-56 t 64-76 7 - 7 2 - 198 -95 -378-59- 18 8 - 7 5 - 51 0 5 - 6 7 - 965-85-01 1 1 - 9 1 - 11 2 0 - 8 3 - 21 2 0 - 8 2 - 19 1 - 2 0 - 31 0 6 - 4 7 - 887-68-359-50-79 1 - 5 7 - 67 7 - 4 7 - 488-06-295-95-49 1 - 58 -78 8 - 7 4 - 41 3 1 - 1 1 - 3208-96-899-09-2

4~Methy lpheno l . . . . . . 4 2 0N-N i t r o s o -D i - n -P r o p y l am i n a 4 2 0 ,Hexa c h l o r o e t h a n e . . . . . 4 2 0 ,Ni t r o b e n z e n e . . . . . . . 4 2 0 ,I sophorone . . , . . , . , 420 ,2-N i t r o p h e n o l . . . . . . 430 .2,4-D i f f l e t h y l p h e n o l . . . . 4 2 0 ,Ben z o i c A c i d . . . . . . . 2000 .b i s ( 2 -C h l o r o e t h o x y )M e t h a n e 120 .2 ,4 -D i c h l o r o p h e n o l , . , . 420 .1 , 2 ,4 -T r i c h l o r o b e n z e n e , . 4 2 0 .N a p h t h a l e n e . . . . . . . 4 2 0 .4-Chloroa tn 1 m e . . . . . 4 2 0 .Hexa c h l a r o b u t a d i e n e . , . 4 2 0 .4-Ch l o r o -3-Me t h y l p h @ n o l . 42o !2-Ke t h yJ n a p h t h a l e n e . . . 4 2 0 .Hexa c h l o r o c y c l o p e n t ad i e n e 4 2 0 .2 ,4 ,6 -T r i c h l o r o p h e n o l . , 4 2 0 .2 ,4 ,5 -T r i c h l o r o p h e n o l . - . 2 0 0 0 ,2-Ch l o r o n a p h t h a l e n e . . . 420 .2-N i t r o a n i 1 i n e . . . . . . 2000 .Dine thy l Ph tha l a t e . . . . 420.'Acenaphthy l cne . . . . . . 420.3-N i t r o a n iHn e . . . , . , 2000.

. U

. U- U, U, U

UUUUUUUUUUUUUUUUUUUUUUUUUUUU

8PC Cleanup __ Yes JL NoSeparator? Funnel Extract ion __Cont inuous L iqu i d-L iqu i d Extract ion Yes

. EM Number83-32-951 -28-51 00 -02 -71 32 -64 -91 2 1 - 1 4 - 2606-20-284-66-27005-72-386-73 -71 0 0 - 1 0 - 6534-52 - i86-30-61 0 1 - 5 5 - 31 1 8 - 7 4 - 18 7 - 9 6 - 585-0 1 -81 2 0 - 1 2 - 78 4 - 7 4 - 22 0 6 - 4 4 - 0129 -00 -0B5-68-79 1 - 9 4 - 156-55 -31 1 7 - 8 1 - 72 1 8 - 0 1 - 91 1 7 - 8 4 - 02 0 5 - 9 9 - 2207-08-95 0 - 3 2 - 8193-39-55 3 - 7 0 - 31 9 1 - 2 4 - 2

Acenaph thene - .2 ,4-Q i n i t r o p h e n a l . . . .4-Ni t ropheno l . . . . . .D i b e n z o f u r a n . . . . . . .2 ,4 -D i n i t r o t o i u e n e . . . .2 ,6-D i n i t r o t o l u e n e . . . .B i e t h y l p h t n a l a t e . . . . .4-Ch l o r op h e n y l - p h e n y l e * r ,9rf i.. -4-N i t r o a n i l i ne . . , . , .4 ,6 -D i n i t r o -2 -M e t h y l p h = n o lN-N i t r o god i p h e n y l a s i i n e ' 1 )4- Br o»op hen y l * pheny l e t t e rHexa c h l o r o b e n s e n e . . . .P e n t d c h l o r o p h e n o l . . . .Phenan t h r e n e . . . . . . .Ant h r a c e n eF luo r a i t h e n ePyrene . . . . . . . .Bu t y l b e n z y l p h t h a l a t e .3 , 3 ' - D i ' : h l a r o b e n 2 i d i n e

. . .b i s < 2 -E t h y l h e x y nP h t h aU t eChr y s e ^ e . . . . , . . , .O i - n -Oc t y l Ph t h a l a t e . . .B e n z o ( b ) F l u o r a n t h e n e . . .B e n z o fk )F l u o r a n t h e n e . . .B e n z oU 'P y r e n e . . . . . .I ndeno i 1 , 2 ,3- c ( l )P y r e n e . .D i b e n z fa, h) Anthracene . .Ben zo ( g , h , i JPe r y l e n e . . ,

420. U2000. U2000. U

420, U420 . U420. U420 . U420. U420. U

2000, U2000. U

420, U420 . U420. U

2 0 0 0 . U420. U420 . U420 . U420 . U420 . U4 2 0 . U840 . U420 . U420, U420 . U420 . U420 . U4 2 0 . U4 2 0 . U420. U420. U420 . U

( 1 ) - Cannot be separated frost d i pheny l a s t i n eForm I

000032

001551

£? £C73; ( ; x- * . - * ; ;N

Organics Analysis Data Sheet. . . . . , -

S*mpl« Number

Consent fairer LowDate Extracted PreoaredDate Ana(yz«tf «..—_„.Cone 'Di* Factor ————

Pesticide PCSs@PC DV«s DNo

rvA«f f«fracContinuous Liquid - Liquid Extraction

Percent Moisture (decanted^CAS

On*)3 '3 -3 . i - 53 -9 . 35 ^3 * 9 - 3 6 - 3S3-39-975-^-33C9 X-:102-s-5~-39 5 9 - 3 9 - 36C-5V- '7 : -55 -972-20-33 3 : ' 3 - 6 5 - ?72-5 - i - 31 C 3 - - 0 7 - 3SC- :9 -37:-- l3-55349- : - "C -557 .74-98001 -35 212674 . ; 1 - 21 1 ' 0 4 - 2 9 - 2M M : - ' S - 453469 : • • ?i 35" 2 -29 oM C 9 - 5 3 - *

Aic*3-3*-C3e;a-3HCDe-ta-3^C•od^^a-SHC L'^ea"*1"•*313C"»IOCAiCtT--*«gta;^*o' ssoxiceS^dosuifan iOi-'Gr«ni 4 -OOt;ncrmr^doSut'an !l4 i ' -OOO±-*dosui*3r- Sutfgtea 4 -DOTVletnoavc^lor= -df:n <e!oneC^iofdaneto«ao*«"«AroclOf- 1 0 1 6A. ' -3C IO ' - 122 1Ar s c lO f - 1 232A-3C! e r ^24 :A . - X ! o r - ' 2 4 8A. ' iC 'C' - ' 254

' ^ 0 5 6 - 3 : 5 | A-ac-o ' ' 260

o^ exi'aci in(ec;ed (oOs Volume of watar extrac:ed [ml)• Wetgttt o' sa — s-e e<trac:ecJ !g)> Voiur"« a' total extract mM

or w.000033

001552

n ID: 5100 _ .Speetrix DC # 3296-8

SAMPLE: FD322

Organic a Analysis Data Sheat - Page 5LABORATORY NAME: Speetrix Corporation CASE NO. : 5296QC REPORT NO. : 159 ANALYST: TTO 0ATAFILE: EU01002C03

B. TENTATIVELY IDENTIFIED COMPOUNDS

CAS # SEMI VOLATILE COMPOUND NAMES SC AN# PURITY AMOUNT

-y-

269279290296379

US/*84000 J

1000 J780 J330 J900 J

J » Est imated value - A 1:1 Response Factor is assumed

000035

001553

SPECTR IX DC # 5296-14_ 6ID

. —ENAWECLIENTDATE INJECTEDCAL1B STB DATE

SEMIVQLATILE SOIL REPORTFD322EU01002C05EPA01/24/86 19 :00 :00

INST ID.ANALYSTVERIFIED BY

9100TTO

1/17/86 CQRR. FACTOR 42.00SCAN*

329756

1062131217671995315SOS

1203636956

1397

CI30CI40CI50CI60CI70CI75CS50CS45CS55CS20CS25CS30

SEMIVOLATILE COMPOUNDS1-4-DICHLOROBENZEND-D4 ** IS1 *NAPHTHALENE-08 *# IS2 #*ACENAPHTHENE-D10 ** IS3 ##PHENANTHRENE-D10 ## IS4 **CHRYSENE-D12 ** IS5 *#PERYLENE-D12 ** IS6 #*2-FLUOROPHENQL ** SUt #»PHENOL-D5 ** SU2 **2,4,6-TRIBRQMQPHENOL ** SU5 *#NITROBENZENE-05 ## SU3 **2-FLUUOROBIPHENYL #* SU4 **TERPHENYL-^014 ** SU6 **

M/e1521 36164ias2402641 1299

33082

172244

AMOUNT RRT AREA1680 UG/K61680 UG/KQ1680 UG/KQ1680 US/KG168O UG/KG1680 UG/KG

82 X61 X73 X57 X69 X

124 X

1 .0001 .0001 .0001. 0001. 0001. 0000. 5950. 9551. 1330. 8410. 9000.904

967316113042197107451 1

14862160

288930

27931329

001554

Case Number:jr -^,^r ._

Sample Site Name/Code:

•(3) Regional Office: _j2£—Sampling Personnel:

y^-A r &_ ..frjfasi /"(Name) J

"7/ c '1 * -; •*"*/ "*f(Phone)

Sampling Date: ? /^/Vjgm) (End)

© Shipping Information

...... . . ..... /-l-/1

Name of Camer

Date Shipped:

A'/? ^/^? x*;^Airbill Number:

(D Sample Description__ Surface Water ___ 'Ground Water _y__ Leachate — .

@ SAMPLE CONCmfmfflTON ®^fupTo:(CheckOne) ^Vtr^

- lowConcsntration f9/l Fo^^/ *«>" >^o—— Medium Ccmeetitration Mxui.^^/ r)( v/ j- - Ittte:(3) oAIVlli lj£» IVIA TRJX ^^^^^ « ^ ^^^H ^^ _ ^^^^ ^^^B{^eek is} W^^^^^

__ Water I nsf^r^^-Soil/Sedimeat Ship To:

(D For each sample collected spof containers used and mark von each bottle.

Number ofContainersWater(Extractable)Water(VGA)SoH/Sedlment(Extractable)Soil/Sediment f(VDA)

~sOther

• <* '

ti

_ Mixed Media^Solids

Other (specify)' *> *• -

ecify numberolume level

ApproximateTotal Volume

7- // / ..V.I, .'

@ Analysialrab:^dbr'-^^^CDate tfatAj&Lfy.gg.Sample Conditionon Receipt (e.g., broken, ncice, Chain-oi-Custody, etc.)

® Sample LocationCtoJtf' ac'<^<fyK ?l'?"-7(,'

/r=N Special Handling Instructions:(e.g., safety precautions, hazardous nature)

innnnd?LAB COPY FOR RETURN

001555

atory Maee: 5PECTRIX CORP.MO) Nuibtfr

FD328QR8AHICS ANALYSIS DAIA SHEET

(Page 2)

Concen t ra t i on ;Date Analyzed!Gooe/flU FactaraPercent Mois ture :CASNu s b e r

U^L,flti/flA/flf01/13/96

(De c a n t e d? _

108-95-2l t i -44-495 -57 -85 4 1 - 7 3 - 11 0 6 - 4 6 - 7100-5 1 -695-SO- l95-48-739638-32-91 ^ ' -44 -56. 44 -76 7 - 7 2 - 198-95-378-59 - i8 8 - 7 5 - 51 0 5 - 6 7 - 96 5 - 6 5 - 0l l i -9 i - l1 20 -63 -21 2 0 - 8 2 - 19 1 - 2 0 - 31 0 6 - 4 7 - 89 7 - 6 8 - 359-50-79 1 - 5 7 - 67 7 - 4 7 - 48 8 - 0 6 - 29 5 - 9 5 - 49 1 - 5 8 - 788-74-41 3 1 - 1 1 - 3208-96-899-09-2

Phenol . . . . . . . . . .b i s (2-Ch la ro e t hy l )E th e r ,2-Ch lo raph ena l . . . . . .1 .3 -D i c h l o r o b e n2e n e . . .1 .4-D i c h l a r o b e n z e n e . , .Benzy l Alcoho l . . . . . .J, ,2 -D i c h l o robenzene . , .2-Methy I p h e no l . . . . . .b i 5 {2 -Ch l o r o i s 5 p r o p y l ) E t h e4-Me t h y lD h e n o l . . . . . .N-N i t r o s o -D i - n -P r a p y l aB i n eHexa c h l o r o e t h a n e . . . . .N i troberuen-e . . . . . . .I sopnorone . . . . . . . .2-W i t r o p h e n o l . . . . . .2,4-D i f n e t h y I p h e n o l . . . .Be n z o l e A c i d . . . . . , ,b i s ( 2 -C h I o rOB t h o x / )M e t h a n e2 ,4 -D i c h l o r o p h p n o l . . , .1 , 2 ,4 -T r i c h l o r o b e n z e n e . ,Naph t h a l e n e . . . . . . .4-Ch I o r o a n i l i n e . . . . .Hex a c h l o r o b u t a d i e n e < . .4~Ch l o r a -3-Me t h y l p h e n o l2-Me t h y l n a p h t h a l e n e . . .Hexa c h l o r o c y c l o p e n t ad i e n e2 ,4 ,6 -T r i c h l o r o p h e n o l . .2 ,4 ,5 -T r t c h l o r o p h e n c l . .2 -Ch l a r o n a p h t h a l e n e . . .2-N i t r o a n i 1 i n e . . . . . .Dimethy l Phtha l a t e . . . .Acenaph t hy l e n e . . . . . ,3-N i t r o a n i l i n e . . . . . .

390, U390. U390. U390. U390. U39u. U390. U390. U

r 390 , U390 , U390. U390 . U390 . U390 . U3 9 0 . U390 . U

1900 . U390 . U390 . U390 . U390 . U390 . U390 . U390 . U390 . U390 . U390 . U

1900 . U3 9 0 . U

1900 , U390. U390. U

1900. U

SPC Clsanup __ Yes J^ NoSsparatory Funnel Extract ion __ YesContinuous Liqu id-Liqu id Extract ion Yes

83-32-951 -28-51 0 0 - 0 2 - 7132-64-91 2 1 - 1 4 - 2606-20-284-66-27005-72-386-73-71 00 - 10 -4534-52- 186-30-610 1 -55 -31 1 8 - 7 4 - 187-86 -585 -0 1 -81 2 0 - 1 2 - 78 4 - 7 4 - 22 0 6 - 4 4 - 01 2 9 - 0 0 - 085-68-79 1 - 9 4 - 156-55 -31 1 7 - 8 1 - 72 1 8 - 0 1 - 91 1 7 - 8 4 - 0205 -99 -22 0 7 - 0 8 - 95 0 - 3 2 - 9193 -39-533-70-5( 9 1 -24 -2

Aeenaphthene . . . . . . .2,4-Din i t r oph e no i , , , .4-Nitrophsno l . . . . . .Dibenzofuran . . . . . . .2 ,4-D i n ; t r o t o l u e n e . , . .2 ,6-Din i t r o t t l u e n e . . . ,Die thy l ph t ha l a t e , . . . .4-ChIoropheny l -pheny l e t h e rFluarene . . , , , . . , .4-N i t r o a n i l i r t e . . . . . .4 ,6 -0 i n i t r o -2 -H e t h y l p h e n o lN-N i t r o s o d i p h e n y l am i n e ( 1 )4-Brof f l apheny l -pheny l e t h e rHexa c h l o r ob e n z e n e . . . .Pen t a c h l o r o p h e no l . . . .Phenan th r en e . . . . . . .An t h r a c e n e . . . . . . . .Di - n -Bu t y l p h t h a l a t e . . .F l u o r a n t h e n e . . . . . . .Pyrer ie . . . . . . . . . .Bu t y l b e n z y l p h t h a i a t e . . .3 ,3 ' -D i c h l o r o b e n z i d i n « . .Be n z o ( a I An t h r a c e n e . . . .b i s ( 2 -E t h y l h e x y l ) P h t h aU t eChrysene - , , . . . . . .D i - n -Oc t y l Ph t ha l a t e , . .8eru a ( k )F l u a r a n t h e n e .B e n z cU )P y r e n e . . . .I n d s n o < 1 , 2 ,3 - c d JP y r s n ef i i b e n z ( a , h )An t h r a c e n eB9 n z o ( g , h ,

390. U1900 . U1900 . U

390. U390, U390. U390. U390. U390. U

1900 . U1900 . U

390 . U390 . U390 . U

1900 . U390. U390 . U390 . U390 . U390. U390 . U770 . U390 . U390. U390 . U390, U390. U390, U390 . U390. U390. U390. U

( 1 ) - Canno t be separated froa d ipheny lao ineForm I

001556

SPEtfRIX DC * 5296-14tfU

SAMPLE ID.

CLIENTBATE INJECTEDCALXB STD DATE

SEMIVOLATILE SOIL REPORTFD323EU01002C06EPA01/23/86 14 :48 :00

INST ID.ANALYSTVERIFIED BY

3100TTO

1/17/86 CQRR. FACTOR 39.00

SCAN* SEMIVQLATXLE COMPOUNDS M/e AMOUNT -r RRT AREA954763

1062131117661993377935

1200690956

1596

CI3OCI40ctsoCl^OCI7OCI79CS90CS45CS95CS2OCS25CS30

1.4-DICHLQROBENZEND-D4 »* IS1 *#NAPHTHALENE-DS *» I 82 **ACENAPHTHEWE-D10 *# IS3 **PHENANTHRENE-D10 ** JS4 #*CHRYSENE-D12 #* IS5 *#PERYL£NE~D12 ** IS6 **2-FLUOROPHENOL ** SU1 *#PHENOL.-DS ** 8U2 **2, 4,6-TRIBRQMQPHENGL ** SU5 **NITROBENZENE-09 ** SU3 **2-FLUUOROBIPHENYL ** SU4 **TERPHENYL-D14 *» SU6 *#

19213616413824026411299

33082

172244

15601560i960196015601960

3031

1033145

131

U0/KOUG/K©UO/KCUG/KGUG/KOUG/KGxXXX.Xy.

i.i.i.i.i.i.0.0.i.0.0,0.

000000000000000000631966130S92900904

3103O211492300522351170907901462402

18372913

000055

001557

Agcni D*22313 703 b&7

Organics Analysis Data Sheet(Page 1 (

Sample Numboi

Laboratory NamefLab Sample ID No:Sample MatrixData Release Authorized Sy:

Case NoQC Report No:Contract No:Date Sample Received:

Volatile CompoundsConcentrationf/^ Lovv^) Medium (Circle One)Date Extracted/Prepared;«TDate Analyzed: —_Conc/DM Factor:Percent Moisture:

-pH

Percent Moisture {Decanted}CASNumber ire to On*) CASNurtfoar74-87-374-63-975*01 -475-00-37S-09-267-64-175- IB-075-35-475-34-3156-60-567-66-3107-06-278-93-37 1 -55-656-23-5108-05-475-27-4

ChlofomethaneBromomeihaneVinyl ChloridsChloroeihaneMethylene ChlorideAcetoneCarbon Disulftde1, 1-Oichloroftthene1. 1-OichloroethaneTrans-1, 2-Dichloroe!heneChloroform1, 2-Oichloroethane2-Butanone1 . 1 . l-TnchloroethaneCarbon TetrachlondeVinyl AcetateB ro m odic h lor om ethane

/fi^,4-.6"&.(el.LS.(«A.G,.11A.II.&3A1&,,*/<L ,l . i1 .49.9i,f;

(Circle One79-34-578*87-510061-02-679-01 *6124-48- ;79005• » 1 -43-210061-01 -51 10-75-875-25-2591-78-6108- 10 - 11 27 - 18 -4108-88-3108-90-7100-41-4100-42-5

1 . 1 . 2 . 2-T«trachforoeinan*1, 2-DichIofopre&aneTrans-1 , 3-OiChloropropftneTrichforo« thaneDibromochtorometha ne1 . 1 , 2-Tnchloro«than€Benzenec.s-1, 3-Dichloropropftne2-Chforoethvlvinv(etherBromoform2-Hexanone4-Mcthyt-2-PenianoneTeirechloroethcneTolueneChlorobenieneEthylbenzeneSlyr«neTotal Xylenes

fljA.9&^,^;s. . . *E *Y.7(*l,*l2.V-/,3L5.8

. .3ff/,_A. & 9.41**7^ > L/ . ^/. /K 5i.i

Data Reporting Qualifier*For reporting ratults to EPA. the. following f«iuHs qualifier& arc ut«dAdditional flags or fooinotas aKplnning rasuMj are encourageddafmiiton of each flag mull b* •itplicit

, the

H the raiutt IK a w*'tw 8r***tf |t>an °r •a""1 to *h*detaction limit, irapori the valu*

C

u Iftdtektat eompound w»* enaiyiad forRcpon lh» minimum dfltacfion limn for th« sample with(h* U (• o . 1dU) baMd on neeaitarv eoncamratwn'Ihlution acttoni O**"* >l not fMcatlinly l^» inatrumentdetection limn |Th« footnote ahouldraad UCompound w*i«n»iyT«d'w but rwi*siaci»d Th#

IB th* minimum attainable dctaction limit for

Thtl flag applies <o pwilifitd* p«r«m«(ori wttB^e tK*cd«mifie*l*6A h»t b«tn eonfifnwd by GC'MS QmgleComp«n«nt 0«mctd«i >10 ng 'ul tn (M linal *Mratlthouid ne confirmed by GC 'MS

Thu flag n UMd wh«n th# «rt*tytf tft found in the blank»t wtll as a tampli, \\ mdtcaMt po*t'W» robiirjtirfaJanfc contamination and warn* th* data uwr to take

OthctIndtcaieB an •intn*i«d v*lu» This flao i& ut«d aitnar

• whan aatimfeting a concentration for tantatiw<v~ Mt*nlrfiad comooundt wtw* * t 1 rainnnt*

th* masit »p*f n»* data

ip^eific flsgi and footnolaa may b*prop^'lvdo'ifw l*w rctuliw N u*«d. |h*»mu»l h* fullytfdtrriborj and luch OviMtptKin anachod 10 th* dat*

000072001558

SPECTRIX DC fEmm onmentil Protection Ag*n«v, CLP 6*mpl« Mafttfftment OHic*.P O Box 818. Al««jnd/ra. Vi^jmij 223U 703'S&7-24SO

Organics Analysis Data Sheet(Page 2)

Semivol&tite CompoundsConcentration: Low MediumOtfe Extracted/Prepared:Date Analyzed:Coric/DH Factor;

.ufl/ldr ug/Kgircla One) CASNumber62-7S-9108-95-262-63-311 1 .44-495-57- 6541-73-11Q6-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-186-75-5105-67-96S-85-01 1 1 -9 1 - 1120-83-2120-82-191-20-3106-47*887-66-359-SO-791-57-677-47-486-06-295-95-491-58-788 74-413 1 - 1 1 -3208-96-899092

N-Nnrosodrm*UiylammePhenolAnilinebis(-2-Chloroathyl)Eth«r2-CHforoph«ne>I1 , 3-Dichlorobdnzeno1 , 4-Oichfofobcnten0Benzyl Alcohol1. 2-Dichlorob«nz6ne2-Methylphenolbis{2-chloroisopropyl)£ther4-MethyIph«nolN-Nitroso-Oi-n'ProoyiamineHexachioroethaneNitrob«nz«n«fsophorone2-Nitrophenol2. 4-Oimethy)phenolBanzoic Acidbis(-2-Chlofo«thoxy!Methane2, 4-Oich»orot>henol1 . 2, 4-TrichtorobenzeneNaphthalene4-ChloroanilmeHexflchlorobvUBdione4-Chloro-3-Meihylphenol2-Methytrtaphth«leneHeKachtorctyttep«ntnd(ene2, 4, 6-Tnchtorophenol2. 4. 5-Tf ichtorophenol2-Chloronaphsh«lene2-NitroaniIincOimothyl Phth«latflAcenaphthyteno3-NiitoHniiinn

H1,9JtfeftaiJ*M™IDto.O•?.<(13

^.(ofc.7-6.2."»-SI.T1^4& ,I.Tun

_. ,1*1i*D^.-5O

fl M^-o415.35, „„4^4,fo3.Si -T^.(oft . *73iOl- r

i.*:I3

S3-32-951-28-6100-02-7132-64-9121-14-2606^0-284-66-2700S-72-386-73-71 00-01 -S534-52-166-30-6101-55-31 18-74-187-86-585-01-8120-12-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-9117-64-010549-2207-08-950-32-8193-39-5S3-70-319 1 -24-2

Aeenapmn«ne2, 4-Dinitrophenol4-NitfophcnolDibfln/ofuran2. 4'0initrotofuene2,6-Din-trotoluencDielhylphihalate4-Chforophenvl-phenyletherFluorene4-Nitroantline4, 6-Dimtro-2'Mdthylph«no(N-Nitrosodiphenylamme (1)4-Bromophenyl-phenyletherH«xachlorobenzenePentach(oroo"«nolPhenanthreneAnthraceneD' n-8utylphthafateFluorantheneBenzidinePyfeneButylbenzylphthalate . •3. 3'-Dtchiorobenzidine ^Qfinzo<a}Anthracanebig(2-Ethylhaxyl}PhthataieChryseneOi-n-Oclyt PhthBlat«Bftnzc^h)Fluor«nthene8-?atcHklF!uoranthen«Benzc^alPyfoneIndentML 2. 3-cd)Pyr«neDibeni(a, h)Anthrac«n»Benzo^p, h, iperylene

I .7fe.!Ifc*O ......1.1 _sz3.53«O(.-73.0(&1.1

75.0I.Tl . *7__ _ _I .-7 ....1/7-?.O3.0Z34,foK-7

JP1.7-^ ———i.r?...as

-4i2^_-foeZl.*7.0* .9

9.6(It-Cannot tw Hparated Irom 007

001559

SPECTRIX DClion Ag*ncy, CLP Sampi« Man*gflm*m OH.ce,

*». O. 008 818. Atexfffltaa. Virginia 22313 703 '557-2490

Organics Analysis Data Sheet(Page 3)

Sampl

Pesticide/PCBsConcentration Low MediumOats Extracted'Prepared: —————Date Analyzed:,——————————

(Circle One)

Conc/Dil Factor:CASNumber ug/Kgfete On*)319-84-6319-8S-7319-86-858-89-976-44-8309-00-21024-S7-3959-98-860-57-172-55-072-20-833213-65-97: -54-87421-93-41031-07-850-29-372-43-553494-70-557-74-98001-35-212674- 1 1 -211104-28-21 1 1 4 1 - 1 6 - 553469-21-912672-29-611097-69-11 1096-82-5

AJQha-BHCBeta-BHCDeha-BHCGamma-BHC (Lmdane)HeptaehtorAfdrinHeptachlor EpoxideEndosulfan 1Oieldrin4, 4--0DEEndriciEndosulfan tl4. 4--DDDEndrin AldehydeEndosulfan Sulfate4, 4'-DDTMethoxychlorEndrin KetoneChlordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260

fe.q&.qs.sS.D(b.q3.03.SA.T11i.q\i4.b4. to14n.s

fc,^17Jto40T^M4!ISZ<b

. 16Z.-JOft»fe>

Vp = Volume of extract injected (ul)Vs * Volume of water extracted (ml)Wf B Weight of sampla extracted {QtV, * Volume o* total extract (ul}

orW. V.

000074

001560

Organics Analysis Data Sheet(Page 1 )

Sample O.L..NO.

/orstor> NameLab Sa-npie ID NSarnp'6 Matr ix

SPECTR IX CORPORATION Case NoQC No

Data Release Authorized ByContract No -68-QHDate Sanpie Received

'65 , 70IS. 7149

Volatile CompoundsConcentration (Low) Medium (Circfe One}

Date AnaCone Di!Perceni IS

CASNumtwr74-87-374-83 975-0^-475-00-3

S-09-267-64-17 5 - 1 S - 075-35-475-34-3156-6C-567 -S6 -3107-06-27 8 - 9 3 - 37 1 - 5 5 - 65 6 - 2 3 - 5108-05-475-27 -4

Chloromethar-eSro^iomethancVinvi ChlorideC^'oroetha ogMcT^iylene hic'idcAc*to^cCarbon D'Su'f ide1 . 1 -Dichtoroeftsne1 . 1 -DicnlofQeT"'3*^eTrgrts-1 , 2-DicHi>C'oet"^p' isChloroform1 . 2-Dtch)orcHj:nane2-Bj ianone1 . 1 . l-TrchloroenaneCa rson Te'rac— londcVinyl AcetateB'OTiod.chiofO^eTiane

iyiertFartnr , _ .. .. oH

Moisture (Not Decar

ug 'lorug/Kg(Circle One)

/////£$.0

-~P'& •-•. _,.to,,'.,^

3'*t3$3.13.34 f-V?• 5*3.7

3*.*f-v.v3tf

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CASMumbar78-87-51 0 0 6 ^ - 0 2 - 6

L79-0-6: 2 4 - 4 8 - 17S-OO-57 - 1 -43 -21 0 0 6 1 - 0 1 - S1 1 0 - 7 5 - 87 5 - 2 5 - 25 9 1 - 7 8 - 61 0 8 - 1 0 - 11 2 7 - 1 8 - 47 9 - 3 4 - 5108 88 -31 0 8 ' 9 0 - 7100-4 1 -41 0 C - 4 2 - 5

» 2-0.ch 10 'o3-ODa-^eT ' a n s - l 3-Dic-no 'oc-oae-eTr.c^toroet^e^Dtbrornocnioronetia^e1 1 . 2-Trichioroe:nane8e-,reneC ' S - I . 3 -0 ( C* ^ IO * - 0'OQ6 - 1€2 -Chlo^oe* •* 1viv' '".yict'ie*SfOf^O'O'r^ 1

4 . M e 1 1 v i - 2 • ?e ; a fl o n e2-HexanoneTeirac'Mo'oene^e1 ^ T ^T ^ f c . * * ^ — * * - * «* r i- t

TolueneC*" i fo *oben2&neEinv'benjgnpStvreie> oiai X\ ip^es

ug 'f or ug 'Kg{Circi* One i^/7*j*1£>&>3,7V. 2-^,23,7^V9*^J.35,73'tf1.6*(>4-3*¥*/**£

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but not

3' <M

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so'i at 3j

be*'' coif-'-«(ffi o* GC MSng o' >n in* )"%«i «tira;i s^O t-nea o» GC MS

f ii indicate) oc-ii-tup O'^a-'t t>;a"» r c"1 : <•-'•" *>J TV!^p data dif 16 ta»« loo-OS- *:<• JIM"*

000075

001561

7RIX ClWCRATiJNCase 6865, 7013, 7U9

Concentration Low MediumDate Extracted Prepared —————Date Analyzed ————————-——.Cone 'D

Organics Analysis Data Sheet(Page 2}

Semivolatile Compounds(Circle One)

Sampt« NumberS'/OCD . C . No .

Percent Moisture (Decanted)

GPC Cleanup £Yes CNoSeosratory Punnel Extraction CYesContinuous Liquid - Liquid extract ion

CASNumber1C8-9S-

95 -57 -35 4 1 . 7 3 -

1 00 -5 ' -650-1

3 9 5 3 3 - 3 2 - 9106--J-1-562 1 *64 -6 7 - 7 2 - 198-95 -37 8 - 5 9 - T88-75-5105-67-965-85-0t n - 9 1 - i120-83-2120 -82 - 19 1 - 2 0 - 3106-47-887-68 3S9-50-79 1 -57-677-47-488-06-295-95 -49 t . $ 8 - 788-74.41 3 1 - 1 1 - 3JLSSJL99-09-2

2-010^00^6^0'

Alcoho)

BcnzoiC Acid

1 . 2. 4-Tnehlarot)enzene

4.Cu>loro-3-Metnyl0henoi2 -

2 4 6-TrichlOfQohenol2 4. 5-TfichloroDficnoi2 -C

33.9.0Z.o

30Z.o3-7/Z.2-0

3.O

£3L¥>£3,03,0

GAS

83-32-35 1 - 2 8 - 5

606-20-2

100-02-71 32 -64 91 2 1 - 1 4 - 2

84-66-27005-72-386-73-7100-01-6534-52- 186-30-61 0 1 - 5 5 - 31 1 8 - 7 4 - 187-36-585 -0 1 -81 20 - 1 2 -784-74-2206-A4.Q

29-00-085-68-79 1 . 9 4 - 156 -35 -31 1 7 - 8 1 - 72 1 8 - 0 1 - 91 17-34-0205-99-2207-08-950-32-81 93 -39 -553-70-31 9 1 - 2 4 - 2

2. 4-Oinitropnario!

2 4-2 6-Omitrotolu#ne

4. 6-( 1

Anthracene

Fiuo^anthane

3 3 -

Chrysene

SenzcXblPluorariihene

2. 3<d)Pvene

b* iflp«($i»d from

g.Q*6t O

2112.

Z5>J2L

.££,

73T

7 85

001562

SPE£[Rix CORPORA: rONLaboratory NameCas* No 68-01/6798^X6865. 70 1 : 149

Organtcs Analysis Data Sheet{Page 3)

Stmpla Number&OQO.L.O.C. No .

Concentration LowDate Extracted 'PreparedDate Analyzed _____Cone 'Oil Factor ._'. ... ...

Pesticide/PCBs(Circ le One) GPC Cleanup QYes DNo———————— Separatory funnel Extraction QYes————————— Continuous Liquid - Liquid Extraction GY*s

Percent Moisture (decanted)CASNumber u g - !

On«)3 - 9 - 3 - S - 63 ' 9 - 3 5 - 7319-36-853-39-376-44-0309-00-21024-57-3959-98-860-57- 1• . 2 - 5 5 - 972-20-83 3 2 1 3 - 6 5 - 972-54-81 0 3 1 - 0 7 - 85C-29-372-43-553494-70-55 7 - 7 4 - 98001 -35 21 2 6 7 4 . 1 1 - 21 1 1 0 4 - 2 8 - 21 1 1 4 1 - 1 6 - 55 3 4 6 9 - 2 1 - 91 2 6 7 2 - 2 9 - 61 1 0 9 7 - 6 9 - 11 ' 0 9 6 - 3 2 - 5

Aio^a-BHCBeta-BHCDe)ta-8HCGamma-3HC iLmdaneiMeo:ac^iorAidr>"N«otac->ior EooxioeEndosulfan 1D'eidnn

Hi A'- 006EndrmErtdosui^an II4. 4'-000E^dosulfan Sulfate4. 4'- DOTMethoxvcnlorEndrm KeioneChlordaneToxaphe.neAroc l o r - 1016Arocior-1 221Aroc l o r - 1232Aroc l o r - 1242Arcwlor- l 248Aroc to ' - '254Aroclo^ 1260

/?/3/%/*L.IS/£/$^1$II

12-n* . . . . . . . . . . . . . . . . ./*f/4-W/d1953co&&~%fIIIfoo100//¥71

V( 3 Volume o* QKtract m|3Ci«d (ul)Vs * Volume of water extracted {mtjWg * Weight of sample extracted (g)V = Votuma of total entracr (ul)

orW,

000077001563

tion Aflftncy. CLP S»"'O 6o«eie. Ateiandna. Vtrgmm 2 J 3 1 3 703 5572490

Organics Analysis Data Sheet{Page 3)

Pcsiicide/PCBs

Sample Number

Concentration* C Low ) Medium (Circle One)Date Extracted 'PrepareDale Analyzed ___Conc/Dil Factor: —CASNumber

ug/Kgirele One)

319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-87421-93-41031-O7-850-29-372-43-553494-70-557-74-98001-35-212674 - 1 1 - 21 1 104-28-21 1 1 4 1 - 1 6 - 553469-21-912672-29-61 1097-69- 11 1096-82-5

Alpha-BHCBeta-BHCDelta-BHCGamma-BHC (Lindane)HeptachlorAldnnHeptachlor EpoxideEndosulfan 1Dteldrm4, 4--DOEEndrinEndosutfan 114,4' -ODDEndrin AldehydeEndosulfan Sutfsie4, 4 '-DOTMethoxvchlorEndrin KetoneChlordaneTonanhoneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Arodor-1260

.063,004>• DOS-O03•00^

. .1.0001 . . . . . . . . . .•oosr• OOH• Di• O(j&

^fi&i^• OX.01..Ofe.. 1^. . . n3L.^(p ..„.&m»ot „. it,01 ..«p2.- 0 1• OZ• 003.»0 l . . . „ .*6$

V( - Volume of extract injected (ul)V& - Volume of water extracted (ml)Ws * Weight of sample extracted (fl)V( - Volume of total extract (ut)

or W.

001564

Laboratory Name:Case No: .DC No:

ib:3^00

Organics Analysis Data Sheet(Page 3)

Pesticide/PCBs

mle Number

Concentration:Date Extracted/Prepared:Date Analyzed:

Medium (Circle One)

Conc/Dil Factor:CASNumber ifCircte One)319-84-6319-85-7319-86-868-69-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-87421-93-41031-07-850-29-372-43-553494-70-557-74-98001-35-21 2674 - 1 1 - 21 1 104-28-21 1 1 4 1 - 1 6 - 553469-21-912672-29-61 1097-69-11 1096-82-5

Alpha-BHCBeta-BHCOelta-BHCGamma-bHC (Lindane)HeptschtorAldrinHepiachlor EpoxideEndosulfan 1Dieldfin4. 4'-DOE "EndrinEndosutfan tl4. 4 '-ODDEndrin AldehydeEndosulfsn SuKate4, 4'-DDTMethoxychlorEndrin KetoneChlordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242ArocIor-1248Aroclor-1254Aroclor-1260

.02.

.0W.0*1.Ql.01.01.02-*&1.,04.,&3 _.M-.07>&2~<rtt?JtL.07.22. tf/T.<96AV

-*3&———.20.6!r' £.14$*/&.3F

Vj « Volume o? e>(tract injected {uijVt » Volume of water extracted (ml)Wg * Weight of sample extracted (gjVt ~ Volume of tots! extract (ut)

ofW. V,

001565

No: 529&_C o n t r a c t o r :Co n t r a c t fco : 69 -0 1 -6798

S P E C T R I X C O R P .

I N I T I A L C A L I B R A T I O N D A T ASEH IVOLATSLE HSL C O M P O U N D S

(Pa g e 1 -^ : £PA _ _ _ I n s t r ume n t ID;

Ca l i b r a t i o n Da t e :5 1 0 00 1 / 1 7 / 8 6

M i n i m um AVE RF fo r SPCC i s 0 . 0 5 0 Max i s ua XRSD fo r CCC i s 30'iLabora tory ID E S Q U 7 C Q 3 ESOU7CQ4 E S Q 1 1 7 C 0 6

E10U7C05 i ecc*CompoundPhenol . . . . . . . . . . .b i s ( 2 -C h l o r o e t n y l ) E t h e r . .2-Ch l o r o p n e n o l . . , , . , .1 , 3 -D : c h l o r o b e n z e n e . . . .1 ,4 -O i c h l a r o b e n z e n e . . . .Ben z y l A l c o h o l . . . . . . .1 , 2 -O i c ^ l a r a b e n z e n e . . . .2 -M e t h y I p h e n o l . . . . . . .b i s ( 2 -C h l o r o i s o p r o p y l ) E t h e r4-Me t hy Ipheno l . . . . . . .N-N i t r a s o -D i - n -P r o p y l a f f l i n e .H e x a c h l o r o e t h a n e . . . . . .N i t r o b e n z e n e . . . . . . . .I s o p h o r o n e . . . . . . . . .2 - t r o p h e n o l . . . . . . .2 , -D i r f i e t h y l p h e n o l . . . . .B e n z o i c Ac i d . . . . . . . .b i s ( 2 - C h l o r o e t h o x y ) M e t h a n e ,2 ,4-D i c h l o r o p h e n o l , . . . ,1 , 2 , 4 - T r i c h l o r o b e n r e n e . . .Naph tha l e n e . . . . . . . .4-Ch l o r o a n i 1 i n e . . . . . .H e x a c h l o r o b u t a d i e n e . . . .4-Ch l or c - 1 -Me t h y l p h e n o l . ,N e x a c h l o r o c y c l o p e n t a d i e n e2 ,4 ,6 -T r i c h l o r o p h e n o l . . . ,2,4 , 5 -T r i c h l o r o p h e n o l . . ./2 -Ch I a r o n a p h t h a l e n e . . . .Dime t h y l Ph t h a l a t e . . . . .3 -N i t r o a n i l i n e . . . . . . .A c e n a p h t h e n e . . . . . . . .2 ,4 -D i n i t r o p h e n o l . . . . .4-N i t r o p h e n o l . . . . . . .Oibenzofuran . . . . . . . .

_ _ . .8.F<20J R F ( 3 Q > RJF<JL0) 8FU20) ftfU$0). 1 . 5 0 9 1 .3 16 1 .202 i .2 13 l ~ 185. i. 523 1. 3O9 1. 260 1. 195 1. 198. 1 . 336 1 .2f t l 1 . 1O8 1 . 1 1 8 1 . 0 5 1. 1 . 8 4 3 1 .673 1 . 534 1 . 40 1 1 . 4 1 0. 1 . 8 8 6 1 .699 1 . 53 1 1 . 387 1 . 4 1 6. O. 634 0. 498 O. 460 0. 515 0. 605. 1 . 7 8 6 1 .625 1 . 467 1 . 3 1 7 1 .333. 1. 206 1. OO6 0. 916 O. 915 0. 897. 1 . 8 5 8 1 .665 1 . 6 16 1 . 5 1 2 1 ,473. 1. 135 0. 960 0. 867 0. 903 0. 873. 0. 894 0. 830 0. 771 0. 619 0. 645. 0. 725 0. 659 0. 604 0. 543 0. 566. 0. 570 0. 529 0. 495 0. 474 0 450, 0. 858 0. 821 0. 772 0. 714 0. 689. 0. 188 0. 173 0. 157 0. 170 0, 165. 0. 290 0. 253 0. 231 0. 239 0. 227. 0. 000 0. 109 0. 057 0. 065 0. 062. O. 533 0. 460 0. 445 0. 438 0. 432. 0. 265 0. 237 0. 216 0. 232 0. 219. 0. 412 0. 383 0. 350 0. 323 0. 326. 1. 280 1. 190 1. 024 0. 929 0. 974. 0 . 0 5 4 0.032 0 ,03 1 0 .03 1 0 .05 1. 0. 239 0. 215 0. 194 0. 177 0. 181, 0. 286 0. 277 O. 236 0. 251 0. 237.1. 012 0. 962 0. 824 0. 792 0. 781/a 193 0. 168 0. 118 0. 186 0. 166ffm 365 0. 370 0. 322 0. 352 0. 338yO. 403 0. 369 0. 345 0. 315 0. 304X l .609 1 . 5 0 8 1 .358 1 .286 1 . 257. 0. 355 0. 292 0. 259 0. 166 0. 223. 1 . 0 2 9 1 . 584 1\ 474 1 . 457 1 . 375. 2 . 4 1 7 2 .2 12 1 .9 19 i . 777 1 .729. 0 . 0 2 6 0.023 0 . 0 1 5 0 .0 1 1 0.046. ; 1 .609 1 . 5 1 0 1 . 3 1 0 1 . 240 1 . 247.|0. 042 0. 069 0. 058 0. 060 0. 077, 0. Ill 0. 093 0. It3 0. 089 0. 09@.la. 239 1.^73 1 .733 t. 7S@ i. A99 B

L_AV£_fcfi. 239i. 2981. 1671. 572i. 5840. 5421. 5060. 9881. 6250. 9480. 7520. 6190. 5040. 7710. 1710. 2480. 073O. 4620. 2340. 3591. 0790. 0400. 2010. 2570. 8740. 1660. 3490. 3471. 4040. 2591. 5442. Oil0. 0241. 3330. 061$. 1011.364

...__JLJttt.._ffi£C"9. 407 *9.2438. 636

10. 6521 1 .772 *12. 15911. 3661 1 . 67 1S. 338

10. 45114. 045 * *10. 621S. 3368. 1915. 690 *9.210

28. 6137.9677. 389 *9. S32

12.33626. 3331 1 . 346 *3. 021 *

10. S2615 .815 » *5. 101 *

10. 3439. 587

24. 52010. 19013. Ill48. 62710. 788 *SB. 970 * *$.648 * *li;*W

Response Fac tor (nuf iber is the aaiount a*AVE RF - Average Response Factor

^D - - Per c en t Re l a t i v e Standa rd Dev i a t i o nui."'C - - Cal ibra t i on Check Compound s (*)SPCC - - System Pe r f o rman c e Check Compound s < * * >x - - - Not de t e c tab l e at 20 ng

Farto VI

001566

I N IT IAL C A L I B R A T I O N DATA3 E M I V D L A T I L E HSL COMPOUNDS

(Page Z)No ; 5296

Con t r a c t o r : SPECTRIX CORP.Co n t r a c t N o : 6 8 - 0 1 - 6 7 9 8

Min imum AVELab o r a t o r y IDCompound2 , 4 - D i n i t r o to l u en e . . . . .2 , 6 - D i n i t r o t o l u e n e . , . . «Diethylphthalate . . . . . .4-Ch l o r o p h e n y l - p h e n y l e t h e r .Fluorene . . . . . . . . . .4-Wi t r o a n i 1 i n e . . . . . . .4 ,6 -D i n i t r o -2 -ME t h y l p h e f i o l .N-N i t r o s o d i p h e n y l a f f l i n e ( ! ) .4 -B r o a o p h e n/ l - p h e n y l e t h e r .Hexachl arobenzene . . . . .Pen t a c h l o r o p h e n o l . . . . .Phenanth i ' ene . . . . . . . .Di - n -B u t y l p n t h a l ate . . . ,F 1 - » r a n t h e n e . . . . . . . .Buty loenzy lph tha l a t e . . . .3 , 3 ' - D i c h l o r o b e n z i d i n e , . .b is(2-£thylhexyl)Phthalate .D i - n -O c t y l P h t h a l a t e . . . .B e n r a ( b ) F l u o r a n t h e n e . . . .Ben z a ( V . ) F l u o r a n t h e n e . . . .Benzo a ) Pyren e . . . . . . .I n d e n o t l , 2 , 3 - e d ) Py r e n e . . .Dibenz (a, h) Anthracene . , .Ben z o fa .h , i IP e r y l e n e . . , .

Re q i o n : EPA I n s t r um e n t ID :Cal i b r a t i o n Da

RF tor SPCC is 0 .050 Maximum XRSD *orESQU7CQ3 ESOU7C04 ESOH7COA

.EMmCOiL. ES0U7C05 _ __RF(20).._.. _8F(5ai_..RF<80). RFU20) RFU60)

. 0. 395 0. 368 0. 343 0. 347 0. 273

. 0. 209 0. 279 0. 294 0. 161 0. 263, 1.839 1.569 1 .445 1.343 1 .435. 0. 7S9 0. 674 0. 623 0. 612 0. 574. - 1 . 9 7 2 1 .478 1 . 300 1 . 209 1 .242, 0. 080 0. 049 0. 054 0. 060 0. 030. 0 .065 O. 082 0 . 0 7 1 0 .0 18 0.049. 0. 366 0. 285 0. 263 0. 28S 0. 267. 0. 255 0. 224 0. 209 0. J96 0. 190. 0. 293 0. 266 0. 247 0. 233 0. 222. 0. O56 0. O67 0 .07 * 0 .057 O. 073. 1 .296 1 .230 1 . 100 1 .099 1 . 1 77. 1 .273 1 . 1 5 6 1 .022 0 .752 0 .844. 1 .45 1 1 .369 1 , 1 69 1 . 05 1 0.862. 1. 287 1. 206 1. 026 0. 865 0. 762. 2.215 1 .991 1 .788 1 .638 0.253. 0. 639 0. 642 0. 680 0. 659 0, 536. 0. 093 0. 088 0. 078 0. ill 0. 086. 1 . 1 74 1 . 275 1 . 1 6 4 1 .238 1 . 1 0 7. 0- 699 O. 743 0. 828 0. 903 O. 739. 1 .386 1 . 3 12 1 . 1 6 7 1 . 1 1 6 1 . 1 05, 2. £29 2. £94 2.U6S i. 996 -1. 938 _., 1 .954 2.096 1 .920 2 . 1 1 0 1 .833. 2.302 2 .0 12 2.293 1 .683 1 .956

t A*93 1 "S^A 1 "%m 1 *3f\P 1 •St^. 1 . 576 1 . 467 1 . 604 1 . 4 5 9 1 .467, 1 . 198 1 . 127 1 .213 1 .076 1 .062. 1 .S70 1 . 447 1 . 94 1 1 . 296 1 371 ,V>

5 1 0 0t e : 0 1/ 17/86

CCC is 30Xiii

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19. 1721 1 1O/\1. e£oU9. 862

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7. 90111 . 9814 OAt9. 38392f\&3. 580 *9 Of* *. 374

1 1 393< * • «1/*J

4. 126B. 408f rtOO

Respon s e Fac to r ( nuobe r i s the amount of n a nog r am s )AVE RF - Average Response Fac to rXRSD - - Percent Relat ive Standard Dev i a t i o nCCC - - Ca l i b r a t i o n Ch s c k Compoun d s ( * )SPCC - - Sys tem Perforeunce Che c k Compound s ( * » )x - - - Not de t e c tab l e at 20 ng(t) - - Cannot be separated from diphenylamine

Form VI

QQ008I

001567

?boratory Name:

Organics Analysis Data Sheet(Page l )

Case No:

Sample Numberf?b -323 MS,

Lab Sample !D No: «*&Sample Matrix: —

2- QC Report No:Contract No: _

Data Release Authorized By: Date Sample Received:

CASNumber

Volatile CompoundsConcentration: /Cow^) Medium (Circle One)Date Extracted/Prepared:Date Analyzed:Conc/Dil Factor: .Percent Moisture:

I -pH

Percent Moisture (Decanted): ___ug/lorug/Kg CAS

(Circle One) Number7*-37-374-83-97S-O1 -473-00-37S-O9-267-64-175*15-07S-35-475-34-3'. 56-60-567-66-3107-06-2?fc-93-37 1 -55 -656-23 51C8-05-475-27- 4

ChloromethaneGromomethaneVinyl ChlorideChloroothaneMethylene ChlorideAcetonoCarbon Disulfide1, 1-Oichloroeihene1. 1 -DiehloroethaneTrans 1. 2-DiehloroetheneChloroform1 . 2-Cichloromhano2-8utanone1 . 1 , 1 -TrichloroethaneCarbon TetrachlondeVinyl AcetateBromodichloromethane

ug/Iorug/Kg{Circle One)

79-34-578-87-51 006 J -02 -679-01-6124-48- 179-CO-57 1 -43-210061-01 -51 10 -75-875-25-253 1 -78-61 Q 8 - I O - 11 2 7 - 1 8 - 4103-88-3108-30-7100-41-4100-42-5

1 , 1 . 2 . 2-Tetrachioraethane1 . 2-DichloropfOD3neTrans-1 . 3-OichtoroorooeneTricHoroetheneOibromochloromethane1 . 1 . 2-TnchloroethaneBenzenec i s-1 . 3-Dichloropropene2-ChloroethyfvinvletherSromoform2-Hexanone4-Methvl-2-PentanoncTetracnloroetheneTolueneChlorobenzeneEthylbenzeneSlyreneTotal Xvienes

Oil*th«

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ing Qu*lit<ars

ai» «ncourag*d. , m«

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001568

•L a b o r a t o r y S P E C T R I X_G_ORP. _

!"~ — — — —— ———.^

! Samp l e Nusber !5 2 9 6

ORGAN ICS ANALYS IS DATA SHEET(Pa g e 2 )

SEH IVOLAT ILE COMPOUNDSLOWConc e n t r a t i o n : __ __

Date E r t r a c t e d/P r e p a r e d : QU06/ . g6Date Ana l y z e d :C o n c / C i l Fac to r ;

0 1 / 2 3 / 8 61 .

Per c e n t Mo i s t u r e : (D e c a n t e d )CAS Ni* »ber1 0 8 - 9 S - 2l l l - 4 * - 49 5 - 5 7 - =54 1 -7 > i1 0 6 - 4 e - 71 0 0 - 5 1 - 69 5 - 5 0 - 195~48-~3 9 6 3 8 - 3 2 - 91C" - 4 A - 56 . 6 4 - 76 7 - 7 2 - i98 -95- :7 8 - 5 9 - 18 8 - 7 5 - ^1 0 5 - 6 ? - 96 5 - 8 5 - :1 1 1 - 9 1 - 11 20 -83 -2120-8 : - l9 1 - 2 0 - :1 0 6 - 4 T - 887 " 68 — j59-50- 7

9 1 - 5 7 - s7 7 - 4 7 - 48B -06-29 5 - 9 5 - 49 1 - 58 - *8 8 - 7 4 - 41 3 1 - 1 1 - 3208 -96 -B99-09-;

Phero l . , , . . . . , . .b i 5 f2 -Ch l o r o e t h y l ) E t h e r .2 -C h i o roph eno t . . . . . .l T 3~D i c h l a r o b e n z e n e . . .1 ,4 -D i c h l o r o b e n z s n e . . .B e n z y l A l c o h o l . . . . . .1 , 2 -D i c h l a r o b e n z e n e . . .2-f l e thy lphena l . . . . . .b i s ( 2 -Ch l o r a i s o p r o p y l ) Ether4-Methy l p h e no l . . . . . .N -N i t r a s o -D i - n -P r a p y l a f f l i n eHexa c h l or oe thane . . . . .N i t r o b e n z e n e . . . . . . .I s opho ron e . . . . . . . .2-N i t r oph e no l . . . . . .2,4-D i f l i e t h y l p h e n o l . . . .B e n z c i c A c i d . . . . . . *b i s f 2 -C h i o r o e t h o x y ) Me t h a n e2 , 4-D i c h l o r o p h e n o l . . . .1 , 2 , 4 - T r i C h l o r o b e n z s n e . .Napn t h a l e n e . . . . . . .4 -C h l o r o a n i l i ne . . . . .H e x a c h l o r n b u t a d i e n e . . .4-Ch lor o-3- Methy l pheno l2-He t h y l n a p h t h a l e n e . . .Hexa c h l o r o c y c l o p e n t a d i e n e2 ,4 ,6 -T r i c h l o r o p h e n o I . ,2,4 ,5-Tr i c h l o r o p h e r i a l , .2-Ch l a r o n a p h t h a l e n e . . .2-Ni t roan i l i n s . , . - . .Dif iRthy l Ph t h a l a t e . . . .Acen a p h t h y 1 ynt> . . . . . .3-Nt t r o a r , i ! i n a . . . . . .

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6PC Cleanup __ Yes JL. NoSepara to ry Funne l Ex t r a c t i o n __.. YesCont inuous L i q u i d -L i q u i d Ex t ra c t i o n Yes

CAS Number8 3 - 3 2 - 95 1 -28 -51 0 G - 0 2 - 71 3 2 - 6 4 - 91 2 1 - 1 4 - 2606-20-28 4 - 6 6 - 27005-72-38 6 - 7 3 - 71 0 0 - 1 0 - 653 * -52 - l86-30-61 0 1 - 5 5 - 31 1 8 - 7 4 - 187 -86 -585 -0 1 -81 2 0 - 1 2 - 78 4 - 7 4 - 2206-44-0127-00-08 5 - 6 8 - 79 1 - 9 4 - 156-55-31 1 7 - 8 1 - 72 1 8 - 0 1 - 91 1 7 - 8 4 - 0205-99-2207-08-950-32 -8193-39-553-70-31 9 1 - 2 4 - 2

Acen ap h t h e n e . . . . . . .2 ,4-D i n i t r a p h e n o l . , . .4-N i t ropheno l . . . . . .D i b e n e o f u r a n . . . . . . .2 ,4-D i n i t r o t a l u e n e . . . .2,6-D i n i t r o t o l u e n e . . , .4-Ch l o r oph e ny I - p h e ny l e t h e rF luar ene , . , , . , , . .4-N i t raan i l i n e . . . . . .4 ,6 -D i n i t r o -2 -M e t h y l p h e n o IN-Ni t ro sad i pheny l aa i n e ( 1 )a -8ro i f lOp ! i e n y l - p h e ny l e t h e rr i e x a c h l o r o b&n z e n e . . . .Pen t a c h l o r ooh e n a l . . . .Phenan t h r e n e . . . . . . .An t h r a c e n e . . . . . . . .D i - n -Bu t y i p h t h a l a t s . . .F luo r an t h e n e . . . . . . .Pyrene . . . . . . . . . .B u t y l b e n z y l p h t h a l a t e . . .3 ,3 ' -D i c h l o r o b e n z i d i n e . .B e n z o ( a ) An t h r a c e n e . . . .b i s < 2 -E t h y l h e x y l )P h t h a l a t eChry s e n e . . . . . . . . .D i - n -Oc t y l Ph t h a l a t e . . .B e n20 ( b ) F l u o r a n t h e n e . . .Ben z o ( k )F l u o r a n t h e n e , . .B e n z o ( a ) P y r e n e . . . . . .I ndeno ( i ,2 ,3- c d )Py r e n e . .Dib e n z ( a , h )An t h r a c e n e * .Ben z a ( g , h ,UPe r y l e n e . . .

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001569

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001571

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001572

U.&-ENVIRONMEPfr/ PROTECTION AGENCY -HWI Scrmplo' ' maqeriieni Office

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001573

U.S._ENVIRONMENtA' "ROTECnON AGENCY HWJ Sample' . -nagemcnt Office

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