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Standards Certification Education & Training Publishing Conferences & Exhibits Batch Profile Control

Batch Profile Control

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Page 1: Batch Profile Control

Standards

Certification

Education & Training

Publishing

Conferences & Exhibits

Batch Profile Control

Page 2: Batch Profile Control

22

Presenter

– Greg is a retired Senior Fellow from Solutia/Monsanto and an ISA Fellow. Greg was an adjunct professor in the Washington University Saint Louis Chemical Engineering Department 2001-2004. Presently, Greg contracts as a consultant in DeltaV R&D via CDI Process & Industrial and is a part time employee of Experitec and MYNAH. Greg received the ISA “Kermit Fischer Environmental” Award for pH control in 1991, the Control Magazine “Engineer of the Year” Award for the Process Industry in 1994, was inducted into the Control “Process Automation Hall of Fame” in 2001, was honored by InTech Magazine in 2003 as one of the most influential innovators in automation, and received the ISA Life Achievement Award in 2010. Greg is the author of numerous books on process control, his most recent being Advanced Temperature Measurement and Control. Greg has been the monthly “Control Talk” columnist for Control magazine since 2002. Greg’s expertise is available on the web site: http://www.modelingandcontrol.com/

Page 3: Batch Profile Control

3

Liquid Reactants (Jacket CTW) Liquid Product Basic Control

TT 1-4

TC 1-3

TC 1-4

AT 1-6

LY 1-8

FY 1-6

FT 1-2

FC 1-2

reactant A

reactant B

CAS

residencetime calc

CAS

ratiocalc

AC 1-6

makeup

return

LY 1-8

FY 1-6

reactant A

reactant B

residencetime calc LT

1-8 TT 1-3

LC 1-8

CAS

ratiocalc

product

vent FT 1-1

FC 1-1

FC 1-7

FT 1-7

CAS

PT 1-5

PC 1-5

FT 1-5

CTW

Residence time and composition control is for continuous reactors otherwise theflow, pressure, and temperature controlshown could be for batch or continuous.

Page 4: Batch Profile Control

4

Liquid Reactants (Jacket CTW) Liquid Product Optimization

TT 1-4

TC 1-3

TC 1-4

AT 1-6

LY 1-8

FY 1-6

FT 1-2

FC 1-2

reactant A

reactant B

CAS

residencetime calc

CAS

ratiocalc

AC 1-6

makeup

return

LY 1-8

FY 1-6

reactant A

reactant B

residencetime calc LT

1-8 TT 1-3

LC 1-8

CAS

ratiocalc

product

vent FT 1-1

FC 1-1

FC 1-1CAS

ZC1-4OUT

ZC 1-4

FC 1-7

FT 1-7

PT 1-5

PC 1-5

FT 1-5

CTW

ZC1-4 is an enhanced PID VPC

Valve position controller (VPC) setpointis the maximum throttle position. TheVPC should turn off integral action toprevent interaction and limit cycles. Thecorrection for a valve position less thansetpoint should be slow to provide a slow approach to optimum. The correction fora valve position greater than setpoint mustbe fast to provide a fast getaway from thepoint of loss of control. Directional velocitylimits in AO with dynamic reset limit in anenhanced PID that tempers integral actioncan achieve these optimization objectives.

Page 5: Batch Profile Control

5

Liquid Reactants (Jacket CTW) Gas & Liquid Products Basic Control

TT 1-4

TC 1-4

AT 1-6

LY 1-8

FY 1-6

FT 1-2

FC 1-2

reactant A

reactant B

residencetime calc

CAS

ratiocalc

AC 1-6

makeup

return

LY 1-8

FY 1-6

reactant A

reactant B

CAS

residencetime calc

LT 1-8

LC 1-8

CAS

ratiocalc

product

FT 1-1

FC 1-1

FC 1-7

FT 1-7

CAS

TC 1-3

TT 1-3

product

PC 1-5

FT 1-5

W

PT 1-5

TT 1-10

TC 1-10

CTW

Residence time and composition control is for continuous reactors otherwise theflow, pressure, and temperature controlshown could be for batch or continuous.

Page 6: Batch Profile Control

6

Liquid Reactants (Jacket CTW) Gas & Liquid Products Optimization

TT 1-4

TC 1-4

AT 1-6

LY 1-8

FY 1-6

FT 1-2

FC 1-2

reactant A

reactant B

residencetime calc

CAS

ratiocalc

AC 1-6

makeup

return

LY 1-8

FY 1-6

reactant A

reactant B

CAS

residencetime calc

LT 1-8

LC 1-8

CAS

ratiocalc

product

FT 1-1

FC 1-1

FC 1-7

FT 1-7

CAS

TC 1-3

TT 1-3

product

PC 1-5

FT 1-5

W

PT 1-5

TT 1-10

TC 1-10

ZC 1-4

ZC 1-10

ZC 1-5

ZY 1-1

FC1-1CAS

ZY1-1OUT

low signalselector

ZC-10OUT

ZC-4OUT

ZC-5OUT

ZY-1IN1

ZY-1IN2

ZY-1IN3

CTW

ZC1-4, ZC-5, & ZC-10 are enhanced PID VPC

Page 7: Batch Profile Control

7

Gas & Liquid Reactants (Jacket CTW) Liquid Product End Point Control

TT 1-4

PC 1-5

TC 1-3

TC 1-4

AT 1-6

LY 1-8

FY 1-6

FT 1-2

FC 1-2

gas reactant A

liquid reactant B

CAS

residencetime calc

CAS

ratiocalc

AC 1-6

makeup

return

LY 1-8

FY 1-6

residencetime calc

CAS

ratiocalc

product

purge FT 1-1

FC 1-1

FC 1-5

FT 1-5

LT 1-8

TT 1-3

PT 1-5

LC 1-8

CAS

FC 1-7

FT 1-7

CTW

Pressure control inherentlyprevents an excess of gas reactant providing endpointcontrol for liquid product in continuous andfed-batch reactors.

Residence time and composition control is for continuous reactors otherwise theflow, pressure, and temperature controlshown could be for batch or continuous.

Page 8: Batch Profile Control

8

Resource

Advanced Temperature Measurement and Control - 2nd Ed has a lot of detailson how to improve temperature sensoraccuracy and temperature control of heat exchangers, reactors, and kilns

Biological and Chemical Reactor Controlis an ISA book whose kernel is the ISAAutomation Week tutorial. The book will beavailable in December just in time for the holidays. Surprise your spouse with the bookas a “gift that keeps on giving.” Your spousewill never let you forget it.