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ADDENDUM NO. 7 November 01, 2017
PROJECT: CITY OF SEYMOUR WATER TREATMENT PLANT The following changes and/or additions shall be made to the Plans, Specifications, and Contract Documents for the above referenced project. Bidder shall acknowledge receipt of this Addendum by signing below and returning this Addendum with the Bid.
I. Plan Sheets – The Plan Sheets have been revised to show the following:
a. Sheet A-7 – Evap Pond Berm Details
i. Detail views of the Pond Berms have been included in the attached plan sheet.
b. Sheet 06 – Concentrator Layout i. Changes have been made to the piping from the proposed head tank to the
pump skid. ii. The 4” tee and two automated valves are to be provided by the RO vendor
as part of the pump skid. iii. This change was made to allow the concentrator to perform its pre-flush
and post-flush with raw water. iv. Pre-flush and post-flush cycles shall only utilize raw well water.
Utilization of the existing RO concentrate for pre- and/or post-flush will not be allowed.
c. Sheet 9 – Pump Skid Concentrator “A” P & ID i. The feed pump total dynamic head has been updated from 150 psi to 250
psi.
d. Sheet 10 – Concentrator “B” P & ID i. The feed pump total dynamic head has been updated from 150 psi to 250
psi.
e. Sheet 18 – Control and SCADA Plan i. The control panel for the Concentrators has been updated and moved.
ii. The automated valves shall be controlled by the Concentrators’ control panel.
2 of 4
II. Contract Documents – The Contract Documents have been revised to show the following:
a. Bid Schedule – The Bid Schedule has been revised i. Bid Items 3 through 8
1. Bid Item 3 – Excavation to Finished Grade a. This item includes the provision of all necessary labor and
equipment to provide the Excavation to Finished Grade as specified and shown on the plans.
b. Item shall be paid as a Lump Sum
2. Bid Item 4 – Over Excavate Berm Area a. This item includes the provision of all necessary labor and
equipment to provide the Over Excavation of the Berm Area as specified and shown on the plans. Detail examples of this line item are shown in the attached plan sheet A-7.
b. Item shall be paid as a Lump Sum
3. Bid Item 5 – Excavate Borrow Area a. This item includes the provision of all necessary labor and
equipment to provide the Excavation of the Borrow Area as specified and shown on the plans. This includes the excavation of all the material from 0-6 feet deep.
b. Item shall be paid as a Lump Sum 4. Bid Item 6 – Fill to Pond Floor
a. This item includes the provision of all necessary labor and equipment to construct the pond floor to the grade as specified and shown on the plans. Contractors may use sand material to perform this line item.
b. Item shall be paid as a Lump Sum
5. Bid Item 7 – Placement of Excavated Borrow (Berms) a. This item includes the provision of all necessary labor and
equipment to provide the Placement of the Excavation Borrow into the berms as specified and shown on the plans.
b. Item shall be paid as a Lump Sum
6. Bid Item 8 – Waste Material a. This item includes the provision of all necessary labor and
equipment to provide placement of Waste Material as specified and shown on the plans.
b. Item shall be paid as a Lump Sum
ii. All bids must use the new Bid Schedule labeled “Revised – Addendum #7”
3 of 4
III. Additional Information – The following information is intended to supplement and become part of the Contract.
a. Soil Analysis – Additional Information i. Soil analysis data from soil samples taken on site are included as an
attachment. ii. A map of the sample locations in included on Sheet A-7 attached to this
addendum.
b. Lagoon Liner Ballast Tubes – Additional Clarification i. Ballasts tubes may be constructed out of 30 mil HDPE liner.
c. RO Concentrators – Additional Clarification
i. RO vendors shall meet and match the attached pretreatment process and chemicals.
ii. The system shall use Vitec 158 anti-scalant. The system already utilizes sulfuric acid for pH adjustment. The projection data and chemical uses shown on the attached Overall Recovery projection shall be utilized. This proposal includes anti-scalant and pH adjustment on the existing RO only to carry through to the concentrator. Chemical Injection equipment shown at the concentrators will remain for future use.
iii. Raw water chemistry before it is processed by the existing RO units is attached for RO vendors review.
d. General Contractors and RO Vendors – Additional Clarification i. RO vendors must be pre-qualified per Specification 11.04.01 part 1.7.
ii. RO vendors must submit qualifying information to the Project Engineer, including but not limited to: documentation of similar projects in terms of scope, contract amount, and industry type, references, examples of products and materials, examples of product controls, etc.
iii. RO vendors must have experience in municipal water supply or public water supply projects.
iv. The City of Seymour and the Project Engineer reserve the right to deny pre-qualification. Final approval must come from the project engineer.
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Prepared by: JACOB & MARTIN, LLC. Consulting Engineers 3465 Curry Lane Abilene, Texas 79606 _________________________________ Bidder’s Acknowledgment _________________________________ Date
B-2
For all Labor, Materials, Equipment and Incidentals to Furnish and Deliver the Following:Bid Description Estimated Unit Price ExtendedItem (Price to be Written) Qty. Unit (Numbers) Amount
1 MOBILIZATION, BONDS, AND INSURANCE 1 LS
2 WTP EQUIPMENT 1 LS
3 EXCAVATION TO FINISHED GRADE 1 LS
4 OVER EXCAVATE BERM AREA 1 LS
5 EXCAVATE BORROW AREA 1 LS
6 FILL TO POND FLOOR 1 LS
7 PLACEMENT OF EXCAVATED BORROW (BERMS) 1 LS
8 WASTE MATERIAL 1 LS
9 EVAPORATION POND LEAK DETECTION PIPING 6,312 LF
10 LEAK DETECTION SAMPLING PORT 3 EA
11 60 MIL TEXTURED HDPE SYNTHETIC LINER 1 LS
12 8" CONCENTRATE LINE 2,050 LF
13 8" CONCENTRATE CONNECTION AT PLANT 1 EA
14 8" PLUG VALVES 6 EA
15 POND TRANSFER PIPES 4 EA
16 EVAPORATION POND FENCE 5,100 LF
17 PHOENIX WETLAND BIRD WAILERS or equal 3 EA
18 ELECTRICAL REROUTE THROUGH POND AREA 1 LS
19 WTP ELECTRICAL (NEW EQUIPMENT INTEGRATION) 1 LS
20 WTP CONTROL AND SCADA UPGRADES 1 LS
21 POND INLETS 3 EA
22 6" C900 DR25 PVC WATERLINE 2,430 LF
23 2 - 6" WL RECONNECTIONS 2 EA
TOTAL BASE BID (ITEMS 1-23)
CITY OF SEYMOUR
BASE BID SCHEDULEWTP IMPROVEMENTS
TWDB PROJECT # 62693
Show prices in words and numerals. Words take precedence over numerals. Round off unit prices to two decimal places only.These bid prices must include furnishing & delivering all materials, profits & incidentals to cover the items called for in the Contract Documents. In case of mathematical error in extensions, (Unit Prices) prevails.
*REVISED - ADDENDUM #7*
B-2
Deductible Alternate Bid
D-1 60 MIL TEXTURED HDPE SYNTHETIC LINER 1 LS
D-2 LEAK DETECTION SAMPLING PORT 3 EA
D-3 EVAPORATION POND LEAK DETECTION PIPING 6,312 LF
Additions Alternate Bid
A-1 3' CLAY LINER FOR EVAPORATION POND 1 LS
A-2 BACKUP GENERATOR 1 LS
A-3 EXISTING RO SKID MEMBRANES 288 EA
A-4 EXISTING RO SKID MEMBRANE REPLACEMENT 1 LS
TOTAL CONTRACT PRICE (BB-D1-D-2-D3 + A-1 + A-2 + A-3 + A-4)
Seymour WTP Improvements Soil Test Results
Page 1of 2
Test Pit
Sample ID
Soil D
epth, Ft.
Soil
Descriptio
n
Liquid Lim
it
Plastic L
imit
Plasticit
y Index
Ret No. 4
Ret No. 4
0
Ret #200
1 1A 0.0 - 3.5 Brown Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 2 58.8
1 1B 3.5 - 4.0 Gray Fat Clay (CH) 56 19 37 0 0 11.2
1 1C 4.0 - 6.0Gray Fat Clay with Sand and white particles (CH) 52 20 32 0 3 17.6
1 1D 6.0 - 8.0 Gray Fat Clay (CH) 55 21 34 0 2 9.9
2 2A 0.0 - 3.3 Reddish Brown Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 7 87.1
2 2B 3.3 - 5.0 Gray Fat Clay with Sand (CH) 51 19 32 0 2 19.7
2 2C 5.0 - 6.0 Gray Lean Clay with white particles (CL) 46 17 29 0 3 18.9
3 3A 0.0 - 3.5 Tan Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 5 86.4
3 3B 3.5 - 4.0 Light Tan & Brown Lean Clay with Sand (CL) 42 17 25 0 1 17.6
3 3C 4.0 - 6.3 Orangish Lean Clay (CL) 37 18 19 0 1 6.7
4 4A 0.0 - 3.5 Tan Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 5 87.8
4 4B 3.5 - 4.5 Dark Gray Fat Clay (CH) 62 23 39 0 1 6.1
4 4C 4.5 - 6.3Dark Gray & Brown Fat Clay with white particles (CH) 65 22 43 0 1 6.7
5 5A 0.0 - 3.8 Brown Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 3 87.3
5 5B 3.8 - 4.5Tan lightly cemented Silty, Clayey Sand with rust colored stains (SC-SM) 25 19 6 0 2 54.8
5 5C 4.5 - 5.8 Gray Fat Clay (CH) 71 24 47 0 0 9.3
6 6A 0.0 - 2.7 Brown Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 4 87.9
6 6B 2.7 - 5.0 Yellow, Brown & Gray Fat Clay (CH) 66 23 43 0 0 10.5
6 6C 5.0 - 6.0 Orange Lean Clay with Sand (CL-ML) 24 17 7 1 4 18.8
7 7A 0.0 - 4.0 Reddish Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 3 87.4
Seymour WTP Improvements Soil Test Results
Page 2of 2
Test Pit
Sample ID
Soil D
epth, Ft.
Soil
Descriptio
n
Liquid Lim
it
Plastic L
imit
Plasticit
y Index
Ret No. 4
Ret No. 4
0
Ret #200
7 7B 4.0 - 4.5Tan Sandy Lean Clay with rust colored stains (CL) 31 20 11 0 0 32.1
7 7C 4.5 - 6.1 Gray Fat Clay (CH) 61 23 38 0 1 8.4
8 8A 0.0 - 2.0 Reddish Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 5 87.7
8 8B 2.0 - 4.5 Gray Sandy Lean Clay (CL) 42 17 25 0 2 33.1
8 8C 4.5 - 6.1Brown and Yellow mottled Lean Clay with Sand (CL) 47 20 27 0 4 19.5
9 9A 0.0 - 3.5 Reddish Orange Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 4 77.4
9 9B 3.5 - 5.5 Reddish with Gray streaks Lean Clay (CL) 46 19 27 0 1 14.4
9 9C 5.5 - 5.9Reddish with Gray streaks and white particles Fat Clay (CH) 50 19 31 0 1 14.1
10 10A 0.0 - 3.5Tannish transitioning to Orangish Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 2 86.8
10 10B 3.5 - 5.8 Reddish Orange Lean Clay with sand (CL) 33 16 17 1 7 25.3
10 10C 5.8 - 7.2 Reddish Clayey Sand (SC) 28 16 12 4 37 57.2
11 11A 0.0 - 4.0 Reddish Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 4 86.3
11 11B 4.0 - 4.5 Yellow, Red & Tan mottled Clayey Sand (SC) 37 17 20 0 1 53.1
11 11C 4.5 - 7.0 Gray Lean Clay with Sand (CL) 48 20 28 0 1 25.3
12 12A 0.0 - 7.6 Reddish Tan Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 5 86.9
13 13A 0.0 - 3.5 Brown Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 4 87.5
13 13B 3.5 - 4.5 Reddish Sandy Lean Clay (CL) 29 14 15 0 1 46.1
13 13C 4.5 - 6.0 Red and Gray Sandy Lean Clay (CL) 39 17 22 0 2 44.6
13 13D 6.0 - 6.7 Whitish Lean Clay with Sand (CL) 48 20 28 0 7 21.4
Project: City of Seymour
Recovery: 92% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Overall Recovery
CORPORATE OFFICES
Avista Technologies, Inc. Global Headquaters Avista Technologies (UK) Ltd140 Bosstick Blvd 13 Nasmyth Square, Houstoun Ind EstateSan Marcos, CA 92069 Livingston, EH54 5GG, UK
Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677
AdvisorCi Version 4.4.6 Antiscalant data file 0
Technical Summary
Water Chemistry Scaling Potential
Cations(mg/l) EnteredFeed
AdjustedFeed
CalculatedConcentrate
Sodium 169.00 178.42 2196.57Potassium 5.17 5.17 63.05Calcium 80.30 80.30 995.12Magnesium 52.10 52.10 645.65Iron 0.03 0.03 0.30Manganese 0.00 0.00 0.00Barium 0.07 0.07 0.87Strontium 1.19 1.19 14.74Aluminium 0.00 0.00 0.00Ammonium 0.00 0.00 0.00Anions(mg/l) Chloride 175.00 175.00 2159.94Sulfate 158.00 402.87 5012.26Bicarbonate 468.63 158.11 1915.83Carbonate 0.34 0.02 6.80Nitrate 13.20 13.20 152.87Fluoride 1.55 1.55 18.87Phosphate 0.11 0.11 1.29Silica 11.10 11.10 137.99Carbon Dioxide 58.70 336.27 336.27TDS 1144.87 14085.05
Saturation Level EnteredFeed
AdjustedFeed
CalculatedConcentrate
CCPP 13.08 -269.02 865.26mg/l Calcium Sulfate CaSO4 0.03 0.07 1.72x Barium Sulfate BaSO4 2.71 6.67 216.45x Strontium Sulfate SrSO4 0.03 0.06 2.03x Calcium Phosphate 0.00 0.00 0.03x Calcium Fluoride CaF2 0.01 0.00 1.62x Silica SiO2 0.11 0.11 1.43x Magnesium Hydroxide
Mg(OH)20.00 0.00 0.00x
Saturation Indices Langelier Saturation
Index (LSI)0.41 -1.64 1.12
Stiff and Davis Index (S&DI)
0.18 -1.86 0.89
System Parameters pH 7.60 6.00 6.92 Ionic Strength 0.02 0.02 0.28 Temperature (deg.F) 65.00 65.00 65.00
System Details Antiscalant DetailsUsed in Dosage and Feed Rate Calculations
Feedwater Flowrate Product Flowrate820.0USGPM 754.4USGPM
Concentrate Flowrate65.6USGPM
Operating Conditions% Recovery 92Hours per Day 24Days per Week 7Weeks per Year 52Load Factor 100.0%
Antiscalant Selected Avista 158Dosage 4.36mg/lUsage 42.85 lb per day.Dosed Strength 100%Pump Rate 4.41USGPD
11.59ml/m
There is one dosing pump and chemical tank per membrane train.With 1 trains, each pump will deliver 4.41USGPD
pH CorrectionChemical choice Sulfuric acidDosage: 239.7mg/l 100% H2SO4Delivered Concentration: 98% H2SO4Usage 2403.41 lb per day.Site Dilution: 100%Pump Rate 157.60USGPD
414.56ml/m
There is one dosing pump and chemical tank per membrane train.With 1 trains, each pump will deliver 157.60USGPD
Executive Summary
Membrane and Water TypeFeed Source: Well WaterMembrane Manufacturer: DefaultMembrane Type: Standard BrackishWater Analysis Date: 18-Feb-15
Antiscalant Recommendations
Recommended Product Recommended Dosage System Recovery
Avista 158 4.4mg/l 92%
Dosed Strength Usage Per Day pH Correction
100% 42.85 lb Sulfuric acid
239.7mg/l
Saturation Indicies
0% 10% 20% 30% 40% 50% 60% 70% 80% 90% 100% 110% 120%Percent of Product Limit
CaCO3
CaSO4
BaSO4
SrSO4
CaF2
CaPO4
SiO2
MgOH
Fe
Mn
Al
While every effort has been made to ensure the accuracy of this program, no warranty, expressed or implied, is given as actual application of the products is outside the control of Avista Technologies.
Project: City of Seymour
Recovery: 92% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Overall Recovery
CORPORATE OFFICES
Avista Technologies, Inc. Global Headquaters Avista Technologies (UK) Ltd140 Bosstick Blvd 13 Nasmyth Square, Houstoun Ind EstateSan Marcos, CA 92069 Livingston, EH54 5GG, UK
Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677
AdvisorCi Version 4.4.6 Antiscalant data file 0
Project: City of Seymour
Recovery: 60% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Concentrator RO
CORPORATE OFFICES
Avista Technologies, Inc. Global Headquaters Avista Technologies (UK) Ltd140 Bosstick Blvd 13 Nasmyth Square, Houstoun Ind EstateSan Marcos, CA 92069 Livingston, EH54 5GG, UK
Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677
AdvisorCi Version 4.4.6 Antiscalant data file 0
Technical Summary
Water Chemistry Scaling Potential
Cations(mg/l) EnteredFeed
AdjustedFeed
CalculatedConcentrate
Sodium 939.00 939.00 2312.05Potassium 30.90 30.90 75.38Calcium 458.00 458.00 1135.15Magnesium 302.00 302.00 748.51Iron 0.00 0.00 0.00Manganese 0.00 0.00 0.00Barium 0.37 0.37 0.92Strontium 7.41 7.41 18.36Aluminium 0.00 0.00 0.00Ammonium 0.00 0.00 0.00Anions(mg/l) Chloride 979.00 1192.40 2943.45Sulfate 2004.90 2004.90 4988.69Bicarbonate 770.00 769.87 1862.00Carbonate 0.82 0.96 9.30Nitrate 66.90 66.90 154.96Fluoride 7.76 7.76 18.90Phosphate 0.00 0.00 0.00Silica 63.20 63.20 157.13Carbon Dioxide 0.00 247.98 247.98TDS 5842.84 14550.64
Saturation Level EnteredFeed
AdjustedFeed
CalculatedConcentrate
CCPP 136.78 62.95 907.79mg/l Calcium Sulfate CaSO4 0.60 0.61 1.84x Barium Sulfate BaSO4 62.24 64.20 204.93x Strontium Sulfate SrSO4 0.69 0.71 2.27x Calcium Phosphate 0.00 0.00 0.00x Calcium Fluoride CaF2 0.24 0.24 1.70x Silica SiO2 0.65 0.65 1.63x Magnesium Hydroxide
Mg(OH)20.00 0.00 0.00x
Saturation Indices Langelier Saturation
Index (LSI)0.16 0.11 1.26
Stiff and Davis Index (S&DI)
0.02 -0.03 1.01
System Parameters pH 6.60 6.60 7.03 Ionic Strength 0.14 0.14 0.34 Temperature (deg.F) 65.00 65.00 65.00
System Details Antiscalant DetailsUsed in Dosage and Feed Rate Calculations
Feedwater Flowrate Product Flowrate160.0USGPM 96.0USGPM
Concentrate Flowrate64.0USGPM
Operating Conditions% Recovery 60Hours per Day 24Days per Week 7Weeks per Year 52Load Factor 100.0%
Antiscalant Selected Avista 158Dosage 20.27mg/lUsage 38.86 lb per day.Dosed Strength 100%Pump Rate 4.00USGPD
10.51ml/m
There is one dosing pump and chemical tank per membrane train.With 1 trains, each pump will deliver 4.00USGPD
Executive Summary
Membrane and Water TypeFeed Source: Well WaterMembrane Manufacturer: DefaultMembrane Type: High Rej BrackishWater Analysis Date: 18-Feb-15
Antiscalant Recommendations
Recommended Product Recommended Dosage System Recovery
Avista 158 20.3mg/l 60%
Dosed Strength Usage Per Day pH Correction
100% 38.86 lb -
Saturation Indicies
0% 10% 20% 30% 40% 50% 60% 70% 80% 90% 100% 110% 120%Percent of Product Limit
CaCO3
CaSO4
BaSO4
SrSO4
CaF2
CaPO4
SiO2
MgOH
Fe
Mn
Al
While every effort has been made to ensure the accuracy of this program, no warranty, expressed or implied, is given as actual application of the products is outside the control of Avista Technologies.
Project: City of Seymour
Recovery: 60% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Concentrator RO
CORPORATE OFFICES
Avista Technologies, Inc. Global Headquaters Avista Technologies (UK) Ltd140 Bosstick Blvd 13 Nasmyth Square, Houstoun Ind EstateSan Marcos, CA 92069 Livingston, EH54 5GG, UK
Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677
AdvisorCi Version 4.4.6 Antiscalant data file 0
Project: City of Seymour
Recovery: 80% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Primary RO
CORPORATE OFFICES
Avista Technologies, Inc. Global Headquaters Avista Technologies (UK) Ltd140 Bosstick Blvd 13 Nasmyth Square, Houstoun Ind EstateSan Marcos, CA 92069 Livingston, EH54 5GG, UK
Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677
AdvisorCi Version 4.4.6 Antiscalant data file 0
Technical Summary
Water Chemistry Scaling Potential
Cations(mg/l) EnteredFeed
AdjustedFeed
CalculatedConcentrate
Sodium 169.00 178.42 878.63Potassium 5.17 5.17 25.22Calcium 80.30 80.30 398.05Magnesium 52.10 52.10 258.26Iron 0.03 0.03 0.12Manganese 0.00 0.00 0.00Barium 0.07 0.07 0.35Strontium 1.19 1.19 5.90Aluminium 0.00 0.00 0.00Ammonium 0.00 0.00 0.00Anions(mg/l) Chloride 175.00 175.00 863.97Sulfate 158.00 402.87 2004.90Bicarbonate 468.63 158.11 770.16Carbonate 0.34 0.02 0.82Nitrate 13.20 13.20 61.15Fluoride 1.55 1.55 7.55Phosphate 0.11 0.11 0.52Silica 11.10 11.10 55.19Carbon Dioxide 58.70 336.27 336.27TDS 1144.87 5666.78
Saturation Level EnteredFeed
AdjustedFeed
CalculatedConcentrate
CCPP 13.08 -269.02 84.91mg/l Calcium Sulfate CaSO4 0.03 0.07 0.58x Barium Sulfate BaSO4 2.71 6.67 67.42x Strontium Sulfate SrSO4 0.03 0.06 0.63x Calcium Phosphate 0.00 0.00 0.00x Calcium Fluoride CaF2 0.01 0.00 0.22x Silica SiO2 0.11 0.11 0.56x Magnesium Hydroxide
Mg(OH)20.00 0.00 0.00x
Saturation Indices Langelier Saturation
Index (LSI)0.41 -1.64 0.10
Stiff and Davis Index (S&DI)
0.18 -1.86 -0.05
System Parameters pH 7.60 6.00 6.57 Ionic Strength 0.02 0.02 0.11 Temperature (deg.F) 65.00 65.00 65.00
System Details Antiscalant DetailsUsed in Dosage and Feed Rate Calculations
Feedwater Flowrate Product Flowrate812.5USGPM 650.0USGPM
Concentrate Flowrate162.5USGPM
Operating Conditions% Recovery 80Hours per Day 24Days per Week 7Weeks per Year 52Load Factor 100.0%
Antiscalant Selected Avista 158Dosage 2.30mg/lUsage 22.40 lb per day.Dosed Strength 100%Pump Rate 2.30USGPD
6.06ml/m
There is one dosing pump and chemical tank per membrane train.With 1 trains, each pump will deliver 2.30USGPD
pH CorrectionChemical choice Sulfuric acidDosage: 239.7mg/l 100% H2SO4Delivered Concentration: 98% H2SO4Usage 2381.43 lb per day.Site Dilution: 100%Pump Rate 156.16USGPD
410.77ml/m
There is one dosing pump and chemical tank per membrane train.With 1 trains, each pump will deliver 156.16USGPD
Executive Summary
Membrane and Water TypeFeed Source: Well WaterMembrane Manufacturer: DefaultMembrane Type: Standard BrackishWater Analysis Date: 18-Feb-15
Antiscalant Recommendations
Recommended Product Recommended Dosage System Recovery
Avista 158 2.3mg/l 80%
Dosed Strength Usage Per Day pH Correction
100% 22.40 lb Sulfuric acid
239.7mg/l
Saturation Indicies
0% 10% 20% 30% 40% 50% 60% 70% 80% 90% 100% 110% 120%Percent of Product Limit
CaCO3
CaSO4
BaSO4
SrSO4
CaF2
CaPO4
SiO2
MgOH
Fe
Mn
Al
While every effort has been made to ensure the accuracy of this program, no warranty, expressed or implied, is given as actual application of the products is outside the control of Avista Technologies.
Project: City of Seymour
Recovery: 80% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Primary RO
CORPORATE OFFICES
Avista Technologies, Inc. Global Headquaters Avista Technologies (UK) Ltd140 Bosstick Blvd 13 Nasmyth Square, Houstoun Ind EstateSan Marcos, CA 92069 Livingston, EH54 5GG, UK
Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677
AdvisorCi Version 4.4.6 Antiscalant data file 0
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Page 1 of 102/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Account Project
685118SEYM-N
Report To
City of Seymour
Rick Garcia
301 North Washington
Seymour, TX 76380
Report
Employee Owned Integrity Caring Continual Improvement
Table of Contents
PagesDescriptionReport Name
This report consists of this Table of Contents and the following pages:
685118_r03_03_ProjectResults Ana-Lab Project P:685118 C:SEYM Project Results 8 685118_r03_10_ProjectRLHCompliance Ana-Lab Project P:685118 C:SEYM Project Limits Compliance Results Report 6 685118_r10_05_ProjectQC Ana-Lab Project P:685118 C:SEYM Project Quality Control Groups 16 685118_r99_09_CoC__1_of_1 Ana-Lab CoC SEYM 685118_1_of_1 7
37 Total Pages:
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptTOC Created 10/06/2004 v1.1LDSClient v1.6.7.992
NELAP-accredited #T104704201
Report Page 1 of 38
1
2
3
4
5
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results02/18/2015Printed: Page 1 of 8
Report To
City of Seymour
Rick Garcia
301 North Washington
Seymour, TX 76380
685118SEYM-NAccount Project
Results
BottleCASFlagsRLUnitsResultsParameter
1369496 Well
02/02/2015 13:30:00ClientCollected by:
02/04/2015Received:
Drinking Water Affiliation: City of Seymour
Prepared: 02/05/2015 00:00:00
02/05/2015 00:00:00 QCgroupAnalyzed
sentSkeeter's Attentionz
Prepared: 02/09/2015 10:05:18
600/2-78-054 3.2.19 02/09/2015 10:05:18CAL QCgroupCalculated
3.59 1Sodium Adsorption Ratio - Liquid
Prepared: 02/09/2015 15:06:16
Calculation 02/09/2015 15:06:16CAL QCgroupCalculated
<0.0159 mg/L 0.0159Sulfide as Hydrogen Sulfidez
Prepared: 599920 02/05/2015 09:30:00
EPA 200.7 4.4 02/05/2015 15:47:55LPS QCgroup 600043Analyzed
<0.025 mg/L 0.025 7439-89-6Total Iron 09N
80.3 mg/L P0.500 7440-70-2Calcium 09N
5.17 mg/L P0.500 7440-09-7Potassium 09N
52.1 mg/L P0.500 7439-95-4Magnesium, Total 09N
EPA 200.7 4.4 02/06/2015 14:19:27LPS QCgroup 600201Analyzed
<0.500 mg/L 0.500 7440-42-8Boron 09N
11.1 mg/L 0.500 7740-21-3Silicon Recoverable 09N
EPA 200.7 4.4 02/06/2015 14:57:47LPS QCgroup 600250Analyzed
169 mg/L D2.50 7440-23-5Sodium 09N
Prepared: 599920 02/05/2015 09:30:00
EPA 200.7, Rev. 4.4 02/06/2015 14:19:27LPS QCgroup 600201Analyzed
1.19 mg/L 0.250 7440-24-6Strontium 09N
Prepared: 600855 02/11/2015 10:17:59
EPA 200.7, Rev. 4.4 02/11/2015 10:17:59LPS QCgroup 600855Analyzed
<0.025 mg/L 0.025 7439-89-6Dissolved Iron 03N
Prepared: 599920 02/05/2015 09:30:00
EPA 200.8 5.4 02/06/2015 18:29:00WOB QCgroup 600280Analyzed
<0.0005 mg/L 0.0005 7439-92-1Lead, Total 09N
0.0078 mg/L 0.005 7440-66-6Zinc, Total 09N
0.070 mg/L 0.005 7440-39-3Barium 09N
0.00408 mg/L 0.0005 7440-38-2Arsenic, Total 09N
0.000984 mg/L 0.0005 7440-47-3Chromium, Total 09N
0.0162 mg/L 0.001 7782-49-2Selenium, Total 09N
<0.001 mg/L 0.001 7439-96-5Manganese, Total 09N
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 2 of 38
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Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results02/18/2015Printed: Page 2 of 8
Results
BottleCASFlagsRLUnitsResultsParameter
1369496 Well
02/02/2015 13:30:00ClientCollected by:
02/04/2015Received:
Drinking Water Affiliation: City of Seymour
EPA 200.8 5.4 02/06/2015 18:29:00WOB QCgroup 600280Analyzed
<0.005 mg/L 0.005 7429-90-5Aluminum, Total 09N
0.00428 mg/L 0.001 7440-50-8Copper, Total 09N
<0.0002 mg/L 0.0002 7440-22-4Silver, Total 09N
<0.0005 mg/L 0.0005 7440-43-9Cadmium, Total 09N
Prepared: 599792 02/04/2015 14:15:00
EPA 245.1 3 02/05/2015 12:55:00WOB QCgroup 599968Analyzed
<0.200 ug/L 0.200 7439-97-6Mercury 07N
Prepared: 599986 02/04/2015 12:02:43
EPA 300.0 02/04/2015 12:02:43WJY QCgroup 599986Analyzed
1.55 mg/L 0.500Fluoride 01N
13.2 mg/L 0.100 14797-55-8Nitrate-Nitrogen Total 01N
Prepared: 600138 02/06/2015 02:05:20
EPA 300.0 02/06/2015 02:05:20WJY QCgroup 600138Analyzed
175 mg/L 15.0Chloride 01N
Prepared: 599986 02/04/2015 12:02:43
EPA 300.0 2.1 02/04/2015 12:02:43WJY QCgroup 599986Analyzed
0.704 mg/L 0.500Bromide 01N
<0.152 mg/L 0.152Nitrite-Nitrogen, Total 01N
Prepared: 600138 02/06/2015 02:05:20
EPA 300.0 2.1 02/06/2015 02:05:20WJY QCgroup 600138Analyzed
158 mg/L 15.0Sulfate 01N
Prepared: 599904 02/05/2015 09:55:00
EPA 350.1 2 02/05/2015 13:30:00RSV QCgroup 600021Analyzed
0.0767 mg/L 0.020Ammonia Nitrogen 08N
Prepared: 02/03/2015 18:00:00
EPA 904 (sub) 02/03/2015 18:00:00LLB QCgroupAnalyzed
sent to Outreac EHL1Radium 228 DW Subcontractz
Prepared: 599733 02/04/2015 11:15:00
SM 2130 B-94 02/04/2015 11:15:00CRG QCgroup 599733Analyzed
<1.00 NTU 1.00Turbidity 01N
Prepared: 599795 02/04/2015 12:20:00
SM 2320 B-97 02/04/2015 12:20:00BAA QCgroup 599795Analyzed
384 mg/L 1.00Total Alkalinity (as CaCO3) 01N
Prepared: 02/06/2015 09:35:57
SM 2340 B-97 02/06/2015 09:35:57CAL QCgroupCalculated
415 mg/L 0.500Total Hardness Ca/Mg Eq. CaCO3N
Prepared: 600058 02/06/2015 11:00:00
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 3 of 38
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Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results02/18/2015Printed: Page 3 of 8
Results
BottleCASFlagsRLUnitsResultsParameter
1369496 Well
02/02/2015 13:30:00ClientCollected by:
02/04/2015Received:
Drinking Water Affiliation: City of Seymour
SM 2540 C-97 02/06/2015 11:00:00MLC QCgroup 600058Analyzed
820 mg/L 100Total Dissolved Solids 01N
Prepared: 600324 02/06/2015 10:45:00
SM 2540 D-97 02/06/2015 10:45:00RAH QCgroup 600324Analyzed
10.5 mg/L 2.00Total Suspended Solids 01N
Prepared: 02/05/2015 12:35:16
SM 4500-CO2 D, 20th 02/05/2015 12:35:16CAL QCgroupCalculated
383 mg/L 0.5Bicarbonate (as CaCO3)/Calc
<0.5 mg/L 0.5Hydroxide
SM 4500-CO2 D, 20th 02/05/2015 13:05:58CAL QCgroupCalculated
1.43 mg/L 0.5Carbonate (as CaCO3)/Calc
19.2 mg/L 0.5Free Carbon Dioxide (Calc)
SM 4500-CO2 D, 20th 02/05/2015 13:36:10CAL QCgroupCalculated
357 mg/L 0.5Carbon Dioxide (Calc)
Prepared: 599923 02/05/2015 10:10:00
SM 4500-H+ B-96 02/05/2015 10:10:00JTF QCgroup 599923Analyzed
7.6@14C SU 2.00Laboratory pH 01N
Prepared: 600851 02/11/2015 08:40:00
SM 4500-P E-97 02/11/2015 08:40:00CRG QCgroup 600851Analyzed
0.109 mg/L 0.010 7723-14-0Total Phosphorus 05N
Prepared: 600327 02/09/2015 10:40:00
SM 4500-S2¯ D-2000 02/09/2015 10:40:00BAA QCgroup 600327Analyzed
<0.015 mg/L 0.015Sulfide 06N
Prepared: 600116 02/05/2015 11:38:55
SM 5310 C-96 02/05/2015 11:38:55ALH QCgroup 600116Analyzed
2.36 mg/L 0.500Total Organic Carbon 04N
Prepared: 02/03/2015 18:00:00
SM 7500-Ra B (SC) 19th ED (sub) 02/03/2015 18:00:00LLB QCgroupAnalyzed
sent to Outreac EHL1Radium 226 DW Subcontractz
Prepared: 02/03/2015 18:00:00
Subcontract 02/03/2015 18:00:00LLB QCgroupAnalyzed
sent to Spectra SPANParticle Size Distributionz
1369497 Reject
02/02/2015 14:00:00ClientCollected by:
02/04/2015Received:
Drinking Water Affiliation: City of Seymour
Prepared: 12/31/1899 00:00:00
00:00:00 QCgroupAnalyzed
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 4 of 38
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Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results02/18/2015Printed: Page 4 of 8
Results
BottleCASFlagsRLUnitsResultsParameter
1369497 Reject
02/02/2015 14:00:00ClientCollected by:
02/04/2015Received:
Drinking Water Affiliation: City of Seymour
00:00:00 QCgroupAnalyzed
sentSkeeter's Attentionz
Prepared: 02/09/2015 10:05:18
600/2-78-054 3.2.19 02/09/2015 10:05:18CAL QCgroupCalculated
8.33 1Sodium Adsorption Ratio - Liquid
Prepared: 02/09/2015 15:06:16
Calculation 02/09/2015 15:06:16CAL QCgroupCalculated
<0.0159 mg/L 0.0159Sulfide as Hydrogen Sulfidez
Prepared: 599920 02/05/2015 09:30:00
EPA 200.7 4.4 02/05/2015 15:58:10LPS QCgroup 600043Analyzed
<0.025 mg/L 0.025 7439-89-6Total Iron 08N
30.9 mg/L 0.500 7440-09-7Potassium 08N
EPA 200.7 4.4 02/06/2015 14:28:41LPS QCgroup 600201Analyzed
1.13 mg/L 1.00 7440-42-8Boron 08N
63.2 mg/L 1.00 7740-21-3Silicon Recoverable 08N
EPA 200.7 4.4 02/06/2015 15:07:55LPS QCgroup 600250Analyzed
458 mg/L 5.00 7440-70-2Calcium 08N
302 mg/L 5.00 7439-95-4Magnesium, Total 08N
939 mg/L 5.00 7440-23-5Sodium 08N
Prepared: 599920 02/05/2015 09:30:00
EPA 200.7, Rev. 4.4 02/06/2015 14:28:41LPS QCgroup 600201Analyzed
7.41 mg/L 0.500 7440-24-6Strontium 08N
Prepared: 600855 02/11/2015 10:28:07
EPA 200.7, Rev. 4.4 02/11/2015 10:28:07LPS QCgroup 600855Analyzed
<0.025 mg/L 0.025 7439-89-6Dissolved Iron 03N
Prepared: 599920 02/05/2015 09:30:00
EPA 200.8 5.4 02/06/2015 18:37:00WOB QCgroup 600280Analyzed
<0.0005 mg/L 0.0005 7439-92-1Lead, Total 08N
<0.005 mg/L 0.005 7440-66-6Zinc, Total 08N
0.372 mg/L 0.005 7440-39-3Barium 08N
0.0238 mg/L 0.0005 7440-38-2Arsenic, Total 08N
0.00418 mg/L 0.0005 7440-47-3Chromium, Total 08N
0.0906 mg/L 0.001 7782-49-2Selenium, Total 08N
<0.001 mg/L 0.001 7439-96-5Manganese, Total 08N
<0.005 mg/L 0.005 7429-90-5Aluminum, Total 08N
0.0042 mg/L 0.001 7440-50-8Copper, Total 08N
<0.0002 mg/L 0.0002 7440-22-4Silver, Total 08N
<0.0005 mg/L 0.0005 7440-43-9Cadmium, Total 08N
Prepared: 599959 02/05/2015 10:45:00
EPA 245.1 3 02/09/2015 14:37:00WOB QCgroup 600450Analyzed
<0.200 ug/L 0.200 7439-97-6Mercury 09N
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 5 of 38
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Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results02/18/2015Printed: Page 5 of 8
Results
BottleCASFlagsRLUnitsResultsParameter
1369497 Reject
02/02/2015 14:00:00ClientCollected by:
02/04/2015Received:
Drinking Water Affiliation: City of Seymour
Prepared: 599986 02/04/2015 12:27:21
EPA 300.0 02/04/2015 12:27:21WJY QCgroup 599986Analyzed
979 mg/L 15.0Chloride 01N
7.76 mg/L 5.00Fluoride 01N
66.9 mg/L 1.00 14797-55-8Nitrate-Nitrogen Total 01N
Prepared: 599986 02/04/2015 12:27:21
EPA 300.0 2.1 02/04/2015 12:27:21WJY QCgroup 599986Analyzed
<5.00 mg/L 5.00Bromide 01N
<1.00 mg/L 1.00Nitrite-Nitrogen, Total 01N
Prepared: 600138 02/06/2015 02:29:56
EPA 300.0 2.1 02/06/2015 02:29:56WJY QCgroup 600138Analyzed
1680 mg/L 150Sulfate 01N
Prepared: 599904 02/05/2015 09:55:00
EPA 350.1 2 02/05/2015 13:30:00RSV QCgroup 600021Analyzed
0.0821 mg/L 0.020Ammonia Nitrogen 07N
Prepared: 02/03/2015 18:00:00
EPA 904 (sub) 02/03/2015 18:00:00 QCgroupAnalyzed
sent to Outreac EHL1Radium 228 DW Subcontractz
Prepared: 599733 02/04/2015 11:15:00
SM 2130 B-94 02/04/2015 11:15:00CRG QCgroup 599733Analyzed
<1.00 NTU 1.00Turbidity 01N
Prepared: 599795 02/04/2015 12:20:00
SM 2320 B-97 02/04/2015 12:20:00BAA QCgroup 599795Analyzed
1480 mg/L 1.00Total Alkalinity (as CaCO3) 01N
Prepared: 02/09/2015 10:05:18
SM 2340 B-97 02/09/2015 10:05:18CAL QCgroupCalculated
2390 mg/L 5.00Total Hardness Ca/Mg Eq. CaCO3N
Prepared: 600058 02/06/2015 11:00:00
SM 2540 C-97 02/06/2015 11:00:00MLC QCgroup 600058Analyzed
5370 mg/L 100Total Dissolved Solids 01N
Prepared: 600324 02/06/2015 10:45:00
SM 2540 D-97 02/06/2015 10:45:00RAH QCgroup 600324Analyzed
6.50 mg/L 2.00Total Suspended Solids 01N
Prepared: 02/05/2015 12:35:16
SM 4500-CO2 D, 20th 02/05/2015 12:35:16CAL QCgroupCalculated
1480 mg/L 0.5Bicarbonate (as CaCO3)/Calc
<0.5 mg/L 0.5Hydroxide
SM 4500-CO2 D, 20th 02/05/2015 13:05:58CAL QCgroupCalculated
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 6 of 38
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Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results02/18/2015Printed: Page 6 of 8
Results
BottleCASFlagsRLUnitsResultsParameter
1369497 Reject
02/02/2015 14:00:00ClientCollected by:
02/04/2015Received:
Drinking Water Affiliation: City of Seymour
SM 4500-CO2 D, 20th 02/05/2015 13:05:58CAL QCgroupCalculated
3.49 mg/L 0.5Carbonate (as CaCO3)/Calc
118 mg/L 0.5Free Carbon Dioxide (Calc)
SM 4500-CO2 D, 20th 02/05/2015 13:36:10CAL QCgroupCalculated
1420 mg/L 0.5Carbon Dioxide (Calc)
Prepared: 599923 02/05/2015 10:10:00
SM 4500-H+ B-96 02/05/2015 10:10:00JTF QCgroup 599923Analyzed
7.4@14C SU 2.00Laboratory pH 01N
Prepared: 600851 02/11/2015 08:40:00
SM 4500-P E-97 02/11/2015 08:40:00CRG QCgroup 600851Analyzed
1.07 mg/L 0.050 7723-14-0Total Phosphorus 05N
Prepared: 600327 02/09/2015 10:40:00
SM 4500-S2¯ D-2000 02/09/2015 10:40:00BAA QCgroup 600327Analyzed
<0.015 mg/L 0.015Sulfide 06N
Prepared: 600116 02/05/2015 12:06:34
SM 5310 C-96 02/05/2015 12:06:34ALH QCgroup 600116Analyzed
6.46 mg/L 0.500Total Organic Carbon 04N
Prepared: 02/03/2015 18:00:00
SM 7500-Ra B (SC) 19th ED (sub) 02/03/2015 18:00:00 QCgroupAnalyzed
sent to Outreac EHL1Radium 226 DW Subcontractz
Prepared: 02/03/2015 18:00:00
Subcontract 02/03/2015 18:00:00 QCgroupAnalyzed
sent to Spectra SPANParticle Size Distributionz
Sample Preparation
1369496 Well 02/04/2015Received:
Prepared: 02/02/2015 13:38:00
02/02/2015 13:38:00Cli QCgroupAnalyzed
filteredClient Field Filtration (Onsite)N
02/04/2015 10:48:39 QCgroupAnalyzed
<2 SUBottle pH 02z
02/04/2015 11:05:44CAL QCgroupCalculated
VerifiedSUB Shippedz
Prepared: 600619 02/10/2015 14:57:04
02/10/2015 14:57:04LPS QCgroup 600619Analyzed
COMPLETEDTransfer to ICP/MS 03z
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 7 of 38
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Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results02/18/2015Printed: Page 7 of 8
Sample Preparation
1369496 Well 02/04/2015Received:
Prepared: 599920 02/05/2015 09:30:00
EPA 200.2 2.8 02/05/2015 09:30:00TES QCgroup 599920Analyzed
50/50 mlLiquid Metals Digestion 02N
Prepared: 599792 02/04/2015 14:15:00
EPA 245.1 3 02/04/2015 14:15:00PJD QCgroup 599792Analyzed
50/25 mlMercury Liquid Metals Digestion 02N
Prepared: 599904 02/05/2015 09:55:00
EPA 350.2, Rev. 2.0 02/05/2015 09:55:00JJH QCgroup 599904Analyzed
50/50 mlAmmonia Distillation 06N
Prepared: 599932 02/06/2015 12:16:52
SM 2540 D, 20th Ed. 02/06/2015 12:16:52RAH QCgroup 599932Analyzed
StartedTSS Set StartedN
1369497 Reject 02/04/2015Received:
Prepared: 02/02/2015 14:10:00
02/02/2015 14:10:00CLI QCgroupAnalyzed
filteredClient Field Filtration (Onsite)N
02/04/2015 10:50:08 QCgroupAnalyzed
8(<2) SUBottle pH 02z
02/05/2015 04:05:52CAL QCgroupCalculated
VerifiedSUB Shippedz
Prepared: 600619 02/10/2015 14:57:04
02/10/2015 14:57:04LPS QCgroup 600619Analyzed
COMPLETEDTransfer to ICP/MS 03z
Prepared: 599920 02/05/2015 09:30:00
EPA 200.2 2.8 02/05/2015 09:30:00TES QCgroup 599920Analyzed
50/50 mlLiquid Metals Digestion 02N
Prepared: 599959 02/05/2015 10:45:00
EPA 245.1 3 02/05/2015 10:45:00CLK QCgroup 599959Analyzed
50/25 mlMercury Liquid Metals Digestion 02N
Prepared: 599904 02/05/2015 09:55:00
EPA 350.2, Rev. 2.0 02/05/2015 09:55:00JJH QCgroup 599904Analyzed
50/50 mlAmmonia Distillation 05N
Prepared: 599932 02/06/2015 12:16:52
SM 2540 D, 20th Ed. 02/06/2015 12:16:52RAH QCgroup 599932Analyzed
StartedTSS Set StartedN
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 8 of 38
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Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results02/18/2015Printed: Page 8 of 8
Qualifiers:
D - Duplicate RPD was higher than expected P - Spike recovery outside control limits due to possible matrix
We report results on an 'As Received' or wet basis unless marked 'Dry Weight'. Unless otherwise noted, testing was performed at Ana-lab's
corporate laboratory that holds the following Federal and State certificates: Texas Department of Health Lead Firm Certificate 2110076, US
Department of Agriculture Soil Import Permit S-37592, Texas Commisson on Environmental Quality Drinking Water Laboratory Certificate
TX219, Texas Commission on Environmental Quality NELAP T104704201, Oklahoma Department of Environmental Quality Drinking
Water Certification Lab ID# D9913, EPA Lab Number TX00063, USEPA Approved Perchlorate Testing Lab, Oklahoma Department of
Environmental Quality Laboratory Certificate 8125, Arkansas Department of Environmental Quality Certification #03-070-0, Louisiana
Department of Environmental Quality Laboratory Certification (NELAP, LELAP) #02008, Louisiana Department of Health and Hospitals
Drinking Water (NELAP) # LA030020, US Department of Energy Approved, State of Kansas Department of Health and Environment
Waste Water and Solid/Hazardous Waste Cert. E-10365. The Accredited column designates accreditation by N -- NELAC, or z -- not
covered under NELAC scope of accreditation.
These analytical results relate to the sample tested. This report may NOT be reproduced EXCEPT in FULL without written approval of
Ana-Lab Corp. Unless otherwise specified, these test results meet the requirements of NELAC.
RL is the Reporting Limit (sample specific quantitation limit) and is at or above the Method Detection Limit (MDL). CAS is Chemical
Abstract Service number.
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 9 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Report To
Results and LimitsPage 1 of 602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
City of Seymour
Rick Garcia
301 North Washington
Seymour, TX 76380
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ProjectAccount
685118SEYM
OutUnitsLimitOut Results *ResultsParameter FlagAlert
1369496 Well Collection: 02/02/2015 13:30:00
Column 'Limits' from EPA Drinking Water Limits (40 CFR 141 MCls -- see http://water.epa.gov/drink/contaminants/). Gross Beta Alert Limit is from 40 CFR
141.66 and IS NOT an MCL.
00:00:002/5/15Analyzed
Skeeter's Attention sent
600/2-78-054 3.2.19 CAL10:05:182/9/15Analyzed
Sodium Adsorption Ratio - Liquid 13.59
Calculation CAL15:06:162/9/15Analyzed
Sulfide as Hydrogen Sulfide mg/L<0.0159
EPA 200.7 4.4 LPS15:47:552/5/15Analyzed 600043
Calcium mg/L80.3 P
Magnesium, Total mg/L52.1 P
Potassium mg/L5.17 P
Total Iron mg/L<0.025 MCL 0.300
EPA 200.7 4.4 LPS14:19:272/6/15Analyzed 600201
Boron mg/L<0.500
Silicon Recoverable mg/L11.1
EPA 200.7 4.4 LPS14:57:472/6/15Analyzed 600250
Sodium mg/L169 D
EPA 200.7, Rev. 4.4 LPS14:19:272/6/15Analyzed 600201
Strontium mg/L1.19
EPA 200.7, Rev. 4.4 LPS10:17:592/11/15Analyzed 600855
Dissolved Iron mg/L<0.025 MCL 0.300
EPA 200.8 5.4 WOB18:29:002/6/15Analyzed 600280
Aluminum, Total mg/L<0.005 MCL 0.050
Arsenic, Total mg/L0.00408 MCL 0.010
Barium mg/L0.070 MCL 2.00
Cadmium, Total mg/L<0.0005 MCL 0.005
Chromium, Total mg/L0.000984 MCL 0.100
Copper, Total mg/L0.00428 MCL 1.00
Lead, Total mg/L<0.0005 MCL 0.015
Manganese, Total mg/L<0.001 MCL 0.050
Selenium, Total mg/L0.0162 MCL 0.050
Silver, Total mg/L<0.0002 MCL 0.100
Zinc, Total mg/L0.0078 MCL 5.00
Form rptRLHCompliance Created 06/03/2006 v1.0LDSClient v1.6.7.992
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662 North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
www.ana-lab.com
NELAP-accredited #T104704201
Report Page 10 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Report To
Results and LimitsPage 2 of 602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
City of Seymour
Rick Garcia
301 North Washington
Seymour, TX 76380
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ProjectAccount
685118SEYM
OutUnitsLimitOut Results *ResultsParameter FlagAlert
1369496 Well Collection: 02/02/2015 13:30:00
Column 'Limits' from EPA Drinking Water Limits (40 CFR 141 MCls -- see http://water.epa.gov/drink/contaminants/). Gross Beta Alert Limit is from 40 CFR
141.66 and IS NOT an MCL.
EPA 245.1 3 WOB12:55:002/5/15Analyzed 599968
Mercury ug/L<0.200 MCL 2.00
EPA 300.0 WJY12:02:432/4/15Analyzed 599986
Fluoride mg/L1.55 MCL 2.00
Nitrate-Nitrogen Total mg/L13.2 MCL 10.0
EPA 300.0 WJY02:05:202/6/15Analyzed 600138
Chloride mg/L175 MCL 250
EPA 300.0 2.1 WJY12:02:432/4/15Analyzed 599986
Bromide mg/L0.704
Nitrite-Nitrogen, Total mg/L<0.152 MCL 1.00
EPA 300.0 2.1 WJY02:05:202/6/15Analyzed 600138
Sulfate mg/L158 MCL 250
EPA 350.1 2 RSV13:30:002/5/15Analyzed 600021
Ammonia Nitrogen mg/L0.0767
EPA 904 (sub) LLB18:00:002/3/15Analyzed
Radium 228 DW Subcontract sent to Outreac MCL 5.00
SM 2130 B-94 CRG11:15:002/4/15Analyzed 599733
Turbidity NTU<1.00 MCL 1.00
SM 2320 B-97 BAA12:20:002/4/15Analyzed 599795
Total Alkalinity (as CaCO3) mg/L384
SM 2340 B-97 CAL09:35:572/6/15Analyzed
Total Hardness Ca/Mg Eq. CaCO3 mg/L415
SM 2540 C-97 MLC11:00:002/6/15Analyzed 600058
Total Dissolved Solids mg/L820 MCL 500
SM 2540 D-97 RAH10:45:002/6/15Analyzed 600324
Total Suspended Solids mg/L10.5 MCL 2.00
SM 4500-CO2 D, 20th CAL12:35:162/5/15Analyzed
Bicarbonate (as CaCO3)/Calc mg/L383
Carbon Dioxide (Calc) mg/L357
Form rptRLHCompliance Created 06/03/2006 v1.0LDSClient v1.6.7.992
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662 North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
www.ana-lab.com
NELAP-accredited #T104704201
Report Page 11 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Report To
Results and LimitsPage 3 of 602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
City of Seymour
Rick Garcia
301 North Washington
Seymour, TX 76380
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ProjectAccount
685118SEYM
OutUnitsLimitOut Results *ResultsParameter FlagAlert
1369496 Well Collection: 02/02/2015 13:30:00
Column 'Limits' from EPA Drinking Water Limits (40 CFR 141 MCls -- see http://water.epa.gov/drink/contaminants/). Gross Beta Alert Limit is from 40 CFR
141.66 and IS NOT an MCL.
SM 4500-CO2 D, 20th CAL13:05:582/5/15Analyzed
Carbonate (as CaCO3)/Calc mg/L1.43
Free Carbon Dioxide (Calc) mg/L19.2
Hydroxide mg/L<0.5
SM 4500-H+ B-96 JTF10:10:002/5/15Analyzed 599923
Laboratory pH SU7.6@14C 6.50 - 98.50
SM 4500-P E-97 CRG08:40:002/11/15Analyzed 600851
Total Phosphorus mg/L0.109
SM 4500-S2¯ D-2000 BAA10:40:002/9/15Analyzed 600327
Sulfide mg/L<0.015
SM 5310 C-96 ALH11:38:552/5/15Analyzed 600116
Total Organic Carbon mg/L2.36
SM 7500-Ra B (SC) 19th ED (sub) LLB18:00:002/3/15Analyzed
Radium 226 DW Subcontract sent to Outreac MCL 5.00
Subcontract LLB18:00:002/3/15Analyzed
Particle Size Distribution sent to Spectra
1369497 Reject Collection: 02/02/2015 14:00:00
Column 'Limits' from EPA Drinking Water Limits (40 CFR 141 MCls -- see http://water.epa.gov/drink/contaminants/). Gross Beta Alert Limit is from 40 CFR
141.66 and IS NOT an MCL.
00:00:0012/31/99Analyzed
Skeeter's Attention sent
600/2-78-054 3.2.19 CAL10:05:182/9/15Analyzed
Sodium Adsorption Ratio - Liquid 18.33
Calculation CAL15:06:162/9/15Analyzed
Sulfide as Hydrogen Sulfide mg/L<0.0159
EPA 200.7 4.4 LPS15:58:102/5/15Analyzed 600043
Potassium mg/L30.9
Form rptRLHCompliance Created 06/03/2006 v1.0LDSClient v1.6.7.992
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662 North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
www.ana-lab.com
NELAP-accredited #T104704201
Report Page 12 of 38
1
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Report To
Results and LimitsPage 4 of 602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
City of Seymour
Rick Garcia
301 North Washington
Seymour, TX 76380
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ProjectAccount
685118SEYM
OutUnitsLimitOut Results *ResultsParameter FlagAlert
1369497 Reject Collection: 02/02/2015 14:00:00
Column 'Limits' from EPA Drinking Water Limits (40 CFR 141 MCls -- see http://water.epa.gov/drink/contaminants/). Gross Beta Alert Limit is from 40 CFR
141.66 and IS NOT an MCL.
EPA 200.7 4.4 LPS15:58:102/5/15Analyzed 600043
Total Iron mg/L<0.025 MCL 0.300
EPA 200.7 4.4 LPS14:28:412/6/15Analyzed 600201
Boron mg/L1.13
Silicon Recoverable mg/L63.2
EPA 200.7 4.4 LPS15:07:552/6/15Analyzed 600250
Calcium mg/L458
Magnesium, Total mg/L302
Sodium mg/L939
EPA 200.7, Rev. 4.4 LPS14:28:412/6/15Analyzed 600201
Strontium mg/L7.41
EPA 200.7, Rev. 4.4 LPS10:28:072/11/15Analyzed 600855
Dissolved Iron mg/L<0.025 MCL 0.300
EPA 200.8 5.4 WOB18:37:002/6/15Analyzed 600280
Aluminum, Total mg/L<0.005 MCL 0.050
Arsenic, Total mg/L0.0238 MCL 0.010
Barium mg/L0.372 MCL 2.00
Cadmium, Total mg/L<0.0005 MCL 0.005
Chromium, Total mg/L0.00418 MCL 0.100
Copper, Total mg/L0.0042 MCL 1.00
Lead, Total mg/L<0.0005 MCL 0.015
Manganese, Total mg/L<0.001 MCL 0.050
Selenium, Total mg/L0.0906 MCL 0.050
Silver, Total mg/L<0.0002 MCL 0.100
Zinc, Total mg/L<0.005 MCL 5.00
EPA 245.1 3 WOB14:37:002/9/15Analyzed 600450
Mercury ug/L<0.200 MCL 2.00
EPA 300.0 WJY12:27:212/4/15Analyzed 599986
Chloride mg/L979 MCL 250
Fluoride mg/L7.76 MCL 2.00
Nitrate-Nitrogen Total mg/L66.9 MCL 10.0
EPA 300.0 2.1 WJY12:27:212/4/15Analyzed 599986
Bromide mg/L<5.00
Form rptRLHCompliance Created 06/03/2006 v1.0LDSClient v1.6.7.992
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662 North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
www.ana-lab.com
NELAP-accredited #T104704201
Report Page 13 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Report To
Results and LimitsPage 5 of 602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
City of Seymour
Rick Garcia
301 North Washington
Seymour, TX 76380
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ProjectAccount
685118SEYM
OutUnitsLimitOut Results *ResultsParameter FlagAlert
1369497 Reject Collection: 02/02/2015 14:00:00
Column 'Limits' from EPA Drinking Water Limits (40 CFR 141 MCls -- see http://water.epa.gov/drink/contaminants/). Gross Beta Alert Limit is from 40 CFR
141.66 and IS NOT an MCL.
EPA 300.0 2.1 WJY12:27:212/4/15Analyzed 599986
Nitrite-Nitrogen, Total mg/L<1.00 MCL 1.00
EPA 300.0 2.1 WJY02:29:562/6/15Analyzed 600138
Sulfate mg/L1680 MCL 250
EPA 350.1 2 RSV13:30:002/5/15Analyzed 600021
Ammonia Nitrogen mg/L0.0821
EPA 904 (sub) 18:00:002/3/15Analyzed
Radium 228 DW Subcontract sent to Outreac MCL 5.00
SM 2130 B-94 CRG11:15:002/4/15Analyzed 599733
Turbidity NTU<1.00 MCL 1.00
SM 2320 B-97 BAA12:20:002/4/15Analyzed 599795
Total Alkalinity (as CaCO3) mg/L1480
SM 2340 B-97 CAL10:05:182/9/15Analyzed
Total Hardness Ca/Mg Eq. CaCO3 mg/L2390
SM 2540 C-97 MLC11:00:002/6/15Analyzed 600058
Total Dissolved Solids mg/L5370 MCL 500
SM 2540 D-97 RAH10:45:002/6/15Analyzed 600324
Total Suspended Solids mg/L6.50 MCL 2.00
SM 4500-CO2 D, 20th CAL12:35:162/5/15Analyzed
Bicarbonate (as CaCO3)/Calc mg/L1480
Carbon Dioxide (Calc) mg/L1420
Carbonate (as CaCO3)/Calc mg/L3.49
Free Carbon Dioxide (Calc) mg/L118
Hydroxide mg/L<0.5
SM 4500-H+ B-96 JTF10:10:002/5/15Analyzed 599923
Laboratory pH SU7.4@14C 6.50 - 98.50
SM 4500-P E-97 CRG08:40:002/11/15Analyzed 600851
Total Phosphorus mg/L1.07
Form rptRLHCompliance Created 06/03/2006 v1.0LDSClient v1.6.7.992
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662 North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
www.ana-lab.com
NELAP-accredited #T104704201
Report Page 14 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Report To
Results and LimitsPage 6 of 602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
City of Seymour
Rick Garcia
301 North Washington
Seymour, TX 76380
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ProjectAccount
685118SEYM
OutUnitsLimitOut Results *ResultsParameter FlagAlert
1369497 Reject Collection: 02/02/2015 14:00:00
Column 'Limits' from EPA Drinking Water Limits (40 CFR 141 MCls -- see http://water.epa.gov/drink/contaminants/). Gross Beta Alert Limit is from 40 CFR
141.66 and IS NOT an MCL.
SM 4500-S2¯ D-2000 BAA10:40:002/9/15Analyzed 600327
Sulfide mg/L<0.015
SM 5310 C-96 ALH12:06:342/5/15Analyzed 600116
Total Organic Carbon mg/L6.46
SM 7500-Ra B (SC) 19th ED (sub) 18:00:002/3/15Analyzed
Radium 226 DW Subcontract sent to Outreac MCL 5.00
Subcontract 18:00:002/3/15Analyzed
Particle Size Distribution sent to Spectra
* Out Results are beyond the listed limit. Please verify with your consultant or regulatory authority whether these limits apply to this project.
Qualifiers:
D - Duplicate RPD was higher than expected P - Spike recovery outside control limits due to possible matrix
We report results on an 'As Received' or wet basis unless marked 'Dry Weight'. Unless otherwise noted, testing was performed at Ana-lab's
corporate laboratory that holds the following Federal and State certificates: Texas Department of Health Lead Firm Certificate 2110076, US
Department of Agriculture Soil Import Permit S-37592, Texas Commisson on Environmental Quality Drinking Water Laboratory Certificate
TX219, Texas Commission on Environmental Quality NELAP T104704201, Oklahoma Department of Environmental Quality Drinking Water
Certification Lab ID# D9913, EPA Lab Number TX00063, USEPA Approved Perchlorate Testing Lab, Oklahoma Department of Environmental
Quality Laboratory Certificate 8125, Arkansas Department of Environmental Quality Certification #03-070-0, Louisiana Department of
Environmental Quality Laboratory Certification (NELAP, LELAP) #02008, Louisiana Department of Health and Hospitals Drinking Water
(NELAP) # LA030020, US Department of Energy Approved, State of Kansas Department of Health and Environment Waste Water and
Solid/Hazardous Waste Cert. E-10365. The Accredited column designates accreditation by N -- NELAC, or z -- not covered under NELAC
scope of accreditation.
These analytical results relate to the sample tested. This report may NOT be reproduced EXCEPT in FULL without written approval of
Ana-Lab Corp. Unless otherwise specified, these test results meet the requirements of NELAC.
! Reporting Level above the listed target.
Form rptRLHCompliance Created 06/03/2006 v1.0LDSClient v1.6.7.992
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662 North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
www.ana-lab.com
NELAP-accredited #T104704201
Report Page 15 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 1 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
SEYM-NAccount Project
City of Seymour
Rick Garcia
301 North Washington
Seymour, TX 76380
Report ToDW
685118
EPA 350.1 2Drinking Water 600021
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Ammonia Nitrogen 599904 ND 0.00974 0.020 mg/L 115191783
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Ammonia Nitrogen 2.12 2.00 mg/L 106 90.0 - 110 115191753
Ammonia Nitrogen 2.12 2.00 mg/L 106 90.0 - 110 115191764
Ammonia Nitrogen 2.13 2.00 mg/L 106 90.0 - 110 115191775
Ammonia Nitrogen 2.14 2.00 mg/L 107 90.0 - 110 115191786
Ammonia Nitrogen 2.17 2.00 mg/L 108 90.0 - 110 115191791
Ammonia Nitrogen 2.15 2.00 mg/L 108 90.0 - 110 115191801
Ammonia Nitrogen 2.15 2.00 mg/L 108 90.0 - 110 115191810
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Ammonia Nitrogen 1369818 Duplicate 0.191 0.182 mg/L 4.83 20.0
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Ammonia Nitrogen 2.15 2.00 mg/L 108 90.0 - 110 115191752
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Ammonia Nitrogen 599904 2.14 2.00 mg/L 107 90.0 - 110 115191784
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Ammonia Nitrogen 599904 2.14 2.04 2.00 90.0 - 110 107 102 mg/L 4.78 20.0
Mat. Spike
FileLimits %Recovery %UnitsKnownUnknownSpikeSampleParameter
Ammonia Nitrogen 1369818 2.43 0.182 2.00 mg/L 112 80.0 - 120 115191789
SM 2540 C-97Drinking Water 600058
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Total Dissolved Solids 600058 ND 9.24 10.0 mg/L 115192833
ControlBlk
FileUnitsMQLMDLReadingPrepSetParameter
Total Dissolved Solids 600058 0.0001 grams 115192820
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Total Dissolved Solids 1369086 Duplicate 120 108 mg/L 10.5 20.0
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 16 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 2 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Total Dissolved Solids 600058 192 200 mg/L 96.0 85.0 - 115 115192834
Standard
FileOutLimits%Recover%UnitsKnownReadingSampleParameter
Total Dissolved Solids 92.0 100 mg/L 92.0 90.0 - 110 115192821
SM 2540 D-97Drinking Water 600324
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Total Suspended Solids 600324 ND 2.00 2.00 mg/L 115199089
Total Suspended Solids 600324 ND 2.00 2.00 mg/L 115199123
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Total Suspended Solids 1369400 Duplicate 136 134 mg/L 1.48 20.0
Total Suspended Solids 1369443 Duplicate 4.00 ND mg/L 200 20.0
Total Suspended Solids 1369492 Duplicate 52.9 47.1 mg/L 11.6 20.0
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Total Suspended Solids 600324 49.0 50.0 mg/L 98.0 90.0 - 110 115199122
Standard
FileOutLimits%Recover%UnitsKnownReadingSampleParameter
Total Suspended Solids 573062 98.0 100 mg/L 98.0 90.0 - 110 115199090
EPA 300.0Drinking Water 599986
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Bromide 599986 ND 0.0075 0.050 mg/L 115190737
Chloride 599986 0.0078 0.0053 0.300 mg/L 115190737
Fluoride 599986 ND 0.00863 0.050 mg/L 115190737
Nitrate-Nitrogen Total 599986 ND 0.00185 0.020 mg/L 115190737
Nitrite-Nitrogen, Total 599986 ND 0.00717 0.0152 mg/L 115190737
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Bromide 10.1 10.0 mg/L 101 90.0 - 110 115190734
Bromide 10.1 10.0 mg/L 101 90.0 - 110 115190744
Bromide 9.99 10.0 mg/L 99.9 90.0 - 110 115190745
Bromide 9.89 10.0 mg/L 98.9 90.0 - 110 115190754
Chloride 10.5 10.0 mg/L 105 90.0 - 110 115190734
Chloride 10.4 10.0 mg/L 104 90.0 - 110 115190744
Chloride 10.0 10.0 mg/L 100 90.0 - 110 115190745
Chloride 9.96 10.0 mg/L 99.6 90.0 - 110 115190754
Fluoride 9.99 10.0 mg/L 99.9 90.0 - 110 115190734
Fluoride 9.94 10.0 mg/L 99.4 90.0 - 110 115190744
Fluoride 9.92 10.0 mg/L 99.2 90.0 - 110 115190745
Fluoride 9.88 10.0 mg/L 98.8 90.0 - 110 115190754
Nitrate-Nitrogen Total 2.31 2.26 mg/L 102 90.0 - 110 115190734
Nitrate-Nitrogen Total 2.29 2.26 mg/L 101 90.0 - 110 115190744
Nitrate-Nitrogen Total 2.28 2.26 mg/L 101 90.0 - 110 115190745
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 17 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 3 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Nitrate-Nitrogen Total 2.26 2.26 mg/L 100 90.0 - 110 115190754
Nitrite-Nitrogen, Total 3.13 3.04 mg/L 103 90.0 - 110 115190734
Nitrite-Nitrogen, Total 3.09 3.04 mg/L 102 90.0 - 110 115190744
Nitrite-Nitrogen, Total 3.09 3.04 mg/L 102 90.0 - 110 115190745
Nitrite-Nitrogen, Total 3.06 3.04 mg/L 101 90.0 - 110 115190754
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Bromide 599986 0.982 1.00 mg/L 98.2 90.0 - 110 115190735
Chloride 599986 1.06 1.00 mg/L 106 90.0 - 110 115190735
Fluoride 599986 0.959 1.00 mg/L 95.9 90.0 - 110 115190735
Nitrate-Nitrogen Total 599986 0.232 0.226 mg/L 103 90.0 - 110 115190735
Nitrite-Nitrogen, Total 599986 0.304 0.304 mg/L 99.9 90.0 - 110 115190735
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Bromide 599986 0.982 0.981 1.00 90.0 - 110 98.2 98.1 mg/L 0.102 20.0
Chloride 599986 1.06 1.07 1.00 90.0 - 110 106 107 mg/L 0.939 20.0
Fluoride 599986 0.959 0.943 1.00 90.0 - 110 95.9 94.3 mg/L 1.68 20.0
Nitrate-Nitrogen Total 599986 0.232 0.231 0.226 90.0 - 110 103 102 mg/L 0.432 20.0
Nitrite-Nitrogen, Total 599986 0.304 0.308 0.304 90.0 - 110 99.9 101 mg/L 1.31 20.0
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Bromide 1369280 0.977 ND 1.00 80.0 - 120 97.7 mg/L 20.0
Chloride 1369280 0.953 ND 1.00 80.0 - 120 95.3 mg/L 20.0
Fluoride 1369280 0.908 ND 1.00 80.0 - 120 90.8 mg/L 20.0
Nitrate-Nitrogen Total 1369280 0.237 0.0102 0.226 80.0 - 120 105 mg/L 20.0
Nitrite-Nitrogen, Total 1369280 0.301 ND 0.304 80.0 - 120 99.0 mg/L 20.0
Bromide 1369281 9.68 0.124 10.0 80.0 - 120 95.6 mg/L 20.0
Chloride 1369281 15.1 5.84 10.0 80.0 - 120 92.6 mg/L 20.0
Fluoride 1369281 9.29 ND 10.0 80.0 - 120 92.9 mg/L 20.0
Nitrate-Nitrogen Total 1369281 2.16 0.0115 2.26 80.0 - 120 95.6 mg/L 20.0
Nitrite-Nitrogen, Total 1369281 2.97 ND 3.04 80.0 - 120 97.7 mg/L 20.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Bromide 1369280 0.977 0.968 ND 1.00 80.0 - 120 97.7 96.8 mg/L 0.925 20.0
Chloride 1369280 0.953 0.950 ND 1.00 80.0 - 120 95.3 95.0 mg/L 0.315 20.0
Fluoride 1369280 0.908 0.918 ND 1.00 80.0 - 120 90.8 91.8 mg/L 1.10 20.0
Nitrate-Nitrogen Total 1369280 0.237 0.234 0.0102 0.226 80.0 - 120 105 104 mg/L 0.957 20.0
Nitrite-Nitrogen, Total 1369280 0.301 0.302 ND 0.304 80.0 - 120 99.0 99.3 mg/L 0.303 20.0
Bromide 1369281 9.68 9.75 0.124 10.0 80.0 - 120 95.6 96.3 mg/L 0.730 20.0
Chloride 1369281 15.1 15.0 5.84 10.0 80.0 - 120 92.6 91.6 mg/L 1.09 20.0
Fluoride 1369281 9.29 9.32 ND 10.0 80.0 - 120 92.9 93.2 mg/L 0.322 20.0
Nitrate-Nitrogen Total 1369281 2.16 2.19 0.0115 2.26 80.0 - 120 95.6 96.9 mg/L 1.35 20.0
Nitrite-Nitrogen, Total 1369281 2.97 2.92 ND 3.04 80.0 - 120 97.7 96.1 mg/L 1.65 20.0
EPA 300.0Drinking Water 600138
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Chloride 600138 0.0081 0.0053 0.300 mg/L 115194717
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 18 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 4 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Sulfate 600138 0.033 0.00775 0.300 mg/L * 115194717
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Chloride 10.0 10.0 mg/L 100 90.0 - 110 115194714
Chloride 10.0 10.0 mg/L 100 90.0 - 110 115194731
Chloride 10.0 10.0 mg/L 100 90.0 - 110 115194742
Sulfate 9.99 10.0 mg/L 99.9 90.0 - 110 115194714
Sulfate 10.0 10.0 mg/L 100 90.0 - 110 115194731
Sulfate 10.0 10.0 mg/L 100 90.0 - 110 115194742
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Chloride 600138 1.05 1.00 mg/L 105 90.0 - 110 115194715
Sulfate 600138 1.01 1.00 mg/L 101 90.0 - 110 115194715
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Chloride 600138 1.05 1.05 1.00 90.0 - 110 105 105 mg/L 0 20.0
Sulfate 600138 1.01 0.997 1.00 90.0 - 110 101 99.7 mg/L 1.30 20.0
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Chloride 1369936 174 132 50.0 80.0 - 120 84.0 mg/L 20.0
Sulfate 1369936 181 131 50.0 80.0 - 120 100 mg/L 20.0
Chloride 1369937 161 118 50.0 80.0 - 120 86.0 mg/L 20.0
Sulfate 1369937 161 117 50.0 80.0 - 120 88.0 mg/L 20.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Chloride 1369936 174 172 132 50.0 80.0 - 120 84.0 80.0 mg/L 4.88 20.0
Sulfate 1369936 181 174 131 50.0 80.0 - 120 100 86.0 mg/L 15.1 20.0
Chloride 1369937 161 163 118 50.0 80.0 - 120 86.0 90.0 mg/L 4.55 20.0
Sulfate 1369937 161 161 117 50.0 80.0 - 120 88.0 88.0 mg/L 0 20.0
EPA 245.1 3Drinking Water 599968
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Mercury 599792 ND 0.072 0.100 ug/L 115190303
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Mercury 5.09 5.000 ug/L 102 90.0 - 110 115190302
Mercury 5.10 5.000 ug/L 102 90.0 - 110 115190313
Mercury 5.11 5.000 ug/L 102 90.0 - 110 115190324
Mercury 4.92 5.000 ug/L 98.4 90.0 - 110 115190333
ICL
FileOutLimits%Recover%UnitsKnownReadingParameter
Mercury 19.8 20.00 ug/L 99.0 90.0 - 110 115190301
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Mercury 5.31 5.000 ug/L 106 90.0 - 110 115190300
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 19 of 38
1
2
3
4
5
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 5 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Mercury 599792 5.71 5.00 ug/L 114 85.0 - 115 115190304
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Mercury 599792 5.71 5.73 5.00 85.0 - 115 114 115 ug/L 0.350 20.0
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Mercury 1367344 11.6 0 0.118 10.0 70.0 - 130 115 ug/L 14.0
Mercury 1369521 11.4 0 ND 10.0 70.0 - 130 114 ug/L 14.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Mercury 1367344 11.6 11.5 0.118 10.0 70.0 - 130 115 114 ug/L 0.873 14.0
Mercury 1369521 11.4 11.3 ND 10.0 70.0 - 130 114 113 ug/L 0.881 14.0
EPA 200.7 4.4Drinking Water 600043
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Calcium 600043 0.0545 0.0419 0.500 mg/L 115192515
Magnesium, Total 600043 ND 0.0102 0.500 mg/L 115192515
Potassium 600043 0.104 0.0765 0.500 mg/L 115192515
Total Iron 600043 ND 0.00504 0.025 mg/L 115192515
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Calcium 26.4 25.0 mg/L 106 90.0 - 110 115192512
Calcium 25.2 25.0 mg/L 101 90.0 - 110 115192514
Calcium 26.5 25.0 mg/L 106 90.0 - 110 115192525
Calcium 26.6 25.0 mg/L 106 90.0 - 110 115192536
Magnesium, Total 25.7 25.0 mg/L 103 90.0 - 110 115192514
Magnesium, Total 27.0 25.0 mg/L 108 90.0 - 110 115192525
Magnesium, Total 27.2 25.0 mg/L 109 90.0 - 110 115192536
Potassium 24.0 25.0 mg/L 96.0 90.0 - 110 115192514
Potassium 24.9 25.0 mg/L 99.6 90.0 - 110 115192525
Total Iron 2.52 2.50 mg/L 101 90.0 - 110 115192514
Total Iron 2.65 2.50 mg/L 106 90.0 - 110 115192525
Total Iron 2.67 2.50 mg/L 107 90.0 - 110 115192536
Total Iron 2.65 2.50 mg/L 106 90.0 - 110 115192546
Total Iron 2.64 2.50 mg/L 106 90.0 - 110 115192556
ICL
FileOutLimits%Recover%UnitsKnownReadingParameter
Calcium 49.4 50.0 mg/L 98.8 95.0 - 105 115192507
Magnesium, Total 49.5 50.0 mg/L 99.0 95.0 - 105 115192507
Potassium 50.2 50.0 mg/L 100 95.0 - 105 115192507
Total Iron 4.99 5.00 mg/L 99.8 95.0 - 105 115192507
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Calcium 25.2 25.0 mg/L 101 90.0 - 110 115192511
Magnesium, Total 24.4 25.0 mg/L 97.6 90.0 - 110 115192511
Potassium 23.3 25.0 mg/L 93.2 90.0 - 110 115192511
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 20 of 38
1
2
3
4
5
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 6 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Iron 2.45 2.50 mg/L 98.0 90.0 - 110 115192511
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Calcium 600043 5.50 5.00 mg/L 110 85.0 - 115 115192516
Magnesium, Total 600043 5.48 5.00 mg/L 110 85.0 - 115 115192516
Potassium 600043 5.42 5.00 mg/L 108 85.0 - 115 115192516
Total Iron 600043 0.540 0.500 mg/L 108 85.0 - 115 115192516
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Calcium 600043 5.50 5.56 5.00 85.0 - 115 110 111 mg/L 1.08 25.0
Magnesium, Total 600043 5.48 5.52 5.00 85.0 - 115 110 110 mg/L 0.727 25.0
Potassium 600043 5.42 5.53 5.00 85.0 - 115 108 111 mg/L 2.01 25.0
Total Iron 600043 0.540 0.537 0.500 85.0 - 115 108 107 mg/L 0.557 25.0
LDR
FileOutLimits%Recover%UnitsKnownReadingParameter
Calcium 300 300 mg/L 100 90.0 - 110 115192513
Magnesium, Total 93.6 100 mg/L 93.6 90.0 - 110 115192508
Potassium 102 100 mg/L 102 90.0 - 110 115192508
Total Iron 9.61 10.0 mg/L 96.1 90.0 - 110 115192508
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Calcium 1369109 7.78 0 1.84 5.00 75.0 - 125 119 mg/L 25.0
Sodium 1369109 46.9 0 41.4 5.00 75.0 - 125 110 mg/L 25.0
Total Iron 1369109 0.573 0 0.0256 0.500 75.0 - 125 109 mg/L 25.0
Calcium 1369496 85.8 0 80.3 5.00 75.0 - 125 110 mg/L 25.0
Magnesium, Total 1369496 58.0 0 52.1 5.00 75.0 - 125 118 mg/L 25.0
Potassium 1369496 11.5 0 5.17 5.00 75.0 - 125 127 * mg/L 25.0
Total Iron 1369496 0.529 0 ND 0.500 75.0 - 125 106 mg/L 25.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Calcium 1369109 7.78 7.80 1.84 5.00 75.0 - 125 119 119 mg/L 0 25.0
Sodium 1369109 46.9 46.4 41.4 5.00 75.0 - 125 110 100 mg/L 9.52 25.0
Total Iron 1369109 0.573 0.585 0.0256 0.500 75.0 - 125 109 112 mg/L 2.71 25.0
Calcium 1369496 85.8 86.7 80.3 5.00 75.0 - 125 110 128 * mg/L 15.1 25.0
Magnesium, Total 1369496 58.0 58.4 52.1 5.00 75.0 - 125 118 126 * mg/L 6.56 25.0
Potassium 1369496 11.5 11.4 5.17 5.00 75.0 - 125 127 * 125 mg/L 1.59 25.0
Total Iron 1369496 0.529 0.531 ND 0.500 75.0 - 125 106 106 mg/L 0 25.0
SM 5310 C-96Drinking Water 600116
AWRL
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Organic Carbon 2.00 2.00 mg/L 100 75.0 - 125 115194303
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Total Organic Carbon 600116 0.0979 0.0618 0.500 mg/L 115194302
Total Organic Carbon 600116 0.0775 0.0618 0.500 mg/L 115194328
Total Organic Carbon 600116 0.0994 0.0618 0.500 mg/L 115194347
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 21 of 38
1
2
3
4
5
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 7 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Total Organic Carbon 600116 0.0882 0.0618 0.500 mg/L 115194353
CCB
FileOutUnitsMQLMDLReadingPrepSetParameter
Total Organic Carbon 600116 0.129 0.0618 0.500 mg/L 115194296
Total Organic Carbon 600116 0.115 0.0618 0.500 mg/L 115194307
Total Organic Carbon 600116 0.157 0.0618 0.500 mg/L 115194317
Total Organic Carbon 600116 0.119 0.0618 0.500 mg/L 115194326
Total Organic Carbon 600116 0.0823 0.0618 0.500 mg/L 115194340
Total Organic Carbon 600116 0.143 0.0618 0.500 mg/L 115194345
Total Organic Carbon 600116 0.216 0.0618 0.500 mg/L 115194351
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Organic Carbon 9.79 10.0 mg/L 97.9 90.0 - 110 115194299
Total Organic Carbon 9.72 10.0 mg/L 97.2 90.0 - 110 115194308
Total Organic Carbon 9.78 10.0 mg/L 97.8 90.0 - 110 115194318
Total Organic Carbon 9.87 10.0 mg/L 98.7 90.0 - 110 115194327
Total Organic Carbon 9.65 10.0 mg/L 96.5 90.0 - 110 115194341
Total Organic Carbon 9.99 10.0 mg/L 99.9 90.0 - 110 115194346
Total Organic Carbon 10.2 10.0 mg/L 102 90.0 - 110 115194352
ICL
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Organic Carbon 19.7 20.0 mg/L 98.5 90.0 - 110 115194298
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Organic Carbon 10.6 10.0 mg/L 106 90.0 - 110 115194300
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Total Organic Carbon 600116 5.23 5.00 mg/L 105 100 - 114 115194301
Total Organic Carbon 600116 5.22 5.00 mg/L 104 100 - 114 115194329
Total Organic Carbon 600116 5.16 5.00 mg/L 103 100 - 114 115194348
Total Organic Carbon 600116 5.09 5.00 mg/L 102 100 - 114 115194354
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Total Organic Carbon 1369430 10.0 0 0.783 10.0 93.0 - 113 92.2 * mg/L 20.0
Total Organic Carbon 1369505 17.9 0 7.33 10.0 93.0 - 113 106 mg/L 20.0
Total Organic Carbon 1369780 14.2 0 3.26 10.0 93.0 - 113 109 mg/L 20.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Total Organic Carbon 1369430 10.0 10.1 0.783 10.0 93.0 - 113 92.2 * 93.2 mg/L 1.08 20.0
Total Organic Carbon 1369505 17.9 17.8 7.33 10.0 93.0 - 113 106 105 mg/L 0.948 20.0
Total Organic Carbon 1369780 14.2 14.1 3.26 10.0 93.0 - 113 109 108 mg/L 0.922 20.0
Standard
FileOutLimits%Recover%UnitsKnownReadingSampleParameter
Total Organic Carbon 46.5 50.0 mg/L 93.0 90.0 - 110 115194297
EPA 200.7 4.4Drinking Water 600201
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 22 of 38
1
2
3
4
5
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 8 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Boron 599920 ND 0.00501 0.100 mg/L 115195940
Silicon Recoverable 599920 ND 0.0069 0.100 mg/L 115195940
Strontium 599920 ND 0.00532 0.050 mg/L 115195940
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Boron 5.33 5.00 mg/L 107 90.0 - 110 115195939
Boron 5.16 5.00 mg/L 103 90.0 - 110 115195947
Boron 5.07 5.00 mg/L 101 90.0 - 110 115195948
Silicon Recoverable 5.13 5.00 mg/L 103 90.0 - 110 115195939
Silicon Recoverable 4.95 5.00 mg/L 99.0 90.0 - 110 115195947
Silicon Recoverable 4.83 5.00 mg/L 96.6 90.0 - 110 115195948
Strontium 0.524 0.500 mg/L 105 90.0 - 110 115195939
Strontium 0.499 0.500 mg/L 99.8 90.0 - 110 115195947
Strontium 0.485 0.500 mg/L 97.0 90.0 - 110 115195948
ICL
FileOutLimits%Recover%UnitsKnownReadingParameter
Boron 10.3 10.0 mg/L 103 95.0 - 105 115195933
Silicon Recoverable 10.2 10.0 mg/L 102 95.0 - 105 115195933
Strontium 1.02 1.00 mg/L 102 95.0 - 105 115195933
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Boron 5.31 5.00 mg/L 106 90.0 - 110 115195934
Silicon Recoverable 5.09 5.00 mg/L 102 90.0 - 110 115195934
Strontium 0.512 0.500 mg/L 102 90.0 - 110 115195934
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Boron 599920 1.05 1.00 mg/L 105 85.0 - 115 115195941
Silicon Recoverable 599920 3.66 4.00 mg/L 91.4 85.0 - 115 115195941
Strontium 599920 0.532 0.500 mg/L 106 85.0 - 115 115195941
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Boron 599920 1.05 1.05 1.00 85.0 - 115 105 105 mg/L 0 25.0
Silicon Recoverable 599920 3.66 3.68 4.00 85.0 - 115 91.4 91.9 mg/L 0.545 25.0
Strontium 599920 0.532 0.547 0.500 85.0 - 115 106 109 mg/L 2.78 25.0
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Boron 1369496 1.48 0 0.437 1.00 75.0 - 125 104 mg/L 25.0
Silicon Recoverable 1369496 15.0 0 11.1 4.00 75.0 - 125 97.5 mg/L 25.0
Strontium 1369496 1.78 0 1.19 0.500 75.0 - 125 118 mg/L 25.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Boron 1369496 1.48 1.50 0.437 1.00 75.0 - 125 104 106 mg/L 1.90 25.0
Silicon Recoverable 1369496 15.0 15.0 11.1 4.00 75.0 - 125 97.5 97.5 mg/L 0 25.0
Strontium 1369496 1.78 1.79 1.19 0.500 75.0 - 125 118 120 mg/L 1.68 25.0
EPA 200.7 4.4Drinking Water 600250
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 23 of 38
1
2
3
4
5
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 9 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Calcium 599920 ND 0.0419 0.500 mg/L 115197394
Magnesium, Total 599920 ND 0.0102 0.500 mg/L 115197394
Sodium 599920 ND 0.0315 0.500 mg/L 115197394
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Calcium 25.6 25.0 mg/L 102 90.0 - 110 115197392
Calcium 25.7 25.0 mg/L 103 90.0 - 110 115197403
Calcium 25.8 25.0 mg/L 103 90.0 - 110 115197411
Magnesium, Total 25.8 25.0 mg/L 103 90.0 - 110 115197392
Magnesium, Total 25.9 25.0 mg/L 104 90.0 - 110 115197403
Sodium 25.1 25.0 mg/L 100 90.0 - 110 115197392
Sodium 25.4 25.0 mg/L 102 90.0 - 110 115197403
Sodium 25.4 25.0 mg/L 102 90.0 - 110 115197411
Sodium 25.3 25.0 mg/L 101 90.0 - 110 115197418
ICL
FileOutLimits%Recover%UnitsKnownReadingParameter
Calcium 50.4 50.0 mg/L 101 95.0 - 105 115197387
Magnesium, Total 50.8 50.0 mg/L 102 95.0 - 105 115197387
Sodium 50.7 50.0 mg/L 101 95.0 - 105 115197387
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Calcium 25.8 25.0 mg/L 103 90.0 - 110 115197391
Magnesium, Total 25.6 25.0 mg/L 102 90.0 - 110 115197391
Sodium 25.0 25.0 mg/L 100 90.0 - 110 115197391
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Calcium 599920 5.44 5.00 mg/L 109 85.0 - 115 115197395
Magnesium, Total 599920 5.42 5.00 mg/L 108 85.0 - 115 115197395
Sodium 599920 5.21 5.00 mg/L 104 85.0 - 115 115197395
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Calcium 599920 5.44 5.43 5.00 85.0 - 115 109 109 mg/L 0.184 25.0
Magnesium, Total 599920 5.42 5.42 5.00 85.0 - 115 108 108 mg/L 0 25.0
Sodium 599920 5.21 5.23 5.00 85.0 - 115 104 105 mg/L 0.383 25.0
LDR
FileOutLimits%Recover%UnitsKnownReadingParameter
Calcium 102 100 mg/L 102 90.0 - 110 115197388
Magnesium, Total 99.1 100 mg/L 99.1 90.0 - 110 115197388
Sodium 195 200 mg/L 97.5 90.0 - 110 115197393
Total Iron 10.2 10.0 mg/L 102 90.0 - 110 115197388
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Calcium 1369496 85.9 0 80.3 5.00 75.0 - 125 112 mg/L 25.0
Magnesium, Total 1369496 58.3 0 51.9 5.00 75.0 - 125 128 * mg/L 25.0
Sodium 1369496 175 0 169 5.00 75.0 - 125 120 mg/L 25.0
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 24 of 38
1
2
3
4
5
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 10 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Calcium 1369496 85.9 85.0 80.3 5.00 75.0 - 125 112 94.0 mg/L 17.5 25.0
Magnesium, Total 1369496 58.3 57.1 51.9 5.00 75.0 - 125 128 * 104 mg/L 20.7 25.0
Sodium 1369496 175 173 169 5.00 75.0 - 125 120 80.0 mg/L 40.0 * 25.0
EPA 200.8 5.4Drinking Water 600280
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Aluminum, Total 600280 ND 0.00199 0.005 mg/L 115198445
Arsenic, Total 600280 ND 0.000193 0.0005 mg/L 115198445
Barium 600280 0.000909 0.000574 0.005 mg/L 115198445
Cadmium, Total 600280 ND 0.000209 0.0005 mg/L 115198445
Chromium, Total 600280 ND 0.000282 0.0005 mg/L 115198445
Copper, Total 600280 ND 0.000425 0.001 mg/L 115198445
Lead, Total 600280 ND 0.000227 0.0005 mg/L 115198445
Manganese, Total 600280 ND 0.00033 0.001 mg/L 115198445
Selenium, Total 600280 ND 0.000728 0.001 mg/L 115198445
Silver, Total 600280 ND 0.00006280.0002 mg/L 115198445
Zinc, Total 600280 ND 0.00123 0.005 mg/L 115198445
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Aluminum, Total 0.0492 0.05 mg/L 98.4 90.0 - 110 115198444
Aluminum, Total 0.0476 0.05 mg/L 95.2 90.0 - 110 115198453
Aluminum, Total 0.0502 0.05 mg/L 100 90.0 - 110 115198464
Aluminum, Total 0.0495 0.05 mg/L 99.0 90.0 - 110 115198473
Aluminum, Total 0.0502 0.05 mg/L 100 90.0 - 110 115198480
Aluminum, Total 0.0488 0.05 mg/L 97.6 90.0 - 110 115198491
Aluminum, Total 0.0515 0.05 mg/L 103 90.0 - 110 115198501
Arsenic, Total 0.0526 0.05 mg/L 105 90.0 - 110 115198444
Arsenic, Total 0.0499 0.05 mg/L 99.8 90.0 - 110 115198453
Arsenic, Total 0.0518 0.05 mg/L 104 90.0 - 110 115198464
Arsenic, Total 0.0517 0.05 mg/L 103 90.0 - 110 115198473
Arsenic, Total 0.0521 0.05 mg/L 104 90.0 - 110 115198480
Arsenic, Total 0.0513 0.05 mg/L 103 90.0 - 110 115198491
Arsenic, Total 0.0521 0.05 mg/L 104 90.0 - 110 115198501
Barium 0.0502 0.05 mg/L 100 90.0 - 110 115198444
Barium 0.0499 0.05 mg/L 99.8 90.0 - 110 115198453
Barium 0.0508 0.05 mg/L 102 90.0 - 110 115198464
Barium 0.0502 0.05 mg/L 100 90.0 - 110 115198473
Barium 0.0508 0.05 mg/L 102 90.0 - 110 115198480
Barium 0.0512 0.05 mg/L 102 90.0 - 110 115198491
Barium 0.0516 0.05 mg/L 103 90.0 - 110 115198501
Cadmium, Total 0.0497 0.05 mg/L 99.4 90.0 - 110 115198444
Cadmium, Total 0.0493 0.05 mg/L 98.6 90.0 - 110 115198453
Cadmium, Total 0.0503 0.05 mg/L 101 90.0 - 110 115198464
Cadmium, Total 0.050 0.05 mg/L 100 90.0 - 110 115198473
Cadmium, Total 0.0498 0.05 mg/L 99.6 90.0 - 110 115198480
Cadmium, Total 0.0502 0.05 mg/L 100 90.0 - 110 115198491
Cadmium, Total 0.0498 0.05 mg/L 99.6 90.0 - 110 115198501
Chromium, Total 0.053 0.05 mg/L 106 90.0 - 110 115198444
Chromium, Total 0.0525 0.05 mg/L 105 90.0 - 110 115198453
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 25 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 11 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Chromium, Total 0.052 0.05 mg/L 104 90.0 - 110 115198464
Chromium, Total 0.0533 0.05 mg/L 107 90.0 - 110 115198473
Chromium, Total 0.053 0.05 mg/L 106 90.0 - 110 115198480
Chromium, Total 0.0526 0.05 mg/L 105 90.0 - 110 115198491
Chromium, Total 0.0523 0.05 mg/L 105 90.0 - 110 115198501
Copper, Total 0.0522 0.05 mg/L 104 90.0 - 110 115198444
Copper, Total 0.0507 0.05 mg/L 101 90.0 - 110 115198453
Copper, Total 0.0525 0.05 mg/L 105 90.0 - 110 115198464
Copper, Total 0.0523 0.05 mg/L 105 90.0 - 110 115198473
Copper, Total 0.0532 0.05 mg/L 106 90.0 - 110 115198480
Copper, Total 0.0518 0.05 mg/L 104 90.0 - 110 115198491
Copper, Total 0.054 0.05 mg/L 108 90.0 - 110 115198501
Lead, Total 0.0492 0.05 mg/L 98.4 90.0 - 110 115198444
Lead, Total 0.050 0.05 mg/L 100 90.0 - 110 115198453
Lead, Total 0.0492 0.05 mg/L 98.4 90.0 - 110 115198464
Lead, Total 0.0494 0.05 mg/L 98.8 90.0 - 110 115198473
Lead, Total 0.0489 0.05 mg/L 97.8 90.0 - 110 115198480
Lead, Total 0.0492 0.05 mg/L 98.4 90.0 - 110 115198491
Lead, Total 0.0489 0.05 mg/L 97.8 90.0 - 110 115198501
Manganese, Total 0.0505 0.05 mg/L 101 90.0 - 110 115198444
Manganese, Total 0.0504 0.05 mg/L 101 90.0 - 110 115198453
Manganese, Total 0.0505 0.05 mg/L 101 90.0 - 110 115198464
Manganese, Total 0.051 0.05 mg/L 102 90.0 - 110 115198473
Manganese, Total 0.0506 0.05 mg/L 101 90.0 - 110 115198480
Manganese, Total 0.0503 0.05 mg/L 101 90.0 - 110 115198491
Manganese, Total 0.0498 0.05 mg/L 99.6 90.0 - 110 115198501
Selenium, Total 0.0534 0.05 mg/L 107 90.0 - 110 115198444
Selenium, Total 0.049 0.05 mg/L 98.0 90.0 - 110 115198453
Selenium, Total 0.0506 0.05 mg/L 101 90.0 - 110 115198464
Selenium, Total 0.0512 0.05 mg/L 102 90.0 - 110 115198473
Selenium, Total 0.0515 0.05 mg/L 103 90.0 - 110 115198480
Selenium, Total 0.0495 0.05 mg/L 99.0 90.0 - 110 115198491
Selenium, Total 0.0508 0.05 mg/L 102 90.0 - 110 115198501
Silver, Total 0.0508 0.05 mg/L 102 90.0 - 110 115198444
Silver, Total 0.0499 0.05 mg/L 99.8 90.0 - 110 115198453
Silver, Total 0.0506 0.05 mg/L 101 90.0 - 110 115198464
Silver, Total 0.051 0.05 mg/L 102 90.0 - 110 115198473
Silver, Total 0.0507 0.05 mg/L 101 90.0 - 110 115198480
Silver, Total 0.0509 0.05 mg/L 102 90.0 - 110 115198491
Silver, Total 0.0509 0.05 mg/L 102 90.0 - 110 115198501
Zinc, Total 0.0509 0.05 mg/L 102 90.0 - 110 115198444
Zinc, Total 0.0505 0.05 mg/L 101 90.0 - 110 115198453
Zinc, Total 0.052 0.05 mg/L 104 90.0 - 110 115198464
Zinc, Total 0.0529 0.05 mg/L 106 90.0 - 110 115198473
Zinc, Total 0.0514 0.05 mg/L 103 90.0 - 110 115198480
Zinc, Total 0.0508 0.05 mg/L 102 90.0 - 110 115198491
Zinc, Total 0.0522 0.05 mg/L 104 90.0 - 110 115198501
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Aluminum, Total 0.0463 0.05 mg/L 92.6 90.0 - 110 115198422
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 26 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 12 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Arsenic, Total 0.0513 0.05 mg/L 103 90.0 - 110 115198422
Barium 0.0512 0.05 mg/L 102 90.0 - 110 115198422
Cadmium, Total 0.0506 0.05 mg/L 101 90.0 - 110 115198422
Chromium, Total 0.0515 0.05 mg/L 103 90.0 - 110 115198422
Copper, Total 0.0516 0.05 mg/L 103 90.0 - 110 115198422
Lead, Total 0.0502 0.05 mg/L 100 90.0 - 110 115198422
Manganese, Total 0.0489 0.05 mg/L 97.8 90.0 - 110 115198422
Selenium, Total 0.0506 0.05 mg/L 101 90.0 - 110 115198422
Silver, Total 0.0503 0.05 mg/L 101 90.0 - 110 115198422
Zinc, Total 0.0519 0.05 mg/L 104 90.0 - 110 115198422
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Aluminum, Total 600280 0.565 0.500 mg/L 113 85.0 - 115 115198446
Arsenic, Total 600280 0.537 0.500 mg/L 107 85.0 - 115 115198446
Barium 600280 0.521 0.500 mg/L 104 85.0 - 115 115198446
Cadmium, Total 600280 0.264 0.250 mg/L 106 85.0 - 115 115198446
Chromium, Total 600280 0.539 0.500 mg/L 108 85.0 - 115 115198446
Copper, Total 600280 0.539 0.500 mg/L 108 85.0 - 115 115198446
Lead, Total 600280 0.534 0.500 mg/L 107 85.0 - 115 115198446
Manganese, Total 600280 0.527 0.500 mg/L 105 85.0 - 115 115198446
Selenium, Total 600280 0.527 0.500 mg/L 105 85.0 - 115 115198446
Silver, Total 600280 0.106 0.100 mg/L 106 85.0 - 115 115198446
Zinc, Total 600280 0.522 0.500 mg/L 104 85.0 - 115 115198446
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Aluminum, Total 600280 0.565 0.563 0.500 85.0 - 115 113 113 mg/L 0.355 20.0
Arsenic, Total 600280 0.537 0.530 0.500 85.0 - 115 107 106 mg/L 1.31 20.0
Barium 600280 0.521 0.515 0.500 85.0 - 115 104 103 mg/L 1.16 20.0
Cadmium, Total 600280 0.264 0.261 0.250 85.0 - 115 106 104 mg/L 1.14 20.0
Chromium, Total 600280 0.539 0.538 0.500 85.0 - 115 108 108 mg/L 0.186 20.0
Copper, Total 600280 0.539 0.534 0.500 85.0 - 115 108 107 mg/L 0.932 20.0
Lead, Total 600280 0.534 0.531 0.500 85.0 - 115 107 106 mg/L 0.563 20.0
Manganese, Total 600280 0.527 0.530 0.500 85.0 - 115 105 106 mg/L 0.568 20.0
Selenium, Total 600280 0.527 0.529 0.500 85.0 - 115 105 106 mg/L 0.379 20.0
Silver, Total 600280 0.106 0.104 0.100 85.0 - 115 106 104 mg/L 1.90 20.0
Zinc, Total 600280 0.522 0.515 0.500 85.0 - 115 104 103 mg/L 1.35 20.0
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Aluminum, Total 1369496 0.559 0 ND 0.500 70.0 - 130 112 mg/L 20.0
Arsenic, Total 1369496 0.539 0 0.00408 0.500 70.0 - 130 107 mg/L 20.0
Barium 1369496 0.583 0 0.070 0.500 70.0 - 130 103 mg/L 20.0
Cadmium, Total 1369496 0.255 0 ND 0.250 70.0 - 130 102 mg/L 20.0
Chromium, Total 1369496 0.522 0 0.000984 0.500 70.0 - 130 104 mg/L 20.0
Copper, Total 1369496 0.515 0 0.00428 0.500 70.0 - 130 102 mg/L 20.0
Lead, Total 1369496 0.508 0 ND 0.500 70.0 - 130 102 mg/L 20.0
Manganese, Total 1369496 0.507 0 ND 0.500 70.0 - 130 101 mg/L 20.0
Selenium, Total 1369496 0.522 0 0.0162 0.500 70.0 - 130 101 mg/L 20.0
Silver, Total 1369496 0.102 0 ND 0.100 70.0 - 130 102 mg/L 20.0
Zinc, Total 1369496 0.483 0 0.0078 0.500 70.0 - 130 95.0 mg/L 20.0
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 27 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 13 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Aluminum, Total 1369496 0.559 0.555 ND 0.500 70.0 - 130 112 111 mg/L 0.897 20.0
Arsenic, Total 1369496 0.539 0.531 0.00408 0.500 70.0 - 130 107 105 mg/L 1.89 20.0
Barium 1369496 0.583 0.579 0.070 0.500 70.0 - 130 103 102 mg/L 0.976 20.0
Cadmium, Total 1369496 0.255 0.254 ND 0.250 70.0 - 130 102 102 mg/L 0 20.0
Chromium, Total 1369496 0.522 0.517 0.000984 0.500 70.0 - 130 104 103 mg/L 0.966 20.0
Copper, Total 1369496 0.515 0.509 0.00428 0.500 70.0 - 130 102 101 mg/L 0.985 20.0
Lead, Total 1369496 0.508 0.504 ND 0.500 70.0 - 130 102 101 mg/L 0.985 20.0
Manganese, Total 1369496 0.507 0.502 ND 0.500 70.0 - 130 101 100 mg/L 0.995 20.0
Selenium, Total 1369496 0.522 0.517 0.0162 0.500 70.0 - 130 101 100 mg/L 0.995 20.0
Silver, Total 1369496 0.102 0.102 ND 0.100 70.0 - 130 102 102 mg/L 0 20.0
Zinc, Total 1369496 0.483 0.478 0.0078 0.500 70.0 - 130 95.0 94.0 mg/L 1.06 20.0
EPA 245.1 3Drinking Water 600450
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Mercury 599959 ND 0.072 0.100 ug/L 115202347
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Mercury 4.91 5.000 ug/L 98.2 90.0 - 110 115202346
Mercury 4.98 5.000 ug/L 99.6 90.0 - 110 115202350
Mercury 4.93 5.000 ug/L 98.6 90.0 - 110 115202361
ICL
FileOutLimits%Recover%UnitsKnownReadingParameter
Mercury 19.6 20.00 ug/L 98.0 90.0 - 110 115202327
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Mercury 5.11 5.000 ug/L 102 90.0 - 110 115202326
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Mercury 599959 5.18 5.00 ug/L 104 85.0 - 115 115202348
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Mercury 599959 5.18 5.06 5.00 85.0 - 115 104 101 ug/L 2.34 20.0
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Mercury 1368631 10.4 0 ND 10.0 70.0 - 130 104 ug/L 14.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Mercury 1368631 10.4 10.4 ND 10.0 70.0 - 130 104 104 ug/L 0 14.0
EPA 200.7 4.4Drinking Water 600855
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Dissolved Iron 2.49 2.50 mg/L 99.6 90.0 - 110 115210842
Dissolved Iron 2.48 2.50 mg/L 99.2 90.0 - 110 115210853
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 28 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 14 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
Dir. SPKD
Limit%RPDUnitsDSPKD%DSPK%Limits%KnownUNKDSPKDDSPKSampleParameter
Dissolved Iron 1369496 0.465 0.519 ND 0.500 75.0 - 125 93.0 104 mg/L 11.2 20.0
Direct SPK
UnitsDSPK%Limits%KnownUNKDSPKSampleParameter
Dissolved Iron 1369496 0.465 ND 0.500 75.0 - 125 93.0 mg/L 20.0
ICL
FileOutLimits%Recover%UnitsKnownReadingParameter
Dissolved Iron 5.13 5.00 mg/L 103 95.0 - 105 115210835
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Dissolved Iron 2.55 2.50 mg/L 102 90.0 - 110 115210839
LDR
FileOutLimits%Recover%UnitsKnownReadingParameter
Dissolved Iron 9.96 10.0 mg/L 99.6 90.0 - 110 115210836
SM 2130 B-94Drinking Water 599733
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Turbidity 599733 ND 1.00 1.00 NTU 115186285
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Turbidity 1369325 Duplicate ND ND NTU 20.0
Turbidity 1369497 Duplicate ND ND NTU 20.0
Mat. Spike
FileLimits %Recovery %UnitsKnownUnknownSpikeSampleParameter
Turbidity 1369325 41.9 ND 40.0 NTU 105 70.0 - 130 115186290
Turbidity 1369497 43.6 ND 40.0 NTU 109 70.0 - 130 115186303
Standard
FileOutLimits%Recover%UnitsKnownReadingSampleParameter
Turbidity 599733 9.96 10.0 NTU 99.6 90.0 - 110 115186286
Turbidity 599733 99.8 100 NTU 99.8 90.0 - 110 115186287
Turbidity 599733 9.97 10.0 NTU 99.7 90.0 - 110 115186300
Turbidity 599733 9.98 10.0 NTU 99.8 90.0 - 110 115186304
SM 2320 B-97Drinking Water 599795
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Total Alkalinity (as CaCO3) 599795 ND 1.00 1.00 mg/L 115186307
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Alkalinity (as CaCO3) 25.7 25.0 mg/L 103 90.0 - 110 115186306
Total Alkalinity (as CaCO3) 24.7 25.0 mg/L 98.8 90.0 - 110 115186320
Total Alkalinity (as CaCO3) 24.7 25.0 mg/L 98.8 90.0 - 110 115186333
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Total Alkalinity (as CaCO3) 1368654 Duplicate 49.8 51.3 mg/L 2.97 20.0
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 29 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 15 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Total Alkalinity (as CaCO3) 1369298 Duplicate 98.2 108 mg/L 9.51 20.0
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Alkalinity (as CaCO3) 24.7 25.0 mg/L 98.8 90.0 - 110 115186305
Mat. Spike
FileLimits %Recovery %UnitsKnownUnknownSpikeSampleParameter
Total Alkalinity (as CaCO3) 1368654 77.0 51.3 25.0 mg/L 103 70.0 - 130 115186310
Total Alkalinity (as CaCO3) 1369298 129 108 25.0 mg/L 84.0 70.0 - 130 115186323
SM 4500-H+ B-96Drinking Water 599923
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Laboratory pH 1369061 Duplicate 8.2 8.2 SU 0 20.0
Laboratory pH 1369494 Duplicate 7.9 7.9 SU 0 20.0
Standard
FileOutLimits%Recover%UnitsKnownReadingSampleParameter
Laboratory pH 599923 7.01 7.00 SU 100 90.0 - 110 115189526
Laboratory pH 599923 4.01 4.00 SU 100 90.0 - 110 115189527
Laboratory pH 599923 10.05 10.00 SU 100 90.0 - 110 115189528
Laboratory pH 599923 6.01 6.00 SU 100 90.0 - 110 115189529
Laboratory pH 599923 8.03 8.00 SU 100 90.0 - 110 115189530
Laboratory pH 599923 6.05 6.00 SU 101 90.0 - 110 115189542
Laboratory pH 599923 8.05 8.00 SU 101 90.0 - 110 115189543
Laboratory pH 599923 6.05 6.00 SU 101 90.0 - 110 115189555
Laboratory pH 599923 8.05 8.00 SU 101 90.0 - 110 115189556
SM 4500-S2¯ D-2000Drinking Water 600327
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Sulfide 600327 ND 0.0091 0.015 mg/L 115199183
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Sulfide 1369496 Duplicate ND ND mg/L 20.0
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Sulfide 600327 0.0768 0.075 mg/L 102 90.0 - 110 115199184
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Sulfide 600327 0.0768 0.0753 0.075 90.0 - 110 102 100 mg/L 1.97 10.0
SM 4500-P E-97Drinking Water 600851
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Total Phosphorus 600851 0.00336 0.00285 0.010 mg/L 115210730
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
Report Page 30 of 38
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 16 of 1602/18/2015Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Phosphorus 0.316 0.300 mg/L 105 90.0 - 110 115210731
Total Phosphorus 0.312 0.300 mg/L 104 90.0 - 110 115210746
Total Phosphorus 0.317 0.300 mg/L 106 90.0 - 110 115210759
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Total Phosphorus 600851 0.296 0.300 mg/L 98.8 80.0 - 120 115210732
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Total Phosphorus 600851 0.296 0.287 0.300 80.0 - 120 98.8 95.5 mg/L 3.09 20.0
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Total Phosphorus 1369496 0.430 0 0.109 0.300 70.0 - 130 107 mg/L 20.0
Total Phosphorus 1369592 0.401 0 0.0829 0.300 70.0 - 130 106 mg/L 20.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Total Phosphorus 1369496 0.430 0.410 0.109 0.300 70.0 - 130 107 100 mg/L 6.76 20.0
Total Phosphorus 1369592 0.401 0.381 0.0829 0.300 70.0 - 130 106 99.4 mg/L 6.43 20.0
RPD is Relative Percent Difference: abs(r1-r2) / mean(r1,r2) * 100% Recover% is Recovery Percent: result / known * 100%
Blank - Method Blank; CCV - Continuing Calibration Verification; ICV - Initial Calibration Verification; LCS - Laboratory Control Sample; MS - Matrix
Spike; LDR - Linear Dynamic Range Standard; CCB - Continuing Calibration Blank; AWRL - Ambient Water Reporting Limit
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com
North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633
NELAP-accredited #T104704201
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