FEDERAL OH-SCENE COORDINATOR'S REPORT

FOR

PAGAN ROAD DRUM SITE

Snanit Township, Erie County, Pennsylvania

CERCLA REMOVAL ACTIONJune 9, 1986 through September 2, 1987

REGION III

EMERGENCYRESPONSETEAM

DOTTED STATESENVIRONMENTAL PROTECTION AGENCY

fiRIGGuol:-

Pagan Road Drum SiteFederal OSC Report

TABLE OF CONTENTS

Facts Sheet

Foreword

I. IntroductionA. Nature of the Site/Initial SituationB. Location of the SiteC. Efforts to Obtain Cleanup by Potential Responsible Parties

II. Roster of Agencies, Organizations and IndividualsA. Organization of the ResponseB. Glossary of Abbreviations

III. Narrative of Events

IV. Resources CommittedA. Initial Funding RequestB. Funding IncreasesC. Estimated Total Cost Summary

V. Effectiveness of the RemovalA. Activities of the Various Agencies

1. Potential Responsible Parties2. State/Local Agencies3. Federal Agencies and Special Forces4. Contractors

B. Analytical SynopsisC. Disposal Methods and Quantities Removed

VI. Chronology of Events

VII. Problems Encountered and Recommendations

VIII. Legal Aspects

IX. AppendicesA. Location Map/Site SketchesB. Funding DocumentationC. Site Safety ProtocolD. CorrespondenceE. Background InformationF. Photographic DocumentationG. POLREPffH. Delivery OrderI. ManifestsJ. Incoming Spill Report A p i n TI <;H 11 i L -j - 0

FACTS SHEET

PROJECT 1132REGION IIICERCLA EMERGENCY RESPONSE/IMMEDIATE REMOVAL ACTION PACTS SHEET ~"

—————————SITE: Pagan Road Drum Site

SIZE: Approximately 1 acr*

LOCATION: Summit Township, Erie County, PA

APPROVAL DATE: June 9, 1986

PROJECT DATES: June 9, 1986 through September 2, 1987

DESCRIPTION: Approximately 250 drums of various solvents andchemical wastes were discovered inside an abandonedtrailer during a site assessment on the Marlin Coonproperty on Pagan Road in Summit Township, PA. TheOSC, under $50,000 Delegation of Authority 14-1-A(5/1/85), utilized the emergency funds to restrict siteaccess and begin drum sampling. Additional funding wasobtained to remove drums from the trailer, overpack andstage them on site, conduct complete drum sampling andinventory, and final transportation and disposal atapproved facilities.

HAZARDOUS MATERIAL: Benzene, ethylbenzene, methylene chloride, toluene,carbon tetrachloride, chlorobenzene, trichloroethylene,naphthalene

QUANTITIES REMOVED: 243 55-galIon drums and 50 containers of 1-pint to5-gallon were bulked into 85 drums of product and onerolloff box for final disposal.

OSC: - David P. Wright

REMOVAL CONTRACTOR: O.H. Materials, Inc., Findlay, Ohio

DISPOSAL LOCATIONS! SCA Chemical Services, Chicago, IL (ILD000672121)Chemical Waste Management, Emelle, AL (ALD000622464)

PROJECT CEILING: $410,000

PROJECT COSTS $197,300

COMMENTSI After many delays Including improper drum inventory, aft subsequent additional funding request as necessary inorder to effect final disposal of wastes*

Ttovld P. Wright, OSC

flRioooe?

FOREWORD

AHI00068

Pagan Road Drum SiteFederal OSC Report

FOREWORD

This report is submitted in accordance with procedures outlined in the NationalOil and Hazardous Substance Pollution Contingency Plan (NCP). The primaryobjective of the Plan is to provide a coordinated Federal response capabilityat the scene of an unplanned or sudden discharge of oil or hazardous substancesthat poses a threat to the public health or the evironment. In addition, toprovisions of the Comprehensive Environmental Response, Compensation andLiability Act (CERCLA) promote a coordinated Federal, State and local responseto mitigate situations at hazardous waste sites which pose an imminent hazardto public health, providing a legal basis for Federal response activities. Theprovisions of the National Contincency Plan were implemented by theEnvironmental Protection Agency, Region III, Philadelphia, Pennsylvania.

Special thanks are extended to the many agencies and groups who participated inthis Federal Removal Activity. This well-coordinated team effort on sceneenabled a timely and efficient cleanup which prevented a major environmentalincident due to the chemical hazards present on site.

David P. WrightOn-Scene CoordinatorU.S. EPA Region IIIPhiladelphia, Pennsylvania

SECTION I

INTRODUCTION

A R I O J 0 7 G

Pagan Road Drum SiteFederal OSC Report

I. INTRODUCTION

A. Initial Situation and Nature of the IncidentOn October 4 and 16, 1984, Pennsylvania Department of Environmental Resources(PADER) representatives notified EPA Region III of spillage of hazardoussubstances resulting from a responsible party cleanup of drums on the Coonproperty in Summit Township, Pennsylvania. EPA responded with a siteassessment on October 22, 1984, at which time evidence of drum burning wasfound on the property, although an imminent threat was not presented by thesecircumstances.

On June 19, 1985, EPA performed another site assessment, at the request ofPADER, and found that a threat of fire and/or explosion existed based on airmonitoring results obtained. The monitoring was done near drums discoveredin the woods located beyond the area of the first assessment. Enforcementactions by the State to effect a cleanup continued.

On June 9, 1986, EPA reviewed PRP cleanup actions taken to date and found a42-foot trailer on the property containing approximately 200 waste drumsranging In size from 5 to 55 gallons, with another 50 drums scattered aroundthe property. The OSC activated the $50,000 Delegation of Authority, 14-1-A,(5/1/85) on June 9, 1986 to provide emergency site security and overpackingof leaking drums* A threat to human health and the environment was presentedby the danger of fire and/or explosion from leaking drum emissions inside thetrailer. There was Also waste leaking from drums onto the ground surface.Wastes present on site Included methylethylketone (MER), methylene chloride,trichlorqethylene (TCE), and various other flammable liquids and solids.

Removal actions commenced on June 9, 1986 and continued until final disposalon September 2, 1987*

B. Site LocationThe Pagan Road Drum Site was located on the Marlin Coon property, Pagan Road,Summit Township, Erie County, Pennsylvania. The site, consisting of approxi-mately two, -acres, was situated in a rural/residential area with anestimated21 residences within a l/4-mil« radius of the site.

ARI0007f

Pagan Road Drum SiteFederal OSC ReportINTRODUCTION (continued)

C. Efforts to Obtain Cleanup by Potential Responsible PartiesOwnership of the chemical materials (wastes and products) on site and, there-fore site waste removal and remedial work, were being held up by litigationinvolved in the bankruptcy of Tri-State Insulation, the previous occupant ofthe site and probable generator of the wastes on site. Mr. Marlin Coon wasthe owner of the property as well as the president of both Tri-StateInsulation and Coon Refrigeration. Coon Refrigeration was the firm occupyingthe business at the site during this removal action. Mr. Coon hadimplemented some initial consolidation of drummed materials; however, thiswork had been stopped pending resolution of the bankruptcy proceedings.

A Notice of Violation from the PADER Bureau of Solid Waste Management (seeAppendix H) was sent to Mr. Vedder J. White, trustee of Tri-State Insulation,Inc.; Marlin K. Coon, President of Tri-State Insulation, Inc. and CoonRefrigeration; and Mr. Thomas V. Purvis, Vice President of Tri-StateInsulation, Inc. on September 24, 1984. They were given explicit timeperiods and direction as to the cleanup and disposal of the toxic waste.

After an inspection of the site by the PADER Bureau of Solid Waste Managementon October 4 and 16, 1984, a follow-up letter was sent to the potentialresponsible parties listed above regarding their negligence toward conductingcleanup activities. They were advised not to continue cleanup activities atthat time as they could further compound cleanup problems and increase costsof cleaning up the site.

A R I C 3 Q 7 2

SECTION II

ROSTER OF AGENCIES, ORGANIZATIONS AND INDIVIDUALS

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R R I C J 0 7 G

Pagan Road Drum SiteFederal OSC ReportROSTER OF AGENCIES, ORGANIZATIONS AND INDIVIDUALS (continued)

B. Glossary of Abbreviations

ATSDR Acute Toxic Substance and Disease Registry (formerly CDC)

CDC Centers for Disease Control

EPA U.S. Environmental Protection Agency

ERCS/OHM Emergency Response Contract Services/0.H. Materials, Inc.

Erie Erie County Department of Health

OPA U.S. EPA Region III, Office of Public Affairs

OSC U.S. EPA Region III, Federal On-Scene Coordinator

PADER Pennsylvania Department of Environmental Resources

PADOH Pennsylvania Department of Health

TAT Technical Assistance Team (Roy F. WESTON, Inc.)

A R I G 3 0 7 7

SECTION III

NARRATIVE OF EVENTS

A R ! n r* n iH 11 I _ *j l

Pagan Road Drum SiteFederal OSC Report

III. NARRATIVE OF EVENTS

The Coon Refrigeration Site, later named the Pagan Road Drum Site, was locatedon the Marlin Coon property in Erie County, Pennsylvania. This was a wooded/residential area with a number of residences within 1/4 mile of the property.

OSC Jack Downie and TATMs Mark Selman and Bill Follett met with PADER SolidWaste Specialist, Mark German, at PADER, Meadville Regional Office on June 18,1985. Mr. German informed them that until filing for bankruptcy on November15, 1983, Tri-State Insulation operated an insulation and coating business atthe site and was the probable generator of the accumulated wastes. Mr. MarlinCoon, owner of the property and President of both Tri-State Insulation and CoonRefrigeration and, was operating Coon Refrigeration on the site at that time.

On June 19, 1985, the OSC, TATMs and Mr. Gorman performed a site assessment.They met with Mr. Coon who explained that the materials located on the siteincluded solvent-thinned asphalt roof coatings, resin side of urethane foam,silicon coatings, and the solvents used for equipment cleanup. Mr. Coon statedthat he had initiated the bulking of some materials by consolidating 5-galloncans of material into 55-gallon drums, but ceased these efforts pending theoutcome of the bankruptcy hearings.

During a tour of the site with Mr. Coon, the assessment team observed approxi-mately 170 drums and 5-gallon cans in the rear of the Coon Refrigerationbuilding. About 120 of these drums were stacked three drums high in rows of 40drums against the wall of the building. At least 20 55-gallon drums wereobserved lying on their side, with some of them leaking at the rear of thestacked drums. These drums were located within ten yards of the drinking waterwell that supplied the property and within 50 yards of a large pond. A totalof seven samples was collected and arrangements were made with Weston Labs foranalysis for priority pollutants, RCRA ignitability and RCRA reactivity.

On June 9, 1986, a 42-foot trailer was found on the property containing approx-imately 200 waste drums. OSC Wright activated $50,000 in emergency fundingunder the Delegation of Authority 14-1-A (5/1/85) for stabilization andsampling of the drums. Analytical data revealed the following, hazardous, _

L-i r i I i " - ; /substances in the drums and on the ground: - « _- ^

Pagan Road Drum SiteFederal OSC ReportNARRATIVE OF EVENTS (continued)

Benzene Ethylbenzene Methylene ChlorideToluene Carbon Tetrachloride ChlorobenzeneTrichloroethylene Naphthalene

On June 10, 1986, ERCS mobilized to the site to begin drum inventory, stagingand sampling. The trailer was emptied by a 215 backhoe with grappler whichexperienced difficulty due to the stacking of drums two and three high, as wellas muddy conditions at the site.

All of the drums were unloaded, secured, overpacked as needed, and covered withvisqueen as of June 14, 1986. Delays were incurred due to compliance issuesand inaccurate drum inventory conducted by ERCS resulting in an additionalfunding request as a result of higher disposal costs. On January 23, 1987, aceiling increase was approved to cover these additional costs. As March 1987approached, the drums were still on site awaiting disposal. Finally, theseproblems were cleared and as of September 2, 1987, all final disposaloperations were completed. A total of 85 product drums had been transported toThermalKEM Disposal Facility, Rock Hill, South Carolina for incineration. Onerolloff box of crushed drums and site-generated trash was transported toChemical Waste Management, Emelle, Alabama. On September 3, 1987, the OSCreceived disposal notification of acknowledgement for wastes transported toboth facilities.

n i --, - p n .-R 1 - - L O L

SECTION IV

RESOURCES COMMITTED

nD l n " " 3Hit I W - w J

Pagan Road Drum SiteFederal OSC Report

IV. RESOURCES COMMITTED

A. Initial FundingSince improper actions had been taken by the potential responsible party (Mr.Marlin Coon) to clean up the site, the OSC decided to initiate a Removal Actionby utilizing $50,000 Delegation of Authority 14-1-A (5/1/85) emergency fundingon June 9, 1986. A copy of Special Bulletin A documenting the use of theDelegation of Authority is included in Appendix B of this report.

B. Funding IncreasesOn June 13, 1987 the Regional Administrator, James M. Seif, approved anAdditional Funding Request of $150,000 thereby increasing the total projectceiling to $200,000.

Additional funding was reguired to address the task of expanding the stagingarea, further emptying the trailer, sampling and disposal. Resources wererequired beyond the $50,000 emergency funding for the following reasons:

1) Disposal costs were not addressed in the original funding,

2) an increased scope of work due to the need for an additional stagingarea which involved the clearing of woods,

3) slow progress following EPA takeover due to ongoing businessoperations of the property owner.

A second funding increase was approved by the Regional Administrator on January23, 1987 for an additional $210,000 necessary to complete final disposal ofwastes on site. The new project ceiling was $410,000.

Copies of these Additional Funding Requests are included in Appendix B of thisreport.

n RH II

Pagan Road Drum SiteFederal OSC ReportRESOURCES COMMITTED (continued)

C. Estimated Total Cost SummaryThe following is a breakdown of estimated costs for the Pagan Road Drum SiteRemoval Project. The estimated total cost of the project at its closure onSeptember 2, 1987 was $197,300.

Further cost information can be found in Appendices N and 0, Contractor Dailiesand Contractor Invoices.

1. EXTRAMURAL

A. ERCS prime removal contractor (O.K. Materials) $178,200

B. TAT 12,800

EXTRAMURAL Subtotal $191,000

2. INTRAMURAL

EPA $ 6,300

TOTAL ESTIMATED TOTAL PROJECT COSTS $197,300

PROJECT CEILING: $410,000

% of ceiling utilized - 48%

SECTION V

EFFECTIVENESS OF THE REMOVAL

Pagan Road Drum SiteFederal OSC Report

V. EFFECTIVENESS OF THE REMOVAL

A. Activities of Various Agencies

1. Potential Responsible PartiesAt the time of the EPA takeover on June 9, 1986, the property owner, Mr. MarlinK. Coon, had ceased in an attempt to consolidate materials on the site into 55-gallon drums and store them in a box trailer on his property. The drums hadbeen stacked two and three high in the trailer and there were still many drumsscattered on the ground. Some had fallen over and were leaking. Mr. Coonceased in his efforts upon his declaration of bankruptcy on November 15, 1983.

The effectiveness of the removal was hindered by Mr. Coon and Mr. White(Trustee of Tri-State Insulation) who were trying to determine the owner of thewastes and products on site. There was also a slight hinderance from CoonRefrigeration, which was an operating facility having trucks making deliverieswhile EPA had heavy equipment at work on the property.

2. State and Local ForcesThe Pennsylvania Department of Environmental Resources (PADER) Meadville Officenotified EPA of the community threat presented at this site and assisted in thepreliminary assessments.

An Environmental Health Specialist from the Pennsylvania Department of Healthadvised the EPA as to the hazards present and helped coordinate State andFederal efforts.

An Environmental Protection Specialist from the Erie County Department ofHealth investigated the site and provided assistance to the OSC.

3. Federal Agencies and Special ForcesDavid P. Wright served as the On-Scene Coordinator for the duration of thisremoval project. The OSC was responsible for the overall success of thecleanup including contractor task direction and coordination of all technicalaspects of mitigating the threat to human health and the environment.

Pagan Road Drum SiteFederal OSC ReportEFFECTIVENESS OF THE REMOVAL (continued)

A. Activities of Various Agencies (continued)

3. Federal Agencies and Special ForcesEPA's Office of Public Affairs addressed any inquiries from concerned residentsor the property owner.

EPA's Office of Regional Counsel and Enforcement Office assisted with sitestatus and the initiation of activities under the $50,000 Delegation ofAuthority.

The EPA Environmental Response Team (ERT) assisted in the preliminary siteassessment.

4. ContractorsThe Spill Prevention and Emergency Response Division (SPER) of Roy F. WESTON,Inc. provided personnel from the Technical Assistance Team (TAT) to providesupport to the OSC in the areas of water sampling, photographic documentationof site activities, contractor monitoring, site activities documentation,coordination of laboratories and review of analyses for QA/QC.

O.H. Materials, Inc. of Findlay, Ohio served as the ERCS prime removalcontractor responsible for the actual cleanup of the site and providing thenecessary materials, equipment and personnel. OHM coordinated drum analyses,transportation and disposal by subcontractors, trucking firms and disposalfacilities in addition to providing necessary field operations logistics.

B. Analytical SynopsisDrum samples were analyzed at Weston Labs for GC Pesticides by EPA Method 608;GC/MS Fraction, Volatile Compounds by EPA Method 624; GC/MS Fraction, BaseNeutral Compounds by EPA Method 625; and GC/MS Fraction, Acid Compounds by EPAMethod 625. Analysis revealed the presence of hazardous substances includingbenzene, ethylbenzene, methylene chloride, toluene, carbon tetrachloride,chlorobenzene, trichloroethylene and naphthalene.

Due to the volume of analytical data generated at this site, in the interest ofpresenting an informative and succinct OSC report, hard copies of theanalytical results have not been added to this report. However, the hardcopies are maintained in the site file at the office of the U.S^EPA, Regio^III, Philadelphia, Pennsylvania, and are available upon request!' I «- s. c u 0

Pagan Road Drum SiteFederal OSC ReportEFFECTIVENESS OF THE REMOVAL (continued)

C. Disposal Methods and Quantities RemovedA total of 243 drums and 50 small containers (1-pint to 5-gallon) wereidentified, bulked into 85 product drums, and disposed of from the site in thefollowing waste streams:

1) Flammable organic liquids 66 drums2) Non-flammable organic liquids 66 drums3) Non-flammable solids 21 drums4) Flammable solids (composite of tar drums) 22 drums5) Non-flammable inorganic liquids 37 drums

212 drums

SECTION VI

CHRONOLOGY OF EVENTS

p ih i

, .h i , . J 0 0

Pagan Road Drum DumpFederal OSC Report

VI. CHRONOLOGY OF EVENTS

This section presents with a brief summary of the major events as they occurredat the Pagan Road Drum Site. A more detailed description can be found inAppendix K (POLREPs), as well as other sections, of this report.

10/16/84 The site was reported to ERS by PADER.

10/22/84 First site assessment performed by EPA.

06/19/85 Second site assessment performed by EPA at the request of PADER.

06/09/86 OSC Wright activated $50,000 Delegation of Authority 14-1-A (5/1/85)emergency funding for stabilization and sampling of drums. A 42-foottrailer was found on the property containing approximately 200 wastedrums ranging in size from 5 to 55 gallons, with another 50 drumsscattered throughout the property.

National Geographic film crew on scene filming EPA Emergency Responsepersonnel during their assessment procedures.

06/10/86 OSC, TAT and ERCS evaluated removal options for site. OSC Wrightsubmitted Special Bulletin A to Regional Office describing activationof emergency funding the previous day.

06/11/86 Mobilization of 215 backhoe with grappler on site. ERCS inventoriedcontents of trailer. Water samples from four residences near sitewere taken. Additional funding request was submitted to EPA RegionalOffice.

06/12/86 ERCS used 215 with grappler to stage drums. The majority of drumsrequired overpacking. Trailer contained drums stacked two and threehigh.

06/14/86 No volatile organics found in water samples. Funding request wasapproved for $150,000; ceiling to $200,000. Trailer unloaded of alldrums which were secured, overpacked as necessary, and covered withvisqueen.

Pagan Road Drum DumpFederal OSC ReportCHRONOLOGY OF EVENTS (continued)

08/21/86 OSC Wright contacted ERCS Program Office and response manager concern-ing analytical delays and WPR preparation several times over the lasttwo months.

09/10/86 TAT performed an inspection of the site on 9/10/86 and discovered atree on the fence as well as visqueen off several drums. TAT receivedno HNU readings above background.

09/17/86 OSC and TAT inspected the site and found what appeared to be bulletholes in the overpacks. Mr. Coon removed the empty trailer from thesite. The protective fence was cut and pushed aside from the stagingarea. OSC and TAT repaired the fence.

09/26/86 OSC spoke with Bill Buchan of OHM this date to discuss the WPRs thatwere signed and forwarded to OHM.

01/10/87 Drums remained on site awaiting disposal. OSC Wright felt that themain reason for this was compliance issues, extremely slow approvalprocess specifically for CERCLA wastes and added bureaucracy at theState level.

01/23/87 A Funding Increase of $210,000 was approved bringing the projectceiling to $410,000 to cover increased disposal costs due to delays ineffecting final disposal.

03/06/87 Drums still on site awaiting disposal. Total estimated disposal andtransport cost - $140,000.

03/10/87 OSC Province, TATM Donegan and ERCS representative Ken Kuhn receivedsite logistics and equipment needs for drum segragation and removalactivities scheduled for the week of 3/15/87.

03/17/87 Two truckloads of drummed waste were transported to SCA in Chicago forincineration.

03/18/87 Due to no storage facilities being in compliance, the flammable soliddrums were stored on site with permission of the property owner.There were several significant problems encountered which weredirectly attributable to errors made by O.H. Materials, both in thefield and in the office. These problems were addressed by the OSC andMr. Ohneck of OHM. The specific problems are described in Section VII(Problems Encountered and Recommendations) of this report.

03/19/87 TAT and ERCS completed overpacking and staging of tar drums on Coonparking lot; drums of unknowns staged with tar drums. All drums werefenced off and bannerguarded. Drums considered empty by ERCS werestaged along access road, covered with visqueen and bannerguarded.Site was secured and everything was demobed for the time being.

n p i n '•• n o nH i V I _ ~ _> - s,'

Pagan Road Drum DumpFederal OSC ReportCHRONOLOGY OF EVENTS (continued)

04/06/87 TAT and ERCS completed inventorying, marking and sampling of the120 drums remaining on site.

08/28/87 OSC notified by OHM of disposal approvals. TAT performed a walk-through inspection of the drum staging areas and met with Mr. Coon.

09/01/87 ERCS labeled all product drums, bulked hazardous waste liquid intooverpack drums, crushed all empty drums, placed drums on woodenpallets for transportation, and overpacked drums that had previouslybeen overpacked and subsequently damaged by gunshots. The propertyowner was informed of EPA's intention to remove all drums and trashfrom the site.

09/02/87 Removal operations were completed this date. Overpack operationsgenerated a total of 85 product drums that were loaded, manifestedand transported by Chem Freight, Inc. to the ThermalKEM DisposalFacility in Rock Hill, SC, for incineration. One rolloff box wasloaded with crushed drums and site-generated trash, manifested, andtransported by Dart Trucking to Chemical Waste Management, Emelle,AL, for final disposal.

09/03/87 OSC received disposal notification of acknowledgement for wastestransported under manifest to Chem Waste Management and Thermalkem.

RRI 0309 I

SECTION VII

PROBLEMS ENCOUNTERED AND RECOMMENDATIONS

n p I r- ~ P. 0 9f\ U i J ~ J ^ <-

Pagan Road Drum SiteFederal OSC Report

VII. PROBLEMS ENCOUNTERED AND RECOMMENDATIONS

The problems encountered during this removal action are summarized below to

enable the reader to appreciate the challenges and difficulties faced and toserve as a learning tool during future cleanup actions.

A. WeatherMuddy ground was encountered due to excessive rain which prevented the use of a555 bulldozer on site; rather, a 215 bulldozer had to be used to clear densevegetation to prepare a drum staging area. Site operations were also delayeddue to a severe lightning storm.

The region of Pennsylvania where this site was located has been notorious forinclement weather. The type of equipment used has to be adjusted prior to thecommencement of site activities for such weather and work conditions to provideoptimum effectiveness. It is important to take advantage of days on which theweather is good to make up delays due to poor weather conditions.

B. LocationDense woods, two operating businesses, and a family living on the same propertywithin 50 yards of the work area all contributed to difficulties in conductingsite operations. Drums being stacked three high as part of the PRP's cleanupefforts in a box trailer posed problems for the grappler, while having to clearwoods to stage the drums caused considerable confusion in project documenta-tion. More difficulty was encountered when the original staging area wasexhausted and more trees had to be cleared uncovering a new group of drums.Upon sampling and moving of these drums, it was later discovered that ERCSdocumentation of these drums was inadequate in that some were found to bemissing and some had not been documented at all.

AR! 30033

Pagan Road Drum SiteFederal OSC ReportPROBLEMS ENCOUNTERED AND RECOMMENDATIONS (continued)

C. ERCS LogisticsThere was a considerable delay incurred due to compliance issues as ERCSattempted to find a temporary storage (TSD) facility for the overpacked drums.In the interim, disposal costs increased. In addition, drum inventory taken byERCS proved to be inaccurate causing an even greater delay when unaccounted fordrums were later found. The following is a list of the problems encounteredboth in the field and in the office directly attributable to ERCS:

1) One (1) overpack was not numbered. It contained approximately 14smaller containers, all unmarked.

2) One (1) overpack numbered 214 was listed as "empty". It contained apartially full drum of flammable liquid, as per commercial labels on the druminside.

3) The following containers were found on site, but not on OHM's inventorylist: 163E, 163C, 175D, 189C, 191D, and 57 tar drums.

4) The following containers were found on the OHM inventory list, but noton site: 189G, 192D, 192B, 164E, 124, 162, 197, 243A, 192C.

5) Two (2) overpacks labeled as being #193 were found on site. One (1)actually contained Drum #220 (an "empty" as per your list).

6) The drum logs from Wastex listed two (2) drums #205 on the Non-Flammable Solids list. The Wastex logs also listed Flammable Inorganics asNon-Flammable Inorganics, although the flashpoint was 102°F and the disposalsite was expecting Flammable Inorganics.

7) The drum logs from Wastex, which were used to arrange disposal, hadeach small container listed separately as if It were a 55-gallon drum. Theseconatiners, numbered from A to F on the Wastex sheets, when bulked andoverpacked, actually resulted in much smaller loads to the TSDs.

n i.

Pagan Road Drum SiteFederal OSC ReportPROBLEMS ENCOUNTERED AND RECOMMENDATIONS (continued)

C. ERCS Logistics (continued)

8) OHM neglected to inform the OSC that 42 drums, all of which wereoverpacked during the week of March 16, 1987 by SLC, were considered "empty" byOHM. The drums were subsequently removed from the overpacks (once the OSC wasinformed of this) and the majority of "empties" were found to contain wasteliquids and solids.

9) As a result of not identifying the presence of tar drums before mobeon March 16, 1987, disposal arrangements could not be made, thereby delayingcompletion of the removal further.

10) On March 23, 1987, the OSC and TAT were informed by Chem Waste inEmelle, Alabama of that facility's refusal to accept the waste shipment sentoff site March 18, 1987. At first Chem Waste could not accept the wastebecause the drums were labeled as being 19 drums solids and 5 drums liquids, asopposed to the 20 drums solids and 4 drums liquids shown on the manifest. Thedrums were opened at Chem Waste and found to contain either solids, liquids orsludges, of which there were 4 drums. After this problem was resolved on March23, 1987, Chem Waste called the TAT (Pat Donegan) on March 24, 1987 andinformed her that the shipment could not be accepted because the manifest IDNumber (D003) did not match the WPR ID Number (P030). After much checking onour part, it was determined that the WPR, original sent to Chem Waste, ModelCity, was sent to Chem Waste, Emelle internally after Model City was found innoncompliance. According to a Chem Waste, Emelle, representative, the WPR IDNumber was changed in their office to P030 after a phone conversation with aMr. Roger Wheelock, an OHM chemist who approved the change. This revision didnot go through OSC Dave Wright or myself, and furthermore, there was no copy ofthe revised WPR in our files, resulting in misunderstandings and confusionbetween EPA, TAT, ERCS and the TSD. As a result, the drums remained intemporary holding at Chem Waste until September 2, 1987, at which time finaldisposal was accomplished.

Special attention should be given to accuracy when taking any drum inventory.Closer contractor monitoring may be necessary to prevent a recurrence of thistype of situation on another drum removal site.

Letters of. correspondence addressing these problems can be found in Appendix Eof this report. AR ! CGG95

SECTION VIII

LEGAL ASPECTS

A R I O : 0 9 G

Pagan Road Drum SiteFederal OSC Report

VIII. LEGAL ASPECTS

At the time of this writing, the U.S. EPA CERCLA Removal Enforcement Sectionis investigating and pursuing responsible party activities and cost recoverytechniques. All legal issues are considered to be sensitive. Informationregarding legal aspects can be obtained through U.S. EPA Region III Office ofRegional Counsel.

A R I u G u S /

SECTION XI

APPENDICES

A R I G G J 2 G

APPENDIX A

LOCATION MAP/SITE SKETCHES

A R I C G Q S 9

PAGAN ROAD DRUM SITESUMMIT TOWNSHIP, ERIE COUNTY, PA

PAGAN ROAD DRUM SITE , SUMMIT TOWNSHIP, ERIE COUNTY, PA

/' ' D. UN

• • f i R i C O i u i

TOO Number: 8505-05

PCS Number: 3352

PAGAN ROAD DRUM SITESUMMIT TOWNSHIP, ERIE COUNTY, PA

n P\\ lv

SECTION B

FUNDING DOCUMENTATION

A R I O O I 0 3

f

Toi T. MASSEY (EPA9374)Prow: T. MASSE Y (EPA9374) Postedi TUB lO-Juna-flfc 13:15 EOT bys

Subject i PAGEN

SPECIAL BULLETIN A

Summit Twp. , Erie County, PATOt EPA FillData i June 1O, 1986FROM a David Wright

On-Scene CoordinatorTHRU i Stephen Uassersug, Diractor

Hazardous Waste Management DivisionTHRU i Thomas Voltaggio, Chiaf

Suparfund BranchTHRU: Thomas Massey, Chiaf

Emergency Response Sac t ion

I. INTRODUCTIONA preliminary assessment was performed by EPA in accordance witn

the National Contingency Plan at the Pagan Road site in Summit Twp. , ErieCounty, PA, on June 9, 1986. Data received by the OSC indicates thepresence of hazardous substances as defined in Section 1O1 14 (c) ofApproximately 25O drums are on site in various conditions, some are open anhave spilled their contents onto the ground surface and into the surfaceMaters of ' the Commonwealth. both closed and leaking drums yielded positivereadings on organic vapor instrumentation indicating the presence of airreleases of hazardous vapors on site. Based on the assessment performed,the OSC has determined that activation of the *50, OOO Emergency Fund isnecessary at this site. CDC has reviewed data for tnis site and certifiesas to the immediacy of the health threat. Section lO4(a)(l) of CERCLftprovides for the initiation of an immediate removal action where trie re is *release or threat of a release of a contaminant into the environment whichmay present a substantial danger to public health or the environment.

The Delegation of Authority 14-1-A (May 1, 1985) authorizes tne OnScene Coordinator to approve emergency CERCLA funding in the amount ofS5O, OOO for the initiation of removal actions. Therefore, the OSC n-sapproved the use of CERCLA Emergency funding to provide stabilization anasampling at the Pagan Road Drum Site.

I I . BACKGROUNDThe Pagan Road site is located on approximately 2 acres in a

rural/residential area of Erie County, PA. Approximately 21 residences arelocated within 1/4 mi la of the site, and all depend on private wells forpotable water. At present, drums and other containers mentioned previouslyare throughout the property. According to PADER representative, previousattempts by the property owner to clean up the site were not successful. TlJune 9, 1986, assessment of the site revealed the presence of a serni trails.on site loaded with drums, some open, which had previously been scatteredabout the property. The property owner, Marlin Coon, has declined toany action and has given the OSC approval to enter upon the property toperform CERCUA activities. 14 R I J ^ 1 U 4

a

III. THREATAnalytical data received from previous sampling revealed the presence

of hazardous substances both in drums and on the ground surface from lea^ircontainers. These include benzene, ethylbenzene, methylene chloride,toluene, carbon tetrachloride, chlorobenzene, trichloroethylene, andnapthalene, which are regarded as hazardous substances under CERCLA.Several of tha drums contain materials which are classified under RCRA ashazardous for ignitabi 1 ity (flashpoint less than 140) degrees F). Thepresence of these materials on site presents a threat to human health andtha environment from fire and explosion, direct contact, inhalation, aridingest ion. No previous successful attempts by the state or property ownerhave been undertaken at this site.

IV. SCOPE OF WORK

Under the »5O,OOO emergency funding the OSC proposes to initiatestabilization of the vita and Mitigation of the threat presented by thematerials on site. Activities proposed will include staging, sampling,overpacking drums, which ara presently leaking or emitting hazardousorganic vapors, arid drum removal to an approval storage facility.

V. OSC ACTION

Because conditions at this site meet tha CERCLA criteria for initiaticof emergency removal activities, tha OSC has activated the »50,000 ernergencremoval funding for this sita at 16O6 hours, 6/9/86. The estimated totalcost of this emergency action is *50,OOO.

Dav7d~WrIght7~OSCU. S. EPA, Region IIIPhiladelphia, PA

A R i G 3 ; G 5

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III

841 Chestnut BuildingPhiladelphia. Pennsylvania 19107

Request for Additional Funds - CERCLA Removal _SUBJECT: Action, Pagan Road Drum Site, Summit Township, DATE /J&K( \3 1986

Erie Councy, PA '"'

FROM: D«vid p» Wrlghc, On-Scene Coordinacor, fL tf/ljb -jf 2L. /7Emergency Response Seccion (3WH22) t*F*r ** -ft~J&~* Vs

TO: James M. SeifRegional Administrator (3RAOO)

THRU: Stephen R. Wassersug, Direceor'V s~\C VHWM Division (3HWOO)

I. Issue

ceor'Vj?

/}/? JT*? / "Tr%$ <*~><r< f

In order to continue the immediate removal action at the PaganRoad Drum Site in Erie County, Pennsylvania, the OSC is requesting anadditional $150,000. The cotal project costs will thus be increasedco $200,000. The requested funds will be used co stage, sample, anddispose of approximately 250 drums of hazardous substances presentlyonaice. Ac the present time, drums of hazardous substances in varyingconditions are scattered across the property; many are emittingorganic vapors ac hazardous levels. The sice is located in arural/resldenclal area, and the nearest occupied dwelling is less chan100 yards from the sice* CDC and che Pennsylvania Department ofHealth have certified as co che immediacy of che threat co che publichealth and Che environment presented by Chis site.

II. Background

The Pagan Road Drum Sice is located on approximately two acresof land owned by Mr* Marion Coon, owner/operator of Che CoonRefrigeration Company, which is located dlrecdy adjacent Co chesice. Approximacely 21 residences are located within 1/2 mile of chesice; all depend on wells for po cable wacer.

An EPA assessment performed June 9, 1986, revealed approximately250 drums onsice, moec of which are located inside an unmarked tractortrailer, also onslte. EPA filee Indicate ehac drums may have beenscored on che property since 1982. when Che Tri-Scate InsulationCompany operated an Insulation and coaclng business ac this sice. Airmonitoring performed daring che assessment revealed high levels oforganic vapors near bung openings from drums on Che ground surface, aswell as in Che erector trailer. The trailer contains various sizeddrums, stacked from floor Co ceiling near the entryway, preventing anaccurate inventory of contents, although open drums of liquid werevisible.

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Drum samples taken previously by CPA and the TechnicalAssistance Team reveal the presence of several hazardous substancesonslte. These included benzene, ethyl benzene, toluene, methylenechloride, carbon Cecrachlorlde, chlorobenzene, trlchloroethylene, andnaphthalene. These substances are regarded aa hazardous substancesunder CERCLA as per Section 307 of this Clean Water Act. Severalsamples also contained flashpoints of less than 140*F, constitutingRCRA hazardous waste for ignitabillty.

At Che presenc time, these materials remain onsice in drumswhich are unsuitable for containment and which continue to vent toxicvapors and discharge onto the ground surface. The drums also presenta fire and exploaion threat in the confinement of che trailer. Arequest for an additional $150,000 is being made ac this time Copermit che continuance of emergency removal actions undertaken by cheOSC as per the $50,000 Delegation of Authority. The OSC haa plannedto demobilize personnel and equipment from che sice June 13, 1986, acwhich time Che available emergency funding is estimated to beexhausted.

III. Actions Taken to Dace

Sice Accions taken to date Include assessments and activation ofthe Emergency Funding In order co initiate sice stabilization andsecurity. A site survey and drum and soil sampling haa beenperformed, and ambient air readings have been taken as pare of theassessment. The action begun under che Emergency Funding includesoverpacklng and scaging of drums on che ground surface as well asinitiation of removal of che drums from che crailer with overpackingand sCaging of Chem as well. Samples are being taken from che drumsfor disposal purposes. Access to the site haa been restricted, andoptions for storage and diapoaal have been evaluated by che OSC.

IV. Presenc Scatus

At Che presenc time, a number of drums have been overpacked incontainers sulcable for shipping. More drums require overpacks, andall drums muse be removed from che sice Co an approved TSD fordisposal, as recent investigations into che opclon of temporaryscorage indlcace chac no facllieles are available at ehis time.

The OSC has considered alcernaclves eo che coneinued removal ofhazardous materials from Che sice and found Chem Co be inadequate in•dclgating che chreat to public healch and Che environment. Referralof Chls sice Co Che EPA Sice Investigation and Support Section (SISS)will be done after the immediate threat co the public as presented byche drums and surface contaminated aoil la eliminated.

A R 1 C 0 1 C 7

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V. Summary of Costs

The following Is a summary of Che proposed and existing projectcosts for Che Pagan Road Drum sice:

Original funding Request $50,000ERCS 10,000 (The estimated expend-

itures as of 6/11/86.)TAT ~ Hoc applicable, not from emergency celling.EPA — Hoc applicable, noc from emergency celling.

Proposed Funding Increase $150,000ERCS 100,000TAT 35,000EPA 15,000

VI. Proposed Actions

With che additional $150,000 che OSC propoees Co completethe overpacking and securing of all drummed materials, complete thesampling for disposal, and dispose of all hazardous materials in anEPA approved facility.

VII. Remedial Actions

Thia sice la noc currently on che NPL List nor is it beingconaidered for inclusion ac chis time.

VIII. Enforcemenc

All pocencial responsible parties have declined'eo assumeresponsibility for removal of hazardous substances on Chis sice atchis clae.

XI. Regional Recommendation

To eliminate the threat co Che nearby public and che environment,consistent with che Immediate removal criteria contained in Section300.65 of Che NCP, I recommend Chac you approve^ Chis additional$150,000 ceiling Increase.

DISAPPROVAL: _______ ______________ DATE

P. oA R I G G I O G

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III

841 Chestnut BuildingPhiladelphia. Pennsylvania 19107

Additional Funding RequestSUBJECT: for the Pagan Road Drum Site, DATE: JAN 28 1987

Summit Townsh ), Erie Cjjunty, Pennsylvania

FROM: James M. SelfRegional A

Dr. J. Wlnston Porter, Assistant AdministratorSolid Waste and Emergency Response (WH-562-A)

Pursuant to the April 16, 1984 Delegation 14-1-A, I have approved

additional funding for this site in the amount of $210,000.

Attachments

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III

841 Chestnut BuildingPhiladelphia. Pennsylvania 19107

Request for Additional Funding ..« 2 8 t367SUBJECT: for the Pagan Road Drum Site, Suamlt Township DATE: JW1

Erie County, Pennsylvania _

FROM: David P. Wright, On-Scene CoordinatorEmergency Response Section (3HW22)

T0: James M. SelfRegional Administrator (3RAOO)

THRU: Stephen R. Wassersug,Hazardous Waste Management D

I. PURPOSE

A CERCLA immediate removal action was Initiated at the Pagan Roadsite in Erie County, Pennsylvania oo June 9, 1986 and an exemption froithe six-month limitation was granted December 8, 1986 to allow forcontinued emergency response actions. At this time, a request foradditional funds in the amount of $210,000 is being made to allow forthe completion of overpacklag, transportation, and disposal ofapproximately 250 drums of hazardous waste on the site and eliminatethe threat to human health and the environment presented by thesesubstances. The total project ceiling will be increased to $410,000with the approval of this request. An exemption to the $1,000,000limitation is not anticipated.

II. BACKGROUND _ '

The Pagan Road Drum site Is located on approximately two acres ofland owned by Mr. Marlin Coon on Pagan Road, in Summit Township, ErieCounty, Pennsylvania. An EPA assessment was performed June 9, 1986 andrevealed numerous drums on the site, on the ground surface and in anabandoned trailer. Emergency removal activities were initiated thatdace under the $50,000 Delegation of Authority to provide site securityand mitigate the emergency situation. The OSC determined that thehazardous wastes found on the site in approximately 250 unsecured anddamaged drums presented a threat to human health and Che environmentthrough fire end explosion, based on the high levels of organic vaporsfound in the ambient air onaite and initial laboratory analyses on drumsamples. Additional funding for $150,000 was approved June 13, 1986,fqr continued removal activities. Work performed at that time included

A R I Q 3 I 1 0

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removal of leaking drums from surface water on the site, overpacking leakingdrums, staging all drums, and providing site security. The OSC receivedcomplete analytical results on the drums in September 1986 at which time TSDfacilities were selected, and the OSC continues to await disposal approvals forseveral waste streams. An exemption from the six-month limitation was grantedDecember 8, 1986.

III. ACTIONS TAKEN TO DATE

As previously mentioned, many of the waste drums were overpacked, and alldrums were removed from fhe trailer and staged onsite. A temporary snow fencewas erected around the drums and the area was posted with bannerguard. Periodicinspections of the site were made by the OSC and TAT during the months followingdemobilization in June 1986 to ensure site security while EPA awaited TSDdisposal approvals.

Due to the variations in waste streams on the site, it was necessary toseek approvals from at least seven TSD facilities. The non-flammable organicliquid drums were rejected by the first choice, most cost effective TSDs due totheir tendency to be "uncontrollably reactive". Aa stated by the contractor,the secondary choices for disposal will be sore expensive than the facilitiesoriginally considered for disposal at the onset of the removal. Incinerationof wastes will be the disposal method of choice by the OSC in keeping with theland-disposal restrictions and EPA policy concerning permanent solutions toSuperfund cleanups, however this has become one of the least cost-effectiveoptions in recent months ($900 per drum).

IV. THREAT

Although the drums have been removed from the trailer and overpacked, theyremain staged onsite on the Coon property. The potential for vandalism of thehazardous materials remains, and what appeared to be bullet holes werediscovered iri several overpacks by the OSC during a recent inspection of thesite. Although the drums were secured during the initial stages of theemergency removal, the potential for deterioration, leakage, and air emissionsexists as long as they remain onsite.

The presence of lerge quantities of flammable and toxic materials in thisrural/residential area will constitute an immediate risk to public health andthe environment until they are removed to an approved disposal facility.Preliminary lab analyses revealed wastes present with flashpoints of less than140F, along with hazardous substances including benzene, ethylbenzene,methylene chloride, carbon tetrachlorlde, and trichloroethylene. These drumswill remain stable on a short-term basis, but will deteriorate in time,resulting in the release of these materials into the environment.

V. ENFORCEMENT

The OSC has worked with CERCLA Enforcement and the State to identifypotential responsible parties. To date, no PRP has assumed cleanupresponsibilities. . , , ,A R I Q 0 1 M

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VI. PROPOSED PROJECT AND COSTS

The OSC proposes to complete overpacking of damaged drums, of whichapproximately 100 will require overpacking before disposal; load andtransport wastes to approved TSDs; remove contaminated soil, if any; andrestore the ground surface as needed. As of January 11, 1987, approxi-mately $93,000 remains in the original ERCS ceiling to be used toward theaforementioned site activities In conjuctlon with the requested additionalfunds. The ERCS total costs will include transportation, disposal, personneland equipment.

The distribution of project funds is as follows:

Current Ceiling - $200,000ERCS - $150,000EPA - $ 15,000TAT - $ 35,000

Requested Additional Funds - $210,000ERCS - $145,000EPA - $ 10,000TAT - $_____

Subtotal $155,000(15Z of $155K for EPA HQ) $ 23,250(15Z of $200K for EPA HQ) $_____

Requested Total - $210,000

Total Project Cost - $410,000

VII. JUSTIFICATION

The state DER and CDC have certified the threat or risk to publichealth presented by uncontrolled discharges from, and access to, this site.In order to mitigate che ongoing threat to human health and welfare and theenvironment, 1C will be necessary for the OSC to obtain additional funding.Further aasistance from any other Federal or State agency will not beforthcoming, and without a funding increaae this site will not be stabilizedand secured on e timely basis. This site is not on the National PrioritiesList (NPL).

VIII. REGIONAL RECOMMENDATION

The conditions at the Pagan Road Drum site meet the criteria set forthin the National Contingency Plan Section 300.65 for a removal action. Yourapproval is recommended for this additional funding request for $210000.

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Tou may indicate your approval cr disapproval by signing below.

APPROVE \A. ——— IUA. ^T1 DATE t t , t 7/ /?//i

DISAPPROVE ____________________ DATE

i O&R1C-.M -°

APPENDIX C

SITE SAFETY PROTOCOL

A R 1 0 Q !

SITE SAFETY PROTOCOLPAGAN ROAD DRUM SITE 6/10/86

SUMMIT TOWNSHIP-ERIE COUNTY, PA

INTRODUCTION

THE ATTACHED SITE SAFETY PROTOCOL APPLIES TO CLEAN-UPACTIVITIES AT THE PAGAN ROAD DRUM SITE. THESE PROTOCOL REPRESENTSAFETY GUIDELINES SET FORTH BY THE EPA ON-SCENE COORDINATOR ANDHIS SUPPORT STAFF TO INSURE WORKER SAFETY DURING THIS CERCLAACTION. THIS DOCUMENT MAY BE AMMENDED BY OSC DIRECTION AS SITECONDITIONS CHANGE.

ALL PERSONNEL INVOLVED IN THE ACTIVITIES AT THE PAGAN ROADDRUM SITE SHALL READ, UNDERSTAND AND ADHERE TO THE FOLLOWINGSAFETY PROTOCOL AND ACKNOWLEDGE SO BY SIGNING THE ATTACHED SHEET.THE PROTOCOL WILL REMAIN IN EFFECT UNTIL THE OSC CERTIFIES THATTHE CERCLA ACTIVITIES HAVE BEEN TERMINATED.

RESPIRATORY PROTECTION PROGRAM

ALL CONTRACTOR AND GOVERNMENTAL PERSONNEL INVOLVED IN THI'SCERCLA ACTION SHALL HAVE A WRITTEN CERTIFICATION OF FITNESS INORDER TO WEAR RESPIRATORY PROTECTION EQUIPMENT. ALL PERSONNELWEARING AIR-PURIFYING RESPIRATORS ARE REQUIRED TO HAVE A WKfTfi-NRECORD OF PROPER FIT TESTING, WHILE THOSE WEARING PRESSURE-DEMANDSELF-CONTAINED BREATHING APPARATUS CSCBA) OR AIR LINE APPARATUS,MUST BE PROPERLY TRAINED AND EXPERIENCED IN THEIR USE.

ALL RESPIRATORY PROTECTION EQUIPMENT WILL BE PROPERLYDECONTAMINATED AT THE END OF EACH WORK SHIFT OR WORK DAY. ALLRESPIRATORY PROTECTION EQUIPMENT WILL BE INSPECTED BEFORE EACHUSE.-

PERSONS HAVING BEARDS WILL NOT BE PERMITTED TO WEAR AiK:-PURIFYING OR PRESSURE-DEMMAND REPIRATORY EQUIPMENT.

TRAINING AND MEDICAL MONITORING

ALL PERSONNEL WILL HAVE EITHER FORMAL TRAINING OR ON-THE-JOBTRAINING AND MUST DISPLAY THE ABILITY TO PERFORM THEIR INDIVIDUALJOB FUNCTION IN A COMPITENT MANNER.

ALL CONTRACTOR AND GOVERNMENT PERSONNEL SHALL BE ENROLLED INA MEDICAL MONITORING PROGRAM WHICH IS ADMINISTERED BY QUALIFIEDMEDICAL PERSONNEL. ON-SITE MEDICAL MONITORING WILL BE PERFORMEDWHEN TEMPERATURES EXCEED 80 DEGREES F. ALL CONTRACTOR ANDGOVERNMENT PERSONNEL WILL BE REQUIRED TO FORCE LIQUIDS TO PREVENT

n p i nH ni i L

DEHYDRATION AND REDUCE THE POSIBILITY OF DEVELOPING HEAT STRESSAND HEAT STROKE.

ALL SITE PERSONNEL WILL BE REQUIRED TO REVIEW THE PROVIDEDCHEMICAL INFORMATION OF KNOWN ON-SITE CHEMICALS.

X

Site Safety ProtocolIC/vo Kfwv f\ J. \i?

General Safety Rules and Equipment

a. There will be no eating, drinking or smoking in the Exclusion Area or hotside of the Contamination Reduction Area.

b. All personnel must pass through the Contamination Reduction Area to enterthe Exclusion Area.

c. An emergency eye wash will be on the hot side of the ContaminationReduction Area.

d. As a minimum, an emergency deluge shower/spray can is to be located on theclean side of the Contamination Reduction Area.

e. At the end of the work, all personnel working in the Exclusion Area shalltake a hygenic shower.

f. All supplied breathing air shall be certified as Grade D or better.

g. Where practical, all tools/equipment will be spark proof, explosionresistant and/or bonded and grounded.

h. Fire extinguishers will be on-site for equipment or personnel fires only.

i. Since site evacuation may be necessary if an explosion, fire, etc., occurson-site, an individual shall be assigned to sound a horn. For example, cheevacuation signal may be two long blasts every 30 seconds until allpersonnel are evacuated and accounted for. This procedure will be reviewedat each morning's safety meeting.

j. A first-aid kit will be on-scene at all times during operational hours. Anoxygen inhalator respirator and a qualified operator will be available.The location of these items on-site will be posted.

Morning Safety Meeting

A morning safety meeting will be conducted each day for all site personnel whosign a daily attendance sheet. The safety procedures, evacuation procedures,and escape procedures, as well as the day's planned operations, should bediscussed.

f l R I O Q I 1 7

Site Safety Protocol

CONTROL AT THE SITE

Access Co Che site will be restricted by a continuous chain link fence orinstalled during the immediate removal phase at this site and exit from thesite shall be through the gate in the n Reduction Area except in alife-threatening emergency.

All persons entering the site shall sign in and out at the OSC command post.

DESIGNATION OF WORK AREAS AT THE SITE

The entire site will be divided into three areas: (1) Exclusion Area whichknown to be or have a potential for becoming contaminated: (2) theContamination Reduction Area where decontamination of personnel and equipmentexiting the Exclusion Area is performed; (3) the Support Area which is notcontaminated.

The Exclusion Area (EA)

At the Rtj. EI-ivJ Site, the Exclusion Area shall initially includeall areas inside the chain link fencezjc tst\n ti-o.ard-

The Contamination Reduction Area (CRA)

At the &C.CVA i?<j(\A Site, the Contamination Reduction Area will belocated LnmedLately outside the access gate and will be delineated by ropedoff area.

The Support Area (SA)

At the R*( R<y\.t\_____Site, the Support Area will be the area outside thechain linK tence not roped off.

Changes in Designation of Work Areas

As work progresses on-site, Che OSC may determine Chat an area previouslydesignated an EA is no longer classified in that manner. It is not intended,however, co change Che designation of Che CRA since chis may involve Chemovement of Che decontamination facilities and added expense.

SAFETY PROCEDURES AND LEVELS OF PROTECTION

Exclusion Area

1. All personnel shall enter and exit the Exclusion Area through theContamination Reduction Area.

2. Emergency escape routes from the Exclusion Area will be established andreviewed as appropriate at each morning safety meeting.

n n I !""> ."•. ! IDA n I u J i i u

Site Safety Protocolr?>r,n «\ £cy\ d.

SAFETY PROCEDURES AND LEVELS OF PROTECTION (continued)

Exclusion Area

3. All personnel in the Exclusion Area shall use the'protective equipmentdesignated for their job function but in no case shall less than LEVEL C beused.

4. Personnel performing the following job functions in the Exclusion Area willutilize the designated level of protection equipment.

Prime Contractor

a. Barrel handling, including opening, sampling, pumping, moving,emptying, or any direct or indirect disturbance of a full-barrel willbe performed in Level B. This applies to anyone involved, includingequipment operators.

b. Excavation operations will be performed in LevelC

c. Soil removal operations will be r-rformed in LevelC

Contamination Reduction Area

1. Personnel and equipment decontamination will be performed in Level C.

2. All personnel entering the CRA will utilize a minimum of Level Cprotection.

3. All personnel entering the CRA must decontaminate which will be performedin Level C.

4. All equipment entering Che CRA must be decontaminated prior to leaving theCRA.

Support Area

1. No contaminated equipment or personnel may enter the Support Area.

n D i r, 0 I I 0tt n l o% w i i ^

DECONTAMINATION

ALL EQUIPMENT AND PERSONNEL ENTERING THE EXCLUSION AREA MUSTBE THOROUGHLY DECONTAMINATED BEFORE LEAVING THE CONTAMINATIONREDUCTION AREA. DUE TO THE VARIETY OF EQUIPMENT UTILIZED ON-SITE, THE OSC AND HIS STAFF WILL DETERMINE IF THE PROPOSEDDECONTAMINATION METHODS ARE APPROPRIATE. THESE DETERMINATIONSWILL BE MADE ON A DAILY BASIS.

AIR MONITORING .

PERIMETER AIR MONITORING SHALL BE PERFORMED DURING PERIODS'OF HIGH SITE ACTIVITY AS SEEN APPROPRIATE BY THE OSC. ALL AIRMONITORING DATA WILL BE RECORDED IN A LOG WHICH WILL BEMAINTAINED AS PART OF THE SITE FILE.

AIR MONITORING WILL BE PERFORMED WITH A PID OR FID TO DETECTORGANIC VAPORS AS A MINIMUM. THE PURPOSE OF THIS MONITORING ISTO INSURE THE SAFETY OF SUPPORT AREA PERSONNEL AND THE GENERALPUBLIC. ADDITIONAL MONITORING MAY BE REQUESTED BY THE OSC ASADDITIONAL ON SITE CHEMICALS ARE ENCOUNTERED OR SUSPECTED.

A R I Q G 1 2 0

1066 itMi-r HiiiM. Peaicillia GC,,H,4O.. mol wt 266.21. C 76.67%. H 3.30%. O 11.03%.Prrpn: Buu-Hoi. taudct. U.S. pal. 3.01X042 (1961 lo Soc.Beige r Azote Prod. Cbim. Marly). Pharmacological itud-Mt: Barchewiu ti ai. Arummitui-Fonc*. 22, 333 (1972).

CXx -o

CryMala. mp 124.3*.THULAS CAT: For incraaaad capiUary fragility.106*. BaiTlTaln PeakUlui G. fmieitli* O mmmmnt

with N,Nf-a-itemylaifrytoiee-iaaitoa; A/. '-dibaazylelbyleM-diamine b»i(ben»ylpeninllin); dibenxylethvltnadiamine di-pmalun O; penicillin O mil ol *.4V'-dibaBzyletbyi«Mdi-anuna; beawthacU; diamine penicillin; Baaollia; Mejaiilliii

allia; OUaoia; Permapen; Duropcninctllia; OBEO Penicillin; Pemdural; TardocilluK Dibancil:

View Neolia; Pan-Oi-Bno; Pewdura; Moldamin;

Ccpealma. C-H,,N4OfSJ; mo* wt 909.11. C6.21%. N 9.23%TO 14.01%. S 7.03%. Activity o

Eaicncilline; Longacilina; Loogial: Pcnadur: Peadilan;~ 63.41%. H

Activity not leaa thanI03O uaili/mg (theory: 1307 uniu/mg). Prapd by addingan aq tola ol one mole W. V'-dibmnylathylenadiamine di-acetate to an aq iola ol 2 molai andium penicillin O: Sxabo•i ai. AIHIO** e) CtomctfAer. I. 499 (1931); bate. Bruce.VJi. pat. 2.6X7.491 (1933 lo Wyeth).

TMUAT CAT: Antibaeurui.1061.

(1-3-(3.3-dibromo-4.

hydroaybenaoyl)-2-ethylbenxoluran; 2-ethyl-3-benxoluraa-yl 4-hydroay-3.3-dibromophcnyl keiooe; 2-etb»l-3-O.S-di-bromo-4-hydro»ybcnzoyl)ben2ofuraa; 2-etbyl-J-(3.S-di-bromo-4-bydro»yben»oyl)o«a»ndrn»: 2-ctbyl-3-beuofuryl3.3-dibromo-4-bydnuyplMByl ketooe; L 2214; MJ 10061;Oaauric; Minunc; Uncovac. CI*HUBV,O.; mol wt 424.11. C41.13%. H 2.13%. Br 37.6*%. O lT.32%. Prepn: Bat* pal.$33.621 (1937 lo Lakax): Buu-Hoi *tmi.J. Cftcm. Sac. 19S7.623; Buu-Hoi. Smiirtal U.S. pal. 3 1X042 (1961 to Soc.Beige r Azote Prod. Cairn. Marly). Structure-activity•tudy: Ddbarre tt ai. OHm. 7»er. S, 47O (I9M). Pharma-cology: Mcrtx. tivnett**. ttfd. tVocluiuekr. III. 491(19*9); ZoaUaer a ai. K/te. WectoucV. 4S, 426 (I970XZoellncr. Oroeboer. Amttnttut-tone*. 21. 1300 (I97IX

Ycllowiah priaou. mp 131*THUAT CAT: Uricoauric.1069. Btaaeaa. Bauol; cydohaaairioM. C f» mol wt

71.11. C 92.23%. H 7.73%. Diacoverad by Faraday iaoomprcMad od gaa ia 1123. Obtained im the coking of coal

Hydraied. taaidea* cryctaU. mp 123-124*. Mf(c — 0.103 ia formanude). Soly in water — 0.13 mg/ml(about 2OO uniu/ml); ia naiiaain — 0.31 mg/ml; la ale —3.2 mg/ml; in aeetocie — 1.3 mg/ml; ia fonnamide — 21.0mg/ml. pH ol aald aq tola about 6. Solubilitiea determinedby Wow tl al. Aniibm a\ OnmotlttT. 7. 374 (1937) inmg/ml: water 0.313; methanol 16.9; etaaaol 13.4.THERAP CAT: Aaubacicrial.TNaaAr CAT (VOT: Aaobacterial.1067. BeauthlM Pc dllla V. PeniciUia V OBEO: Oi- Yr

irocillmc. Biallia V; Falcopen V. Prapd in a manner analo- "'/O1*-goua to bouathine penicillin C from one mole MAf'-dibenz-ylcihylenedtaminc and 2 mole* phenosymcthyl penicillin.SolubiliucB determined by Watt* « tl. Aiuioiot a\ Otumo-<A*r 7. 374 (1937) in mg/ml al about 2f: watercthanol 14.6.

. *9 I.17. 4ll (Thorae tt al. M fug. Ottn. Anal £et 17. 4ll (1943).

Flaah pi 10-ir. Sol ia 1430 pan* water auaabte with alco-hol, chloroform, ether, carbon duulAde. carbon letrachlo-ride, glaoal acetic acid, acetone, oil*. Kftf ia w»U-ekm*4oo*i*a*n u, a cool plan »nd »*oy from fl*. LO. orally inrau (young adulla): 3.1 atl/kg. Knnura tt al. TotitolHtarmaetL It. 699 (1971).Sodium _danvC.HNa.f*«.y»<«.«. Pr.: Schlo*«r

1070. Hianaatnoaic Add. Phaiylanoaic acid. C.H,-mol wi 202.03 C 33.67%. H 3.49%. A> 37.01%. O

Cry*l powder, mp 131-162* with dec. Sol in 40 pantwater. 30 part* alcohol: inaal in chloroform.USB: JUegcni for tin.1071. Beaxeaeboroak Add. >**m/<*0nMicaciApbeny|.

boric acid; phenylboron dihydrojuUe. C.H,BO- mol wt121.94. C 39.10%. H 3.79%. B 1.17%, O 26.24%. Prepd bythe reaction ol phaaylmagncaium bromide with methylbo-aie: Wuhbura tt mi. Advanca in Cktmairy Jenat 23,102-12* (1939). oCrysuli from water. Sponiaoaou* convenioa to CtH(BO.

dry air. although the beat method i* by aiaouopic dehydra-tion with toluene, mp 213-216* (anhydride). Ka 13.7.Oipole monMBl 1.72 (diokanc). Soly in water ai 23*: 2.3%.

1.73%. «yleM: 1.2%. ether: 3OJ%. methaaol:171%.

1072. BcaMacatiaoaic AclaV. Dikr4n*?ri»n,UiitoinatUft pbenyUtibonic acid: phanylMibinic aod. cJi.O.Sb;BMl wi 24*.t7. C 21.93%. H 1*4%. O 19.29%. Sb 4«.92%.C,H bO(OH)r Arytolibonic acida caul ia the lolid «aie a*polymer* of high mol wt. aacocialad by H-boad*. Tae ioaaaxial probably ia the form (ArSMOH).]-. BaaTanmlibonicacid i* prepd from henianediiionium chloride and antimonyIrioaidc in che pnacnca of alkali: Schmidl. A**. 421. 176,1(1 (1920); Car. pal. 234,421; Clum. Zmir. 1913, L 343;Frdl 11. 10*4. From the double compd of bennnartiatoni-urn chloride and antimony trichloride by the action ol alkali:May. J. Ctom Sot. 101. 1033 (1912); VS. pat. 1J4O.707.Miaule cry*ial* from acetic aod. larger diamond-ihapad.

gliiteaing cryual* from alcohol-chloroform aualura on theaddition of water. Not melted al 23O*. dac al higher lamp*.

and in the production ol illuminating ga* from coal. Puri-fkaiion by waahing with water: Brit. pat. M3.7I1 (1961 10Schiovaa-Caamic and H. Koppcr* GmbH). CA. 33, 1697lf(1961). Lab prepn by oauotisation of amliaa, followed byreduction of the diajomum *ali in NaOH iota uaiag »iaa-noua chloride: Oaltamana-Wieiand. frmjui am e aawcAenCWmi4t»(de Oniyicr. Berlin. 4Oih ed.. 1961) p 247. Pro-ductioo ol pure benzene: Fmach. 1*4. Clumia 39. 9-12(1963). Toaiaiy: t Browning. Toxxuy and M«taao/um oftndtitinal Saiitint (Ebevier. New York. 1963) pp 3-43.

¥"iA.-.L/'>a*"><'UJi 'ar - 2

Oaar. eotorlaaa. highly OaaamaMa liquid; ehancleruiicodor. dfO.I7t7. bp atXI- SoUdif +}.r. *9 I.JOI Ot

um av. ..a. ••M/ •.«. rapn: cX<if»« Ckam. 76, 1*7 (1964). Solid nuua. dac byacid*, alkalka. Sol ia liquid ammonia, lauahydraluran.tftunaa TaucttjK Aetat (Iram iagaMioo or MihaUnon)

iniiauon of mucou* OMmbranaa. ~ •' ———— coavuUtotu.eioiamant. drpreanna. Oaata may follow from impuatory ^ " 107S. I

Ant. Our-~ Light ucryiullueitefiea upc

(atlura. CknMicr bone marrow drpraaiion and aplaata; rare- *>J ride; _ly. leukonia. Harmful ami* may be abaorbad through akin. I Sa 176.62. iUU: Manul ol mertinnal cfagnical*. dye* and many other ' LU 11.13%. l

organic compound*, aniftoal laather. linoleum, oil doth. ( *fi" from the iairplane doom, vanuahaa, lacquani a* Mivenl lot waae*. I . /" POCL.. Arauna. oila, ate. , ~_i' Or,. j>* <THUAT CAT (Ym: DaMroy* tcrcwwonn larvae ia wound*. I •> 1941).

P»St DO w a a M r w j M . _ . ,.. _ ,A R I 0 D 1

Colorlessbp*. 231-2and liable t

1076. L;oxyquiao!.31.06%. Prmet banal, ttanhydride oi1941) p 317

Mon aclinictol in water.chloroform, cTnmcthyl <Tnacrute,

Radily hydrtusa: In gai

ju*t aa good i1077. B«aj

aae. Ocio(c41ir291.41. C (0.pom big. Theignatod benieiSynihmi Slu

h

. ItfM. EtfcyUaJllM. ' M-SHtfltaMtammmlitai ethylpbeayl.aanaa. CMHH: mol wtl21.lt. C 79.29%. H 9.13%. N11.36%. Produced by healing aniline hydrachlorlde andaloohoi at ISO*. •>*"' ' ' • '• -

V*ry refractive liquid; rapidly bacoaM* brown on empoaurato light and air. Aniline-lit» odor. 40.0.93*. bp 2O4.r.SotidiAea below MT. ma -63.r. af 1.3339. Uuol in waternuaobie with ale. ether and away other organic aotvenia.K»*r **U tlam* amm f aiirliiiyham %*t LDm orally m rattt

3701. Ethyl FHirn.air.fin 4-H*r~r~<<-»*~r.3695. BthylBHlnWj CJH* mat wt 106.16. C 90.30%.

H 9.30%. C.H.C.K,- PraiMB. aW. 4*7la3f O»13k Oatlarmaaa-Wletaod. fnutu dm

' Ottmikan (da Omytar. Berlin. 40Ui ad.. 1961)p 331 By Huaag-Mialoa modiAcaoon of WoUMCiahocrrediwtion: A. 1. Vogei. ftm liual Ormumit CJtamiury (Long-

3rd ad.. 1939) p 316.arlm* ttquM; flammib

-93.01': Oibbon* ttat.J Am. Ckrm. Sac. 60. 1130(1946).Calarlm* ttquM; flammibli dj 0.*66. bp 136.23*. fp

1.4932. FlM. p«20*.

dj 0.*Ckrm.

yl CJMT. C,H.p.S; mol wt 1*6.23.23.77%. S 17.12%7 C,MfSO,CtHrium tinnienaiiilfnnate and dMthyf

fmtamnml/anie atia>C 31.39%. H 3.41%.Obtained by bearing

___ ______ __ __ _.._..'*uBaUM 130*.ColorieM to ilightly yellow, almoal odorlea* liq. df 1.219.

bp,, 136*. Slightly tol in water, avactble with alcohol, benz-ene, chloroform, ether.36*7. Ethyl Beataoata. lunate aeU artyl mtar. CM-Of

mot wt I3ai7. C 7U9«%. H 6.71%. O 2131%. C.H,COO.C,H,.Coloriaa*. dear, refractive liq; aromatic odor vapor* cauaa

cough, df 1-030. bp 2ll-2ir. mp -34'. nf 1.306.AJmoal nuol ia water; nuecible with alcohol, chloroform.ether, petr ether. LOM orally • rat* 6.4* g/kg. Smyth atai. Aifh. l*m. UH. Oecuf. Meat 10. 61 (1934).list la perfumery under the naaae tmmct at Ma**; ia

maauf of ftam e"a>a«ne;arancul fruit mi aim36M. Ethyl BanJoylacaUle.

acid etftyl amor. ~ " '6.29%. O 24.9TLiquid; pteaai

and light. du 1.I2X b|with tiaam. aff 1.333*.bokcihcr. JCany Ji ttaut flam atr amiMM. a-EthyBMwyl Alcrtri. ••

.-cthylbenzyl alcohol; l-phemyl-l-propanal: l-pheaylprop.yl alcohol: ethyl phanyt cartinol; e-bydroiypropyibeuanc;SH 261: Epbd; Uvoaal; Phanycholon; Phaniaok Phenychot:Fenieol; Pencun Fnatrepa. CJl O Ml wt 136.19. C79.37%. H *.*•%. Q 11.73%. Prepd from baualdeaydc orfrom ethyl phenyl ketonai Narria. ConaM. J. Am, Chem.Sac. 49, 2640 (1927).

Oily liquid. Weak. auar-Mae odor. Swenith. mgbtly irri-tating uau. df 0.99U. bpM. 2I9*; bp, lOT. bp. If. •«1.3169. uv ma* (•MthaaoUT 23O. 260 am U 173. 114).Miaable with methanal. ethanot. ether.olive oil. LOa orally • rata: 1300 mg/kg.uta: A* heal tr*nafer medium; ia) perfuau

Tuajt 4M Camalt lot tram inner ar/wv aaiaf fait action.

•3700 EthylaenzyUiillM.- N.EtltjI.N-mkm fmvamtm,211.29. "? 13.26%. H a.11%. N 6.73%; Prepn: MartiTMarQuean. UA pal. 1 07.772 (1933 lo Oowk Burgatahler/ Am. Chtm. Sec. 73, 3021 (1931). ;

Light yellow, oily liq. df 1.034. bp 2ST with alight———— bpM 170-latr. - af 1.393*. Practically inaol inwater. One ml

Picraie. eryMala. mp 11S-12O*.Maauf dyaai in orgaaie tyai

acM atAyl «Mr; ethyl b 4-hydre«ycoumar. . --inyDacatata: ethyldicoumaroi acetate; bi»-3.3'-<4-bydro*y r oiiwtcumanayDacetic acid ethyl eater. 3.3--carboiymethyl*nc rS«»b»(4.hydro*ycoumana)ethyl eater, ethyl '-dihydrojiydi- _y*r*!coum4wiay|. 3.31 -acetate; B.O.E.A.: Dicumacyl; Tromeaan; ._ nTromeaan Ethyl Acetate: Pelenun. CaHHOi; mol wi , >«»> m401.33. C 64.70%. H 3.93%. O 31.34%. >rapnT Roaicky. ' 3701. I

Crystal*, dimorpboua. mp 177-112* and mp 134-137* . cocnac etiBitter, peniiianl taita. Practically inaol in water. Sol in 20pan* acetone, alao tol ia benzene. Slightly *ol in alcohol. 3710. 'ether. LOM orally ia mica: **0 mg/kg. *-kyl cvbiTHUUr CAT: Anticoagulant. , H L33%. <

' Mar 72. 33702. Ethyl Branalni. BrumooOto** moaobromoethanc; 3J 14,762bromic ether, hydrobramic ether. C,H,Br. mol wt IOt.9*. LMuid.C 22.04%. H 4.62%. Br 73.33%. CH,CA.Br. Mad* by di*- mir <Htilling from • mixture of HBr. ethyl alcohol and H.SO,: naaable wKamm. Marvel. Or» S>* aatt. ML L 2* (1941). By pnoa- unt Sopboru* and bromine method: Ooahorn «* al. ibid. 36, nn mnhiColorlea*. n*mmabla. volaoJe liq; ethereal odor, burning

mate; tianom** yellowuh on *»poaure to air and Hght. Vapor l*- *barmrul. df 01.4*12: df 1.4313. bp 3«.2*: Mumford. Pml- Prapd (roalipa, J. Cftem. See, 19*0, 75. SoiidiAM -119*. a* 1.4242. , alkali andAbaorption (pectrum: Hantach. aWr. SO, 619 (I923X Soly rida. fUviin water (g/100 g) at 0*: 1.067; KT a963; 20*: a9!4; MT: *«• O»nwa*96i muable with aloohoi. ether, chloroform and with *»"* Iother organic tolventa. Ezptooivc limila (% by vol m air). *ub*otuuolower 6.73. upper 11.23. Auuxgnition lamp 932T (31 I*C). ««i of 43-Lethal amwn for rat* in air; 20.000 ppm. Haarfaae* o/ToJu- ethyl aceuatloo ML l, W. S. Spector. Ed. (SauodM. Pbueoalphia, . vwyl accu1936) pp 336-337. - IcuachlorvHuman TtudcU* Irritating lo reapirmiory tract: narcotic <Maa "»"*

a* high ~—>~- - •rrnnhemMl: Eihylniiag aganl in organic lyntheaia; aa rafrigaraat. •. . wai InTMInAf CAT: •nnaiBiitm anaeimra" ' ' 37123703. Ethyl o-BfMobiilyratt. 3*tiwmatmlanaic atU Eucnlially

atAjrfaMT. C(H.,BcOy mol wt 193.06. C 36.94%. H 3.6*%. ' •ada (chaiBr 40.97%, O 16.40%. CH.CH.CHBrCOOCJi.. Pale-yellLiquid. dB 1.329. bp IT7-l7r with alighl dee. Inaol in '. . ' uwa. l«

water. muabU with alcohol, ether, ffotaa /ram UaM . . (chloralon370*. Ethyl a.Brnm.pfOilnaal*. ). »****+**«, ~ia "' • f ~*

atnjrf umr. CMM>j mol wt 1*1.04. C 3X17%. H SJ>I%.Br44.l4%.O ir6t%. CH,CHBrCOOCIHr J7i« ILiquid: (harp, mmganl odor; batciiie* yellow on exposure chlontbyl;

M tight d| 1.447. bp !39-l«<r. aUo dated aa 160-163*. *g chloric cU1.44*9. Into! in water, miaoble with alcahoi. ether. r>w*ct - AaatWtic

Maju. •'.., 7.11V a :

R R I Q Q i |2

»

S,

l.llO-tnmcth-anine. C—H,.-%. N 4.10%. O..) Schwmgg. *

or.: fnotot elfGadamer, Arch.Autt. J. Cn*m.

• 23, 12 (1961).'3D: Cullaad tttent. i*4 1939,r. Hubcr. W«/»Manske. Can. J.etani tt al. Ttt-Berczhinskaya tt(I96e). CA. 60,

Am. CWm. Soc. 72. 727 (1930): from bui.2-ynoic aod: Al-lan M ai. J. Cntm. Sec. 1933. ll«2. from CH.CH—CH-MgBr -t- COf Nominal. Mailla. Bull Soc. CJum. Ffaitct1936, 1439. Structure: Auwer*. Wisaebech. Btr 36. 713(1923): Plitov. Bogatskii. ZA, Oothch. Kktm. 27, 360 (1937).CA. 31. I340lc(l937).Liquid, bp, 33-36*; bpH 62-64'; bp . 161-169*. mp 13.3-

14.3*; crystallized from pen Lane, ng 1.4450. uv max (93%ethanot): 203.3 nm (« 13.300).Methyl eater. C,H,O_ liquid, bp IIr of 1.4173. uvx (93% ethanot): 203.3 am (« 14.000).

<** Wo1+*»* Benzyl eater. CuHuOr liquid. bpM I2l-I2r. af 1.3110.' Caution: Can cauae sever* irritation of akin, mucous

p 211-221*.S020.atnfit-l,+tif*minoai»tnanamintimt atfromiat; (1,4-fi-

1,4-bia(2-(benzyleihylamino)ethyl|piperazine diclhobro-mide; MW.bia(diethylamino*lbyl)ptpcrazioa bn(beazylbromide); MAT-bi*(dieihylamino*iliyl)pip*razine dibromo-benzylala; LBC 131 C-H BrjN.. mot wt 626.39. C37.31%. H (.04%, Br 23.51%. N *.94%. Prepn: Hazard Mai. Art*. Int. fharmaeoa'yn. 94, I (1933): Hazard er ai. Pr.pat. 1.093,977 (1933 to Lab*. Bruneau). CA. S3, I3l9h(1939). Qanglion Mocking aganl.

*'?:i2ar"

>]? +193* in

\a-,'.'' > Crystal, mp 219. r.

S02L Uocyaak Add. CHNO-, mol wt 43.03. C 27.91%.H 134%. N 3136%. O 37.19%. HN-C-O. Prepn fromiaocyaauric acid: Sleyennark. / O» CAem. 20, 3*6 (1963).

. . l Crystal itructura: Voa Oohlen. Carpenter. Afia Ciytl. t,

The free acid m the vapor phai* or in ether tola pv«a no**' acnoaa> a>&B\ • - ;~' ol bautc a mixture, and all the evidence lupport*•jKajT«»*« - • J»L ••«•• M, ^ w» W^WA • "•' *• —» •"• —— •" -™fr

^ iu'T- j*!**?! the i*o Mntctura. HNCO. wharea* in aq aoln cyanic.*»««' '3a! HOCN ia pnaeat: N. V. Sidgwick. 77M Cntmieol Slamena

*ro-J,f.J«.«rtV- *$j! anaf 7T»*t> Cwiipmuiett vat. I (Oxford, 1930) p 673.5022.

pound 7 II; experimental inaectkade no. 711. CuH.Q., mol*» '**»»• «= »•«*• H 121%. 0 3*.30%. Prepn: Lutov;Blueatone. UA pnta. 2.63377; 2 76,132 (1953. 1934 lo

Stntctun *M Aldrin which ia the tnCryMala. mp 24O-24r. LOM orally in male, female rate"

- 0.4 to <

I.JH>TaummatMfltamtana. CJiH iaSI%. Occur* in coal tar.

on 2 .6-uimethyl.Or, II. 66 (1931).

) 37.17%.*?dabydeiwill

""" llllllM 5024.

AbU-ta-«pMBtrairiene-3.l7d-diut; Ba-eatradiol: l-«pie*ira-diol: l-<*oeairadiol-170. CUHMO.; mol wt 272.37 C79.37%. H *.ll%, O 11.73%. >rapn by high pressure hydro-genation of dihydroaquiltn: Senni. Logemann. Btr. 71, U6(1931); by hydroganauoo of equilenin with Rancy nickel at2*00 D*I and tf. Deuban. Ahramjian. / m. CArm. Sac.7*. 633 (1936). Prepo of oV-form from aV-equilenio andsieraochemutry: Joaosoa tt al. ioioi BO, 6*1 (1931).

rf-Form. crystal* from oil methanol •+• chloroform, mpltl* W* •*•»«• (16 mg in 2 ml dioxane).3-Bcnzoaie. C_HMO> crystals from ethyl acetate, mp

I90T. [m\g >9.3*llfmg ia 2 ml dioxaae).4-Form. niidlai from dil - hantrt. mp 213.3-214*.

17-ant; 4UJ'l-«pt*airalnca-3-ol-l7-one; la-eatronc; IcpMBirooe. C HaOf mot wt 27tt36. C 79.96%. H a.20%.O 11.**%. Prepn: Serini. Logamaan. aVr. 71. 186 (1938);Johnson ti al. J. Am. Cntm. Sac BO, 661 (1931): A4iaochen.ko. Torgov. Tarantdron Lttttn IMS, 1333.

dl-Fom. priun* from mnhanol. mp 234-23T.4AMethyl ether. C..HJ.OF bladea from mcthaool. mp

e*/-Benxoata. CmH~Or priama from - ii- /o, mp 197-I9r.5026. tMMtknrinc. i,4-Dihta'r9xr*~(l'<uofnfrlami.

nolfrofjtjfmji alrakolf a-(l-i*opropylaminopropyl)pfou>-catechuyl alcohol; AMaopropyletaylnorepuicplinac. I-O.4-dibydroxypbenyl)-2-isopropylamino-1 -butaaol; ctyprena-Una; iaoetanne; Win 3046; Oilabroo; Neoi*uprd. C..HU-NO.: not wt 239.31. C 63.24%. H *.»%. N 3.13%. O20.06%. Prepn: Boclunuhl rr al. Gar. pat. 630.630 (1936 toI. O. Farben.). CMS*. 3209*(1937). Phaimneology: Laad*•I ai. J. fnarmaeol E*p. Tktr. 9*. 43 (1930k eidwn. / Am.

47. 744 (I93«).

Hydrochloride. C,.HaaNO.. Attnmalltan. Numotac.OryuiJ* from aMtbanol •»• athar. mp 212-21T (dec).TU»«»» /-»T- •m.ihndl'.lnr " •• •" •' ' ' <

5027. iMWSMai, 3-Matlta*f4.ft9ffn)lfntnut. 4-nydr-Liauid. dl a*96l: df* a*906. mp -24* OP..1979-. o»y-J-BMtho»y-l-propan»lban«aa)*s 4-propenylguaiacol."Jq<?=- jr™I*.4?V-*!r_ IM;I* to uTl- to <"»iHuOi: •>«* «* i*4.aa ,c 73.149*. H 7.37%. o 19.49%.

tTo1: toli77 O-jW 631n b«,l eflV nf °»*» » X"—*-*!-* •«! other easenOal eila. Prapd from»i.ir; >p. '/... Dp.mj... pp w.« na; -||-tl|o| h—b-g ^ ^ po,., W— .;. ^ c ./nd. St. 27S (IMOfc tmffi, Zn, Otaftcn. Xtum. 20, 2239(193*). Starannhaniiiirr vo» Auwera. far. 60. 1346(1933);Puxedda. llattu. Caw CUn. liaL 67, 647 (1937X ,

CamtmU J* cram U*to tifoM uttnf. ikii m&u. Pm«* 677n n i ? iVJ J I I- <->AR

07*141*,-. Forma blue *c4n in water: varyUa.alaohoL.wuh, a reddish brown

;;•»••. -.- .- w .UH: Solvent for

Hinds.THIftAf' CAT!5933. MathyleoedJpUk Add.

tytamtfU aci*7 C H..©-; mol wtH J.43%, O 43,42%. MadTby beaangid. formaldehyde and oil HO on the

'tMohaa C&, t~* •*•• ft matbylthioa": 'inToaina. chloruta; 3.7-bu<dimetkylamiao>-!c bri9K Swu* bluei CI. 52015; solventoiua7 CuH-QN i mol wt 373.90. C

-H 3.67%. Q U.09%. N 13.14%. S 10.03%. MayHh,3,f*nd3mot*H,0. Pint prapd byMunU/Mpd from dtmetnylanilina andH.|£V-Plan-David. L. Blangay. Fun,

prapd by Caro iaFunaamtnial

New York. 1949) p

j dark gisan odorleaa cryatala with bronxe lue-; powder. Abeorpoon max: 66*. 609 am. One

_[ diaadve* in about 25 ml water, about 63 ml alcohol;••mi b chloroform. Inaol ia ether. In aq solo it i* decolorizedf byZa duet and dil H.SO* but color ia reatored oa exposure\ ai.aw.aad a»ore rapidly upon addn ol NH.OH. Forma dou-

: salt*. Intompat; Camtic al-, i__ _ a*, reducing agent*.

_ ),». foe•-. Slain in bacteriology; reagent for teveral <——•'•••;'* lit Mixed indicator*; a* oxidation -reduction indicaior.

CAT: Anrimeihemoglobinenuc; antidote (cyanide).CAT (vent Antiseptic. dJaJntactani. antidote for

' cyanide-end ailrata poisoning*.~ Ditfemommhnn*.

»?»M wt 173.16. C 6.91%. H 1.16%. Br 91.93%. Prepn:>*£ rbrtmaa. Drager. O>* 3>» eatt. »**. I. 337 (1941). Manuff~ - •long with bromochloromelhaae. from dichloromelhaae:

"* '- Lake. Aaadonsn, UJS. pat. 24*341* (1951 to Dow).7 ;T15uid. bp 9T. mp-317*. df 1495*. ng 1.3419. Soly•'. (g/IOOO g water): 11.70 (15*): 11.93 (JOT). Miadbte with

'-"- •• 5*3L a-Melhyleae Batyralacton*. «.3>D<ayaVe.J»,i-rmatnfltn».J(JH>-jfurmnona. CJHJOf met wt 9*. 10. C'l»Ul%.H 6.17%. 03162%. Isola from aq extract* of Sry; Innnlum mmtriean»m Her.. Ullattat (dogtooth violet):

Ckvalttko. rUskdl. / Am. OWm. Soc. 60. 2332 (1944X'r< '•» «i.• * »J.

"Liquid. Polymsriiai eaaily whan heated above TO*, bp,S7-60T. Sol in WM«. pH 4 (130 mg/ml). The lacuna ia

in ail part* of tha plant and can be extracted eaaily, r—— •*•;•• with water, but Ml with ethano!, ether, ethyl acetate.. i! aalgroloiBi. Canrinsv Irritating lo the akin.

or

2*i-Diaiiropbanylbydradae derivativa. €, ,0,, red•rywala from athanci. dee 190-I9T.5*32. Mntfcylnn Calorlan. " tMtnlommttnnnt, methylene

rtkaluiiJe. MlhytaM bichloride. CH.Q,; met wi *4.94. C14.14%. H 137%. Q $3,49%. Prepn by ehlorinelioa at

Lukes at oL U4V pat. 2,7*2.433 (1957 to Dia-mono Alkaak PUk Better. US. pat. 237*441 (19*1 toStauffark Burkh. Obrecat. UA. pat. 3.124.419 (19*4 toSlauftar).

; vapor ia notwith air is MI explaeive. bp,., ».1T. Solidil -93*. d)1.36174; df 1.33479; df 1.3253; df 1.30777. iff 1.4244.*ol in about 30 pan* WMV. •iaetbt* wwh ale. - " '

U>_ orally in rala (young adultah 1.6 ml/kg.

Inaol in cold, sparingly ia hot water, sol in alco-

MethylanadiaalkyUc Acid. AJ--Ma^/tawaonioit ecie**; 4.4'-dihydroaydipbenylmeth-

ane-3.3'-dicarboxylic edd. C-.H-jO mol wt 2M.2S. C6130%. H 4.20%. O 33.30%. pVepd from salicylic aod andformaldehyde in the p res mce ol sulfuric acid: Oemm*n*en,Heiiman. J. Am. Cntm. Sec. 13. 737 (I911X

COON

'•£^!-?M

Wedge-like cryst from aonoBe •+• baazeae. Bitter taste.Dec 231* (highcr-mdung material may b* impure). Turn*red at !M* and atana giving off COr Frady sol in metha-noU cthanoi. ether, acetone, glacial acetic add. Very slightlysol ia not water. Practically inaol in hennne. chloroform.

Badtracin salt. «w Badlraaa Mcthylenediaalicylk Acid.Diacetyl denv, C»HMO,(CH,CO)r while powder, mp

142*. practically inaoTtn water, sol in-acetone, cihanoi.5*35. Methyles* Udida. DiicdamMeae, CH,Jr mol wi

267.17. C 4.4*%, H 073%. I 94.76%. Prapd by the raduc-lion of iodoterm with sodium anemic Adam*. Marvel. Off.Sim. vai. t. p 37 (1921). Also by beating iodoform withsodium acetate in alcohoi; Bagnara. Sna, Mininm J. frmt116, 51 (1923).Very heavy, highly refractive liq. Piers-an* oa exposure to

light, air. aod moisture, df 3.32337. SoUdMtea in leaflet* at3.2* or in thin nsedlai at 3.7*. Usually cooling to 0* i* aacea-sary la wart cryatn. mp 6.0*. bp KI-. bp. IOT; bp,. 6T.a*i 1.7359; ng 1.7425. ViMOdlytn oaatipoiM*: 3.3sVlOO:1*0 O0*k 13*(30*). AtMorpuoa tpactrum: Lowry. Saaa. J.Cntm. Sec. 1*24, 624; Siepnnov. Acta Htfakoehim. UKSS20. 174 (1945). Sol in about 70 part* water, aviadble withalcohol, propanol. iaopropanot. hcxana. cydoheiane, ether.chWoform. benzene. CH,I, duaolvea sulfur and phoapoorua(more than 1:1 ai 230.Ua: In sepantiag m.zture* d minerato. In determining

the spedlic gravity ol minerals and other mbiiancei, U themanufactura ol x-ray contrast lasrtia593*.

ylamiao.|-phenylpropanai:ylnorephedrin* Cj nMOt mol wt 179.25. C 73.70%. H9.36%. N 7.11%. O 193%. bate of Man* from ffnefraaUaacAvaL. (X. tlgon* Rich.k and alhed fjnuanear Smith.J. Cntm. Sac. 1*27. 205*; Wolfes. Arc*, fnann. 260, 327(1930). Prepn d Monn: Smith, let. eiL.-at af-. *-. and 4t-forma, aad rceoluuoa of rammiti mixture: Nagai. *——Ann. 470. 157 (1929k of aU-forai: PUnz. Muller. Arc*.

—— ""'Ml ( A R I Q Q I 2 1 ;««•(€»,),

tt oL Toueoi AffL fnarmacol 19. 699 (I97IX

CfcunJf AtttamimmaM mt/an aiiag tkit maiam. fmaa 7*1

2,4'DUMcytMta

103-106*. frantically iaaot hi water. Ml inpropytene glyeafc Invited

LDM orally in ratai MOmg/kg.

\>peridiao-2.a»ethyI-3-<>tolyl>.3-propaao8a;Vpiparidlno-1 -f totylprnpaa-1 -one; mydetooc.•Zolwt 243.33. C 7*.32%. H 9,43%. N 5.71%. Oepai. Xadc* at ai. Huaa. pat. 1444*7 (1936kmoL *-f— P**- 304MC6C) (to Eisai). Phar-Pomez it al. ncm PAjoiot Acorn. Sd. Hunt, 10,Aamalmlntl-Foneh. U. 237 (1961X

•".'.An-T..;•«*.*'"* i :b"W*J.>a*,../.*.'"4-ifK.'-Irochloride. C H-ONO. N-S3J. Mnaoalia. M^ttmlmjit from methyl ethyl katoaa. mp 176-ITT. LD, ia•620 arng/kg »A•AT CAT: lit ami muade rdaxaat.ml. Tolpariaaaa "M. l-C Iodo-l»1l-batzylpolyeth-I 1 nmnliiaanar iortiaaiart totuidine polyviayipyr-

dio-«dinated («»*1) ' ~

ra«'fneBt*a-ael; l-<2-methylpheBXixy>-3Hperirtajno)-2-propnnol; Ml.l3.6-tetrahydropyridiao)-3

£fDtBeranoal fli**anan ol aourc* ol by]

922L TalKMlna. J.a.OiayaVa .fin. mer»jf>n«nev»»>.-<3-

• satyloxypropaa.2 1; l-a»-p«peridino-3-».to*oxypcopao-%9Bi;.«-A>-pip*ridiao-f-hydroxy-Y-»toloxypropane; Pro*pnanii CuJHn>40J; mol wt 247.3X C 71*4%. H a.36%. NP*V%7oi£94%\ Prapa: Beaaley tt at, JL Mann, fhormo-ml 10.47 (I93»k Brit pat. 0*0470 oomap to Berger. Lud-Iwlc. UX pat. 14004M (1961 1**X both la Carter Prod*.).

, .Hydroehlorida. CvH aNO, cryMala. daa I3*>l37.r.

•oar tana. Pro-ay tol ia water. pH ol a 10% aq note about3.1. Aa Mia* an *Ub*e to beat, bat ••itiHi la acida aad•tkaliea. LO.Lp.ka-immhfaat •--'-

3-dia*MB ylaaiiao-l-ph4«V>-l->t«iylpr«PMia; Pragma*:Tyiagd. CMH.N: jaot wt 253.37. C *SJ2%. H 9.13%. N5.33%.Hnecaaik Klosa. / front. Cnam. 34, f 12 (19*6). Phanaa-

Saadrall. Olaiaea. Tktroftt IS, 119 (I960).

Hydrochtoride, CuHaN.HO. mp 1*2- 1*4*.TMBJLA* CAT Toptcal iBrihiilaminii aadpruritic.9223. •>Tan*al4*ny4a >Mntn*M«uaUrtjrfe; e-toluyl-

•Idehyda. C O, mat wt 12ai4. C 79.97%. H 6.71%. O13.32%. Prapd by reacting aitropropaae with e-xytyt bro-Or» 5/» 30, 9* (1930).

Liquid, df 1.03*6. bp . 20O-2Or. bp_ 94.96*: bp, 64-7T. ng 1.343ft a|> 1.149; af 1.3423; af 1.363ft a» 1.579*.9224. ••TlaniBilii >MeMv<taiuaaiia«. CJVKX mol

wt 135.16. C 71.09%. H 6.71%. N ia3*%.O lt.*4%. Prapdby raectiag eMoluaitrile. hydrogen peroiide. 95% alcohol.and sodium hydroxide at 40-50T: Noller. Or» Sfn. ceil. *ai.U. 516 (1943). Caution: Keep away from open dame. Anexplosion occurred during thia prepa when the tamp roteabove 50*. Alao prepared by reacting the nitrite with boronfluoride in dil acetic acid: Hauaer, HorTaaberg. / Org.Chem. 20, 144* (1933).

Crystal* from water, mp 144-145*. Very sol ia alcohol.hot water, coned Hd. lea* sol in ether. Sparingly tol inbeazaaa; practically ia*oi in cold water.•225. Tainan. MatAylietumc toluol: phenytanethane;

Methadda. CjH mol wt 9113. C 91.25%, H a.73%. Ob-

i-like odor, df O.16*.Solidtf -93*; bp 110.6*; »g 1.4967. Flaah pt 6-10*. Vvy•lightly sol ia water, miaable with ale. rhtornlnnB. ether.

glndal ac«ic acid, carbon diaulfida. LD, orally iarara: 7.53 ml/kg. Smyth M al. Am. Inm. K/g. Amnc. J. 30.470 (19*9).

USa: la mania* baainir acid, baaialdehyd*, expioeivm.dyee, aad away oiber organic eompda; alao aa a solvent iathe aatncraaa of vane is* principle* from plant*. Ciuiion:May cause asild •acraeytjc anemia bat not laukoneal*. ' 1aU*Hft waaW4*9 tiwatfl k*awlAnwaV*L NAfOOUaC mm mMntlm OOwMttaVt B* I I

Browwiag. Taaidiy ana* UttnaoUtm a/ Inmuuhat Sohna Jj . }(BlaavMV. New York. I9*i) pp 66-76. JH {•22C Talnaae 2,4-DUaacyaaata. 14-Duaocyanaiotolu-

*J*f£!2!L,'!3J*'%r'*. __ __. —.._...,-.1 37%. Uaually prapd from toluenc-14-diaasiac and phos- "! -I j i I

2 tolyleae dnaocyaaala; TDI: Naccoaaie I0a C.H.-N.O.; mot wt 174.13. C 6107%. H 3.47%, N 16.09%. O

AR I 00125Liquid at room temperature. Sharp. puagBM odor, mp

19.3-21.3*. df bq 1.2244. bp 251*; bp,, 126*. Darken* oa— ' lo lunighl React* with water with evolutioa of

I Imii

i!geae ia a •oiveal. tuck at a ichJorobeanae or toluene.Numerou* patatu. 4*U»*n»r Aatla. Imtmfthal Orfanit Nitre- JJ-. Ui<ea Canyoaaawfrlew York. 19*1) pa 234-3IX

\.I j

UM Carbon Saboxid*frtoarmiirt Inorganic Cntmatfy vet. t, G. Brauer. Ed. (Aca-demic Press. New York. 2nd ad.. 1963) p 646. Review oftoxic effect* in human*: Stcw*n. Ann. Rt*. Biocntm. 15,409-423 (1973).Highly prmonoua. odorless, colorless, tasteless gas- v*ry

flammable. bums in air with a bright blue flame. Ignition ptin air: 700*. mp -203.0*. bp- 191.5* d,-"* (liq) 0.114. dd,-"

: 1.2(gaa) 0.9** (air - 1.000). dj at 7*0 mm: 1.230 §/liter. Thetop pfssiur* i* 1300 pii. Flammable limn* w *ir: 12 to 73vol %. Cnl ores* 33 Mm. oil lamp —139*. Heal capacityat 20*: 6.93 cal/mole/*C Heal value per m*: 3033 kcatHeat of formation: - 26.39 kcal/mol. Dac into carbon tadcarbon dioxide bsi«sen 400 aad 700*. at lower tamp when iacontact with catalytic surface*. Above BOOT the equilibriumreaction lavora CO formation. Hopcalite. a mixture of theoxide* of manganese and copper, catalyse* the decompn atroom lamp, aa does Pd on ultca gd. Sparingly tot ia water:3.3 ml/100 ml Hf> at QT. 13 ml/100 ml H,O at 20T-. treatyabsorbed by a coned sain of cuprous chloride in HO or inNH,OH. Appreciably sol in some organic solvents, such aaethyl acetate. CHQ. acetic acid. The soly in methane! aadethanol i* about 7 tune* aa great aa the soly in water.Mli Aa reducing agent in metallurgical operation* **paa-

*Uy in the Mood proem* for the recovery of nickd: in or-ganic *yathaa* especially ia the Fi»cher-Trop*ch procetieifor petroleum-type product* aad ia the oxo reaction: ia themanuf of metal carbonyla. Caution: Combine* with thehemoglobin of the Wood lo form carboxybemoglobia whichi* unltii w an oxygen earner. Toxic *vmpio«iuv Headache,mental dullness, di-nines weakness, nausea, vomitiag. lo**ol muacular control, increased then decreased pulse and

, ' reapiratory rale*. ooUapea. unconsoouaoess. omth. Anudota:Oxygoi.

1*20. Carbon Sahexid*. Tricarboa dioxide. C.O.; molwi 61.03. C 3196%. O 47.04%. O-C-C-C-O Prapn

; • by thermal dacompa of malomc sod: Glcmscr ia Handbooki{ of frtporoti* Inorganic Chtmuuy. voL 1. G. Brauer. Ed.-, . -r- -- - -. .

(Academic Pr***. New York. 2nd ed.. 1963) p 641. Raac-• f. (Academic fres*. New Torn. 2nd so.. iveJi p MB. ncec-t f lion* ia organic lyntheais: Daankcvicb. Balm. Xua, Chtm.

T X". 36, 391 (1967). Campr*Acnnv* review*: fUyenan.Kobe. Chtm. ««•* 7. 479 (19JO). VoTkcoshlcin. UtftU

I Khim. 4. 610 (1933k Orauer. Cnimia 14, 11 (1960).Colorless, highly rafrmctive liquid or colorless gas which

•* bums with a blue, sooty flame. Odor like acrolein and mua-• inrdcil. mp-lll.r. bp ,*.!* dll.114. H, 1.43314; a u< 1.46737. Vapor pressure al 0*: 317-319 mm. Explosive

I limit*. 6 to 30 vol % in air. Dtpoie moment: 0.7D. Ther-modynamic constants: Thompson. TVanx. Faraday Sac 37,

J , 249 (1941). The ga* can be stored at pressures of up lo 100mm. but even at these pressures potymcnzauoo may occur.

X ' giving a red. waicr-eot product. Thi* invariably occur* al* I higlMr [••nut or ia_lha liquid Male. Polymerization faol-

itated by pnaeaot of P,O,. Dec when passed through healedglee* tuba*, terming a mirror surface. Difficultly tot iacarbon rtsnilflftt ijlaat With water form* anlnair addquaatiianvdy. Fonat mtloaamirl* withUU: Prapa m milnati*r iatproviag dye affinity of ftban.

~ a lacrijaasar; ia " B*1*

U21.Car.eaT.Nacatoria*; Baaiianfona.- . CO^ mol wt

IJ } ty. B. Browaiag. Tt11 MWtflatwwr. »«a«

Toxactty mum mttaaolam o/lnduarial Set-- York. 1963) pp 173-111.

t oa odor, at 1.5**. bp 7*.r. Soiidifia* at -IT. af 1.4607.One aa aCdva* ia 2000 -ml water, misobs* with ilmhol,

a. ether, carbon ditulne*. pairlor mice ia ain> about 10.000 ppav

Uurno* Toaidqr -Poiaooing by mhalarirm,

liv« Mtjunt., Caa ha niul.

but kidney taiury and visual disturbance* also occur. Skincontact can lead to dermatitis through detailing avtioa,Cauisaa; Aloohol intensifies action.UU: A* fire cxtinguubar; (or daaning clothing; rendering

banzui nonflammable; aa azaotropic drying agent for wetspark plug* ia automobilca; a* tolwmi for oils. fat*, lacquers.vamnhm, rubber waxes, reaiai; extracting oil from flower*.lasdi; eaicnniaaiing destructive uuect*; solvent: startingmaterial m manuf of many organic compda. Cantasa.- Mayform phosgene when uaad to put out a"anneal are*. Urnonlf wmm aalafuaie »ea<i<eiiaa oj rttf'rliTMIBAI* CAT: Anthdmiauc.THUUr CAT (VBT): Aathelmiauc.1022. Canaa Tetnllaorld*. TdraAuaramethanc; Frc-

oa-14. CFV mol wt 11.01. C 13.65%. P 16.33%. Prepdfrom carbon or carbon mono side and lluorias. Yo*i. Inarm,Syn. 1. 34 (1939); Simon*. Block. / Am. Cntm. Soc. 61. 2962(1939k Kwaaaik ia Handbook a/ frtporea*t InorganicChtmiurf vet 1. O. Brauer. Ed. (Academic Press. NewYork. 2nd an,. 1963) p 203. May alto ha prepd from S.C P Prieat. Inarm, Svn. X 171 (1930).Cotorleii. odorleM gaa. Thermally (table. Chemically

••'!»- -«*.'

very man. d (solid. -195*) 1.9*. d Qiq. -113*) 1.19. mp u-113.6*. bp -I27.r. May be Morad m sted cylinders, -.?,%UU: Low Ump rdrigeraau guaou* iaaulalor. Caution: .<£

Narcotic in high coacaa. ^U23, Carwaaj Tdntodiae. d.; mol wt 519.65. C 2.31%, 7&

t 97.69%. Prapd by the interaction of carbon ictrachlond* ..'.-aad aluminum or calcium iodide: Ouatavioa. Aitn. 172, 173 '-'(1174k boron iodide: Moiasaa. CompL Head. 113. 19(1191k lithium or calcium iodide: Laateaoi*. ibid 136, 1313(1913k ethyl iodide ia the prmmce of aluminum chloride:Walker. J. Chtm. Sec. IS, 1090 (!9O4k McArthur. Simona.Inarm. Sfn. 3, 37 (1930). -'. f*Red cubic crystals. Odor of iodine. Dec to iodine and 4 •

latniodaathyleBC under the influence of light or haac. df • '"4.31 mp 171*. Sol ia benzene, chloroform. Die by but si. «&eohol. Practically inaol ia water, but hydrotyaa* slowly ia ,,"aoaiact with water, formiag iodoform Mid iodine. •? • •'%

1C24. N.'V-CarboBylaUaildaxale. t.r.Carboaylbi»? "nI M-iaudazola. CrH.N.0. mot wt 1*2,1 J. C 3I.*3%. r!3.73%. N 34.36%. O 9.17%. Prepd from phosgene sod——taWa-MOwC IB <4fy ntfnaliyitfofan'n oc dry bvtiataw: Si«h> 'fAnn, 609. 73 (1937k Andenon. Paul. / Am. Chtm. Sac, BU, - V4423(1951). . -,/

»ir\ /»»l \ / IL/-- Q

:-M•Mm"V*

Crystal* from tatraaydrofuraa or baaaeae. mp M 3.3-116, Should be h-M'-il uadar sidudon of tuaoephenc moisture.'HydfOlyiad by watar ia a few sec with evoiuuon of COy'Ual: U ttt* *yaib*au of ptptidn. Kaacu readily

?*$

bagyfic qjojof to lorat acyl iasidaaDleB; *ubaeau atwith aaunaa to form amidsa fjom ataoothly.

1*95. Caftaayt FlawtaW. Carteayl difluoride; nuopho*''-.. CF.O; moi wt 66.01. C 11.19%. F 37.57%. O 24.24%,-*V Prapd tram CO tad F. or BrF, and CO-. Ruff. Mfltiazky. Z. Anorg. Attaem. Cntm. 231, 154 (1935k KwataiKe)

13XM. C 7.«1%. Q »2.t»%. Obtaiaad fro. ceraoa dleul. to Oanmaaok o/frmomrntl* Inorganic O*mm*r*. *wL VQ"fid* Md efetanat ia prmanci of • catalyat. *.g- SaC Fa Hrmutr m-t (Zend*JBn Ti a»kI4ewYora. 2nd ed |96J) rfUiao. or by in* chlorinalioa of hydrocarboaa: HardM ia *n"Mt' ** ^tuamtr "•»• N<w Tanu •»a «• * '-*«

- tfmfttaaftia a/ Cmtmiaml Technology vaL *New Yon. 2nd ed. I9o4) pf 132-134, Toad-

. : l*W*2*a Cta-llifctt

206. Altaraati ram* from OO + AgF.; Pariow tt al.art.Syn.4. 135 (I960). - ' I ' "* ttPucgaxt. ««ry hygroacopic gaa. d (*olid. -190*): 'iSaal

dOK|,-H4*): 1.13*. mp-114.0*. bp -*3.r-HcafMforauooa: 166.6 kcal. laataatly.kydrolyMd by wat<3Ctsiftoa.* A ttroag initial to akin, eye*, itaoma membraor-_~ 7 ~ — —— •* . ». • f.oti it * • _.*.fc».einipliiioii tnct.

<JUtoTwVaWlVVf)fM*9jlWatft%ll/ »QLO> fmmfmljt mntm^ .WIC WO*1phanyOthio)akethyi| qOdUthyl phoaphoroaitbinste;X3lO-diathyl S4f Bhlorophanylthio)mdhyl photphoradithiciag:R 1303; <3an n*»a 1Mlh*oa. .H341*5. C 34.531*. H 441%. Q 4IU*%, I

A R I O O I 2 S

•193 NFredy kot in water (40 g dissolve in 100 ml) and in alcohol.

| Slightly 10! in chloroform; insot in banirne, ether. A 1% eqj sola has a pH ol about 6.1 LDm s.c. ia rats: 3*3 sag/kg.i TMUA* CAT: AdrcncrgK (vaaoconslnctor).

•193. Naphthacea*. T*trac*ae: 2.3-benzanthractnc;

thracea* to which a impart* a yellow color. Itoia: Cook ttai. free. XOK Sac London Bill. 433 (1932). laotn fromcrude aathrarani by chromatography: Wiaianteio tt ai. Z.Htyuol Chtm. 230, 139 (1934). Syntbcau) by coadeniingtuocinic *ad and phihalic anhydride ia the prate-ire ol aodi-urn acetate: Gabrid. Michael. Btr. 10, 1359. 2207 (1177k

\i 1L 1612 (1171); Rcaer. Btr. 17. 2744 (1*14); Naihaaton.[*t Mar. 24, 2512 (1193k Oabnd. Leupold. Btr. 31. 1139. 1272

(1191k Waaag. Btr. 70. 274 (1937k from l-oaphlhot andphihalic anhydride: Deichlcr. Weumana. Btr. 36, 347. 719(1903k Gar. pal. 2*0443 (1916); from 1.5-dihydroxynaph-thalene and phthalic anhydride: Bentley tt al. J. Chtm. Sac•1, 411. 1311 (1907); from letralia and phthalic anhydride:Schrocicr. Btr. 34. 2242 (1921). Gar. pal. 346.673 (1911); c/Fiasar. J. Am. Chtm. Sec 53, 2329 (1931). Other lynlheaca:Coulson. J. Chtm. Sec. 1933. 77; Wdanana tt al. ibid. 1*3*.39*.

Orange leaflet* from xylcne. d 1.35. Sublime* In tamo.mp 341* (open capillary tube), mp 357* (copper Mock).Absorption spectrum: Oar. Btr. 69, 607 (1936). Fluores-cence maxima: Knshmaa. Sanaa. Z Knu. 0*. 331 (1934).Difficultly *ol ia tno*l solvent*. Solas show slight greenfluoreaance ia daylight. Doe* aot form a picrala,•194. Naaathalea*. Naphthalin; aaphthanc; tar cam-

phor. C«H mol wt 121.16. C 93.71%. H 6.29%. MoatsrmnrtinT angle constituent of coal tar. Dry coal tar eon-lain* about 11%. Crystallize* from the middle or "carbolicoil" fraction of the distilled tar. Purified by hot prsaang,which may be followed by washing with H4O, NaOH. aadwater, then by fractional distillation or by sublimation.Review and bibliography (173 pages): Rood tiai. Thetmt'tCnenonoiy a/Afflled CWmiavyS, 263 (1947).

i}

Moaoctiaic priamatic plate* from ether or by ialao *oid a* whit* srslai powder, ball*, or cake*, mp 10.2*.Odor of raoth bell*. Volatiluaa appracsaMy al room lamp.df 1.161 df 0.9*2*. Subumas appreciably at temps abovemp« volatile with ateam. bp,. 217.9*; bp— 193.21 bp,.167.r. bpM. 145.3*; bp. l30.2Ybp-ll9.r, bp, 101.7*; bp_.13 r. Ftaeh pc opaa oup 174T O9*Ck do**d cup 19O*P

Ay-ling-**-— tamp I05JT (567*O. nf 1.3*211i ia Kg light (pew ether tola). Vllravioiet

riiticba ' ' -—- -aaeorpooa: Several characteristic band* tierw*an 217.5 aad320 am la hexana. fatal hi water. Oae graaa disaorve* ia 13

I or etkaaol. ia 3.3 ml benzene or toluene, ia •ml olive oil or nirpaaone. in 2 mi chloroform ar carboalamchlonda. ia 1.2 ml carbon dnmlfida. Very mat m «k«_tovAt oBo%Botin ommmmmmm ttt aaaVfld eMb4a! VQaaftlaaiat Qalswa

Human Tanlcuye Postoaiag may occur by an*trina ollatgm do***. uit~'"'— o> skia abaorpooa. Symptom* •netatgnx- aautea. voaalang. limltrhi, ilitphnr*Bii bamaturia.besaotytic tanalt fever, hepatic aacroda. ooavaldoaa.

Maaiaf phthalic and

^go. ladaaikreaa. aad irifhtnilaiTthini dye*.

Maaul of hydro*)** (atphihnltX uaiao (naehtbyiaauactXtuafoaic add aad ttmUot compda utad ia Ik* dye tadisurie*.MaaiaJ of syataetic raraaa, cdluloid. lampblartr. •aohdatapowder. .Mania* of hydronapklkalaae* CTetralin. Daealia)

~ ' « uaed aa tolvenia. la lubricants, tad ia motor fuda.

_ -«u"Maaial of syataatic radaa. cdluloid. lampblartr. •aokdaai •—- - —— , . , , >ia.,, a-J

- - - - ' ' ' Bea (Tetralin, _ __ __ _mot wt 211.30. C 41.66%. H IKM

Tha us* of aapnthalene aa a moth rcpdlcnt and insecticidedecreasing due to the latroducuca of calonnaMI comesuch aa t rlirhlnrohennnsTHtftAT CAT: Anuaepuc (topical aod tatcaiinal): antb,

61*5. l-Naphthaleaeacetic Ada*. .-Naphthalcacaceacid; naphihylacctic acid; NAA; Plaaolix. C..HUO. mol1*6.20. C 77.40%. H 5.41%, O 17.11%. p£pant!on lr(naphthalene -t- caloroacetic acid: Ogata. Ishiguro. / AChtm. Sec. 71 4302 (1950k Souihwick tt ai. ibuL 76, 7(1934); UA pat. 2.633431 (1953 to Food MachineryChemicals); from aaphihylaoetoailrilc: Wanner. U i p2.40*440 (1949 10 Hoflmann-La Rocaek J. Org. Chtm.54* (1930).

CMjCOOM

from water, mp 134.5-133.5*. Sol ia aboutpart* alcohol: fredy Ml in acetone, ether, chloroform. &ia water at IT: a31 g/1. LD, orally in nit: approxg/kg. Handbook of Toxicology vat. 1, W S. Spector. I(Sauaden. Philartriphia. 1936) pp 201-209.Ml: To promote rooting of plant dipping*. ]•194. l.l-Napathaleaadiamiae. l.l-Di*miaoo*phti

leoe. C H.N.. mot wt Ue.20. C 73.92%. H 6.37%.17.71%. Prepd by reduciag l.l-diailronapbihalca* wphospbonu triiodide: Meyer. Muller. Btr. 30. 773 (US

Cryaial* from dil ale, mp 66.3*. bpu 20r; <.*•• I.Mdj" 1.1265. Subiimable. Tun* brown on Handing. Sol*ia alcohol or ether, slightly sol ia water or chloroform..Dihydrochlorida. CJlaajNr leaflet*, mp 2MT. ',;,UTft Aalioaidaal for lubncaling oua. Dnecttoa ol •

aium and nitrite*. . •• ' ;61*7. U-Naphthaleaen aifoak Add. Ewer-Pick a<

CH.0,8,; mol wt 211.30. C 41.66%. H 2.10%, O 33.30*22724%. Prepn: Fien-David. Healer, fitl*. (Mm. Aat1134(1923). •><

CryMala. Vary *ol ia water. *oi ia alcohok pncoaiatol ia ether. r ••'6190, 2,*-Naphth«lea«eU*alfoaic Add. Ebcrt.M

0-add. C-H.O.S,; mot wt 2**.3a C 41.66%. H 1IOK33.30%. S 2124%. Prapa: Ften-David. Rich to. iCam*, Acta 20, 257 (1943).

»ejj

Vary *ol ia water, aloohol; practie

A R I O Q I 2 7

•90S TcmchJom«taiazidetil* tongue, mp 147-1 SO*. Sol in 7 pans water, in alcohol;inaol in ether, benzene. The aq ioln is neutral to litmus. Aqtola* are stable aod may be itcnlized by bnd baling. LDMi.p. ia mice: 70 mg/kg, Dawes. Bra. J. Pharmatoi Chtmo-thtf. 1. 90(1946).THUUS CAT: Local *n**thettc.THUU* CAT <v(D: Topical anesthetic.1905. Tetrachloraietmiazia*. t-Chloro-3.4-4ihfdro-

tnchloromtthfi- iH' 1,2,4- btniolhiadiatinf 7.,ul/onamidt1,1-diotidt; 6-chloro-3,4-dihydro-7-sulf*moyl-3-trichloro-mcthyl-24V-l,14-benzolhiadiazine 1.1-dioxide; 3-trichloro-

! mcthylhydrochioroihiazide; teclothiazide. PS 207; K 33:4 Dcplcd. Cd.N.O.S,. mol wi 413.13. C 23.13%. H| 1.70%. Q 34.17%. N 10.12%. O 13.42%. S 13.43%. Prepn:

Ooee tt al. J. Am. Chtm. Sec. 11 1132 (I960); Novdlo ttal. J. Org. Chtm. 23. 970 (1960).

i!

. ('

. .|

jlj :

cr •

Crystal*, mp 300-3O3* (Ooaek mp 217* (Novdlo).TMBAf CAT. Diureoc.I MX. Tttrachlaroalkaa*. l,l.2.t*TatrmtMlorotthont;

•rnctelrachloroethaac; acetylene tetrachloride; Cdlon:Bonofona. C.H.C*,; mot wt 167.16. C 14.31%. H 1.20%. a14.49%. a,CHCHar Maauf by catalytic addition of chlo-rine lo acetylene: Peter*. Neumann. Aitgtw. Chtm. 43, 261

k i; (1932k by chloriaaiioo of ethylene: Pye. U.S. pat 2.732,402- •' (193* to Dowk by catalytic cblorinaiioa of ethane: Joseph.

U.S. pat. 1731401 (1956 lo Dowk by cUorioaitoo of 1.2-dichloroethane: Conrad. U.S. pat. 2,723.413 (1953 to EthylCorp.); Fox. U.S. pat. 2446.404 (1931 to Moaiaaio). Tox-idly: B. Browning. Toxicur and Mttobolam of InduitrimiSWwnii(Ela*vMr. New York. 19*5) pp 220-229.Nonflammable, heavy, mobile liquid. Sweetish, suffocat-

ing, chloroform-lika odor, df 1.5165*. mp -44*. bo*,I4*.5*. af 1.49419. Very sparingly *ol ia water. At 25* onegram ditaolve* ia 330 ml ICJO. MitdMe with mcthanol. eth-

•tasttV* IMtf •Ctt-tft CM bUU lettfBCiyOfidnV CiklO*

diaulfld*. dimcthytfonnaauda. oil*. Ha* thehighest solvent power of the chlorinated hydrocarbon*.

•olveat for fal*. oila. waxes, retina.cdluhM* acetate, rubber, copal, phosphorus, sulfur. Aa sol-vent in certain type* of Friedd-Craft* rear, linn* or phihalicanhydride condensations. Ia the maauf ol paint, vanush.aad mat remover*. Ia soil itarikzauoa and weed killer andinsecticide formulation*, la the determination of thaooro-mine in cacao. A* inunanion fluid ia cryttallograpby. lathe biologicd laboratory to produce pathological changat iagaatroiaieauad tract, b'ver. aad kidney*. lalermadiate ia themaauf of irichloroathyiane tad other rhlorintied hydrocar-bon* having two carbon

poiaoa. ForFarcbJoraetkylaa*t cthyleae

Idrafhlnriilar latrachlorathyleae; Ntmtr Tetncap; Tetronsk- - - . - . - - - - - OM| wt 165.15. C14.40%. Q M.52%. QjC-CO/ Praprt ky Faraday ia

|K 1*21, Manaf by aatalytM aaidattoa of 1.14 -tatnchloro--" -- — ••-• • " —— "• - *•••••'••''"-«*-—. "• r-f I Oa)IUfl *nBV«SOUt*n**BVni CaaWnaWX •"' •(aataVtV art

!< , MOMOO (19*2 to- Pituburgh Plata Ottaak by catalyticchlori«*rloa f tadylMr TaaraMt, Parvi, UJL pat. 2430,-•31 (19*0 w tadal* d'tlain m liaiii*. .d'Otctnai aiallurgie el

aMJCtrique* dOJgine).bleUqTetaaraaJ odon'df 1.6311; df

1.6230. .bp 121', Soadif abotu -22*. *f 1.5055: Mumford.PkiUlpa. J. CnmmTSml'tftm, 75. .SoJ ia about 10400 volwaian araidnfa with'alcbkoL ether, chloroform, heaian*

, orally hi mjottt t*5 g/kc lethal ooaca for auce in air.ppak Hmmdleeli o/Tmrtnttmy <at I, W. S. Spector. Ed.

(Sauadan. Pttilidalpaii, 1*56) pp 290-293. 350-351Human TmxteHp Narcotic la high <

i lend to dermatib*.•aetala; wlvtat.

TMUA> CAT: Anlhdmiaitc (hookworm* andi).

TMCBA4- CAT tvm: Anthdminiic.1900. TcovcbJoroitopaltuloaitrll*. 2,<j> Tmrachlefm.

f .J- btnttntdicarbonUnU; I.3-dicyano-2.4.3.6-letraehwI.,———— «"" 1717; Oaconil; Forturf: TarauL^^^mol wi 263.19. C 36.13%. Q 53.33%, N 10.53%Batlenhdl tt al. Fr. pet. 14*7421 (1965 to fv,,kali). CA. 63. 4212c (1963k Minoni Taahiro Tjaawl"pat. 224*9('60> (lo Show* Daako). CA. 70, 7ll«9y(l9wHFungicidd activity: Turner it al. Corona. ~/ML 22, 303 (1964).

Cl

Crystals, df 1.7. mp 243-247*. b , 33O*. Vspor prwa<O.OI at 4O* Practically inaol in water (soly si room •—.reponed a* 0.6 ppm). Soly ia organic solvents et 23* (w/wkxyleae 1%. cydobaxane 3%. acetone 2%. kmtiae < lOk.LDW orally ia rat* > 10.0 g/kg. Turner <rai.aic.ctt,MK Fungicide, baciericid*, •anialiniilt Agriculuml al~

horticultural fungmde. ' ~" '~•909. 34S4'4-T4«ncalaraMUcylaailUte.

CJ1HTa4NO.. mol wt44*40%. N 199%. O 9.lida*: Bindler. Modd.

351.03. C 44.41%, H101%/a12%. Prepn of potybalcaaucyUd.

Crystals, mp 161*. Fluoreece* under ultravialti MgkLPractically insol in water. Sol ia alkaline aq tola* aad hisolas of wetting agent*. Sol ia asaay orgaaio *M*b Bacicnoatai in formulaooa* of aurgical

dry soaps, riaae*. polishes, shampoos, daodoranlipratervtiive in textile finish**, certain petroleum .odlulote c*t*r*. cutting **.t.- coolnnta. fiswttfinatat'lB'tttmaauf of iberoopUsoc artidaa: Tdlar. V& •pat. JtmVTm '(19*1 10 Weco Product*). Cannon.- Consult lana* Oowa.'meat ragultrion* oa ua* ia drug* aad

0910. TatncalorTiaakoa. fnetfhortc<3,4.t-tnchtofoahtnrl thtnyl Mmmmjt tmtrj. a-*hlor»»U-(14.3.trichloroph*nyl)vuiyl dimethyl paoaphalanl4>O>«

SO ... . . __ .Ptacapaate-type petucide of low aunamaiW-*na ryr««)**'aiag*. lot fax Cantr. 12, 2* (I97O). Pnpa: PkJBt*-*"****? "

>. UA pat*. 3,102443 aad 34334*7 (I9*a 9n*aa**l •P.«mry. UJ. pal*. 3.10243 aad 343345*7 (I963.1T7J wajlA' jtoShdlX Propertiee: WkasMoaa at ol. J.-Agr?fmoa <***«T j14, 352 (19*6). • -T'U • .iffiBM

mp*7-9r. Vapor praman at 20* -waun II ppm; ia xytaac: < 155k40>5OK°a>room tamp. LOM (75% wditdg/kg orally. CAT*. 93332k ' ~

L

A R I O O !

f.J-9319 TrteBloractayktMO 10.71%. Ca,CH,OH. Prepd by reduction of the corrc*-

, ponding eater, acid chloride, or acid with lithium aluminumhydride: Sroog « ai. / Am. Chtm. Soc. 71, 1710 (1949).

I Manufacture by raducuoa of chloral hydrate with an amiacj boranc: Cnamberlaia. Schachter. U.S. fat. 24*147* (1939' to Gallery Chem.).

Hygroscopic liquid, ethereal odor. Al low tempe it cry*-Ullizas ia rhombic tablet*, mp *t If: bp 131-133*: dg 1.33.Sol in about 12 pan* water, ousable with alcohol or ether.pH of aq soln i* 5-6. but on prolonged contact with watersome frae add ia lormed. Ktto •*!! clotod and prottcttd fromlight. LDgj orally ia rat*; 600 mg/kg. Handbook of Toxicol-ogy vmL 1,V. S. Spactor. Ed. (Saundan. Phiiaddphia. 1933)pp 302-303.THULAS CAT: Hypaotfc. aacalbeuc.

9319. Trichloroethylea*. Trichlotmnhont: ethinyl tri-chloride; Tri-Ocae: Tndene; Tnleac: Tnchloran; Trichlo-raa: Algylen: Trimar. Tnliac; Tri; Trethylenc; Wesuosol.Chlorylea: Oemal|sn«; GemMlgane. CMQr mol wt131.40. C 11.21%. H 0.77%. a 10.95%. CC1,-CHCI.Usually prepd from jvm-tetrachloroethaAc by dimmeiion ofHa (by bailing with lime): Gar. pat. 171400. By paaaaglatrachloraethane vapor over CaO, catalyst at VXT. Gar.

I i

i!

Cad, catat 430-47pal. 263,437; without catalyst at 430-470T: Brk. pal. S7S.

330 (194* to du Pont). Modem process survey: S. A. Mil-ler. Chtm. frocma Eng. 47. 261 (19*6). Toxidiy and metab-diam: E. Browning. Taxiciiy and Httabolltm of induanalScW«*na(El**vicr. New York. 1965) pp 119-211Nonflammable, mobile liquid. Chancteriauc odor res em -

biiag that ol chloroform, d} 1.4904; df 1.4693: df 1.4649.Vapor density: 4.33 (air - 1.00). Solidifies at -14.r.bp,- sa-T; bp_ 67.CT bpM 41.0*: bp_ 31.4*; bpw 20.0*:bp, -1.0-. op- -12.4*; bp, -22.1V bpu -43.r. ntt1.47914; nf 1.41560. Practically iaaol in water, misablewith ether, alcohol, chloroform. Dissolve* most fixed aadvolatile oil*. Slowly dac (with forma of Hd) by light ia thepresence of moisture. Trichlorocthytac for medicinal pur-

i may contain tome thymol or ammonium carbonatemore than 20 mg/100 ml) a* a ilibilurrr. laduatnal

grade* of trichioroethyleoe may contain other stabilizer*tuch •• triethaaolamine *u*rate and creaoi. LOn orally iarata: 4.92 ml/kg. lethal coacn (4 brs) in rale: MOO ppm.Smyth at ml. Am. Ind. Hyg. Aaoc. J. 3O, 470 (1969).Caution: Vm with odoquou rtntilouon. PT***T>I Irichlo*

roethyleae in i salad, light-nsistaat ampul* or ia Irangibla,lithe nditiui glass tuba*. Avoid praloogad axpoaura of thaproduct to excmaive heat. It muet be dispensed in the un-opened glaa* onnrtiner ia which it we* placed by the manu-facturer.Human Tcuucirv.4 Moderate exposures can cauae symp-

toms wailar to alcohol inebriation. Higher eoacaa can havenarcotic affect. Paathi oacurriag after heavy exposure havebean attributed to ventricular Abrillaaoa. Liver mjury i* notddlaitdy established in oeeupenood exposures. Fouad to

(not i

eat litali, such aa ckloraaoetic acid.•1TttHLAf< CATS *iaalt**ir (inhalation).

•CATtvm Inhalant

i hepainndliilar carcinoma* ia Natioeal Cancer Insii-tat* teat* oa mice: Chem. a Eng. Una34. 4 (Apr. S. 1976). —— " —'——— ——————— . ..-KV:Ma: Sotvaa! for tau. wax**, rada*. oil*, rubber, paint*. 9323. 2,44-TrkhlaropheaoL Dowicide 2& OmaL .C

aad varaiehe* Solvent lor odlulose *Man aad ether*. Used H.C1.O; mol wt 197.46. C 36.49%. O 1.10%. H 1.53%. Ifor sctveat *Mracaoa ia nsaay Industrie*. In decreasing, la 53.17%. Prapd by dinct chloriaatioa of pbcaol: -Tkttaidry daeaing. la the maauf of organic ehaairili. pharma- Hoc. Trar. Chim. SO. 115 (1931k Chulkov ttal. Org, Cm

Ind. VSSA S, 97 (l»37k Chem. Zentr. U30, 1.1419; £Ai4967 (1937). . . *..:: ivr.il *-r

. . .... , 4-..* r.em - • ->--•*<* ---*'

*3**V Trtcaloroflaoromethaac. Tricaloromonofluoro-•dhtnr BuafotrichloroBetbaae; Fraoa 11; Frigea 11:Amoa 9. COJ*; aMl wt 137.31. C 1.74%. a 77.43%. P1X13%. Prapa from carbon letnchloride aad antimony tri-•uonda:. Heaaa. Organic Aam-awu 2, 64 (1*44). . , .,Llqind at lamp* bdow 23.T. Faiat atheonl odor.. Noa-

•ammablev,fU*J l.494id» 3.0*(*ir - I), mp -111*.•a.7 bo_'+*.r: bo_ -9.1*l'bo_ -23.0Vbo_ -bp, -5»>: bp, -4T.r. b*. 3>.or. bo. -fl.6-.bnv.—aVr. Crif, lamp 19T. cril praMl 43.2 aaa (635 lb/*q ioca.BbaX a*M 1 J**5. JDipol* moment 0.45. Practically ia*ol iawater. Sol la alcohol, ether, other, organic loivent*. Lme

tkaa carboa dioxide, but aacoaa poses iato harmful

lecu»> si aegative ptcesurie. A* serosol prop Uat. .no* May b* narcotic IB high concentrations. >*Nott: Coaaull lateat Government regulation* ~. '

aaroiol propaUaai. ^ •*9321. 3,4,6-TrlcUof«-2-alti«pk*aol. Z-N.iro.j .V.

chloropheaol: 14,3-inchloro-6-Biuophcnol: Oowlan r-'H,a.NOr mol wt 230.43. C 26.06%. H 0.ir*V. Cl«4.i«rN 6.01%. O 20.13%. Prepd by diuolvini I4.'.»wl>pbcaol in glacial acetic acid and treating with coattTau.!.aad: Kohn. Fink. Monaah. SO, 73 (1931); Hanuo. «w/ Chtm. Sac. 1*43, 233. **

-sU

Pale yellow crystal* from petr ether, mp 92-93*. <. iv r,USB: To combat the tea lamprey, an ed-uk* Ash *M

attacks trout, especially ia the Great Lake* rapon.9322. 2,44-TrichloropheaoL Colluaotoi: __

C.H.CljO; mot wt 197.46. C 36.49%, H 1.33%. O 110%, Q33.17%. Prapd by treating 1,14,3-tetrachlorooename wmmmethanolic NaOH ia autoclave at 160* (or several hra: Hot*nsoo « al. J. Chtm. Sac. 1*43, 235; Agfa. Gar. pat. 411jHD(1923k C*«n, Ztntr. 1*2*. I. 2411. , ~

Meadlai from alcohol or ligroia. Strong pboaolk vooimp6T. Sublime*, bp 241*. bp , 233*. Weak moaotaeiaad. K at 25* -. 4.3 x 10-*. Soly <g"00 g of idveata25*): ac-eioae 615; hanieni 163: carbon uirachlonos J|ether 525; deaalurad alcohol formula 30. 323; OMthaad 61]liquid petrolatum (al 50*) J*. toybean oil 79; uluaw.122water <0.1 LO_ orally ia rat*-. 0.12 g/kg.V ^ IA4W km'*. C

froc. 1 76 (194Sodium salt esaquihydrala. Doncidt 0. Plskes [prepd M

cording to VS. pal. 14*142* (1933 to Dow)]. Sdutaal(g/100 g solvent *t 23*k acetone 163; denatured kleofcformula 30, 116; cthykae glycol 33; methanol 241; -«M113. pH of inid aq sola 11.0-13.0. •-.-.-**.*Complex with triuobutyl phosphate. CuH_aO,*», TV

cMew. Prepa: Bouulcane-Wallrand tt ai. Pr. pat. MM(1961 ia Pechiney). Liquid, bp , 94-lor. .«. <

Crydala tram ligroia. Strong phenolic odor. 'jVotowith steam, but not from alkaline tola- d 1.490l.:.«t>-j

24**. Soly(g/100gaf*olvent): Acetone 323; born*.... carboa tatnchloride 37; diaeetoo* alcohol 335r-l354; dtuturad alcohol formula 30. 400; methand 325).Oil 1*3; Stoddard tolwt 16; toluene 10ft turpojoarwalar <0.1. • ' -. • •--••• '•'••- •n-*'JiJ?«

tall axMobydrata. flaky crystal! Iprepni ;«••

kp.,.Ilit

aitteritl* by flsmai or high heat;',.:.M«J 'In rdngeraooa msi hinarj requiring a rafrigtrant at-

1230 CammJt mm crmm iatte at/an mttmg iku t,—-AR I 00129

Sice Safety Protocol

EMERGENCY PROCEDURES

In the event of a aedicol or other emergency, the OSC or hia deoignee willnotify the Appropriate Authority. The following liot of phone number* will bepooted prominently ot each telephone on-oite:

1. Fire

2. Ambulance «££ f. .- C I H I

3. Police

4. Federal Government ' (%~CJ "-/O*-/ —

5. State Government <?|M *7 .:?<-/ -*8S3£ PADtr?

6. County/City Government MSt " 5^ 11_____

7. EPA Environmental Reoponoe Team (3cJ 3"3l-6

8. Hoopitalo

H. Holiday "~ --•e?bl

A R I G O S 3 0

SAFETY PROTOCOL ACKNOWLEDGEMENT PAGE OFPAGAN ROAD DRUM SITE

NAME REPRESENTING DATE

, 'i

* ^

A R I G Q ;

SAFETY PROTOCOL ACKNOWLEDGEMENT PAGE OFPAGAN ROAD DRUM SITE

NAME REPRESENTING DATE

SAFETY PROTOCOL ACKNOWLEDGEMENT PAGE OFPAGAN ROAD DRUM SITE

NAME REPRESENTING DATE

44-

O *"'o u

APPENDIX D

CORRESPONDENCE

A R I n <"! ! 31-M n i v^ -• i •-' '

The following certified correspondence (Notice of Violation) has been recreatedto be included in this report as copies obtained from the issuing Departmentwere not printable. In addition, referenced enclosures could not be obtainedfor inclusion in this report.

AR 10:1 35

1012 Water StreetMeadville, Pennsylvania 16335Telephone: A.C. 814/724-8526

September 24, 1984

CERTIFIED MAIL »P 446 369 569

NOTICE OF VIOLATION

Subject: Unpermitted Solid Waste Disposal SiteTri-State Insulation; Coon RefrigerationSummit Township, Erie County

Vedder J. White, Esq. Coon Refrigeration, Inc.Trustee: Tri-State Insulation, Inc. 8164 Pagan Road501 Marine Bank Building Erie, PA 16509Erie, PA 16501

Mr. Thomas V. PurvisMarlin K. Coon, President Vice PresidentTri-State Insulation, Inc. Tri-State Insulation, Inc.8164 Pagan Road 1070 Apple Hill LaneErie, PA 16509 Allison Park, PA 15107

Dear Sirs:

Pursuant to the Pennsylvania Solid Waste Management Act of July 7,1980, P.L. 380, No. 97, 35 P.S. 6018.101 et seq. (copy enclosed) and theHazardous Waste Rules & Regulations adopted on September 4, 1982 pursuant tothat Act and to Chapter 75, Rules & Regulations for Solid Waste Management (25Pa. Code 75.1 et seq.) the Department of Environmental Resources regulates themanagement of hazardous and other solid waste within the Commonwealth ofPennsylvania.

As a result of inspections conducted by staff from this office onSeptember 10, 12 and 18, 1984 at the above referenced site, and as a result ofSeptember 18, 1984 meeting between Mr. Coon and staff from this office, it hasbeen determined that solid wastes have been disposed at the site for a periodof at least two (2) years and that those wastes consist of at least municipaland residual waste, as defined by the Solid Waste Management Act (Act 97).Those conditions place Coon Refrigeration, Inc., and Tri-State Insulation,Inc., in violation of Act 97 and the Pennsylvania Hazardous Waste ManagementRules & Regulations as follows:

1. Tri-State Insulation/Coon Refrigeration have dumped or depositedand/or permitted the dumping or depositing of solid waste (asdefined by Act 97) at the above referenced site. No permit for suchan activity has been obtained from the Department [Section 610(1);Act 97].

2. Tri-State Insulation/Coon Refrigeration have constructed, operatedand/or utilized a solid waste storage and/or disposal# ja ijlilt j 35without a permit from the Department [Section 610(2); ct 9*7].

A R 1 0 G 1 3 6

- 2 -

3. Section 75.262(b)(l) of the Pennsylvania Hazardous Waste ManagementRegulations states that a person generating solid waste shalldetermine if that waste is a hazardous waste using procedures definedtherein. Tri-State Insulation has generated solid waste withoutdetermining if said wastes were hazardous wastes using proceduresoutlined in Section 75.262(b)(l).

4. Tri-State Insulation/Coon Refrigeration have operated and/ormaintained the site in a manner so as to adversely effect or endangerpublic health, safety and welfare or the environment, or cause apublic nuisance [Section 302(b)(6); Act 97] at a minimum in that theDepartment has measured air contamination resulting from wastedisposal activities at the site.

5. Tri-State Insulation/Coon Refrigeration have stored/disposed ofresidual waste without having first obtained a permit from theDepartment [Section 301; Act 97].

Be advised that Act 97 defines as disposal any storage of waste in excessof one year unless there is clear and convincing evidence to the contrary.

Also, be advised that any violation of any provision of Act 97constitutes a public nuisance and that any person commiting such violations isliable for costs of abatement of any pollution and any public nuisance causedby such violation.

In order to abate the above referenced violations, Tri-State Insulation,Coon Refrigeration, Marlin K. Coon and Thomas V. Purvis should:

1. Immediately cease all solid waste disposal activities at the site.

2. Within seven (7) days of receipt of this notice, inventory those 55-and 5-gallon containers of material at the site and accurately deter-mine and record in writing which containers hold usable product andwhich containers contain waste.

3. Within fourteen (14) days of receipt of this notice, any liquidwastes held in drums which are leaking, which are without lids orbungs, or which are otherwise not completely closed should betransferred into secure, closed drums.

4. Within fourteen (14) days of receipt of this notice, rearrange allcontainers of waste at the site so that those containers can beaccurately inventoried by Departmental staff.

5. Within thirty (30) days of receipt of this notice, determine, usingprocedures outlined in Section 75.262(b)(l) of the PennsylvaniaHazardous Waste Regulations (copy enclosed), which wastes arehazardous wastes.

6. Within five (5) days of receipt of any sample results used in thedetermination of the status of site wastes, send copies of thosesample results to this office.

AR!Oj:37

- 3 -

7. Within fifteen (15) days of completion of the hazardous wastedetermination referenced in no. 5 above [i.e. within forty-five (45)days of receipt of this notice], arrange for the proper treatment,storage and/or disposal of all site wastes at an off-site facilitypermitted to accept such wastes.

8. Notify the Department in writing of arrangements made (as referencedin no. 7 above) within five (5) days of making those arrangements.

9. Within one hundred-twenty (120) days of receipt of this notice, haveall site wastes transported to an off-site facility permitted totreat, store and/or dispose of such wastes.

Failure to abate the above referenced violations may result in theinitiation of legal action.

Be advised that the Solid Waste Management Act provides for penalties forviolations of each of its sections on separate days.

Also, be advised that this letter does not waive, either expressly or byimplication, the power or authority of the Commonwealth of Pennsylvania toprosecute for any and all violations of law arising prior to or after theissuance of this letter or the conditions upon which the letter is based.

This letter shall not be construed so as to waive or impair any rights ofthe Department of Environmental Resources, heretofore or hereafter existing.This letter shall also not be construed as a final action of the Department ofEnvironmental Resources.

Should you have any questions concerning the above matters, please feelfree to contact me at this office.

Sincerely,

Mark E. GermanSolid Waste SpecialistBureau of Solid Waste Management

MEG/skg

Enclosures

cc: Paul Burroughs, Attorney for the CommonwealthRobert G. Dwyer, Esq.

i n n i oi i U w i 0 u

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III

841 Chestnut BuildingPhiladelphia. Pennsylvania 19107

SUBJECT: Coon's Refrigeration Site DATE: May 16, 1986

FROM: Michael Zickler, Senior On-Scene Coordinator, -j]7.Emergency Response Section (3HW22) V

TO: Charles Walters, Public Health Specialist,Agency for Toxic Substances Disease Registry (3HW20)

Attached are a CDC summary sheet, draft action memo with data summary,

site sketch, and site pictures for Coon's Refrigeration (Pagan Road Drum

Site),, Summit Township, Erie County, Pennsylvania.

MZ:ah

Attachment

0..'

COONS REFRIGERATION-CDC- Hay, 1966

SUMMARY SHEET

I. Identifying information:

Coons RefrigerationPagan RoadErie CountyMillcreek Township, Pennsylvania

This is a drum site.

II. Substances present or believed present:

la. Labels:Ureflex, trlchlorofluoromethane, polymeric Isocyanite,

lacquer stain, silicon prime coat (combustible), component a-lso-cyanate.

Ib. By analysis:Benzene, ethyl benzene, methylene chloride, toluene, carbon

tetrachloride, chloirobenzene, crichloroethylene, naphthalene, tetra-chloroechane.

2. Quantities (estimated):Approximately 250 (total) 55-gallon drums, of which an

estimated 150 drums contain materials and an undetermined number of5-gallon cans. Of the 250 drums:

(1) Approximately 120 drums stacked against the wall ofthe building.

(2) Approximately 20 drums on side leaking contents.These drums are located within 30 feet of the drinking water well forCoons property and within 150 feet of a large pond (see map).

(3) Numerous other drums are scattered on property and Inwooded area to the rear of the property. These are in various statesincluding a number in poor condition believed to contain asphalt andleaking on ground.

III. Geographic and demographic data:

1. The distance from the Coon residence (closest residence) tothe site Is approximately 250 feet.

2. No signs or barriers to prevent access to the site areevident.

3. There are 21 residences within 1/4-mile of the site. Theseresidences do utilize groundwater for drinking water use.

A R I C Q U O

_ -.c! 1! sc^<- Reo .:rv'J

Site

Memorandum

From Accing DirectorOffice of Health Assessment

Subiect Coon's Refrigeration (Pagan Road Drum Site), Summit TownshipErie County, Pennsylvania SI-86-125

To Mr. Charles J. WaltersPublic Health AdvisorEPA Region IIIPhiladelphia, Pennsylvania

BACKGROUND

U.S. EPA Region III requested the assistance of ATSDR to review thesubmitted data package to determine the public health threat posed by thematerials present at the Coon's Refrigeration Site.

DOCUMENTS REVIEWED

1. Summary sheet of substances present or believed to be present,geographic and demographic data.

2. Draft action memo with data summary of site.

3. Site sketch snd site pictures for Coon's Refrigeration dated June1985.

DISCUSSION

The Coons Refrigeration-Pagan Road Site is located on approximately twoacres in a rural/residential area of Erie County, Pennsylvania.Approximately 21 residences are located within 1/4 mils of the sits, andall depend on private veils for potable vater. Drums and other containersare scattered around the sits, with a majority of drums directly outsidethe rear of ths Coons refrigeration building. A preliminary assessmentand sampling were conducted by EPA in June 1985. Over 250 drums and anundetermined number of smaller containers were observed. Behind a seriesof stacked drums, thsrs ars 20 additonal containers on their sides. Someof them vere leaking their contents. These containers ere located within10 ysrds of the veil vhich supplies drinking water to ths building. It isalso located within 150 feet of a large pond. Scattered around theremainder of the property are small groups of drums and other containers,most notably a group of 40 drums contsinlng solvent-thinned asphaltcoating. Many of these drums have ruptured and released their contents

p. r> i on I '• !rA n I u u I -H

Page 2 - Mr. Charles J. Walters

onto the ground surface. A review of the laboratory data indicates levelsof carbon tetrachloride at 510 ppm in Sample *4, benzene (which isleukemogenic) at 13,000 ppm in Sample #3, ethyl benzene at 33,000 ppm inSample *6, methylene chloride at 140 ppm in Sample #2, and1,1,1-trichloroethane at 12,000 ppm in Sample #4. Not only are thesecompounds harmful if ingested by groundwatsr contamination, the flashpoint snd explosion potentisl is a serious threat to public health. Thepossibility of human exposure due to direct contsct is enhanced by thelack of signs or barriers to prevent access to the site.

CONCLUSIONS

Based on the information provided, we feel that the materials present atthe Coons Refrigerstion Site represent s potsntisl public health threatand that measures should be taken to reduce that threat. Risk factors sremultiple as noted sbove:

1. Poor site security increases the risk for direct exposure.

2. Risk of fire and explosion is reslized by identificstion of materialswith low flashpoints.

3. Leaking drums threaten groundwater for the approximate 21 residenceswithing 1/4 mile of the site using groundwater for drinking water.

4. There is a potential for hazardous materials on-site to leave theproperty due to uncontrolled stormwatsr runoff or air releases.

RECOMMENDATIONS

The presence of the above mentioned material warrants an immediate removaland we therefore recommend that:

1. Appropriate security measures be taken to limit sccsss.

2. Following staging snd removal, appropriate water and soil samples betaken to evaluate residual contamination.

We will be available for future consultations if end when it Is necessary.

Jeffrey A. Lybarger. M.D.

A R l C G U r

KriOLKGraham McLaughl120 WEST TENTH STREET ERIE. PENNSYLVANIA 16501-1461

814-459-2800ATTORNEYS AND COUNSELORS

June 16, 1986.•MCifMSfTT• ••AITV :-

The Honorable Warren W. BentzUnited States Bankruptcy Court

__ 316 U.S. Federal Court House '£*[*'•«*»** Erie, Pennsylvania 16501

KMtiMT « Re: Purco, Inc.

Dear Judge Bentz:• u UOM»

This letter is to inform you that the/premises pre-viously occupied by Purco, Inc. have been invaded by represen-tatives of the D.E.R. and the E.P.A. and that many of theassets and inventory of Purco, Inc. are now the subject ofsome kind of a massive cleanup campaign. All of this is beingdone over the objection of the officers of Purco, Inc. and theowners of the property in question. From the outset the variousregulatory officials were informed that all of the materialthat they are now dealing with is a part of a legal disputebefore your Honorable Court but this has made absolutely nodifference. Nothing that is being done has been approved of byMr. Coon either as a representative of Purco, Inc. or as a repre-sentative of the owner of the property.

In all due deference'to all concerned, it now appearsthat tens of thousands of tax dollars are being squandered in abelter skelter fashion with* the end result being questionable atbest. I do not know if Mr. White gave these people permissionto do what they are doing and if he did not, I do not understandhow these people can supercede the jurisdiction of the BankruptcyCourt.

Very truly yours,

KNOX GRAHAM McLAUGHLIN GORNALLAND SENNETT, INC.

JWB/bms

cc: Mark E. GermanDepartment of Environmental ResourcesMeadville, Pennsylvania 16335

•"""Environmental Protection AgencyPhiladelphia, Pennsylvania 19107

Vedder J. White, EsquireMarlin K. Coon

j?\

1*0 "•*, UNITED STATES ENVIRONMENTAL PROTECTION AGENCY. Jfe- REGION III*SSZ*V/ 841 Chestnut Building

* Philadelphia. Pennsylvania 19107

June 24, 1986 CERTIFIED MAIL RETURN RECEIPT REQUESTED

Mr. Vedder White, Esquire (Ae trustee for Purco, Inc.)SOI Marine Bank BuildingErie, Pennsylvania 16501

Deer Mr* White: •'

This is CO confirm Che oral notice given to your represent!ve, Stacy Shimek,on your behalf, aC 1:20 p.a. on June 9, 1986. The United State.* EnvironmentalProtection Agency (EPA) has documented Che releaee end threatened release ofhazardous eubetancee, pollutanta end conceminence at che property located at8164 Pagan Road, Summit Township,'Erie County, Pennsylvania. EPA is currentlyexpending public funda ac this site.

Under che Comprehensive Environmental Response, Compensation, and LiabilityAct of 1980 (CERCLA), and other laws, responsible parties may be liable for allmonies expended by Che Federal Government Co cake necessary response actions acuncontrolled hazardous waste sites, including investigation, planning, removal "~and remedial actions at these sices, and enforcement. Responsible parties underCERCLA Include che current and past owner and operator, and persons who generatedthe hazardous substances or were Involved in transport, treatment, or disposalof them ac Che sice. Based on our review of EPA records, EPA has Information thatindicates that you may be a responsible party aa defined by CERCLA, as trustee inbankruptcy for Purco, Inc.*

This letter la Co notify you that EPA is currently undertaking or isplanning Co undertake che following activities:

9

1.) Staging, sampling, removal, transportation and disposal of surface drumsand concamlnated soils found co be hazardous by definition after sampling.

2.) Meaaurlng and sampling of drums, soils, and water to fully assess areasof concern*

3.) Restriction of access Co che areas in question.

4.) Sice stabilization, Co Include but noc be limited to regradlng, erosionconcrol and revegitation.

5.) Provide personnel, equipment and other support services necessary toaccomplish che above. A R 1 C " ! L!- L'

In my conversation with Ms* Shlmek she Indicated that you could not bereached under any circumstances and would noc be able co take corrective actionto clean up Che site as outlined above. EPA has authority to enter and performsuch activities under S 104 of CERCLA.

Where you are already involved in discussions with EPA, State or localauthorities or engaged in any voluntary action, you should continue that activityand reporc Che status of Chese discussions or that action in a letter. Pleaseprovide a copy of your latter co any other pertiea«*jLnvolved in those discussions.Your letter should be seat co:

Ellen C. TepllczkyAssistant Regional CounselOffice of Regional Counsel (3RC21)U.S, Environmental Protection Agency841 Chestnut BuildingPhiladelphia, Pennsylvania 19107

If you need further information on the nature and extent of release orthreatened release or our determination that you may be a responsible party, youmay contact Ms. Teplltzky at (215) 597-9405.

Sincerely yours,

David P. WrightOn Scene CoordinatorEPA Region III

cc: Regional CounselV

John W. Beatcy, Eaquira

Marlin Coon

10 U Water StreetMcadvLUe, Pennsylvania 16? 35

A. C. 811/721-8526October 18, 1Q8U

tf I .-Jo) id Wa^t* Lisponal Sitelr'U>'r.'»tf -Insulation; Corn Refrigerationkumlt Po*-ri-4hip, trie County

V'-.H:"- -1. *i>l'..«», P><:. Coon Refrigeration, Inc.Tn"M ••»: irJ-St%v.«*j J trul* t ion, Inc. 8164 Pagan Road!'*'.i * rl-:- r.trk iMiHing Erie, Pennsylvania 16509

Mr. K-rij-i K. <"<-,•«», Pr*." L dent Mr. Themes V. Purvis, Vice Presidenti'iK*»u.in' ion, ln«*. Trl-Statfl Insulation, Inc.

i f-oaU 1070 Apple Hill LaiWPrn-vylv-tnia IbiO1; Alii son Park, Pennsylvania 15107

-Lr".1

:-'aff' iron t!ii~ office Inspected th« abmyej r«f«renc«d site on-r 'i -nd 1fi, 1o-«U piraiiant. to th« S«pt«nb«r ?4, 1«81 Notlo* of Violation3 vi /r^n M»l-i off IQ« H'sm ing unparaltted solid waste tanag aant a,ii.~. Cb-mr-vations on October 4 and 16, 1981 lndlo*t«d that, i**thmr thanvl'ii. unp*r itt'--d ulna conditions, olemn up activities at tlia site w<sreiro> in Ojrth-tr rlnk.*t to tha environment and publio h«Mlth In that area.Un' 'v, -fi«t h-is lv»*n reported to oa "aspbait* diluted with unspaoiflednt" m obr-Mrvd f«j>lll«d on thej ground on both data*. f\jrth#?r, soil,M? I br**i unJ#>riyinc what prevlat^ly waa th*a drum 3torag«/di»po«al area,

b • -«n '-> -id»! into =» c 'ttralirod pile and alxed with various unidentifiable ..- . ;'j",it-orin* of th- aoilArant* pile on Cstoomr 16. 1984 indicated thatp< IP n/^ rf?iv-n«lM({ orpttnio compound •» into tn« atavDspbtra. Air oonltorlng on>b. r K. r»i5;o indir:*tt«d that cr«noral air quality in and around th* alt* ia

!xl ro-ipar«x) with th«t air quality in araaa raanvad and upwind of tha aite.i r>i «lr quality d>tftr*td«tion ippeantd to Include standing druns of liquids

in n-)( -n too oontaineris thtf above sptolfiad apilled "a.iphalt/solvant" andiri< nil-%; and * pil« of open 5-gallon oontainers Mhioh, Until Ootobar 4, ;«id th«j reportrd •aspbalt/solvant" aixtur*. ^ , _ .

'' <. .•on should be advised tha'. aoti?itla« leading to tha abors olUd

oondif icnv ray furthrr ocnpound olmn-up problMM and coats of olean-up at thainci r. y place j r-jons in and around the) ait* at rlak regarding tbair par*- »..*

V

l-« further «»dvJ i«d that Section 75.26l(h)(4)(U) of the Psnnaylvaniai'r:Mj' v-T-te h*»tmretMnt Kule t 4 Regulations states in part that any

ro>i*->. tn-it^l soil or other debris rojulting froai tha clean up of a spill is a>.a-*c*r,;MU* /ntt<> if ar1 wh»n it is discarded or Intended to be discarded and Ifth« -r'ur1 -vii^rlal \vta * generic siaa* listed In Section 75.26l(h)(4)(rl).Vjr.v ^*p*r-A- irv>j-trJ\l r,olvent*« ar*« listed in Section 75.261(h)(4)(vl). A^ro,

i.e. ;.;V; :?> i -<v. «cii i ontstnlng :-uch compounds list«*»d In Section7J..-MCh)C'>(vi) ItHRif beeom9*s n ha. rduus waste if and utwn It is intended to{;f -II vv.!--i («Jro Oeci (on 75.*-6l(h)('i)(J)J. Finally, be advised that Section75. :Mfh)( ;,)(!!) r>tat>-i in part t.hat "any solid waste generated from the treat-n«n: , -:,or-'-"» or di*»pc •;*»1 of a h*zar<\<yua waste, including any sludge, spillr*»?i-J:i« . .V, enif-olor. control du.it or leaohat*, but not including precipitationrunoff, t ) f h*i*-,ir'.iou- w-i"*,*?". The nbovs cited sections may apply, therefore,if rM.'-riT.] s or i-in^to/ art' lifted in Section 75.26Kh)('0(vl).

1 1. ••!•<•» or-», t ised upon <>.e nbovG information, you should not attempt toor r'. r/s HIP ab^ve nferencod roll/waste pile or any other spill residue,

c'ebri- -ir r'-^ihly oontanla-ited soil at the site until it can be verified thatraid rnterJ-*! in not f waste or if a waste, until the spilled "solvent" androurc-->( 0 of ooll pile contaainatlcn are identified to the Oepartaient • srati.-r.?--*,;. -!, so tltat ^he ./aste can be properly Managed.

V» should b<? prepared to rroperly evaluate site conditions followingfr!Tir"'l w^st--» r»-Tov-*l undertakrn pursuant to the abatement processne i in tnc Depart "tent '9 September 2'4, 1984 Notice of Violation. Then,

bA.i.."i i:;>ori t 'int ^v^lu^Mon (which flfK-uld include at a minimum noil and water•»n«.ly*>-- irt .-»rid nr und th<« ilte), be prepared to properly close the site tonlni".i7- pphlic hen.lth and environowntal risks.

Pi "•»«.• oont-t^t this office xt your earliest convenience so that ai -rt.i'i- arrnr rr"»pc!vsthle r rtie?i can be arranged to dHcuss proper site closurein n:r? d.?».iJ[l.

.-• -ul'i y-7u ?nv<» nny qucr.tlcna regarding the above natters, please.o1 <nr rit tfii.-? office.

Sincerely,

Hark E. GermanSolid Waste SpecialistBureau of Solid Waste Manag«s»nt

cc: P-Tii ynirouT^. A'.tornoy for the CocrwonwealthMO'-ort '"J. l> y*?r, Ksq.

be: BSWJj - Central Office«6adville Regional File/Coon RefrigerationErie County FileCht'on.

U R I C C ! '•' I1 1 1 * ' - - ' •

\iSmmi

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY\ REGION III

841 Chestnut BuildingPhiladelphia, Pennsylvania 19107

June 24, 198* CERTIFIED MAIL RETURN RECEIPT REQUESTED

Mr. Merlin Coon8164 Pagan RoadErie, Pennsylvania 16509

Dear Mr. Coon: '*

This la to confirm Che oral notice given you ac 9:10 a.m. on June, 10 1986.The United Scacea Envlronmencal Protection Agency (EPA) has documented che releaseand threatened release of hazardous substances, pollutants and contaminants at theproperty locaced at 8164 Pagan Road, Summit Township, Erie County, Pennsylvania.EPA is currenCly expending public-funds ac this sice.

Under che Comprehensive Environmental Response, Compensation, and LiabilityAce of 1980 (CERCLA), and other laws, responsible parties may be liable for allmonies expended by Che Federal Government Co cake necessary response actions acuncontrolled hazardous waste sites, including investigation, planning , removal ~~and remedial actions ac these sites, and enforcement. Responsible parties underCERCLA include Che current and past owner and operator, and persons who -generatedthe hazardous substences or were involved in transport, treatment, or disposalof Chem at Che sice. Based on our review of EPA records, EPA haw information thatIndicates that you may be a responsible party as defined by CERCLA.

t

This letter le Co notify you that EPA ie currently undertaking or isplanning Co undertake Che following activities:

1.) Staging, sampling, removal, transportation and disposal of surface drumsand concern!naced soils found co be hazardous by definition after sampling.

*

2.) Measuring and sampling of drums, soils, and water to fully assess areasof concern.

3.) Restriction of access co che areas in question.

4.) Sice stabllizaclon, co Include buc noc be limited Co regradlng, erosioncontrol and revegitation.

5.) Provide personnel, equipment and other support services necessary toaccomplish che above*

In our conversation you Informed me that you are financially and legallyunable co cake corrective actions to clean up the site as outlined above. Youalso advised me that you granted EPA access co perform che said activities.EPA has authority co enter and perform such activities under S 104 of CERCLA.

Where you are already Involved in discussions with EPA, State or localauthorities or engaged in any voluntary action, you should continue that activityand report Che status of these discussions or that action in a letter. Pleaseprovide a copy of your letter to any other parties involved in those discussions.Your letter should be sent to:

Ellen C. Teplltzky '•Assistant Regional CounselOffice of Regional Counsel (3RC21)U.S. Environmental Protection Agency841 Chestnut BuildingPhiladelphia, Pennsylvania 19107

If you need further information on the nature and extent of release orthreatened releeee or our determination that you may be a responsible party, youmay contact Ms. Teplltzky at (215) 597-9405.

Sincerely yours,

David P. WrightOn Scene CoordinatorEPA Region III

cc: Regional Counsel

John W. BeaCCy, Esquire

' Vedder White, Esquire

UNJTED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III

841 Chestnut Building'«* /wo**1* Philadelphia, Pennsylvania 19107

June 24, 1986 CERTIFIED MAIL RETURN RECEIPT REQUESTED

Mr. John W. BeaCCy, EsquireKnox, Graham, Mclaughlin, Gornall, and Sennetc, Inc.120 West Tench StreetErie, Pennsylvania 16501-1461

.«,.Dear Mr. Beatty:

This is to notify you as counsel for Purco, Inc. that the United StatesEnvironmental Protection Agency (EPA) has documented the release and threatenedrelease of hazardous substances, pollutants and contaminants at the propertylocated at 8164 Pagan Road, Summit Township, Erie County, Pennsylvania as wellaa the property located on Rotunda Drive, Summit Township, Erie County, Penn-sylvania. EPA ia currently expending public funds ac these sites.

Under the Comprehensive Environmental Response, Compensation, and LiabilityAct of 1980 (CERCLA), and other laws, responsible parties may be liable for allmonies expended by Che Federal Government co cake necessary response actions atuncontrolled hazardous waste sites, including investigation, planning , removaland remedial actions at these sites, and enforcement. Responsible parties underCERCLA Include Che currenC and past owner and operator, and persons who generatedthe hazardous substances or were involved in transport, treatment, or disposalof them at the site.

This letter le to notify you that EPA is currently undertaking or isplanning to undertake the following activities:

1.) Staging, sampling, removal, transportation and disposal of surface drumsand contaminated soils found to be hazardous by definition after sampling.

2.) Meaauring and sampling of drums, soils, and water to fully assess areasof concern,

3.) Rescrlctlon of access co the areas in question.

4.) Site sCablllzatlon, Co include but not be limited to regrading, erosioncontrol and revegication.

5.) Provide personnel, equipment and other support services necessary toaccomplish the above.

EPA haa auChorlty to enter and perform such activities underftPdd^of CKfcCLA.

Where you are already involved in discussions with EPA, State or localauthorities or engaged in any voluntary action, you should continue that activityand report the statue of these discussions or that action in a letter. Pleaseprovide a copy of your letter to any other parties involved in those discussions.Your letter should be sent Co:

Ellen C. TeplltzkyAssistant Regional CounselOffice of Regional Counsel (3RC21)U.S. Environmental Protection Agency841 Chestnut BuildingPhiladelphia, Pennsylvania 19107

If you need further information on the nature and extent of release orthreatened release, contact Ms. Teplitzky at (215) 597-9405.

Sincerely yours,

David P. WrightOn Scene CoordinatorEPA Region III

cc: Regional Counsel

Vedder White, Esquire

Marlin Coon

RRI 00151

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III

841 Chestnut BuildingPhiladelphia, Pennsylvania 19107

The Honorable Warren W. BentzUnited States Bankruptcy Court316 U.S. Federal Court HouseErie, Pennsylvania 16501

Re: Purco, Inc.Docket No. 83-00544E June 30, 1986

Dear Judge Bentz:

This is in response to a letter to your honor from John W.Beatty, Esq., counsel to Purco, Inc., the bankruptcy of whichis pending in your court. In his letter, Mr. Beatty describedcertain actions recently undertaken by the EnvironmentalProtection Agency ("CPA"), which he apparently regards asimproper. Mr. Beatty has not formally petitioned for particularrelief from the court and it is, therefore, difficult toascertain the exact nature of his complaint. This letter isEPA's response to Mr. Beatty's concerns.

Last summer, EPA received information from the PennsylvaniaDepartment of Environmental Resources ("PADER") that hazardoussubstances were dumped or improperly disposed of on thesubject property.* Preliminary investigation at that timeconfirmed that hazardous substances had been deposited onthe site. This preliminary assesment was conducted pursuantto 40 C.F.R. $300.64. Over 250 drums and numerous smallercontainers were discovered, some of which were leakingsubstances onto the ground within 10 yards of a well whichsupplies drinking water. The well is approximately 150 feetfrom a large pond.

The Agency for Toxic Substances and Disease Registry("ATSDR", formerly the Centers for Disease Control) reviewedlaboratory results of analysis of samples taken from the sitewhich indicated the presence of carbon tetrachloride, benzene,(which is leukemogenic), ethyl benzene, methylene chloride,and 1,1,1-trichloroethane. ASTDR found that "not only are thesecompounds harmful if ingested by groundwater contamination,flash point and explosion potential is a serious thr^aft |ttahealth."

ftR I 0 2"It is our, understanding that the property belongs to CoonRefrigeration, Inc., which has leased it to Purco, Inc.

-2-

In early June 1986, David Wright, EPA's On-Scene Coordinator("OSC"), arrived on the site to supervise cleanup operationsat the site. He contacted Marlin Coon, the owner of theproperty and advised him that, under the terms of Section107(a) of CERCLA, Mr. Coon was responsible for the costs ofcleaning up the site. Mr. Coon was given the opportunity toundertake the actions on his own, but he declined to do so.Mr. Vedder White, trustee of Purco 's estate in bankruptcywas also notified of the cleanup.

From June 9 to 14, 1986, Mr. Wright directed the initialstages of the cleanup on the site. He and his team removedthe drums from the trailer in which they had been stored, inorder to sample their contents and determine the most appropriatemanner of disposal. All drums which were leaking or deterioratedwere placed in overpack containers to prevent further spillageof hazardous substances onto the ground. A sample was takenfrom each drum and we are presently awaiting the results ofthe analysis. In addition, the drums were stored on thesite in a manner which reduces the potential for leaking ortampering by unauthorized persons. This removal action wasconducted pursuant to 40 C.F.R. $300.65.

The implication of Mr. Beatty 's letter is that EPA has actedimproperly by commencing a cleanup designed to abate a hazardto public health and the environment. He also intimated thatthe agency's failure to obtain approval for the cleanup fromparties responsible for the site was also improper. As Mr. Beattydid not cite any authority for these positions, it is difficultto respond to them. I am not aware of any legal authoritywhich states that the filing of a petition in bankruptcyoperates to suspend operation of CERCLA or the authority of thisagency.

I have spoken with Mr. Beatty and discussed his opinion ofthe cleanup, and he has indicated to me that he will not be filingformal objections with your honor. He also assured me thathe will call me to discuss any problems with EPA's activitieswhich may arise in the future.

r r, tU K I

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I would like to take this opportunity to assure your honorthat we at EPA have no desire to interfere in a matter pendingin your court. We are, however, committed to fulfillment of ourobligation to respond to environmental hazards when and where theyoccur. In this case, fortunately, these goals are not mutuallyinconsistent. Should your honor require additional information,please do not hesitate to contact me at 215-597-9405. Thankyou for your consideration of this response.

Respectfully submitted,

Ellen C. TeplitzkyAssistant Regional Counsel

cc: John W. BeattyVedder J. WhiteDavid Wright *^-

RR I DO 151:-

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III

841 Chestnut BuildingPhiladelphia, Pennsylvania 19107

August 22, 1986

Mr. Bob Ohneck0. H. MaterialsP. 0. Box 557Findlay, Ohio 45839-0551

SUBJECT: Pagan Rd. - Site 0114/Project #132Rotunda Drive - Site #115, Project #133

Dear Mr. Ohneck:

As discussed during our phone conversation of August 22, 1986, we are returningthe enclosed Waste Profile Reports, as much of this information is incomplete,incorrect, and totally unsuitable for EPA use.

The lab results and WPR's have been enclosed and "red pencilled" to avoidreiteration of the individual errors discussed Friday. However, in general, thesubraittal of WPR's and lab results should, from now on, include the following:

1. A complete explanation, or summary, of the work and analyticalresults performed in narrative form, as an introduction to theraw data.

2. Copies of all raw data, field notes, lab notes, and Chains ofCustody relative to the project.

3. References on each page of data, to the EPA project by formalEPA facility name, EPA identification number, or EPA project number.

4. Total QA/QC data on all laboratory analyses performed, with StandardMethod and/or RCRA procedure references, as required.

5. Submit tal of all data in one package, Instead of individual seeminglyunrelated packages.

We trust that this information will be sufficient to allow correction and returnof all WPR's and related information to this office by August 29, 1986.

Sincerely,

David P. Wright p p l fi f, \ 5 5On-Scene Coordinator H U » •>- ~On-Scene CoordinatorU.S. Environmental Protection Agency

, UNITED STATES ENVIRONMENTAL PROTECTION AGENCYr| REGION III/ 841 Chestnut Building

Philadelphia, Pennsylvania 19107

March 24, 1987

Mr. Bob OhneckO.H. Materials, Inc.P.O. Box 551Findlay, OH 45839

SUBJECT: Pagan Road Drum Site CERCLA Removal, Erie County, PA

Dear Mr. Ohneck:

As per our conversation of March 18, 1987, there were several significantproblems encountered during the Pagan Road removal which were directlyattributed to errors made by O.H. Materials, both in the field and in theoffice. These problems were as follows:

1) One (1) overpack was not numbered. It contained approximately 14smaller containers, all unmarked.

>•

2) One (1) overpack numbered 214 was listed as "empty". It contained apartially full drum of flammable liquid, as per commercial labels on the druminside.

3) The following containers were found on site, but not on OHM's inventorylist: 163E, 163C, 175D, 189C, 191D, and 57 tar drums.

4) The following containers were found on the OHM inventory list, but noton site: 189G, 192D, 192B, 164E, 124, 162, 197, 243A, 192C.

5) Two (2) overpacks labeled as being #193 were found on site. One (1)actually contained Drum #220 (an "empty" as per your list).

6) The drum logs from Wastex listed two (2) drums #205 on the Non-Flammable Solids list. The Wastex logs also listed Flammable Inorganics asNon-Flammable Inorganics, although the flashpoint was 102*F and the disposalsite was expecting Flammable Inorganics.

7) The drum logs from Wastex, which were used to arrange disposal, hadeach small container listed separately as if it were a 55-gallon drum. Theseconatiners, numbered from A to F on the Wastex sheets, when bulked andoverpacked, actually resulted in much smaller loads to the TSDs.

A R I

Pagan Road Drum SiteMarch 24, 1987Page Two

8) OHM neglected to inform the OSC that 42 drums, all of which wereoverpacked during the week of March 16, 1987 by SLC, were considered "empty" byOHM. The drums were subsequently removed from the overpacks (once the OSC wasinformed of this) and the majority of "empties" were found to contain wasteliquids and solids.

9) As a result of not identifying the presence of tar drums before mobeon March 16, 1987, disposal arrangements could not be made, thereby delayingcompletion of the removal further.

10) On March 23, 1987, the OSC and TAT were informed by Chem Waste inEmelle, Alabama of that facility's refusal to accept the waste shipment sentoff site March 18, 1987. At first Chem Waste could not accept the wastebecause the drums were labeled as being 19 drums solids and 5 drums liquids, asopposed to the 20 drums solids and 4 drums liquids shown on the manifest. Thedrums were opened at Chem Waste and found to contain either solids, liquids orsludges, of which there were 4 drums. After this problem was resolved on March23, 1987, Chem Waste called the TAT (Pat Donegan) on March 24, 1987 andinformed her that the shipment could not be accepted because the manifest IDNumber (D003) did not match the WPR ID Number (P030). After much checking onour part, it was determined that the WPR, original sent to Chem Waste, ModelCity, was sent to Chem Waste, Emelle internally after Model City was found innoncompliance. According to a Chem Waste, Emelle, representative, the WPR IDNumber was changed in their office to P030 after a phone conversation with aMr. Roger Wheelock, an OHM chemist who approved the change. This revision didnot go through OSC Dave Wright or myself, and furthermore, there was no copy ofthe revised WPR in our files, resulting in misunderstandings and confusionbetween EPA, TAT, ERCS and the TSD. At this writing, this issue has not yetbeen resolved, and the wastes remain in temporary holding at Chem Waste.

As you know, we also continue to await your selection of disposal sitesfor the drums remaining on site.

In conclusion, your firm's performance during this job has been totallyunsatisfactory and has resulted in additional expense to the project, for whichEPA will not be responsible.

Very truly yours,

U.S. ENVIRONMENTAL PROTECTION AGENCY

Vickie L. Province,On-Scene Coordinator

RRI 0-157

APPENDIX B

BACKGROUND INFORMATION

.Suiic J, 50'JO txiilfdl Highway, IVims.mUn, NJ

THC'.HNICAL ASSISTANCE TEAM FOR EMERGENCY RESI'ONSE REMOVAL AND I'KLVI'NTIONLl'A CONTRACT 6JJ-OI-666V

MEMORANDUM

TO: Roger Meyer, OSC, EPA Region III TDD #8410-71Tftfr- Tttomto / mA £T) Dty £?# jjftLTHRU: Rich Habrukowich, TATL, Region Ill/My PCS #3073

FROM: Garrett Arai, TATM, Region III

DATE: October 22, 1984

SUBJECT: Coon Refrigeration, Inc. Site Assessment

On October 16, 1984 the Emergency Response Section received a call from thePennsylvania Dept. of Environmental Resources (PADER) in reference to 300drums stored by the Coon Refrigeration Co., Inc., 8164 Pagan Road, Erie, PA.

At approximately 1630 hrs. on October 16, 1984 Tom Massey, Chief, EmergencyResponse Section, contacted On-Scene Coordinator Roger Meyer in Bradford, PA corelay the message and check out the situation.

On October 17, 1984 OSC Roger Meyer and TATM Garrett Arai met Mark Gorman(PADER Field Inspector) at 1015 hrs. to discuss the initial situation. MarkGorman indicated that Tri State Insulation was the previous owner of thebuilding and Mr. Coon was the previous owner of that company. The name of thecompany has changed to Coon Refrigeration, but Mr. Marlin Coon (814 866-1711)is still the owner. •Mr. Gorman stated that the State has given the Coon Refrigeration Co. a letterof violation and wanted Mr. Coon to clean up the drums and the property. CoonRefrigeration began to clean up the drums and property by consolidating similarmaterials together from 5-gallon cans into 55-gallon drums and also burningmaterials from drums. Mr. Gorman also stated that in previous conversationswith Mr. Coon that Mr. Coon didn't know the hazardous properties of thematerials involved, and did not have safety data of the materials. Mr.German's opion was that a bigger mess was being created by the cleanupactivities of Mr. Coon.

At 1040 hrs. OSC, TATM and PADER arrived on scene and gained entrance throughMs. Velma Southworth, a secretary of the company. Mr. Coon was not present.

PADER has taken samples of water from a pit that was dug by Coon Refrigerationand one drum for VGA's, cyanate and cyanides. The analyses are pending andwill be forwareded to the OSC.

Roy F. Weston, Inc.SPILL PREVENTION & EMERGENCY RESPONSE DIVISIONIn AtkOcUfion with ICF Inc., Jacobs Engineering Group I nc.,C.C. Johnson & \ :>CK.LAC.CS. luc.tanJ Telru Tech, Inc.,

MEMORANDUMCoon Refrigeration Site AssessmentOctober 22, 1984

Page Two

Facts and Statistics

1. Approximately 280 to 300 drums are present scattered in wou<ls and arouuJthe building.

2. Approximately 100 to 150 actually contain materials.

3. Approximately 100 5-gallon containers are present in a pile Umpcy an<lbent).

4. Approximately 50 5-gallon containers are present with materials(scattered).

5. A burnt ash and waste pile is present; approximately 20 to 25 cubic yards.The ash pile contains paint cans, thinner cans, 1 drum, ashes, soil, metal,etc.

6. A pit in the woods waa dug with 1 5-gallon can and a cardbojr.l box in it.Water was in the bottom of the pit; 12* x 8' x 6* deep.

Drums with Labels

Blue drum: Polymeric Isocyanate White drum: Foam Systems Co.M.I.C.S. llreflex 108103 Evergreen Avenue Batch No. ROSC-13Pittsburgh, PA 15208 Brown - 55-gal.

Orange drum: Foam Systems Inc.P.O. Box 5347I960 Atlanta AvenueRiverside, CA 92507(714) 684-8333

PDLPolymer Development Labs, Inc.69-83 Dickinson StreetNewburgh, NY 12550(914) 561-5500 (polymethlene polyphenol isocyanate)

MEMORANDUMCoon Refrigeration Site AssessmentOctober 22, 1984

Page Three

Summary

Upon entry to the drums a slight odor was apparent. HNU readings indicated0-0.5 readings. The point source was discovered to be the burned waste pile(approximately 25 cubic yards) which registered readings, at 5-10 ppm. Ten feetaway almost no reading was apparent.

Drums were scattered upright and laying on their sides. Drums and 5-galloncontainers were found in the woods, at the edge of the woods, in the open areabehind the building, and right next to the building. One drum WHS found in thewaste pile, and one 5-gallon can was noticed in the pit located in the woods.

Next to the waste pile a pile of empty and buried 5-gallon cans was presnc. Astack of empty 55-gallon drums, some of which were burned, was also on theproperty. Upon entry into the woods a corroded drum halfway down the side wasnoticed containing oil. Drums were scattered in a 200-foot radius. Si m i l a rdrums seemed to be stored together. A small pit was dug approximately 100 feetinto the woods. The size of the pit was approximately 12* long x 8* wide x 6'deep. (Mr. Coon admits to having previously put "junk" into the pit.) One5-gallon can and cardboard were all that was noticed in the pit. The pitcontained about a foot of water.

The condition of the drums seemed to be fair to good. Some were punctured,corroded, and one was noticed to have been shot with a rifle. About 6 to 10drums were bulging on both ends. Holes were noticed in a couple of thesedrums. One drum was noticed open with paint sludge in it. HNU readings w^-re10-20 ppm at the top of the drums.

Types ot materials that were noticed in drums were asphalt, oil, paint ream,and reacted foam insulation.

Two drums were noticed to be leaking. One drum was on its side leaking oil.One drum was leaking a syrup-like (clear) resin material.

Mr. Coon previously stated to Mr. Gorman that solvents of xylene, MEK andmineral spirits were used to clean out the coating lines used by therefrigeration company. Small quantities of freon and isocyanate resin couldalso be present.

An attempt is being made by Mr. Coon to clean up the property. Very littlesoil appeared to be contaminated on the surface.

MEMORANDUM jCoon Refrigeration Sice Assessment .October 22, 1984

Page Four

Recommendation , , .

The Scat* should try to work with Mr. Coon and advise him more clearly of theRCRA regulations. Advice of what not co do and "just to clean it up" isinaufficient. Advice of what is hazardous and what is non-hazardous and howthey should separately be treated and disposed of should be sufficient. A listof waste disposal facilities and contractor! and a tine frame for cleanup wouldbe adviseable. . .

CHA:lal

Attachment

.* • *,•

f

ftRIOO!62

SUBJECT

av r>ATP >•> DIV -S- SHEET __ /__ rCHKD BY ____ DATE ______ DEPT _______ W D. NO. . _ . _______

O 0^ t>

TZ." U'/

\

f l R I O O I 6 3

Suiic 3, 5090 Central Highway, I'emiNaukcn, Nj UttlUSl • i«nW-

TECHNICAL ASSISTANCE TEAM FOR EMERGENCY RESPONSE REMOVAL AND PREVENTIONEPA CONTRACT 68-01-6669

MEMORANDUM

TO; Roger Meyer, OSC, EPA Region III PCS #3073Titty*. J0ff\ ffif&&, VflO, tP*THRU; Rich Habrukovich, TAIL, Region III

FROM; Garrett Arai, TATM, Region III £&.

OATEl November U, 1984

SUBJECT: Coon Refrigeration

On November 13, 1984 TATM Garretc Arai contacted PADER, Mark German, inreference Co the status of Che Coon Refrigeration Sice and pending analysis.

Mr. Gorman stated chat che analysis shows Che following:

1) Low level VOA concentrations from rainwater accumulated on cop of drums,

2) no contamination in the well water from che plant or nearby house,

3) no contamination in the neighboring pond, .

4) trace chlorinated hydrocarbon concentrations in che small excavated pic inChe woods. - - . -

A list of cleanup and disposal contractors haa been supplied co CoonRefrigeration Company by the Scat* of Pennsylvania.

CHA:Ui

Roy F. Western, Inc. A R I 0 Q I 6 USttLLPttEVtiXTlOK 1 EMEfcaV.T-iCY RKSl'ONSi* DIVISION Hn ' U

M E M O

TO: Thonas I. Massey, Chief Response Section

FROM: Roger L. Meyer, OSC

DATE: 11/20/84

SUBJECT: Sice Investigation: Coon Refrigeration, Erie County, Pa.

On October 16, 1984, Roger Meyer was notified of a potentialproblem at che Coon Refrigeration Plant in Erie County, Pa.TAT Garrett Arai and OSC Roger Meyer wet with PADER RepresentativeMark Gorman co investigate conditions ac chis site.

Enclosed is a copy of Che crip report furnished by GarrettAral, TAT, and the analytical results from sample, taken by PAOr.R.

This site hsa been referred to the State wich Che recommendationthat further, more complete guiudance should be given to Mr. Coonin his clean up effort that is currently on-going ac che State'sdirection.

If there are any further developments ac chis location theState, Mark German, will notify EPA for additional assistance.

PRELIMINARY ASSESSMENTTRI-STATE PAGAN ROAD SITE -

McKEAN TOWNSHIP, ERIE COUNTYPENNSYLVANIA

Wastes have been scored and disposed ac che Tri-Scace Pagan Road siceac lease since approximately 1982. Material on site reportedly consists of thefollowing: off-specification asphalt coating diluted wich xylene and toluene;waste urechane foam impregnated (at lease ac che time of disposal) withsolvents such as methyl echyl kecone, methyl Isobutyl ketone, and naptha, whichsolvents were used Co clean foam spray/injection equipment; spent and/or off-speclficacion urechane foam components containing up Co 302 trichlorofluoromethane; spent methyl echyl kecone; and various other produces used in cheurechane foam/foam coaclng business, which produces are believed Co contain orga-nic chlorinated and non-chlorinated solvents. Ac lease some of che above-listedmaterials have been spilled from and/or leaked from drums on-site onto theground surface, potentially leading to groundwater contamination.

Strong solvent-type odors and hlgher-Chan-background HNu photoionl^erreadings indicate site air contamination from contaminated soils and open drums.A mixture of solvent-contaminated soil and waste is piled-up on che site and hasbeen observed co be a source of air contamination, as indicated by an HNu photo-Ionizer.

The populacion around Che sice is relacively sparse, although che fewrural homes and che one small business in che area depend on private wells as .twater supply. One nearby well has been sampled. Those results indicated no con-tamination.

Ownership of cbo chemical materials (wasces and produces) on site and,therefore, sice wasce removal and remedial work is being held up by litigationInvolved In tha bankruptcy of Tri-Scace, Insulaelon, ehe previous occupant of thesice and probable generator of Che wasce« on sice. Marlin Coon is che Presidentof Tri-Scace Inaulatlon and of Goon Refrigeration, che firm presently occupyingche business ac che eice and owning che site property. Mr. Coon had Implementedsome initial druuMd Material consolidation at Che site. However, that work hasbeen stopped pending resolution of che bankruptcy proceedings.

Methodist Bldg, Suite 112, Eleventh & Chapline Streets,Wheeling, WV 26003 • (304) 233-1610

TECHNICAL ASSISTANCE TEAM FOR EMERGENCY RESPONSE REMOVAL AND PREVENTIONliPA CONTRACT 68-01-6669

TRIP REPORT

DATE: June 28, 1985

SUBJECT: Preliminary Site Assessment, Coon Refrigeracion PCS: #3362Pagan Road Sice, Summit Township, Erie Councy, PA TDD: #8505-05

FROM: William FolleCC - TATM Region IMark Selman - TATM - Region III

THRU: Sceven Jarvela, DPO, Region III

TO: Jack L. Downie, OSC - Region IIIWheeling, WV - Emergency Response Section

Please find attached:

- Trip Report- Sice Sketch- POLREPS- Photographs

n n • f> ' r -»M n i U j l 6 /

Roy F. Weston, Inc.SPILL PREVENTION & EMERGENCY RESPONSE DIVISION' >vs I •linn w«fh Iff" Itic f-.ti-olr* (••! •im-rriiv f • ',. • !,.».- _n 5 * •' >if '

OSC Jack Downie and TATM's Mark Selman and Bill Follett met with PADept. of Environmental Resources, Solid Waste Specialist, Mark Gorman atthe PADER, Meadvilie Regional Office. The meeting was Co discuss the CoonRefrigeration Pagan Road Site and the Rotunda Drive Drum Site, scheduledto be assessed June 19, 1985. PADER supplied the OSC with maps of thearea, analytical results of previous PADER sampling and results of thePADER preliminary investigation.

Until filing for bankruptcy on November 15, 1983, Tri-State Insulationoperated an insulation and coating business at the site and is the probablegenerator of the accumulated wastes. Mr. Marlin Coon is the president ofTri-State Insulation and of Coon Refrigeration and is currently operatingCoon Refrigeration from the facility.

Mr. Gorman stated that Mr. Coon had implemented some initial materialconsolidation and cleanup efforts at the site. However, the cleanup actionshave ceased pending resolution of the bankruptcy proceedings. Mr. Coon andMr. Vedder White (Trustee for Tri-State Insulation) cannot agree upon theownership of the inventory and the wastes. Mr. White wanes Co take posses-sion of the inventory and not the wastes, while Mr. Coon insists that allInventory, wastes and remedial action liabilities be taken by the Tri-StateInsulation trusteeship. No agreement has been reached.

Mark Gorman informed the OSC that the PADER was drafting an order tothe responsible parties for the cleanup of the drums and contaminated soilbut anticipates that an appeal of this order to Commonwealth Court will de-lay Implementation.

Arrangements were made with the PADER to meet with the OSC and TATMsat the Pagan Road Site at 0900 hours, June 19, 1985 to conduct the prelimi-nary assessment.

Wednesday June 19, 1985

0900 hours - OSC and TATMs met Mark Gorman, PADER at the Coon Refriger-ation Pagan Road Site. The assessment team met with Mr. Coon who explainedthat che materials located onsite included solvent thinned asphalt roofcoatings, resin side of urethane foam, silicon coatings, and the solventsused for equipment cleanup. Mr. Coon stated that he initiated some bulkingof materials by consolidating five gallon cans of material into 55 gallondrums but had to cease these efforts pending che outcome of the bankruptcyproceedings. He also provided the OSC with technical data sheets for someof the raw materials onaite.

During a tour of the site with Mr. Coon the assessment team observedapproximately 170 drums and five gallon cans in the rear of the Coon Re-frigeration building. About 120 of these drums were stacked three drumshigh in rows of 40 drums against the wall of the building. On the topmost row of drums was an undetermined number of five gallon cans. Also,at least 20 55 gallon drums were observed on their sides, some leaking atthe rear of the stacked drums. These drums are within ten yards of thedrinking water well that supplies the property and within 50 yards of alarge pond. A R i 0 C ! G 8

Further observations of the site revealed many other drums in variousconditions scattered around the property and in the wooded area at the rearof the property. Some of the drums in the wood appear to contain asphaltand are in poor condition, the contents of some have leaked on Co the ground.

Drums labeled polymeric isocyanate, mineral spirits, Dow Corning (siliconprimer), trichlorofloromethane were observed (see photographs of drums labels)

Many five gallon cans were observed in the woods and a 6'xl5' pit con-taining 5* of water contained floating five gallon cans and a drum.

A 20-30 cubic yards waste pile containing contaminated soil scrapedfrom the drum areas and an obviously burned five gallon can was observed.

A total of approximately 250 drums and an undetermined number of fivegallon cans and other containers are scattered around the site.

After the initial visual inspection of the site, TATM's Mark Selman andBill Follett screened drum contents with the HNU Photolonlzer, OVA-128, andexplosimeter with oxygen meter. Samples were collected from drums exhibitinghigh volatility (by the OVA-128) and the presence of explosive vapors.

TAT observed the following:

* Foam Systems Co., orange drum with brown lettering, drum had holepunched in it. 400 ppm - OVA No explosivity readings (no samplecollected).

* DOT 17E Drum, FlasChem coatings, black drum with white top, rusecolored stains on drum. >1000 ppm OVA 90Z LEL on explosimeter.Two 8 oz. glass jars of rust colored gel-like material were collected(Station #02).

* DOT 17H Drum of black thick asphaltic material, OVA MOOO ppm 20%LEL. Two 8 oz. glass jars of the viscous semi-solid were collected(Station #01)

* Brown drum with orange lettering, label reads: Contains isocyanatecompounds. No OVA readings due to lack of oxygen Inside drum02 < 16Z. One 8 oz. glass jar collected of grey semi-solid.(Station 104).

* White drum labeled "Uref lex" Foam Systems Co. , OVA MOOO ppm,explosivity 35Z LEL. One 8 oz. glas jar collected of clear gel-like material (Station #06).

* Blue Dow Corning drum, 3-5000 silicon construction prime coat,color dark grey. OVA MOOO ppm, explosivity 24Z LEL (No samplecollected).

* Orange drum with brown letters, "B" stenciled on top of drum. OVA>1000 ppm, 202 dropped from 21.5Z to 16Z inside drum explosivity2-3Z LEL. Label reads contains Trichlorfloromethane. Two 8 oz.glass Jars collected of a brown viscous liquid (Station #06).

* Drum labeled Polymeric Development Laboratories, Inc., 17E Drumblack with white top OVA-85 ppm, explosivity no readings, 02 - 182(No sample collected).

* Five gallon cans near pit - two samples collected of a beige gel-like material (Station #03).

* Composite samples collected from waste pile. Two 8 oz. jars andtwo 40 ml VOA vials of soil were collected (Station #07).

A total of seven samples were collected and arrangements were made withWeston Labs for Priority Pollutants, RCRA Ingitability and RCRA Reactivityanalysis. Analytical results are expected by July 15, 1985.

Summary

The accumulated waste materials improperly stored and disposed of atthe Coon Refrigeration may pose a significant threat of harm to publichealth and the environment. Analytical data from samples collected shouldconfirm our opinion that this site conforms to the stated criteria for aCERCLA Immedite Removal Action. The wastes present pose the threat of fireand explosion and of direct human contact to known hazardous and toxicmaterials. Additionally, continued releases of these materials may Impactgroundwater .which supplies drinking water to 21 residences within a quartermile of the site.

Efforts should be undertaken to prepare and submit an action memorandum•:o mitigate the hazards posed by the Coon Refrigeration, Pagan Road Site.

Photograph *1 - Small vaste pile on-site. There is evidencethat the pile was burned at one time.

Photograph t2 - Waste pile. Note the proximity of" n

'.„•» v. a-

A R 1 0 0 172

Photograph <5 - Drove along tht tret line. More druan arelooted in the wooded are*.

Photograph *6 - Druu leafcinc fron the bong. Hot* thecontaminated aoil. . . ;

AR I 00173

*7 -.One of the leaking drum in the wood..

ii - Excavated pit in the woo-i. The pit ia overfeet deep and may contain other container* of vacte.

A R I O O I 7 I -

Photograph 49 - Asphalt coating drums inside the voodcdarea. Th* mound in the foreground may hide buried containers.

Photograph flO - Ruptured • sphdt drum th«t It** Ic.kcd it* „' . _ _r t«t". " A R I Q 3 I 7 5

Photorraphg f 13 t -^14 * TJLT campling drums on-site*

AR I 00 I 76 \J

Photographs *M5 ft f!6 - Drum labels

AR I 09 177

Photographs 017 & #18 - Dram labels

AR I 03178

DATE. ————— DIV ________ SHEET —————————— OFCHKO BY ———— DATE 6t PPPT ——— ,,0.

SUBJECT

flRIOOI79»t

SUITE 3. SO*) CENTRAL HIGHWAYPENNSAUKEN NJ08109HHONE 609-663-7995

MEMORANDUM

TO: David P. Wright, OSC, U. S. EPA, Region III PCS*: 5265

THRU: Richard Habrukowich, TATL, Region III *"

FROM: Patricia A. Donegan, TATM, Region III

SUBJECT: Pagan Road Site Assessment of June 9, 1986

DATE: June 24, 1986

TATMs Donegan, Janlec and MazeIon mobilized by 2000 hours on June 8, 1986, toperform an assessment of the Pagan Road Drum Site in Summit Township, ErieCounty, PA, with OSC Dave Wright on June 9, 1986. The assessment consisted ofLevel "C" and "B" site inspections by TAT and EPA with air monitoring in Level"B" with an HNU, an OVA, a CGI-02 meter and a radiation meter.

The site consisted of an abandoned 42* trailer filled with various sized drums,as well as approximately 50 drums scattered on the ground surface nearby. TATopened several drum* and took drum and spillage samples to permit observation ofthe physical state of the material at the site. Organic vapors at high levels(>200 ppm) were detected in drums at the site and in the ambient air in thetrailer once the tailgate was opened. No radiation above background wasdetected on site.

TAT reported site information to the OSC, who designated this site for emergencyremoval action. TAT prepared a Special Bulletin POLREP on $50,000 Authorizationand followed up with a Request for Additional Immediate Removal Funds. Due toactivation of the $50,000 emergency funding, all TAT personnel were required tocontinue providing on-acene technical assistance until June 13, 1986, at whichtime the staging, sampling and overpacking of drums was completed.

Also, TATM obtained drinking water samples of five residences near the site onJune 11, 1986, aa per OSC instruction. The results of the analysis and sitesketch are attached.

All phases of the site assessment and the initiation of removal actions wererecorded on film by a National Geographic film crew.

A R I O G i C OPAD:ah

CLIENT/SUBJECT l4-<FlPA - PS t &. LVAJ hL __________1_ W.O. NO____________TASK DESCRIPTION d /t ttt-lA. fbUjjt*. AubL. L M jd r t cL TASK NO 2 5"

/)n~\ f J" ' /i I . ________________if mm A f^a , + / + I m+ / ~ ~ • ~ ~"~———"™——PREPARED BY r.fl.A.______ HPPT 73T____ HATF A/la./to APPROVED BYBY—————————— DEPT_________ DATE-

METHOD REV. BY _________ DEPT_________ DATE. DEPT______ DATE_ ___

' AA*Avirtr \

»6C-mV*r*Tn"•-X7™t r 3r** ^ ^ ^

&(£-ar»rr>*<SatnAi

Coont ' ' "

*mt

fjm.fit>m.HCm>

an 103 is

MESTON SPER DIVISIONHQZQRDOUS WQSTE SITE INVESTIGATION QND EMERGENCY RESPONSE"

SAFETY PLftNREGION I I {~

Qss i gnor : J ) ^ e. W r-. t* ________ _. _______ TDD No. __£&55Date of Inspecti on :__5jL 2-._fc Time: _ _. ____ PCS No. l£._L?_Original Safety Plan: Yes_^_ No ___ Modification No. _~~_

Site Name s i-/ l>-\g fiJLjL .JU

Site Address: Street No.CityCountyState _______ A _____ Zip Code

Site Contact : /ft tLtJLs<. Qt-rtLo . fcuXbt Phone //f/jfj £4..~/>lcU./ ' "

Directions to Site:

Map ftttacned: V e s _ _ NoIf Remote Location: Latitude__________ LongitudeSITE HI STORY :

INCIDENT DESCRIPTION (cheek one from A, &, and C>

TYPE; ft) Spill___ ftir Release_.__: Fire___ HW Site_^_ Other___

B) Assessment___ Sampling___ Emergency Response____

C1 ean-up/Remova 1 ____/Ot her X spec i f y) fji JLToJ n<UHMJ.- *zZ~~- f\d SGUH&CLAG.

C) Ur ban/Res i dent ial___ Commercial___ IndustriaT___

Rural_vC_ Remote____

PHYSICflL DESCRIPTION

Size of Site:_________ Terrains______.__^_ Weather:___________

Containers Involved In the Release or Incident

Drums_j/'l_ No. _25i? Tanks_._ No. ___

Truck___ License No. ____ Tanker__ Box__

Railroad Car___ Tank No.___ Box No.__

Spill___ Source_________________________ Approx. Vol._______

a.j

MATERIALS INVOLVED;

Name '&& PEL. //W) IDLH Cp/ ) ,1 Overexposurejf**"! Symptoms

SPECIAL HAZARDS:

ANTICIPATED LEVEL OF PROTECTION (circle one) : A C D

WHY : 0 ^ 4< / ^

FIRST AID INSTRUCTIONS FOR KNOWN CONTAMINANTS:

PERSONNEL EXPOSURE HAZARDS: <H»hight M-moderate, L«lowf U-unknown>

Inhalation__\_^ Skin Contact^ _ Ingestionj^_ Radioactive __

Biological ___ Pil>"«____ Explosion_\_f__ Unknown ___

PERSONNEL PHYSICAL SAFETY HAZARDS :

H«*t_wl_ Cold ___ Noise ___ Underground Utilities ___

Overhead Utilities ___ Heavy Equipment ___ Slip. Trip, Fall_v/_

Sharp Objects ___ P'ressurized Airlines ___ Cycl indersj,2__

Ladders __ _ Scaffolds ___ Unguarded Openings-Mall. Floor ___

Liquids in Open Containers, Ponds, Lagoons ___ oS ~ ~ A R 1 C 0 I 0 0

ACTIONS TAKEN ON SITE;fie/-*

Was Entry Made: YES_jl_ NO.

/ rSCBA_i ._ APR____ Model______ Cart./Can. Type______

Tyvek___ Poly Tyvek___ Saran Tyvek_v_/_ Acid Suit___

Rain Gear___ Cotton Coveralls___

Gloves: Inner_^_ Butyl__ Nitrile__ Viton__ Other__

Foot Gear: Safety Boots \j Outer Boots__ Booties__/ Othi

Description of Decontamination Used; _Q £££• •"} t"r*\ <: IS. rCCj._ .a**k_I ~ _ __ V _ I _ ._.. -" - 1 . Z ~ -* . -i_. . . t *J >*» _ - —^Lj±S h:vr. _fir jpj«sflA r i.'

MONITORING __ . Performed b y :~7o (k. trfrrmctL . CUL uL**. . t f z e K , /

Instrument Readings: Radiation Meter_____ CGI______

OVA_____ HNU_____ Detector Tube___________

Other_______________________________________

Wind: Speed___ Direction____ Temp. ____ Rel. Hunt.____ B. P.___

Summarize ftir Monitoring Data________.______._____________————

SAMPLING Performed by :

Sampling Plan <Y or N) ^__ If yes attach copy to safety plan" ————

No. of Samples: Solid ____ Liquid ____ Gas ____ Other

Laboratory: _________________________________

Has Lab Been Notified of Potential Hazard Level? Yes_J-No — _

Ana 1 yses :

Sarnpl ing Comments:

DOCUMENTATI ON Performed by: __QJS£__SQ_,_«_-__

Type: Photo__^/_ Log Book___y__ Recorder____ Video______

PUBLIC IMPACT

Distance to Nearest t Residence____ School___ Hospital___

Public Building___ Other_____________

Evacuation: Yes__ No_j__ Number____ By Whom:_________________

ENVIRONMENTAL IMPACT:

Nearest Waterway:_.____________________ Distance:_______

Cond it ion Observed Potent ial Norn

Surface Water ContaminationGround Water ContaminationDrinking Water ContaminationAir ContaminationSoil ContaminationStressed VegetationDead Fish, Other Animals

PERSONNEL INVOLVED; < NAME, AGENCY. PHONE, ON or OFF SITE )

SITE MANAGER :

SITE SAFETY COORDINATOR;

Have Read - Understood TheSite Safety Plan (check)

EPA

TAT

STATE

OTHER

EMERGENCY INFORMATION

EMERGENCY PHONE NUMBERS:Location Phone Notified(Y/N)

FirePolice

AmbulanceHospital

Nearest Phone _________________ __________________

DIRECTIONS TO HOSPITAL;(ATTACH MAP)

ADDITIONAL EMERGENCY PHONE CONTACTS;

CHEMTREC (800) 424-93012TSCA HOTLINE (SOiZD 4£4-30fc5. (2*2) 554-1434CDC (404) 452-4100 (day), (404) 329-2688 (night)BUREAU OF ALCOHOL, TOBACCO 4 FIREARMS (800)424-9555,(202)566-7777NATIONAL RESPONSE CENTER (800) 424-8802WESTON MEDICAL EMERGENCY SERVICE (513) 421-3063 ( 24 hour )WESTON 24 HOUR HOTLINE (215) 524-1925, 1926PESTICIDE INFORMATION SERVICE (800) 845-7633EPA ERT EMERGENCY (201) 321-6660RCRA HOTLINE (800) 424-9346BUR. OF EXPLOSIVES, A. A. RAILWAYS (202) 835-9500

Prepared by:

Reviewed by: _________________T_______ Date:

Approved byi ________________________ Date:

SPER HSO Review by:___________________ Date:.Followup Required: Yes___ No___Followup Performed: Date:_____ With:,Comment s: ________________________—

A R I G O I G G

H R I G C I 3 7

APPENDIX F

PHOTOGRAPHIC DOCUMENTATION

R R I O J l S S

Pagan Road Drum SiceFederal OSC Report

APPENDIX FPHOTOGRAPHIC DOCUMENTATION

Photo # ______7________Date Taken March 17. 1987Photographer Pat Donegan, TATDescription Wooded area was smoothed over following removal of drums.

R R I O U 1 3 3

Pagan Road Drum SiteFederal OSC Report

APPENDIX FPHOTOGRAPHIC DOCUMENTATION

'

'

PhotoDate Taken March 16, 1987Photographer Pat Donegan. TATDescription ERCS personnel marking and overpacking drums in preparation

remove them from wooded area.

AR I 00 I SO

Pagan Road Drum SiteFederal OSC P r-ort

APPENDIX FPHOTOGRAPHIC DOCUMENTATION

•JW*//'> i,'iE.il.V/----"'/1' -*'*»-tN

Photo #Date Taken March 16. 1987Photographer .Pat .Donegan., TATDescription ERCS personnel removing overpacked drums from wooded area.

A R I O O I 9 !

Pagan Road Drum SiteFederal OSC Report

APPENDIX FPHOTOGRAPHIC DOCUMENTATION

.;• •*-_.-, ••;•>••?*'**>•••-;.,•

PhotoDate Taken March 17, 1987Photographer Pat Donegan. TATDescription ERCS subcontractor SCA staffing overpacked drums that were

removed from wooded area.

Pagan Road Drum SiteFederal OSC Report

APPENDIX FPHOTOGRAPHIC DOCUMENTATION

l-' '- f - jf S *-' ;"":.-f":"v" 7"j!«t-'' -.;;&»*>& vr >'•*'••''*''S---:s'""" .'» -•*+*4rv/i;t ' 5- '"'"-'I' te a ^ vk,;.iS :1 V ?,"•'•.'v*7J-.-'- T - .1 •.*.'7K,,-- ;.-->•'-.-,/,. :.. icV :-,fj;T.» _Ajt-*: V*i. . : ri*|te|v%j:!H:J?'•' • ;i':"%:;r4;J; ;'v- -;v f '-| - ' ?5:-%:SK^iilUl&iMiB*iA « i V!u.juadiM*w£ Jj MlnSlMb«MuUrii MttlHl ^

^ -'-.•=---:'". .-"".-.v.-' -s&i!--:- :- -• ...''a ,;

PhotoDate Taken March 17. 1987Photographer Pat Donegan. TATDescription Overpacked drums were properly placarded for transport off

site.

A R I O O I 9 3

•»: •,•.--•**..

Pagan Road Drum SiteFederal OSC Report

APPENDIX FPHOTOGRAPHIC DOCUMENTATION

<— iw ••* r-r-Trf-•- - -3I>-'

PhotoDate Taken March 17. 1987Photographer Pat Donegan. TATDescription Staged overpacked drums awaiting..transport.

Pagan Road Drum SiteFederal OSC Report

APPENDIX FPHOTOGRAPHIC DOCUMENTATION

,

-v, .. iy.^Mv***?1**^

Photo // ______6_______Date Taken March 17. 1987Photographer Pat Donegan. TATDescription ERCS subcontractor SCA loading overpnckpd drums onto truck

for transport to SCA facility.________________________

A R 1 0 G 1 S 5

APPENDIX 6

POLREPS

A R I C : i 2 S

POLREP II - Coon RefrigerationPagan Road SiteSummit Twp, Erie Cty, PA

I. Situation (6/19/85 - 2000 hours). . — • . •< • • • - • • « _ '

A. Per Bonne Ion scene: .'

•TAT - •>•• •-•••••- • --• "• - •--. i • . TAT ••*••• 2 '- •• ••I Uv'. '-.: - PADER ;- 1 '- :- '.. =' '•Coon Refrigeration - 1 r fi

. • ' . . . ' ' " ' • . • ";-: ' ' -. '• '• ' ' -.'.".'-• -CivvV; "• ' •-: .

- - ^• - , C. At the request of PADER,. OSC conducted a preliminary asaecament' at: the Pagan Road site thia date. The now defunct Tri-State Inaulation jwaa ; ,;•/::a commercial industrial- applicator of •- foamed inaulatlon" and reaia'cpatings. "X; ;^ The materiala .handled J>y the company included: poly-aerie iaocynatea, ure- j ';. ;".thane foam precursors, silicon primers, asphalt coatings and industrial:.; '' '..solvents for solubilizlng resins and equipment cleanup/ The solvents^ included,xylene, trlchlorof lorome thane, MEK, MIBK, and others. The containers- , observed

.onsite are. the remaining inventory of raw materials, off-spec produtaV andwastes generated during operations. PADER has requested EPA assistance becausecurrent ownership of the raw material inventory and waste materials has been .complicated by bankruptcy proceedings involving former operator Marlin Coonand a court appointed trustee for Tri-State Insulation. This controversy hasled to delay in cleanup actions. ; • • . • - . vi:.': '•

• " ' " " • " ' ' '- ' '. ' ••• '''•': <•-' •, '. ' ?'.i\ ',-* •:,•''„•; D. Prior assessment conducted by E PA/TAT in October 1984 revealed .approx.280, drums sea ttered. around Ivthe- property t', half of which appear to^pntaltt" ' .-,

v. ;Mee*rt«l«.i :"4|»p)r(D»rtMtiily ; 1/3 of "the;; 100 (5) gallon containers /In7yarious .lo-!: ;."' cations' oo Vfite.l contain" material. -v A small waste pile waaalsorobseryedr, At ',:,t hat. "tine tSe*'respoh8ible party appeared yllllng. to initiate cleanup. EPA" -.. ;^ supported responsible. party, cleanup wi,th coordination by state .RCBA- personnel.^ :'•..•;.-•;..'•• '• " ' •-. '; *' . »•"•'•;-. •''.'-'-.• •••.••:• : . - -• •.. • - :-'••• . jirV:-.;". *;'i* •;'&.';.•-••• - . - ; • ' . •• ';•-'•-.'•'•'•- - . •••"••• --. '; ~ - •*--O E. 0900 hours, OSC, PADER and TAT met with Marlin Coon, .owner of Coon^Refrigeration and former shareholder in Tri-State Insulation. '' Mr.' Coonvacated that the trustee of Tri-State Insulation Mr. Vedder White, ordered J.-1 . . '

Coon to not' disturb-' or use any of the contested materials, therefore,•••••&*••i«-i'*r«mremoval operations by Mr. 4 Coon we re. suspended until such time as•-- •• •- r •• • *' •-• . - - - • * -*• - - ...... * . *~ .. .' » -_• _r __.

-v vjw-,, ....-* -of vthe. drums^and cans ihaye 'been/stacked at the"rear'ipf:-5-J jf.rlger'atl.ir->? in'the .rear ,of;;theysitey vSome; of the drums -are^breached-^and s<V:J>V It is apparent' that'no effort is being, made, to contrpl or cleanup

''r::- ' B. TAT used OVA .and Exloalmeter to screen drums opened for; organl c-r.vapors-(and ignltable Vapors.' Some of the drums contained combustible vapora and of :.the drums sampled, all exhibited concentrations of organic vapors above i 000 ; V:.tpprn. .TAT collected six drum samples and one soil sample from-.the waste pile.,

1001

> riPage 2 - POLREP t\ - Coon Refrigeration

II. Actions Taken

C. Approximately twenty residences are situated within 1/4 miles ofthe site. Water is supplied by private wells and prior PADER assessmentof the Coon well indicated trace concentrations of one of the materialsfound onsite. The drums are located In an unsecured area and are begin-ning to show signs of deterioration, some have breached and leaked theircontents. Poor housekeeping is evident.

III. Future Plan*

. . - . - • . . . .- .•' : : ~'- ';";': :.4>>V . ''".'!C. OSC to coordinate with PADER on further response actions:as needed,

• D. TAT to ship samples collected 6/19/85 to commercial laboratory foranalysis. ''' '"' ;'" ;'•'' '' 7' ' '" •

_____&Zf>: '"' Y" ''• :.' •• • \; •:.::. -• -, > ?v -:-..-*-i.: -JfCK L.t Downie, OSC ,.-.•/ ,*

i.\ ""—•-'

TLX II RECV CONNECTED lO-Jun-86 14*22 33

EPAOHM PHA

'U INFOMASTER 4-O246648161-OO1 06/10/86C8 IPMMTZZ C8P8144362961 DGM TDMT UG ERIE PA 22O 06-10 0217P E8TTWX 71O67OO716 EPAOHM PHAEMERGENCY RESPONSE4218 EPA PHA

CERCLA REMOVAL ACTIONPAGAN ROAD DRUM SITESUMMIT TOWNSHIP ERIE COUNTY PAI. SITUATION UBOO HOURS 6-9-86)A. OSC MOBILIZED TAT PERSONNEL ON SUNDAY JUNE 8 1986 TO ERIE COUNTY PATO PREPARE FOR AN EMERGENCY ASSESSMENT AT THE PAGAN ROAD DRUM SITEB. NATIONAL GEOGRAPHIC FILM CREW ON SCENE FILMING EPA EMERGENCY RESPONSEPERSONNEL DURING THEIR ASSESSMENT PROCEDURESC. OSC DAVID WRIGHT SPOKE (113O HOURS 6-9-86) WITH THE POTENTIALRESPONSIBLE PARTY (MARLIN COON) TO GIVE VERBAL NOTICE TO CLEAN UP ANSTABILIZE THE EXISTING CONTAMINATION AND HAZARDOUS MATERIALS WHICHREMAIN ON SITE AT THE PAGAN ROAD SITE. MR COON DECLINED TO COMMENT UNTILHE SPOKE WITH LEGAL COUNSEL.

D. PERSONNEL ON SCENEl EPA-3 TAT-3 ERIE COUNTY HEALTH DEPARTMENT-2PADER-3 NATIONAL 6EOGRAPHIC-4E. WEATHER-SUNNY AND MILD, HIGH 7O'STI. ACTIONS 'TAKEN. EPA AND TAT PERSONNEL CONDUCTED A SITE ASSESSMENT AT PAGAN ROAD DRUM

SITE FINDING APPROXIMATELY 23O ABANDONED AND LEAKING DRUMS. HIGH LEVELSOF ORGANIC VAPORS WERE OBSERVED USING A FID AND PID.B. THE OSC ACTIVATED *5OK EMERGENCY FUNDING AT 16O6 HOURS THIS DATE FOR8TABLIZATION AND SAMPLING OF DRUMS ON SITE.III. FUTURE PLANSA. OSC TO MEET WITH ERCS RESPONSE MANAGER ON 6-1O-86 AT OOOO HOURS TOFORMULATE REMOVAL STRATEGIES AND OPTIONS.B. OSC TO CONTINUE TO UPDATE EPA REGIONAL OFFICE ON SITE ACTIVITIES.DAVID WRIGHT

1419 ESTAEPAOHM PHA

n D I p f. ! Q 0J-t i k I L - i J ^

ATTN TOM MASSE Y AND TIM FIELDS

POLERI

REP »3 CERCLA REMOVAL ACTION, PA6AN ROAD. DRUM SITE. SUMMIT TOWNSHIP,IE COUNTY PA

I. SITUATION 18OO HOURS O6/1O/B6•*-*

A. OSC, TAT ERCS EVALUATE REMOVAL OPTIONS FOR SITE. DISPOSAL OF ALLHAZARDOUS SUBSTANCES DIRECTLY WITHOUT TEMPORARY TSD OR ON SITE STORAGESELECTED AS BEING MOST ENVIRONMENTALLY SAME OPTION AND MOST EFFICIENT INMITIGATING THE THREAT TO PUBLIC HEALTH NOW IN EX I STANCE.

B. PERSONNEL ON SCENE i EPA-3, TAT-3, ERCS-1, STATE DER-O, ERIE COUNTYHEALTH DEPARTMENT-2, NATIONAL GEO6RAPHIC-4

C. WEATHER CLEAR, MILD HIGH 7O8

II. ACTIONS TAKEN

A. OSC MET WITH PROPERTY OWNER MARLIN COON AT O910 HOURS TO DISCUSSPROPOSED SITE ACTIVITIES AND INQUIRE A8 TO HIS INTENT TO ASSIST IN THEREMOVAL OPERATION. MR COON STATED THAT PRESENT LEGAL STATUS PRECLUDESHIS PARTICIPATING IN THE REMOVAL.

B. OSC CONTACTED EPA/OPA AND CARDINAL, EPA ENFORCEMENT VICK JANOSICAND EPA LEGAL ELLEN TIPLITSKI REGARDING SITE STATUS AND INITIATION OFACTIVITIES UNDER THE ftSOK AUTHORIZATION.

C. EPA/OSC TAT AND ERCS PREPARED AND EVALUATE OPTION OR SITEOPERATIONS. ERCS INFORMED OSC THAT AS OF THIS DATE, TEMPORARY STORAGEFACILITIES ARE EITHER UNAVAILABLE OR COST PROHIBITED DUE TO RECENTADDITION OF INSURANCE COST PER DRUM *1OO.

D. WORK OPTION SELECTED BY OSC WRIGHT TO MITIGATE THE THREAT AT THISTIME INCLUDES STAGING DRUMS, SAMPLING, OVERPACKING, RESTRICTING SITEACCESS, AND DISPOSAL OF ALL HAZARDOUS SUBSTANCES.

E. MR COON EXPRESSED CONCERN WITH VEHICLES BLOCKING ACCESS TO HISBUILDING. MR MAS8EY OSC REP FOR DAVE WRIGHT, SPOKE WITH MR COON ANDINFORMED HIM THAT VEHICLES WOULD NOT INTERFERE WITH HIS OPERATION.LIKEWISE, MR MA88EY REQUESTED THAT THE PROPERTY OWNER NOT INTERFERE WITHEPA OPERATIONS.

F. nar m»tftuT aiiaxTTTfp apcf-ffl*, MS i fTTfl. »£» *-g REGIONAL OFFICEDESCRIBING ACTIVATION OF EMERGENCY FUNDING ON JUNE 9TH 1986.

III. FUTURE PLANS

B. CONTINUE SITE OPERATION AS EMERGENCY FUNDING ALLOWS.

SIGNEDDAVID WRIGHT, OSC, EPA REGION 3 „ -, PPHILADELPHIA PA' p. n I P ~ 9 Q GDAVID WRIGHT, ON-SCENE COORDINATOR H F* » «- - -

1949 E8T

ATTN TOM MASSEY AND TIM FIELDS

POLREP 4CERCLE IMMEDIATE REMOVAL PAGAN ROAD DRUM SITE 1 STTUATQM (18OO HOURS6-11-86)

A. SITE ACTIVITIES BEGIN WITH FULL ERCS CREW PREPARING STAGING AREA ANDDOING INVENTORY OF DRUMS ON SITE. RAINY WEATHER LIMITING SITE ACTIVITIESIN USE OF HEAVY EQUIPMENT

B. PERSONNEL ON SAMElEPA-3, TAT-3 ERCS-6 NATIONAL GEOGRAPHIC-4 PA STATE HEALTH DEPT-1

CDC-1 PADER-O

C. ESTIMATED COST TO DATE COD 6-11-86 (CEILING »5OK)

ERCS EQUALS »13K

D. WEATHER SEVERE THUNDERSTORMS A LIGHTNING, HIGH 7O'S

II. ACTIONS TAKEN

A. ERCS PREPARES DRUM STAGING AREA. MUDDY GROUND PREVENTS USE OF 355 ONSITE AT APPROXIMATELY O8OO HOURS. MOBILIZATION OF 213 BULLDOZER WITHGRAPPLER REQUESITION BY OFC, 213 ON SITE AT 16OO HOURS THIS DATE

B. ERCS BEGINS INVENTORY OF TRAILOR CONTENT AS PER OFC INSTRUCTION AFTERAFETY MEETING. APPROMIXATELY 4O TO 43 DRUMS NEED OVERPACKING OUT OF 73

i>RUMS ON GROUND SURFACE.

C. SITE OPERATIONS SUSPENDED BY OFC-DESIGNATED SITE SAFETY OFFICER AT1710 HOURS DUE TO LIGHTENING STORM. ALL PERSONNEL OFF SITE AT 1730 HOUS.D. TAT DONEGAN WITH STATE HEALTH DEPARTMENT ASSISTANCE OBTAINED POTABLEWATER SAMPLES FROM 4 RESIDENCES NEAR THE SITE.

E. OFC HAS DETERMINED THAT COMPLETION OF SITE OPEATIONS INCLUDING LABANALYSIS, TRANSPORT AND DISPOSAL COSTS WILL REQUIRE ADDITIONAL FUNDING.A REQUEST FOR «19O,OO IN ADDITIONAL FUNDS WAS SUBMITTED TO EPA REGIONALOFFICE THIS DATE. DEMOBILIZATION OF PERSONNEL AND EQUIPMENT SCHEDULEDFOR 06-13-86 IF ADDITIONAL FUNDS ARE NOT APPROVED BEFORE THAT TIME* IF

ISTE DEMOBILATION OCCURS THIS MAY LEAVE THE SITE UNCONTROLLED AND ALLOWTHE TREAT TO PUBLIC HEALTH (PER CBC) TO CONTINUE UNCHECKED.

II. FUTURE PLANS

A. SITE ACITIVIES TO CONTINUE AS FUNDS PERMIT. CONTINUE STAGING ANDINVENTORY TO BE PERFORMED O6-12-86

B. OFC AWAITING ANALYTICAL RESULTS ON DRINKING WATER SAMPLES. 24 HOUR'URN AROUND TIME REQUESTED.DAVID WRIGHT OSC EPA REGION 3 PHIL PA

A R ! G u 2 0 i

WU INFOMASTER 4-OO2734S164-OO1 06/13/86ICS IPMMTZZ CSP8144362961 DGM TDMT UG ERIE PA 181 O6-13 0731A EST

TWX 7106700716 EPAOHM PHAEMERGENCY RESPONSE4218 EPA PHA

ATTN TOM MA88EY AND TIM FIELDSPOLREP f PAGAN ROAD DRUM SITESUMMIT TOWNSHIP ERIE COUNTY PAI. SITUATION (19OO HOURS 6-12-86)

A. SITE ACTIVITIES CONTINUE WITH STAGING AND OVERPACKING OF DRUMS INSPITE OF TORRENTIAL RAINS THIS DATE. INVENTORY OF TRAILER CONTAININGDRUMS BEGIN. STAGE DRUMS ON GROUND AWAITING SAMPLING.

B. PERSONNEL ON SCENE EPA-1 TAT-3 ERCS-6 PADER-O

C. ESTIMATED COSTS CLOSE OF BUSINESS 6-12-86 (CEILING »3OK> ERCS EQUAL7K EPA EQUALS 2K TAT EQUALS 4K

D. WEATHER-SEVERE THUNDER STORMS AND LIGHTING TORNADO WARNING AND FLASHFLOODING

II. ACTIONS TAKENA. ERCS USING 213 WITH GRAPPLER TO STAGE DRUMS ON SITE. THE MAJORITY OFDRUMS REQUIRE OVERPACKING ON GROUND SURFACE.

B. TRAILER OPENED APPROXIMATELY 12OO HOURS INSPECTION OF CONTENTSREVEALED DRUMS STACKED 2 AND 3 HIGH THROUGHOUT ENTIRE LENGTHS OFTRAILER. 4O DRUMS REMOVED FROM TRAILER AND STAGED THIS DATE.APPROXIMATELY 8O ADDITIONAL DRUMS REMAIN IN TRAILER.

III. FUTURE PLANSA. COMPLETION OF ON SITE ACTIVITIES TENATIVELLY SCHEDULED FOR 6-13-86PENDING ADDITIONAL FUNDINGB. STAGED DRUMS TO BE SAMPLED FOR DISPOSALC. OSC AWAITING LAB ANALYSIS ON POTABLE WATER WELLSDAVID WRIGHT OSC EPA REGION 3 PHILADELPHIA PA

SPILLSEPA WSH

ATTN TOM MASSEY/ TIM FIELDS

POLREP *6PAGAN ROAD SITECERCLA REMOVAL ACTIONSUMMIT TOWNSHIP, ERIE COUNTY, PENNSYLVANIA

I. SITUATION 2000 HOURS 6/14/86

A. DRUM SAMPLING, STAGING, OVERPACKING AND FENCING COMPLETED THISDATE. A TOTAL OF 243 33-GALLON AND SO SMALLER CONTAINERS ON SITESECURED AND AWAITING DISPOSAL.

B. PRELIMINARY RESULTS ON DRINKING WATER SAMPLES FROM WELLS IN THEAREA INDICATE NO VOLATILE ORGANIC CONTAMINATION.

C. APPROVAL OF •ISO,OOO IN ADDITIONAL FUNDING FOR THIS SITERECEIVED IN THE REGIONAL RESPONSE CENTER AT 132O HOURS 6/13/86. OSCRECEIVED OFFICIAL NOTIFICATION OF THE APPROVAL AT 1643 HOURS 6/13/86.

D. PERSONNEL ON SCENEI EPA-1, TAT-1, ERCS-6

E. ESTIMATED COSTS TO DATE COB 6/14/86*

EPA *3,OOOTAT *6,OOOERCS »38,OOO

TOTAL 49,000

F. WARM, PARTLY CLOUDY, MUDDY CONDITIONS.

II. ACTIONS TAKEN

A. ON SITE BOX TRAILER UNLOADED OF ALL DRUMS AND CONTAINERS BYIOCS HOURS 6/13/86. TRAILER CONTAINED ISO DRUMS AND SO SMALLERCONTAINERS,

B. ALL DRUMS SECURED ON SITE, OVERPACKED IF NEEDED, AND COVEREDWITH VISQUEEN. AREA 18 FENCED AND BANNERGUARDED. OSC CONCERNED ABOUTEXTREME AMOUNTS OF RAIN AND MUDDY CONDITIONS AT THE SITE. SITE HAS BEENVERY DIFFICULT TO WORK AT DUE TO DENSE WOODS AND THE FACT THAT TWOBUSINESSES AND A FAMILY LIVE ON THE SAME PROPERTY AND ARE WITHIN SOYARDS OF THE WORK AREA.

III. FUTURE PLANS

A. OSC AWAITING ANALYTICAL RESULTS ON DRUM SAMPLES FOR ULTIMATEDISPOSAL. DISPOSAL CLOCK BEGINS 6/16/86.

B. REMOB TO SITE AS SOON AS DISPOSAL APPROVAL IS RECEIVED.

DAVID WRIGHT ^ 'v ' ° ~ ~ °ON SCENE COORDINATOREPA REGION III

ATTN TOM MASSEY / TIM FIELDS

PQLREP «7PAGAN ROAD SITECERCLA REMOVAL ACTIONSUMMIT TOWNSHIP, ERIE COUNTY, PENNSYLVANIA

I. SITUATION 10OO HOURS THURSDAY AUGUST 21, 1986 "'"

A. DRUMS AND CONTAINERS REMAIN ON SITE AT THIS TIME AWAITINGDISPOSAL ARRANGEMENTS. TO DATE OSC HAS NOT RECEIVED A COMPLETEANALYTICAL PACKAGE FROM OHM. WPR'S THAT HAVE BEEN SENT TO THE OSC LACKTHE NECESSARY INFORMATION FOR COMPLETION. OSC CONTINUES TO WAIT FORTHIS INFORMATION. OSC CONCERNED ABOUT OHM'S LACK OF RESPONSIVENESS INTHE AREA OF ANALYTICAL AND DISPOSAL ARRANGEMENTS. SAMPLES WERE TAKENDURING THE 2ND WEEK OF JUNE.

II. ACTIONS TAKEN

A. OSC HAS CONTACTED ERCS PROGRAM OFFICE AND RESPONSE MANAGERCONCERNING THE ANALYTICAL DELAYS AND WPR PREPARATION SEVERAL TIMES OVERTHE LAST TWO (2) MONTHS. OSC REQUESTED AND RECEIVED A WRITTENEXPLANATON OF THE DELAY. OSC CONSIDERS OHM'S PERFORMANCE IN THIS MATTERTO BE QUESTIONABLE. OSC UNDERSTANDS THAT DISPOSAL IS ONE OF THE MOSTCOMPLICATED ASPECTS OF A REMOVAL ACTION, HOWEVER DOES NOT FEEL OHM ISPROVIDING ADEQUATE EXPLANATIONS FOR PROBLEMS ENCOUNTERED IN THIS MATTER.

III. FUTURE PLANS

A. AS SOON AS OSC IS SATISFIED WITH OHM ANALYTICAL/DISPOSALOPTIONS AND DISPOSAL APPROVALS ARE RECEIVED OSC WILL REMOVE THEMATERIALS FROM THE SITE.

DAVID P WRIGHTON SCENE COORDINATOREPA REGION III

A R I G G 2 0

TLX II 7108229269^ONNECTED 26-Sep-B6 11;17 21

SPILLSEPA WSHATT TOM MASSEY / TIM FIELDS

DISREGARD PREVIOUS POLREP tt8

POLREP^PAGAN ROAD SITECERCLA REMOVAL ACTIONSUMMIT TOWNSHIP, ERIE COUNTY, PENNSYLVANIA

I. SITUATION 10:15 AM SEPTEMBER 26, 1986

A. ESTIMATED PROJECT COSTS TO DATE:ERCS 54KEPA 4KTAT 12K

TOTAL 70K

B. OSC CONTINUES TO AWAIT DISPOSAL APPROVAL AND ARRANGEMENTS.

I. ACTIONS TAKEN

A. AT THE OSC'S DIRECTION TATM PERFORMED INSPECTION OF THE SITEON 9/10/86. SEVERAL MINOR PROBLEMS WERE NOTED AT THE SITE (TREE ONFENCE, VISQUEEN OFF OF SEVERAL DRUMS) HOWEVER NO HNU READINGS ABOVEBACKGROUND WERE NOTED. PROPERTY OWNER INDICATED HE WANTED SOMEEQUIPMENT AND POSSIBLY THE TRAILER THAT WAS IN THE DRUM STAGING AREA.MR COON ALSO EXPRESSED CONCERN OVER SITE CONDITIONS.

B. OSC SPOKE WITH BILL BUCHAN OF OHM THIS DATE TO DISCUSS THEWPR'S THAT WERE*SIGNED AND FOWARDED TO OHM. OHM HAS THEM IN THEIRPOSSESSION AND AFTER RECEIVING SAMPLES TO BE SENT ALONG WITH THE WPR'STO THE DISPOSAL FACILITY, WILL FOWARD THEM TO THE APPROPRIATEFACILITIES. THIS IS THE SECOND GO AROUND ON THE WPR'S AS THE FIRSTBATCH PROVIDED TO THE OSC BY OHM WAS INCOMPLETE, INACCURATE AND SLOPPY.JOHN COPUS AND BOB OHNECK HAVE BEEN MADE AWARE OF THE SITUATION ANO HAVEACKNOWEDGED THE PROBLEMS. BOTH HAVE ASSURED THE OSC THAT OHM'S CONDUCTON THIS PROJECT WILL IMPROVE.

III. FUTURE PLANS

A. OSC TO MOB AS SOON AS DISPOSAL APPROVALS ARE RECEIVED.»

B. OSC TO EVALUATE SITE CONDITIONS AND RECTIFY AS APPROPRIATE.

n P i n r n *-iOAVID WRIGHT UK I _ J - L JON SCENE COORDINATOREPA REGION III

To: ERD/OERR (EPA5511)To: T.MASSEY (EPP9374)

From: M. ZICKLER (EPP9347) Posted: Sat 18-Oct-86 1£:O7 EOT Sys £Subject: pagan9.pol """

PQLREP«9Pagan Road Drum SiteCERCLA Immediate RemovalSummit Twp., Erie County PAAttn: T. Massey and T. Fields

I. SITUATION (150O hours 10/17/86)A. OSC/TAT in site this date to inspect site conditions and meet

briefly with property owner.

B. Personnel on Scene: EPft-1, TAT-1

C. Estimated costs to datetERCS- *54KTAT- * 5KEPA- *13K

Total to date- *72K Cei1ing=*£OOk

II. ACTIONS TAKENA. OSC, TAT arrive on site at O845 hours this date. OSC discussed the

day*s plans with property owner Marlin Coon before enteringthe property. OSC and TAT visually inspected staged drums on site.Several drums had what appeared to be bullet holes in the overp ' -Mr. Coon had removed and empty trailer from site; the proptectis--fence was cut and pushed aside from the staging area. OSC and THioff site at 091O hours after repairing the fence.

III. FUTURE PLANSA. OSC awaiting disposal approval for final disposition of drums.

David Wright, OSCEPA Region IIIPhiladelphia, PA

ATTN TIM FIELDS/ TO*- MASSEY

SPECIAL BULLETIN B—SPECIAL BULLETIN B—SPECIAL BULLETIN B

.PAGAN ROAD DRUM SITE•CERCLA REMOVAL ACTIONSUMMIT TOWNSHIP, ERIE COUNTY, PENNSYLVANIA

I. SITUATION 1:30 PM THURSDAY DECEMBER 4, 1986

A. OSC WAS ADVISED THIS DATE BY ERD-HQ THAT A SIX MONTH EXEMPTIOtREQUEST WAS REQUIRED FOR THIS SITE. THE SIX MONTH 'STATUTORY LIMIT WILLBE REACHED ON TUESDAY DECEMBER 9, 1986.

B. OSC WAS ADVISED BY ERD-HQ ON OCTOBER 30, 1986 AND DECEMBER 1,1986 THAT A SIX MONTH EXEMPTION REQUEST WOULD NOT BE REQUIRED TOCONTINUE REMOVAL ACTIONS AT THE SITE. CURRENTLY THERE ARE 233 DRUMS OfSITE AWAITING DISPOSAL APPROVALS. ALTHOUGH THE SITE IS TEMPORARILYSECURED. THE DRUMS MUST BE PROPERLY DISPOSED OF TO FULLY MITIGATE THETHREAT. NO FACILITIES WOULD ACCEPT THE DRUMS FOR STORAGE WITHOUTAPPROVALS FOR DISPOSAL.

C. THE OSC WAS OBSERVING OSWER 920O.3-O2 " IMPLEMENTATION STRATECFOR REAUTHORIZED SUPERFUNDi SHORT TERM PRIORITIES FOR ACTION" SIGNED ETHE AA AND DATED OCTOBER 24, 1986. PAGE 2 PARAGRAPH I I I.A.I " TIME AN[DOLLAR LIMITS" READSJ

" THE NEW LAW RAISES THE TIME AND DOLLAR LIMITS FOR REMOVALOPERATIONS FROM SIX MONTHS AND *1 MILLION TO TWELVE MONTHS AND *2MILLION ( S 104 <•)(!) ). ALTHOUGH NEW TIME AND DOLLAR LIMITS AREEFFECTIVE IMMEDIATELY, THE REGIONS ARE NOT CURRENTLY DELEGATED THEAUTHORITY TO SIGN ACTION MEMORANDA ABOVE *1 MILLION. UNTIL DELEGATIONTO THE REGIONS OF ADDITIONAL AUTHORITY, HEADQUARTERS APPROVAL OF CEILIhINCREASES AND EXEMPTION REQUESTS ABOVE »1 MILLION WILL BE REQUIRED.REGIONS ARE ALREADY DELEGATED THE AUTHORITY TO APPROVE EXTENSTIONS OFANY TIME LIMITS. ANY FINDINGS BY THE REGION THAT AN EXTENSTION OF TIMEIS NEEDED MUST BE MADE AS EARLY AS PRACTICABLE, AND AT LEAST BEFORE THEEXPIRATION OF THE NEW OF THE NEW STATUTORY TIME LIMIT OF 12 MONTHS. "

D.. THE OSC WAS ADVISED BY ERD-HQ THAT THE REASON FOR THEAPPPARENT CONFUSION 18 THE FACT THAT THE EXECUTIVE ORDER ALLOWING THEDELEGATION OF ADDITIONAL AUTHORITIES IN SARA HAS -NOT BEEN SIGNED AND OG-HQ IS ADVISING TO PREPARE THE SIX MONTH EXEMPTION REQUESTS.

6 MONTH EXEMPTION REQUEST-6 MONTH EXEMPTION REQUEST

BY REASON OF THE CURRENT SITUATION, AND THE SITE MEETING THE THREECRITERIA FOR THE SIX MONTH EXEMPTION UNDER CERCLA 1980 (104 (C) ) THEOSC REQUESTS THE REGIONAL ADMINISTRATOR'S APPROVAL AND SIGNATURE TOAUTHORIZE THE EXEMPTION FOR THIS SITE.

APPROVE DATE

A R 1 G Q 2 G 7

E. OSC FEELS THIS SITUATION ONLY EXEMPLIFIES THE URGENT NEED r ^AGRESSIVE POSTURE FROM HQ REGARDING GUIDANCE AND SUPPORT UNDER THE xSARA WHICH WAS SIGNED BE THE PRESIDENT OF THE UNITED STATUS ON OCTOBER17,1986.

F. OSC ADVISED THE SBC TOM VOLTAGGIO OF THE SITUATION THIS DATE.PER THE SBC'S GUIDANCE THE OSC'S SHOULD REQUEST THE RA'S APPROVAL VIA APOLREP ON THE SITE. THE OSC SUPPORTS THIS RECOMMENDATION

G. AS THE SIX MONTH STATUTORY LIMIT WILL BE REACHED ON 12/9/86,IMMEDIATE CONSIDERATION OF THIS REQUEST IS NEEDED.

DAVID P. WRIGHTON SCENE COORDINATOREPA REGION III

IMMEDIATELY FOWARD TO TOM VOLTAGGIO FOR PRESENTATION TO THE RA.

(\R!Q020£

L

• . r~' r: : t •• "!-.,•.:..-51 - ' ,' r-i F JELL'5

__•.-> :::i; i -.:.. ::ui. !..::rm c—SPECIAL PULLET IN c--SPECIAL BULLETIN c

FV-C.MN F-.'OAP PRUri ^ITEr :i-{»-;' . r, PLT-o'.'Ai. ACTIONSurrilT TOWNSHIP, ERIE COUNTY, PENNSYLVANIA

'SUBJECT: REQUEST FOR EXEMPTION FROM SIX MONTH LIMITATION ANDCONTINUATION OF REMOVAL ACTIVITIES AT THE PAGAN ROADDRUM SITE, SUMMIT TOWNSHIP, ERIE CO., PENNSYLVANIA

DAVID P. WRIGHT, ON-SCENE COORDINATOR . /C-.MERGENCY RESPONSE SECTION (3HW22) / 2. /S I

TO: JAME-.ri M. SEIPREGIONAL ADMINISTRATOR (3RAOO)

RESPONSE ACTIONS AT THE PAGAN ROAD DRUM SITE CANNOT CONTINUE PASTSIX MONTHS UNLESS AN EXEMPTION TO SECTION 104 (C) OF CERCLA (1980) ISGRANTED. PEP HEADQUARTERS GUIDANCE, THE OSC IS REQUESTING THISEXEMPTION DESPITE THE PROVISIONS OF SARA (1986) WHICH SET THE STATUTORYLIMIT AT 12 MONTHS. THE INITIAL RESPONSE ACTION AT THE SITE BEGAN ONJUNE 9, 19B6 AND THE SIX MONTH TIME LIMIT WILL EXPIRE ON TUESDAYDECEMBER 9, 1986

STATUTORY CRITERIA

IN ORDER TO COMPLETE THE REMOVAL AND MITIGATE THE ONGOING THREAT ITIS NECESSARY TO EXTEND RESPONSE ACTIVITIES PAST SIX MONTHS. SECTION1O4(C) OF CERCLA (1980) LIMITS RESPONSE ACTIONS TO SIX MONTHS UNLESS THEFOLLOWING THREE CRITERIA ARE METi

1.) CONTINUED RESPONSE ACTIONS ARE IMMEDIATELY REQUIRED TOPREVENT, MITIGATE AN EMERGENCYi

ALTHOUGH THE DRUMS ARE STAGED ON SITE IN A FENCED AREA, SAMPLES HAVESHOWN DRUMS WITH FLASHPOINTS OF <72 DEGREES FARENHEIT, UNCONTROLLABLYREACTIVE MATERIALS, AND CONTAINING CYANIDE. AS SOON AS THE APPROPRIATEDISPOSAL FACILITIES ARE LOCATED AND APPROVALS ARE RECEIVED THE WASTESCAN BE REMOVED FROM SITE. WASTE STREAMS BEING REJECTED, INCINERATORBACKLOG, AND RCRA COMPLIANCE PROBLEMS ARE DELAYING PROPER DISPOSAL. THEDRUMS MUST BE DISPOSED OF AS SOON AS POSSIBLE.

2.) THERE IS AN IMMEDIATE RISK TO PUBLIC HEALTH AND THEENVIRONMENT:

THE DRUMS CONTINUE TO PRESENT AN IMMEDIATE RISK OF FIRE/EXPLOSION,POTENTIAL DIRECT CONTACT THREAT AND INHALATION HAZARD. A WORKPLACE ANDRESIDENCE ARE LOCATED WITHIN 200 FT.

3.) ASSISTANCE WILL NOT OTHERWISE BE PROVIDED IN A TIMELY MANNER:

THE PROPERTY OWNER AND TRUSTEE IN BANKRUPTCY FOR THE COMPANY WHICH OWNEDAND HANDLED THE WASTES HAVE DECLINED TO TAKE ANY ACTION AT THE SITE.

G R I C -CLLOS

RECOMMENDATION

BECAUSE THE CONDITIONS AT THE PAGAN ROAD DRUM SITE MEET THECONDITIONS OF SECTION 104(C) OF CERCLA (1980), I RECOMMEND THAT YOUAPPROVE AN EXEMPTION FROM THE SIX MONTH LIMIT.

APPROVE: DATE:

DAVID P. WRIGHTON SCENE COORDINATOREPA REGION III

A R I 0 0 2 I O

POLREP »10PAGAN ROAD DRUM SITE~CERO_A REMOVAL ACTION 5SUMMIT TOWNSHIP, ERIE COUNTY, PENNSYLVANIA •»

I. SITUATION lOtlO AM ON JANUARY 9, 1987

A. DRUMS REMAIN ON SITE AWAITING DISPOSAL. THE OSC FEELS THAT THEMAIN REASON FOR THIS 18 COMPLIANCE ISSUES, EXTREMELY SLOW APPROVALPROCESS BPECIFICIALLY FOR CERCLA WASTES AND ADDED BUREAUCRACY AT THESTATE LEVEL. THE IMPACT ON THIS AND OTHER PROJECTS 18 OBVIOUS.

B. CURRENT DISPOSAL STATUS BY WASTE STREAM IS AS FOLLOWSt

NON FLAMMABLE ORGANIC LIQUID—HfcJECTfcD BY THREE FACILITIES DUE-• TO BGrNG REACTIVE. CHEM WASTE ALABAMA'S LAB HAS APPROVED.

'• AWAITING FINAL APPROVAL AND CONTRACT

FtAMMABLE 3OLIDS—APPROVAL PENDING AT CHEM WASTE/SCA CHICAGO.INCINERATION ANALYSIS BEING PERFORMED.

•- NON FLAMMABLE SOLIDS—APPROVED AT CHEM WASTE EMELLE

FLAMMABLE INORGANIC LIQUID—APPROVED AT CALDWELL BUT CAN NOTJ ' SHIP UNTIL APRIL. APPROVAL PENDING AT SCA IN CHICAGO.

r FLAMMABLE ORGANIC LIQUID—APPROVED AWAITING CONTRACT WITH SCA•• IN CHICAGO*

ALL ABOVE WASTE STREAMS WERE AFFECTED BY COMPLIANCE ISSUES.r OSC REFER .CES LETTERS TO JEAN WRIGHT FROM OHM DATED DECEMBER,>•' 9TH AND DECEMBER 3O, 1986. ~.

C. OSC RECOMMENDS THAT DISPOSAL-ISSUES BE THE TOP PRIORITY FOR TOPMANAGEMENT.IN THE SUPERFUND PROGRAM. THE ISSUES HAVE BEEN NOTED BY THEREGIONS FOR THE PAST YEAR AND THE SITUATION GETS WORSE EACH DAY.

• POSSIBLE SOLUTIONS FOR CONS I DERATION*. '

r-' i. THE AGENCY OBTAIN GENERIC APPROVALS OF VARIOUS WASTE' >STREAMS AT SEVERAL STORAGE, DISPOSAL, TREATMENT. AND INCINERATION 'FACILITIES IN THE REGIONS. - -THIS 18 CURRENTLY DONE IN PRIVATE INDUSTRY.

r 2*' THE AGENCY ARRANGE WITH SOME OTHER FEDERAL AGENCY TOCONSTRUCT' A HAZARDOUS WASTE STORAGE, TREATMENT, INCINERATION ETC. '•FACILITY ON FEDERAL I_AND. FACILITY COULD ACT AS A CLEARING HOUSE FORWASTES FROM SUPERFUND SITES, EMERGENCIES, AND STATE CLEANUPS. FACILITYCOULD BE MANAGED BY EPA AND OPERATED BV A CONTRACTOR.

• S. THE AGENCY WORK CLOSELY 1IITH THE STATES TO SPEED UP THE «- APPROVAL PROCESS AND GIVE A HIGHER PRIORITY TO CERCLA WASTES AT THE -MFACILITIES. •*

-• II. FUTURE PLANS -

A. OSC AWAITS DISPOSAL APPROVALS •

B. . AFTER-APPROVALS ARE RECEIVED, EVALUATE COSTS,- THE NEED FOR—ADDITIONAL MONEY AND RENOB TO SITE FOR REMOVAL OF WASTES *-

/9u>j) r- w^ibiir . ' ^ «- ' -' —-—— r D ! nr o • 'DISCONNECTED O9-Jan-87 'lOtSB 29^ MSG 72A H i\ I O 'J (. I I

Tei ERD/OERR . (EPA3311) -Tot T.WASSEY (EPA9374)

Fromi D.WRIGHT (EPA9346) Postedi Fri 6-Mar-67 • 16i5£ EST By* 63Subject! PAGAN RD POLREP 411

PQLREPttll ' ; f :•, • • v..' : . . ' - ' " . - . - . ' . : -> -PftGQN ROAD DRUM SITE .CERCLA REMOVAL ACTION , . - - ,SUMMIT TOWNSHIP, ERIE COUNTY, PENNSYLVANIAAttni T. Hassey and T. Fields . .

I. SITUATION (1430 hrs. 3/6/67). A. Drums remain on sit* awaiting disposal. Currant disposal status

by Mast* stream is as follows! " ..

Non-flammabla organic liquids (6S drums at *30O *a. > approved fordisposal at Chaw-Wast• Emails,. Alabama. :

Flammabls- solids (temporary storage at «10O/drum initially, tSO/drummonthly thereafter) tentatively scheduled for AMD TSD.

... - • . ' / . •Non-flammable solids (£1 drums at S68.50 aa.) approved for disposalat Che« Waste, Emelle, AL.

Flammable inorganic liquids (37 drums at t900 ea.) approved forincineration at SCA, Chicago.

Flammable organic liquids (6G drums at »9OO ea.> approved forincineration at SCA, Chicago. .

(Total estimated disposal and transport cost* *140K>

II. FUTURE PLANS ; .

A. As per OSC direction, TAT and ERCS to be on scene 3/1O/67to review site logistics for drum staging and loading.

B. Drum loading and transport scheduled for 3/16/67 through 3/19/67concurrent with acceptance schedules of TSD's mentioned above.

David Wright, 03C .EPA Region IIIPhiladelphia, PA ,' , ,

flRI002l'2

Toi ERD/OERR (EPA5511)Toi T.MASSEY (EPA9374)

From* T.MBSSEY (EPA9374) Po«t»d: Fri 13-M»r-87 14i39 EST Sy« 63 (38)Subjecti PAGAN ROAD POL 12

POLREP #12PAGAN ROAD DRUM SITESUMMIT TWP., ERIE CO., PA.CERCLA REMOVAL ACTION

ftTTN: TOM MftSSEY * TIM FIELDS

I. SITUATION (3/10/87)

A. OSC PROVINCE, TATM DONEGAN, AND ERCS REP. KEN KUHN REVIEWEDSITE LOGISTICS AND EQUIPMENT NEEDS FOR DRUM SEGREGATION ANDREMOVAL ACTIVITIES SCHEDULED FOR WEEK OF 3/15/87. ADEQUATESTAGING SPACE APPEARS AVAILABLE WITHOUT DISTURBING SITEOWNERS PROPERTY.

B. PERSONNEL ON SCENEi EPA - 1, TAT - 1, ERCS - 1.

C. WEATHER: CLEAR, COLD TEMP. MID 20* S.

II. ACTIONS TAKEN

A. OSC, TAT, AND ERCS ON SITE AT 1515HRS THIS DATE. DRUMSSTAGED EARLIER DO NOT APPEAR TO HAVE BEEN DISTURBED SINCELAST SITE INSPECTION. FENCE REMAINS INTACT, WITHBANNERGUARD. OSC ATTEMPTED TO CONTACT PROPERTY OWNER WHILEON SITE| PROPERTY OWNER NOT AVAILABLE.

III. FUTURE PLANS

fl. REMOVAL ACTIVITIES SCHEDULED BEGINNING 3/15/87 WITHMOBILIZATION OF PERSONNEL ft EQUIPMENT. COMPLETION OFREMOVAL EXPECTED BY 3/2O/87 PENDING UNFORESEEN DELAYS.

VICKIE PROVINCE, OSCU.S. EPA, REGION IIIPHILADELPHIA, PA.

A R I G 0 2 !

2.

EPAOHM PHA

WU INFOMASTER 4-OO1892SO78-OO1 03/19/87IC6 IPMBNGZ C8P8144962961 DGM TDBN ERIA PA 369 O3-19 0638A E8T

TWX 7106700716 EPAOHM PHAEMERGENCY RESPONSE4218 EPA PHA

ATTN T MASSEY AND T FIELDS

ATADDITIONAL

C WEATHER - SUNNY, COLD HIGH 30*8JTIMATED COST TO DATE EPA - 14K TAT - 6K ERCS - 6OK CEILING EQUALSQ ES

1 TIONS TAKENk .m*W?Tjff »T4raW? r SS-0*? ?LE

BVs o . t e ,ERCS TO REMOVE TRAILER FROM FROZEN GROUND FAILED. THIS RESULTED INSEVERELY LIMITED SITE ACCESS AND CONSTRAINT ON STAGING SCHEDULETHROUGHOUT WORKDAY.B AS PER OSC INSTRUCTIONS, ERCS MOBILIZED FRONT END MOTOR AND 75OVERPACK AT APPROXIMATELY O830 HOURS AND 1OOO HOURS RESPECTIVELY.APPROXIMATELY SO OVERPACKS JTILIZED THIS DATE ON DAMAGED DRUM.M 8ITE "a*""1*-* 120°E ALL DAMAGED DRUMS SCHEDULED FOR DISPOSAL AT BCA ON 3-17-87 WERE STAGEDAND OVERPACKED BY 19OO HOURS. SITE WORK DISCONTINUED DUE TO LIMITEDDAYLIGHT HOURS. OPENING AND SORTING OF APPROXIMATELY 19 OVERPACKSCONTAINING MULTIPLE SMALLER CONTAINERS DELAYED UNTIL 3-17-87.F OSC INFORMED BY J. COPUS THIS DATE THAT SCHEDULED STORAGE OF FLAMMABLESOLIDS CANNOT OCCUR AT AMO FACILITY AS PLANNED DUE TO UNFORESEENEMERGENCY STORAGE AT THAT FACILITY. OSC AND J. COPUS MADE REPEATED

8TORA6£ «•"-"'»• COPU8 T0III FUTURE PLANSA COMPLETE SORTING AND OVERPACKING OF SCA WASTE.B BEGIN STAGING AND OVERPACKING OF WASTE DESTINED FOR DISPOSAL AT CHEMWASTE AND EMELLE ALABAMA ON 3-18-87.

OVERPACKS 3-17-87.

VICKI PROVINCE, OSCEPA REGION 3PHILADELPHIA PA n D I (~i Q 9 \VICKI PROVINCE HIX w

0645 EST1

EPAOHM PHA

To: ERD/OERR (EPA5511)To: T.MASSEY (EPA9374)

From: V.PROVINCE (EPA9343) Posted: Tue 24-Mar-87 14:55 EST Sys 63Subject: POLREPS 13 & 14 PAGAN ROAD SITE

POLREP 9*3 /7-J?Pagan Road Drum SiteSummit Twp., Erie County, PAAttn: T. Massey and T. Fields

I. Situation ( 19OO hrs. 3/18/87 )A. Site prematurely dernobed this date at 19OO hours due to

inability to characterize drums on site as a result ofinaccurate inventory prepared by the ERCs contractor.

B. Personnel on scene:EPA-1, TAT-1, ERCS-8, PADER-1 (3/17/87)

C. Weather-Clear, Cold

II. Actions Taken

A. 3/17/87- Two truckloads of drummed waste transported toSCA in Chicago for incineration this date. Shipments consistedof 27 drums flammable inorganics, 1 drum flammable solids (foranalysis), and 31 drums flammable organics. Original estimatefor disposal was 37 drums of flammable inorganics and 66 drumsflammable organics. Substantial cost savings acheived by OSC indisposal of these drums by bulk-packing smaller containers inoverpacks to reduce total number of drums for shipment.

B. 3/17/87— While preparing remaining drums for shipment on3/18/87, TAT and ERCS discovered a large number of 55-gallonoverpacked drums not listed on ERCs schedule for removal. OSCcontacted OHM immediately to get description of unknown drumcontents. No OHM personnel available for information byCOB 3/17/87.

C. 3/18/87-OSC Province contacts RCRA TSD coordinator inregion. No storage facilities in compliance at this timefor storage of Superfund waste. Seek advice and guidance onability to store waste at TSD with violations not relating tooperations; EPA HQ will not permit use of a facility in violation.OSC reluctantly decides to store flammable solid drums and secureon site for later disposal.

D. 3/18/87- OSC talked to property owner Coon regardingtemporary storage of flammable solids and other drums on propertywhile awaiting disposal approvals.. Mr. Coon agreed to the use ofhis property for this interim storage.

f i R I 0 3 2 i 5

E. 3/18/87-OSC and OHM Ohneck and Buchan discussuncategorized drums; OHM locates original drum log that RM shouldhave on site. Approximately 10O drums of tar and protectiveclothing and 4O "empty" drums were not accounted for in ERCsinventory supplied to the OSC. All disposal arrangements omittedthese drums, thus delaying completion of the projectindefinitely.

F. OSC very disturbed at ERCS performance OSC informs OHMOhneck that OHM should immediately undertaken a thorough checkof all drum inventory and then check that against site inventoryand shipped inventory at OHM expense. Any additional analyticalwill be absorbed by OHM. Any transportation of drums that wereoverlooked will b* absorbed by OHM and the additional rnobe/demobecharges will also be absorbed by OHM. Disposal of flammablesolids and any other waste streams identified on site to bearranged ASAP.

III. FUTURE PLANS

A. ERCS and TAT to continue staging and logging drums onsite.

B. As per OSC instruction, OHM to review drum logs andlaboratory results in their office, and arrange to coordinatefuture druin removal on site as soon as possible.

C. Site removal activities to be completed as much aspossible. Drums remaining on site will be staged and securedbefore dernobe.

Vicky Province, OSCEPA Region IIIPhiladelphia, PA

AR I 00216

POLREPPagan Road Drum SiteSummit Twp., Erie County, PAATTN: T. Massey and T. Fields

I. SITUATION ( 1200 hours 3/13/87)

A. Total drums off site by COB 3/18/87 as follows:31 drums flammable organics to SCA, Chicago, 3/17/87£7 drums flammable inorganics to SCA, Chicago, 3/17/871 drum flammable solid to SCA, Chicago for analysis,

3/17/8748 drums non-flammable organic liquids to Chem waste,

3/18/872O drums non—flammable organic solids and 4 drums non-

flammable liquids, to Chem Waste, Emelle, 3/18/67

B. Total drums remaining on site this date as follows:SO drums tar1C drums visqueen36 drums "empty", many containing waste material2 drums unknown contents

C. Personnel on scene:TAT-1, ERCS-8

D. Total Estimated Costs to date:EPA- *15KTOT- *8KERCS-*145 (est. transport and disposal costs-*a5k)

E. Weathei— Clear, Cool, high 40's

II. ACTIONS TAKEN

A. TAT and ERCS complete overpacking and staging of tar drumson Coon parking lot. Tar drums surrounded with fencing andbannerguard} drums of visqueen and unknowns staged with tardrums.

B. Drums considered empty by ERCS in previous assessmentstaged near Coon trailer along access road, covered with visqueenand bannerguarded.

C. Disturbed earth graded on site and in parking lot.Equipment demobed this date; Bobcat off site at O930 hours.

D. Approx. SO overpacks not used- to be removed from site at140O hours this date.

A R I G C - 2 1 7

E. TAT informed Coon secretary, as Mr. Coon unavailable atdemobe, of site conditions to date. Attempts to remove trailerpad unsuccessful, however, trailer leveled as requested byproperty owner.

F. Site secured before dernobe at 12OO hours this date,3/19/87.

III. FUTURE PLANS

A. ERCS to arrange for disposal of tar and other drumsremaining on site, as per OSC instruction. Remobe expected innear future to complete removal activities.

Vicky Province, OSCEPA Region IIIPhiladelphia, PA

OA R I G 0 2 i 8

10

To: ERD/OERR (EPA5511)To: T.MASSEY (EPA9374)

From: T.MASSEY (EPA3374) Posted: Fri 17-Apr-87 9:28 EOT Sys 6Subject: PAGAN ROAD POL 15

POL RE Q. lioPagan Road Drum SiteSummit Twp., Erie Co., PA

ATTN: T. Massey and T. Fields

I. Situation (18OO hrs. 4/6/87)

A) ERCS and TAT on site this date to completeinventory, marking, and sampling of the approx. 12O drumsremaining on site. Because ERCS failed to provide an accurateinventory of wastes on site at the start of this removal, delaysin obtaining disposal and continued remobi1ization werenecessary. The OSC has determined that EPA will not befinancially responsible for those delays and additional expensesincurred in correcting any errors, and therefore no cotfts havebeen incurred against the project for today's ERCs activities.

B) Personnel on scene:TAT-1ERCS-3

C) Estimated costs to date:ERCS-»158.9k; ceiling *2lGkTAT- * 1O.Ok; ceiling * 35kEPA- * 15.0k; ceiling » £5k

Total project ceiling «»4lOkD) Ueathei—cold, heavy fog, rain

II. ACTIONS TAKEN

A) TATM on site O745 hours this date. Site remains securedsince last activities 3/19/87. ERCS crew consisting of responsemanager, chemist,and technician on site 0815 hours.

B) ERCS performs inventory of remaining drums on site,consisting of tars, flammable solids, and "empties". Six samplestaken from liquid* in "empty" drums, one tar sample taken for newWPR. One previously unmarked solids drum could not be sampled,as materials had solidified inside. Site activates complete atapprox. 170O hours this date.

III. FUTURE PLANS

A) OSC to receive lab results from drum samples, along withrecommendations for disposal from CRCS. Disposal approvals to beobtained as soon as possible.

B) Remaining drums to be removed from site for storage ordisposal. Removal activities to be completed at that time.

•'ickie L. Province, OSC . r -,, r.PA Region III AK I U U <-

Philadelphia, PA

To: ERD/LiERRTo: T.MASSEY (EPA9374)

From: T.MASSEY (EPA9374) Delivered: Tue l-Sep-87 16:04 EDT by--Subject: PAGAN ROAD POLRtP *17Mail Id: IPM-163-67G9Cl-lH46O089c:

PGLHEP *i7 - Pctuon Hoad Drum SiteErie County, PA

ATTENTION: Tom flassty and Tirn Fields

I. Situation (£OOG hours - 8/31/87)

A. On &/c:6/a7, OSC notified by O.H. Materials of disposalapprovals for the following waste streams: Non-hazardous<tras>h), hazardous waste liquid, hazardous waste solids: wasteflammable liquid <bi-phaseJ, waste flammable liquid (pureliquia). Nori— hazardous waste to be transported to Chemical wasteManagt>men t , Ernel le, Alabama P'or disposal. All other wastestreams to be transported to Tficfrmc*lK£i'l, Nock Hili, SC f'-jri ric i nercst ion.

B. c^tidiated Co&tt» to D^tt :Cout to Da be Ceiliny

* £, O'.>O * £"_), OoOi H! 1O,OOO 35, OOOERCS 178, £5£ £95, OOO

II. Actions Token

H. Per OSC (Wright) instruction, TAT traveled to tne siteon 6/iia/fc7 arid performed a walk through inspection of the drumstaying areas. TAT noted that 99 product arums remained on siteas well as 3b drums containing non— hazardous waste. While onsite, TAT met with property owner, Mr. Coon. Mr. Coon expressedconcern regarding damage of a box trailer which he claimedoccurred during drum staging operations in March, 1987.

B. QSC (Clark) contacted ERCS (Bill Buchan) on 8/c:a/a7 andmade tentative arrangements for pre-dispo-al operations at toesite.

C. QSC Clark tasked ERCS to be on site 3/1/87 to preparefor t rantauort at ion and disposal of all drums arid site activitygenerated trash staged on site.

AR1C0220

1£

III. Future Plans

H. ERCS to rnobe on site GS30 hours 9/1/87.

B. Fraritaijor t at ion and Uisuos^l >.if oil drums to beoinat the site.

Dave wriunt, OSCi_iSc» Marie Ciar'h. Jr. OSCU.S. EPA Region IIIPh i i aue 1 ph i d. (••£*

RRIQD22!

13

Co:f...:

From: T. MnSSEY (EPA9374) Delivered: T ue tj--b-'p-a / to:.-..- cu\Subject : PAGAN r\OAO DRUM bl'lE PuILREf'lail Id: i Pl'l-1 o3-&70'3ii.)to-0 76 !£'."+7o

4 t --*hOnD L'.Rui'l

tRit., ERIE COUNTY, PH

M l T u : TbiM MASSE Y MHO TiM FIELDS

1. oiTUHTiOlM (iOOO HHS. , TUESDAY, OS/Ol/bV)M. USC CLrtrtK, TAT, HMD ErtCa (*)ti.T UlM SiTb O..l3>.> hn'S "i n i c

DATE TO BEGIN PKE-TRHNSPun I AT IDl-4 OPERATION^ hUnREMHiNlNb WHbTt bl'RtLHi'lS. DlbPGiAL. L'Pt r<H r I un-s 1 L'INCLUDE Tr-iki KbiMUVHL UF <-iLL D'<UhG UNO S I T trl LiEhEnuT LuT RnSri LUKhtNlLt STAlaED CuvJ biTti. DitaHUai-iL F i-iL i L i f IL-.SMf-Li I'HtLKftMLKEM, ROCKHil_l_, SC MNb CHEM WHJJ . E

L'Ul'lNij DHUl'l LHttkl'LlNb HNl; StbritQrtM T I UN. e.«LSINFORMED avjc THMT btvEn^L DRUMS HMD btt.N SHOT ^iKlKLc LnUtilNb H PuRlluivt Uh" T Hfc DKbi-iS LUNTtN I S "! L)uN'iO THE uHUUND bUUFHCE. 'I ht UbC ulHtLTt-O bKCi 1uuVL-.r<i'ML.rx HuL. Lt^bilS UniCh HHL) t<tbiv< t.HOf

hD S01i_ INlO UVbRPHLKb.

L.. .'Ur.rMjNNtiL. ON SCt' t : C.Pn~l, iHT-c:, fcr<CS-7

D. t.b'l innTtU CUSTS Tu UnfL: 1-iut.NLY C. T. u.t. PH or.THT IC:K

*itHThtR: PARTLY Cl-OuDN , CQuL TEMPtRn fURE^, HlbH r,O?

11. ML i i UIM'SS l wKtNM. u L, MET WITH PROPERTY GwNtH vl-lR. M. LuON) HIMU i

HIM OF EPA'S INTENTiQMa "i Q RtfiOve HLL DRUMS Hf-iDKRuM THE SITE.

b. OSC SPOKE WITH TnE PrtUHtiHTY OWi^tR nEuMRDiNla i HtTRAILER DrtMAGtD DURING PREVIOUS RESPONSE ALTIVlTItS UNSITE. use INFORMED PRuPt-K'i t uwi^tR O'-IR. U.OUN.I TnuiHHrxM:\titMfeNT)s WOULD b£ MADE THROUbH THE ERCS CuNTRnCTuRTO Ht-iVt HuL DHWHbtS

C. U'-C DIRECTED ERCS REaPuNbt MnNAbER TO CONTnC THPpROPRlnTE IND1V1DUMLS Tu RtPnlR DnMnGtD BOX 1 RH .1 i_t.R.

P. P14 11

l£

tr<l'.3 ALT 1VI f ItS Trtl:-: UnTf. l.^UuUULlD ME L.Mft.L. I i (b Or n.-L.PRODUCT DRUMS ON Sllti, BULGING bF hAi.ARi.-ObS *JA i L Llu'UiuINIU blX Cb) GVtRPACK DRUMS. L. RUSH 1 fab uF HL.I_ EMPTYDRUMS, PLACEMENT bF DhfUMS UNTO *lbODt:N PALi-ET S FDr-;1 RANbPOR i nil ON (AS RciL'.J.tRED b f IVtERi-lALKcil'1 DISf'bbALFACILITY) AND THE OVERPAYING uF DRUt'iS DAMf-.bLD bYbUNU-HO'l S <5) .

111. FUTUPvE PLANSA. LUi-iDING AND T RAiMbPUH FA I I uN Of DRUMS HNU i/iTc!

TRASH SCHEDULED TO BEGIN 090O HRS. , u9/Oi/67.MHlt-.'RiAuS ti£I,NG TRftNSPGRTEu fcY i_.ii_ENSED

WASTE HAULERS, CHLM FKEiuHf, INC. Al<D DARTTRuCKiNb.

'vt URIb'HY, UbCU.n r*U<Rt'r£. I.'.L HI->, JR. GSC

f.."l-'H atf-.b I ON IIII L I .Mi.,'t_L I-l I i H, t^H

A R I 0 3 2 2

To* EnD/uERR"I.-..: t . Mi-tS£>EY

Fi'om: T. MASSE r' (t_F'n9,.'w4> Del i vered : "I '.((.:; e-bt'U—a/ lO: ii ti/lSuD.i6.-ct: PAGAN ROAD POLREP 19flail ia: 1 Pfl-1 £.3-87O9Ot3-0':> 177i.>ati«i

IX ri' i-iLji \.-4 HUMP L-Rl.'M SITE!ERIE, ERIE COUNTY, PA

A l VIM: "f ui'l MHSSEY AND TIM F'lELDS

i. SITUATION (iioo HRS., WEDNESDAY, o9/oi/87/A. NbiSMUNSb OPERATIONS COMPLb'Tfc: Ai TrtIS S t Tt w I T n I Hb

REMOVAL UF ALL DRUMS AND SITE bENtRATED TrtASH. ArUThlL. uF M'5 PRuDUC f DRUMS Ur.Rt LUADEID, I-IANI Fh'S l ED. ANDTRANSPOHTbD bY CHbM FhblGHT, INC. 10 Th£Rr*lHi_Kr.MDISPUbHi_ FACILITY, RULK HILL SC hbR I NC NERA f I uN. uivt.RbLLOF~F BOX WAS LOADED WITH CRUbHLD DRUMS AND SITEb£NEhAFED I RASH, MnN 1 Ffcl J f bD, AND TRANSPORTED Er D. IH iVKUCJK1NG TO CHEMICAL WAS i E MANNbEMENT, £M£LL£, Ai_HL:AMA.

b PtK-aiJNNEL UN SCENE: bPA-1, TAT -c . c.RCS-/.CntM. FRE1GH I'-cl, unrtT 1 RUCK [ No- 1

L. wbA'Hi£R: KH1N. CUbL, i cMHEHnTUKb IN 6«.)' L>

D. ESTIMATED COSTS TO DAVE: AGENCY C. T. D. CEILIi-.E.PH t£-. 3r, c._i'r1'AT li. aK 2'_,rbRL.S i ("t). £lrv c.-J'Jr

II. HLViUNS 1HKENn. USC CLARK LGNlHCTbD PwuPERTY GwNtR O-lR.

INFORMED HIM THAT ALL SITE OPERATIONS WEr-E COdPLE'l E.

b. cIRCS COMPLETED LOADING OF t)5 PRODUCT DRUMS A: DAPPROXIMATELY 5 TONS OF SITE GENERATED TRAbH FbRTRANSPORTATION TO DlS^ObAL FV<C iL I T It.S. ALL DRUMS wEK-PROPERLY LABELED ANO PLnCED bN WOODEN PALLETS PRIOR VOSHIPPING. THE PRODUCT DRUMS WcRb TKAiMSt'URrtD UNDtKSOUTH CAROLINA STA'lE MANIFEST NUMBER Ob5u5 AND ObSOti.SITE GENERATED TRASH W; ;S THANSPOR TED UNDER MI_MC<HIMI iSTATE MANIFEST NUMBER CwMA 35tt5i_O.

C, OSC DIRECTED ERCS RESPONSE MANAGbR TO ArtRANbE FORREPAIRS TO PROPERTY OWNER'S BOX TRAILER WITHiN £ WEEKSOF THIS DnT£.

F u ruh £ PLANSn. NU AUDITiUNAL EMERGENCY rt£5PGNSE ACTIVITIES An f 11_ I rn Tiii

FOR THIS SITE.

b. OSC TO AWAIT WASTE DtSPObHL ACKiMGWLC.DbMc.jMTS r Ru'.<\DISPOSAL FACILITIES IN SOUTH CAROLINA AND ALABAMA.

c. use "(o AWAIT FINAL INVOICE FROM ERCS CGNrhnC ron.

D OSC 10 SUBMIT FINAL PGLREP FOLLOWING MET CONDITIONS uFPLANS "B. " AND "c. "

DAVt WHliiHT, OBCLibA MMRIE CLARK. JR. useUS EPA KEG ION I IIP!-I i I_HL>£ t-PH i A. I-'A

AR1Q0225

TO: ERD/bERR vEPAS'ili)F r''-'iii : T.i'iAsScY ^EPA'J37*'»^ i/ei i vt-red : vit-'O 'r?~bt-uject: PAGAN ROAD POLREP £0l i~u: 1 l-'i'l— 1 c/3-b /ij' t.»y— 1 liiiHH-.'t) i j,

PULRfc-PN nUHt) DRbi'l SITE

fcHlt, tRlE COUNTY, PA

H T"i N: i ui'l MH'obiiY HND i'.M F

I. SITUATION (13UO HRS., FRIDAY, o9/O:'i/ti7)H. USC LLHHK NUf'lFlfcD <j'dO».' Hf<S. i i i i 'o DM I'c. LIT i i u .i-<i'iHi..Kt.:-'i

THn'T THERti APPEARED TO bE A T Y PtLubRhPH l CHL EUNGrt UNMHNirt-'bl <.'C.5i.'G. UKbi'O l'lHr<Kt_U I -»'d'* 1 Wt-io L J. ... I I: U Lil-jMANIFEST AS 14991. OSC NOTIFIED OHM U. COPUb Ar.D b.SKELLEY) Ol- I HL Hi<UbLC.M Hi\Jb Hi-UiJt.b I t U I MUM (U L.i,_t.Ti itKMALKtM 10 VERIFY OR DENY 'i Y PLGbftHPh ICuL ERROK. t b.:,LWH'.J NU I It".ILL; f, If i I it'-^'Ji kxHib HN t. i<KuK HNU bi'iUULi; ::M'»IBbt.N L1ST£D ON THE MANiFtS T AS 14'-JHl. T.-it"UMAi.Kc.MTbi_L' LiMM il'.». '-jl'.LLLt. Y ; I l 1H I L'ULUl'ILN I H I 1 LJlM Ul LNfiUoL- L'LJL.1G ERROR UN MANIFEST WOULD L£ SENT TO ObC Al-»D THnT DHUMHAD L>LL.N HLL-LPlLU !-Ul< L'lbiJbUHL l;L.bf--i i I. I'iUlM 1 r t_ L- i I.,LJ

NUTiFlLU lUJiU H.<b. I Hit, I'M It. LI r L-HLl-lTHAT RULLGFF SHIPMENT HEJUIRLD

1CA r iUN BT ut_NtRAfUt< vMLKfi j,i..'U'<. L1 ; . tj.. ...VERBALLY NOTIFIED ChEM WASTE MANAGEMENT THAT r<ULLbKFCGNiAlNb'D HPMKUA il'iH I !-£L / "TJ i UNi, Ui" LKIJ^MtlD U-<U.'lo.ViSQLclEN, PROTECTIVE CLOl'HiNG, AND OTHLR SOLID Wnbit.Dl£L<KiS C'tNLRHFtiD Al l i l t I'i il)riN K'UHU LiKU>'i i. I I . •". i . u . iWASTE MANHbEMENV TOLD OiiC THAT CERT iFICA I IbN WbUL.J I..LAuDtD TO I'HL MMNlFESl. CtRT 1F 1 CH i luN WUbLU BL Uu It..... i;.<GLNbRATQR-S COPY OF THE MANIFEST, AND TI ••:/,!A LtiTTER DOCUMENTING Tub AuUlllUN WUULU b;.. i,LN i ! u I i ILosc. • osc CLAKK NOTIFIED OHM tj.copua AND u. S^ELLE--)OF THti Sli'UAflUN W l l H LHt-.r-l WHb I L MuNnULMt-N I HI ML) b;- i . it-APPLICABLE RCRA REGULATION CONCERNING BULK bn1P

r U i Ui<L r-LHNia

A. hlNHL HGLHUP WILL BfJ WIXlT I LN bh'UN f •iLKHUliLUL/bu.l'lLI I IE DISPOSAL AND UPON FiNHL INVOICING F RbM tRCb.

DH'»'L .^H i LJ.-I : . uSCL. [ bA MWRIE. CLAWK, JK. useL-'.J t.r-'H r<._ L' A UN . 1 11

PKJ.LADt!LPHlA, PA A P 1 H J 2 2 6

To: ERD/u£KR (EPA55I1)To: T.MASSEY (EPA9374)

From: S.JARVELW (EPA93-+1) Delivered: T..te JJ^-Sea-fa/ 1 . 4 i iliVubject: POLREP 21 PAGAN ROAD

".•lail Id: IPM-163-87O929-13219122S

PULRL'P #21PAGfTN ROAD DRUM SITEERlL. I-'A

ATTN: TOM MASSEV AND TIM FIELDS

I. SlTUA)ION

A. OSC RECEIVED DISPOSAL NOTIFICATION OF ACKNOWL-EDbEMbNTFOR WASTES TRANSPORTED UNDER MANIFESTS CWt-lA 35u5.'0(DISPOSAL AT LHbM WAS7L MtlNHbLMLNT ) . AND Ofc,5i.''.j ANDOt-tii.'b (DISPOSAL AT THLKMALKEM) .

E. osc AWAITING FINAL INVOICING F;?G,I ERCS.

C. FIIMML PULREP WILL BE WRITTEN uPuU liuCLiPT OF F INuL

- nVlD WRIGHT. OEr.CLISA MARIE CLttRK. JR. GSCEPA REGION III

A. PA

A R 1 G C 2 2 7

PAGAN ROAD DRUM SITESUMMIT TWP., ERIE CO., PA

ATTNl TIM FIELDS AND MIKE ZICKLER

SPECIAL BULLETIN - PROJECT STATUS

I. SITUATION (12OO HOURS, FRIDAY, OCTOBER 30, 1967)

A. FINAL DISPOSAL OF REMAINING DRUMS HAS BEEN COMPLETED.

B. OSC REPORT IN DRAFT.

C. OSC HAS DETERMINED FINAL PROJECT CLOSURE AS OF

II. FUTURE PLANS

A. OSC REPORT TO BE FINALIZED AND SUBMITTED AS PER NCPREQUIREMENTS PENDING SITE CLO6EOUT AS DETERMINED BY THE OSC.

DAVID WRIGHT; oscEPA REGION IIIPHILA., PA

APPENDIX H

DELIVERY ORDER

r- /"* pi, t- J

DELIVERY ORDER .OR EMERGENCY RESPONSE CLEANUP SERVICES

(Thrt dmttvory ortmr it iftuod tubfaet to mil farm* and condrteont of tfm eontroa idmfXitimd in Bloc* 2.1. DATE OF ORDER 2. CONTRACT NUMBER 3. ORDER NUMBER

4. TIME OF INITIAL ORDER flf irmiml ardorwot vorbol)

TtmmZano)

6. DELIVERY ORDER CEIUNG AMOUNT (OUiamtod Amount)]f, /;•/)J V,

GAM6. ACCOUNTING AND APPROPRIATION DATAAppropciation Numbar Documant Control No. Account Numbar Object Claw

7m. ISSUED TO: CONTRACTOR (Nmiim. Addrmtt. and ZIP Coda)

IIBa. ISSUED BY: ORDERING OFFICE r/Vwrw.

2ZZT//£:

pH 'LA PELPmA . ?*'7b. PROGRAM MANAGER (Norm and Phono Numoor) EPA REGIONlSCG DISTRICT^

1ZL8c. ZONE

7c. RESPONSE MANAGER (N»mm mrd Phorm NumlMr) 8d. ON-SCENE COORDINATOR /rVwm •«/ />/><•/>• Numbor)

9. RESPONSE LOCATION (Sfto fiamt end/or Addrou and ZIP Coda)

• \ji-r.mr

10. CONTRACTOR REQUIRED ON SITE fD*M am/ r/m#;tSpocrfy Jimm Zona) O XDP*

1 1 . REQUIRED WORK COMPLETION DATEc /•? /£•

tMPLETtONI

i/641 2. STATEMENT OF WORK

Th« Contractor •hell furnith th« rwctMMry porsonrwl. m»t«r i.l«. wrvlcM, f«cillti«t. and otrwrwHM do all thing*nocMMry lor or inektont to th« p«rformanc« of Jho work Ml forth b*tow:fjrtACTGH. h^ii. ^.TAthe, i JVc*? /><«y^ »«/ *i.yz.tf /•"-

70/ A/O/A *- P/Sr*O-C4fc.

j r- r fo -rPAcrot ."*<.*. PGILF **™ ZCXL. /%7n-»4-»xt<-,S7>i A /'*/<£• ;"'

TD

o*»neiU xjr. /ruiT? TOT C esc.

. . _, .70 comtx- AMQ srA&iuimt -TH£.S/T&

13 ORDERING OFFICERNAME/TITLE SIGNATUR DATE

/O^tr /?6(,

APPENDIX I

MANIFESTS

n P ! n ~i 9 oAU I u J -•-

HAZARDOUS WASTE MANIFEST(As Required By The Alabama Department of Environmental Management) —

Meate print or type. (Form omtrgnad for too on olito (tl-pach/ typewriter.) Fom, Approved. 0MB No. 20SO4039 E«p»« 8-30-w

WASTE MANIFESTGenerator s US EPA ID No. Manifest 2. Page 1 I Information in the shaded areas' ~ "~———"- is not required by Federal

law.

15. Specul Handling Instructions and Additional Irformetion

16 GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above byproper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highwayaccording to applicable international and national government regulationsIf I am a large quantity generator. I certify that I have a program m place 10 reduce the volume and toncity of waste generated to the degree I have determined to beeconomically practicable and that I have selected the practicable method ol treatment, storage, or disposal currently available to me winch mmimnes the present andfuture threat to human health and the environment. OR. if I am a small quantity genernto/. I have made a good faith effort to mmimite my waste generation and selectiMe best waste management method that is available to me and that I can allord

I >rintad/T<

TVi/'K*yped Name ^ ]>Jpna)Mra/' /•• y / Month Oty Yeer

__________I <£?! AX•&IT.TWnaoortar 1 Admowlajgamern of Receipt of Materials

Printad ypad Name Signature . / j£> -- s» / Month Oey Year

18. Transporter 2 AdtnooHadBarnanot Receipt of MaterialsSignature j pjPrlmad/Tvpad Name

19.0iaerapancy Indication SpaceP P ! r ~ 9 :It h I w ~ - -

20.Facility Owner or Operator Certification of receipt of hazardous materials covered by this manifest e«cept as noted in Hem 19.Printed/Typed Name I Signature

HAZARDOUS WASTE MANIFEST(As Required By The Alabama Department of Environmental Management)

Mease print or type. /Form devonod for toe on elite (12-pHch) typewriter.) Fom Approve. 0MB Ho. 2060-0039 Ejmrei 9-30-86nA£AnUUU5 i generator * u*» SPA 10 NO. Manifest

WASTE MANIFEST2. Page '

ofInformation in tha shaded areasis not required by Federallaw.

4. Ganarator-f Phone (s. transporter i company Name 6. US EPA ID Number

" •• • • ._____________________I '-I 'I -I -I • I -I -I "I 'I r-| '-Ia. US EPA ID Number

I I I I I I I I I I I Ime. f .icuiiy name ano 9110 Aooress i u. US EPA ID Numbar

CHEMICA. . ASTE MANAGEMENT. INCEmelle FeeAlabama H,? -ay 17 at Mile Marker 163Emelle. Alaba.-na 35459_____________________II Ll P| °l °l °l 6 I 2 I 2I * I 6 I *

11. US DOT Description (Including Proper Shipping Nome. Hazard Clet*. end 10 Mumoarf

.:« I -.'J

CWM Profile Number •'.... -'.'"• ,

CWM Profile Number

CWM Profile Numbar

CWM Profile Numbar

15. Special Handling Instructions and Additional Information

V

16 GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above byproper shipping name and are classified, packed, marked, and labeled, and are m all respects m proper condition for transport by highwayaccording to applicable international and national government regulations.If I am a large quantity generator. I certify that I havo a program m place to reduce the volume and loudly of waste generated to the degree I have determined to beeconomically practicable and thai I have selected the practicable method of treatment, storage, or disposal currently available to me which rninimxes the present andfuture threat to human health and the environment. OR. it I am a small quantity generator. I have made a good faun effort to minimize my waste generation and selectthe best waste management method that is available to me and that I can afford _____________________________________________Printed/Typed Name Signature Month Day Year

.-____. . . *•—* i i'--i/ i-i i1 Acknowledgement of Receipt of Materials

Printed/T Signature • Month Day Year

IS.Transportar 2 Acknowledgement of Receipt of MetertelkPrinted/Typed Name Signature Month Day Year

19. Discrepancy Indication Space

20.Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Hem 19._____________Printed/Typed Name I Signature " Month Day Year

IAM-OSIO •LPCC2IVS1

Form Approved. Qua No. aeoofla». exatrm KM»in «w ahadad aneaa ia not

PfrPranoAaofc* i'JgSSr od ttSXm?"*''"*"*"1OSIPA•41 CttMtnc B«il41aff. PbLUtUlsM*. PA 19107

SfT-JlUAttt tev»5. Tnraportar 1 Company Nama7 7 Inc.

7. TranaporMr 2 Company Nama

9. OMigr»M Fatitty Mm* and SMaSCA ChtMfr-1 S«rvieM11700 8. Stooy XoludChle«r»a

11. US DOT OMCrfpdan (nttumng Smofina Homo, Hum* Cmm*, ami

OU1M3. 0» C46115

P.O. IJ3S97I-24547 VopttOrfer

w fuNy Mid •ccureMly dMCribtd ibovv byprap«r stripping mm* and am dmMlacl paotod, matted, and labilidl and an In aN napacti In pfopar condition for transport byhighway aoooftfkig to appHc*Ha bUMatfoml «td Mttonal penaiiimanl nouJaHnrn, and NUnote raguiatlona.

3002(b» ol RCftA, 11 aiap o 1>r7ttSl haiia a prog Jn piaca to >«tooa tt%» wohanayl ladcHy of waala ganaralad to th dagnNTJ>aw« «nTWni«l"tb'baaoonoffltoaUy piacllcaMa and I hava aalaclad ttia nalfwd of traaftnianta atoraoa or dlaD0aal cunantly avallabia to ma wMch minlmizM tha praaont and futurettmom omt tat •M ^ aa. tmomammmfem mmmmam t ammt ammmmmmmmjmammmmmmmmmt • • .^ r — ' •' C ™™™— ^ ^ ~UWWa. IW allWi n nV BVI flHB HV Wmfrft'aWim mwm - _ f f * * ~\ - • " "I l* Mf.A

7,. **««* Oar

Montr* Day

'i i. i it9. macrapMtcy IndkaQpn Spac-*

aaPadlKy Owner or Oparaaor CartHlcaMon of facrtpt of hMardoua malarlala cooar l by tMa manMaat axcapt aa noi'viniaoYTjr'poo Nawia

»202 / 426-2675PUtt-im-P*. P+KT - 6 GENERATOR

2*mCHURCMXROAa aUJMOB 62706 (217) 7*2-6761

tu Qanaiaaji'a US EPA O Na aga t Rnaflaneithaahadsd** • f«Mred by Federal Im

B.

•41•MO* nan (L 215'' i S97-31M Act!

& Tranapprtar 1 .7 7 Zm.

7. TranaporHr 2 Company Item* USERADMnte

FacBfNBnaand USEPADNUrtMr

11700 S. StMj X«ln4 AT*.

11. US DOT PaaeiEttjn (mrtimmg SMpping Mama. Nuartf Ctaa*. e*d 0

P.O. fJ3at7K*-24547

«MaMa of tMa conatgrmanl am iMRy and accutatary daacdbad abova by__^ t kaAadA ••«< -— T- M _ ^ _ •— ^ ^ - - - -«*• - _MI ••••Hk mi HV m» am ivaoade •• mnmmt Mmmmn

mmfmmjf auuntng toUntaaalama orravjMWi feoMttaAily to a« ari'4rrirnlzailioncartlrlcatk)n under Secltoo

flta votusna and toatrtly of vaala pananMad to Ina daQflaa I hava datarminad to baordtapeaal CMWrtty a«aia_Wa to ma wMch minimizes the praaant and future

I DataMorrtft Oaf

I 1 I I I

mtonm Day YamrI I I L I I . ,

Moorn Day raar

. 1 1 1 1 1 !MUJNOI& 217/7*2-3637___________ '24 HOUR EMEflOENCY ANO SPTU. ASSgTANCg NUMBCflS' QUTSCg TIIIMOet 600 / 424 602 or 202 / 426-2675

PAST - 6 OEfCRATORMRT-3MCajTV PART - 4

• • s m-. *»• M-"B> •«•> ••••• «» •»•«

2200 CHURCHtL ROAD, SPBWGFeLD, LUNCHS 62706 (217) 782-6761 I.S32-OS10^ LPC6ZS/81

part or lype._____{Tom o»ooj»« lor uee on om» (12-o»c*»| lyt-xnur) EPA Form 8700-22 (3-84) Form Approved. OMB No. 2O5OOOM Expires 9-3O-ae

t

UNIFORM HAZARDOUS i- Generator's US EPA D No. Document No.WASTE MANIFEST IP A ? OOOOO 2 D6X I 00001

3. ir-1'COftCQQ841 Chestnut Building, Philadelphia, PA 19107 'L * iDPUbOO4. Getwator-s Phone ( 215 ) 597-3184 Att; Dave Wright

2. Page 1of 1

formation in tha snaOed areas s notrequred by Federal law, but * recjured

Matjfa-n Oocumant Nunbar

-f , , , AS. Transporter 1 Company Nama 6. us EPA C Number7 7 Inc. I OHD000772558

CJ. Tranporter'sP/rt.,+4.,1 .«p. 7.04216), 336-8877 Tmporlar%Pnona'

7. Transporter 2 Company Nama 8. us EPA ID Numbar Tranaportar's D••*'- .-k f :-,*r, .-e- Tranapcrter'a Phone

9. Designated Facility Nama and Site Address 10. US EPA to NumberSCA Chemical Services11700 S. Stony Island Ave.Chicago, IL 60617 I ILD000672121

HFadMy*a Phona'(312) £646-5700

11. US DOT Description (Including Propar Shipping Nmmm, Hazard C'ass, and /O Number J

0 =Waste Flammable Liquid N.O. S. Flammable LiquidUN1993, OHM-632261

Waste Flammable Solid N.O.S. Flammable SolidT UN1325, OHM-G46117

J.

15. Special Handling Instructions and Additional Information / *v*!cr>!_*r*Z*'v»**> \£f7f.

P.O. # J3897E-24547 Work Order #87-0667

16. GENERATOR'S CERTIFICATION: I hereby declare that the contents oi this consignment are fully and accurately described above byproper shipping name and era classlNed, packed, marked, and labeled, and are in all respects In proper condition tor transport byhighway according to applicable International and national government regulations, and Illinois regulations.Unless I am a small quantity generator who haa been exempted by statute or regulation from the duty to make a waste minimization certification under Section3002fb» of RCRA, I a»eo certify that I have a program In place to reduce the volume and toxlcity of waste generated to the degree I have determined to beeconomically practicable and I have selected the method of treatment, storage, ordiepfcsa) currentr eTfailabla to me which minimizes the present and futurethreat to human health and the environment_________________/^s ____./ /______ ________I Dat>

*"""" Dt>' Yt"tedfTyped Name

i7TTransporteri Acknowledgement of Receipt of MaterialsMonfft Day rearPrinted/Typed Name

TB. Transporter 2 Acknowledgement of Receipt of MaterialsPrlntedrTyped Name

Discrepancy Indication Space /fWTZ&tS

20. Facility Owner or Operator Certification of receipt of hazardous materials covered by ttHa manifest except as noted In Hem 19.____p—— 0*tt-PftitedrTyped Name —— ^Mame ^ _,

fr C7 f#*Mja*-£:Stgnatur»«r\ .^) . , _^ Month Dty Yamr

•4 fLUNOtS: 217/762-3637 _________________ "24 HOUR EMERGENCY AND SFXL ASSISTANCE NUMBERS* . .

DtSTRtBUTION: PART - 1 GENERATOR PART- 2 KRA BART - 3 FACUTY PART - 4 TRANSPORTER FKFfT • 5 tEP*. P T J Q Q 2 3 b

»» «g«<«i mu* • amm* *•< in mi' "»> ** nmm*umi <g»t »••«. THi lorn *m i1 1 1» totem 11.mat mamtt «

«J»»«**e*eNlA_HHOT6CTIONAG£M;Y OMSKM OF LAND POLU/TKM CONT

2200 CHURCHU.Rr>ia

Of mJLtttlMS

XfUJNOS 62706 (217)7*2-6761•*

«7OO-tg f X4| ' Pe»B) Aapeiad. OH* MeUNIFORM HAZARDOUS - l-Gerwato-sUSEPAce

A I (SBSl

Ml4 Generator's Phone (

. FA 19107) 3*7-3184 Attl D*W»

5. Tranaportar i Company Nama US EPA O Numbar7725M

7. Tranaportar 2 Company Nama USEPADMaitfMr

9. Daalgnated FadKy Mama and Site US EPA D Numbar

11700 S. fumy ?•!••« AT*,IL 40*17

11. US DOT DaacrtpUon (Indudmg ***>* Snipping Mama. Kazard Clam*, mad O Mkanberl

0*1993. OU-C322il

V««c« rimmmmblm Solid B.O.S.QI1325. Ofl«-«44I17

»!?•• -•*.

15. Special Handling Instructions and AdrMonal trrformatlon

P.O. * J3S97B-24547 Work Order M7-06*7

16. 0,IEr«***-JTOR*8Cgl*Tlr-*CATlOI»: _ --__.*.-- __•__. -proper tMpplng AMM •nd cm dBMntod ptdMdi flMtted, <nd tebthNit end w HI AN iwpoctB MI prapor oondftiOei fof tmwport byMghway according to applicable IntemeBonel and natter (

lion under Sectiondetermined to be

eoonoalcalry practicable and11 mum ealectad the method of treatment, storage, or djaqpael cunentl eealiabie to ma whtet> mfcijrntoas the present and futureto human health and we eflvvonment* ^? / f \ i^

' *_________-^______________I ^____umim

that the contents of Ma oonatanment mrm fwRy ar, marked, and labeled, end are In en leepecla m |t rmHormm government lagutabens, end IHinote re

3002<t of RCF>O 4J<joiC<ir tt*ail ha»e apmgry In p«e«y to redi rhe volume end taddty cf weale ganeraledlonie degree! heve i. eoonofflcalty practicable and I Nave aelocted Vie raettiorl of tfaetmeirt, etomoe, or dtonpeeJ cunentfy aeilable to me which rnMfnbee the ei

Month Day VeerL I 1 4 I I

1ftanCI

20. Facility Owner or Operator CertlUcaBua o> feeerp< of naaartfoue materials covered by Ma ia*iHea* except as noted, hi Hem 19. I DataPrtnteoyTyped Name Slgneture . \ Month Day Year

'______I I I I I I•mOJNOB: 217 / 7*3-3637____________ -n,-- «»«-««->.. ~~ *r .~*~, >~ .~~-~ , QtuTSCfS UJIOBt *00 / 42»«a02 or 202 / 426-2675I^TIIBUIIUHPART-IOENERATOR PART-2**yi> fWTT • 3 FJOOLfTY BART - 4 TRANSPORTgR PART-SgRA PERT - * GENERATOR___________"*•"• *L _ _ _ _ ^ _ _ . SH i f L MiMT_l*_OO MOT

V mfmWmmW mt Pmt » MiMd StlMO »V *» «f tMMM. »«rihrtM «l Mb iMll ••• fMr •«•.• »> • *• I* » SMAOO M tf*

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141Qtawatof'aPtanVf

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11700 m. mtfJmJ Imlmmm A»»ett 40*17

11. US DOT Oaacrtptton (ttc*d*g

OU991* Omm 9322,1

mfAU 1.0.1.17

P.*. f J3197B-24MT «ulk te**c M7

**•»•» determinedtttapieeent and*

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1 1 I I 'I I

M HHOB: 217 / 7*2-3*37_______•mTRBUTTON.ROUT• 1 QPgUTDR MHT-t

APPENDIX J

INCOMING SPILL REPORT

RRIQC23S

•I <U«V. <: 'tPCCMPC SPILL REPORT CASPJL//-

RBGION m BY» :** /<? ____ _ gqgi /ey/A/p? TIME;3RTED TO NPC O BY*

PHCME •

>w-» /%

LLERi NKC» jflftr. ^^ ^w //<f*>*,»4v» -25v. PHONE I P /. - /

ADORES3:

LL LOGMRCNsA3TON:

ACORCSSt

CITYi COJtTY; SIrVTE;

NEAREST

_LL CtMA; QrttE:

GVUSE:

SPILLCDt 1ff& efT~m$ -&!» STREW: RSJ10VM. OOOE:_

CLL OOMDiatlPtri *J#/7<S- CLEW-UP:JPOKSE

7 rjgqs; MHEELING FIELD OFFICE:.

SOSTE/iaCfdea_____________ OTHER:

A R! C C d' :• 0