ocdimage.emnrd.state.nm.usocdimage.emnrd.state.nm.us/.../AO/B-53688/PENV000000AP1_0049.… · SX\TE...

AP - O0\

ANNUAL MONITORING REPORT

YEARfS):

STATE OF NEW MEXICO DEPARTMENT OF HEALTH

SCIENTIFlU LAPCTtATORY DIVISION P.O. Bo:; 47C0 700 Camino de Salud, NE

Albuquerque, NM 87126-S700 [505]-841-2500 WATER CHI USTRY SECTION [5051-841-2555

May 26, 1994

Request ID No. 014374

E I S n E M E E E n L J a B B E I E a i

• A ! LYriCAL REPORT 3 S 0 Aicesdon ilo. WC-94-1188 • Distribution

( J User 70320 (}J Submitter 260 (20 SLD Files

To: R. Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088

From: Water Chemistry Section Scientific Laboratory Div. 700 Camino de Salud, N.E. P.O. Box 4700 Albuquerque, NM 87196-4700

Re: A water,Nonpres/No sianpL i .:Lr.:» '.•> j thie 1 ."v.3tory cn March 28, 1994

_ ^I ' . iOC A I i;±C t)ATA COLLECTION " """ LOCATION

0«:25-Mar-94 By: Ols . . . • - MW-9/5 At: 10:40 hrs. In/Near: SunlardPaik

ANALYTICAL RESULTS Analvsis VHue D. Lmt. Units

calcium 2.'..00 mG/L magnesium 107.00 mG/L potassium l>.00 mG/L sodium 1440.00 mG/L bicarbonate . 712.00 mG/L carbonate 0.C0 mG/L chloride 1199.00 mG/L fl u o r i d e 0.80 mG/L sulfate 2102.00 mG/L Ion Balance 96.20 % t o t a l diss resid 5730.00 mG/L

Kcviiweu By: C. Rachael Howell 05/18/94 Analyst, Water Chemistry Section

S X \ T E OF NEW MEXICO DEPARTMENT OF HEALTH

SCIENTIFIC LABORATORY DIVISION P.O. Box 4700 700 Camino de Salud, NE

Albuquerque, NM 87196-4700 [505] -841-2500 AIR & HEAVY METALS SECTION [5051-841-2553

May 11, 1994 I ANALYTICAL REPORT • ^ T - T ^ n • • Q£ Submitter 260

S)No.St 014373 • SLD Accession No. IC-94-0046 B « SLD Files

Distribution

R. Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088

From: Air & Heavy Metals Section Scientific Laboratory Div. 700 Camino de Salud, NE Albuquerque, NM 87106

A water,Nonpres/No sample submitted to this laboratory on March 28, 1994

User: NM Energy & Min - Oil Conserv. , NM

DEMOGRAPHIC DATA COLLECTION LOCATION

On: 25-Mar-94 By: Ols . . . MW-9% o At: 10:40 hrs. In/Near: Sunland Park

ANALYTICAL RESULTS in mG/L Analvsis Value Analysis Value Analvsis Value

Aluminum 1.80 Copper < 0.10 S i l v e r < 0 .10 Barium < 0.10 I r o n 13.00 Strontium 5 .70 B e r y l l i u m < 0.10 Lead < 0.10 Ti n < 0.10 Boron 1.10 Magnesium 110.00 Vanadium < 0 .10 Cadmium < 0.10 Manganese 3 .90 Zinc < 0 .10 Calcium 350.00 Molybdenum < 0.10 Mercury < 0.0005 Chromium < 0 .10 Nicke l < 0.10 Selenium < 0.0050 Cobalt < 0.05 S i l i c o n 0.80

Laboratory Remarks; ICP by method 200.7 on 4/29/94 by RAH. Mercury by method 245.1 on 4/13/94 by SD. Selenium by method 270.2 on 4/8/94 by RAH.

Reviewed By: Jim F. Ashl Supervisor,

5/11/94 & Heavy Metals Section

Al * & HEAVY METALS ANALYTICAL REQUEST FORM

SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E.. ALBUQUERQUE. NM 87106

Air & Heavy Metals Section - Telephone: (505) 841-2553 31 Request

1 ID No.:

SLD No.

Date Received

_U Priority Code»

TftttyT

2JUser Code #: I 7 I 0 I 3 I 2 I 0 I

6 I County: ~

cil EID-SLD

Facility Name:

8 IState

Sample U 1 I _ Gf <C Location: il 1 iW i i / \~* i I I I I i i ' i ' i

raj Collected By: JLL

First 0\l\ s\Qh ILlatalt.

On: W / O ^ / >S At:l l \ Q \ 9 \ Dl hrs. Data: (YY/MM/OO) Tima: a«w.«o«

XOOwn • '300 hr*.

_njCodes: . l l l l l l I I l - l l 1 i i i l l l l

12 Latitude (DDMMSS)

I I I I I I I i m0i» in Submitter WSS # Organization Longitude (OODMMSS) I*1***

I I I I I I I N I 13 Report 14l Phone #: To: Roger Anderson (505) 827-5812

Longitude (OODMMSS) I*1*** I I I I I I I N I

Addrra

New Mexico Oi l Conservation Division i c Sampling Information: « . «. ^ G r a t J S a m p l * PurpOM: r^Pomoo«it« (Comeout*

p. n. Rox ?nas • - Complianca n - Flow Proportioned n-Chock Q. Equal Aliquot S£Monitoring Sampla Split w/Permiftea • • Spatial Q . Chain of Custody

City, SUM Zip

Santa Fe, New Mexico 87504-2088

• - Complianca n - Flow Proportioned n-Chock Q. Equal Aliquot S£Monitoring Sampla Split w/Permiftea • • Spatial Q . Chain of Custody

Data: PH: **7i i , Conductivity: 3 umhos ^2. *£~ Tamparatura: 1181 Flald Notaa/ — 1 Samnla * :

Chlorina C, RasiduaJ: mg/l, Row:

17| Sample Source: U-Stream •-Lake •-Drain •-Pool •-WWTP

^S^Well; Depth: . T>Spring •-Distribution ••Point-of-Entry •-Other

J9J Sample Type: J^-Water, Q-SoB, Q-Food, 3-Wastewater, •-Other

20| Preeervation: n-VVNF Watar f « * Praaarvad; Filtarad j&WNN Watar Not Praaarvad; Not Filtared

' • • W f Watar Praaarvad with Nitric Add (HN03); Filtarad • WPN Watar Praaarvad wtth Nitric Add; Not Filtartd ' WNL Watar Not Praaarvad in Fiald; Plaaaa Add HN03 at Lab ^ICE Watar load

a**™ —

This form accompanies a alngta sampta consisting of: / -1 liter cubitainers (1 quart)

- 4 liter cubitainers (1 gallon)

111 Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required.

• - (721) SDWA Group I + other parameter(s) marked below M - (704) ICAP Scan • - (720) SDWA Group I Only

• - Aluminum • - Arsenic • - Barium • - Cadmium • - Chromium • - Cobalt • - Copper • - Iron

Remarks:

• - Lead • - Manganese

Mercury - Molybdenum - Nickel Selenium

0 - Silver • - Uranium

• -Vanadium • -Zinc • -• -• -

•-zzzzz • - Z Z Z Z • -

S L D 8 9 1 2 - H M Form Naw 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPY I

"STATE OF NEW MEXICO DEPARTMENT OF HEALTH SCIENTIFIC LABORATORY DIVISION

P.O. Box 4700 700 Camino de Salud, NE « Albuquerque, NM 87196-4700 [505]-841-2500 U ORGANIC CHEMISTRY SECTION [505]-841-2570

i^ 9 4 m 8 50

S ANALYTICAL REPORT •

• SLD Accession No. OR-94-0915 g

Distribution QUser 70320

Submitter 260 (x) SLD Files

To: Roger Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088

From: Organic Chemistry Section Scientific Laboratory Div. 700 Camino de Salud, N.E. P.O. Box 4700 Albuquerque, NM 87196-4700

Re: A water,Purgeable sample submitted to this laboratory on March 28, 1994

On: 25-Mar-94 At: 12:45 hrs.

By: Ols . . . In/Near: Sunland Park

ANALYTICAL RESULTS: Aromatic & Halogenated Purgeable [EPA-601/21 Screen (754) Parameter Value Note POL Units

Benzene 127.00 10.00 ppb Toluene 2 .40 T 10.00 ppb Ethylbenzene 1.90 T 10.00 ppb p- & m-Xylene 8 .40 T 10.00 ppb o-Xylene 3 .00 T 10.00 ppb Isopropylbenzene 15 .30 10 . 00 ppb

See Laboratory Remarks for Additional Information Notations & Comments: PQL = Practical Quantitation Level. A = Approximate Value; N = None Detected above Detection Limit: T = Trace (< Detection Limit); U Evidentiary Seals: Not Sealed^|

P = Compound Present, but not quantified; Compound Identity Not Confirmed. Intact: No | ~ | , Yes|~| & Broken By: Date:

Laboratory Remarks: Foamy sample; unable to achieve a lower detection l i m i t

Reported compound i d e n t i t i e s were confirmed by GC/MS

Compound Note Value PQL (ppb) n-Propylbenze 29 10 1,2,4-Trimethylbenzene T 3.2 10 sec-Butylbenzene T 6.9 10 n-Butylbenzene T 6.3 10 Naphthlene 23 .7 10 Methylene c h l o r i d e 10.9 10 1,2-Dichloroethane T 2.7 10

(Continued on page 2.)

ANALYTICAL REPORT SLD Accession No. OR-94-0915 Continuation, Page 2 of 4

VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: NM SCIENTIFIC LABORATORY DIVISION N/A

Lab Code: N/A Case No. Ma t r i x : ( s o i l / w a t e r ) Water Sample w t / v o l : 5.0 (g/mL)_ Level: (low/med) Low % Moisture: not dec. N/A dec. N/A E x t r a c t i o n : (SepF/Cont/Sonc) N/A GPC Cleanup: (Y/N) No pH:

SAS No, Contract: N/A

N/A SDG No. N/A

Lab Sample ID: SLD Batch NO:

OR-94-915 127

Date Received: 3/28/94 Date Extracted: N/A Date Analyzed: 4/05/94 D i l u t i o n Factor: 10 CONCENTRATION UNITS: (ug/L or ug/Kg) : ug/L

This sample was analyzed f o r the f o l l o w i n g compounds

CAS NO. COMPOUND CONC. Q POL 67-64-1 Acetone U 50.0 71-43-2 Benzene 127 10.0 108-86-1 Bromobenzene U 10.0 74-97-5 Bromochloromethane U 10.0 75-27-4 B romod i c hioromethane U 10.0 75-25-2 Bromoform U 10.0 78-93-3 2-Butanone (MEK) U 50.0 104-51-8 n-Butylbenzene 6.3 J 10.0 135-98-8 sec-Butylbenzene 6 . 9 J 10.0 98-06-6 tert-Butylbenzene U 10 .0 1634-04-4 t e r t - B u t y l methyl ether (MTBE) U 50.0 56-23-5 Carbon t e t r a c h l o r i d e U 10 . 0 108-90-7 Chlorobenzene U 10 . 0 67-66-3 Chloroform U 10 . 0 95-49-8 2-Chlorotoluene U 10 . 0 106-43-4 4-Chlorotoluene U 10 .0 96-12-8 1,2-Dibromo-3-chloropropane U 10.0 124-48-1 Dibromochloromethane U 10 . 0 106-93-4 1.2-Dibromoethane U 10 .0 74-95-3 Dibromomethane U 10 . 0 95-50-1 1,2-Dichlorobenzene U 10 .0 541-73-1 1.3-Dichlorobenzene U 10.0 106-46-7 1,4-Dichlorobenzene U 10.0 75-71-8 Dichlorodifluoromethane U 10.0 75-34-3 1,1-Dichloroethane U 10.0 107-06-2 1.2-Dichloroethane 2.7 J 10.0

75-35-4 1,1- D i c h l o r o e t h e n e U 10 . 0 156-59-4 c i s - 1 , 2 - D i c h l o r o e t h e n e U 10.0 156-60-5 t r a n s - 1 . 2 - D i c h l o r o e t h e n e U 10.0 78-87-5 1,2-Dichloropropane U 10.0 142-28-9 1,3-Dichloropropane U 10.0 590-20-7 2,2-Dichloropropane U 10.0 563-58-6 1,1-Dichloropropene U 10.0 1006-01-5 c i s - 1 . 3 - D i c h l o r o p r o p e n e U 10.0 1006-02-6 t r a n s - 1 . 3 - D i c h l o r o p r o p e n e U 10.0 100-41-4 Ethylbenzene 1.9 J 10 .0 87-68-3 Hex a c h l o r o b u t a d i e n e U 10.0 98-82-8 Isopro p y l b e n z e n e 15 .3 10.0 99-87-6 4 - l s o p r o p y l t o l u e n e U 10 . 0 75-09-2 Methylene c h l o r i d e 10.9 10.0 90-12-0 1-Methylnaphthalene U 10.0 91-57-6 2-Methylnaphthalene U 10.0 91-20-3 Naphthalene U 10.0 103-65-1 n-Propylbenzene 29 10.0 100-42-5 Styre n e U 10.0 630-20-6 1.1.1.2-Tetrachloroethane U 10.0 79-34-5 1.1.2,2-Tetrachloroethane U 10.0 127-18-4 T e t r a c h l o r o e t h e n e U 10.0 109-99-9 T e t r a h y d r o f u r a n (THF) U 50 . 0 108-88-3 Toluene 2.4 J 10 . 0 87-61-5 1,2,3-Trichlorobenzene U 10 . 0 120-82-1 1,2,4-Trichlorobenzene U 10 .0 71-55-6 1 , 1 , 1 - T r i c h l o r o e t h a n e U 10.0 79-00-5 1 , 1 , 2 - T r i c h l o r o e t h a n e U 10 . 0 79-01-6 T r i c h l o r o e t h e n e U 10 . 0 75-69-4 T r i c h l o r o f l u o r o r n e t h a n e U 10.0 96-18-4 1 , 2 , 3 - T r i c h l o r o p r o p a n e U 10.0 95-63-6 1,2,4-Trimethylbenzene 3.2 J 10 . 0 108-67-8 1,3,5-Trimethylbenzene u 10.0 75-01-4 V i n y l c h l o r i d e u 10.0 95-47-6 o-Xylene 3 J 10.0 N/A p- & m-Xylene 8.4 J 10.0 N/A T o t a l Xylenes 11.4 J 20.0

* CONC = CONCENTRAION DETERMINED PQL = Practical Quantitation Limit (Approximately 10 times MDL)

* Q = Q u a l i f i e r D e f i n i t i o n s :

B - I n d i c a t e s compound was detected i n the Lab Blank as w e l l as i n the sample.

D - I n d i c a t e s value taken from a secondary ( d i l u t e d ) sample a n a l y s i s . E - I n d i c a t e s compound concentration exceeded the range of the

standard curve. J - I n d i c a t e s an estimated value f o r t e n t a t i v e l y i d e n t i f i e d compounds,

or f o r compounds detected and i d e n t i f i e d but present a t a conc e n t r a t i o n less than the q u a n t i t a t i o n l i m i t .

N - I n d i c a t e s t h a t more than one peak was used f o r q u a n t i t a t i o n . U - I n d i c a t e s compound was analyzed f o r , but not detected above the

con c e n t r a t i o n l i s t e d ( Q u a n t i t a t i o n L i m i t ) .

QUALITY CONTROL SUMMARY FOR VOLATILES SCREEN

METHOD BLANK: A l a b o r a t o r y method blank was analyzed along w i t h t h i s sample t o assure the absence of i n t e r f e r i n g contaminants from l a b reagents, instruments, or the general l a b o r a t o r y environment. Unless l i s t e d below, no contaminants were detected i n t h i s blank above the reported d e t e c t i o n l i m i t .

COMPOUND DETECTED No Compounds Detected

CONCENTRATION (PPB)

SURROGATE RECOVERIES: SURROGATE

Bromofluorobenzene 2 -Bromo-1-chloropropane

CONCENTRATION 25.0 ppb 25.0 ppb

RECOVERY 95.6 90.8

SPIKE RECOVERY: The % recoveries f o r compounds i n the batch spike were from 80% t o 120% w i t h the exception of the compounds l i s t e d below: COMPOUND CONCENTRATION % RECOVERY

No exceptions . ppb

Analyst: Patrick F. Analyst, Organic Chemistry

Reviewed By: 5k Richard F. Meyerhein 05/04/94 Supervisor, Organic Chemistry Section

ORGANIC CHEMISTRY ANALYTICAL REQUEST FORM

SCIENTIFIC LABORATORY DIVISION 700 CAMINO OE SALUD N.E.. ALBUQUERQUE, NM 87106

Organic Chemistry Section - Telephone. (505) 841-2S70 I3J Request User

Code* I 7 i a i 3 ; 2 | 0 i

Name? S f r J d z J i ^ ^ I t r

^quest ID No.

IIIII IIII III 028742-C

SLD No.

Oate Received

ij&eUnty:

J J Priority Code#:

M i ( W f o r T . cwBO>SLD

7--^JSample Location;

ipJCollected By:

i i i I I I L J I L J I L

Rrat ILIaUlt... On: W / O J / Z T " At:I / I ^ ^iJThrs

Data: (W/MM/OO)

Latitude (DOMMSS)

, 1 „L ' j 1 1

Longitude (DOOMMSS)

< I » '» I I

11 (Codes:

Submitter J I L

13| Report" To: Roger Anders.on

WSS # - I I I I 1.1

Orgai nizatlon

141 Phone* ^ (505) 827-5812

New Mexico Oi l Conservation Division

City, SUM Z * P. 0. Prrc ?naa Santa Fe, New ffexico 87504-2088

^ D a t a : P H : 7 ' ^ ' Conductivity: umhoa® 7 / ' / *fc

12 i_J 2 0lgrtlO

UU Sample Purpoaa

• - Complianoa "-Chack

Storing Spacial

S'toonitoring bj£ fFSpacial T f .

Sampling Information Grab Compoaita Q- Row Proportion* ff- Equal Aliquot

• samp pla Split w/Parmittaa Chain ot Cmtody

18|FlaWNotoa7 Tamparatura:

Chlorina C, Raaidual: mg/l, Row.

17| Sample Source •-Stream G-Lake •-Drain •-Pool •-WWTP

K-Well; Depth: . MJ-Spring

•-Distribution •-Point-of-Entry •-Other

U*((- MLHl

19J Sample Type: ^Water, Q-Soi Q-Food, 201 Pre—rvatton; 1 Q-NP No PraaarvHon; Sampla atorad at room tamparatura

Tglp-loa SampJa atorad in an tea bain (Not Prown) P-TS Sampla Praaarvad with Sodium TWoautfata to ramova chlorina rasiduai

•-P-HOJ SlJT^f^aaMvadwrmHydrecMorto jgC-Ottar ^ < f f _

• -Wastewater, TJ -Other, This form accompanies a alngta «ampl« consisting of:

>— septum vial(s) (volume - 7t> * I ) - glass jugs (volume - ) - (volume • )

211 Analyses Requested: Please check the appropriate box(es) below to indicate the type of analytical screen(s) required. Whenever possible, list specific compounds suspected or required.

Volatile Screens; (753) Aliphatic Headspace (1 -5 Carbons) (754) Aromatic & Halogenated Purgeables (EPA 601 & 602)

j • (765) Mass Spectrometer Purgeables (EPA 624) • - (766) SDWATotaJ Trirjalwnethanes (EPA 501.1) Q - (774) SDWA VOCs I (8 Regulated +1 (EPA 502.2) • - (775) SDWA VOCs II [EDB & DBCP] (EPA 504)

g Other Specific Compounds or Classes:

• - ( )

SI j = Remarks:

SemivQlatile Screens; - (763) Acid Extractables - (751) Aliphatic Hydrocarbons - (755) Base/Neutral Extractables (EPA 625) - (756) Base/Neutral/Acid Extractables (EPA 8270) • (758) Herbicides, Chlorophenoxy Acid • (759) Herbicides, Triazines - (760) Organochlorine Pesticides • (761) Organophosphate Pesticides - (767) Polychlorinated Biphenyls (PCB's) - (764) Polynuclear Aromatic Hydrocarbons • (762) SDWA Pesticides & Herbicides

SLD8912-QR torn Naw 12/se This Form WBI NOT Be Returned With Your Results. Please RETAIN A COPYI

* SCIENTIFIC LABORATORY DIVISION P.O. Box 47C0 700 Camino de Salud, NE

Albuquerque, NM 87196-4700 [505]-841-2500 WATZR CHEMISTRY SECTION [505]-841-2555

May 26, 1994

H K B E C l a E E E a a r S C B C r a H H B H M H H M H U I

\ /*JA TICAL REPORT \ * U ccisaij" fJo. WC-94-1191 m

Distribution QUser 70320

Submitter 260 (x) SLD Files

To: R. Anderson From: Water Chemistry Section NM Oil Consv. Div. Scientific Laboratory Div. State Land Office Bldg. 700 Camino de Salud, N.E. P.O. Box 2088 P.O. Box 4700 Santa Fe, NM 87504-2088 Albuquerque, NM 87196-4700

Re: A water,Nonpres/No sample submitted to tlar laboratory on March 28, 1994

DEMOGRAPHIC DAIA COLLECTION LOCATION

On: 25-Mar-94 By: Ols . . . V , MW-11 At: 12:45 hrs. In/Near: Sunlau! Prrl-

ANALYTICAL RESULTS Analvsis _ Value D. Lmt. Units

calcium 50.00 mG/L magnesium 60.00 mG/L potassium 15.00 mG/L sodium 1120.00 mG/L bicarbonate 1756.00 mG/L carbonate ' '0.00 mG/L chloride 863.00 mG/L fl u o r i d e 2.80 mG/L sulfate 3.80 mG/L Ion Balance U 6 . J % t o t a l diss ret i d 3798.00 mG/L

Reviewed By: C. Rachael Howell 05/18/94 Analyst, Water Chemistry Section

WATER CHEMISTRY ANALYTICAL REQUEST FORM

SCIENTIFIC LABORATORY DIVISION - 700 CAMINO DE SALUD. ALBUQUERQUE. NM 87106

Water Chemistry Section • Telephone: (505) 841 -2555

SLO No.

Date Received

LlUser Code*: ' 7»° <2 '2 '° '

31 Request ^ I D No.:

PUcm Form O StieaatHwt

5 Facility Name:

6 I County:

Priority Code #:

pr i -or T . c*il EiO-SLO Coordinanr)

TJCTtyy / fl 8 [State

MM. - ^ S a m p l e U T . _ ) /

Location: IPMIIA/I I l \ I i i i i ' i ' J I L J I I L lOlCollected*/ T I

By: Utlll^ First | 3 (Oh

ILIalal t . On: ? < / / & 3 / ^ At:l / 1>1 V1 J> I hrs.

Data: (YY/MM/OO) ~ Tim*' 2 4 •"• c l o c*

rycodes: .1 1 I I I 1 1 1 1 " 1 1 1 I I I I I I I

12| Latitude (DDMMS.S)

I I I I I I I o ni0i« in Submitter WSS # Organization Longitude (DOOMMSS) <•!<••*•*

I I I I I I I II I I 131 Report To:

Roger AAderson 14 Phone # : — 1 (305) C27-5S12

Longitude (DOOMMSS) <•!<••*•* I I I I I I I II I I

New Mexico O i l C o n s e r v a t i o n D i v i s i o n i c i Sampling information:

XT- Grab Sampla Purpoaa: 1ft. Compoarta g°"5°—

• - Compiianca r> Flow Proportioned n-Chaek r j - Equal Aliquot

JKfrMonrtoring Sampla Split w/Parmittee LTSpacial Q. Chain ot Custody

P. 0. 2088

i c i Sampling information: XT- Grab

Sampla Purpoaa: 1ft. Compoarta g°"5°— • - Compiianca r> Flow Proportioned n-Chaek r j - Equal Aliquot

City, SUM Zip Santa F e , New Mexico 87504-•2088

i c i Sampling information: XT- Grab

Sampla Purpoaa: 1ft. Compoarta g°"5°— • - Compiianca r> Flow Proportioned n-Chaek r j - Equal Aliquot

•^Data: PH: ~7*(?2-< Conductivity: U^j

17| Sample Source: •-Stream •-Lake •-Drain G-Pool ••WWTP

I9j Sample Type:^-WatBr, • -Wastewater, Q-Other_

2 / i i _ * j & Tamparatura: 2— umhoa i

18| Plaid Notaa/ Sampla # :

Chlorina C. Rasiduai: mg/), Row:

forVell; Depth: '•-Spring •-Distribution •-Point-of-Entry •-Other

tn~j* Uf.ll MUTU

20| Preservation: 1 — 0 - V M F Watar Not Praaarvad; Hltarad

^ W N N Watar Not Praaarvad; Not Rltarad Q- WPF Watar Praaarvad with Sulfuric Add (H2S04); Rltarad • - W P N Watar Praaarvad with Sulfuric Add: Not Rltarad Q-WNU Watar Not Praaarvad in Fiatd; Plaaaa Add H2S04 at Lab

ICE Watar lead Othar

• -So* . •-Food,

This form accompanies a single sampla consisting of: / -1 liter cubitainers (1 quart)

2iJ Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required. Group AnaJyaaa: • - (854) SDWA Group II (Nitrate as N) • • (861) SDWA Group ill (Fluoride) • • (860) SDWA Complete Secondary

Q (859) SWQB SS Anion • Cation Group + O (868) SWQB NPS Anion, Cation, Physical + TSS Q (869) SWQB Nutrient Analysis Group +

^(867) Major Anions & Cations

Cations: • - Calcium (as Ca) • - Magnesium (asMg) ~ •-Potassium (as rQ ~ •-Sodium (as Na) " • - Total Hardness (as CaC03)~ Anions: • - Alkalinity (as CaC03) • - Bicarbonate (as HC03) • - Carbonate (as COS) ~ •-Chloride (as CQ •-Fluoride (as F) • - Sulfate (as S04) "

Ion Charge Balance

Remarks:

Phys ica l Parameters: •-Color •- Conductance <mcnit*>e»9nQ •-Odor • - P H ••Surfactants • - Total Dissolved Solids •-Turbidity O t h a r • -

o-• -• -

Surfaca and Waste Watar: • - Biological Oxygen Demand ••Total Suspended Solids • - Chemical Oxygen Demand • - Total Organic Carbon • • Cyanide Nutrients: • - Nitrate + Nitrite (as N) • - Ammonia (as N) •-Total Kjeldahl (as N) • - Nitrite (as N) • - Orthophosphate (as P) • - Total Phosphorus (as P)

S L D 8 9 1 2 - W C Form Maw 12/89 This Form WSJ NOT Be Returned With Your Results. Please RETAIN A COPYI

STATE OF NEW MEXICO . . . f DEPARTMENT OF HEALTH

Albuquerque, NM 87196-4700 [505]-841-2500 AIR & HEAVY METALS SECTION [505]-841-2553

August 12, 1994

ANALYTICAL REPORT | SLD Accession No. IC-94-0049 \

• Distribution (JUser 70320

Submitter 260 (20 SLD Files

From: Air & Heavy Metals Section Scientific Laboratory Div. 700 Camino de Salud, N.E. P.O. Box 4700 Albuquerque, NM 87196-4700

Re: A wat not preserved sample submitted to this laboratory on March 28, 1994

On: 25-Mar-94 At: 12:45 hrs.

ANALYTICAL RESULTS in mG/L Analvsis Value Analvsis Value Analvsis Value

Aluminum 12.00 Copper < 0.10 S i l v e r < 0.10 Barium 1.30 I r o n 15.00 S t r o n t i u m 3.20 B e r y l l i u m < 0.10 Lead < 0.10 T i n < 0.10 Boron 1.40 Magnesium 72.00 Vanadium < 0.10 Cadmium < 0.10 Manganese 0.89 Zinc < 0.10 Calcium 120.00 Molybdenum < 0.10 Mercury < 0.0005 Chromium < 0.10 N i c k e l < 0.10 Selenium < 0.0050 Cobal t < 0.05 S i l i c o n 10.00

Laboratory Remarks: Acidified and Digested at SLD ICP by method 200.7 on 7/27/94 by RAH. Mercury by method 245.1 on 4/13/94 by SD. Selenium by method 270.1 on 4/8/94 by RAH.

Reviewed By: JimF. Ashby 08/11/94 Supervisor, Air & Heavy Metals Section

AIR & HEAVY METALS ANALYTICAL REQUEST FORM

' V, SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E.. ALBUQUERQUE. NM 87106

Air & Heavy Metals Section - Telephone: (505) 841 -2553

SLD No.

Date Received:

User Code #: I 7 I 0 13 I 2 I 0 I

Request ID No.:

Plan Form C Priority Code #: <3> [ K ' l ' O l T .

c«iiSO-SL3

^NameT firJJ+J. ( f ^ i Z

-iisamDie Kil I / i I / Sampie K/1 I / / / Location: I/V{I1A/I \ l\ I i

6J County:

arm J I L J L _ L J I L

jOj Collected By: QdlllML

LkJJiiiL On: 9 9 / 0 3 ! ^ At:l / l ^ l / i f l h r s .

' Data: (YY/MM/DD)

T2I Latitude (DDMMSS) XOO om - 1500 hn.

111Codes:

Submitter J I I I " I L

wss# 13J Report

TO: Roger Anderson

OrganizatTorT 14 Phone #: — 1 (505) 827-5812

New Mexico Oil Conservation Division

City, SUM Zip

Santa Fe, New Mexico 87504-2088 Data: P H : *7» > 2- • Conductivity: ^ / ^ 2^ umho« ® ^ / , | Temparatura:

17J Sample Source: ' l ^ s a S f f a T '

Longitude (DODMMSS)

i I I '» I •

2 Digit IO

•icl Sampling Information:

Sampla Purpoaa: composita ! w ? « w • - Complianca H- Row Proportioned'

^n^Chack r j - Equal Aliquot Monitoring jsjr: Sampla Split w/Permirtee

••Spacial • • Chain of Custody Chlorina

C. Residual: mg/l, Row:

17| Sample Source: i_i-Stream G-Lake C-Drain G-Pool ---WWTP

^-Well; Depth: •-Spring •-Distribution •-Point-of-Entry •-Other:

MUb~ UII ML/-11

19] Sample Type: pa Water, -Wastewater, •-Other_

• -SoU. •-Food, 20

This form accompanies a single sample consisting of: -1 liter cubitainers (1 quart) - 4 liter cubitainers (1 gallon)

Preservation: • - WMF Watar Not Praaarvad; Rltarad

Watar Not Praaarvad; Not Rltarad Watar Praaarvad with Nitric Acid (HN03); Rltarad Watar Praaarvad wtth Nitric Add; Not Rltarad Watar Not Praaarvad in Raid; Plaaaa Add HN03 at Ub Watar toad

Q W N N • - W P F • - W P N

' Q J Othar.

(704) ICAP Scan (720) SDWA Group I Only

• - (721) SDWA Group I + other parameters) marked below

• -Lead •-Manganese ]Er Mercury • - Molybdenum • - Nickel

Selenium • -Silver • - Uranium

• - Vanadium • -Zinc • -• -• -• -• -• -

Remarks:

S L D 8 9 1 2 - H M Form Naw 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPYI

AIR & HEAVY M E T A L S ANALYT ICAL R E Q U E S T FORM

' ~* SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E., ALBUQUERQUE. NM 87106

Air & Heavy Metals Section - Telephone: (505) 841 -2553

SLD No.

Date Received: _U Priority

Code#: JJUser

Code *: l 7 I 0 I 3 I 2 | 0 | 31 Request

ID No.: PtaoaFormQ SMcMrrMr*

[t "l" oi "3" can EiD-SLC Coorainaior

TJCTtyT ~ ~ iSJStat

SJJ Perl Wlt 5 Facility

Name: ML f 6 County

/ffu - i J Sample K/i \ f _ 1 r

Location: I Tli W| i J>i ° i J L_J I I I—L

10 Collected By: u;llr<

First I P i l \ J \ O n On: ' 1 0 1 1 2 ^ At:l / \ 2 - \ O \ 0 1 hrs

| L | « f i t 'Date: (YY/MM/DD) Time: ^ l 1 " : ? ^ . -100om • I9O0nn.

Tf] Latitude (DDMMSSI

I I I I I I I 2 Digit ID

Longitude (OOOMMSS)

I I I 'I

111Codes:

J . l . l I Submitter WSS# Organization

13 Report To: Roger Anderson

14] Phone #: l~ 1 (505) 827-5812

City, Slate Zip P. n. Rnv ?naa

Santa Fe_ New Mexico 87504-2088 — Data: P H : * 7 > 1 • Conductivity: 3 4> umhos ® T J '^""Temperature:

Sampla Purpoaa: • • Complianca

fc—Ttpling Information:

Grab Composite (Como

H- Check „ • Monitoring •-Special

f j - Row Proponioned v J j - Equal Aliquot .^f^&mple Split w/Permittee

G • Chain of Custody

181 Field Notee/ 1 Samala *:

Chlorine C, Residual: mg/l, Row:

17| Sample Source: •-Stream •-Lake •-Drain •-Pool n-WWTP

jS^Well; Depth: /U-Spring

J-Distribution •-Point-of-Entry •-Other

JL r Ul ML/- Is

19j Sample Type: Ijgj-Water, 2 -Wastewater, •-Other,

• -Soi. •-Food,

This form accompanies a single sampla consisting of: JK~ -1 liter cubitainers (1 quart)

20| Preservation: ' — • - W N F Watar Not Praaarvad; Rltered

Water Not Praaarvad; Not Rltered Watar Praaarvad with Nitric Acid (HN03); Rltered Watar Praaarvad wtth Nitric Add; Not Rltered Watar Not Praaarvad in Raid; Please Add HN03 at Lab Watar load

n-WNN • - W P F • - W P N

^ W N L

Othar.

- (704) ICAP Scan -(720) SDWA Group I Only

• - >J21) SDWA Group I + other parameters) marked below

• -Lead • -Manganese J2[- Mercury • - Molybdenum n - Nickel M: Selenium

"LT'• Silver • - Uranium

• - Vanadium • - Zinc • -

• -• -• -• -

Remarks:

S L D 8912-HM Form New 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPYI

""STATE OF NEW MEXICO DEPARTMENT OF HEALTH

- C , o L , : : Altaquerque, NM 87196-4700 [505]-841-2500 il l . . l ORGANIC CHEMISTRY SECTION [505]-841-2570

-May4, 1994^ 8 50

g ANALYTICAL REPORT • • SLD Accession No. OR-94-0916 £

Distribution QUser 70320 Q$ Submitter 260 (x) SLD Files

To: Roger Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088

From: Organic Chemistry Section Scientific Laboratory Div. 700 Camino de Salud, NE Albuquerque, NM 87106

On: 25-Mar-94 At: 12:00 hrs.

ANALYTICAL RESULTS: Parameter

Aromatic & Halogenated Purgeable [EPA-601/21 Screen {754} Value Note POL Units

0.00 Additional

N 10 Information

00 EPA 601/2 V o l a t i l e s (60) See Laboratory Remarks fo r

Notations & Comments: PQL = Practical Quantitation Level. A = Approximate Value; N = None Detected above Detection Limit; P = Compound Present, but not quantified; T = Trace (< Detection Limit); U = Compound Identity Not Confirmed. Evidentiary Seals: Not Sealed^; Intact: No | ~ | , Yes|~| & Broken By:

Laboratory Remarks:

Late e l u t i n g compound confirmed by GC/MS as Octanal, aldehyde.

This sample was f i r s t analyzed on 4/5/94 and the a n a l y t i c a l results were judged unacceptable by the analyst. The sample was re-analyzed on 4/6/94 y i e l d i n g the results on t h i s form.

Lab Name: NM SCIENTIFIC LABORATORY DIVISION C o n t r a c t : N/A Lab Code: N/A Case No. : N/A SAS No. : N/A SDG No.:.

Water (g/mL) mL

Matrix: ( s o i l / w a t e r ) _ Sample wt/vol: 5.0 Level: (low/med) Low % Moisture: not dec. N/A Extraction: (SepF/Cont/Sonc) GPC Cleanup: (Y/N) No pH:

dec. N/A

Lab Sample ID: SLD Batch No:

OR-94-916 127

Date Received: 3/28/94 Date Extracted: N/A Date Analyzed: 4/05/94 D i l u t i o n Factor: 10 CONCENTRATION UNITS:

(ug/L or ug/Kg) : uq/L

This sample was analyzed for the following compounds using EPA Methods 601 & 602

CAS NO. COMPOUND CONC. 0 POL 67-64-1 Acetone U 50.0 71-43-2 Benzene U 10.0 108-86-1 Bromobenzene U 10 .0 74-97-5 B romo c hioromethane U 10.0 75-27-4 Bromodichloromethane U 10.0 75-25-2 Bromoform U 10 . 0 78-93-3 2-Butanone (MEK) U 50.0 104-51-8 n-Butylbenzene U 10.0 135-98-8 sec-Butylbenzene U 10.0 98-06-6 tert-Butylbenzene U 10 . 0 1634-04-4 t e r t - B u t y l methyl ether (MTBE) U 50 . 0 56-23-5 Carbon t e t r a c h l o r i d e U 10 .0 108-90-7 Chlorobenzene U 10.0 67-66-3 Chloroform U 10.0 95-49-8 2-Chlorotoluene U 10.0 106-43-4 4-Chlorotoluene U 10.0 96-12-8 1.2-Dibromo-3-chloropropane U 10 . 0 124-48-1 Dibromochloromethane U 10 . 0 106-93-4 1,2-Dibromoethane U 10 .0 74-95-3 Dibromomethane u 10.0 95-50-1 1,2-Dichlorobenzene u 10.0 541-73-1 1,3-Dichlorobenzene u 10.0 106-46-7 1,4-Dichlorobenzene u 10.0 75-71-8 Dichlorodifluoromethane u 10.0 75-34-3 1.1-Dichloroethane u 10 . 0 107-06-2 1.2-Dichloroethane u 10 . 0 75-35-4 1.1-Dichloroethene u 10 .0 156-59-4 cis-1,2-Dichloroethene u 10.0 156-60-5 trans-1,2-Dichloroethene u 10.0 78-87-5 1,2-Dichloropropane u 10.0 142-28-9 1,3-Dichloropropane u 10.0 590-20-7 2,2-Dichloropropane u 10 . 0 563-58-6 1,1-Dichloropropene u 10.0 1006-01-5 cis-1,3-Dichloropropene u 10.0 1006-02-6 trans-1,3-Dichloropropene u 10.0 100-41-4 Ethylbenzene u 10.0 87-68-3 Hexachlorobutadiene u 10.0

98-82-8 I s opropylbenz ene U 10.0 99-87-6 4-Isopropyltoluene U 10 .0 75-09-2 Methylene c h l o r i d e U 10 . 0 90-12-0 1-Methylnaphthalene U 10.0 91-57-6 2-Methylnaphthalene U 10 . 0 91-20-3 Naphthalene U 10 . 0 103-65-1 n-Propylbenzene U 10 .0 100-42-5 Styrene U 10.0 630-20-6 1,1,1.2-Tetrachloroethane U 10.0 79-34-5 1,1,2,2-Tetrachloroethane U 10.0 127-18-4 Tetrachloroethene U 10.0 109-99-9 Tetrahydrofuran (THF) U 50.0 108-88-3 Toluene U 10.0 87-61-5 1,2,3-Trichlorobenzene U 10.0 120-82-1 1,2,4-Trichlorobenzene U 10.0 71-55-6 1,1,1-Trichloroethane U 10 . 0 79-00-5 1,1,2-Trichloroethane U 10 . 0 79-01-6 Trichloroethene U 10.0 75-69-4 Trichlorofluorornethane U 10 . 0 96-18-4 1,2,3-Trichloropropane U 10.0 95-63-6 1,2,4-Trimethylbenzene U 10.0 108-67-8 1,3,5-Trimethylbenzene U 10.0 75-01-4 V i n y l c h l o r i d e U 10 . 0 95-47-6 o-Xylene u 10 . 0 N/A p- & m-Xylene u 10.0 N/A To t a l Xylenes u 20.0

TENTATIVELY IDENTIFIED COMPOUNDS DATA SHEET

The following compounds were t e n t a t i v e l y i d e n t i f i e d by Mass Spec: CAS NO. I COMPOUND I MATCH I RT I EST. CONC. I 0 124-13-0 octanal 974 19 . 97

* Q = Q u a l i f i e r D e f i n i t i o n s : B - Indicates compound was detected i n the Lab Blank as well

as i n the sample. D - Indicates value taken from a secondary (diluted) sample analysi E - Indicates compound concentration exceeded the range of the

standard curve.

J - Indicates an estimated value for t e n t a t i v e l y i d e n t i f i e d compounds, or f o r compounds detected and i d e n t i f i e d but present at a concentration less than the quantitation l i m i t .

N - Indicates that more than one peak was used f o r quantitation. U - Indicates compound was analyzed f o r , but not detected above the

concentration l i s t e d (Quantitation L i m i t ) .

METHOD BLANK: A laboratory method blank was analyzed along with t h i s sample to assure the absence of i n t e r f e r i n g contaminants from lab reagents, instruments, or the general laboratory environment. Unless l i s t e d below, no contaminants were detected i n t h i s blank above the reported detection l i m i t .

COMPOUND DETECTED No Compounds Detected

CONCENTRATION (PPB)

SURROGATE RECOVERIES: SURROGATE

Bromofluorobenzene 2 -Bromo-1-chloropropane

CONCENTRATION 25.0 ppb 25.0 ppb

RECOVERY 97.2

SPIKE RECOVERY: The % recoveries f o r compounds i n the batch spike were from 80% to 120% with the exception of the compounds l i s t e d below: COMPOUND CONCENTRATION % RECOVERY

No exceptions . ppb

Analyst: Patrick F. Basile Analyst, Organic Chemistry

Reviewed By: Richard F. Meyerhein 05/04/94 Supervisor, Organic Chemistry Section

SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E.. ALBUQUERQUE. NM 87106

Organic Chemistry Section • Telephone: (505) 841-2570

rn JjFacHrty

-^J Sample Location:

2jUser C o d e *

31 Request ID No.:

Request ID No.

111 ii un tn 014378-C

SLD No.

Date Received _U Priority

Code# unty:

MM 0916 C

(**'-<wT.

lJ fil M •M.U-3,5 J I L ' 1 I I L ' ' ' ' ' I I L ' i ' i '

ipJCollected

Hntt IM>t«|t-On: 1 < / / Q 3 / X T At:l / t^OlOlhrs

Oata: (YY/MM/OO) " "

iJJCodes: Tim*- 2 4 * e"901

3.-00flrti . I50QWH. T2I Latitude (DOMMSS)

I A 'l I I Longitude (DDDMMSS;

I » 1 '» I I I 11

J . I . I I L _ L Submitter W S S #

13J Report To: Roger Anders.on

Organization 141 Phone #:

(505) 827-5812 New Mexico Oil Conservation Division

Diy, SUM Zip P. n. Bnv ?naa Santa Fe, New Mexico 87504-2088

• ^ D a t a : P H : *7»"7 . Conductivity. ~73£> umhoa® Tamparatura: e« i_ c> 11 al Raid NotM/

2 Digit IO

ipllng Information:

Sampla Purpoaar^ Compoaita &T££n •-Complianoa Q- Row Proportional ^

Chadt Equal Aliquot Monitoring >g. Sampla Split w/Parmittaa SpaciaJ >Q. Chain of Cuttody

| 1 8 | Plaid No»a/

, Chlorina C. Aasidual: mg/l, Flow:

171 Sample Source •-Stream •-Lake •-Drain •-Pool •-WWTP

Sf-Well; Depth: ^D-Spring

•-Distribution •-Point-of-Entry •-Other. _____

19J Sample Type: M-•-Wastewater, J \ 2 -This form accompanies a -Intfa aamplq consisting of. ____- septum vial(s) (volume » VO r+\ )

- glass jugs (volume • )

20|Prea ervatlon: '"""• Q-NP No Praaarvttion; Sampla atorad at room tamparatura

]lg~P-loa Sampla atorad in an ica bath (Not Froxan) L^P-TS Samp- Praaarvad with Sodium Thtoautfata to ramova chlorina ratidual fT-P-HCl Sampla Praaarvad with Hydrochloric Add (2 dropa/40 ml) fi-Ofter Tr OT I I

-Water, -Other.

• -Soi •-Food,

(volume J _U Analyses Requested: Please check the appropriate box(es) below to indicate the type of analytical screen(s)

required. Whenever possible, list specific compounds suspected or required.

t l • • • • • • • •

Volatile Screens: (753) Aliphatic Headspace (1-5 Carbons)

i (754) Aromatic & Halogenated Purgeables (EPA 601 & 602) ' (765) Mass Spectrometer Purgeables (EPA 624) (766) SDWA Total Trihalomethanes (EPA 501.1) (774) SDWA VOCs f [8 Regulated +] (EPA 502.2) (775) SDWA VOCs II [EDB & DBCP] (EPA 504)

Other Specific Compounds or C l a s s y

Semiv.latile Screens; • - (763) Acid Extractables ~| - (751) Aliphatic Hydrocarbons •-(755) Base/Neutral Extractables (EPA 625) • • (756) Base/Neutral/Acid Extractables (EPA 8270)

8- (758) Herbicides. CNorophenoxy Acid • (759) Herbicides, Triazines

• - (760) Organochlorine Pesticides

S- (761) Organophosphate Pesticides - (767) Polychlorinated Biphenyls (PCB's)

•-(764) Polynuclear Aromatic Hydrocarbons • - (762) SOWA Pesticides & Herbicides

Remarks:

SLD 8912-OR Form Naw i2/8» This Form Will NOT Be Returned With Your Results. Please RETAIN A COPY! I

Albuquerque, NM 87196-4700 [505]-841-2500 WATER CHEMISTRY SECTION [505]-841-2555

June 2, 1994

\ ANALYTICAL REPORT • \ SLD Accession No. WC-94-1190 \

Distribution QUser 70320 (JJ Submitter 260 (x) SLD Files

Re: A water,Nonpres/No sample submitted to this laboratory on March 28, 1994

On: 25-Mar-94 By: Ols .. . MW-3X C At: 12:00 hrs. In/Near: Sunland Park

ANALYTICAL RESULTS Analvsis Value D. Lmt. Units

calcium 139.00 mG/L magnesium 67.30 mG/L potassium 11.00 mG/L sodium 1430.00 mG/L bicarbonate 692.00 mG/L carbonate 0.00 mG/L chloride 1659.00 mG/L fl u o r i d e 1.30 mG/L sulfate 745.00 mG/L Ion Balance 102.00 % t o t a l diss resid 4424.00 mG/L

WATER CHEMISTRY ANALYTICAL REQUEST FORM

SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD, ALBUQUERQUE, NM 87106 Water Chemistry Section - Telephone: (505) 841 -2555

SLD No.

Date Received:

2 User Code*: I 7 I ° >3 I 2 l° I

Request ID No.:

P _ » F o r m O StiexrHa—

41 Priority Code#: ,3

[If "I-or T . call EIO-SLC Coordinator'

5 Facility Name:

__J3ounty: , 8 IState

j M j ! --i Sample

Location: •M.l/.-l3,J, J I l _J I I—L J I L ipJCollected

Firtt On:

TUala l t .

q y / O l l * T At-.l / l ^ l Q\Q I Oate: (YY/MM/OO) Tima: * 4 h ' e , ° "

3.-00 O— • 1500 riri.

hrs. (YY/MM/OO)

Latitude (DDMMSS)

'l I 1 11(Codes:

J . l . l I I I I I ' l Submitter WSS #

13 Report To:

Roger AAderson

I •! I. I I Organization

14) Phone #: 1—' (505) C27-5C12

Add~a :aw Mexico Oil Conservation Division

P. 0. 2088 City, SUM Zip

Santa Fe, New Mexico 87504-2088

J I Longitude (DOOMMSSJ

I I *l I I

2 Digit ID (Hr

i c | ^Sampling Information:

Sampla Purpoaa: "fj j . Compoaita E^ I • - Complianoa n - Flow Proportioned' n-Chaek ff- Equal Aliquot 63: Monitoring £T. Sampla Split w/Permittea • - S p a d a l • • Chain ot Custody

16| Field <-) —) < ~ l n / /,"<=> . . Chlorina — D a t a : P H : / • / .Conductivity: / J f , umhoa@6wV7 FT Tamparatura: C, Rasidual: mg/l, Flow: 17 Sample Source:

"~H C t r a a m Nr~I^AA/«_ll• n a n M i *

18 Plaid Notaa/ — 'Samnla * : /

, i-o ir earn Pypweii. UBLTUI. •-Lake -LPSprlng •-Drsn •-Distribution G-F •-Point-of-Entry n-W. sTP n-Other

19 Sample Type: JSrWater, • -Soil, • -Food, n -Wastewater. (~l -Other This form accompanies a single sampla consisting or.

I • 1 liter cubitainers (1 quart) • 4 liter cubitainers (1 gallon)

20| Preservation: — n-Wrtf Watar Not Praaarvad; Rltarad

§ fWNN Watar Not Praaarvad; Not RKarad • • WPF Wktar Praaarvad with Sulfuric Add (H2S04); Filtarad •-WPN Watar Praaarvad wtth Sulfuric Add; NotFlltarad •-WNL Watar Not Praaarvad in Flald;Plaaaa Add H2S04 at Ub 50-ICE Watar toad

211 Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required. Group Analysts; Q (859) SWQB SS Anion - Cation Group + • • (854) SDWA Group II (Nitrate as N) Q- (868) SWQB NPS Anion, Cation, Physical + TSS • - (861) SDWA Group III (Fluoride) Q- (869) SWQB Nutrient Analysis Group + • - (860) SDWA Comptete Secondary r E £ (867) Major Anions & Cations

Cations; • • Calcium (as Ca) • - Magnesium (as Mg) " • - Potassium (as K) [ • - Sodium (as Na) [ • - Total Hardness (as CaC03)~ Anions; • - Alkalinity (as CaC03) • - Bicarbonate (as HC03) • - Carbonate (as G03) •-Chloride (as a ) •-Fluoride (as F) •-Sulfate (as S04) ~

^ lon Charge Balance

Remarks:

Physical Parameteri; •-Color • - C O n d U C t a n C e (Mtaomho.«JSQ '

•-Odor • - p H • • Surfactants • • Total Dissolved Solids •-Turbidity Other • -• -• -• -

Surface and Waste Water: • - Biological Oxygen Demand • - Total Suspended Solids Q- Chemical Oxygen Demand • - Total Organic Carbon •-Cyanide Nutrients: • • Nitrate + Nitrite (as N) • - Ammonia (as N) •-Total Kjeldahl (as N) • - Nitrite (as N) • - Orthophosphate (as P) •-Total Phosphorus (as P)

S L D 8 9 1 2 - W C Form Naw 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPYI

"STATE OF NEW MEXICO DEPARTMENT OF HEALTH

SCIENTIFIC LABORATORY DIVISION , ^ P.O. Box 4700 700 Camino de Salud, NE

Albuquerque, NM 87196-4700 [505]-841-2500 p ,j f j r;g ORGANIC CHEMISTRY SECTION [505]-841-2570

May 23, 1994 mmmmmmmmmmmmmmmmmmmmmmmmummmmmmumummmmmm Distribution

• ANALYTICAL REPORT • ^7 TZa • • ( i j Submitter 260

ro No.St 014375 S S L D Accession No. OR-94-0917 : « SLD Fues

To: Roger Anderson From: Organic Chemistry Section NM Oil Consv. Div. Scientific Laboratory Div. State Land Office Bldg. 700 Camino de Salud, N.E. P.O. Box 2088 P.O. Box 4700 Santa Fe, NM 87504-2088 Albuquerque, NM 87196-4700

On:25-Mar-94 By: Ols . . . MW-6X-At: 11:30 hrs. In/Near: Sunland Park

ANALYTICAL RESULTS: Aromatic & Halogenated Purgeable rEPA-601/21 Screen {754} Parameter Value Note POL Units

Tetrahydrofuran 11.00 T 50 . 00 ppb Benzene 101.00 10. 00 ppb Toluene 2 .60 T 10. 00 ppb Ethylbenzene 46.00 10 . 00 ppb p- & m-Xylene 13 .00 10 . 00 ppb o-Xylene 8.90 T 10 . 00 ppb Isopropylbenzene 21.00 10 . 00 ppb

See Laboratory Remarks f o r A d d i t i o n a l I n f o r m a t i o n Notations & Comments: PQL = Practical Quantitation Level. A = Approximate Value; N = None Detected above Detection Limit; P = Compound Present, but not quantified; T = Trace (< Detection Limit); U = Compound Identity Not Confirmed. Evidentiary Seals: Not Sealed^); Intact: No |~ | , Yes|~| & Broken By: Date:

Laboratory Remarks: Foamy sample; unable to achieve a lower detection l i m i t .

Reported compound i d e n t i t i e s were confirmed by GC/MS.

Compound Note Value PQL n-Propylbenzene 52 10 1,2,4-Trimethylbenzene 270 10 Naphthlene 13 10 Methylene c h l o r i d e 29 10

Lab Name: NM SCIENTIFIC LABORATORY DIVISION Contract:_N/A Lab Code: N/A Case No. : N/A SAS No. : N/A SDG No.: N/A Matrix: (soil/water) Water Lab Sample ID: OR-94-917 Sample wt/vol: 5.0 (g/mL) mL SLD Batch No: 127 Level: (low/med) Low Date Received: 3/28/94 % Moisture: not dec. N/A dec. N/A Date Extracted: N/A Extraction: (SepF/Cont/Sonc) N/A Date Analyzed: 4/05/94 GPC Cleanup: (Y/N) No pH: D i l u t i o n Factor: 10

CONCENTRATION UNITS: (ug/L or ug/Kg) : ug/L

This sample was analyzed f o r the following compounds using EPA Methods 601 & 602

CAS NO. COMPOUND CONC. 0 POL 67-64-1 Acetone U 50 .0 71-43-2 Benzene 101 10 . 0 108-86-1 Bromobenzene U 10 . 0 74-97-5 Bromochloromethane U 10 . 0 75-27-4 Bromodichloromethane U 10.0 75-25-2 Bromoform U 10.0 78-93-3 2-Butanone (MEK) U 50 .0 104-51-8 n-Butylbenzene U 10 .0 135-98-8 sec-Butylbenzene U 10.0 98-06-6 tert-Butylbenzene U 10 .0 1634-04-4 t e r t - B u t y l methyl ether (MTBE) U 50 . 0 56-23-5 Carbon t e t r a c h l o r i d e U 10 . 0 108-90-7 Chlorobenzene U 10 .0 67-66-3 Chloroform U 10 .0 95-49-8 2-Chlorotoluene U 10 . 0 106-43-4 4-Chlorotoluene U 10.0 96-12-8 1,2-Dibromo-3-chloropropane U 10.0 124-48-1 Dibromochloromethane U 10.0 106-93-4 1,2-Dibromoethane U 10.0 74-95-3 Dibromomethane u 10.0 95-50-1 1,2-Dichlorobenzene u 10 .0 541-73-1 1,3-Dichlorobenzene u 10 .0 106-46-7 1,4-Dichlorobenzene u 10.0 75-71-8 Dichlorodifluoromethane u 10.0 75-34-3 1.1-Dichloroethane u 10 .0 107-06-2 1,2-Dichloroethane u 10 .0 75-35-4 1.1-Dichloroethene u 10.0 156-59-4 cis-1,2-Dichloroethene u 10.0

156-60-5 t r a n s - 1 , 2 - D i c h l o r o e t h e n e U 10.0 78-87-5 1,2-Dichloropropane U 10.0 142-28-9 1,3-Dichloropropane U 10 .0 590-20-7 2,2-Dichloropropane U 10 .0 563-58-6 1,1-Dichloropropene U 10.0 1006-01-5 c i s - 1 , 3 - D i c h l o r o p r o p e n e U 10.0 1006-02-6 t r a n s - 1 , 3 - D i c h l o r o p r o p e n e U 10.0 100-41-4 Ethylbenzene 46 10.0 87-68-3 He x a c h l o r o b u t a d i e n e U 10.0 98-82-8 Is o p r o p y l b e n z e n e 21 10.0 99-87-6 4 - I s o p r o p y l t o l u e n e U 10 .0 75-09-2 Methylene c h l o r i d e 29 10 .0 90-12-0 1-Methylnaphthalene U 10.0 91-57-6 2-Methylnaphthalene U 10.0 91-20-3 Naphthalene 13 10.0 103-65-1 n-Propylbenzene 52 10 .0 100-42-5 Styre n e U 10 . 0 630-20-6 1,1.1,2-Tetrachloroethane U 10.0 79-34-5 1,1,2,2-Tetrachloroethane U 10 .0 127-18-4 T e t r a c h l o r o e t h e n e U 10 .0 109-99-9 T e t r a h y d r o f u r a n (THF) 11 J 50.0 108-88-3 Toluene 2.6 J 10.0 87-61-5 1,2,3-Trichlorobenzene U 10.0 120-82-1 1.2.4-Trichlorobenzene U 10.0 71-55-6 1 . 1 . 1 - T r i c h l o r o e t h a n e U 10.0 79-00-5 1 , 1 , 2 - T r i c h l o r o e t h a n e U 10.0 79-01-6 T r i c h l o r o e t h e n e U 10.0 75-69-4 T r i c h l o r o f l u o r o r n e t h a n e U 10 . 0 96-18-4 1 , 2 , 3 - T r i c h l o r o p r o p a n e U 10.0 95-63-6 1.2.4-Trimethylbenzene 270 10.0 108-67-8 1,3,5-Trimethylbenzene U 10.0 75-01-4 V i n y l c h l o r i d e U 10.0 95-47-6 o-Xylene 8.9 J 10.0 N/A p- Sc. m-Xylene 13 10.0 N/A T o t a l Xylenes 21.9 20 . 0

The f o l l o w i n g compounds were t e n t a t i v e l y i d e n t i f i e d by Mass Spec: CAS NO. COMPOUND MATCH RT EST. CONC. 0

637-50-3 1-propenylbenzene 953 20 . 65 200

933-98-2 1 - e t h y l - 2 , 3 - d i m e t h y l benzene 974 21.35 100

7525-62-4 1-ethenyl-3 - e t h y l -benzene 900 21.60 100

874-41-9 1 - e t h y l - 2 , 4 - d i m e t h y l benzene 834 21.17 100

611-14-3 1 - e t h y l - 2 - m e t h y l -benzene 973 19 .29 90

488-23-3 1 , 2 , 3 , 4 - t e t r a m e t h y l -benzene 968 22 .12 90

824-63-5 2 , 3- d i h y d r o - 2 - m e t h y l -l h - i n d e n e 970 22 .62 50

* CONC = CONCENTRAION DETERMINED PQL = P r a c t i c a l Q u a n t i t a t i o n L i m i t (Approximately 10 times MDL)

* Q = Q u a l i f i e r D e f i n i t i o n s : B - I n d i c a t e s compound was detected i n the Lab Blank as w e l l

as i n the sample. D - I n d i c a t e s value taken from a secondary ( d i l u t e d ) sample a n a l y s i s . E - I n d i c a t e s compound concentration exceeded the range of the

standard curve. J - I n d i c a t e s an estimated value f o r t e n t a t i v e l y i d e n t i f i e d compounds,

or f o r compounds detected and i d e n t i f i e d but present a t a conce n t r a t i o n less than the q u a n t i t a t i o n l i m i t .

N - I n d i c a t e s t h a t more than one peak was used f o r q u a n t i t a t i o n . U - I n d i c a t e s compound was analyzed f o r , but not detected above the

conc e n t r a t i o n l i s t e d ( Q u a n t i t a t i o n L i m i t ) .

METHOD BLANK: A l a b o r a t o r y method blank was analyzed along w i t h t h i s sample t o assure the absence of i n t e r f e r i n g contaminants from l a b reagents, instruments, or the general l a b o r a t o r y environment. Unless l i s t e d below, no contaminants were detected i n t h i s blank above the reported d e t e c t i o n l i m i t .

COMPOUND DETECTED CONCENTRATION (PPB) No Compounds Detected

SURROGATE RECOVERIES: SURROGATE CONCENTRATION % RECOVERY

Bromofluorobenzene 25.0 ppb 90.0 2-Bromo-l-chloropropane 25.0 ppb 92.0

No exceptions . ppb

Reviewed By: _ RicharcTF. Meyerhein 05/04/94 Supervisor, Organic Chemistry Section

SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E., ALBUQUERQUE, NM 87106

Organic Chemistry Section - Telephone: (505) 841 -2570 JJUser

Code#: I 7 I tt i 3 j 2 i 0 |

^Name? S f i M c J

31 Request ID No.:

Request 11111 UU Ui ID No. 014375-C

SLD No.

Date Received Jj Priority 7"

Code #: \£j

0R94 0917 C

caaeO-SLD

-^J Sample Location: ( -AS I I I I L J I I L J I I I I L J I

lOjCollected By:

Brat ILIitUt On: 9±M21I2^Z At: 1 j) l\J\Q\hrs

Dm: (YY/MM/OO) ~ jjJCodes:

Submitter

Tima- 2* <*• oae* 3.-00 cm • '300 ~v

JJ] Latitude (D0MM,ss)

. 1 uL 'i ' 1 ' 1

Longitude (DOOMMSS)

I > I 'I I 1

1 I I L 13j RePOrt Ntrcm

To: Roger Anders.on

'wssV 1_J L Organization

141 Phone #: ^ (505) 827-5812

Addrea New Mexico Oil Conservation Division

City, SUM Zip p. o_ Bnv ?nafl Santa Fe, New Mexico 87504-2088

2 Digit ID l» itt eta)

j 5 j .Sampling Information:

Sampla Purpoaa: •fcompo«it« £"« • • Complianoa n- Row Proportionad

• Sim!

lOOtlt*

Monitoring t?£ Special /XJ.

pit Split w/Parmittaa Chain of Custody

• ^ D a t a : P H : ( > J $ • Conductivity. umho>®^6.(o Tamparatura:

17J Sample Source •-Stream •-Lake •-Drain •-Pod •-WWTP

101 Flald Nota*/ 1 — 1 Sampta »

Chlorina C, flaaidual: mg/l, Row:

19J Sample Type: ^-Water. • -Wastewater, Q -Other.

^-Well; Depth: . TJ-Spring ••Distribution •-Point-of-Entry •-Other

201 Preservation: Q N P MB Pnaaarvatton; Sampta atorad at room tamparatura

££P4oa Sampla aion»d In an lea bath (Not Bonn)

SP-TS Sampla Praaarvad with Sodium TMoautfata to ramova chlorina rasidual P+O Sampla Praaarvad with Hydrochloric Acid (2 dropt/40 ml)

&09m fyU?

• - S o i D-Food.

This form accompanies a single sample consisting of : septumvial(s) (volume - yo mj ) glass jugs (volume -

(volume ) 2iJ Analyses Requested: Please check the appropriate box(es) below to indicate the type of analytical screen(s)

Volatile Screens:

(753) Aliphatic Headspace (1 -5 Carbons) (754) Aromatic & Halogenated Purgeables (EPA 601 & 602) (765) Mass Spectrometer Purgeables (EPA 624) (766) SDWA Totai Trihalomethanes (EPA 501.1) (774) SDWA VOC's f (8 Regulated +] (EPA 502.2) (775) SDWA VOCs li {EDB & DBCP) (EPA 504)

Other Specific Compounds or Classes; ( ) .

Semivolatile Screens; • - (763) Acid Extractables • - (751) Aliphatic Hydrocarbons • • (755) Base/Neutral Extractables (EPA 625) • - (756) Base/Neutral/Acid Extractables (EPA 8270)

8 - (758) Herbicides. Chlorophenoxy Acid - (759) Herbicides, Triazines

8- (761) Organophosphate Pesticides - (767) Polychlorinated Biphenyls (PCB's)

• - (764) Polynuclear Aromatic Hydrocarbons • - (762) SDWA Pesticides & Herbicides

Remarks:

SLD 8912~OR Form Naw 12/S» This Form Will NOT Be Returned With Your Results. Please RETAIN A COPY!

i£TATE OF NEW MEXICO DEPARTMENT OF HEALTH SCIENTIFIC LABORATORY DIVISION

P.O. Box 4700 700 Camino de Salud, NE Albuquerque, NM 87196-4700 [505]-841-2500

WATER CHEMISTRY SECTION [505]-841-2555

May 26, 1994

ANALYTICAL REPORT ior No. WC-94-1189 g SLD Acc;

Distribution QUser 70320 (2£ Submitter 260 (x) SLD Files

R. Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088

A water,Nonpres/No sample submitted to this laboratory on March 28, 1994

DEMOGWK1C DATA COLLECTION LOCATION

On: 25-Mar-94 At: 11:30 hrs.

ANALYTICAL RESULTS Analvsis

calcium magnesium potassium sodium bicarbonate carbonate chloride f l u o r i d e sulfate Ion Balance t o t a l diss resid

Vy-Ioe 147.00 108 .00

16 .00 1575.00 1772.00

0 .00 1796.00

1.00 107.00 104.00

S200 .00

D. Lmt. Units mG/L mG/L mG/L mG/L mG/L mG/L mG/L mG/L mG/L

% mG/L

W A J E R C H E M I S T R Y ANALYT ICAL R E Q U E S T FORM

j SCIENTIRC LABORATORY DIVISION 700 CAMINO DE SALUD, ALBUQUERQUE. NM 87106 Water Chemistry Section - Telephone: (505) 841 -2555

SLD No.

Date Received

2jUser C o d e * : ' 7 ' ° *2 I2 l° I

31 Request ID No.:

P t a o f e n n O SdoawHam

_U Priority Code#: 3,

[ T V o r V . call EIO-SU Coortinalo»|

U Facility Name:

Sample Location: I I I I L J I

lOj Collected By:

First On:

IM«l«|t. 9( / /C3/ + r At:l/ | / | 3 | Q l h r s , 0>i«: (YY/MM/OO) ~ Tim*' 24 m. ciocn

3.00 twn - IS0OW1. 111Codes:

•I J , I l3jReport

Submitter I I 1 l - l I I I L

Roger AAderson "?4[ Phone #:

1— 1 (505) C27-5C12

' I I Organization

New Mexico Oil Conservation Division P. 0. 2088

City, Slaw Zip Santa Fe, New Mexico 87504-2088

16|P'eld-Data:

TJ] Latitude IODMMSS)

Longitude (OOOMMSS)

• I I 'l I I I H

2 Digit IO (Si

Sampling Information:

Sampl* Purpo**: ' Q ? Composit* P^ESS, • - Complianc* n- Flow Proportioned'"* n- Cnadc Q- Equal Aliquot

JSg Monitoring Jg\. Sampla Split w/Permittee ^••Spaciai • • Chain ot Custody

pH: b r f f i . Conductivity: j ? f ) Q umhoa@(^.^ Tamparatura:

171 Sample Source: 18| Plaid Not**/ Sampla »

, Chlorina C, Residual: mg/l, Row:

•-Stream U-Lake •-Drain •-Pool --WWTP

J9] Sample Type: J3-Water~ • -Wastewater, • -Other.

frf-Well; Depth: /LT-Spring •-Distribution •-Point-of-Entry •-Other

Q-Soit, • -Food , 201 Preservation: 1 " W N F Watar Not Pr***rv*d; Rltarad

Watar Not Praaarvad; Not Firtarad Watar Praaarvad with Sulfuric Acid (H2S04); Filtarad Watar Praaarvad wtth Sulfuric Add; Not Firtarad Watar Not Praaarvad in Raid; Ptaaaa Add H2S04 at Ub Watar lead

This form accompanies a ainoja sampla consisting of: j -1 liter cubitainers (1 quart)

FWNN ••WPP •-WPN •-WNL

Othar.

2JJ Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required. Group ArtalYitsi Q . (559) SWQB SS Anion - Cation Group +

• - (854) SDWA Group 11 (Nitrate as N) Q (868) SWQB NPS Anion. Cation, Physical + TSS • - (861) SDWA Group III (Fluoride) Q- (869) SWQB Nutrient Analysis Group + • - (860) SDWA Complete Secondary J&£ (867) Major Anions & Cations

Cations: • - Calcium (as Ca) • - Magnesium (as Mg) n - Potassium (as K) •-Sodium (as Na) • • Total Hardness (as CaC03)[ Anions; •-Alkalinity (as CaC03) • - Bicarbonate (as HC03) • - Carbonate (as C03) • - Chloride (as Cf) •-Fluoride (as F) •-Sulfate (as S04)

Physical Parameters: • -Color • * Conductance (M«O«T*O«®29C> • -Odor • - P H • • Surfactants O - Total Dissolved Solids •-Turbidity Other • -• -• -• -

Surface end Waste Water: • - Biological Oxygen Demand ••Total Suspended Solids • - Chemical Oxygen Demand • - Total Organic Carbon •-Cyanide Nutrients; • - Nitrate + Nitrite (as N) • - Ammonia (as N) •-Total KJeldahl (as N) Q-Nitrite (as N) • - Orthophosphate (as P) • - Total Phosphorus (as P)

lon Charge Balance

Remarks:

SLD8912-WC FormNawt2/ao This Form W3I NOT Be Returned With Your Results. Please RETAIN A COPY!

* SCIENTIFIC LABORATORY DIVISION P.O. Box 4700 700 Camino de Salud, NE

Albuquerque, NM 87196-4700 [505]-841-2500 AIR & HEAVY METALS SECTION [505]-841-2553

May 11, 1994

ANALYTICAL REPORT g SLD Accession No. IC-94-0047 g

Distribution (JUser 70320

Submitter 260 (x> SLD Files

From: Air & Heavy Metals Section Scientific Laboratory Div. 700 Camino de Salud, NE Albuquerque, NM 87106

A water,Nonpres/No sample submitted to this laboratory on March 28,1994

User: NM Energy & Min - Oil Conserv. , NM

On.-25-Mar-94 By: Ols . . . M W - ^ < At: 11:30 hrs. In/Near: Sunland Park

ANALYTICAL RESULTS in mG/L Analvsis Value Analysis Value Analvsis Value

Aluminum 4 .40 Copper < 0 .10 S i l v e r < 0 .10 B a r i u m 1.40 I r o n 12 .00 S t r o n t i u m 4 .90 B e r y l l i u m < 0 .10 Lead < 0 .10 T i n < 0 .10 Boron 1.20 Magnesium 100.00 Vanadium < 0 .10 Cadmium < 0 .10 Manganese 1.30 Z i n c < 0 .10 C a l c i u m 270 .00 Molybdenum < 0 .10 M e r c u r y < 0 .0005 Chromium < 0 .10 N i c k e l < 0 .10 S e l e n i u m < 0 .0050 C o b a l t < 0 .05 S i l i c o n 0.20

Laboratory Remarks: ICP by method 270.2 on 4/29/94 by RAH. Mercury by method 245.1 on 4/13/94 by SD. Selenium by method 270.2 on 4/8/94 by RAH.

Reviewed By: Jim F. Ashbyy// 05/11/94 Supervisor, Air tk Heavy Metals Section

AIR & HEAVY METALS ANALYTICAL REQUEST FORM SCIENTIFIC LABORATORY DIVISION

700 CAMINO DE SALUD N.E., ALBUQUERQUE. NM 87106 Air & Heavy Metals Section - Telephone: (505) 841-2553

SLD No.

Date Received:

JJUser Code #:

U Facility Name:

I 7 I 0 I 3 I 2 I 0 I 31 Request

ID No.: Plot* FormO

6J County:

i f Priority -> U O d S # • I s j I Coordin*o«|

(Ifl" 0»T , C*II EID-SLD

[TJCTty 8 JStatei

3J Location: I I I

jtpjCollected i A j .

Rrat /lJ\<S>H On: At:| / \ / \ 3 IO I hrs

|Lla|alt Ofc»: (YY/MM/DO) Time; *«J»: <??£!_ 100cm • '800hn.

11 [Codes:'

•4 I, I I L ubmitter

I I - I I I I—L WSS»

nization Report To: Roger Anderson

14) Phone #: U J (505) 827-5812

City, SUM Zip P . n. BOV ?na«

Santa Fe, New Maxico 87504-2088

12 Latitude (DDMMSS) e '

, • ul 1 1 1 1 1

Longitude (DODMMSS)

I t 1 I I . I N

2 Digit IO

iH4 PajfioO^

1 c j dimpling Information:

Sampla Purpoaa:' [^Composite pompo*. • - Complianoa n - Plow Proportioned H- Check n - Equal Aliquot

Jj2*"Monitoring ^fif- Sampla Split w/Permittee 1j>Specia] Q . Chain of Custody

16) Field Data: P H : C - • Conductivity: Q umhos ® L\ * £ " Tamparatura:

e . m n i . c« . . r«» . 1181 Raid Notsa/ l8|PiaidNotaa/ — Sample »:

Chlorine C, Residual: mg/l, Row:

17| Sample Source: ~-Stream •-Lake •-Drain •-Pool r-i-WWTP

^-Well; Depth: . U-Spring •-Distribution • -Point-of-Entry •-Other:

20| Preservation: 1 — • • W N F Watar Not Praaarvad; Rltarad

Watar Not Praaarvad; Not Rltarad Watar Praaarvad with Nitric Acid (HN03); Rltarad Watar Praaarvad wftf) Nitric Add; Not Rltarad Watar Not Praaarvad in Raid; Please Add HN03 at Lab Watar load

tsj Sample Type: ^-Water, • -Wastewater, • -Other,

•-Sofl. •-Food,

This form accompanies a aingia sample consisting of: \ -1 liter cubitainers (1 quart)

-Q-WNN -g-wpf

JWPN WML ICE

Lj-Othar. 21 j Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required.

ft (704) ICAP Scan (720) SDWA Group I Only

• - (721) SDWA Group I + other parameter (s) marked below

• -Lead Q - Manganese

Mercury • -Molybdenum Q- Nickel M.- Selenium • -Silver • - Uranium

• - Vanadium • -Zinc • -• -• -• -

• •ZZZZZ • -

Remarks:

S L D 8912-HM Form New 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPYI

, >; r -

CL' in u i JU

STATE OF NEW MEXICO DEPARTMENT OF HEALTH SCIENTIFIC LABORATORY DIVISION

,- n u ' J f*.<0. Box 4700 700 Camino de Salud, NE Albuquerque, NM 87196-4700 [505]-841-2500

f ' f l 8 5 0 ORGANIC CHEMISTRY SECTION [505]-841-2570

May 23, 1994 M^^m^mmamL^umam—mmmm^ Distribution

• ANALYTICAL REPORT • ^^ e r I° 3 2L • • ( i j Submitter 260

ID No. 014372 B S L D Accession No. OR-94-0918 : (x> SLOPES

To: Roger Anderson From: Organic Chemistry Section NM Oil Consv. Div. Scientific Laboratory Div. State Land Office Bldg. 700 Camino de Salud, N.E. P.O. Box 2088 P.O. Box 4700 Santa Fe, NM 87504-2088 Albuquerque, NM 87196-4700

0«.-25-Mar-94 By: Ols . . . MW-9X 5 At: 10:40 hrs. In/Near: Sunland Park

ANALYTICAL RESULTS: Aromatic & Halogenated Purgeable [EPA-601/21 Screen (754) Parameter Value Note POL Units

EPA 601/2 V o l a t i l e s (60) 0.00 N 1.00 ppb See Laboratory Remarks fo r Additional Information

Notations & Comments: PQL = Practical Quantitation Level. A = Approximate Value; N = None Detected above Detection Limit; P = Compound Present, but not quantified; T = Trace (< Detection Limit); U = Compound Identity Not Confirmed. Evidentiary Seals: Not Sealed pj£|; Intact: No |~ | , Yes |~ | & Broken By: Date:

Laboratory Remarks: No target compounds observed, however C8, C9, C10, aldehydes observed on GC/MS, but not quantified.

Reported compound i d e n t i t i e s were confirmed by GC/MS.

Lab Name: NM SCIENTIFIC LABORATORY DIVISION Contract: N/A Lab Code: N/A Case No. : N/A SAS No. : N/A SDG No.: N/A Matrix: (soil/water) Water Lab Sample ID: OR-94-918 Sample wt/vol: 5.0 (q/mL) mL SLD Batch No: 127 Level: (low/med)_Low Date Received: 3/28/94

Moisture: not dec. N/A dec. N/A Date Extracted: N/A Extraction: (SepF/Cont/Sonc) N/A Date Analyzed: 4/05/94 GPC Cleanup: (Y/N) No pH: D i l u t i o n Factor: 1

CONCENTRATION UNITS: (ug/L or ug/Kg) : ug/L

This sample was analyzed for the following compounds using EPA Methods 601 & 602

CAS NO. COMPOUND CONC. 0 POL 67-64-1 Acetone U 5.0 71-43-2 Benzene U 1.0 108-86-1 Bromobenzene U 1.0 74-97-5 Bromochloromethane U 1.0 75-27-4 Bromodichloromethane U 1.0 75-25-2 Bromoform U 1.0 78-93-3 2-Butanone (MEK) U 5.0 104-51-8 n-Butylbenzene U 1.0 135-98-8 sec-Butylbenz ene U 1.0 98-06-6 tert-Butylbenzene U 1.0 1634-04-4 t e r t - B u t y l methyl ether (MTBE) U 5 . 0 56-23-5 Carbon t e t r a c h l o r i d e U 1. 0 108-90-7 Chlorobenzene U 1.0 67-66-3 Chloroform U 1.0 95-49-8 2-Chlorotoluene U 1.0 106-43-4 4-Chlorotoluene •TJ 1.0 96-12-8 1.2-Dibromo-3-chloropropane U 1. 0 124-48-1 Dibromochloromethane U 1.0 106-93-4 1,2-Dibromoethane U 1.0 74-95-3 Dibromomethane U 1.0 95-50-1 1.2-Dichlorobenzene U 1.0 541-73-1 1.3-Dichlorobenzene U 1.0 106-46-7 1,4-Dichlorobenzene u 1.0 75-71-8 Dichlorodifluoromethane u 1.0 75-34-3 1.1-Dichloroethane u 1. 0 107-06-2 1,2-Dichloroethane u 1. 0 75-35-4 1.1-Dichloroethene u 1.0 156-59-4 cis-1,2-Dichloroethene u 1. 0 156-60-5 trans-1.2-Dichloroethene u 1.0 78-87-5 1, 2-Dichloropropane u 1. 0 142-28-9 1.3-Dichloropropane u 1. 0 590-20-7 2.2-Dichloropropane u 1.0 563-58-6 1.1-Dichloropropene u 1.0 1006-01-5 cis-1,3-Dichloropropene u 1.0 1006-02-6 trans-1,3-Dichloropropene u 1.0 100-41-4 Ethylbenzene u 1.0 87-68-3 Hexachlorobutadiene u 1.0 98-82-8 Isopropylbenzene u 1. 0 99-87-6 4-lsopropyltoluene u 1. 0

75-09-2 Methylene c h l o r i d e U 1 .0 90-12-0 1-Methylnaphthalene U 1 .0 91-57-6 2-Methylnaphthalene U 1 .0 91-20-3 Naphthalene U 1 .0 103-65-1 n-Propylbenzene U 1 .0 100-42-5 Styren e U 1 .0 630-20-6 1,1.1, 2 - T e t r a c h l o r o e t h a n e U 1 .0 79-34-5 1,1,2, 2 - T e t r a c h l o r o e t h a n e U 1 .0 127-18-4 T e t r a c h l o r o e t h e n e U 1 .0 109-99-9 T e t r a h y d r o f u r a n (THF) U 5 .0 108-88-3 Toluene U 1 .0 87-61-5 1,2,3-Trichlorobenzene U 1 .0 120-82-1 1,2,4-Trichlorobenzene U 1 .0 71-55-6 1 , 1 , 1 - T r i c h l o r o e t h a n e U 1 .0 79-00-5 1 , 1 , 2 - T r i c h l o r o e t h a n e U 1 .0 79-01-6 T r i c h l o r o e t h e n e U 1 .0 75-69-4 T r i c h l o r o f l u o r o r n e t h a n e U 1 .0 96-18-4 1, 2 , 3 - T r i c h l o r o p r o p a n e U 1 .0 95-63-6 1,2,4-Trimethylbenzene U 1 . 0 108-67-8 1,3,5-Trimethylbenzene U 1 .0 75-01-4 V i n y l c h l o r i d e U 1 . 0 95-47-6 o-Xylene U 1 .0 N/A p- & m-Xylene U 1 .0

CAS NO. COMPOUND MATCH RT EST. CONC. 0 124-19-6 nonanal 967 21.97 5 112-31-2 decanal 978 23 .84 2 124-13-0 o c t a n a l 984 20. 2

6032-29-7 2-pentanol 839 7.01 2

* Q = Q u a l i f i e r D e f i n i t i o n s : B - Indicates compound was detected i n the Lab Blank as well

as i n the sample. D - Indicates value taken from a secondary (diluted) sample analysis. E - Indicates compound concentration exceeded the range of the

standard curve. J - Indicates an estimated value f o r t e n t a t i v e l y i d e n t i f i e d compounds,

or f o r compounds detected and i d e n t i f i e d but present at a concentration less than the quantitation l i m i t .

N - Indicates that more than one peak was used f o r quantitation. U - Indicates compound was analyzed f o r , but not detected above the

concentration l i s t e d (Quantitation L i m i t ) .

METHOD BLANK: A laboratory method blank was analyzed along with t h i s sample to assure the absence of i n t e r f e r i n g contaminants from lab reagents, instruments, or the general laboratory environment. Unless l i s t e d below, no contaminants were detected i n t h i s blank above the reported detection l i m i t .

COMPOUND DETECTED CONCENTRATION (PPB) No Compounds Detected

SURROGATE RECOVERIES: SURROGATE CONCENTRATION % RECOVERY

Bromofluorobenzene 25.0 ppb 98.0 2-Bromo-l-chloropropane 25.0 ppb 101.0

No exceptions . ppb

Analyst:

Analyst, Organic Chemistry Supervisor, Organic Chemistry Section

SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E., ALBUQUERQUE, NM 87106

Organic Chemistry Section - Telephone: (505) 841-2570 2lUser

Code*: I 7 i 0. j 3 j 2 | 0 | 31 Request

^"TDNo.

Request ID No.

SLD No.

Date Received:

014372-C Priority Code #:

r**'"<x"r. eauElO-SLO

mo* 8|State

m ^Name? S r i J l L j fief.

Location: ftl.W-.9-s J I L J—J I I I I I I I L JL—J I—l lOjCollected

By: Rftt

Mil JJslltSlL

on On: 9< / /d3 / *S~ At: I ) \ Ol V lO l hrs. Data: (YY/MM/DO) Tima- 34 •"• °oc*

a.-oeem - isoomi. Latitude (OOMMSS)

Longitude (ODOMMSS)

I I I 'I 1 1

iiJCodes:

1 J , I. I I Submitter

13| Report To: Roger Anders.on

wss» J I L I l

Organization 14J Phone #:

(505) 827-5812 New Mexico Oil Conservation Division

City. S U M Zip P. 0. rVTX ?0RR Santa Fe, New Mexioo 87504-2088

^ D a t a : P H : 1 \ 1 , Conductivity: umhoa ® 6^ Tamparatura:

Sample Source: v i miFiaid Nota./

12 2 Digit IO

(RnaMad)

15] \Sampling Information

Sampla P u r p o a a : ^ Compoaita •-Complianoa ~ • Row Proportion*

• Chack . R . Equal Aliquot - Sampla Split w/Parmittaa

[ComooK* •m« Ptnorf)

Monitoring Spatial Chain ot Custoqy

1 8in.ldho»a/ r~-*simo|a»;

Chlorina C, Raaidual: mg/l. Row:

17] Sample Source: •-Stream G-Lake •-Drain •-Pod •-WWTP

]§<Well; Depth: •^Spring

•-Distribution •-Point-of-Entry •-Other

20| Preservation: "" NP No Praaarvatlon; Sampla atorad at room tamparatura

P-tea Sampla atorad In an tea bath (Not Froxan) _ P-TS Sampla Praaarvad with Sodium Thtoaultata to ram ova chlorina raaidual • - P-HQ SampMi Praaarvad with Hydrochloric Acid (2 dropa/40 ml) BTOthar CP I I

191 Sample Type: J^-Water. • - Wastewater, • -Other.

O-Sol, ••Food,

This form accompanies a aingjai sampla consisting of: X • septum vial(s) (volume • HO M I )

- glass jugs (volume - )

(volume J 2ij Analyses Requested: Please check the appropriate box(es) below to indicate the type of analytical screen(s)

Volatile Screens:

(753) Aliphatic Headspace (1 -5 Carbons) '(754) Aromatic & Halogenated Purgeables (EPA 601 & 602) • (765) Mass Spectrometer Purgeables (EPA 624) (766) SDWA Total Trihatomethanes (EPA 501.1) (774) SDWA VOCs I [8 Regulated + ] (EPA 502.2) (775) SDWA VOCs II (EDB & DBCP] (EPA 504)

Other Specific Compounds or Classes:

Semivolatile Screens; • - (763) Acid Extractables • - (751) Aliphatic Hydrocarbons • - (755) Base/Neutral Extractables (EPA 625) • - (756) Base/Neutral/Acid Extractables (EPA 8270)

a - (758) Herbicides, Chlorophenoxy Acid - (759) Herbicides, Triazines

B - (761) Organophosphate Pesticides • (767) Polychlorinated Biphenyls (PCB's)

• * (764) Polynuclear Aromatic Hydrocarbons • - (762) SDWA Pesticides & Herbicides

Remarks:

SLD8912-OR Form Naw 12/88 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPY)

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