JONES EIYVIRONMENTAL
Client: Intcri'liase Eiiviroiirnenldl, Inc. Report Date: 09/09/05 Client Address: 6200 I'eacl~tree Sti-ect J E L Rcf. No.: A-5428
Los Aiigeles, CA 90040 Client Ref: No.: 05253
Attn: Paola Caldeion Date Sanlpled: 09/09/05 Date Received: 09/09/05
Project: Delp111 (32486-000) Date Ailaly7ed: 09/09/05 Project Address: 1201 N Magnolia, Anahc~m, CA Physical Slate: Soil Gau
1. EPA 82608- Volatile 01-gaoics by CCIMS + Oxygei~ates
Sampling - Soil Gas samples are collcctcd in glass gas-tight syringes eq~~ipped with Tefloii plungers. Tubing placed in the groiiiid for soil gas sampiii~g is purged three different times as recommended by DTSCIRWQCB regulations. This purge test dcternli~ies lrow inany purges of the soil gas tubing are needed tliroughout the project. One, tiwee and seven pusge voluilics were analyzed to inake this detei-minalioii.
A tracer gas. 11-1'1-opanol, is placed at thc tubing-surface interrace before sainpling. This compound is analyzed during the 8260U aiialyticai ruii to determine ifthere are surFdcc leaks into the suhsurFdce due to impsopel. installation of the probe. No 11-Propanol was found in any of the saliiples repovted lierein.
'The sampliiig sate was 200 cc/min using a battery operated sampling puiiip equipped with a rotainctcr. The saiiipli~~g pump was calibrated at tiic beginning ofthc day using a certilied flow inelcr. 1 purge voluincs were used since this purging levcl gnvc tlie liigl?csl res~ilts.
Aiialytical - Soil Gas sa~iiplcs were analyzed using CPA Method 8260 that includes extra coinpounds required by L>TSC/IWQCB (such as Frcoii 1 13). Instrul~ient Coiiti~iuillg Caiibratio~~ Verification; QC Reference Standards, instrumei~t Dlaiiks and Ambient Air Blaiiks are aiialyzed every 12 hours as prescribed by the ii~ethod. in addition, Matrix Spike (MS) and Matrix Spike Duplicates (MSD) are analyzed witli each batch of Soil Gas samples. A duplicate sainplc is analyzcd each day of the sanipling activily.
Approval: V
Stcvc Jones, PI1 D Ldholatolp Manager
Client: Intc~Phase i'~?viron~i?ental, Inc Report Date: 09/09/05 Clietlt Addrccc: 6200 Peacht~ec Sticet .)EL Ref. Yo.: A-5428
Lo? Aiigclcs, CA 90040 Clieut Ref. No.: 05253
Attn: Paola Cdideion Date Sampled: 09/09/05 Date Received: 09/09/05
Project: Dclphi (32486-000) Date Analyred: 09/09/05 Project A d d r e w 1201 Y Magnoha, A~idheim, CA Physical State: Soil Gds
E P h 82600- Volatile Organics by GCIMS + Ovygenates
Sample 11):
Analytes: Rciiici~c Bi-oii~obrnzeiie 13romoclilorornct!li111~ Broiiiodiciiloioiiietl~i~i~e I3roiiiohnn i3romomethane 13-liotylbci~rcne sec-Biiiylbc~~iene tert-Biitylbenzcne Carbon tetrachIoridc Chloiobenzenc Ciiloi-ocdianc CIilornSorni ~hli~roiiieiliaiie 2-ChIomt<iiueiic -1-ChlosotoIiiei?c l?ibroii1ocliloro1l?e1i~d~1e
1.2-Dibromo-3-chloropropane I ,2-DiliromoclI1ailc (IiDB) L~ibromomellienc l,2- D~ci,iorobcnrriie I .3-ilic!iloi-obc1,reile !,4-llichlorobciirclir i?icl~loiodiiluoso~~~cthane I,l-Diciiloiocthaiie 1.2-L>icliIorocihai?c 1 ; I -13ichloi-oetlienc
DP0133- Practical SG-005 Ouantitation
NU = No1 Dctccted
2
JONES ENVIRON'MENTAZ,
LABORATORY RESULTS
Client: InterPlidse Eii\~is onmental, inc Report Date: 09/09/05 Client Address: 6200 Peaclitice Street JEL Ref. KO.: A-5428
Loi Ailgelc\, CA iiU040 Client Iict. No.: 05253
Alln: Pdola Cdldcion Date Sampled: 09/09/05 Date Received: 09/09/05
I'toject: Dclphi (32486.000) Date Analyred: 09/09/05 Project Address: 1201 N Magnolia, Anahesm, CA Physical State: So11 Gds
EPA 8260B- Volatile Organic? by GClhlS + Oxygenate?
DP0131- DP013I- D1'0 130- DP0130- DP0133- Ssrnoie ID: SG-005 SG.015 SG..005 SG-015 SG 005 Ouantitation (:nits -
i,lmits
ND - Not Detectcd
XD ND ND ND NU 5.51 ND NU ND ND NU NU ND 0.16 ND ND ND E D ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NL) 0.88 ND 0.17 NI) ND NU NU N D 25.4 ND \ID N D I'D
JONES ENVIRONMENTAL
Client: lilteil'ha~c En\~iioi~mental, l i ~ c Report Date: 09/09/05 Client Address: 6200 Peachtree Sliect JEL Ref. Yo.: A-5428
Los Angcles, CA 90040 Client Ref. KO.: 05253
Atln: Pnold Caideroii Date Sarnpled: 09/09/05 Date Received: 09/09/05
Project: Delphi (32486-000) Date Analy~cd: 09/09/05 Project Address: 1201 Y Magnol~a, Andllcim, CA Physical State: Soil Gal
EPA 8260B- Volatile Orgarlics by GCIMS + Oxygenates
Analytes: 'Siichioiollitoion?etlianc 1,2~3-Trichioropiop;iiie I , ~ ~ ~ - T ~ ~ I I ~ c ~ I I ~ I ~ c I I ~ , ~ I I ~ I ,3.5-Trinictl?ylhemeiie Vinyl cliloiidc Xylenes MTBE Etliyl-tert-biilylsth ili-isiipropylztl~ei- ici-i-aniyli~icthylcilier run-Huiyl;ilci~Iid
JONES EYVIRONMENTAI,
Client Address: 6200 i'eaclitree Stleet JEL Ref. No.: A-5428 Los Angcies, CA 90040 Clienl Ref. Ro.: 05253
Attn: Pmla Cdldcro~i Date Satnpled: 09/09/05 Date Received: 09/09/05
I'rojcct: Delphi (12486.000) Date Analyzed: 09/09/05 Project Address: 1201 N Mdgnolla, Aiiaiic~m, CA Pbysical State: Sorl Gab
IEPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0133.. Sample ID: SG-015
Analytes: Benzeiie ND Bi-oinobcnzei~e ND Li i -omocl~loro~~!ei l i i~~~e ND Kroii~odichloroiiicilii~i~c ND Hromoibim ND iii-omoinetli;mc ND n-B~iiylbeiizciie ND sec-tiiitylbcnzei~c N I1 wit-Riiiylhciizeiic ND ('arbon icii-:ichIoridc ND i:iiloi-obcilzc~ic NII C'liioi-oeihaiie ND C!~IoroSbram 0.74 Chloioniethane ND 2-Cliloiotoiuaie ND 4-Chlorotolucne ND i)ibroiiiochIoromcthme ND ! ,2-Dibromo-3-cliloio~~ropdne ND 1.2-Dibi-oinocihaiir (ED13) ND Dibromonicll~snc ND 1,2- Dichloi-ohcnreiie N 11 i ,3-ilichioi-obenz:r1e ND I .4-Diciilorobciizm NU I~~c l i lorodi f luo i -o i~~eth i~~~e D 1.1 -i)icliIoiocthaiic 72.3 I ,2-ijichioroetlianee ND 1 , I -J)ichiorocthci~e 542
Prectical Ouantitation Units -
7111 : Not Dcttctcd
Client: I~ltcrPhase T.nv~~onmentai, 111c Kcport Date: 09/09/05 Client Adrlrcss: 6200 Peacht~cc Street JEL Ref. No.: A-5428
Lo\ Angcles, CA YO040 Client Ref. Nu.: 05253
Attn: Paold Caldelo~?
l'roject: ~clplii(12486-000) Project Address: 1201 N Magnolia, Andlieim, CA
Date Sampled: 09/09/05 Date Received: 09/09/05 Date Analyzed: 09/09/05 Pliysical State: So11 Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DPO133- DP0134- Sample ID: SC-015 SG..005
Analytes: cis-I ,2-L)icliloroetliciie ND ND isaiis-I ,2-Dicliiorocibeiic ND ND I ,2-1)icliloropiopenc 78.4 2.67 1 ,3-1)icliloropropanc ND ND 2,2-DichIoroj?rope11c ND NI) I , I -Dicliioropropcne ND N11 1:tliylbeiizcne N D ND 1.i-coil 1 13 ND NU 1 l ~ s ~ ~ c l ~ l ~ ~ ~ ~ ~ l ~ ~ ~ ~ ~ ~ l ~ c t ~ c KD NU Isopro~~ylbcnrciic ND ND 4 Isopropyitolueiie ND ND Mctliylc~ic chloiide ND ND UaipliiI:alene ND ND 11-Propylbenze~~e ND ND Styrene ND ND 1 .I ,1,2-TetracliIoioethciie ND ND i,l,2,2-Teliacliloioeihclic ND ND I'etrncl~iokieth~lene 14.1 0.51 'Soliieiie ND ND i ,2,3-'l'ricliliirobe~ne1ic N D ND 1,2,4-TrichIorol~cnzc1ie ND ND I . I . I -'~riclilometliiine 343 18.2 I, I "2-'Sricliloroetlia~~e 0.26 ND Trichloroetliylcne 0.61 ND
Practical Ouantitation
Limits
0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010
I\D = Not Derc~led
6
Client: lnterf hase E~ivironmenldl, l i i ~ Report Date: 09/09/05 Client Addless: 6200 Peaciilrcc Streel JEI, Ret. No.: A-5428
Los Ai~geles, CA 90040 Client Ref. No.: 05253
i tto: i'aoia Cdldcroii Date Sampled: 09/09/05 Date Received: 09/09/05
P~oject: Dclplii (32486-000) Date Analyzed: 09/09/05 Projcct Addrew 1201 U Magiioli'~, Anaheim, CA Physical State: Soil Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0133- DI'0134- D1'0 1 34- DP0135- DP0135- Samplc ID: SG-015 SG-005 SG-015 SCj-005 SG-015 Ournfi tat~on units
Lirnlts - -
Analytes: 'iriclilorofluoio1i1etli'd1ie I ,2,3-'~i?cliloiopio~~i~~ic 1.2,4-~l'rimelhy!l~e~ize~1e 1,3,5-~~ri1~ieiliyll~e1~ie~1e Vinyl chloride Xyleilcs M'fDE litliyl-ten-butylcI1ie1- Di-isopiopylether tei-r-amylmelliylciliei- ~rii-Buryialcol~ol
Surrogate Recoverv : QC Lilnils Dibromofl~~o~o~iiethane ..... * 86% ..--.+ 91% ...--+ 60 - 140 ioliielie-d3 98% 100% 98% 101Yo 101% 60 - 140 4-Bromofl~ioiobe!~rene 94Yo 9 8% 92% 95% 9 4% 60 - 140
ND = Not Detc~ted liitcrfcreilces pie\rentcd ddequate smrogdte lecovciy for this sanlplc
JONES EhVlRONRfENTAL
Client: IntcrPhase Envisonmelitdl, Inc. Report Date: 09/09/05 Client Address: 6200 Pcachtsee Streel JEL Rcf. No.: A-5428
Los Arrgeles, CA 90040 Client ReE No.: 05253
iittn: Pdold Calden~ii Dale Sampled: 09/09/05 Date Received: 09/09/05
1'1ojcct: Delplii (32486.000) Date Analyzed: 09/09/05 Project Atldrew: 1201 U Magnol~a, Anaheim, CA Physical State: So11 Gas
EPA 8260B- Volatile Orgallics by GCIMS + Oxygenates
Sarnplc ID:
Analyles: Rcnrei~e 13minobeirzcnr l3ioiiiochlol-oiiicilia>ie 13roinodiclrIoro1iietixl11e Bioiiroforni Brornonicthaiie n-Butylbenranc src-i3iilylbeiizene ,., ,it . . Botylbeiizcnc i'ai-boil tetrachloride Cliloi-obciizciic Cliloroctl~aiie Chlorofoi-in Chloroiiictl~ane 2-C:!~iusololucne 4-Cliiorotoliiciic i~ihio~~iocliloroincihane I ,2-Dibromo-3-chioi~11j~~-oj3anc I .2-DibmiiioeiIia1ie (EDH) Ilibsoinomeiliai,c I ,?- Dichlol-olx?nzo?r I ,3-Dichlol-abenzene !,4-Dichloi-obeilzeiic i)ic!~loi-odifioos~~~~ieilia~~e 1 ,I -Diclilomclliane ! ,2-Dicliloroztliaiie 1.1 -1~icliIorociliei1e
ND = Not Detectcd
i)P0 114- DP012X- SG-005 SG 015
DCP
Client: 1nterPhdse Fnviro~~mei~tdl , Inc Report Date: 09/09/05 Clicr~t Addre%: 6200 Peachtrec Street JEL Ref. No.: A-5428
Lo, Aiigclcs, CA 90040 Clier~t Ref. Yo.: 05253
Attn: Paola Caldeion Date Sampled: 09109105 Date Received: 09/09/05
I'roject: Dclphi (32486-000) Date Analyled: 09/09/05 Project Addres: 1201 N Magnolid, Ailal~elm, CA Physical State: Soil Gar
hPA 8260B- Volatile Organics by GCIMS + Oxyge~rates
DI'0134- DP0128- DP0009- D P O I 2 8 DP0129- Practical S a n ~ i ~ l c 11): SG 9 0 5 SG-015 SG.015 SG-005 SG-015 Onanfitation Units
DUP I,imit\
Analytes: cii-l,2-D1chIorocihene ND ND YD ND ND 0 010 ug/L tian\- l,2-D1cIiloioetheilc NU NU ND ND ND 0 010 uglI_. 1,2-I)~~hloiopropane 3.66 4.14 6.68 2.78 11.4 0 010 uglL I ,? t)i~lrioiopiop~ne WD ND NU ND ND 0 010 ug/L 2,2-L)icliloropiopa~ic ND ND NU YD ND 0 010 ug/L :, I-ij~cliloropiopeni ND ND ND ND ND 0 010 ug/L Ill~ylbiiliene ND NU ND h D ND 0 010 uglL 1 rcoii 1 13 ND ND ND ND ND 0 010 ugL i leuacliloiobiit,idie~ie ND ND ND ND N D 0 010 I I ~ L i\opiopylbcniei~c ND ND ND UD ND 0 010 ug/l 4 I\opiopyltol~iene ND ND ND ND ND 0 010 ug/L Mclhyienc chloiide ND ND ND KD ND 0 0 1 0 ug'l Napl~thaie~ic ND ND ND ND ND 0 010 us/[ )I-Propy lheiizeiic ND ND ND ND ND 0 010 ug/L \l)icblc ND h D ND ND ND 0 010 iig/I 1.1 1,2- 1 r~racliloroeihene NL) NII ND ND ND 0 0 1 0 ug/L ! , I 2,2 ~eliacliloroeihciie N 17 UII ND ND ND 0 010 ug/L Tcr~ai iiloioelli) lciii- 0.46 0.12 0.21 0.21 0.85 0 010 iigll loliienc 0.14 ND ND NI) NII 0 010 iiglL I ,? 3 T!iiiiloiobeiiz~nc ND h D ND ND ND 0 010 ug/L 1,2 4- T~~~hloiobcii ic~~e ND ND ND ND ND 0 010 ug/L l,l.l-Tii~bloioelliaii~ 18.3 17.6 25.0 12.0 52.2 0 0 1 0 ug/L I ,l,2-1 ricliloioetlio~ie ND ND ND NU ND 0 010 ug/L T~ichIoroelb),Iene ND ND ND NU ND 0 010 ug/L
ND = Not Lletected
9
JONES ENVIRONMENTAL
C licnt: IiitciPhasc Eiiviioii~~ie~ital, I ~ L Client Address: 6200 Pcacht~cc Street
Lo? Aiigcles, CA 90040
Keport Ilate: JEI, Ref. No.: Client Ref. No.:
(\ttil: Pdold Caldeioii Date Sampled: Date Received:
Project: Delphi (32486-000) Date Analy~cd: Project Addreqs: 1201 N Magilolia, Ai~aheim, CA Physical State:
09/09/05 09/09/05 09/09/05 Soil Gd5
EI'A 82608- Volatile Organicc by GCIMS + Oxygenates
DP0134- DP0128- DP0009- DP0128. DPOI29- Practical Sa~rlple ID: SG-005 SG-015 SG-015 SG-005 SG-015 Ollantitation - Units
DUP
Dilution Factor
OC Limits 9l1% 60 - 140
ND = No1 Detected
JONES ENVIROI\IMENTAI,
Client: Intc~Phdse Environmental, Inc Report Date: 09/09/05
Clielll Address: 6200 Pedchtiee Stlcet JEL Ref. ho.: A-5428 Los Angeles, CA 90040 Client Ret. No.: 05253
Attn: Paold Calderoii Date Sampled: 09/09/05 Date Received: 09/09/05
ii'~.oject: Delphi (32486-000) Date Analyzed: 09/09/05 Project A d d l c t ~ : 1201 N bfdg~iol~a, Andhc~rn, CA Physical State: Soil Gay
EYA 8260B- Volatile Orgarlics by GCIMS + Oxygenates
Sa~nple Spiked: AMUlbhT AIR
MS MSD Acceptability Pdra~~iclci Rccoveiy ii%) Rccoveiv (96) RPD RilllRe(%)
Mctliod RI,iiik = Yot Detected
MS = Matlix Sprkc MSD - Matlrx Spike Dupl~cate RPI) = Rcidt~ve Percent Diifeience
J(j)hlEs PO. Box 5387 Fullerton, CA 92838
~ ~ \ ~ ~ [ f Q ~ ~ ) ~ ~ ~ ~ ~ t \ ~ Fax (714) (714) 449-9937 449-9685 TESTING IARORATORIES
Chain-of -Custody Record Analysis Reqiicsfnd
U Rush 24-48 Hours Rush 72-96 liours
authorization to p e h r m the analyses specified above under the Terms and Conditions set forth on the hack hereof
~~XEf3 PO. Box 5387 Fullerton. CA 92838
ENVIRQN)lENTL4id (714) 449-9937
TESTING LIIDORATORIES Fax (714) 449-9685 Chain-of-Custody Record
The delivery of sainpies and the signni~~rr 0'1 this Chain of Ciistody iorm constitutes
e inquis e y signairire authorization to perform the analyses specified above under the Terms and Conditions set ioith on the back hereoi
Jones Environmental, Inc. Testing Laboratories P.O. Box 5387 Fullerton, CA 92838
(714) 4429-9937 FAX (714) 4 4 9 - W
JONES ENVIRONMENTAL
LABORATORY REPORT
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. No.: A-55 18 Client Ref. No.: 32486-007
Attn: Paola Calderon
Project: Delphi (32486-000) Project Address: 1201 N. Magnolia, Anaheim, CA
Date Sampled: 08/22/06 Date Received: 08/22/06 Date Analyzed: 08/22/06 Physical State: Soil Gas
ANALYSES REQUESTED
1. EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Sampling - Soil Gas samples are collected in glass gas-tight syringes equipped with Teflon plungers. Tubing placed in the ground for soil gas sampling is purged three different times as recommended by DTSCIRWQCB regulations. This purge test determines how many purges of the soil gas tubing are needed throughout the project. One, three and seven purge volumes were analyzed to make this determination.
A tracer gas, n-Propanol, is placed at the tubing-surface interface before sampling. This compound is analyzed during the 8260B analytical run to determine if there are surface leaks into the subsurface due to improper installation of the probe. No n-Propanol was found in any of the samples reported herein.
The sampling rate was 200 cclmin using a battery operated sampling pump equipped with a rotameter. The sampling pump was calibrated at the beginning of the day using a certified flow meter. _I_ purge volumes were used since this purging level gave the highest results.
Analytical - Soil Gas samples were analyzed using EPA Method 8260 that includes extra compounds required by DTSCIRWQCB (such as Freon 1 13). Instrument Continuing Calibration Verification , QC Reference Standards, Instrument Blanks and Ambient Air Blanks are analyzed every 12 hours as prescribed by the method. In addition, Matrix Spike (MS) and Matrix Spike Duplicates (MSD) are analyzed with each batch of Soil Gas samples. A duplicate sample is analyzed each day of the sampling activity.
Approval: - I I 'U
Steve Jones, Ph.D. Laboratory Manager
Jones Environmental, Inc. PO. Box 5387 Fullerton, CA 92838
Testing Laboratories (714) 449-9937 FAX (714) 449-9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, C A 90040
Attn: Paola Calderon
Project: Delphi (32486-000) Project Address: 1201 N. Magnolia, Anaheim, CA
Report Date: 08/22/06 JEL Ref. No.: A-55 18 Client Ref. No.: 32486-007
Date Sampled: 08/22/06 Date Received: 08/22/06 Date Analyzed: 08/22/06 Physical State: Soil Gas
S a m ~ l e ID:
Analytes: Benzene Bromobenzene Bromochloromethane Bromod~chloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachlor~de Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene D~bromochloromethane 1,2-D~bromo-3-chloropropane 1,2-Dlbromoethane (EDB) Dlbromomethane 1,2- D~chlorobenzene 1,3-Dlchlorobenzene 1,4-Dlchlorobenzene D~chlorod~fluoromethane I, l -D~chloroethane 1,2-D~chloroethane I , l -Dlchloroethene
EPA 8260B- Volatile Organics by GCMS + Oxygenates
Practical Quantitation
Limits
N D = Not Detected
es Environmental, Inc. Testing Laboratorie~
P.O. Box 5387 Fullerton, CA 92838 (714) 449-9937 FAX (714) 449-9685 -
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, C A 90040
Report Date: 08/22/06 JEL Ref. No.: A-5518 Client Ref. No.: 32486-007
Attn: Paola Calderon Date Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Sample ID:
Analytes: cis- 1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane I, l -D~chloropropene Ethylbenzene Freon 1 13 Hexachlorobutadiene Isopropy lbenzene 4-Isopropyltoluene Methylene chloride Naphthalene n-Propylbenzene Styrene I,], 1,2-Tetrachloroethene 1,1,2,2-Tetrachloroethene Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Tr~chlorobenzene I, I, l -Trichloroethane 1,1,2-Trichloroethane Trichloroethylene
Practical Ouantitation
Limits Units -
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories
PO. Box 5387 Fullerton, CA 92838 (714) 449-9937 . FAX (714) 4423-9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Attn: Paola Calderon
Project: Delphi (32486-000) Project Address: 1201 N. Magnolia, Anaheim, CA
Report Date: 08/22/06 JEL Ref. No.: A-55 18 Client Ref. No.: 32486-007
Date Sampled: 08/22/06 Date Received: 08/22/06 Date Analyzed: 08/22/06 Physical State: Soil Gas
Sample ID:
Analytes: Tr~chlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Tr~methylbenzene 1,3,5-Tr~methylbenzene V~nyl chlor~de Xylenes MTBE Ethyl-tert-butylether Dl-~sopropylether tert-amylmethylether tert-Butylalcohol
Dilution Factor
Surrogate Recovery : Dibromofluoromethane Toluene-ds 4-Bromofluorobenzene
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Practical Quantitation Units -
Limits
QC Limits 60 - 140 60 - 140 60 - 140
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories
P.0. Box 5387 Fullerton, CA 92838 (714) 449-9937 FAX (714) M9-9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. No.: A-55 1 8 Client Ref. No.: 32486-007
Attn: Paola Calderon Date Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0287- DP0288- DP0288- DP0288- DP0285- Practical Sample ID: SG-02 1 - SG-005- SG-0 15- SG-020- SG-005- Ouantitation - units
0 1 0 1 01 01 0 1 Limits - Analytes: Benzene Bromobenzene Bromochloromethane Bromod~chloromethane Bromoform Broniomethane n-Butylbenzene sec-Butylbenzene tert-Buty lbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene D~bromochloromethane 1,2-Dlbromo-3-chloropropane 1,2-Dlbromoethane (EDB) Dlbromoniethane 1,2- Dlchlorobenzene 1,3-D~chlorobenzene 1,4-D~chlorobenzene D~chlorod~fluoromethane I, 1 -Dichloroethane 1 ,2vDichloroethane I, l -Dichloroethene
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories P.0. Box 5387 Fullerton, CA 92838
(714) 449-9937 FAX (714) 449-9685 J-
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. .No.: A-55 18 Client Ref. No.: 32486-007
Attn: Paola Calderon Date Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0287- DP0288- DP0288- DP0288- DP0285- Practical Sample ID: SG-02 1- SG-005- SG-0 15- SG-020- SG-005- Quantitation - units
0 1 0 1 01 01 0 1 Limits - Analytes: CIS- 1,2-D~chloroethene trans- 1,2-D~chloroethene 1,2-D~chloropropane 1.3-Dlchloropropane 2,2-D~chloropropane I, 1 -Dlchloropropene Ethylbenzene Freon 1 13 Hexachlorobutadlene Isopropylbenzene 4-Isopropyltoluene Methylene chlor~de Naphthalene n-Propy lbenzene Styrene 1,1,1,2-Tetrachloroethene 1,1,2,2-Tetrachloroethene Tetrachloroethylene Toluene 1,2,3-Tr~chlorobenzene 1,2,4-Trichlorobenzene I , I, 1-Trlchloroethane 1,1,2-Tr~chloroethane Trlchloroethylene
ND = Not Detected
Jones flnvironrnenta, Inc. Testing Laboratories PO. Box 5387 Fullerton, CA 92838
(714) 449-9937 FAX (714) 449-9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. No.: A-55 18 Client Ref. No.: 32486-007
Attn: Paola Calderon Date Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
EPA 8260B- Volatile Organics by GCMS + Oxygenates
DP0287- DP0288- DP0288- DP0288- DP0285- Practical Sample ID: SG-021- SG-005- SG-0 1 5- SG-020- SG-005- Ouantitation - Units
0 1 0 1 0 1 01 01 Limits
Analytes: Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene I ,3,5-Trimethylbenzene V ~ n y l chloride Xy lenes MTBE Ethyl-tert-butylether Di-isopropylether tert-amylmethylether tert-Buty lalcohol
Dilution Factor 1 /20* 1 4
Surrogate Recovery : Dibromofluoromethane
QC Limits 92% 60 - 140 104% 60 - 140 95% 60 - 140
ND = Not Detected * = Dilutions for these compound(s); first number for all others
Jones Environmental, Inc. Testing Laboratories P.O. Box 5387 Fderton, CA 92838
(714) 44999937 FAX (714) 44999(i85
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. No.: A-55 18 Client Ref. No.: 32486-007
Attn: Paola Calderon Date Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
Sample ID:
Analytes: Benzene Broinobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Buty lbenzene tert-Buty lbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane . 2-Chlorotoluene 4-Chlorotoluene D~bromochloromethane 1,2-Dtbromo-3-chloropropane 1,2-Dlbromoethane (EDB) Dlbromomethane 1,2- D~chlorobenzene 1.3-Dlchlorobenzene 1,4-Dlchlorobenzene D~chlorod~fluoromethane I, l -Dichloroethane 1,2-Dichloroethane I, l -D~chloroethene
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Practical Quantitation
Limits - 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20
Units -
N D = Not Detected
Jones Environmental, Inc. Testing Laboratories PO. Box 5387 Fullerton, CA 92838
(714) M9-9937 FAX (714) M9-9685 r
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. No.: A-55 1 8 Client Ref. No.: 32486-007
Attn: Paola Calderon Date Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
Sample ID:
Analytes: CIS- 1,2-D~chloroethene trans- l,2-Dichloroethene 1,2-D~chloropropane 1,3-D~chloropropane 2,2-D~chloro~ropane I , l -D~chloropropene Ethy lbenzene Freon 1 13 Hexachlorobutadlene lsopropylbenzene 4-Isopropyltoluene Methylene chlor~de Naphthalene n-Propy lbenzene Styrene ],I, 1.2-Tetrachloroethene 1,1,2,2-Tetrachloroethene Tetrachloroethy lene Toluene 1,2,3-Tr~chlorobenzene 1,2,4-Tr1chlorobenze11e l , l , 1-Tr~chloroethane 1,1,2-Tr~chloroethane Trlchloroethylene
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0285 DP00284 DP0284 DP0284 DP0289 Practical - SG-0 13: SG-005- SG-0 151 SG-0221 SG-OO~I ~uantitation
0 1 01 01 01 02 - Limits Units -
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories P.0. Box 5387 Fullerton, CA 92838
(714) M9-9937 FAX (714) PT9-!%85 - JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. No.: A-55 1 8 Client Ref. No.: 32486-007
Attn: Paola Calderon pate Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
Sample ID:
Analytes: Tr~chlorofluoromethane 1,2,3-Tr~chloropropane 1,2,4-Tr~methylbenzene I ,3,5-Tr~methylbenzene Vlnyl chloride Xy lenes MTBE Ethyl-tert-butylether Dl-lsopropylether tert-amylmethylether tert-Buty lalcohol
Dilution Factor
Surrogate Recovery : Dibromofluoromethane Toluene-d8 4-Bromofluorobenzene
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Practical Quantitation Units -
Limits -
OC Limits 60 - 140 60 - 140 60 - 140
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories
RO. Box 5387 Fullerton, CA 92838 (714) 449-9937 FAX (714) @9-!9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. No.: A-55 18 Client Ref. No.: 32486-007
Attn: Paola Calderon Date Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
Sample ID:
Analytes: Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Buty lbenzene Carbon tetrachlor~de Chlorobenzene Chloroethane Chloroform Chloroniethane 2-Chlorotoluene 4-Chlorotoluene Dl bromochloromethane 1,2-D~bromo-3-chloropropane 1,2-D~bromoethane (EDB) Dibromomethane 1,2- Dichlorobenzene 1,3-D~chlorobenzene 1,4-Dlchlorobenzene D~chlorodifluoromethane I, l -Dichloroethane 1,2-Dichloroethane 1.1 -Dlchloroethene
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Practical Quantitation
Limits Units -
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories
P.O. Box 5387 Fullerton, CA 92838 (714) &9-9937 FAX (714) 449-%85
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. No.: A-55 18 Client Ref. No.: 32486-007
Attn: Paola Calderon Date Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
Sample ID:
Analytes: cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane I, l -Dichloropropene Ethy lbenzene Freon 1 13 ~exachlorobutadiene Isopropy lbenzene 4-Isopropyltoluene Methylene chloride Naphthalene n-Propy lbenzene Styrene 1,1,1.2-Tetrachloroethene 1,1,2,2-Tetrachloroethene Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene I , 1, l -Trichloroethane 1,1,2-Trichloroethane Trichloroethylene
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Practical Ouantitation
Limits -
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories RO. Box 5387 Fullerton, CA 982338
(714) 449-9937 FAX (714) 449-9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 08/22/06 JEL Ref. No.: A-55 1 8 Client Ref. No.: 32486-007
Attn: Paola Calderon Date Sampled: 08/22/06 Date Received: 08/22/06
Project: Delphi (32486-000) Date Analyzed: 08/22/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
Sample ID:
Analytes: Tr~chlorofluoromethane 1,2,3-Trlchloropropane 1,2,4-Tr~methylbenzene 1,3,5-Tr~methylbenzene Vlnyl chlorlde Xylenes MTBE Ethyl-tert-butylether Di-~sopropylether tert-amylmethylether tert-Butylalcohol
Dilution Factor
Surrogate Recovery : Dibromofluoromethane Toluene-d8 4-Bromofluorobenzene
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Practical Quantitation Units -
Limits -
OC Limits 60 - 140 60 - 140 60 - 140
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories
P.O. Box 5387 Fullerton, CA 92838 (714) 449-9937 FAX (714) 449-9685
JONES ENVIRONMENTAL
QUALITY CONTROL INFORMATION
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Attn: Paola Calderon
Project: Delphi (32486-000) Project Address: 1201 N. Magnolia, Anaheim, CA
Report Date: 08/22/06 JEL Ref. No.: A-55 18 Client Ref. No.: 32486-007
Date Sampled: 08/22/06 Date Received: 08/22/06 Date Analyzed: 08/22/06 Physical State: Soil Gas
EPA 8260B- Volatile Organics by GCMS + Oxygenates
Sample Spiked: AMBIENT AIR
Parameter
1 , l -Dichloroethylene Benzene Trichloroethylene Toluene Chlorobenzene
MS MSD Acceptability Recovery (%) Recoverv (%) Range (%)
Method Blank = Not Detected
MS = Matrix Spike MSD = Matrix Spike Duplicate RPD = Relative Percent Difference
JONES ENVIRONMENTAL TESTING LABORATORZES
P.O. Box 5387 Fullerton, CA 92838
(714) 449-9937 Fax (7 14) 449-9685 Chain-of -Custody Record
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JONES ENVIRONMENTAL TESTlNG LABORATORlES
P.O. Box 5387 Fullerton, CA 92838
(71 4) 449-9937 Fax (71 4) 449-9685 Chain-of-Custody Record
Company Time Company Time forth on the back hereof.
JONES EYVIRONMENTAI,
Client: Inte~Phase Env~~onniental, 11ic Iieport Datc: Client Addrecc: 6200 Peachtiec Strcct JEI, Ref. l o . :
Los Angeles, CA 90040 Client Ref. Yo.:
Attn: Paola Calde~ on
Projec-t: Delphi (32486-000) Project Address 1201 N Magilolid, Aliaheini, CA
Date Sarnpled: Date Received: Date Analy~ed: Pbysical State:
I EPA 82600- Volatile O~ganics by GCIMS + Oxygenates
Sampling - Soil Gas san~ples are collected in glass gas-tight syri~iges equipped with Teflon plungers. Tubi~ig placed in the groulid for soil gas sampling is purged tlirec different tiincs as recommcndcd by I)TSC/RWQCB regulations. This purge test detcr~i~incs how many purges of tire soil gas tubing are needed throughout tlie pro,ject. One, three arid seven purge volunics were analyred to make this dctermiiiation.
No 11-Propanoi was foiind in ally ofthe sa~l>ples reported lierein.
'i'lic saiiipliiig mtc was 200 cclmiii using a battery operated sampling puinp equipped wit11 a I-otanicter. The sampling pu111p was calihratcd at tlie beginiring of the day using a certiiied flow meter. 1 purge volu~?ws were used si~ice this purging level gave the liigiiest results.
A~ialytical - Soil Gas saiiiplcs were aiialyzed using EPA Metliod 8260 that i~iciudcs extra conipounds rcqtiired by DTSClRWQCk (such as i'reon 1 13). Instruiilcnt Continuing Calibration Verification , QC Referciice Standards, Instrument BianI<s and Aiiuhiciit Air Blanks are airaiyred every 12 hours as prescribed by the method. 111 addition, Matrix Spike (MS) alid Matrix Spike Di~plicates (MSD) arc analyzed wit11 each batch of Soil Gas samples. A duplicate sample is a~inlyrcd each day of tlie salilpiing activity.
Approval: , - d
Steve Tones, Pli I3 Ldboratory Mandger
JOVES ENVIRONMENTAL
Client: IntcrPIia?e Enviroiii~iental, Inc Client Address: 6200 Peacht~cc Strcet JEI, Ret. No.: B-4117
Los Angelcs, CA 90040 Client lief. No.: 05253
Attn: Paola Cdlderon Date Sampled: 1011 1/05 Date 12eceivcd: 1011 1/05
Project: Delpii~ (32486-000) Date Analy~ed: 1011 1105 Project Address: 1201 Y Magnolia, Andhcim, CA Pllysical State: Sod Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0193- S a n ~ ~ l e ID: SG-005
Analytes: Benicne ND 13roinobenzeiie ND Rro~nocl~iui-omeiliriiic ND Dioi~iodichloi-ooiclhm ND Rrotnofoim ND Bioiiioiiictiiane ND n-Bulylbcnzcne ND sec-hitylbenzcnc ND tei-t-Butylbenrcne NO Carboii tcti-achioridc ND Ciiloi-ol~cnzeiie ND C'hioroe~i~anc ND Chloroform ND CIiIoromeilianc ND 2-Cliloi-otoluene ND 4-('iiioroioiuenr ND Ilibi-oiiiocliloroii~ctl~d~le ND 1 ~2-I)ihroo~o-3-cl~Ioi-oprop~ii1e ND I ,?-Dibi-omoetli (IXDB) ND l>ibromoinsthai~e ND I,2- L>icl~lorobenzcnc ND I ;l-llichlorobcnicne ND I .4-Dichlor(1heiizene NU L7icl~loi-odifliioionieil1a1~e ND 1 ,I-llichioioethane 25000 I ,2-l.>ichloi-oetlia11c ND 1 ,I -DicIiloroethciir 490000"
DP0193- D1'0193- SG-005 3 - 0 1 5
DUP
NLI - Not Detected
JONES ENVIROXMENTAE
Client: IntcrPhdsc hnvlioni~lcntd~, lllc Report Date: 10/12105 Client Address: 5200 Peachtree Strect JEI, Ref. No.: B-41 I7
Los Angeles, CA 90040 Client ReE No.: 05253
Atln: Pdola Cdldeioil Date Sampled: 1011 1/05 Dale Received: 1011 1/05
Project: Delphi (32486-000) Date Analy~ed: 1011 1/05 I'roject Address: 1201 N Magi~olia, A ~ ~ d h c ~ m , CA Physical State: So11 Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
IIP0193 DPOI93- DP0193- DP0194- DP0194- Santj~le ID: SG-005 SG-005 S C 0 l S SG 022 SG-015 CM""titatiol1 Unit\
DUP Limits
Analytcs: cis-l.2-C)icl1loi-oethciie ND ND ND ND N 1) 10 ug!hf3 ti-ans-1.2-Dicliioi-oetlienc ND ND ND hrD NI) 10 I I~IM' I ,2-Dichlol-opropanc ND ND ND ND NII 10 u ~ / M ' I ,?-IDicRloropropanc ND ND ND ND N I) 10 2,2-i)iciriosopl-opc ND ND ND ND ND 10 ug/M3 I , i -l>~chioropropenr ND ND ND ND ND 10 u ~ / M ' L:tbylbrnie~~e ND ND ND ND NII 10 ug/M3 Fi-eoii 113 ND ND N I) ND NU 10 ug/hf3 iiexachioi-ohiitadiei~c ND ND ND ND N 11 10 U~/M'
lso~?ropplbcnzne ND ND ND ND N I1 10 u ~ / M ' 4-lsoplo~iylioi~1~1ic ND ND ND ND NU 10 ag/M3 .Mciliyleiic chloride ND N D ND ND N I l 10 u d ~ ' Naphthalcrlr ND ND ND NU NII 10 u d ~ ' n-I'ropylhe~izc~rc ND ND ND ND Ni l 10 ng/hf3 Styi-eile ND ND ND ND ND 10 1 i f 1 ~ ' I ; I. I ,2:Sctracliloroc~iimc ND ND N D ND ND 10 ugM3 1,1,2.2-Trtrachioroethcne ND ND ND NU ND 10 udMJ 'Scii-iichioiocthylcoe ND ND 4100 ND 4100 10 ag/hf3 Toliieiie NI) ND ND ND N I 1 10 ug/M3 i ,2,3-Trichiorohcnzene ND ND ND ND N 11 10 LL~/M' 1,2,4-Triclilol-obc~1ie~ie ND NU ND NI) ND 10 ug/M? I , I .I-Triclrlul-oetiiaiie 240000* 230000* 440000* 210000" 430900 10 uE1hf3 1 , I ,2-Ti-icliloi-ocLIlaiic ND ND ND ND ND 10 UF/M' TI-icliloi-oc~liylel~c ND ND ND ND ND 10 iig/hf3
ND = Not Detected
3
JONES ENVIRONMENTAL
Client: Iiite~Phdse l 1ivi1oiimenid1, 111c Report Date: 10/12/05 tl icot Address: 6200 Peaclit~ee Slreci JEL Ref. No.: B-4117
I 07 AngcIc5, CA 90040 Client Ret. No.: 05253
Attn: Pdoia Calderoll Date Sampled: 1011 1/05 Date Received: 1011 1/05
Project: Ileiphi (32486-000) Dale Analyzed: 1011 1/05 I'lojcct Address: 1201 N Magilolid, Anahclm, CA Physical State: Soil Gel\
EPA 82608- Volatile Orgallies by CCIMS + Oxygel~ates
DP0194- DPO 195- DPOI95- 01'0195- DP0196- Practical S a ~ ~ i p l c ID: SG-005 SG-022 SG-015 SG-005 SG-022 Quantitation - units
Bromon,ei!ian; ND ND !1-l3i~tylbenzsne NU ND scc-8iitylhe!!icnc ND ND tcrt-Buiyibciizene ND ND Carbon iciiachloriiic ND ND Clilorobeiize~ic ND ND Clrloi-oeil>ane ND ND Chloioiol-iii ND ND Ciilorometlraiic ND ND 2-Cliloioioluene ND N D 4-Cliliiiotoiiienc ND ND llibroiiiochloi-oii7etiiatie ND ND 1,2-Djl~rnn~o-l-chloropr~1pa11ii ND ND 1,2-1libromoethaiie (EDB) ND ND Llibromoiuethene ND ND I .2- I)iclilorobenze~ie ND ND 1,3-Dicliloi-oheiizene NI) NU I ,4-Dichlorobciirm ND ND llichloi-odifliioio~iietliaiie ND ND i , I -I>icliloioetIiaiie 13000 31000 i .2-l~icliloroethaiie ND ND i ,I-Dicliiol-oetheliz 520000" 700000"
JONES EhVIRONMENTAL
Client: 1n taPbd~c Envitonmental, Iilc Report Date: 10/12/05 Client Address: 6200 Pcachtiec Streci JEL Ret. No.: B-4117
Log Angelcs, CA 90040 Client Ref. No.: 05253
Altrt: Paola Calderoii Date Sampled: 1011 1/05 Date Received: lO/l 1/05
l'roject: Delphi (32486-000) Date Analyzed: 1011 1/05 Project Addre~s: 1201 N Magnolia, Ailahcim, CA Physical Statc: So11 Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0194- UP0195 DP0195- DP0195_ DP0196- PI actical Sample ID: SG-005 SG. 022 SG-015 S u 0 5 SCi-022 Ouantitation urlits
I.imil\ -
.4nalytes: cis-i,2-Dichloiocihe1ic ND ti-811s-l,2-Dicliloi-octhene ND 1.2-Dichlot-opropat,c ND I ,3-1)icl:loroprot~m ND ,2-Diciiioi-opi"1inns ND I , I -1)icIiloi-oi?i-opeiic KD F.thyihe!~zeiie ND Freon 1 13 ND l~Iexuclilo?obiitadirnz hiD lsoplapylbenzrne ND 3-1so~)ropyIioloeiie N D Melhylenc cliloridc ND N:phtliii!cne ND hi-Prapyibciizene ND Styretic ED i.1,1,2-l~tracl~loroctl:c1ie ND 1,1.2,2-'rcti-achlorocthene N 13 Tcti-achloroctliyieiie ND 'i'oluciie ND 1,2,3-Tr1c!~lorobenzene ND ! ,2.4-~i'iiciiiorobe1r~ei1~ ND I,] ;I-Ti-ichlorozthane 300000* I , I $2-'iriciiiorosiiiane ND Tiichloroetl~yicne ND
JORES ENVIRO3MCN I'AL
Clicnt: 11iterPhasc Environmental, Inc. Report Datc: 10/12/05 Client Address: 6200 Pcachlree Slreel JGL Ref. No.: R-41 17
Los Angcles, CA 90040 Client Ref. No.: 05253
Attn: I'aola Caldcro~i Date Sampled: 1011 1/05 Date Received: 1011 1/05
Projec(: Delplri (32485-000) Dale Analyzed: I 011 1/05 Prqject .\MI-ess: 1201 X. Magnolia. Analicim, CA Pl~ysical State: Soil Gas
EPA 8260B- Volatile Orgallics by GCIMS + Oxygenates
DPO 194- DP0 195- DP0195- DP0195- DPOI96. Practical Sample ID: SG-005 SG-022 SG-015 SG-005 SG 022 Ou""fitafio11
I,imd\
Analytes: 'is~cliloi?~iluoioii~etliane I ,2.3-Ti-ichloropro~~ii1ie I . l . i- ' : 'r i inctI iylbct~~e~~c
I ,3,S-?'rimctl1yli~c~iicnc Vinyl chlol-lde Xylcnes MTHE Ethyl-tcit-biityiellic~~ Di-~sopi.opylclhcs icrt-amylmcthyletlici icil-U~~tylalc~hnl
Surroeate Rccoverv : l)~I)iomoflrio~ orlrcthaiic Toli~ei~e-db 4-Uiornofluorobe~iieile
ND = hot Detected A - D~lulio~rv f o ~ tlrese corripound(v), first numbei Tor all other?
QC Limits 66% 60 - 140 106% 60 - 140 94% 60 - 140
JONES ENVIRONMEN'I'AL
Client: InterPhase I? i ivi ro~~ine~l ta i , tnc. Report Date: l0/12/05 Client Address: 6200 Peaclitree Street JEL ReC No.: B-4117
Los Angeles, C A 90040 Client Ref. No.: 05253
Attn: Paold Calderoil Date Sampled: 10/1 1/05 Date Received: 10/1 1/05
I'rojcct: Delphi 132486-000) Date Analyzed: 1011 1/05 1'1 ojcct Addresc: 1201 h Mag~iol ia , Aiiahell??, CA Physical State: Soil G a i
EPA 8260B- Volatile Organics by CCIMS + Oxygenates
DI'O 196- DP0196- DPO 197- DP0197- DP0197 - Practical S;unple 11): SG. 015 SG-005 SG-022 SGJ15 SG-005 Quantitation
Limitr,
Analytes: cis-I .2-Dichloroelhenc ND ND N D ND N I1 10 uP'M3 trans-I ,2-Dic11lorosthenc N D ND ND NII NII 10 L I ~ M ~ 1.2-Dichloropiopane ND ND N D N D NII 10 ug/M3 1,3-i>ichioropiopanc N D ND ND ND N 11 10 iiir/M" 2.2-Llicliloropro~1a1ie N D ND ND N D NII 10 uli'M3 I . I -ilicliloi-ojiiopei~ ELliylbcil~ciic I'rcoii 1 13 ilexach!oi-obutadiclie lsopropylbenienc 4-Isopiopyltoliicne Vcil~ylciie chloride Na!~hiIialo~c n-Propylhrnrciie Styi-eiir
l ; i .I.?-Tetmcl~loi-oel!ic~iii
1,1,2,2-Tetrac1lLoioetheiie Tcli-achloroctliylene 'ioi:iene 1.2.3-Tricli!orol>eiizenc l,2.4-l'i-ichIorohc11~~1ie I , I .l-7ricl~lomethane I . I ,2-'~ricliIoroetliai~e .I'l-icliloroetliylciic
N U = h o t Detected
N 11 N U NI) N II NII N D ND N U ND N 11 ND NU ND ND ND Nn 540 ND ND
JONES ENVIROWMENTAL
Clieot: 111teiPhaic E~~viroiimental, llic Report Date: 101 12/05 Client Addres?: 6200 l'cachtree SQcet .JEL Ref. No.: R-4117
Los Aiigelei, CA 90040 Client Ref. No.: 05253
Attn: Paold Caldeioii Date Sampled: 1011 1105 Date Received: 1011 1/05
Project: Delphi (32486-000) Date A!?alyzed: 10/11/05 Project Address: 1201 Y Mdgnol~a, Anahelill, CA Physical Sedte: Soil Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
UP0196 UP0196- DP0197. UP01 97- DP0197 - P~actical S a n t ~ l e ID: S c 0 l 5 SG-005 SG.022 SG. 015 SG 005 Ou"ntit"'io11
I,imi(a
Analytes: TrichIoroili1oso1iictlia1ii I ,2,3-Triciiloropropai~e i ,2,4-l'i-imeiliyIbe11ieiie i ,3,5-'l'si111ctl~ylbe~iie1i~
Viiiyl cliloride Xylcnes MTBE iihyl-tcl-1-biiiyicthsr Di-isopropyietbcr terl-arnylmctl~yleilie~ ten-13uiyialcoI1ol
Surroyate Recover, : QC Lirnits I I ib~o~~io f l i io~o~i~c t I~anc 112% 126% 120% 129% 117% 60 - 140 iol~ienc-d8 I 02IYo 106% 101% 105% 105% 60 - 140 4-Rio~~~ofluoiobeiizenc 89%" 90% 93%) 95% 97% 60 - 140
NU = Not Detected
10
JONES ENVIRONMENTAL
Client: InterPhdsc Envrronmenldl, Inc Report Date: 1011 2/05 Client Address: 6200 Pedchtrcc Street JEL Ref. No.: B-4117
1,os Angcles, CA 90040 Client Ref. No.: 05253
Altn: l'dold Cilldeion Dale Sampled: 1011 1/05 Date Received: 1011 1 105
Project: Delphi <32486-000) Date Analy~ed: 1011 1/05 Project Address: 1201 N Mdgiioiia, Alidhelln, CA Physical State: Soil Gas
EPA 82608- Volatile Organics by GCIMS + Ohygenates
Sample Spiked: AMBlEhl AIR
MS MSD Acceptabilily I',II ai~icici Recovery (36) Rccovery (%) RPD Range (%,I
i i -Diciilol oethylcne 89% 97% 8 0% 60 - 140 Ben7ene 118% 119% 1 0% 60 - 140 rriclilo~ oelliylenc 109% 103'/0 5 0% 60 - 140 Tolucne 126% 109% 14% 60 - 140 Chiorobenzeiic 98% 88% 11% 60 - 140
Sample Spiked: AMBIENT AIR
1h45 MSD Acceptab~lrty I'<~ra~nctc~ Itccoverv i%) Recoverv (761 RPD Rd~itzc (961
Mcthori Blank = Not Dcteclcd
MS = M<~lrix Spikz MSD = Mdtiix \pikc Duplicalc Rl'D = Relative Peicziit Differcr~cc
11
JONES Po. BOX 5387 Fuilerton. CA 92838 Eh-IJTIR;QNJIEhTTAiL (714) 449-9937
~ E S T I I Y G L4DORATORIES Fax (714) 449-9685
Turn Around Requested:
3 Immediate Anention
il Rush 72~9 f i Hours
I Sample ID I Discussion I Date / Time I
Chain-of -Custody Record
Laboiu toy Sampie Number
/ I J E L Project #
Sample Condition as Received.
Chilled II yes
I ~ " " ' w Y " ~ . : , ~, t 1 ' " " ' L . I The deliverv of samples and the siunature on , . * > i " ~:o:@.,~ ,j v?iL?,:brk- I this Chain i f ~ustody form constitutes
@ ~eiinquished by (sigi(btuie) Date 10 Reccived byzborboiatory (signature) Date authorization to perform the analyses specified
Company l ime Company l ime
above under the Terms and Conditions set foith on the back hereof.
JONES PO. Box 5387 Fullerton CA 92838
EK1781R~IX?%%~XTd2iL Fax (714) (714) 449 449-9685 9937 TEST1 YG L4RORAI'ORiES
I I 1
Ttme forth on the back hereof.
Company Time Company
JONES EYVIRONMENTAI,
Client: Inte~Phase Env~~onniental, 11ic Iieport Datc: Client Addrecc: 6200 Peachtiec Strcct JEI, Ref. l o . :
Los Angeles, CA 90040 Client Ref. Yo.:
Attn: Paola Calde~ on
Projec-t: Delphi (32486-000) Project Address 1201 N Magilolid, Aliaheini, CA
Date Sarnpled: Date Received: Date Analy~ed: Pbysical State:
I EPA 82600- Volatile O~ganics by GCIMS + Oxygenates
Sampling - Soil Gas san~ples are collected in glass gas-tight syri~iges equipped with Teflon plungers. Tubi~ig placed in the groulid for soil gas sampling is purged tlirec different tiincs as recommcndcd by I)TSC/RWQCB regulations. This purge test detcr~i~incs how many purges of tire soil gas tubing are needed throughout tlie pro,ject. One, three arid seven purge volunics were analyred to make this dctermiiiation.
No 11-Propanoi was foiind in ally ofthe sa~l>ples reported lierein.
'i'lic saiiipliiig mtc was 200 cclmiii using a battery operated sampling puinp equipped wit11 a I-otanicter. The sampling pu111p was calihratcd at tlie beginiring of the day using a certiiied flow meter. 1 purge volu~?ws were used si~ice this purging level gave the liigiiest results.
A~ialytical - Soil Gas saiiiplcs were aiialyzed using EPA Metliod 8260 that i~iciudcs extra conipounds rcqtiired by DTSClRWQCk (such as i'reon 1 13). Instruiilcnt Continuing Calibration Verification , QC Referciice Standards, Instrument BianI<s and Aiiuhiciit Air Blanks are airaiyred every 12 hours as prescribed by the method. 111 addition, Matrix Spike (MS) alid Matrix Spike Di~plicates (MSD) arc analyzed wit11 each batch of Soil Gas samples. A duplicate sample is a~inlyrcd each day of tlie salilpiing activity.
Approval: d
Steve Tones, Pli I3 Ldboratory Mandger
JOVES ENVIRONMENTAL
Client: IntcrPIia?e Enviroiii~iental, Inc Client Address: 6200 Peacht~cc Strcet JEI, Ret. No.: B-4117
Los Angelcs, CA 90040 Client lief. No.: 05253
Attn: Paola Cdlderon Date Sampled: 1011 1/05 Date 12eceivcd: 1011 1/05
Project: Delpii~ (32486-000) Date Analy~ed: 1011 1105 Project Address: 1201 Y Magnolia, Andhcim, CA Pllysical State: Sod Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0193- S a n ~ ~ l e ID: SG-005
Analytes: Benicne ND 13roinobenzeiie ND Rro~nocl~iui-omeiliriiic ND Dioi~iodichloi-ooiclhm ND Rrotnofoim ND Bioiiioiiictiiane ND n-Bulylbcnzcne ND sec-hitylbenzcnc ND tei-t-Butylbenrcne NO Carboii tcti-achioridc ND Ciiloi-ol~cnzeiie ND C'hioroe~i~anc ND Chloroform ND CIiIoromeilianc ND 2-Cliloi-otoluene ND 4-('iiioroioiuenr ND Ilibi-oiiiocliloroii~ctl~d~le ND 1 ~2-I)ihroo~o-3-cl~Ioi-oprop~ii1e ND I ,?-Dibi-omoetli (IXDB) ND l>ibromoinsthai~e ND I,2- L>icl~lorobenzcnc ND I ;l-llichlorobcnicne ND I .4-Dichlor(1heiizene NU L7icl~loi-odifliioionieil1a1~e ND 1 ,I-llichioioethane 25000 I ,2-l.>ichloi-oetlia11c ND 1 ,I -DicIiloroethciir 490000"
DP0193- D1'0193- SG-005 3 - 0 1 5
DUP
NLI - Not Detected
JONES ENVIROXMENTAE
Client: IntcrPhdsc hnvlioni~lcntd~, lllc Report Date: 10/12105 Client Address: 5200 Peachtree Strect JEI, Ref. No.: B-41 I7
Los Angeles, CA 90040 Client ReE No.: 05253
Atln: Pdola Cdldeioil Date Sampled: 1011 1/05 Dale Received: 1011 1/05
Project: Delphi (32486-000) Date Analy~ed: 1011 1/05 I'roject Address: 1201 N Magi~olia, A ~ ~ d h c ~ m , CA Physical State: So11 Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
IIP0193 DPOI93- DP0193- DP0194- DP0194- Santj~le ID: SG-005 SG-005 S C 0 l S SG 022 SG-015 CM""titatiol1 Unit\
DUP Limits
Analytcs: cis-l.2-C)icl1loi-oethciie ND ND ND ND N 1) 10 ug!hf3 ti-ans-1.2-Dicliioi-oetlienc ND ND ND hrD NI) 10 I I~IM' I ,2-Dichlol-opropanc ND ND ND ND NII 10 u ~ / M ' I ,?-IDicRloropropanc ND ND ND ND N I) 10 2,2-i)iciriosopl-opc ND ND ND ND ND 10 ug/M3 I , i -l>~chioropropenr ND ND ND ND ND 10 u ~ / M ' L:tbylbrnie~~e ND ND ND ND NII 10 ug/M3 Fi-eoii 113 ND ND N I) ND NU 10 ug/hf3 iiexachioi-ohiitadiei~c ND ND ND ND N 11 10 U~/M'
lso~?ropplbcnzne ND ND ND ND N I1 10 u ~ / M ' 4-lsoplo~iylioi~1~1ic ND ND ND ND NU 10 ag/M3 .Mciliyleiic chloride ND N D ND ND N I l 10 u d ~ ' Naphthalcrlr ND ND ND NU NII 10 u d ~ ' n-I'ropylhe~izc~rc ND ND ND ND Ni l 10 ng/hf3 Styi-eile ND ND ND ND ND 10 1 i f 1 ~ ' I ; I. I ,2:Sctracliloroc~iimc ND ND N D ND ND 10 ugM3 1,1,2.2-Trtrachioroethcne ND ND ND NU ND 10 udMJ 'Scii-iichioiocthylcoe ND ND 4100 ND 4100 10 ag/hf3 Toliieiie NI) ND ND ND N I 1 10 ug/M3 i ,2,3-Trichiorohcnzene ND ND ND ND N 11 10 LL~/M' 1,2,4-Triclilol-obc~1ie~ie ND NU ND NI) ND 10 ug/M? I , I .I-Triclrlul-oetiiaiie 240000* 230000* 440000* 210000" 430900 10 uE1hf3 1 , I ,2-Ti-icliloi-ocLIlaiic ND ND ND ND ND 10 UF/M' TI-icliloi-oc~liylel~c ND ND ND ND ND 10 iig/hf3
ND = Not Detected
3
JOUES ENVIRONMENTAL
Client: IntcrPlidse knviioiiii~enldl, 11lc Report Dale: 101 12/05 Client Adclreu: 6200 Peachl~ee Siieel J E L Rcf. No.: B-4117
Lob A~igcles, CA 90040 Client Rcf. No.: 05253
Attn: Paola Caldcro~i Date Satnpled: IOII 1/05 Date Received: 1011 1/05
Projccl: Delphi (32486-000) Date A ~ ~ a l y r e d : lO/l 1/05 Project Address: 120 1 N Magiiolia, Analieim, CA Physical State: Soil Cds
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0191- DP0193- DP0!9?_ DIJ0194- DP0194- Practical Sample ID: SG-005 S G 0 0 5 SG-015 SG-022 SG-01 5 Ouanfitation
DIJP Limit, Aaalytes: 'i'riclilol-ofluoromcilia~ic I ,2,3-'i'riciiioropr<1~~a!ie 1,2,?-Tri1iietiiylben~ei1e i ,3,5-'iriniciliyIbe1izciic Vinyl chloride Xylcncs MTl3E I;thyl-lcrl-l~u1ylet1ier Di-isopropylet11i.i. icrl-aii~ylmelhyleilizr ici-1-Br~tylalcolini
Dilution Factor
Surrogate Recovery : OC Lirnits D~b~oi~ioIIuotoiiictli~~ne 90% 78% 64% 71% 103% 6 0 - 140 Toliieoe-dQ 9Y00 95% 102% 101% 96% 60 - 140
- = D~liii~ons for these com]~ouiid(s), fiist number f o ~ all orheis
JONES ENVIRONMENTAL
Client: Iiite~Phdse l 1ivi1oiimenid1, 111c Report Date: 10/12/05 tl icot Address: 6200 Peaclit~ee Slreci JEL Ref. No.: B-4117
I 07 AngcIc5, CA 90040 Client Ret. No.: 05253
Attn: Pdoia Calderoll Date Sampled: 1011 1/05 Date Received: 1011 1/05
Project: Ileiphi (32486-000) Dale Analyzed: 1011 1/05 I'lojcct Address: 1201 N Magilolid, Anahclm, CA Physical State: Soil Gel\
EPA 82608- Volatile Orgallies by CCIMS + Oxygel~ates
DP0194- DPO 195- DPOI95- 01'0195- DP0196- Practical S a ~ ~ i p l c ID: SG-005 SG-022 SG-015 SG-005 SG-022 Quantitation - units
Bromon,ei!ian; ND ND !1-l3i~tylbenzsne NU ND scc-8iitylhe!!icnc ND ND tcrt-Buiyibciizene ND ND Carbon iciiachloriiic ND ND Clilorobeiize~ic ND ND Clrloi-oeil>ane ND ND Chloioiol-iii ND ND Ciilorometlraiic ND ND 2-Cliloioioluene ND N D 4-Cliliiiotoiiienc ND ND llibroiiiochloi-oii7etiiatie ND ND 1,2-Djl~rnn~o-l-chloropr~1pa11ii ND ND 1,2-1libromoethaiie (EDB) ND ND Llibromoiuethene ND ND I .2- I)iclilorobenze~ie ND ND 1,3-Dicliloi-oheiizene NI) NU I ,4-Dichlorobciirm ND ND llichloi-odifliioio~iietliaiie ND ND i , I -I>icliloioetIiaiie 13000 31000 i .2-l~icliloroethaiie ND ND i ,I-Dicliiol-oetheliz 520000" 700000"
JONES EhVIRONMENTAL
Client: 1n taPbd~c Envitonmental, Iilc Report Date: 10/12/05 Client Address: 6200 Pcachtiec Streci JEL Ret. No.: B-4117
Log Angelcs, CA 90040 Client Ref. No.: 05253
Altrt: Paola Calderoii Date Sampled: 1011 1/05 Date Received: lO/l 1/05
l'roject: Delphi (32486-000) Date Analyzed: 1011 1/05 Project Addre~s: 1201 N Magnolia, Ailahcim, CA Physical Statc: So11 Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0194- UP0195 DP0195- DP0195_ DP0196- PI actical Sample ID: SG-005 SG. 022 SG-015 S u 0 5 SCi-022 Ouantitation urlits
I.imil\ -
.4nalytes: cis-i,2-Dichloiocihe1ic ND ti-811s-l,2-Dicliloi-octhene ND 1.2-Dichlot-opropat,c ND I ,3-1)icl:loroprot~m ND ,2-Diciiioi-opi"1inns ND I , I -1)icIiloi-oi?i-opeiic KD F.thyihe!~zeiie ND Freon 1 13 ND l~Iexuclilo?obiitadirnz hiD lsoplapylbenzrne ND 3-1so~)ropyIioloeiie N D Melhylenc cliloridc ND N:phtliii!cne ND hi-Prapyibciizene ND Styretic ED i.1,1,2-l~tracl~loroctl:c1ie ND 1,1.2,2-'rcti-achlorocthene N 13 Tcti-achloroctliyieiie ND 'i'oluciie ND 1,2,3-Tr1c!~lorobenzene ND ! ,2.4-~i'iiciiiorobe1r~ei1~ ND I,] ;I-Ti-ichlorozthane 300000* I , I $2-'iriciiiorosiiiane ND Tiichloroetl~yicne ND
JORES ENVIRO3MCN I'AL
Clicnt: 11iterPhasc Environmental, Inc. Report Datc: 10/12/05 Client Address: 6200 Pcachlree Slreel JGL Ref. No.: R-41 17
Los Angcles, CA 90040 Client Ref. No.: 05253
Attn: I'aola Caldcro~i Date Sampled: 1011 1/05 Date Received: 1011 1/05
Projec(: Delplri (32485-000) Dale Analyzed: I 011 1/05 Prqject .\MI-ess: 1201 X. Magnolia. Analicim, CA Pl~ysical State: Soil Gas
EPA 8260B- Volatile Orgallics by GCIMS + Oxygenates
DPO 194- DP0 195- DP0195- DP0195- DPOI96. Practical Sample ID: SG-005 SG-022 SG-015 SG-005 SG 022 Ou""fitafio11
I,imd\
Analytes: 'is~cliloi?~iluoioii~etliane I ,2.3-Ti-ichloropro~~ii1ie I . l . i- ' : 'r i inctI iylbct~~e~~c
I ,3,S-?'rimctl1yli~c~iicnc Vinyl chlol-lde Xylcnes MTHE Ethyl-tcit-biityiellic~~ Di-~sopi.opylclhcs icrt-amylmcthyletlici icil-U~~tylalc~hnl
Surroeate Rccoverv : l)~I)iomoflrio~ orlrcthaiic Toli~ei~e-db 4-Uiornofluorobe~iieile
ND = hot Detected A - D~lulio~rv f o ~ tlrese corripound(v), first numbei Tor all other?
QC Limits 66% 60 - 140 106% 60 - 140 94% 60 - 140
JONES ENVIRONMEN'I'AL
Client: InterPhase I? i ivi ro~~ine~l ta i , tnc. Report Date: l0/12/05 Client Address: 6200 Peaclitree Street JEL ReC No.: B-4117
Los Angeles, C A 90040 Client Ref. No.: 05253
Attn: Paold Calderoil Date Sampled: 10/1 1/05 Date Received: 10/1 1/05
I'rojcct: Delphi 132486-000) Date Analyzed: 1011 1/05 1'1 ojcct Addresc: 1201 h Mag~iol ia , Aiiahell??, CA Physical State: Soil G a i
EPA 8260B- Volatile Organics by CCIMS + Oxygenates
DI'O 196- DP0196- DPO 197- DP0197- DP0197 - Practical S;unple 11): SG. 015 SG-005 SG-022 SGJ15 SG-005 Quantitation
Limitr,
Analytes: cis-I .2-Dichloroelhenc ND ND N D ND N I1 10 uP'M3 trans-I ,2-Dic11lorosthenc N D ND ND NII NII 10 L I ~ M ~ 1.2-Dichloropiopane ND ND N D N D NII 10 ug/M3 1,3-i>ichioropiopanc N D ND ND ND N 11 10 iiir/M" 2.2-Llicliloropro~1a1ie N D ND ND N D NII 10 uli'M3 I . I -ilicliloi-ojiiopei~ ELliylbcil~ciic I'rcoii 1 13 ilexach!oi-obutadiclie lsopropylbenienc 4-Isopiopyltoliicne Vcil~ylciie chloride Na!~hiIialo~c n-Propylhrnrciie Styi-eiir
l ; i .I.?-Tetmcl~loi-oel!ic~iii
1,1,2,2-Tetrac1lLoioetheiie Tcli-achloroctliylene 'ioi:iene 1.2.3-Tricli!orol>eiizenc l,2.4-l'i-ichIorohc11~~1ie I , I .l-7ricl~lomethane I . I ,2-'~ricliIoroetliai~e .I'l-icliloroetliylciic
N U = h o t Detected
N 11 N U NI) N II NII N D ND N U ND N 11 ND NU ND ND ND Nn 540 ND ND
JONES ENVIROWMENTAL
Clieot: 111teiPhaic E~~viroiimental, llic Report Date: 101 12/05 Client Addres?: 6200 l'cachtree SQcet .JEL Ref. No.: R-4117
Los Aiigelei, CA 90040 Client Ref. No.: 05253
Attn: Paold Caldeioii Date Sampled: 1011 1105 Date Received: 1011 1/05
Project: Delphi (32486-000) Date A!?alyzed: 10/11/05 Project Address: 1201 Y Mdgnol~a, Anahelill, CA Physical Sedte: Soil Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
UP0196 UP0196- DP0197. UP01 97- DP0197 - P~actical S a n t ~ l e ID: S c 0 l 5 SG-005 SG.022 SG. 015 SG 005 Ou"ntit"'io11
I,imi(a
Analytes: TrichIoroili1oso1iictlia1ii I ,2,3-Triciiloropropai~e i ,2,4-l'i-imeiliyIbe11ieiie i ,3,5-'l'si111ctl~ylbe~iie1i~
Viiiyl cliloride Xylcnes MTBE iihyl-tcl-1-biiiyicthsr Di-isopropyietbcr terl-arnylmctl~yleilie~ ten-13uiyialcoI1ol
Surroyate Recover, : QC Lirnits I I ib~o~~io f l i io~o~i~c t I~anc 112% 126% 120% 129% 117% 60 - 140 iol~ienc-d8 I 02IYo 106% 101% 105% 105% 60 - 140 4-Rio~~~ofluoiobeiizenc 89%" 90% 93%) 95% 97% 60 - 140
NU = Not Detected
10
JONES ENVIRONMENTAL
Client: InterPhdsc Envrronmenldl, Inc Report Date: 1011 2/05 Client Address: 6200 Pedchtrcc Street JEL Ref. No.: B-4117
1,os Angcles, CA 90040 Client Ref. No.: 05253
Altn: l'dold Cilldeion Dale Sampled: 1011 1/05 Date Received: 1011 1 105
Project: Delphi <32486-000) Date Analy~ed: 1011 1/05 Project Address: 1201 N Mdgiioiia, Alidhelln, CA Physical State: Soil Gas
EPA 82608- Volatile Organics by GCIMS + Ohygenates
Sample Spiked: AMBlEhl AIR
MS MSD Acceptabilily I',II ai~icici Recovery (36) Rccovery (%) RPD Range (%,I
i i -Diciilol oethylcne 89% 97% 8 0% 60 - 140 Ben7ene 118% 119% 1 0% 60 - 140 rriclilo~ oelliylenc 109% 103'/0 5 0% 60 - 140 Tolucne 126% 109% 14% 60 - 140 Chiorobenzeiic 98% 88% 11% 60 - 140
Sample Spiked: AMBIENT AIR
1h45 MSD Acceptab~lrty I'<~ra~nctc~ Itccoverv i%) Recoverv (761 RPD Rd~itzc (961
Mcthori Blank = Not Dcteclcd
MS = M<~lrix Spikz MSD = Mdtiix \pikc Duplicalc Rl'D = Relative Peicziit Differcr~cc
11
JONES Po. BOX 5387 Fuilerton. CA 92838 Eh-IJTIR;QNJIEhTTAiL (714) 449-9937
~ E S T I I Y G L4DORATORIES Fax (714) 449-9685
Turn Around Requested:
3 Immediate Anention
il Rush 72~9 f i Hours
I Sample ID I Discussion I Date / Time I
Chain-of -Custody Record
Laboiu toy Sampie Number
/ I J E L Project #
Sample Condition as Received.
Chilled II yes
I ~ " " ' w Y " ~ . : , ~, t 1 ' " " ' L . I The deliverv of samples and the siunature on , . * > i " ~:o:@.,~ ,j v?iL?,:brk- I this Chain i f ~ustody form constitutes
@ ~eiinquished by (sigi(btuie) Date 10 Reccived byzborboiatory (signature) Date authorization to perform the analyses specified
Company l ime Company l ime
above under the Terms and Conditions set foith on the back hereof.
JONES PO. Box 5387 Fullerton CA 92838
EK1781R~IX?%%~XTd2iL Fax (714) (714) 449 449-9685 9937 TEST1 YG L4RORAI'ORiES
I I 1
Ttme forth on the back hereof.
Company Time Company
Jones Environmental, Inc. Testing Laboratories
P.0. Box 5387 Fullerton, CA 92838 (714) 449-9937 FAX (714) 449-!3685
JONES ENVIRONMENTAL
LABORATORY REPORT
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 0313 1/06 JEL Ref. No.: B-4 188 Client Ref. No.: 32486-001
Attn: Paola Calderon
Project: Delphi (32486-000) Project Address: 1201 N. Magnolia, Anaheim, CA
Date Sampled: 0313 1/06 Date Received: 0313 1/06 Date Analyzed: 0313 1/06 Physical State: Soil Gas
I ANALYSES REQUESTED
I 1. EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Sampling - Soil Gas samples are collected in glass gas-tight syringes equipped with Teflon plungers. Tubing placed in the ground for soil gas sampling is purged three different times as recommended by DTSCIRWQCB regulations. This purge test determines how many purges of the soil gas tubing are needed throughout the project. One, three and seven purge volumes were analyzed to make this determination.
A tracer gas, n-Propanol, is placed at the tubing-surface interface before sampling. This compound is analyzed during the 8260B analytical run to determine if there are surface leaks into the subsurface due to improper installation of the probe. No n-Propanol was found in any of the samples reported herein.
The sampling rate was 200 cclmin using a battery operated sampling pump equipped with a rotameter. The sampling pump was calibrated at the beginning of the day using a certified flow meter. 1 purge volumes were used since this purging level gave the highest results.
Analytical - Soil Gas samples were analyzed using EPA Method 8260 that includes extra compounds required by DTSCIRWQCB (such as Freon 1 13). Instrument Continuing Calibration Verification , QC Reference Standards, Instrument Blanks and Ambient Air Blanks are analyzed every 12 hours as prescribed by the method. In addition, Matrix Spike (MS) and Matrix Spike Duplicates (MSD) are analyzed with each batch of Soil Gas samples. A duplicate sample is analyzed each day of the sampling activity.
Approval: 7
Steve ~ o n e s , > h . ~ . Laboratory Manager
Jones En*omental, Inc. Testing Laboratories
P.O. Box 5387 Fullerton, CA 9'2838 (714) 449-9937 FAX (714) @9-9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Attn: Paola Calderon
Project: Delphi (32486-000) Project Address: 1201 N. Magnolia, Anaheim, CA
Report Date: 0313 1106 JEL Ref. No.: B-4188 Client Ref. No.: 32486-001
Date Sampled: 0313 1/06 Date Received: 0313 1106 Date Analyzed: 0313 1/06 Physical State: Soil Gas
Sample ID:
Analytes: Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2- Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1 , l -Dichloroethane 1,2-Dichloroethane 1.1-Dichloroethene
EPA 8260B- Volatile Organics by G C N S + Oxygenates
Practical Quantitation
Limits Units -
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories P.O. Box 5387 Fullerton, CA 92838
(714) &9-9937 FAX (714) M999fB5 I I JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 0313 1 106 JEL Ref. No.: B-4188 Client Ref. No.: 32486-001
Attn: Paola Calderon Date Sampled: 0313 1/06 Date Received: 0313 1/06
Project: Delphi (32486-000) Date Analyzed: 0313 1/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
Sample ID:
Analytes: CIS- 1,2-D~chloroethene trans-l,2-D~chloroethene 1,2-D~chloropropane 1,3-Dtchloropropane 2,2-D~chloropropane 1,l -D~chloropropene Ethylbenzene Freon 1 13 Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene chlorlde Naphthalene n-Propy lbenzene Styrene 1,1,1,2-Tetrachloroethene 1,1,2,2-Tetrachloroethene Tetrachloroethylene Toluene 1,2,3-Trlchlorobenzene 1,2,4-Tr~chlorobenzene 1 , I , l -Trlchloroethane 1,1,2-Tr~chloroethane Trlchloroethylene
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Practical Ouantitation
Limits - Units -
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories PO. Box 5387 Fullerton, CA 92838
(714) 4C4-9-9937 FAX (714) 449-9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 0313 1 106 JEL Ref. No.: B-4188 Client Ref. No.: 32486-001
Attn: Paola Calderon Date Sampled: 0313 1/06 Date Received: 0313 1/06
Project: Delphi (32486-000) Date Analyzed: 0313 1/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
Sample ID:
Analytes: Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xy lenes MTBE Ethyl-tert-butylether Di-~sopropylether tert-amylmethylether tert-Butylalcohol
Dilution Factor
Surrogate Recovery : Dibromofluoromethane Toluene-d8 4-Bromofluorobenzene
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Practical Quantitation
Limits
QC Limits 60 - 140 60 - 140 60 - 140
Units -
ND = Not Detected
Jones Environmental, Inc. RO. Box 5387 a Fullerton, CA 93838 Testing Laboratories (714) 449-9937 . FAX (714) 449-!%335
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, C A 90040
Report Date: 0313 1 106 JEL Ref. No.: B-4188 Client Ref. No.: 32486-001
Attn: Paola Calderon Date Sampled: 0313 1/06 Date Received: 0313 1/06
Project: Delphi (32486-000) Date Analyzed: 0313 1/06 Project Address: 120 1 N. Magnolia, Anaheim, C A Physical State: Soil Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0067A- DPOO 14B- DPOO 14B- DP00 14C- DPOO 14C- Practical S a m ~ l e ID: SG-005- SG-005- SG-0 15- SG-005- SG-0 15- Ouantitation
0 1 0 1 0 1 0 1 0 1 Limits
Analytes: Benzene ND ND ND ND ND 1 0 Bromobenzene ND ND ND ND ND 1 0 Bromochloromethane ND ND ND ND ND 1 0 Bromodichloromethane ND ND ND ND ND 1 0 Bromoform ND ND ND ND ND 1 0 Bromomethane ND ND ND ND ND 1 0 n-Butylbenzene ND ND ND ND ND 1 0 sec-Butylbenzene ND ND ND ND ND 1 0 tert-Butylbenzene ND ND ND ND ND 1 0 Carbon tetrachloride ND ND ND ND ND 1 0 Chlorobenzene ND ND ND ND ND 1 0 Chloroethane ND ND ND ND ND 1 0 Chloroform ND ND ND ND ND 1 0 Chloromethane ND ND ND ND ND 10 2-Chlorotoluene ND ND ND ND ND 1 0 4-Chlorotoluene ND ND ND ND ND 10 D~bromochloromethane ND ND ND ND ND 1 0 1,2-D~bromo-3-chloropropane ND ND ND ND ND 1 0 1,2-Dlbromoethane (EDB) ND ND ND ND ND 1 0 Dlbromomethane ND ND ND ND ND 10 1,2- D~chlorobenzene ND ND ND ND ND 1 0 1,3-Dlchlorobenzene ND ND ND ND ND 1 0 1,4-D~chlorobenzene ND ND ND ND ND 10 Dlchlorod~fluoromethane ND ND ND ND ND 10 1, 1 -Dichloroethane ND ND ND ND ND 10 1,2-D~chloroethane ND ND ND ND ND 1 0 I , l -D~chloroethene ND ND ND ND ND 1 0
ND = Not Detected
Units -
Jones Environmental, Inc. Testing Laboratories P.O. Box 5387 Fullerton, CA 92838
(714) 449-9937 FAX (714) 449-9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Report Date: 0313 1/06 Client Address: 6200 Peachtree Street JEL Ref. No.: B-4188
Los Angeles, CA 90040 Client Ref. No.: 32486-001
Attn: Paola Calderon Date Sampled: 0313 1/06 Date Received: 0313 1/06
Project: Delphi (32486-000) Date Analyzed: 0313 1/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DP0067A- DPOO 14B- DPOO 14B- DPOO 14C- DPOO 14C- Practical Sample ID: SG-005- SG-005- SG-0 15- SG-005- SG-0 15- Ouantitation - units
01 0 1 0 1 0 1 0 1 Limits - Analytes: CIS- 1.2-Dichloroethene ND ND ND ND ND 10 u g / ~ ~ trans-1,2-Dichloroethene ND ND ND ND ND 10 u r n 3 1,2-Dichloropropane ND ND ND ND ND 10 ug/M3 1,3-Dichloropropane ND ND ND ND ND 10 u g / ~ ~ 2,2-D~chloropropane ND ND ND ND ND 10 ug/M3 I, I-Dlchloropropene ND ND ND ND ND 10 ug/M3 Ethy lbenzene ND ND ND ND ND 10 ug/M3 Freon 1 13 ND ND ND ND ND 10 ug/M3 Hexachlorobutadiene ND ND ND ND ND 10 ug/M3 Isopropy lbenzene ND ND ND ND ND 10 ug/M3 4-Isopropyltoluene ND ND ND ND ND 10 ug/M3 Methylene chloride ND ND ND ND ND 10 ug/M3 Naphthalene ND ND ND ND ND 10 ug/M3 n-Propy lbenzene ND ND ND ND ND 10 ug/M3 Styrene ND ND ND ND ND 10 ug/M3 1,1,1,2-Tetrachloroethene ND ND ND ND ND 10 ug/M3 1,1,2,2-Tetrachloroethene ND ND ND ND ND 10 ug/M3 Tetrachloroethy lene ND ND ND ND ND 10 ug/M3 Toluene ND ND ND ND ND 10 ug/M3 1,2,3-Tr~chlorobenzene ND ND ND ND ND 10 ug/M3 1,2,4-Tr~chldrobenzene ND ND ND ND ND 10 ug/M3 l , l , 1-Tr~chloroethane ND ND ND ND ND 10 ug/M3 1,1,2-Tr~chloroethane ND ND ND ND ND 10 ug/M3 Tnchloroethylene ND ND ND ND ND 10 ug/M3
ND = Not Detected
Jones Environmental, Inc. Testing Laboratories P.O. Box 5387 Pullerton, CA 92838
(714) 44-9-9937 PAX (714) 449-9685
JONES ENVIRONMENTAL
I LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Attn: Paola Calderon
Project: Delphi (32486-000) Project Address: 1201 N. Magnolia, Anaheim, CA
Report Date: 0313 1/06 JEL Ref. No.: B-4188 Client Ref. No.: 32486-001
Date Sampled: 0313 1/06 Date Received: 0313 1/06 Date Analyzed: 0313 1/06 Physical State: Soil Gas
EPA 8260B- Volatile Organics by G C N S + Oxygenates
Sample ID:
Analytes: Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes MTBE Ethyl-tert-butylether Dl-isopropy lether tert-amylmethylether tert-Butylalcohol
DPOO 14B- SG-005-
01
ND ND ND ND ND ND ND ND ND ND ND
DPOO 14B- SG-0 15-
01
ND ND ND ND ND ND ND ND ND ND ND
DPOO 14C- SG-005-
01
ND ND ND ND ND ND ND ND ND ND ND
DPOO 14C- SG-0 15-
01
ND ND ND ND ND ND ND ND ND ND ND
Dilution Factor 1 1 1 1 1
Practical Quantitation
Limits - 10 10 10 10 10 10 10 10 10 10 50
Units -
Surropate Recoverv : 9 C Limits Dibromofluoromethane 94% 119% 116% 117% 116% 60 - 140 Toluene-d8 95% 104% 106% 105% 104% 60 - 140 4-Bromofluorobenzene 110% 105% 105% 105% 110% 60 - 140
ND = Not Detected
Jones I$nvironmentaI, Inc. Testing Laboratories P.0. Box 5387 Fullerton, CA B838
(714) 449-9937 FAX (714) 449-9685 r
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 0313 1/06 JEL Ref. No.: B-4 188 Client Ref. No.: 32486-001
Attn: Paola Calderon Date Sampled: 0313 1/06 Date Received: 0313 1/06
Project: Delphi (32486-000) Date Analyzed: 0313 1/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
DPOO 14A- Sample ID: SG-0 15-
0 1
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
Analytes: Benzene ND Bromobenzene ND Bromochloromethane ND Bromod~chloromethane ND Bromoform ND Bromomethane ND n-Butylbenzene ND sec-Butylbenzene ND tert-Buty lbenzene ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND Chloromethane ND 2-Chlorotoluene ND 4-Chlorotoluene ND D~bromochloromethane ND 1,2-Dlbromo-3-chloropropane ND 1,2-Dlbromoethane (EDB) ND Dlbromomethane ND 1,2- D~chlorobenzene ND 1,3-Dlchlorobenzene ND 1,4-Dlchlorobenzene ND D~chlorod~fluoromethane ND 1,l -D~chloroethane ND 1,2-D~chloroethane ND 1,l-Dlchloroethene ND
DPOO 14D- DPOO 14D- DPOO 1 4A- SG-0 1 5-
02
Practical Quantitation
Limits Units -
ND = Not Detected
8
-
Jones Environmental, Inc. Testing Laboratories P.0. Box 5387 Fullerton, CA 92838
(714) 449-9937 FAX (714) 449-9685 JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Report Date: 0313 1/06 Client Address: 6200 Peachtree Street JEL Ref. No.: B-4188
Los Angeles, CA 90040 Client Ref. No.: 32486-001
Attn: Paola Calderon Date Sampled: 0313 1/06 Date Received: 0313 1/06
Project: Delphi (32486-000) Date Analyzed: 0313 1/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
EPA 8260B- Volatile Organics by GCIMS + Oxygenates
DPOO 14A- DPOO 1 4 4 DPOO 1 4 4 DPOO 14A- Practical S a m ~ l e ID: SG-0 15- SG-005- SG-015- SG-0 15- Quantitation - units
0 1 01 01 02 Limits - Analytes: cis-1,2-Dichloroethene ND ND ND ND 10 ug/M3 trans- l,2-Dlchloroethene ND ND ND ND 10 ug/M3 1,2-D~chloropropane ND ND ND ND 10 ug/M3 1,3-Dichloropropane ND ND ND ND 10 ug/M3 2,2-Dichloropropane ND ND ND ND 10 ug/M3 1,l -Dichloropropene ND ND ND ND 10 ug/M3 Ethylbenzene ND ND ND ND 10 ug/M3 Freon 1 13 ND ND ND ND 10 ug/M3 Hexachlorobutadiene ND ND ND ND 10 ug/M3 Isopropylbenzene ND ND ND ND 10 ug/M3 4-Isopropyltoluene ND ND ND ND 10 ug/M3 Methylene chloride ND ND ND ND 10 ug/M3 Naphthalene ND ND ND ND 10 ug/M3 n-Propy lbenzene ND ND ND ND 10 ug/M3 Styrene ND ND ND ND 10 ug/M3 1,1,1,2-Tetrachloroethene ND ND ND ND 10 ug/M3 1,1,2,2-Tetrachloroethene ND ND ND ND 10 ug/M3 Tetrachloroethylene ND ND ND ND 10 ug/M3 Toluene ND ND ND ND 10 ug/M3 1,2,3-Tr~chlorobenzene ND ND ND ND 10 ug/M3 1,2,4-Tr~chlorobenzene ND ND ND ND 10 ug/M3 I, I, l -Trichloroethane ND ND ND ND 10 U ~ / M ~ 1,1,2-Trichloroethane ND ND ND ND 10 u g / ~ ~ Tr~chloroethylene ND ND ND ND 10 u g / ~ ~
ND = Not Detected
9
i
Jones Environmental, Inc. Testing Laboratories P.O. Box 5387 Fullerton, CA 92838
(714) 44r9-9937 FAX (714) 449-9685
JONES ENVIRONMENTAL
LABORATORY RESULTS
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 0313 1/06 JEL Ref. No.: B-4188 Client Ref. No.: 32486-001
Attn: Paola Calderon Date Sampled: 0313 1/06 Date Received: 0313 1/06
Pr~ject: Delphi (32486-000) Date Analyzed: 0313 1/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
Sample ID:
Analytes: Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes MTBE Ethyl-tert-butylether Di-isopropy lether tert-amylmethylether tert-Butylalcohol
EPA 8260B- Volatile Organics by GC/MS + Oxygenates
DPOO 14A- DPOO 1 4 D DPOO 14D- DPOO 14A- SG-0 15- SG-005- SG-0 15- SG-0 1 5-
0 1 01 0 1 02
Dilution Factor 1 1 1 1
Surro~ate Recovery : Dibromofluoromethane . Toluene-d8 4-Bromofluorobenzene
ND = Not Detected
Practical Quantitation
Limits -
OC Limits 60 - 140 60 - 140 60 - 140
Units -
Jones Environmental, Inc. RO. Box 5387 Fullerton, CA 92838
Testing Laboratories (714) 449-9937 FAX (714) 44B-9685
JONES ENVIRONMENTAL
QUALITY CONTROL INFORMATION
Client: Interphase Environmental, Inc. Client Address: 6200 Peachtree Street
Los Angeles, CA 90040
Report Date: 0313 1 106 JEL Ref. No.: B-4188 Client Ref. No.: 32486-001
Attn: Paola Calderon Date Sampled: 0313 1/06 Date Received: 0313 1/06
Project: ~ e l ~ h i (32486-000) Date Analyzed: 0313 1/06 Project Address: 1201 N. Magnolia, Anaheim, CA Physical State: Soil Gas
--
EPA 8260B- Volatile Organics by GCMS + Oxygenates
Sample Spiked: AMBIENT AIR
Parameter MS
Recovery (%I
1,l -Dichloroethylene 103% Benzene 101% Trichloroethylene 100% Toluene 98% Chlorobenzene 97%
Sample Spiked: AMBIENT AIR
Parameter
1,l -Dichloroethylene Benzene Trichloroethylene Toluene Chlorobenzene
Method Blank = Not Detected
MS Recovery (%I
MSD Recovery (%)
MSD Recovery (%I
RPD - Acceptability
Range ('76)
Acceptability Range (%)
MS = Matrix Spike MSD = Matrix Spike Duplicate RPD = Relative Percent Difference
JONES p.0. BOX 5387 Fullerton, CA 92838
ENVIRON&IENTA4L (71 4) 449-9937
TESTlNG LABORATORlES Fax (71 4) 449-9685 Chain-of -Custody Record
The delivery of samples and the signature on this Chain of Custody form constitutes authorization to perform the analyses specified above under the Terms and Conditions set
Company Time Company Time forth on the back hereof.
JONES P.O. Box 5387 Fullerton, CA 92838
ENVIRONMENTAL (71 4) 449-9937
TESTlNG LABORATORlES Fax (714) 449-9685 Chain-of -Custody Record
Client
Project Name
QF;W*\ Project Address
I ~ I , k AG6 '
k w l k , (A Project Contact
Tb* T**L
JEL Project #
Analysis Requested
Client Project #
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Page '1, 2_ Turn Around Requested: of
0 Immediate Attention Lab Use Only Rush 24-48 Hours
Sample Condition a Rush 72-96 Hours as Rece~ved:
a Normal Chilled O yesdno
@ Mobile Lab Sealed H O no
Sample ID
W~C,I+&,SG ,oK,~
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above under the Terms and Conditions set forth on the back hereof.
Laboratory Discussion Sample Number rksISpecial Instructions
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$ 3 1 ~ 1 3 I SG X
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Bill To
Interphase Environmental, Inc. 6200 Peachtree Street Los Angeles, CA 90040 Attn: Paola Calderon
lnvoice #
313 112006 B4188 8 JONES ENVIRONMENTAL, INC. Invoice PO BOX 5387 FULLERTON, CA 92838 7 14-449-9937 FAX # 714-449-9685
L
P.O. No.
32486-001
Terms
Net 30
Project
Amount
1,500.00 0.00
Total $~,SOO.OO
Rate
1,500.00
Quantity
1 14
Thank you for
Description
HALEY & ALDRICH - DELPHI - 1201 N. Magnolia Ave., Anaheim, CA (0313 1106) Daily Mobil Lab Rate EPA 8260B+ OXYGENATES
your business.