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1 What’s important in liner and medium physical properties Roman Popil, Ph.D. [email protected] Institute of Paper Science Georgia Tech, Atlanta Presentation for a general technical audience, sponsored by AbitibiBowater Coosa Pines Al,

What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. [email protected]. Institute of Paper

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Page 1: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

1

What’s important in liner and medium physical properties

Roman Popil, [email protected]

Institute of Paper ScienceGeorgia Tech,

Atlanta

Presentation for a general technical audience, sponsored by AbitibiBowater

Coosa Pines Al,

Page 2: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

2

Who is Roman Popil ? •

Georgia Tech/IPST senior research scientist in Atlanta since 2002

Principal Investigator of Engineered Packaging research consortium program

Manager of IPST Paper Analysis lab for contract testing and research –

yes, send those

samples to me !•

Been in paper industry R&D since 1986: MacMillan Bloedel, Honeywell-measurex

PhD in plasma physics from the University of British Columbia –

Canadian, eh ?

hmm…

Page 3: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

3

Paper Physical Analysis Paper Physical Analysis Testing Services at IPSTTesting Services at IPST

Contact Roman Popil, Ph.D.Lab Manager 404 894 9722

[email protected], seminars, consulting, research…

Page 4: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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IPST@ GT Paper Analysis Lab

Page 5: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

5

What was requested for this seminar

1.

Liner and medium properties how they relate to end-use

2.

The IPST testing lab capabilities

3.

Market rends, use of recycle

4.

Lab equipment for tetsing

Page 6: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

6

What you will see in this talk ? Specifically…•

How BCT is related to ECT related to liner and medium compression strength

Why caliper and bending stiffness matter as well•

Why RCT is not a good measurement for product optimization

How SCT is better for product optimization•

How to use the SCT for product development

Some basic paper physics for background •

How the TSI with BW and SCT can be used to predict RCT anyway (if you must have RCT)

How to implement in an Autoline to predict RCT

Page 7: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

7

Why measure compression strength of medium or linerboard ?

A warehouse of stacked boxes, the customer wants the boxes to remain stacked and protect the contents

Linerboard shows a buckling pattern from vertical applied load

ECT creep test

BCT creep test

Strains increase until box panels buckle, fold and collapse –

stacks topple

What happens instead….

Page 8: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

8

United States Rule 41 –

since 1991 certificastion

for shipping containers

Old rule–

Burst(Mullen)–

Why ??

alternative rule–

ECT –

much better

The requirement for ECT allows reduction in basis weight my increasing the strength of the board

Page 9: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

9

What’s going on out there ???

Reports typical values

Reports guaranteed values

Scandinavia 1 Scandinavia 2 Spain Germany

Basis weight Basis weight Basis weight Basis weight

Moisture Moisture Moisture Moisture

Caliper Caliper

SCTCD (STFI) SCTCD (STFI) SCTCD (STFI) SCTCD (STFI)

SCTMD (STFI)

Tensile stiff. MD Tensile stiff. MD

Tensile stiff. CD Tensile stiff. CD

Burst Burst Burst Burst

Cobb Cobb Cobb Cobb

Scott bond Scott bond

ZDT

Pick resistance

Air permeance Air permeance Air permeance

Roughness Roughness

Friction Friction

Scandinavia 1 Scandinavia 2 Spain Germany

Basis weight Basis weight Basis weight Basis weight

Moisture Moisture Moisture Moisture

Caliper Caliper

SCTCD (STFI) SCTCD (STFI) SCTCD (STFI) SCTCD (STFI)

SCTMD (STFI)

Tensile stiff. MD Tensile stiff. MD

Tensile stiff. CD Tensile stiff. CD

Burst Burst Burst Burst

Cobb Cobb Cobb Cobb

Scott bond Scott bond

ZDT

Pick resistance

Air permeance Air permeance Air permeance

Roughness Roughness

Friction Friction

Tests on liners medium

Page 10: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Country RequirementBelgium Burst, FCTDenmark Burst, PunctureFEFCO Burst, ECT ,Puncture France Burst, ECTItaly Burst, FCTSouth-East Asia Burst, Basis weightSweden Burst, ECT, FCTSwitzerland Burst, ECTUSA,Canada Burst, ECT, basis weightUnited Kingdom Burst, FCTJapan Thickness, ECT,FCT

Tests on corrugated board

Page 11: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Corrugated board weight trend

From the magazine: Solutions! February 2006

143#

122#

102#

Page 12: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Compression strength is a key property for box performance

Box compression is predicted by the McKee (1963) equation:

ZDDECTCBCT CDMD4/14/3 ))(

Board edge compression strength

board bending stiffness Box perimeter

BCT in lbs

ECT in lb/in

D’s in lb-in

Z = box (length + width) x 2 in inches

Page 13: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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ECT is related to liner and medium compression strengths

)2(" mediumliner SCTSCTCECT

Compression strength of linerboard

Board take-up factor (length of medium to liner)

C flute 1.42

B flute 1.25

A flute 1.50

Compression strength of medium

Page 14: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

14

ECT Methods: Clamp vs

Neckdown vs

Waxed Edge

Sumitomo and Emerson ECT clamps, 200 grit sandpaper on jaw faces, 10 psi pressure from spring clamps, we measure 5 psi –

is that ok ?

References on T 839: Schampfer

10, 15, Eriksson 40

L&W neckdown ECT sample cutter, localizes compressive failure

References: Koning

23, Frank, 38, Eriksson 40

Page 15: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

15

Bending stiffness of corrugated board

2

2boardlinerliner htE

D

Board caliper Liner modulus

Liner caliper

linerliner tEstrengthtensilelinerboard

Page 16: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

16

Measurement of transverse shear stiffness of board

using the IPST torsion pendulum tester also requires 4 point measurement of board bending stiffness

•Ensis Papro “DST”

tester measures the twisting frequency of 4 x 1”

board specimens

•Both methods require cutting and mounting of samples

Page 17: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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How do we measure loss of transverse shear from crushing ?

developed at IPST from 1st

principles, calibrated output using weights

damped twisting motion of a board is analyzed by a computer program to find the twisting stiffness

bending stiffnesses of the test specimen are found by 4 point L&W tester

the transverse shear stiffness is calculated using an equation

Ensis Papro (New Zealand) also has developed a similar dynamic twist tester

IPST torsion pendulum

Page 18: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

18

Box performance depends on the strength of the components

Historically, strength of board and components has been measured by:

Mullen burst•

Ring Crush

Short Span Compression Test (SCT)•

Edge Crush test (waxed method) also clamp method

Page 19: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Other alternatives to measure transverse shear:

BQM from XQ Innovations Australia, measures the resonant frequency of a board vibrated along the MD, -

no sample prep required, one button press provides a number in seconds

The measured area of the board must not have anything underneath it.

MD

Page 20: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

20

Hydraulic sample clamp actuated by moving rings down

Rubber diaphragm bulges outward as glycerin gets pumped into the chamber

Electronic display of max burst pressure in psi

Note:

After burst you must

pull

the lever back to neutral, otherwise the diaphragm will burst !!

“CA”

type Mullen for testing handsheets and paper up to 100 psi. Calibration foils are 30, 65 and 110 psi

Page 21: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Ctrl+9 to start a new measurement

“PF2”

Spec no. 1 or 100

L&W Burst tester for linerboard, Calibration foils are 110 and 160 psi

Page 22: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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The line of the burst will often be along the MD

Page 23: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Burst measures a combination of properties

From theory considerations the pressure to burst a sheet is proportional to:

MD and CD tensile strengths, s –

MD stretch at failure, R diaphragm curvature

Page 24: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Burst is dependent on many factors

Page 25: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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SCT and RCT testing worldwide

USA –

Some are using only RCT

other only SCT–

Some both, SCT on low basis weight and RCT on high basis weight

Europe–

SCT dominating

Asia–

RCT almost only

Australia–

Moving from RCT to SCT

Page 26: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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TestsBasis

Weight Hard

Caliper Density

(g/m2) (microns) (g/cm3) md cd Ex (GPa) Ey (Gpa) Vxy Vyx G (Gpa)Roll 96048 14# med 65.82 144.24 0.46 0.33 0.13 4.16 1.74 0.18 0.42 0.98Roll 96044 16# med 78.16 162.74 0.48 0.55 0.17 4.7 1.13 -0.03 -0.13 0.96Roll 96038 18# med 86.36 175.6 0.49 0.79 0.28 4.42 1.71 0.14 0.36 1.03Roll 96033 20# med 94.58 183.65 0.51 0.94 0.36 4.41 2.05 0.17 0.37 1.14Doug C 26# med 125.25 252.9 0.5 2.03 0.8 1.85 4.31 0.32 0.14 1.08Roll 99004 33# med 162.69 329.6 0.49 4.23 2.11 3.64 2.05 0.18 0.32 1.07

42# Liner A 203.97 293.26 0.7 9.31 4.61 7.13 3.54 0.17 0.33 1.94

42# Liner B 209.54 294.22 0.71 8.46 2.95 7.04 2.34 0.05 0.016 1.63

42# Liner C 211.78 318.84 0.67 11.42 3.66 6.46 2.59 0.14 0.34 1.55

2 pt L&W (mNm) In-plane Ultrasonic velocities data

Some typical properties for linerboard/ medium set

Density of medium is 0.5 g/cm3

Density of linerboards are 0.7 g/cm3

Bending stiffness

Page 27: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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TestsSTFI lbf/in

(cd only) Taber units in mN-m

MD Slope (N/mm)

CD Slope (N/mm)

MD Ten.Stiff (N/mm)

CD Ten.Stiff (N/mm) md cd md cd

Roll 96048 14# med 63.606 26.723 445.336 187.124 6.04 1.66 0.73 0.162846 0.071613Roll 96044 16# med 86.484 24.94 605.6 174.643 6.8 2.82 0.93 0.276642 0.091233Roll 96038 18# med 75.5 23.057 529.48 161.583 7.96 3.53 1.43 0.346293 0.140283Roll 96033 20# med 81.783 27.492 573.532 192.661 8.8 4.52 2.15 0.443412 0.210915Doug C 26# med 112.549 41.728 788.64 292.429 13.55 12.38 6.43 1.214478 0.630783Roll 99004 33# med 130.31 60.093 912.764 421.027 19.82 26.79 14.1 2.628099 1.38321

42# Liner A 194.91 88.752 1365.885 622.111 27.12 53.56 31.65 5.254236 3.104865

42# Liner B 182.951 61.354 1281.896 429.92 22.47 50.87 17.96 4.990347 1.761876

42# Liner C 191.789 70.67 1343.845 495.546 23.36 61.03 23.6 5.987043 2.31516

Instron (tensile) dataBending Stiffness

(Taber Unit) (gmf-cm)

Some properties of linerboard/medium

Virgin unbleached 42# softwood kraft80/20 virgin/recycle

Page 28: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Box performance is predicted based on strength of the components of the board

Figure 1) Whitsitt Relationship of ECT to Composite Ring Crush

Whitsitt 1983, IPC

Related ECT to RCT:

(1)

ECT = 0.8 * (RCT1 + RCT2 + αRCTMed

) + 12

For linerboards > 42 lb/msf

(2)

ECT = 1.27 * (RCT1 + RCT2 + αRCTMed

) -

6

For linerboards < 42 lb/msf

Different equations for different basis weights…hmmm…

Page 29: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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ECT predictive models based on SCT are simpler

7.0

2

C

SCTSCTCECT mediumliner

87.5

CZtECTCBCT

Simplified McKee equation for box compression:

Take-up factor for the medium ~ 1.42

for C flute

Corrugated board caliper

Box footprint perimeter

Page 30: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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But…the linerboard industry still sells by the Ring Crush spec

manual measurement, cannot be automated

requires accurate cutting of sample –

can’t easily do handsheets

• handling of the sample

measurement of sample caliper and selection of the correct fixture insert

it is actually a combination of compression and…

bending failure, this is not good for optimization programs

Ford Highland Park plant –

Model T magneto assembly line

Page 31: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Ring Crush method

Sample and holder between compression platens –

what could go wrong ??

Page 32: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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By golly, you’re right

!!

These results are absolutely ridiculous

!!

Ohh…let’s just send the report out anyway –

ha,ha.ha!!

The trouble of RCT measurement…

RCT measurement is prone to many types of errors…some can be human

Page 33: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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The RCT vs SCT “debate”For RCT:

1.

Frank, Benjamin (Tappi J., Sept. 2007) RCT has lower coefficient of variation, correlation with ECT is better because:

a) test occurs over a larger test piece more averaging, smaller variability

b) Bending occurs in ECT and box failure

Against RCT:

2.

Seth, Fellers etc., SCT is the intrinsic compression strength of

the linerboard,

3.

Variability is inherent in the linerboard due to contaminants, defects, formation

4.

SCT is more easily optimized through wet end deification, furnish changes or refining

5.

RCT is not available on in-line automated testing machines.

6.

RCT requires more sample preparation and handling.

Page 34: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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RCT is supposed to predict BCT

BCT test

Page 35: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Then which way is the length of the test strip for CD and MD tests ?

Can you cut the strips exactly along MD or CD, should they be together or spread apart, how far apart is good enough, what do you do for small handsheets ?

Page 36: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Cutter for 15 mm wide 4 inch span samples

However, parallel edges not so critical for SCT can use a ratchet cutter for consecutively adjacent strips handy for handsheet samples

Page 37: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Got to use a different cutter for ring crush though…

Both look the same –

need to read the small label !

Page 38: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Ring Crush

Samples are 6 inches long and 12.5 mm (1/2”) wideUse different center “island”

inserts depending on the caliper for the specimen

Page 39: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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I don’t know about you, but I am wearing gloves to protect my nice new nail job !

Gloves ?? Nah…What for ?!

Calm cool technicians required with dry hands

Page 40: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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IPST data ex Mike Schaepe I sure hope you like my

data !

What’s this ??

Page 41: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Short Span Compression Test is SCT

STFI = SVENSKA TRÄFORSKNINGSINSTITUTET (Swedish Forest Products Research Laboratory , now renamed “Inventia”)

Test method was developed by Christer Fellers in the

late 1970’s

The short span compression test is not “STFI”

Christer gets another award from Jeffrey Suhling

Page 42: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Fun Fact (from a student presentation

)•

Compression tests are all called *CT, e.g. FCT, ECT, BCT, but SCT is rather new…

Many call the short span compression test SCT as “STFI”, pronounced “stiffy”

Why is this a bad

idea ??•

Answer: ________

Unfortunately, I can see your “STFI”

is way down today…

Ahem.. um, ah…

my what

?!!!..

Page 43: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Corrugated medium comparison – SCT and RCT

ECTSCT

RCT

ECT increased in accordance with SCT results.RCT predicted ECT decrease.

Conclusion:SCT is better suited for low grammage corrugated medium than RCT.

IPC, Whitsitt 1985

Page 44: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Note the difference between STFI and RCT (about 2 X)

At very high basis weights and calipers, get slip: more surface compression

SCT and RCT comparison

Page 45: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Effect of grammage and density

RCT

Christer Fellers’

slide

Increased buckling for lightweights decreases RCT with density

Page 46: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Sample strip

Pressurized clamps prevent slipping

CD

0.7 mm gap between clamping jaws

Page 47: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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The L&W SCT On-board test sample moisture correction is available, based on resistance measurement requires calibration that is furnish dependent –

unused at IPST since all samples are conditioned

Instrument is checked periodically using a selected standard paper sample kept in a drawer with its data history for instant comparison

For mill QC use –

samples must be conditioned to 50% RH equilibrium…fastest way cut 6”

x 15mm strips, place in microwave oven for 10 seconds, hang separated strips in a draft for ~ 2 hours, then

test

Simple strip insertion, one button operation

Strip edge parallelism not critical

Page 48: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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After many years of service…Thermal dot matrix printer dots fades,

rollers wear out

Green LED read-out fades,

missing dots

Keyboard button contacts become

erratic or fail

Unit must be in a conditioned lab, if taken into humid environments (e.g. mill floor) electronics will be affected

Page 49: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Shows that specific STFI is independent of basis weight and is a property of the fiber consolidation

SCT works because over the 0.7 mm test span there is no bending

Euler buckling curves

Page 50: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

50

Real compressive failure is marked by material breakdown and occurs when the column height prohibits buckling

When testing a strip, the crease is often hard to see –

looks like nothing has happened

Page 51: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

51

STFI or SCT (Short Span Compression Test) is considered to be the intrinsic compression test strength for linerboard –

this is how you can understand

what affects it through a “Page equation”

model for SCT:

Note the dependence on fiber modulus (fibril angle,species)

and sheet density (wet pressing)

Can affect this by low consistency

refining

Page 52: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Effects of Processes on Compressive strength using SCT

Excerpted from “Paper Physics”

by Niskanen

Page 53: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Shows the only way to change SCT is to change the furnish and beating level of fibers

Recall the Shallhorn Gurnagul model for SCT…

Graphs excerpted from the Handbook of Physical Testing

Using SCT

Page 54: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Ring Crush is affected by the bending stiffness and the caliper of the test specimen so is not a true compression test

Note the dependence on Taber and caliper in this empirical relationship

Note that Taber is a bending stiffness measurement

Tappi Journal 1998

Page 55: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Why the bending stiffness of linerboard mattersVideo observation of ECT tests show:a) No out-of-plane buckling at higher basis weightsb) Slight buckling at low basis weights for A and C flute boards

Schaepe and Popil2006

Buckling of linerboard

facings occurs in A and C flute, more so for lightweights

Page 56: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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We can calculate the buckling load for linerboard using MD and CD Bending Stiffness

Taber has historically been used for 2 point bending stiffness of liners and medium, Taber measures bending moment

M not stiffness EI/b !

We did a lot of work with an L&W 2 point stiffness tester, a more straightforward design, cross calibrated instruments with stainless steel shims.

From linear elasticity theory, the conversion factor from Taber moment M to stiffness D is:

67.13

M

bLM

bEID

This means that Taber x 1.67 bending stiffness !!

Page 57: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

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Wet pressing increases SCT but lowers bending stiffness

12/3EtD

As density increases SCT increases but bending stiffness goes down

what is going on is that the caliper decreases lowering D

STFI vs density

200 gsm: y = 24.501Ln(x) + 42.411R2 = 0.9949

300 gsm y = 40.655Ln(x) + 61.97R2 = 0.9999

160 gsm: y = 12.587Ln(x) + 25.411R2 = 0.9895

100 gsm: y = 10.107Ln(x) + 19.315R2 = 0.954

5

10

15

20

25

30

35

40

45

50

0.35 0.45 0.55 0.65 0.75 0.85 0.95

Density gsm

STFI

lb/in

Lab data using kraft handsheets pressed to various densities

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58

Wet pressing increases SCT but lowers bending stiffness

0

5

10

15

20

25

30

35

40

0.35 0.45 0.55 0.65 0.75 0.85

Density (g/cm3)

Geo

met

ric m

ean

bend

ing

stiff

ness

(mN

-m)

10 gsm150 gsm200 gsm300 gsm 12/3EtD

As density increases SCT increases but bending stiffness goes down

what is going on is that the caliper decreases lowering D

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59

Wet pressing increases density increases SCT but decreases

bending stiffness

12

3EtD

For linerboard: Modulus increases with wet pressing from increased bonding

Linerboard caliper

ESCT

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60

3

4

5

6

7

8

9

0.25 0.35 0.45 0.55 0.65 0.75 0.85 0.95 1.05

Density (g/cm3)

ECT

(kN

/m)

100 gsm160 gsm200 gsm

Predicting ECT for handsheets using SCT and bending stiffness relationships to determine the ECT as a function of density for handsheets for various basis weights as specified.

More buckling occurs with increased wet pressing so this limits ECT

The ECT buckling model is used to predict the optimum liner density for ECT

The ECT buckling model predicts the optimal density for 160 gsm liner single wall C flute to be 0.75 g/cm3

Note the Peak ECT occurs here

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61

How can RCT and SCT be related ? (current IPST ongoing research)

RCT is a combination of bending and compression failure

SCT is compression failure only•

McKee reasoning for plate failure as a combination of compression and bending takes the empirical form:

)1(`)()( bb loadBucklingstrengthnCompressioloadfailurenCompressio

Related to the bending stiffness which depends on the structure e.g, round tube, plate, flute shape, etc.

Page 62: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

62

Buckling load for a thin walled tube:

rtE

cr

)1(3 2

r = 24.2. mm

t = 0.3 mm

l

= 6 mm

“E x t ” is tensile stiffness

For this formula to hold need to fit one half wave into the tube height:

mmtrml 7.472.1

Yep, specimen is high enough to buckle -

so we can use this formula for buckling of the RCT sample

From Timoshenko and Gere:

Page 63: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

63

We can get a measure of the ring buckling load using the L&W TSI

By measuring the speed of sound in paper, basis weight and the caliper we can estimate the tensile stiffness

The tensile stiffness is directly proportional to the buckling load of a thin walled tube.

This can all be done instantly and automatically…

Page 64: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

64

Combining measurements to predict RCT

The Autoline for linerboard will have SCT, caliper, basis weight, and a TSI –

these measurements can be combined to fit an RCT model, the model can be programmed into the Autoline software to provide a

calculated estimated equivalent value for RCT …

But first let’s review a few concepts before we see how to do this…

Page 65: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

65

MD

ZD

CD

Paper consists of 50 to 30% air and a network of bonded fibers aligned predominantly along the MD –

machine direction

Fibers: former wood cells, typically 1 –

3 mm long, 50 microns wide

PAPER STUCTURE - OVERSIMPLIFIED

SEM surface

SEM x-section

For box making applications, only CD compression is considered

Page 66: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

66

Paper as a 3D spring:

CDCDCD E MDMDMD E

In 1D we have Hooke’s law for the Force F to move a spring distance x

F = k x

For a 3D solid slab such as paper, we have by analogy, (actually a good physical analogy is the common cellulosic cleaning sponge) the pressure or stress

σ

required to displace the solid by a strain ε

for each principal direction:

ZDZDZD E

The E’s here are the elastic moduli for each of the 3 directions

The ε’s are the strains i.e. relative changes in displacement : ∆ℓ

/ ℓ

0

Page 67: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

67

To a good approximation:

E’s and sound speed

22112

2

22112

2

)1(

)1(

CDCDCD

MDMDMD

VVE

VVE

Moduli (MD or CD) = apparent density x velocity squared

We can measure the speed of sound propagating along the plane of

the sheet using a pair of transducers:

timeVolts

Transmitted pulse Received pulse

?

Page 68: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

68

Bimorph “paddle”

transducers apart for “far”

readingClose up of transducers for “near”

reading in shear mode, transducers are rotated for longitudinal mode

IPC 1970’s Robot Arm difference method technique

From successive pairs of measurements a 2 distances get Poisson ration, and shear modulus –

15 minutes per test

Measuring sound speed in paper

Page 69: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

69

IPST Robot Arm – from the 1980’s

4 user selectable measuring stations

Robot arm end effector rotates for polar plots

Takes an hour for a 2 degree resolution plot

You know, I’d rather not wait an hour

for just one polar plot, thanks !!

A typical lab tech’s response

Lars Ingman

marketed a version through “Robotest”

Sonisys

now has an updated version called “UTI”

Page 70: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

70

L&W TSI comes to the rescue

8 pairs of transducers fixed distance, head comes down at a higher pressure for basis weights > 100 gsm

Polar plot and V2 produced in 6 seconds but:

Might be influenced by low density and high roughness to produce

underestimates of V2

So…correlation of V2

from TSI vs tensile stiffness has to be verified for particular sample sets

Page 71: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

71

L&W TSI measures VCD2

= TSI_CD

CDTSIBWtVt

BWtVtECD _22

For the buckling load part in the RCT model we need E x tThis is the same as:

So the buckling load in an RCT model becomes:

CDTSIBWCrtE

cr _)1(3 2

With C’’

being constant since r and the Poisson ratio’s do not change appreciably

Page 72: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

72

Modeling RCT in terms of combined compression and

buckling strengths

bb EtSCTCRCT 1)()(•Based on McKee reasoning for the compression strength of a plate

but instead replacing the buckling load of a plate by that for a thin cylindrical ring (e.g. Roark’s formulas) where:

•Pcr is the buckling load for a ring is proportional to Et

•Et = tensile stiffness ( modulus E times sheet thickness t) = constant x (v2) x basis weight

•Can get v^2 ( specific stiffness) from L&W TSI output

• so…

can now get an RCT value by measuring SCT, BW and TSI_CD

The model for ring crush is proposed as:

Page 73: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

73

Ultrasonic tensile vs Instron N/mm

y = 1.7524x - 73.305R2 = 0.9829

0

200

400

600

800

1000

1200

1400

0 200 400 600 800 1000

Series1Linear (Series1)

This shows that TSI * BW = Et when E x t is measured by the Instron as tensile stiffness

TSI x

BW

(N

/mm

)

Instron tensile stiffness (N/mm)

Ultrasonically measured values are always higher than mechanical equivalents

Page 74: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

74

IPS

T in

-pla

ne s

peci

fic s

tiffn

ess

(km

/s)2

TSI index

TSI vs IPST V^2

y = 1.0821x - 0.1875R2 = 0.9782

2

4

6

8

10

12

14

2 3 4 5 6 7 8 9 10 11 12

Series1Linear (Series1)

Sample ID

42 lb kraft liner

33 lb medium

26 lb medium

56 lb liner WC

16 lb medium

18 lb medium

OCC 42lb liner

20 lb medium

3m mylar

yellow copy

inkjet mylar

WAM 33#

blotter

TSI checkout with IPST Robot

CD valuesMD values

Correlation looks ok for a variety of various liners medium, copy paper and plastic film

Page 75: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

75

C = 0.349467355b = 0.362403921

STFI (lb/in)) Ring Crush (lb) ET Model error^218.6 61.48 688.8574233 65.02243389 12.54883787

22.43 76.06 837.696652 78.83173899 7.68253705622.069 101.15 1066.474227 91.41300701 94.8090325230.813 118.4 1172.550736 109.5963138 77.5048899231.231 122.4 1350.911968 120.5385411 3.46502940433.467 129.6 1378.359952 125.192706 19.4242404446.08 158.41 1640.9707 157.1106897 1.688207376

35.829 126.49 1421.312619 130.8608967 19.1047379153.631 161.49 1652.173551 166.7145053 27.2954553226.209 98.46 1136.489074 101.3153034 8.15275758840.786 160.2 1556.65121 145.3418956 220.763265321.702 74.34 875.2949972 80.10608446 33.2477300634.443 125.36 1285.666476 121.0113364 18.9108747816.051 61.98 680.5922305 61.16781024 0.659652228.64 98.77 1063.086323 100.264588 2.233793158

22.178 87.82 961.1309916 85.70075308 4.49120749914.288 39 661.461174 57.58578752 345.431497717.155 65.7 882.722197 73.96061475 68.237756097.539 15.15 281.03 26.46449812 128.01786768.599 21.9 331.8952 30.86274479 80.33079429.981 25.47 394.284 36.35707584 118.5284204

14.975 44.99 534.2069 51.11413764 37.505061822.193 74.09 747.9719 73.05644945 1.068226737

1331.101873 sum error RSQ= 0.980453481

model:

RCT = (STFI)^b(Et)^(1-b)

Et = TSIxBW

C = 0.35, b = 0.36

q38

This is the spreadsheet analysis using Excel “Solver”

to fit the model RCT = C x (SCT)b

x (Et)(1-b)

i.e., a “McKee”

style equation for RCT using a combination of compression strength (SCT) and buckling load ( ~ Et which in turn, is TSI x BW)

Data is for a series of linerboards and medium of a wide range of basis weights

64.036.0 )()(35.0 CDTSISCTRCT

Model to calculate an equivalent RCT

Got data ? Send it to me to analyze ! [email protected]

Page 76: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

76

Ring Crush vs SCT

y = 3.591x - 1.3082R2 = 0.9371

y = 0.8825x + 12.246R2 = 0.9805

0

50

100

150

200

250

0 50 100 150 200

SCT (lb/in) or 0.35 SCT.36(TSI).64

Rin

g C

rush

(lb/

6 in

) Ring Crush (lb)

Bending model

Linear (Ring Crush(lb))Linear (Bendingmodel )

This shows that the r2

improves from 0.94 to 0.98 if we use a non-linear bending model for RCT: the value is that we get a better prediction for RCT using SCT, BW and TSI_CD

MSE linear = 2.26 lbs

MSE bending model = 1.59 lbs

64.036.0 )()(35.0 CDTSISCTRCT

Page 77: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

77

Will this always work ?•

If just using Et = D x (TSI_CD) x BW the assumption of stiffness being proportional to failure may not hold if:

1.

stress-strain curve is changed by increased or decreased ductility of paper

2.

addition of filler, starch, impregnation with polymer, radical change in fiber species

Compression load

Compression Displacement

TSI_CD

RCT 1 –

linerboard

RCT 2 –

waxed linerboard

RCT –

refined linerboard

Comparable

stiffnesses but different failure loads can occur…

Page 78: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

78

Relevance to Industry, you, me, the world and everything else..

Current requirement to address the manufacture of recyclable boxes for food and produce transport meeting FDA specs must be produced locally –demand cannot decline with a growing population.

Chinese corrugated production volume surpassed US already in 2008Overseas product and shipping containers are not a threat to this market: food transport and packaging

Mullens here are bogus

Doublewall BC box for furniture shipping Single wall B flute box for

PC monitor

Page 79: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

79

Corrugated is not going away

Thank you:Abitibi-Bowater

Awwright !!Let’s make boxes !!

Yeeaahh!!

Hasta la Vista, RCT

!!

Questions, problems, testing, research…

[email protected]

Page 80: What’s important in liner and medium physical properties · 1 What’s important in liner and medium physical properties Roman Popil, Ph.D. Roman@gatech.edu. Institute of Paper

80

Thank you

“serving the paper industry since 1929…to survive is to do research, to thrive is to implement…”