water reports/ACZ Level 2...BD[ Laboratories, Inc. 2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 Analytical Report SPF Water Engineering 300 E. Mallard Drive, Suite

BD[ Laboratories, Inc.2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493

Analytical

Report

SPF Water Engineering

300 E. Mallard Drive, Suite 350

Boise, ID 83706

ACZ Project ID: L17362

Jason Thompson:

Enclosed are the analytical results for sample(s) submitted to ACZ Laboratories, Inc. (ACZ) on March 21, 2014. This project has been assigned to ACZ's project number, L17362. Please reference this number in all future inquiries.

All analyses were performed according to ACZ's Quality Assurance Plan. The enclosed results relate only to the samples received under L17362. Each section of this report has been reviewed and approved by the appropriate Laboratory Supervisor, or a qualified substitute.

Except as noted, the test results for the methods and parameters listed on ACZ's current NELAC certificate letter (#ACZ) meet all requirements of NELAC.

This report shall be used or copied only in its entirety. ACZ is not responsible for the consequences arising from the use of a partial report.

All samples and sub-samples associated with this project will be disposed of after May 11, 2014. If the samples are determined to be hazardous, additional charges apply for disposal (typically $11/sample). If you would like the samples to be held longer than ACZ's stated policy or to be returned, please contact your Project Manager or Customer Service Representative for further details and associated costs. ACZ retains analytical raw data reports for ten years.

If you have any questions or other needs, please contact your Project Manager.

Jason Thompson

April 11, 2014

Project ID: Calico 1st Quarter 2014 Sampli



Boise, ID 83706

Crystal Jensen

Report to: Bill to:

Page 1 of 63L17362-1404111040


Case

Narrative



April 11, 2014

Sample Receipt

Sample Analysis

Holding Times

Text10:ACZ Laboratories, Inc. (ACZ) received 8 ground water samples from SPF Water Engineering on March 21, 2014. The samples were received in good condition. Upon receipt, the sample custodian removed the samples from the cooler, inspected the contents, and logged the samples into ACZ's computerized Laboratory Information Management System (LIMS). The samples were assigned ACZ LIMS project number L17362. The custodian verified the sample information entered into the computer against the chain of custody (COC) forms and sample bottle labels.

Text10:These samples were analyzed for inorganic parameters. The individual methods are referenced on both the ACZ invoice and the analytical reports. The extended qualifier reports may contain footnotes qualifying specific elements due to QC failures. In addition the following has been noted with this specific project:

Some of the dissolved Cobalt values exceed the corresponding total values for project L17362. In some cases, RPDs between dissolved and total values exceed the standard acceptance limit of 20%. Samples were re-analyzed for verification, and results for both parameters were confirmed. This is a consistent anomaly with these sample types, and discrepancies may be attributed to a matrix or field sampling issue.

Text10:Any analyses not performed within EPA recommended holding times have been qualified with an "H" flag.


REPAD.03.06.05.01 Page 2 of 63L17362-1404111040

ACZ Sample ID: L17362-01

Sample ID: PW-4

Sample Matrix: Ground Water


Project ID: Calico 1st Quarter 2014 Sa


Inorganic Analytical

Results

Date Sampled: 03/18/14 10:50

Date Received: 03/21/14

Parameter EPA Method Result Units MDLQual AnalystDatePQL

Inorganic Prep

XQDilution

Cyanide, total M335.4 - Manual Distillation bsu03/28/14 15:31

Cyanide, WAD SM4500-CN I- distillation mss203/27/14 15:12

Phosphorus, total M365.1 - Auto Ascorbic Acid Digestion

bsu04/04/14 12:28

Total Hot Plate Digestion

M200.2 ICP jjc03/27/14 12:01


M200.2 ICP-MS scp04/07/14 14:38

REPIN.02.06.05.01 * Please refer to Qualifier Reports for details.

Page 3 of 63L17362-1404111040


Sample ID: PW-4






Results

Date Sampled: 03/18/14 10:50



Metals Analysis

XQDilution

Aluminum, dissolved M200.7 ICP 0.11 mg/L 0.2B jjc0.03 03/25/14 10:141

Aluminum, total M200.7 ICP 6.11 mg/L 0.2 jjc0.03 03/28/14 11:231

Antimony, dissolved M200.8 ICP-MS mg/L 0.002U las0.0004 04/02/14 0:141

Antimony, total M200.8 ICP-MS mg/L 0.002U las0.0004 04/01/14 20:211

Arsenic, dissolved M200.8 ICP-MS 0.0127 mg/L 0.001 las0.0002 04/02/14 0:141

Arsenic, total M200.8 ICP-MS 0.0148 mg/L 0.001 las0.0002 04/01/14 20:211

Barium, dissolved M200.7 ICP mg/L 0.02U jjc0.003* 03/25/14 10:141

Barium, total M200.7 ICP 0.017 mg/L 0.02B jjc0.003 03/28/14 11:231

Beryllium, dissolved M200.8 ICP-MS mg/L 0.0003U las0.00005 04/02/14 0:141

Beryllium, total M200.8 ICP-MS 0.00032 mg/L 0.0003 las0.00005 04/01/14 20:211

Bismuth, dissolved M200.7 ICP mg/L 0.2U jjc0.04* 03/25/14 10:141

Bismuth, total M200.7 ICP mg/L 0.2U aeb0.04* 03/28/14 15:171

Boron, dissolved M200.7 ICP 0.12 mg/L 0.05 jjc0.01* 03/25/14 10:141

Boron, total M200.7 ICP 0.14 mg/L 0.05 jjc0.01 03/28/14 11:231

Cadmium, dissolved M200.8 ICP-MS mg/L 0.0005U las0.0001 04/02/14 0:141

Cadmium, total M200.8 ICP-MS mg/L 0.0005U las0.0001 04/01/14 20:211

Calcium, dissolved M200.7 ICP 7.3 mg/L 0.5 jjc0.1 03/25/14 10:141

Calcium, total M200.7 ICP 11.6 mg/L 0.5 jjc0.1 03/28/14 11:231

Chromium, dissolved M200.8 ICP-MS mg/L 0.002U las0.0005 04/02/14 0:141

Chromium, total M200.8 ICP-MS mg/L 0.002U las0.0005 04/01/14 20:211

Cobalt, dissolved M200.8 ICP-MS 0.00025 mg/L 0.0003B las0.00005 04/02/14 0:141

Cobalt, total M200.8 ICP-MS 0.00028 mg/L 0.0003B las0.00005 04/01/14 20:211

Copper, dissolved M200.8 ICP-MS mg/L 0.003U las0.0005 04/02/14 0:141

Copper, total M200.8 ICP-MS 0.0007 mg/L 0.003B las0.0005 04/01/14 20:211

Gallium, dissolved M200.7 ICP mg/L 0.5U jjc0.1* 03/25/14 10:141

Gallium, total M200.7 ICP mg/L 0.5U jjc0.1* 03/28/14 11:231

Iron, dissolved M200.7 ICP 0.25 mg/L 0.05 jjc0.02 03/25/14 10:141

Iron, total M200.7 ICP 6.06 mg/L 0.05 jjc0.02 03/28/14 11:231

Lead, dissolved M200.8 ICP-MS mg/L 0.0005U las0.0001 04/02/14 0:141

Lead, total M200.8 ICP-MS 0.0048 mg/L 0.0005 las0.0001 04/01/14 20:211

Lithium, dissolved M200.7 ICP 0.081 mg/L 0.04 jjc0.008* 03/25/14 10:141

Lithium, total M200.7 ICP 0.094 mg/L 0.04 jjc0.008 03/28/14 11:231

Magnesium, dissolved M200.7 ICP 0.3 mg/L 1B jjc0.2 03/25/14 10:141

Magnesium, total M200.7 ICP 1.3 mg/L 1 jjc0.2 03/28/14 11:231

Manganese, dissolved M200.8 ICP-MS 0.0357 mg/L 0.003 las0.0005 04/02/14 0:141

Manganese, total M200.8 ICP-MS 0.0640 mg/L 0.003 las0.0005 04/01/14 20:211

Mercury, dissolved M1631, Atomic Fluorescence ng/L 0.5U las0.2 04/01/14 16:211

Mercury, total M1631, Atomic Fluorescence 4 ng/L 3 las1 03/31/14 12:275

Molybdenum, dissolved M200.8 ICP-MS 0.0105 mg/L 0.003 las0.0005 04/02/14 0:141

Molybdenum, total M200.8 ICP-MS 0.0109 mg/L 0.003 las0.0005 04/01/14 20:211

Nickel, dissolved M200.8 ICP-MS mg/L 0.003U las0.0006 04/02/14 0:141

Nickel, total M200.8 ICP-MS 0.0007 mg/L 0.003B las0.0006 04/01/14 20:211

Potassium, dissolved M200.7 ICP 0.7 mg/L 1B jjc0.2 03/25/14 10:141


Page 4 of 63L17362-1404111040


Sample ID: PW-4






Results

Date Sampled: 03/18/14 10:50


Potassium, total M200.7 ICP 1.1 mg/L 1 jjc0.2 03/28/14 11:231

Scandium, dissolved M200.7 ICP mg/L 0.5U jjc0.1* 03/25/14 10:141

Scandium, total M200.7 ICP mg/L 0.5U jjc0.1* 03/28/14 11:231

Selenium, dissolved M200.8 ICP-MS mg/L 0.0003U las0.0001 04/02/14 0:141

Selenium, total M200.8 ICP-MS mg/L 0.0003U las0.0001 04/01/14 20:211

Silver, dissolved M200.8 ICP-MS mg/L 0.0003U las0.00005 04/02/14 0:141

Silver, total M200.8 ICP-MS mg/L 0.0003U las0.00005 04/01/14 20:211

Sodium, dissolved M200.7 ICP 158 mg/L 1 jjc0.2 03/25/14 10:141

Sodium, total M200.7 ICP 177 mg/L 1 jjc0.2 03/28/14 11:231

Strontium, dissolved M200.7 ICP 0.035 mg/L 0.03 jjc0.005 03/25/14 10:141

Strontium, total M200.7 ICP 0.060 mg/L 0.03 jjc0.005 03/28/14 11:231

Thallium, dissolved M200.8 ICP-MS mg/L 0.0005U las0.0001 04/02/14 0:141

Thallium, total M200.8 ICP-MS mg/L 0.0005U las0.0001 04/01/14 20:211

Tin, dissolved M200.8 ICP-MS mg/L 0.0005U las0.0001* 04/02/14 0:141

Tin, total M200.8 ICP-MS 0.0004 mg/L 0.0005B msh0.0001* 04/09/14 19:381

Titanium, dissolved M200.7 ICP mg/L 0.03U jjc0.005 03/25/14 10:141

Titanium, total M200.7 ICP 0.029 mg/L 0.03B jjc0.005 03/28/14 11:231

Uranium, dissolved M200.8 ICP-MS mg/L 0.0005U las0.0001 04/02/14 0:141

Uranium, total M200.8 ICP-MS 0.0019 mg/L 0.0005 las0.0001 04/01/14 20:211

Vanadium, dissolved M200.8 ICP-MS mg/L 0.001U las0.0002 04/02/14 0:141

Vanadium, total M200.8 ICP-MS 0.0007 mg/L 0.001B las0.0002 04/01/14 20:211

Zinc, dissolved M200.7 ICP mg/L 0.05U jjc0.01 03/25/14 10:141

Zinc, total M200.7 ICP 0.01 mg/L 0.05B jjc0.01 03/28/14 11:231


Page 5 of 63L17362-1404111040


Sample ID: PW-4






Results

Date Sampled: 03/18/14 10:50



Wet Chemistry

XQDilution

Alkalinity as CaCO3 SM2320B - Titration

Bicarbonate as CaCO3

177 mg/L 20 dcw2 03/26/14 0:001

Carbonate as CaCO3 4 mg/L 20B dcw2 03/26/14 0:001

Hydroxide as CaCO3 mg/L 20U dcw2 03/26/14 0:001

Total Alkalinity 182 mg/L 20 dcw2* 03/26/14 0:001

Chloride M300.0 - Ion Chromatography 40.0 mg/L 12.5 tcd2.5* 03/26/14 19:185

Conductivity @25C SM2510B 841 umhos/cm 10 dcw1 03/26/14 17:441

Cyanide, total M335.4 - Colorimetric w/ distillation mg/L 0.01U mpb0.003* 03/31/14 15:210.5

Cyanide, WAD SM4500-CN I-Colorimetric w/ distillation

mg/L 0.01U mpb0.003* 03/27/14 16:490.5

Fluoride M300.0 - Ion Chromatography 1.86 mg/L 2.5B tcd0.5* 03/26/14 19:185

Hardness as CaCO3 SM2340B - Calculation 20 mg/L 7 calc1 04/11/14 8:13

Nitrate/Nitrite as N M353.2 - H2SO4 preserved mg/L 0.1U pjb0.02 03/28/14 22:531

Nitrogen, ammonia M350.1 - Automated Phenate 0.10 mg/L 0.5B tcd0.05* 03/27/14 16:051

pH (lab) SM4500H+ B

pH 8.4 units 0.1H dcw0.1 03/26/14 0:001

pH measured at 21 C 0.1 dcw0.1 03/26/14 0:001

Phosphorus, total M365.1 - Auto Ascorbic Acid (digest)

0.05 mg/L 0.05 pjb0.01* 04/05/14 13:461

Residue, Filterable (TDS) @180C

SM2540C 490 mg/L 40 id20* 03/25/14 11:272

Residue, Non-Filterable (TSS) @105C

SM2540D 190 mg/L 80 enb20* 03/25/14 12:064

Sulfate M300.0 - Ion Chromatography 133 mg/L 12.5 tcd2.5 03/26/14 19:185


Page 6 of 63L17362-1404111040


Sample ID: GW-4






Results

Date Sampled: 03/18/14 11:40



Inorganic Prep

XQDilution




bsu04/04/14 12:43


M200.2 ICP jjc03/27/14 12:12


M200.2 ICP-MS las03/27/14 11:58


Page 7 of 63L17362-1404111040


Sample ID: GW-4






Results

Date Sampled: 03/18/14 11:40



Metals Analysis

XQDilution

Aluminum, dissolved M200.7 ICP 0.06 mg/L 0.2B jjc0.03 03/25/14 10:231

Aluminum, total M200.7 ICP 1.09 mg/L 0.2 jjc0.03* 03/28/14 11:261





Barium, dissolved M200.7 ICP mg/L 0.02U jjc0.003* 03/25/14 10:231



Beryllium, total M200.8 ICP-MS 0.00014 mg/L 0.0003B las0.00005 04/01/14 20:251










Chromium, total M200.8 ICP-MS mg/L 0.002U las0.0005 04/01/14 20:251

Cobalt, dissolved M200.8 ICP-MS 0.00047 mg/L 0.0003 las0.00005 04/02/14 0:241



Copper, total M200.8 ICP-MS mg/L 0.003U las0.0005 04/01/14 20:251



Iron, dissolved M200.7 ICP mg/L 0.05U jjc0.02 03/25/14 10:231

Iron, total M200.7 ICP 0.41 mg/L 0.05 jjc0.02* 03/28/14 11:261





Magnesium, dissolved M200.7 ICP mg/L 1U jjc0.2 03/25/14 10:231

Magnesium, total M200.7 ICP mg/L 1U jjc0.2 03/28/14 11:261




Mercury, total M1631, Atomic Fluorescence 0.8 ng/L 0.5 las0.2 03/31/14 12:321




Nickel, total M200.8 ICP-MS mg/L 0.003U las0.0006 04/01/14 20:251

Potassium, dissolved M200.7 ICP 0.4 mg/L 1B jjc0.2 03/25/14 10:231


Page 8 of 63L17362-1404111040


Sample ID: GW-4






Results

Date Sampled: 03/18/14 11:40


Potassium, total M200.7 ICP 0.7 mg/L 1B jjc0.2 03/28/14 11:261




Selenium, total M200.8 ICP-MS mg/L 0.0003U las0.0001 04/01/14 20:251





Strontium, dissolved M200.7 ICP 0.019 mg/L 0.03B jjc0.005 03/25/14 10:231

Strontium, total M200.7 ICP 0.029 mg/L 0.03B jjc0.005 03/28/14 11:261




Tin, total M200.8 ICP-MS mg/L 0.0005U las0.0001* 04/01/14 20:251




Uranium, total M200.8 ICP-MS 0.0003 mg/L 0.0005B las0.0001 04/01/14 20:251


Vanadium, total M200.8 ICP-MS 0.0005 mg/L 0.001B las0.0002 04/01/14 20:251


Zinc, total M200.7 ICP mg/L 0.05U jjc0.01 03/28/14 11:261


Page 9 of 63L17362-1404111040


Sample ID: GW-4






Results

Date Sampled: 03/18/14 11:40



Wet Chemistry

XQDilution



162 mg/L 20 dcw2 03/26/14 0:001








mg/L 0.01U mpb0.003* 03/27/14 16:500.5

Fluoride M300.0 - Ion Chromatography 2.23 mg/L 0.5 tcd0.1* 03/26/14 20:121



Nitrogen, ammonia M350.1 - Automated Phenate mg/L 0.5U tcd0.05* 03/27/14 16:061

pH (lab) SM4500H+ B

pH 8.5 units 0.1H dcw0.1 03/26/14 0:001



0.07 mg/L 0.05 pjb0.01* 04/05/14 13:491


SM2540C 260 mg/L 20 id10* 03/25/14 11:291


SM2540D 33 mg/L 20 enb5* 03/25/14 12:101

Sulfate M300.0 - Ion Chromatography 88.3 mg/L 2.5 tcd0.5 03/26/14 20:121


Page 10 of 63L17362-1404111040


Sample ID: 59766






Results

Date Sampled: 03/18/14 12:40



Inorganic Prep

XQDilution




bsu04/04/14 12:50


M200.2 ICP-MS scp* 04/07/14 14:48


M200.2 ICP jjc03/27/14 12:24


Page 11 of 63L17362-1404111040


Sample ID: 59766






Results

Date Sampled: 03/18/14 12:40



Metals Analysis

XQDilution

Aluminum, dissolved M200.7 ICP mg/L 0.2U jjc0.03 03/25/14 10:261



Antimony, total M200.8 ICP-MS 0.0006 mg/L 0.002B las0.0004 04/01/14 20:281



Barium, dissolved M200.7 ICP 0.014 mg/L 0.02B jjc0.003* 03/25/14 10:261

Barium, total M200.7 ICP 0.057 mg/L 0.02 jjc0.003 03/28/14 11:291

Beryllium, dissolved M200.8 ICP-MS 0.00005 mg/L 0.0003B las0.00005 04/02/14 0:271

Beryllium, total M200.8 ICP-MS 0.00042 mg/L 0.0003 las0.00005 04/01/14 20:281






Cadmium, total M200.8 ICP-MS 0.0002 mg/L 0.0005B las0.0001 04/01/14 20:281




Chromium, total M200.8 ICP-MS 0.0013 mg/L 0.002B las0.0005 04/01/14 20:281


Cobalt, total M200.8 ICP-MS 0.00144 mg/L 0.0003 las0.00005 04/01/14 20:281


Copper, total M200.8 ICP-MS 0.0020 mg/L 0.003B las0.0005 04/01/14 20:281



Iron, dissolved M200.7 ICP 0.89 mg/L 0.05 jjc0.02 03/25/14 10:261






Magnesium, dissolved M200.7 ICP 2.4 mg/L 1 jjc0.2 03/25/14 10:261




Mercury, dissolved M1631, Atomic Fluorescence 1 ng/L 0.5 las0.2 04/01/14 16:411




Nickel, dissolved M200.8 ICP-MS 0.0035 mg/L 0.003 las0.0006 04/02/14 0:271

Nickel, total M200.8 ICP-MS 0.0049 mg/L 0.003 las0.0006 04/01/14 20:281

Potassium, dissolved M200.7 ICP 8.3 mg/L 1 jjc0.2 03/25/14 10:261


Page 12 of 63L17362-1404111040


Sample ID: 59766






Results

Date Sampled: 03/18/14 12:40





Selenium, dissolved M200.8 ICP-MS 0.0004 mg/L 0.0003 las0.0001 04/02/14 0:271

Selenium, total M200.8 ICP-MS 0.0005 mg/L 0.0003 las0.0001 04/01/14 20:281


Silver, total M200.8 ICP-MS 0.00006 mg/L 0.0003B las0.00005 04/01/14 20:281







Tin, dissolved M200.8 ICP-MS 0.0001 mg/L 0.0005B las0.0001* 04/02/14 0:271



Titanium, total M200.7 ICP 0.112 mg/L 0.03 jjc0.005 03/28/14 11:291

Uranium, dissolved M200.8 ICP-MS 0.0003 mg/L 0.0005B las0.0001 04/02/14 0:271


Vanadium, dissolved M200.8 ICP-MS 0.0005 mg/L 0.001B las0.0002 04/02/14 0:271

Vanadium, total M200.8 ICP-MS 0.0044 mg/L 0.001 las0.0002 04/01/14 20:281




Page 13 of 63L17362-1404111040


Sample ID: 59766






Results

Date Sampled: 03/18/14 12:40



Wet Chemistry

XQDilution



76 mg/L 20 dcw2 03/26/14 0:001

Carbonate as CaCO3 mg/L 20U dcw2 03/26/14 0:001







mg/L 0.01U mpb0.003* 03/27/14 16:510.5



Nitrate/Nitrite as N M353.2 - H2SO4 preserved 0.06 mg/L 0.1B pjb0.02 03/28/14 22:551


pH (lab) SM4500H+ B

pH 7.7 units 0.1H dcw0.1 03/26/14 0:001



0.94 mg/L 0.05 pjb0.01* 04/05/14 13:501


SM2540C 650 mg/L 20 id10* 03/25/14 11:311


SM2540D 85 mg/L 20 enb5* 03/25/14 12:131

Sulfate M300.0 - Ion Chromatography 305 mg/L 25 tcd5 03/27/14 11:1510


Page 14 of 63L17362-1404111040


Sample ID: CYANIDE BLANK






Results

Date Sampled: 03/18/14 00:00



Inorganic Prep

XQDilution


Cyanide, WAD SM4500-CN I- distillation mpb03/31/14 13:40


Wet Chemistry

XQDilution



mg/L 0.01U mpb0.003* 03/31/14 16:090.5


Page 15 of 63L17362-1404111040


Sample ID: PW-1






Results

Date Sampled: 03/18/14 14:45



Inorganic Prep

XQDilution




bsu04/04/14 12:57


M200.2 ICP-MS las03/27/14 12:17


M200.2 ICP jjc03/27/14 12:59


Page 16 of 63L17362-1404111040


Sample ID: PW-1






Results

Date Sampled: 03/18/14 14:45



Metals Analysis

XQDilution


Aluminum, total M200.7 ICP mg/L 0.2U jjc0.03* 03/28/14 11:381





Barium, dissolved M200.7 ICP 0.025 mg/L 0.02 jjc0.003* 03/25/14 10:291



Beryllium, total M200.8 ICP-MS mg/L 0.0003U las0.00005 04/01/14 20:321









Chromium, dissolved M200.8 ICP-MS 0.0006 mg/L 0.002B las0.0005 04/02/14 0:311








Iron, dissolved M200.7 ICP 0.04 mg/L 0.05B jjc0.02 03/25/14 10:291



Lead, total M200.8 ICP-MS mg/L 0.0005U las0.0001 04/01/14 20:321





Manganese, dissolved M200.8 ICP-MS 0.0020 mg/L 0.003B las0.0005 04/02/14 0:311










Page 17 of 63L17362-1404111040


Sample ID: PW-1






Results

Date Sampled: 03/18/14 14:45









Sodium, dissolved M200.7 ICP 34.6 mg/L 1 jjc0.2 03/25/14 10:291









Titanium, total M200.7 ICP mg/L 0.03U jjc0.005 03/28/14 11:381

Uranium, dissolved M200.8 ICP-MS 0.0022 mg/L 0.0005 las0.0001 04/02/14 0:311


Vanadium, dissolved M200.8 ICP-MS 0.0097 mg/L 0.001 las0.0002 04/02/14 0:311





Page 18 of 63L17362-1404111040


Sample ID: PW-1






Results

Date Sampled: 03/18/14 14:45



Wet Chemistry

XQDilution



110 mg/L 20 dcw2 03/26/14 0:001








mg/L 0.01U mpb0.003* 03/31/14 16:100.5



Nitrate/Nitrite as N M353.2 - H2SO4 preserved 0.71 mg/L 0.1 pjb0.02 03/28/14 22:561


pH (lab) SM4500H+ B

pH 8.2 units 0.1H dcw0.1 03/26/14 0:001



0.02 mg/L 0.05B pjb0.01* 04/05/14 13:511


SM2540C 250 mg/L 20 id10* 03/25/14 11:331


SM2540D mg/L 20U enb5* 03/25/14 12:151



Page 19 of 63L17362-1404111040


Sample ID: GW-1






Results

Date Sampled: 03/18/14 15:20



Inorganic Prep

XQDilution




bsu04/04/14 13:04


M200.2 ICP-MS las03/27/14 12:27


M200.2 ICP jjc03/27/14 13:10


Page 20 of 63L17362-1404111040


Sample ID: GW-1






Results

Date Sampled: 03/18/14 15:20



Metals Analysis

XQDilution



Antimony, dissolved M200.8 ICP-MS 0.0004 mg/L 0.002B las0.0004 04/02/14 0:341

Antimony, total M200.8 ICP-MS 0.0004 mg/L 0.002B las0.0004 04/01/14 20:421









Boron, dissolved M200.7 ICP 0.06 mg/L 0.05 jjc0.01 03/25/14 10:321















Iron, total M200.7 ICP mg/L 0.05U jjc0.02* 03/28/14 11:421







Manganese, dissolved M200.8 ICP-MS mg/L 0.003U las0.0005 04/02/14 0:341

Manganese, total M200.8 ICP-MS 0.0010 mg/L 0.003B las0.0005 04/01/14 20:421

Mercury, dissolved M1631, Atomic Fluorescence 0.3 ng/L 0.5B las0.2 04/01/14 16:511








Page 21 of 63L17362-1404111040


Sample ID: GW-1






Results

Date Sampled: 03/18/14 15:20









Sodium, dissolved M200.7 ICP 23.3 mg/L 1 jjc0.2 03/25/14 10:321

















Page 22 of 63L17362-1404111040


Sample ID: GW-1






Results

Date Sampled: 03/18/14 15:20



Wet Chemistry

XQDilution



126 mg/L 20 dcw2 03/26/14 0:001








mg/L 0.01U mpb0.003* 03/31/14 16:120.5





pH (lab) SM4500H+ B

pH 8.1 units 0.1H dcw0.1 03/26/14 0:001



0.02 mg/L 0.05B pjb0.01* 04/05/14 13:521


SM2540C 290 mg/L 20 id10* 03/25/14 11:351


SM2540D mg/L 20U enb5* 03/25/14 12:171



Page 23 of 63L17362-1404111040


Sample ID: 59761






Results

Date Sampled: 03/18/14 16:30



Inorganic Prep

XQDilution




bsu04/04/14 13:12


M200.2 ICP-MS las03/27/14 12:37


M200.2 ICP jjc03/27/14 13:22


Page 24 of 63L17362-1404111040


Sample ID: 59761






Results

Date Sampled: 03/18/14 16:30



Metals Analysis

XQDilution













Boron, dissolved M200.7 ICP 0.06 mg/L 0.05 jjc0.01 03/25/14 10:421















Iron, total M200.7 ICP mg/L 0.05U jjc0.02* 03/28/14 11:511



Lithium, dissolved M200.7 ICP 0.030 mg/L 0.04B jjc0.008* 03/25/14 10:421

Lithium, total M200.7 ICP 0.037 mg/L 0.04B jjc0.008 03/28/14 11:511




Manganese, total M200.8 ICP-MS mg/L 0.003U las0.0005 04/01/14 20:451



Molybdenum, dissolved M200.8 ICP-MS 0.0026 mg/L 0.003B las0.0005 04/02/14 0:371

Molybdenum, total M200.8 ICP-MS 0.0026 mg/L 0.003B las0.0005 04/01/14 20:451





Page 25 of 63L17362-1404111040


Sample ID: 59761






Results

Date Sampled: 03/18/14 16:30










Sodium, total M200.7 ICP 24.2 mg/L 1 jjc0.2 03/28/14 11:511
















Page 26 of 63L17362-1404111040


Sample ID: 59761






Results

Date Sampled: 03/18/14 16:30



Wet Chemistry

XQDilution



128 mg/L 20 dcw2 03/26/14 0:001








mg/L 0.01U mpb0.003* 03/31/14 16:130.5





pH (lab) SM4500H+ B

pH 8.1 units 0.1H dcw0.1 03/26/14 0:001



0.02 mg/L 0.05B pjb0.01* 04/05/14 13:551


SM2540C 280 mg/L 20 id10* 03/25/14 11:371


SM2540D mg/L 20U enb5* 03/25/14 12:201



Page 27 of 63L17362-1404111040








Results

Date Sampled: 03/18/14 00:00



Inorganic Prep

XQDilution




Wet Chemistry

XQDilution



mg/L 0.01U mpb0.003* 03/31/14 16:140.5


Page 28 of 63L17362-1404111040

ACZ Laboratories, Inc.2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493

Report Header Explanations

Batch A distinct set of samples analyzed at a specific time

Found Value of the QC Type of interest

Limit Upper limit for RPD, in %.

Lower Lower Recovery Limit, in % (except for LCSS, mg/Kg)

MDL Method Detection Limit. Same as Minimum Reporting Limit. Allows for instrument and annual fluctuations.

PCN/SCN A number assigned to reagents/standards to trace to the manufacturer's certificate of analysis

PQL Practical Quantitation Limit, typically 5 times the MDL.

QC True Value of the Control Sample or the amount added to the Spike

Rec Recovered amount of the true value or spike added, in % (except for LCSS, mg/Kg)

RPD Relative Percent Difference, calculation used for Duplicate QC Types

Upper Upper Recovery Limit, in % (except for LCSS, mg/Kg)

Sample Value of the Sample of interest

QC Sample Types

AS Analytical Spike (Post Digestion) LCSWD Laboratory Control Sample - Water Duplicate

ASD Analytical Spike (Post Digestion) Duplicate LFB Laboratory Fortified Blank

CCB Continuing Calibration Blank LFM Laboratory Fortified Matrix

CCV Continuing Calibration Verification standard LFMD Laboratory Fortified Matrix Duplicate

DUP Sample Duplicate LRB Laboratory Reagent Blank

ICB Initial Calibration Blank MS Matrix Spike

ICV Initial Calibration Verification standard MSD Matrix Spike Duplicate

ICSAB Inter-element Correction Standard - A plus B solutions PBS Prep Blank - Soil

LCSS Laboratory Control Sample - Soil PBW Prep Blank - Water

LCSSD Laboratory Control Sample - Soil Duplicate PQV Practical Quantitation Verification standard

LCSW Laboratory Control Sample - Water SDL Serial Dilution

QC Sample Type Explanations

Blanks Verifies that there is no or minimal contamination in the prep method or calibration procedure.

Control Samples Verifies the accuracy of the method, including the prep procedure.

Duplicates Verifies the precision of the instrument and/or method.

Spikes/Fortified Matrix Determines sample matrix interferences, if any.

Standard Verifies the validity of the calibration.

ACZ Qualifiers (Qual)

B Analyte concentration detected at a value between MDL and PQL. The associated value is an estimated quantity.

H Analysis exceeded method hold time. pH is a field test with an immediate hold time.

L Target analyte response was below the laboratory defined negative threshold.

U The material was analyzed for, but was not detected above the level of the associated value.

The associated value is either the sample quantitation limit or the sample detection limit.

Method References

(1) EPA 600/4-83-020. Methods for Chemical Analysis of Water and Wastes, March 1983.

(2) EPA 600/R-93-100. Methods for the Determination of Inorganic Substances in Environmental Samples, August 1993.

(3) EPA 600/R-94-111. Methods for the Determination of Metals in Environmental Samples - Supplement I, May 1994.

(4) EPA SW-846. Test Methods for Evaluating Solid Waste.

(5) Standard Methods for the Examination of Water and Wastewater.

Comments

(1) QC results calculated from raw data. Results may vary slightly if the rounded values are used in the calculations.

(2) Soil, Sludge, and Plant matrices for Inorganic analyses are reported on a dry weight basis.

(3) Animal matrices for Inorganic analyses are reported on an "as received" basis.

(4) An asterisk in the "XQ" column indicates there is an extended qualifier and/or certification qualifier

associated with the result.

(5) If the MDL equals the PQL or the MDL column is omitted, the PQL is the reporting limit.

For a complete list of ACZ's Extended Qualifiers, please click: http://www.acz.com/public/extquallist.pdf

REP001.09.12.01

Inorganic

Reference

Page 29 of 63L17362-1404111040

http://www.acz.com/public/extquallist.pdf


Inorganic QC

Summary

ACZ Project ID: L17362SPF Water Engineering


ACZ ID Analyzed RecSample QualLower Upper RPDFoundType UnitsPCN/SCN LimitQC

WG361281

WG361281PBW1 03/26/14 16:40PBW U -20 20mg/L

WG361281LCSW3 03/26/14 16:59 101.6LCSW WC140313- 833.3 90 110mg/L820.0001

L17364-01DUP1 RA03/26/14 18:38 UDUP U 0mg/L 20


WG361281PBW2 03/26/14 20:01PBW 2.5 -20 20mg/L


WG361281PBW3 03/26/14 23:35PBW 2.6 -20 20mg/L


WG361281PBW4 03/27/14 2:35PBW 2.9 -20 20mg/L


Aluminum, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 98.4ICV II140220-1 1.968 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.09 0.09mg/L

WG361133LFB 03/25/14 9:46 92.2LFB II140317-2 .923 85 115mg/L1.0011

L17312-02AS 03/25/14 9:55 U 91.8AS II140317-2 .919 85 115mg/L1.0011

L17312-02ASD 03/25/14 9:58 U 91.8ASD II140317-2 .919 085 115mg/L 201.0011

L17362-06AS 03/25/14 10:36 U 90.3AS II140317-2 .904 85 115mg/L1.0011

L17362-06ASD 03/25/14 10:39 U 90.1ASD II140317-2 .902 0.2285 115mg/L 201.0011

Aluminum, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 96.7ICV II140228-1 1.934 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.09 0.09mg/L

WG361311LRB 03/28/14 10:35LRB U -0.066 0.066mg/L

WG361311LFB 03/28/14 10:38 102.9LFB II140317-2 1.03 85 115mg/L1.0011

L17343-01LFM 03/28/14 10:57 U 107.5LFM II140317-2 1.076 70 130mg/L1.0011

L17343-01LFMD 03/28/14 11:00 U 106.1LFMD II140317-2 1.062 1.3170 130mg/L 201.0011

L17362-03LFM M103/28/14 11:32 2.9 552.4LFM II140317-2 8.43 70 130mg/L1.0011

L17362-03LFMD M103/28/14 11:35 2.9 542.3LFMD II140317-2 8.329 1.2170 130mg/L 201.0011

Antimony, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 106.3ICV MS140331-9 .02129 90 110mg/L.02002

WG361610ICB 04/02/14 0:07ICB U -0.0012 0.0012mg/L

WG361610LFB 04/02/14 0:10 97.6LFB MS140331-2 .00976 85 115mg/L.01

L17362-01AS 04/02/14 0:17 U 99.6AS MS140331-2 .00996 70 130mg/L.01

L17362-01ASD 04/02/14 0:20 U 101.6ASD MS140331-2 .01016 1.9970 130mg/L 20.01

Page 30 of 63L17362-1404111040


Inorganic QC

Summary


Antimony, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 100.2ICV MS140331-9 .02006 90 110mg/L.02002

WG361587ICB 04/01/14 19:20ICB U -0.0012 0.0012mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00088 0.00088mg/L

WG361306LFB 04/01/14 19:27 104.1LFB MS140320-2 .01041 85 115mg/L.01

L17362-07LFM 04/01/14 20:49 U 102.6LFM MS140320-2 .01026 70 130mg/L.01

L17362-07LFMD 04/01/14 20:52 U 103.4LFMD MS140320-2 .01034 0.7870 130mg/L 20.01

Arsenic, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 104.6ICV MS140331-9 .05228 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0006 0.0006mg/L

WG361610LFB 04/02/14 0:10 95.7LFB MS140331-2 .04797 85 115mg/L.0501

L17362-01AS 04/02/14 0:17 .0127 102.1AS MS140331-2 .06383 70 130mg/L.0501

L17362-01ASD 04/02/14 0:20 .0127 100.6ASD MS140331-2 .06308 1.1870 130mg/L 20.0501

Arsenic, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 101ICV MS140331-9 .05051 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0006 0.0006mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00044 0.00044mg/L

WG361306LFB 04/01/14 19:27 103.7LFB MS140320-2 .05193 85 115mg/L.0501

L17362-07LFM 04/01/14 20:49 .0219 99.6LFM MS140320-2 .07178 70 130mg/L.0501

L17362-07LFMD 04/01/14 20:52 .0219 100.3LFMD MS140320-2 .07214 0.570 130mg/L 20.0501

Barium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 96.8ICV II140220-1 1.9352 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.009 0.009mg/L

WG361133LFB 03/25/14 9:46 87.1LFB II140317-2 .4355 85 115mg/L.5

L17312-02AS M203/25/14 9:55 .04 84.5AS II140317-2 .4624 85 115mg/L.5

L17312-02ASD M203/25/14 9:58 .04 83.9ASD II140317-2 .4594 0.6585 115mg/L 20.5

L17362-06AS M203/25/14 10:36 .025 83AS II140317-2 .4401 85 115mg/L.5

L17362-06ASD M203/25/14 10:39 .025 82.9ASD II140317-2 .4394 0.1685 115mg/L 20.5

Page 31 of 63L17362-1404111040


Inorganic QC

Summary


Barium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 96.4ICV II140228-1 1.9285 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.009 0.009mg/L

WG361311LRB 03/28/14 10:35LRB U -0.0066 0.0066mg/L

WG361311LFB 03/28/14 10:38 98LFB II140317-2 .49 85 115mg/L.5

L17343-01LFM 03/28/14 10:57 .021 99LFM II140317-2 .5158 70 130mg/L.5

L17343-01LFMD 03/28/14 11:00 .021 99.4LFMD II140317-2 .5178 0.3970 130mg/L 20.5

L17362-03LFM 03/28/14 11:32 .057 98.8LFM II140317-2 .5511 70 130mg/L.5

L17362-03LFMD 03/28/14 11:35 .057 98.6LFMD II140317-2 .5502 0.1670 130mg/L 20.5

Beryllium, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 101.1ICV MS140331-9 .05054 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.00015 0.00015mg/L

WG361610LFB 04/02/14 0:10 96.8LFB MS140331-2 .04844 85 115mg/L.05005

L17362-01AS 04/02/14 0:17 U 102.1AS MS140331-2 .05112 70 130mg/L.05005

L17362-01ASD 04/02/14 0:20 U 103.5ASD MS140331-2 .05182 1.3670 130mg/L 20.05005

Beryllium, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 98.5ICV MS140331-9 .04926 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.00015 0.00015mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00011 0.00011mg/L

WG361306LFB 04/01/14 19:27 99.9LFB MS140320-2 .04999 85 115mg/L.05005

L17362-07LFM 04/01/14 20:49 U 97.8LFM MS140320-2 .04897 70 130mg/L.05005

L17362-07LFMD 04/01/14 20:52 U 97LFMD MS140320-2 .04854 0.8870 130mg/L 20.05005

Bismuth, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 99.4ICV II140220-1 1.987 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.12 0.12mg/L

WG361133LFB 03/25/14 9:46 89LFB II140317-2 .889 85 115mg/L.999

L17312-02AS 03/25/14 9:55 U 88.8AS II140317-2 .887 85 115mg/L.999

L17312-02ASD 03/25/14 9:58 U 88.1ASD II140317-2 .88 0.7985 115mg/L 20.999

L17362-06AS 03/25/14 10:36 U 87.2AS II140317-2 .871 85 115mg/L.999

L17362-06ASD 03/25/14 10:39 U 87.6ASD II140317-2 .875 0.4685 115mg/L 20.999

Page 32 of 63L17362-1404111040


Inorganic QC

Summary


Bismuth, total M200.7 ICP


WG361427

WG361427ICV 03/28/14 14:42 98ICV II140228-1 1.96 95 105mg/L2

WG361427ICB 03/28/14 14:48ICB U -0.12 0.12mg/L

WG361311LRB 03/28/14 15:01LRB U -0.088 0.088mg/L

WG361311LFB 03/28/14 15:04 94.2LFB II140317-2 .941 85 115mg/L.999

L17343-01LFM 03/28/14 15:11 U 98.6LFM II140317-2 .985 70 130mg/L.999


L17362-03LFM 03/28/14 15:26 U 97.4LFM II140317-2 .973 70 130mg/L.999

L17362-03LFMD 03/28/14 15:30 U 98.8LFMD II140317-2 .987 1.4370 130mg/L 20.999

Boron, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 101.1ICV II140220-1 2.021 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.03 0.03mg/L

WG361133LFB 03/25/14 9:46 90.1LFB II140317-2 .451 85 115mg/L.5005

L17312-02AS 03/25/14 9:55 .06 85.5AS II140317-2 .488 85 115mg/L.5005

L17312-02ASD MA03/25/14 9:58 .06 84.1ASD II140317-2 .481 1.4485 115mg/L 20.5005

L17362-06AS 03/25/14 10:36 .06 86.5AS II140317-2 .493 85 115mg/L.5005

L17362-06ASD 03/25/14 10:39 .06 85.3ASD II140317-2 .487 1.2285 115mg/L 20.5005

Boron, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 98.1ICV II140228-1 1.962 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.03 0.03mg/L

WG361311LRB 03/28/14 10:35LRB U -0.022 0.022mg/L

WG361311LFB 03/28/14 10:38 97.1LFB II140317-2 .486 85 115mg/L.5005

L17343-01LFM 03/28/14 10:57 16.5 95.9LFM II140317-2 16.98 70 130mg/L.5005

L17343-01LFMD 03/28/14 11:00 16.5 117.9LFMD II140317-2 17.09 0.6570 130mg/L 20.5005

L17362-03LFM 03/28/14 11:32 .14 95.5LFM II140317-2 .618 70 130mg/L.5005

L17362-03LFMD 03/28/14 11:35 .14 95.3LFMD II140317-2 .617 0.1670 130mg/L 20.5005

Cadmium, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 98.7ICV MS140331-9 .04935 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0003 0.0003mg/L

WG361610LFB 04/02/14 0:10 91.9LFB MS140331-2 .04606 85 115mg/L.0501

L17362-01AS 04/02/14 0:17 U 96.7AS MS140331-2 .04847 70 130mg/L.0501

L17362-01ASD 04/02/14 0:20 U 95.2ASD MS140331-2 .0477 1.670 130mg/L 20.0501

Page 33 of 63L17362-1404111040


Inorganic QC

Summary


Cadmium, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 98.5ICV MS140331-9 .04925 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0003 0.0003mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00022 0.00022mg/L

WG361306LFB 04/01/14 19:27 100.8LFB MS140320-2 .05051 85 115mg/L.0501

L17362-07LFM 04/01/14 20:49 U 97.3LFM MS140320-2 .04873 70 130mg/L.0501


Calcium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 99.8ICV II140220-1 99.76 95 105mg/L100

WG361133ICB 03/25/14 9:33ICB U -0.3 0.3mg/L

WG361133LFB 03/25/14 9:46 94.6LFB II140317-2 64.3 85 115mg/L67.98099

L17312-02AS 03/25/14 9:55 13.3 92.9AS II140317-2 76.47 85 115mg/L67.98099

L17312-02ASD 03/25/14 9:58 13.3 92.3ASD II140317-2 76.04 0.5685 115mg/L 2067.98099

L17362-06AS 03/25/14 10:36 39.6 92.4AS II140317-2 102.4 85 115mg/L67.98099

L17362-06ASD 03/25/14 10:39 39.6 92.2ASD II140317-2 102.3 0.185 115mg/L 2067.98099

Calcium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 99.6ICV II140228-1 99.62 95 105mg/L100

WG361367ICB 03/28/14 10:22ICB U -0.3 0.3mg/L

WG361311LRB 03/28/14 10:35LRB U -0.22 0.22mg/L

WG361311LFB 03/28/14 10:38 106.9LFB II140317-2 72.64 85 115mg/L67.98099

L17343-01LFM 03/28/14 10:57 152 105.5LFM II140317-2 223.7 70 130mg/L67.98099

L17343-01LFMD 03/28/14 11:00 152 104LFMD II140317-2 222.7 0.4570 130mg/L 2067.98099

L17362-03LFM 03/28/14 11:32 40.5 106.4LFM II140317-2 112.8 70 130mg/L67.98099

L17362-03LFMD 03/28/14 11:35 40.5 105.3LFMD II140317-2 112.1 0.6270 130mg/L 2067.98099

Chloride M300.0 - Ion Chromatography


WG360290

WG360290ICV 03/06/14 13:49 101.6ICV WI140226-1 20.3 90 110mg/L19.98

WG360290ICB 03/06/14 14:07ICB U -1.5 1.5mg/L

WG361247

WG361247LFB 03/26/14 13:20 102LFB WI140306-2 30.6 90 110mg/L30

L17336-01DUP RA03/26/14 18:06 UDUP U 0mg/L 20

L17360-01AS 03/26/14 18:42 2 101.3AS WI140306-2 32.4 90 110mg/L30

Page 34 of 63L17362-1404111040


Inorganic QC

Summary


Chromium, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 99ICV MS140331-9 .04952 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0015 0.0015mg/L

WG361610LFB 04/02/14 0:10 92.6LFB MS140331-2 .04636 85 115mg/L.05005

L17362-01AS 04/02/14 0:17 U 93.8AS MS140331-2 .04696 70 130mg/L.05005

L17362-01ASD 04/02/14 0:20 U 92.4ASD MS140331-2 .04624 1.5570 130mg/L 20.05005

Chromium, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 98.5ICV MS140331-9 .04924 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0015 0.0015mg/L

WG361306LRB 04/01/14 19:24LRB U -0.0011 0.0011mg/L

WG361306LFB 04/01/14 19:27 97.5LFB MS140320-2 .04881 85 115mg/L.05005

L17362-07LFM 04/01/14 20:49 .0011 94.9LFM MS140320-2 .04858 70 130mg/L.05005

L17362-07LFMD 04/01/14 20:52 .0011 94.5LFMD MS140320-2 .0484 0.3770 130mg/L 20.05005

Cobalt, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 98.4ICV MS140331-9 .04921 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.00015 0.00015mg/L

WG361610LFB 04/02/14 0:10 95.2LFB MS140331-2 .04763 85 115mg/L.05005

L17362-01AS 04/02/14 0:17 .00025 97.7AS MS140331-2 .04916 70 130mg/L.05005

L17362-01ASD 04/02/14 0:20 .00025 97.8ASD MS140331-2 .04922 0.1270 130mg/L 20.05005

Cobalt, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 99.2ICV MS140331-9 .04962 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.00015 0.00015mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00011 0.00011mg/L

WG361306LFB 04/01/14 19:27 101LFB MS140320-2 .05056 85 115mg/L.05005

L17362-07LFM 04/01/14 20:49 .00011 99.3LFM MS140320-2 .04979 70 130mg/L.05005

L17362-07LFMD 04/01/14 20:52 .00011 97.5LFMD MS140320-2 .04889 1.8270 130mg/L 20.05005

Conductivity @25C SM2510B


WG361281

WG361281LCSW2 03/26/14 16:45 103.4LCSW PCN43577 1456.4 90 110umhos/cm1408.8

L17364-01DUP1 03/26/14 18:38 3550DUP 3570 0.6umhos/cm 20


WG361281LCSW8 03/26/14 23:11 101LCSW PCN43577 1423.1 90 110umhos/cm1408.8

WG361281LCSW11 03/27/14 2:11 100LCSW PCN43577 1409 90 110umhos/cm1408.8


Page 35 of 63L17362-1404111040


Inorganic QC

Summary


Copper, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 99.1ICV MS140331-9 .04953 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0015 0.0015mg/L

WG361610LFB 04/02/14 0:10 92.3LFB MS140331-2 .04618 85 115mg/L.05005

L17362-01AS 04/02/14 0:17 U 91.3AS MS140331-2 .04572 70 130mg/L.05005

L17362-01ASD 04/02/14 0:20 U 89.9ASD MS140331-2 .04498 1.6370 130mg/L 20.05005

Copper, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 97ICV MS140331-9 .04849 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0015 0.0015mg/L

WG361306LRB 04/01/14 19:24LRB U -0.0011 0.0011mg/L

WG361306LFB 04/01/14 19:27 97.9LFB MS140320-2 .04901 85 115mg/L.05005

L17362-07LFM 04/01/14 20:49 U 93.1LFM MS140320-2 .0466 70 130mg/L.05005


Cyanide, total M335.4 - Colorimetric w/ distillation


WG361515

WG361515ICV 03/31/14 15:14 97.6ICV WI140322-7 .2928 90 110mg/L.3

WG361515ICB 03/31/14 15:15ICB U -0.003 0.003mg/L

WG361445LRB 03/31/14 15:16LRB U -0.003 0.003mg/L

WG361445LFB 03/31/14 15:17 104.5LFB WI140322-4 .209 90 110mg/L.2

L17362-01DUP RA03/31/14 15:22 UDUP U 0mg/L 20

L17362-07DUP RA03/31/14 15:30 UDUP U 0mg/L 20

L17362-08LFM 03/31/14 15:32 U 99.7LFM WI140322-4 .1993 90 110mg/L.2

L17362-02LFM 03/31/14 15:42 U 103.5LFM WI140322-4 .207 90 110mg/L.2



WG361346

WG361346ICV 03/27/14 11:49 98.1ICV WI140322-7 .2942 90 110mg/L.3

WG361346ICB 03/27/14 11:50ICB U -0.003 0.003mg/L

WG361379

WG361349LRB 03/27/14 16:28LRB U -0.003 0.003mg/L

WG361349LFB 03/27/14 16:29 96.3LFB WI140322-6 .1925 90 110mg/L.2

L17332-02LFM 03/27/14 16:43 U 95.2LFM WI140322-6 .1904 90 110mg/L.2

L17333-01DUP RA03/27/14 16:44 UDUP U 0mg/L 20

WG361515

WG361515ICV 03/31/14 15:14 97.6ICV WI140322-7 .2928 90 110mg/L.3

WG361515ICB 03/31/14 15:15ICB U -0.003 0.003mg/L

WG361524

WG361496LRB 03/31/14 16:07LRB U -0.003 0.003mg/L

WG361496LFB 03/31/14 16:08 96.2LFB WI140322-6 .1924 90 110mg/L.2

L17362-04DUP RA03/31/14 16:09 UDUP U 0mg/L 20

L17362-05LFM 03/31/14 16:11 U 95.5LFM WI140322-6 .191 90 110mg/L.2

Page 36 of 63L17362-1404111040


Inorganic QC

Summary


Fluoride M300.0 - Ion Chromatography


WG360290

WG360290ICV 03/06/14 13:49 103.7ICV WI140226-1 4.17 90 110mg/L4.02

WG360290ICB 03/06/14 14:07ICB U -0.3 0.3mg/L

WG361247

WG361247LFB 03/26/14 13:20 104LFB WI140306-2 1.56 90 110mg/L1.5

L17336-01DUP RA03/26/14 18:06 UDUP U 0mg/L 20

L17360-01AS 03/26/14 18:42 .11 105.3AS WI140306-2 1.69 90 110mg/L1.5

Gallium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 98ICV II140220-1 1.96 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.3 0.3mg/L

WG361133LFB 03/25/14 9:46 90.9LFB II140317-2 .91 85 115mg/L1.001

L17312-02AS 03/25/14 9:55 U 88.9AS II140317-2 .89 85 115mg/L1.001

L17312-02ASD 03/25/14 9:58 U 87.9ASD II140317-2 .88 1.1385 115mg/L 201.001

L17362-06AS 03/25/14 10:36 U 90.9AS II140317-2 .91 85 115mg/L1.001

L17362-06ASD 03/25/14 10:39 U 88.9ASD II140317-2 .89 2.2285 115mg/L 201.001

Gallium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 96.5ICV II140228-1 1.93 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.3 0.3mg/L

WG361311LRB 03/28/14 10:35LRB U -0.22 0.22mg/L

WG361311LFB 03/28/14 10:38 100.9LFB II140317-2 1.01 85 115mg/L1.001

L17343-01LFM 03/28/14 10:57 U 101.9LFM II140317-2 1.02 70 130mg/L1.001


L17362-03LFM 03/28/14 11:32 U 100.9LFM II140317-2 1.01 70 130mg/L1.001

L17362-03LFMD 03/28/14 11:35 U 100.9LFMD II140317-2 1.01 070 130mg/L 201.001

Iron, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 98ICV II140220-1 1.959 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.06 0.06mg/L

WG361133LFB 03/25/14 9:46 91.7LFB II140317-2 .918 85 115mg/L1.0014

L17312-02AS 03/25/14 9:55 .15 88.7AS II140317-2 1.038 85 115mg/L1.0014

L17312-02ASD 03/25/14 9:58 .15 87ASD II140317-2 1.021 1.6585 115mg/L 201.0014

L17362-06AS 03/25/14 10:36 U 89.7AS II140317-2 .898 85 115mg/L1.0014

L17362-06ASD 03/25/14 10:39 U 88.9ASD II140317-2 .89 0.8985 115mg/L 201.0014

Page 37 of 63L17362-1404111040


Inorganic QC

Summary


Iron, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 97.1ICV II140228-1 1.941 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.06 0.06mg/L

WG361311LRB 03/28/14 10:35LRB U -0.044 0.044mg/L

WG361311LFB 03/28/14 10:38 100.9LFB II140317-2 1.01 85 115mg/L1.0014

L17343-01LFM 03/28/14 10:57 U 103.1LFM II140317-2 1.032 70 130mg/L1.0014


L17362-03LFM M303/28/14 11:32 3.9 215.6LFM II140317-2 6.059 70 130mg/L1.0014


Lead, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 98.2ICV MS140331-9 .0491 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0003 0.0003mg/L

WG361610LFB 04/02/14 0:10 89.8LFB MS140331-2 .04496 85 115mg/L.05005

L17362-01AS 04/02/14 0:17 U 96AS MS140331-2 .04803 70 130mg/L.05005

L17362-01ASD 04/02/14 0:20 U 95.4ASD MS140331-2 .04775 0.5870 130mg/L 20.05005

Lead, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 98.9ICV MS140331-9 .04943 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0003 0.0003mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00022 0.00022mg/L

WG361306LFB 04/01/14 19:27 94.6LFB MS140320-2 .04735 85 115mg/L.05005

L17362-07LFM 04/01/14 20:49 U 95.2LFM MS140320-2 .04766 70 130mg/L.05005


Lithium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 97.8ICV II140220-1 1.955 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.024 0.024mg/L

WG361133LFB 03/25/14 9:46 86.2LFB II140317-2 .8619 85 115mg/L1

L17312-02AS M203/25/14 9:55 .086 84AS II140317-2 .9264 85 115mg/L1

L17312-02ASD M203/25/14 9:58 .086 83.8ASD II140317-2 .9239 0.2785 115mg/L 201

L17362-06AS M203/25/14 10:36 .04 82.8AS II140317-2 .8682 85 115mg/L1

L17362-06ASD M203/25/14 10:39 .04 82.4ASD II140317-2 .8642 0.4685 115mg/L 201

Page 38 of 63L17362-1404111040


Inorganic QC

Summary


Lithium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 97.6ICV II140228-1 1.9512 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.024 0.024mg/L

WG361311LRB 03/28/14 10:35LRB U -0.0176 0.0176mg/L

WG361311LFB 03/28/14 10:38 96.8LFB II140317-2 .9676 85 115mg/L1

L17343-01LFM 03/28/14 10:57 .778 99.3LFM II140317-2 1.771 70 130mg/L1

L17343-01LFMD 03/28/14 11:00 .778 100.8LFMD II140317-2 1.786 0.8470 130mg/L 201

L17362-03LFM 03/28/14 11:32 .543 96.5LFM II140317-2 1.508 70 130mg/L1

L17362-03LFMD 03/28/14 11:35 .543 97.1LFMD II140317-2 1.514 0.470 130mg/L 201

Magnesium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 97.8ICV II140220-1 97.8 95 105mg/L100

WG361133ICB 03/25/14 9:33ICB U -0.6 0.6mg/L

WG361133LFB 03/25/14 9:46 88.4LFB II140317-2 44.2 85 115mg/L50.00131

L17312-02AS 03/25/14 9:55 9.3 86.8AS II140317-2 52.7 85 115mg/L50.00131

L17312-02ASD 03/25/14 9:58 9.3 86.4ASD II140317-2 52.52 0.3485 115mg/L 2050.00131

L17362-06AS 03/25/14 10:36 7.2 85.9AS II140317-2 50.15 85 115mg/L50.00131

L17362-06ASD 03/25/14 10:39 7.2 85.7ASD II140317-2 50.05 0.285 115mg/L 2050.00131

Magnesium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 97.7ICV II140228-1 97.72 95 105mg/L100

WG361367ICB 03/28/14 10:22ICB U -0.6 0.6mg/L

WG361311LRB 03/28/14 10:35LRB U -0.44 0.44mg/L

WG361311LFB 03/28/14 10:38 102.2LFB II140317-2 51.11 85 115mg/L50.00131

L17343-01LFM 03/28/14 10:57 214 104.6LFM II140317-2 266.3 70 130mg/L50.00131

L17343-01LFMD 03/28/14 11:00 214 101.8LFMD II140317-2 264.9 0.5370 130mg/L 2050.00131

L17362-03LFM 03/28/14 11:32 3.2 102.2LFM II140317-2 54.29 70 130mg/L50.00131

L17362-03LFMD 03/28/14 11:35 3.2 100.9LFMD II140317-2 53.66 1.1770 130mg/L 2050.00131

Manganese, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 101.4ICV MS140331-9 .05071 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0015 0.0015mg/L

WG361610LFB 04/02/14 0:10 94.8LFB MS140331-2 .04747 85 115mg/L.0501

L17362-01AS 04/02/14 0:17 .0357 94AS MS140331-2 .08281 70 130mg/L.0501

L17362-01ASD 04/02/14 0:20 .0357 95ASD MS140331-2 .08332 0.6170 130mg/L 20.0501

WG361642

WG361642ICV 04/02/14 16:04 100.8ICV MS140331-9 .05041 90 110mg/L.05

WG361642ICB 04/02/14 16:07ICB U -0.0015 0.0015mg/L

WG361642LFB 04/02/14 16:11 102.7LFB MS140331-2 .05146 85 115mg/L.0501

L17317-01AS 04/02/14 16:17 .7155 125.1AS MS140331-2 .7782 70 130mg/L.0501

L17317-01ASD 04/02/14 16:21 .7155 109ASD MS140331-2 .7701 1.0570 130mg/L 20.0501

Page 39 of 63L17362-1404111040


Inorganic QC

Summary


Manganese, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 102.9ICV MS140331-9 .05143 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0015 0.0015mg/L

WG361306LRB 04/01/14 19:24LRB U -0.0011 0.0011mg/L

WG361306LFB 04/01/14 19:27 101.2LFB MS140320-2 .05069 85 115mg/L.0501

L17362-07LFM 04/01/14 20:49 U 100.4LFM MS140320-2 .0503 70 130mg/L.0501


WG361643

WG361643ICV 04/02/14 13:17 102.6ICV MS140331-9 .05128 90 110mg/L.05

WG361643ICB 04/02/14 13:19ICB U -0.0015 0.0015mg/L

WG361306LRB 04/02/14 13:22LRB U -0.0011 0.0011mg/L

WG361306LFB 04/02/14 13:24 101.9LFB MS140320-2 .05106 85 115mg/L.0501

L17362-07LFM 04/02/14 13:48 U 103.3LFM MS140320-2 .05175 70 130mg/L.0501


Mercury, dissolved M1631, Atomic Fluorescence


WG361393

WG361393ICV 03/28/14 15:59 98.7ICV HG140325-4 9.87 79 121ng/L10

WG361393ICB 03/28/14 16:04ICB U -0.5 0.5ng/L

WG361562

WG361562CCV1 04/01/14 15:50 96.8CCV HG140325-4 9.68 76.5 123.4ng/L10

WG361562CCB1 04/01/14 15:55CCB U -0.5 0.5ng/L

WG361562PQV 04/01/14 16:00 86PQV HG140325-6 .43 70 130ng/L.5

WG361562LFB 04/01/14 16:12 75LFB HG140325-5 1.5 71 125ng/L2

L17362-01MS 04/01/14 16:26 U 76MS HG140325-5 1.52 71 125ng/L2

L17362-01MSD 04/01/14 16:31 U 76.5MSD HG140325-5 1.53 0.6671 125ng/L 242

WG361562CCV2 04/01/14 17:01 94.6CCV HG140325-4 9.46 76.5 123.4ng/L10

WG361562CCB2 04/01/14 17:06CCB U -0.5 0.5ng/L

WG361562CCV3 04/01/14 17:47 91.9CCV HG140325-4 9.19 76.5 123.4ng/L10

WG361562CCB3 04/01/14 17:52CCB U -0.5 0.5ng/L

WG361562CCV4 04/01/14 18:22 97.1CCV HG140325-4 9.71 76.5 123.4ng/L10

WG361562CCB4 04/01/14 18:27CCB U -0.5 0.5ng/L

Page 40 of 63L17362-1404111040


Inorganic QC

Summary


Mercury, total M1631, Atomic Fluorescence


WG361393

WG361393ICV 03/28/14 15:59 98.7ICV HG140325-4 9.87 79 121ng/L10

WG361393ICB 03/28/14 16:04ICB U -0.5 0.5ng/L

WG361470

WG361470CCV1 03/31/14 11:35 99CCV HG140325-4 9.9 76.5 123.4ng/L10

WG361470CCB1 03/31/14 11:40CCB U -0.5 0.5ng/L

WG361470PQV 03/31/14 11:45 102PQV HG140325-6 .51 70 130ng/L.5

WG361470LFB 03/31/14 11:50 89.5LFB HG140325-5 1.79 71 125ng/L2

WG361470CCV2 03/31/14 12:42 77.2CCV HG140325-4 7.72 76.5 123.4ng/L10

WG361470CCB2 03/31/14 12:47CCB U -0.5 0.5ng/L

L17347-01MS 03/31/14 13:09 8 88MS HG10XPRE 25.6 71 125ng/L200

L17347-01MSD 03/31/14 13:14 8 87MSD HG10XPRE 25.4 0.7871 125ng/L 24200

WG361470CCV3 03/31/14 13:50 106CCV HG140325-4 10.6 76.5 123.4ng/L10

WG361470CCB3 03/31/14 13:55CCB U -0.5 0.5ng/L

WG361470CCV4 03/31/14 14:35 104CCV HG140325-4 10.4 76.5 123.4ng/L10

WG361470CCB4 03/31/14 14:40CCB U -0.5 0.5ng/L

WG361470CCV5 03/31/14 15:05 106CCV HG140325-4 10.6 76.5 123.4ng/L10

WG361470CCB5 03/31/14 15:11CCB U -0.5 0.5ng/L

Molybdenum, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 94.5ICV MS140331-9 .01889 90 110mg/L.01998

WG361610ICB 04/02/14 0:07ICB U -0.0015 0.0015mg/L

WG361610LFB 04/02/14 0:10 89.3LFB MS140331-2 .04464 85 115mg/L.05

L17362-01AS 04/02/14 0:17 .0105 97.6AS MS140331-2 .05928 70 130mg/L.05

L17362-01ASD 04/02/14 0:20 .0105 96.8ASD MS140331-2 .05892 0.6170 130mg/L 20.05

Molybdenum, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 93.3ICV MS140331-9 .01865 90 110mg/L.01998

WG361587ICB 04/01/14 19:20ICB U -0.0015 0.0015mg/L

WG361306LRB 04/01/14 19:24LRB U -0.0011 0.0011mg/L

WG361306LFB 04/01/14 19:27 95.1LFB MS140320-2 .04756 85 115mg/L.05

L17362-07LFM 04/01/14 20:49 .0026 96.2LFM MS140320-2 .05069 70 130mg/L.05

L17362-07LFMD 04/01/14 20:52 .0026 95.9LFMD MS140320-2 .05056 0.2670 130mg/L 20.05

Nickel, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 98.5ICV MS140331-9 .04927 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0018 0.0018mg/L

WG361610LFB 04/02/14 0:10 90.1LFB MS140331-2 .04503 85 115mg/L.05

L17362-01AS 04/02/14 0:17 U 88.7AS MS140331-2 .04434 70 130mg/L.05

L17362-01ASD 04/02/14 0:20 U 86.7ASD MS140331-2 .04334 2.2870 130mg/L 20.05

Page 41 of 63L17362-1404111040


Inorganic QC

Summary


Nickel, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 97.3ICV MS140331-9 .04865 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0018 0.0018mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00132 0.00132mg/L

WG361306LFB 04/01/14 19:27 95.3LFB MS140320-2 .04766 85 115mg/L.05

L17362-07LFM 04/01/14 20:49 U 91.5LFM MS140320-2 .04576 70 130mg/L.05


Nitrate/Nitrite as N M353.2 - H2SO4 preserved


WG361453

WG361453ICV 03/28/14 20:13 106ICV WI140116-3 2.56 90 110mg/L2.416

WG361453ICB 03/28/14 20:14ICB U -0.06 0.06mg/L

WG361455

WG361455LFB1 03/28/14 22:09 109.8LFB WI140215-3 2.195 90 110mg/L2

WG361455LFB2 03/28/14 22:43 107.9LFB WI140215-3 2.158 90 110mg/L2

L17355-01AS 03/28/14 22:45 .26 108.7AS WI140215-3 2.433 90 110mg/L2

L17355-02DUP 03/28/14 22:48 2.19DUP 2.176 0.6mg/L 20

Nitrogen, ammonia M350.1 - Automated Phenate


WG361341

WG361341ICV 03/27/14 11:36 105.7ICV WI131021-1 1.06 90 110mg/L1.003

WG361341ICB 03/27/14 11:39ICB U -0.15 0.15mg/L

WG361369

WG361369LFB1 03/27/14 15:50 106.1LFB WI140113-8 1.061 90 110mg/L1

L17248-01AS 03/27/14 15:52 U 100.4AS WI140113-8 1.004 90 110mg/L1

L17248-02DUP RA03/27/14 15:54 UDUP U 0mg/L 20

L17362-02AS M103/27/14 16:07 U 114.4AS WI140113-8 1.144 90 110mg/L1

L17362-03DUP RA03/27/14 16:10 UDUP .058 200mg/L 20

WG361369LFB2 03/27/14 16:56 107.5LFB WI140113-8 1.075 90 110mg/L1

pH (lab) SM4500H+ B


WG361281

WG361281LCSW1 03/26/14 16:43 99.2LCSW PCN40852 5.95 units6

L17364-01DUP1 03/26/14 18:38 3.6DUP 3.51 2.5units 20





Page 42 of 63L17362-1404111040


Inorganic QC

Summary




WG361833

WG361833ICV 04/05/14 13:38 97.5ICV WI140401-5 .636 90 110mg/L.65228

WG361833ICB 04/05/14 13:41ICB U -0.03 0.03mg/L

WG361801LRB 04/05/14 13:42LRB U -0.03 0.03mg/L

WG361801LFB 04/05/14 13:43 100.2LFB WI140326-3 .501 90 110mg/L.5

L17248-01LFM 04/05/14 13:45 .4 102.4LFM 5XPT 2.961 90 110mg/L2.5

L17362-01DUP RA04/05/14 13:47 .05DUP .049 2mg/L 20

Potassium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 99.3ICV II140220-1 19.85 95 105mg/L20

WG361133ICB 03/25/14 9:33ICB U -0.6 0.6mg/L

WG361133LFB 03/25/14 9:46 90.7LFB II140317-2 90.65 85 115mg/L99.99364

L17312-02AS 03/25/14 9:55 7.4 89.2AS II140317-2 96.6 85 115mg/L99.99364

L17312-02ASD 03/25/14 9:58 7.4 89.5ASD II140317-2 96.91 0.3285 115mg/L 2099.99364

L17362-06AS 03/25/14 10:36 5.2 88.9AS II140317-2 94.07 85 115mg/L99.99364

L17362-06ASD 03/25/14 10:39 5.2 89ASD II140317-2 94.15 0.0985 115mg/L 2099.99364

Potassium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 97.8ICV II140228-1 19.55 95 105mg/L20

WG361367ICB 03/28/14 10:22ICB U -0.6 0.6mg/L

WG361311LRB 03/28/14 10:35LRB U -0.44 0.44mg/L

WG361311LFB 03/28/14 10:38 101.8LFB II140317-2 101.8 85 115mg/L99.99364

L17343-01LFM 03/28/14 10:57 29.2 105.2LFM II140317-2 134.4 70 130mg/L99.99364

L17343-01LFMD 03/28/14 11:00 29.2 106LFMD II140317-2 135.2 0.5970 130mg/L 2099.99364

L17362-03LFM 03/28/14 11:32 10.1 101.8LFM II140317-2 111.9 70 130mg/L99.99364

L17362-03LFMD 03/28/14 11:35 10.1 101.5LFMD II140317-2 111.6 0.2770 130mg/L 2099.99364

Residue, Filterable (TDS) @180C SM2540C


WG361151

WG361151PBW 03/25/14 11:00PBW U -20 20mg/L

WG361151LCSW 03/25/14 11:01 94.6LCSW PCN45341 246 80 120mg/L260

L17322-05DUP 03/25/14 11:25 2220DUP 2198 1mg/L 10

Residue, Non-Filterable (TSS) @105C SM2540D


WG361160

WG361160PBW 03/25/14 11:41PBW U -15 15mg/L


L17362-01DUP RA03/25/14 12:08 190DUP 188 1.1mg/L 10

L17385-04DUP RA03/25/14 12:31 30DUP 32 6.5mg/L 10

Page 43 of 63L17362-1404111040


Inorganic QC

Summary


Scandium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 98.5ICV II140220-1 1.97 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.3 0.3mg/L

WG361133LFB 03/25/14 9:46 90.9LFB II140317-2 .91 85 115mg/L1.0009

L17312-02AS 03/25/14 9:55 U 88.9AS II140317-2 .89 85 115mg/L1.0009

L17312-02ASD 03/25/14 9:58 U 87.9ASD II140317-2 .88 1.1385 115mg/L 201.0009

L17362-06AS 03/25/14 10:36 U 85.9AS II140317-2 .86 85 115mg/L1.0009

L17362-06ASD 03/25/14 10:39 U 85.9ASD II140317-2 .86 085 115mg/L 201.0009

Scandium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 98.5ICV II140228-1 1.97 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.3 0.3mg/L

WG361311LRB 03/28/14 10:35LRB U -0.22 0.22mg/L

WG361311LFB 03/28/14 10:38 105.9LFB II140317-2 1.06 85 115mg/L1.0009

L17343-01LFM 03/28/14 10:57 U 107.9LFM II140317-2 1.08 70 130mg/L1.0009


L17362-03LFM 03/28/14 11:32 U 105.9LFM II140317-2 1.06 70 130mg/L1.0009


Selenium, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 101.3ICV MS140331-9 .05063 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0003 0.0003mg/L

WG361610LFB 04/02/14 0:10 90.7LFB MS140331-2 .04542 85 115mg/L.05005

L17362-01AS 04/02/14 0:17 U 99.3AS MS140331-2 .0497 70 130mg/L.05005

L17362-01ASD 04/02/14 0:20 U 98ASD MS140331-2 .04904 1.3470 130mg/L 20.05005

Selenium, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 101.8ICV MS140331-9 .0509 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0003 0.0003mg/L

WG361306LRB 04/01/14 19:24LRB .00017 -0.00022 0.00022mg/L

WG361306LFB 04/01/14 19:27 100.9LFB MS140320-2 .05051 85 115mg/L.05005

L17362-07LFM 04/01/14 20:49 .0014 96.9LFM MS140320-2 .0499 70 130mg/L.05005

L17362-07LFMD 04/01/14 20:52 .0014 95.7LFMD MS140320-2 .04932 1.1770 130mg/L 20.05005

Silver, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 98.6ICV MS140331-9 .01974 90 110mg/L.02002

WG361610ICB 04/02/14 0:07ICB U -0.00015 0.00015mg/L

WG361610LFB 04/02/14 0:10 96.1LFB MS140331-2 .009625 85 115mg/L.01002

L17362-01AS 04/02/14 0:17 U 100.3AS MS140331-2 .01005 70 130mg/L.01002

L17362-01ASD 04/02/14 0:20 U 99.2ASD MS140331-2 .009936 1.1470 130mg/L 20.01002

Page 44 of 63L17362-1404111040


Inorganic QC

Summary


Silver, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 96.7ICV MS140331-9 .01935 90 110mg/L.02002

WG361587ICB 04/01/14 19:20ICB U -0.00015 0.00015mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00011 0.00011mg/L

WG361306LFB 04/01/14 19:27 99LFB MS140320-2 .009905 85 115mg/L.01001

L17362-07LFM 04/01/14 20:49 U 96.1LFM MS140320-2 .009616 70 130mg/L.01001


Sodium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 99.9ICV II140220-1 99.9 95 105mg/L100

WG361133ICB 03/25/14 9:33ICB U -0.6 0.6mg/L

WG361133LFB 03/25/14 9:46 91.3LFB II140317-2 91.31 85 115mg/L100.0393

L17312-02AS 03/25/14 9:55 86 88.4AS II140317-2 174.4 85 115mg/L100.0393

L17312-02ASD 03/25/14 9:58 86 87ASD II140317-2 173 0.8185 115mg/L 20100.0393

L17362-06AS 03/25/14 10:36 23.3 89.2AS II140317-2 112.5 85 115mg/L100.0393

L17362-06ASD 03/25/14 10:39 23.3 89ASD II140317-2 112.3 0.1885 115mg/L 20100.0393

Sodium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 98.8ICV II140228-1 98.78 95 105mg/L100

WG361367ICB 03/28/14 10:22ICB U -0.6 0.6mg/L

WG361311LRB 03/28/14 10:35LRB U -0.44 0.44mg/L

WG361311LFB 03/28/14 10:38 100.8LFB II140317-2 100.8 85 115mg/L100.0393

L17343-01LFM 03/28/14 10:57 578 96.4LFM II140317-2 674.4 70 130mg/L100.0393

L17343-01LFMD 03/28/14 11:00 578 102.4LFMD II140317-2 680.4 0.8970 130mg/L 20100.0393

L17362-03LFM 03/28/14 11:32 138 101.8LFM II140317-2 239.8 70 130mg/L100.0393

L17362-03LFMD 03/28/14 11:35 138 99.5LFMD II140317-2 237.5 0.9670 130mg/L 20100.0393

Strontium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 99.7ICV II140220-1 1.993 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.015 0.015mg/L

WG361133LFB 03/25/14 9:46 91.2LFB II140317-2 .456 85 115mg/L.5

L17312-02AS 03/25/14 9:55 .337 87.2AS II140317-2 .7729 85 115mg/L.5

L17312-02ASD 03/25/14 9:58 .337 87ASD II140317-2 .7719 0.1385 115mg/L 20.5

L17362-06AS 03/25/14 10:36 .188 88.9AS II140317-2 .6326 85 115mg/L.5

L17362-06ASD 03/25/14 10:39 .188 89ASD II140317-2 .6328 0.0385 115mg/L 20.5

Page 45 of 63L17362-1404111040


Inorganic QC

Summary


Strontium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 99ICV II140228-1 1.9792 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.015 0.015mg/L

WG361311LRB 03/28/14 10:35LRB U -0.011 0.011mg/L

WG361311LFB 03/28/14 10:38 99.6LFB II140317-2 .4978 85 115mg/L.5

L17343-01LFM 03/28/14 10:57 1.96 97.8LFM II140317-2 2.449 70 130mg/L.5

L17343-01LFMD 03/28/14 11:00 1.96 100.2LFMD II140317-2 2.461 0.4970 130mg/L 20.5

L17362-03LFM 03/28/14 11:32 .139 99.9LFM II140317-2 .6386 70 130mg/L.5

L17362-03LFMD 03/28/14 11:35 .139 99.7LFMD II140317-2 .6376 0.1670 130mg/L 20.5

Sulfate M300.0 - Ion Chromatography


WG360290

WG360290ICV 03/06/14 13:49 102.5ICV WI140226-1 51.2 90 110mg/L49.95

WG360290ICB 03/06/14 14:07ICB U -1.5 1.5mg/L

WG361247

WG361247LFB 03/26/14 13:20 102LFB WI140306-2 30.6 90 110mg/L30

L17336-01DUP 03/26/14 18:06 299DUP 299 0mg/L 20

L17360-01AS 03/26/14 18:42 14.3 100AS WI140306-2 44.3 90 110mg/L30

Thallium, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 105.9ICV MS140331-9 .05296 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0003 0.0003mg/L

WG361610LFB 04/02/14 0:10 95.1LFB MS140331-2 .04772 85 115mg/L.0502

L17362-01AS 04/02/14 0:17 U 103.4AS MS140331-2 .05191 70 130mg/L.0502

L17362-01ASD 04/02/14 0:20 U 101ASD MS140331-2 .05071 2.3470 130mg/L 20.0502

Thallium, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 107.3ICV MS140331-9 .05366 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0003 0.0003mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00022 0.00022mg/L

WG361306LFB 04/01/14 19:27 100.4LFB MS140320-2 .05042 85 115mg/L.0502

L17362-07LFM 04/01/14 20:49 U 101.8LFM MS140320-2 .05111 70 130mg/L.0502


Tin, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 98.8ICV MS140331-9 .04951 90 110mg/L.0501

WG361610ICB 04/02/14 0:07ICB U -0.0003 0.0003mg/L

WG361610LFB 04/02/14 0:10 90.3LFB MS140331-2 .04518 85 115mg/L.05005

L17362-01AS 04/02/14 0:17 U 96.1AS MS140331-2 .04808 70 130mg/L.05005

L17362-01ASD 04/02/14 0:20 U 95.6ASD MS140331-2 .04783 0.5270 130mg/L 20.05005

Page 46 of 63L17362-1404111040


Inorganic QC

Summary


Tin, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 98.3ICV MS140331-9 .04927 90 110mg/L.0501

WG361587ICB 04/01/14 19:20ICB U -0.0003 0.0003mg/L

WG361306LRB BF04/01/14 19:24LRB .00034 -0.00022 0.00022mg/L

WG361306LFB 04/01/14 19:27 98LFB MS140320-2 .04907 85 115mg/L.05005

L17362-07LFM 04/01/14 20:49 U 98.5LFM MS140320-2 .0493 70 130mg/L.05005


WG362051

WG362051ICV 04/09/14 19:17 102.2ICV MS140331-9 .05122 90 110mg/L.0501

WG362051ICB 04/09/14 19:21ICB U -0.0003 0.0003mg/L

WG361782LRB 04/09/14 19:24LRB U -0.00022 0.00022mg/L

WG361782LFB 04/09/14 19:27 104.5LFB MS140331-2 .05231 85 115mg/L.05005

L17464-02LFM 04/09/14 20:08 U 107.5LFM MS140331-2 .05382 70 130mg/L.05005


Titanium, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 96.3ICV II140220-1 1.9255 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.015 0.015mg/L

WG361133LFB 03/25/14 9:46 88.6LFB II140317-2 .8857 85 115mg/L1

L17312-02AS 03/25/14 9:55 U 88.2AS II140317-2 .8822 85 115mg/L1

L17312-02ASD 03/25/14 9:58 U 87.3ASD II140317-2 .8734 185 115mg/L 201

L17362-06AS 03/25/14 10:36 U 87.6AS II140317-2 .8762 85 115mg/L1

L17362-06ASD 03/25/14 10:39 U 87.5ASD II140317-2 .8746 0.1885 115mg/L 201

Titanium, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 97ICV II140228-1 1.939 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.015 0.015mg/L

WG361311LRB 03/28/14 10:35LRB U -0.011 0.011mg/L

WG361311LFB 03/28/14 10:38 100.6LFB II140317-2 1.006 85 115mg/L1

L17343-01LFM 03/28/14 10:57 .006 101.2LFM II140317-2 1.018 70 130mg/L1

L17343-01LFMD 03/28/14 11:00 .006 101.1LFMD II140317-2 1.017 0.170 130mg/L 201

L17362-03LFM 03/28/14 11:32 .112 107LFM II140317-2 1.182 70 130mg/L1

L17362-03LFMD 03/28/14 11:35 .112 107LFMD II140317-2 1.182 070 130mg/L 201

Uranium, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 102.8ICV MS140331-9 .05141 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0003 0.0003mg/L

WG361610LFB 04/02/14 0:10 98LFB MS140331-2 .04901 85 115mg/L.05

L17362-01AS 04/02/14 0:17 U 108.2AS MS140331-2 .05409 70 130mg/L.05

L17362-01ASD 04/02/14 0:20 U 108ASD MS140331-2 .05401 0.1570 130mg/L 20.05

Page 47 of 63L17362-1404111040


Inorganic QC

Summary


Uranium, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 105.3ICV MS140331-9 .05266 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0003 0.0003mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00022 0.00022mg/L

WG361306LFB 04/01/14 19:27 103.8LFB MS140320-2 .05191 85 115mg/L.05

L17362-07LFM 04/01/14 20:49 .0029 107.6LFM MS140320-2 .0567 70 130mg/L.05

L17362-07LFMD 04/01/14 20:52 .0029 107.5LFMD MS140320-2 .05665 0.0970 130mg/L 20.05

Vanadium, dissolved M200.8 ICP-MS


WG361610

WG361610ICV 04/02/14 0:03 97.5ICV MS140331-9 .04874 90 110mg/L.05

WG361610ICB 04/02/14 0:07ICB U -0.0006 0.0006mg/L

WG361610LFB 04/02/14 0:10 93.7LFB MS140331-2 .04691 85 115mg/L.05005

L17362-01AS 04/02/14 0:17 U 98.3AS MS140331-2 .04919 70 130mg/L.05005

L17362-01ASD 04/02/14 0:20 U 97ASD MS140331-2 .04855 1.3170 130mg/L 20.05005

Vanadium, total M200.8 ICP-MS


WG361587

WG361587ICV 04/01/14 19:17 98.4ICV MS140331-9 .04919 90 110mg/L.05

WG361587ICB 04/01/14 19:20ICB U -0.0006 0.0006mg/L

WG361306LRB 04/01/14 19:24LRB U -0.00044 0.00044mg/L

WG361306LFB 04/01/14 19:27 99.6LFB MS140320-2 .04985 85 115mg/L.05005

L17362-07LFM 04/01/14 20:49 .0207 99.7LFM MS140320-2 .07059 70 130mg/L.05005

L17362-07LFMD 04/01/14 20:52 .0207 98.4LFMD MS140320-2 .06994 0.9370 130mg/L 20.05005

Zinc, dissolved M200.7 ICP


WG361133

WG361133ICV 03/25/14 9:27 96.8ICV II140220-1 1.935 95 105mg/L2

WG361133ICB 03/25/14 9:33ICB U -0.03 0.03mg/L

WG361133LFB 03/25/14 9:46 88.5LFB II140317-2 .443 85 115mg/L.5005

L17312-02AS 03/25/14 9:55 U 87.3AS II140317-2 .437 85 115mg/L.5005

L17312-02ASD 03/25/14 9:58 U 87.3ASD II140317-2 .437 085 115mg/L 20.5005

L17362-06AS 03/25/14 10:36 U 85.3AS II140317-2 .427 85 115mg/L.5005

L17362-06ASD 03/25/14 10:39 U 84.9ASD II140317-2 .425 0.4785 115mg/L 20.5005

Page 48 of 63L17362-1404111040


Inorganic QC

Summary


Zinc, total M200.7 ICP


WG361367

WG361367ICV 03/28/14 10:16 97.8ICV II140228-1 1.955 95 105mg/L2

WG361367ICB 03/28/14 10:22ICB U -0.03 0.03mg/L

WG361311LRB 03/28/14 10:35LRB U -0.022 0.022mg/L

WG361311LFB 03/28/14 10:38 103.1LFB II140317-2 .516 85 115mg/L.5005

L17343-01LFM 03/28/14 10:57 U 105.3LFM II140317-2 .527 70 130mg/L.5005


L17362-03LFM 03/28/14 11:32 .02 102.3LFM II140317-2 .532 70 130mg/L.5005

L17362-03LFMD 03/28/14 11:35 .02 101.7LFMD II140317-2 .529 0.5770 130mg/L 20.5005

Page 49 of 63L17362-1404111040


Inorganic Extended

Qualifier Report


ACZ ID PARAMETER QUAL DESCRIPTIONMETHODWORKNUM

M2 Matrix spike recovery was low, the recovery of the associated control sample (LCS or LFB) was acceptable.

M200.7 ICPBarium, dissolvedL17362-01 WG361133

MA Recovery for either the spike or spike duplicate was outside of the acceptance limits; the RPD was within the acceptance limits.

M200.7 ICPBoron, dissolved


M200.7 ICPLithium, dissolved

RA Relative Percent Difference (RPD) was not used for data validation because the sample concentration is too low for accurate evaluation (< 10x MDL).

M300.0 - Ion ChromatographyChlorideWG361247


M335.4 - Colorimetric w/ distillation

Cyanide, totalWG361515


SM4500-CN I-Colorimetric w/ distillation

Cyanide, WADWG361379

DC Sample required dilution. Non-target analyte exceeded calibration range.

M300.0 - Ion ChromatographyFluorideWG361247


M300.0 - Ion Chromatography


M350.1 - Automated PhenateNitrogen, ammoniaWG361369


M365.1 - Auto Ascorbic Acid (digest)

Phosphorus, totalWG361833

RO The duplicate originally assigned to this sample was not used for precision assessment because residue density exceeded the method limits. Another duplicate in the batch was used to assess precision. Method required duplicate frequency was not met.

SM2540CResidue, Filterable (TDS) @180CWG361151


SM2540DResidue, Non-Filterable (TSS) @105CWG361160

RA Relative Percent Difference (RPD) was not used for data

validation because the sample concentration is too low for accurate evaluation (< 10x MDL).

SM2320B - TitrationTotal AlkalinityWG361281

REPAD.15.06.05.01

Page 50 of 63L17362-1404111040


Inorganic Extended

Qualifier Report



M1 Matrix spike recovery was high, the recovery of the associated control sample (LCS or LFB) was acceptable.

M200.7 ICPAluminum, totalL17362-02 WG361367


M200.7 ICPBarium, dissolvedWG361133



M3 The spike recovery value is unusable since the analyte concentration in the sample is disproportionate to the spike level. The recovery of the associated control sample (LCS or LFB) was acceptable.

M200.7 ICPIron, totalWG361367


M200.7 ICPLithium, dissolvedWG361133

BF Target analyte in prep / method blank at or above the acceptance criteria. Target analyte was not detected in the sample [< MDL].

M200.8 ICP-MSTin, totalWG361587














M350.1 - Automated Phenate











REPAD.15.06.05.01

Page 51 of 63L17362-1404111040


Inorganic Extended

Qualifier Report



DJ Sample dilution required due to insufficient sample.M200.2 ICP-MSTotal Hot Plate DigestionL17362-03 WG361782


M200.7 ICPAluminum, totalWG361367





M3 The spike recovery value is unusable since the analyte

concentration in the sample is disproportionate to the spike level. The recovery of the associated control sample (LCS or LFB) was acceptable.








M335.4 - Colorimetric w/

distillation







M1 Matrix spike recovery was high, the recovery of the

associated control sample (LCS or LFB) was acceptable.















Cyanide, totalL17362-04 WG361515




REPAD.15.06.05.01

Page 52 of 63L17362-1404111040


Inorganic Extended

Qualifier Report







































REPAD.15.06.05.01

Page 53 of 63L17362-1404111040


Inorganic Extended

Qualifier Report




































REPAD.15.06.05.01

Page 54 of 63L17362-1404111040


Inorganic Extended

Qualifier Report










































REPAD.15.06.05.01

Page 55 of 63L17362-1404111040


Certification

Qualifiers


Metals Analysis

The following parameters are not offered for certification or are not covered by NELAC certificate #ACZ.









REPAD.05.06.05.01

Page 56 of 63L17362-1404111040


Sample

Receipt

SPF Water EngineeringCalico 1st Quarter 2014 Sampling

ACZ Project ID:

Date Received:

Received By: mtb

03/21/2014 08:44

L17362

Date Printed: 3/21/2014

Chain of Custody Related Remarks

Client Contact Remarks

NANOYES

X

X

X

X

X

X

1) Is a foreign soil permit included for applicable samples?

2) Is the Chain of Custody or other directive shipping papers present?

3) Does this project require special handling procedures such as CLP protocol?

4) Are any samples NRC licensable material?

5) If samples are received past hold time, proceed with requested short hold time analyses?

6) Is the Chain of Custody complete and accurate?

7) Were any changes made to the Chain of Custody prior to ACZ receiving the samples?

Receipt Verification

NANOYES

X

X

X

X

X

X

X

X

X8) Are all containers intact and with no leaks?

9) Are all labels on containers and are they intact and legible?

10) Do the sample labels and Chain of Custody match for Sample ID, Date, and Time?

11) For preserved bottle types, was the pH checked and within limits?

12) Is there sufficient sample volume to perform all requested work?

13) Is the custody seal intact on all containers?

14) Are samples that require zero headspace acceptable?

15) Are all sample containers appropriate for analytical requirements?

16) Is there an Hg-1631 trip blank present?

17) Is there a VOA trip blank present?

18) Were all samples received within hold time?

Samples/Containers

X

X

Shipping Containers

Client must contact an ACZ Project Manager if analysis should not proceed for samples received outside of their thermal preservation acceptance criteria.

Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- ------- -------------NA19328 0.5 16 Yes

X

Was ice present in the shipment container(s)?

Yes - Wet ice was present in the shipment container (s).

REPAD LPII 2012-03

Page 57 of 63L17362-1404111040

Page 58 of 63L17362-1404111040

Page 59 of 63L17362-1404111040

Page 60 of 63L17362-1404111040

Page 61 of 63L17362-1404111040

Page 62 of 63L17362-1404111040

Page 63 of 63L17362-1404111040


Analytical

Report



Boise, ID 83706


Jason Thompson:







Jason Thompson

April 14, 2014




Boise, ID 83706

Crystal Jensen

Report to: Bill to:

Page 1 of 60L17433-1404141323


Case

Narrative



April 14, 2014

Sample Receipt

Sample Analysis

Holding Times






REPAD.03.06.05.01 Page 2 of 60L17433-1404141323


Sample ID: 59772






Results

Date Sampled: 03/24/14 11:05



Inorganic Prep

XQDilution

Cyanide, total M335.4 - Manual Distillation tcd04/01/14 15:31



bsu04/01/14 15:30


M200.2 ICP jjc03/31/14 11:54


M200.2 ICP-MS las04/02/14 11:13


Page 3 of 60L17433-1404141323


Sample ID: 59772






Results

Date Sampled: 03/24/14 11:05



Metals Analysis

XQDilution

Aluminum, dissolved M200.7 ICP mg/L 0.2U aeb0.03 03/27/14 16:411


Antimony, dissolved M200.8 ICP-MS 0.0006 mg/L 0.002B msh0.0004 04/07/14 15:431

Antimony, total M200.8 ICP-MS 0.0007 mg/L 0.002B msh0.0004 04/03/14 22:071

Arsenic, dissolved M200.8 ICP-MS 0.0372 mg/L 0.001 msh0.0002 04/07/14 15:431

Arsenic, total M200.8 ICP-MS 0.0348 mg/L 0.001 msh0.0002 04/03/14 22:071

Barium, dissolved M200.7 ICP 0.024 mg/L 0.02 aeb0.003 03/27/14 16:411


Beryllium, dissolved M200.8 ICP-MS mg/L 0.0003U pmc0.00005 04/09/14 4:331

Beryllium, total M200.8 ICP-MS mg/L 0.0003U msh0.00005 04/03/14 22:071

Bismuth, dissolved M200.7 ICP mg/L 0.2U aeb0.04* 03/27/14 16:411

Bismuth, total M200.7 ICP mg/L 0.2U jjc0.04* 04/01/14 10:301

Boron, dissolved M200.7 ICP 0.08 mg/L 0.05 aeb0.01 03/27/14 16:411


Cadmium, dissolved M200.8 ICP-MS mg/L 0.0005U pmc0.0001 04/09/14 4:331

Cadmium, total M200.8 ICP-MS mg/L 0.0005U msh0.0001 04/03/14 22:071

Calcium, dissolved M200.7 ICP 37.9 mg/L 0.5 aeb0.1 03/27/14 16:411


Chromium, dissolved M200.8 ICP-MS 0.0007 mg/L 0.002B msh0.0005 04/07/14 15:431

Chromium, total M200.8 ICP-MS 0.0008 mg/L 0.002B msh0.0005 04/03/14 22:071

Cobalt, dissolved M200.8 ICP-MS 0.00016 mg/L 0.0003B msh0.00005 04/07/14 15:431

Cobalt, total M200.8 ICP-MS 0.00008 mg/L 0.0003B msh0.00005 04/03/14 22:071

Copper, dissolved M200.8 ICP-MS mg/L 0.003U msh0.0005 04/07/14 15:431

Copper, total M200.8 ICP-MS mg/L 0.003U msh0.0005 04/03/14 22:071

Gallium, dissolved M200.7 ICP mg/L 0.5U aeb0.1* 03/27/14 16:411


Iron, dissolved M200.7 ICP mg/L 0.05U aeb0.02 03/27/14 16:411

Iron, total M200.7 ICP mg/L 0.05U jjc0.02 04/01/14 10:301

Lead, dissolved M200.8 ICP-MS mg/L 0.0005U msh0.0001 04/07/14 15:431

Lead, total M200.8 ICP-MS mg/L 0.0005U msh0.0001 04/03/14 22:071

Lithium, dissolved M200.7 ICP 0.038 mg/L 0.04B aeb0.008 03/27/14 16:411


Magnesium, dissolved M200.7 ICP 6.8 mg/L 1 aeb0.2 03/27/14 16:411


Manganese, dissolved M200.8 ICP-MS mg/L 0.003U msh0.0005 04/07/14 15:431

Manganese, total M200.8 ICP-MS mg/L 0.003U msh0.0005 04/03/14 22:071


Mercury, total M1631, Atomic Fluorescence ng/L 0.5U las0.2 04/03/14 10:171

Molybdenum, dissolved M200.8 ICP-MS 0.0034 mg/L 0.003 msh0.0005 04/07/14 15:431

Molybdenum, total M200.8 ICP-MS 0.0038 mg/L 0.003 msh0.0005 04/03/14 22:071

Nickel, dissolved M200.8 ICP-MS mg/L 0.003U msh0.0006 04/07/14 15:431

Nickel, total M200.8 ICP-MS mg/L 0.003U msh0.0006 04/03/14 22:071

Potassium, dissolved M200.7 ICP 5.8 mg/L 1 aeb0.2 03/27/14 16:411


Page 4 of 60L17433-1404141323


Sample ID: 59772






Results

Date Sampled: 03/24/14 11:05



Scandium, dissolved M200.7 ICP mg/L 0.5U aeb0.1* 03/27/14 16:411


Selenium, dissolved M200.8 ICP-MS 0.0030 mg/L 0.0003 pmc0.0001 04/09/14 4:331

Selenium, total M200.8 ICP-MS 0.0025 mg/L 0.0003 msh0.0001 04/03/14 22:071

Silver, dissolved M200.8 ICP-MS mg/L 0.0003U msh0.00005 04/07/14 15:431

Silver, total M200.8 ICP-MS mg/L 0.0003U msh0.00005 04/03/14 22:071

Sodium, dissolved M200.7 ICP 25.3 mg/L 1 aeb0.2 03/27/14 16:411


Strontium, dissolved M200.7 ICP 0.196 mg/L 0.03 aeb0.005 03/27/14 16:411


Thallium, dissolved M200.8 ICP-MS mg/L 0.0005U msh0.0001 04/07/14 15:431

Thallium, total M200.8 ICP-MS mg/L 0.0005U msh0.0001 04/03/14 22:071

Tin, dissolved M200.8 ICP-MS mg/L 0.0005U msh0.0001* 04/07/14 15:431

Tin, total M200.8 ICP-MS mg/L 0.0005U msh0.0001* 04/03/14 22:071

Titanium, dissolved M200.7 ICP mg/L 0.03U aeb0.005 03/27/14 16:411


Uranium, dissolved M200.8 ICP-MS 0.0015 mg/L 0.0005 msh0.0001 04/07/14 15:431

Uranium, total M200.8 ICP-MS 0.0017 mg/L 0.0005 msh0.0001 04/03/14 22:071

Vanadium, dissolved M200.8 ICP-MS 0.0168 mg/L 0.001 msh0.0002 04/07/14 15:431

Vanadium, total M200.8 ICP-MS 0.0181 mg/L 0.001 msh0.0002 04/03/14 22:071

Zinc, dissolved M200.7 ICP mg/L 0.05U aeb0.01 03/27/14 16:411



Page 5 of 60L17433-1404141323


Sample ID: 59772






Results

Date Sampled: 03/24/14 11:05



Wet Chemistry

XQDilution



102 mg/L 20 dcw2 03/27/14 0:001



Total Alkalinity 102 mg/L 20 dcw2 03/27/14 0:001



Cyanide, total M335.4 - Colorimetric w/ distillation mg/L 0.01U tcd0.003* 04/02/14 13:530.5


mg/L 0.01U mpb0.003* 03/31/14 16:280.5



Nitrate/Nitrite as N M353.2 - H2SO4 preserved 1.28 mg/L 0.1 pjb0.02* 04/05/14 14:541


pH (lab) SM4500H+ B

pH 8.2 units 0.1H dcw0.1 03/27/14 0:001



0.03 mg/L 0.05B pjb0.01* 04/02/14 23:491


SM2540C 280 mg/L 20 enb10 03/28/14 14:521


SM2540D mg/L 20U dcw5* 03/28/14 15:151

Sulfate M300.0 - Ion Chromatography 36.6 mg/L 2.5 tcd0.5* 04/03/14 19:301


Page 6 of 60L17433-1404141323


Sample ID: 59760






Results

Date Sampled: 03/24/14 12:35



Inorganic Prep

XQDilution




bsu04/01/14 15:39


M200.2 ICP-MS las04/02/14 11:23


M200.2 ICP jjc03/31/14 12:05


Page 7 of 60L17433-1404141323


Sample ID: 59760






Results

Date Sampled: 03/24/14 12:35



Metals Analysis

XQDilution


















Calcium, total M200.7 ICP 39 mg/L 0.5 jjc0.1 04/01/14 10:331





Copper, dissolved M200.8 ICP-MS 0.0062 mg/L 0.003 msh0.0005 04/07/14 15:461

Copper, total M200.8 ICP-MS 0.0115 mg/L 0.003 msh0.0005 04/03/14 22:101






Lead, total M200.8 ICP-MS 0.0007 mg/L 0.0005 msh0.0001 04/03/14 22:101

Lithium, dissolved M200.7 ICP 0.047 mg/L 0.04 aeb0.008 03/27/14 16:561





Manganese, total M200.8 ICP-MS 0.0061 mg/L 0.003 msh0.0005 04/03/14 22:101



Molybdenum, dissolved M200.8 ICP-MS 0.0029 mg/L 0.003B msh0.0005 04/07/14 15:461






Page 8 of 60L17433-1404141323


Sample ID: 59760






Results

Date Sampled: 03/24/14 12:35


























Page 9 of 60L17433-1404141323


Sample ID: 59760






Results

Date Sampled: 03/24/14 12:35



Wet Chemistry

XQDilution



132 mg/L 20 dcw2 03/27/14 0:001








mg/L 0.01U tcd0.003* 04/02/14 14:590.5





pH (lab) SM4500H+ B

pH 8.2 units 0.1H dcw0.1 03/27/14 0:001



0.02 mg/L 0.05B pjb0.01* 04/02/14 23:501


SM2540C 280 mg/L 20 enb10 03/28/14 14:551


SM2540D 22 mg/L 20 dcw5* 03/28/14 15:181



Page 10 of 60L17433-1404141323


Sample ID: 59760-DUP






Results

Date Sampled: 03/24/14 12:40



Inorganic Prep

XQDilution




bsu04/01/14 15:48


M200.2 ICP-MS las04/02/14 11:32


M200.2 ICP jjc03/31/14 12:17


Page 11 of 60L17433-1404141323








Results

Date Sampled: 03/24/14 12:40



Metals Analysis

XQDilution























Copper, dissolved M200.8 ICP-MS 0.0040 mg/L 0.003 msh0.0005 04/07/14 15:501

Copper, total M200.8 ICP-MS 0.0080 mg/L 0.003 msh0.0005 04/03/14 22:141






Lead, total M200.8 ICP-MS 0.0004 mg/L 0.0005B msh0.0001 04/03/14 22:141







Mercury, dissolved M1631, Atomic Fluorescence ng/L 0.5U las0.2* 04/01/14 17:371

Mercury, total M1631, Atomic Fluorescence 0.2 ng/L 0.5B las0.2 04/03/14 10:371







Page 12 of 60L17433-1404141323








Results

Date Sampled: 03/24/14 12:40








Silver, total M200.8 ICP-MS 0.00005 mg/L 0.0003B msh0.00005 04/03/14 22:141


















Page 13 of 60L17433-1404141323








Results

Date Sampled: 03/24/14 12:40



Wet Chemistry

XQDilution



116 mg/L 20 dcw2 03/27/14 0:001








mg/L 0.01U tcd0.003* 04/02/14 15:010.5





pH (lab) SM4500H+ B

pH 8.2 units 0.1H dcw0.1 03/27/14 0:001



0.02 mg/L 0.05B pjb0.01* 04/02/14 23:511


SM2540C 270 mg/L 20 enb10* 03/28/14 15:021


SM2540D 13 mg/L 20B dcw5* 03/28/14 15:201



Page 14 of 60L17433-1404141323








Results

Date Sampled: 03/24/14 00:00



Inorganic Prep

XQDilution




Wet Chemistry

XQDilution



mg/L 0.01U tcd0.003* 04/02/14 15:020.5


Page 15 of 60L17433-1404141323


Sample ID: DEPOSIT RE-SAMPLE






Results

Date Sampled: 03/16/14 12:35



Metals Analysis

XQDilution

Mercury, dissolved M1631, Atomic Fluorescence 0.4 ng/L 0.5B las0.2* 04/01/14 17:421



Page 16 of 60L17433-1404141323


Sample ID: BLM






Results

Date Sampled: 03/24/14 13:45



Inorganic Prep

XQDilution


Cyanide, WAD SM4500-CN I- distillation tcd04/04/14 11:00


bsu04/01/14 15:57


M200.2 ICP jjc03/31/14 12:52


M200.2 ICP-MS las04/02/14 11:42


Page 17 of 60L17433-1404141323


Sample ID: BLM






Results

Date Sampled: 03/24/14 13:45



Metals Analysis

XQDilution





Arsenic, dissolved M200.8 ICP-MS 3.630 mg/L 0.04 pmc0.008 04/10/14 6:2540

Arsenic, total M200.8 ICP-MS 3.750 mg/L 0.04 pmc0.008 04/09/14 22:0940




Beryllium, total M200.8 ICP-MS mg/L 0.01U pmc0.002 04/09/14 22:0940







Calcium, dissolved M200.7 ICP 157 mg/L 0.5 aeb0.1 03/27/14 17:031


Chromium, dissolved M200.8 ICP-MS mg/L 0.002U msh0.0005 04/07/14 15:531

Chromium, total M200.8 ICP-MS mg/L 0.002U msh0.0005 04/03/14 22:241

Cobalt, dissolved M200.8 ICP-MS 0.08330 mg/L 0.0003 msh0.00005 04/07/14 15:531

Cobalt, total M200.8 ICP-MS 0.08309 mg/L 0.0003 msh0.00005 04/03/14 22:241





Iron, dissolved M200.7 ICP 163 mg/L 0.05 aeb0.02 03/27/14 17:031

Iron, total M200.7 ICP 156 mg/L 0.05 jjc0.02 04/01/14 10:461


Lead, total M200.8 ICP-MS mg/L 0.0005U msh0.0001 04/03/14 22:241





Manganese, dissolved M200.8 ICP-MS 1.31 mg/L 0.1 pmc0.02 04/10/14 6:2540

Manganese, total M200.8 ICP-MS 1.34 mg/L 0.1 pmc0.02 04/09/14 22:0940

Mercury, dissolved M1631, Atomic Fluorescence 0.5 ng/L 0.5 las0.2* 04/01/14 17:571



Molybdenum, total M200.8 ICP-MS 0.0015 mg/L 0.003B msh0.0005 04/03/14 22:241

Nickel, dissolved M200.8 ICP-MS 0.0844 mg/L 0.003 msh0.0006 04/07/14 15:531

Nickel, total M200.8 ICP-MS 0.0831 mg/L 0.003 msh0.0006 04/03/14 22:241

Potassium, dissolved M200.7 ICP 6 mg/L 1 aeb0.2 03/27/14 17:031


Page 18 of 60L17433-1404141323


Sample ID: BLM






Results

Date Sampled: 03/24/14 13:45





Selenium, dissolved M200.8 ICP-MS mg/L 0.0003U pmc0.0001 04/09/14 4:421

Selenium, total M200.8 ICP-MS mg/L 0.0003U msh0.0001* 04/03/14 22:241



Sodium, dissolved M200.7 ICP 275 mg/L 1 aeb0.2 03/27/14 17:031










Uranium, dissolved M200.8 ICP-MS 0.0002 mg/L 0.0005B msh0.0001 04/07/14 15:531

Uranium, total M200.8 ICP-MS 0.0002 mg/L 0.0005B msh0.0001 04/03/14 22:241

Vanadium, dissolved M200.8 ICP-MS mg/L 0.001U msh0.0002 04/07/14 15:531

Vanadium, total M200.8 ICP-MS mg/L 0.001U msh0.0002 04/03/14 22:241

Zinc, dissolved M200.7 ICP 0.60 mg/L 0.05 aeb0.01 03/27/14 17:031

Zinc, total M200.7 ICP 0.58 mg/L 0.05 jjc0.01 04/01/14 10:461


Page 19 of 60L17433-1404141323


Sample ID: BLM






Results

Date Sampled: 03/24/14 13:45



Wet Chemistry

XQDilution



28 mg/L 20 dcw2 03/27/14 0:001








mg/L 0.01U tcd0.003* 04/04/14 15:420.5



Nitrate/Nitrite as N M353.2 - H2SO4 preserved mg/L 0.1U pjb0.02* 04/05/14 14:211

Nitrogen, ammonia M350.1 - Automated Phenate 0.72 mg/L 0.5 tcd0.05* 04/02/14 13:041

pH (lab) SM4500H+ B

pH 6.6 units 0.1H dcw0.1 03/27/14 0:001



0.35 mg/L 0.05 pjb0.01* 04/02/14 23:521


SM2540C 1640 mg/L 20 enb10* 03/28/14 15:051


SM2540D 116 mg/L 20 dcw5* 03/28/14 15:231

Sulfate M300.0 - Ion Chromatography 1070 mg/L 50 tcd10* 04/04/14 11:3620


Page 20 of 60L17433-1404141323


Sample ID: 59763






Results

Date Sampled: 03/24/14 15:15



Inorganic Prep

XQDilution




bsu04/01/14 16:06


M200.2 ICP-MS las04/02/14 11:52


M200.2 ICP jjc03/31/14 13:03


Page 21 of 60L17433-1404141323


Sample ID: 59763






Results

Date Sampled: 03/24/14 15:15



Metals Analysis

XQDilution


Aluminum, total M200.7 ICP 0.12 mg/L 0.2B jjc0.03* 04/01/14 10:491








Beryllium, total M200.8 ICP-MS mg/L 0.0003U msh0.00005* 04/03/14 22:271

















Iron, dissolved M200.7 ICP 0.09 mg/L 0.05 aeb0.02 03/27/14 17:061








Manganese, dissolved M200.8 ICP-MS 0.0838 mg/L 0.003 msh0.0005 04/07/14 15:571










Page 22 of 60L17433-1404141323


Sample ID: 59763






Results

Date Sampled: 03/24/14 15:15






Selenium, total M200.8 ICP-MS 0.0004 mg/L 0.0003 pmc0.0001 04/09/14 22:121




















Page 23 of 60L17433-1404141323


Sample ID: 59763






Results

Date Sampled: 03/24/14 15:15



Wet Chemistry

XQDilution



166 mg/L 20 dcw2 03/27/14 0:001




Chloride M300.0 - Ion Chromatography 19.6 mg/L 25B tcd5* 04/03/14 21:1710




mg/L 0.01U tcd0.003* 04/02/14 15:030.5

Fluoride M300.0 - Ion Chromatography mg/L 5U tcd1* 04/03/14 21:1710


Nitrate/Nitrite as N M353.2 - H2SO4 preserved mg/L 0.1U pjb0.02* 04/05/14 14:231


pH (lab) SM4500H+ B

pH 8.2 units 0.1H dcw0.1 03/27/14 0:001



0.05 mg/L 0.05 pjb0.01* 04/02/14 23:531


SM2540C 1170 mg/L 20 enb10* 03/28/14 15:081


SM2540D mg/L 20U dcw5* 03/28/14 15:261

Sulfate M300.0 - Ion Chromatography 580 mg/L 25 tcd5* 04/03/14 21:1710


Page 24 of 60L17433-1404141323


Sample ID: BISHOP






Results

Date Sampled: 03/24/14 17:50



Inorganic Prep

XQDilution




bsu04/01/14 16:15


M200.2 ICP jjc03/31/14 13:15


M200.2 ICP-MS las04/02/14 12:01


Page 25 of 60L17433-1404141323


Sample ID: BISHOP






Results

Date Sampled: 03/24/14 17:50



Metals Analysis

XQDilution



Antimony, dissolved M200.8 ICP-MS mg/L 0.002U msh0.0004 04/07/14 16:001

Antimony, total M200.8 ICP-MS mg/L 0.002U msh0.0004 04/03/14 22:311



Barium, dissolved M200.7 ICP 0.015 mg/L 0.02B aeb0.003 03/27/14 17:091



Beryllium, total M200.8 ICP-MS mg/L 0.0003U msh0.00005* 04/03/14 22:311


















Iron, total M200.7 ICP 0.04 mg/L 0.05B jjc0.02 04/01/14 10:521

Lead, dissolved M200.8 ICP-MS 0.0002 mg/L 0.0005B msh0.0001 04/07/14 16:001






Manganese, dissolved M200.8 ICP-MS 0.0060 mg/L 0.003 msh0.0005 04/07/14 16:001










Page 26 of 60L17433-1404141323


Sample ID: BISHOP






Results

Date Sampled: 03/24/14 17:50


























Page 27 of 60L17433-1404141323


Sample ID: BISHOP






Results

Date Sampled: 03/24/14 17:50



Wet Chemistry

XQDilution



120 mg/L 20 dcw2 03/27/14 0:001








mg/L 0.01U tcd0.003* 04/02/14 15:040.5





pH (lab) SM4500H+ B

pH 8.4 units 0.1H dcw0.1 03/27/14 0:001



0.12 mg/L 0.05 pjb0.01* 04/02/14 23:541


SM2540C 260 mg/L 20 enb10* 03/28/14 15:111


SM2540D mg/L 20U dcw5* 03/28/14 15:281



Page 28 of 60L17433-1404141323


Sample ID: MERCURY TRIP BLANK






Results

Date Sampled: 03/24/14 17:40



Metals Analysis

XQDilution


REPIN.02.06.05.01

Page 29 of 60L17433-1404141323















QC Sample Types
























Method References






Comments








REP001.09.12.01

Inorganic

Reference

Page 30 of 60L17433-1404141323



Inorganic QC

Summary




WG361281

WG361281PBW1 03/26/14 16:40PBW U -20 20mg/L



WG361281PBW2 03/26/14 20:01PBW 2.5 -20 20mg/L


WG361281PBW3 03/26/14 23:35PBW 2.6 -20 20mg/L


WG361281PBW4 03/27/14 2:35PBW 2.9 -20 20mg/L

L17433-08DUP 03/27/14 5:14 123DUP 125.4 1.9mg/L 20




WG361340

WG361340ICV 03/27/14 15:22 96.5ICV II140220-1 1.929 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.09 0.09mg/L

WG361340LFB 03/27/14 15:41 99.5LFB II140317-2 .996 85 115mg/L1.0011

L17433-01AS 03/27/14 16:44 U 98.7AS II140317-2 .988 85 115mg/L1.0011

L17433-01ASD 03/27/14 16:47 U 99ASD II140317-2 .991 0.385 115mg/L 201.0011



WG361527

WG361527ICV 04/01/14 9:28 98.1ICV II140228-1 1.961 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.09 0.09mg/L

WG361468LRB 04/01/14 9:47LRB U -0.066 0.066mg/L

WG361468LFB 04/01/14 9:50 102.5LFB II140317-2 1.026 85 115mg/L1.0011

L17381-01LFM 04/01/14 9:56 19.9 123.9LFM II140317-2 21.14 70 130mg/L1.0011


L17433-03LFM M104/01/14 10:40 .37 172.3LFM II140317-2 2.095 70 130mg/L1.0011

L17433-03LFMD M104/01/14 10:43 .37 177.5LFMD II140317-2 2.147 2.4570 130mg/L 201.0011



WG361845

WG361845ICV 04/07/14 14:18 109.5ICV MS140331-9 .02192 90 110mg/L.02002

WG361845ICB 04/07/14 14:21ICB U -0.0012 0.0012mg/L

WG361845LFB 04/07/14 14:24 94.1LFB MS140331-2 .00941 85 115mg/L.01

L17399-08AS 04/07/14 15:23 U 87.5AS MS140331-2 .00875 70 130mg/L.01

L17399-08ASD 04/07/14 15:26 U 89.4ASD MS140331-2 .00894 2.1570 130mg/L 20.01

Page 31 of 60L17433-1404141323


Inorganic QC

Summary




WG361760

WG361760ICV 04/03/14 20:59 107.2ICV MS140331-9 .02146 90 110mg/L.02002

WG361760ICB 04/03/14 21:02ICB U -0.0012 0.0012mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00088 0.00088mg/L

WG361557LFB 04/03/14 21:09 103.2LFB MS140331-2 .01032 85 115mg/L.01

L17433-08LFM 04/03/14 22:34 U 101.7LFM MS140331-2 .01017 70 130mg/L.01

L17433-08LFMD 04/03/14 22:37 U 101.7LFMD MS140331-2 .01017 070 130mg/L 20.01



WG361845

WG361845ICV 04/07/14 14:18 98.7ICV MS140331-9 .04934 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.0006 0.0006mg/L

WG361845LFB 04/07/14 14:24 103.7LFB MS140331-2 .05197 85 115mg/L.0501

L17399-08AS 04/07/14 15:23 .0011 101.1AS MS140331-2 .05177 70 130mg/L.0501

L17399-08ASD 04/07/14 15:26 .0011 98.2ASD MS140331-2 .05029 2.970 130mg/L 20.0501

WG362063

WG362063ICV 04/10/14 5:36 101ICV MS140331-9 .05049 90 110mg/L.05

WG362063ICB 04/10/14 5:39ICB U -0.0006 0.0006mg/L

WG362063LFB 04/10/14 5:43 88.9LFB MS140331-2 .04454 85 115mg/L.0501

L17282-01AS 04/10/14 5:49 .0042 97AS MS140331-2 .05282 70 130mg/L.0501

L17282-01ASD 04/10/14 5:52 .0042 101.8ASD MS140331-2 .05521 4.4270 130mg/L 20.0501



WG361760

WG361760ICV 04/03/14 20:59 101ICV MS140331-9 .0505 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0006 0.0006mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00044 0.00044mg/L

WG361557LFB 04/03/14 21:09 104.6LFB MS140331-2 .0524 85 115mg/L.0501

L17433-08LFM 04/03/14 22:34 .0078 95.9LFM MS140331-2 .05586 70 130mg/L.0501

L17433-08LFMD 04/03/14 22:37 .0078 95.3LFMD MS140331-2 .05554 0.5770 130mg/L 20.0501

WG361975

WG361975ICV 04/09/14 21:56 101.6ICV MS140331-9 .05079 90 110mg/L.05

WG361975ICB 04/09/14 21:59ICB U -0.0006 0.0006mg/L

WG361557LRB 04/09/14 22:02LRB U -0.00044 0.00044mg/L

WG361557LFB 04/09/14 22:05 109LFB MS140331-2 .05462 85 115mg/L.0501

L17433-08LFM 04/09/14 22:18 .008 98.6LFM MS140331-2 .05742 70 130mg/L.0501

L17433-08LFMD 04/09/14 22:21 .008 99.1LFMD MS140331-2 .05763 0.3770 130mg/L 20.0501

Page 32 of 60L17433-1404141323


Inorganic QC

Summary




WG361340

WG361340ICV 03/27/14 15:22 97.7ICV II140220-1 1.9548 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.009 0.009mg/L

WG361340LFB 03/27/14 15:41 96.8LFB II140317-2 .4842 85 115mg/L.5

L17433-01AS 03/27/14 16:44 .024 98AS II140317-2 .5138 85 115mg/L.5

L17433-01ASD 03/27/14 16:47 .024 98.4ASD II140317-2 .5161 0.4585 115mg/L 20.5



WG361574

WG361574ICV 04/01/14 15:18 98.4ICV II140228-1 1.9688 95 105mg/L2

WG361574ICB 04/01/14 15:24ICB U -0.009 0.009mg/L

WG361468LRB 04/01/14 15:37LRB U -0.0066 0.0066mg/L

WG361468LFB 04/01/14 15:40 101LFB II140317-2 .5051 85 115mg/L.5

L17381-01LFM 04/01/14 15:46 .024 99.6LFM II140317-2 .5221 70 130mg/L.5

L17381-01LFMD 04/01/14 15:49 .024 99.3LFMD II140317-2 .5206 0.2970 130mg/L 20.5

L17433-03LFM 04/01/14 16:30 .056 101.8LFM II140317-2 .565 70 130mg/L.5

L17433-03LFMD 04/01/14 16:33 .056 101.9LFMD II140317-2 .5655 0.0970 130mg/L 20.5



WG361971

WG361971ICV 04/09/14 3:41 94.5ICV MS140331-9 .04727 90 110mg/L.05

WG361971ICB 04/09/14 3:44ICB U -0.00015 0.00015mg/L

WG361971LFB 04/09/14 3:47 90.8LFB MS140331-2 .04547 85 115mg/L.05005

L17399-08AS 04/09/14 4:03 U 100.7AS MS140331-2 .05038 70 130mg/L.05005

L17399-08ASD 04/09/14 4:07 U 100.6ASD MS140331-2 .05034 0.0870 130mg/L 20.05005

L17475-03AS 04/09/14 5:08 .00058 98.2AS MS140331-2 .04971 70 130mg/L.05005

L17475-03ASD 04/09/14 5:12 .00058 98.8ASD MS140331-2 .05002 0.6270 130mg/L 20.05005



WG361760

WG361760ICV 04/03/14 20:59 96.5ICV MS140331-9 .04824 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.00015 0.00015mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00011 0.00011mg/L

WG361557LFB 04/03/14 21:09 98.4LFB MS140331-2 .04925 85 115mg/L.05005

L17433-08LFM 04/03/14 22:34 U 100.5LFM MS140331-2 .05031 70 130mg/L.05005


WG361975

WG361975ICV 04/09/14 21:56 91.3ICV MS140331-9 .04566 90 110mg/L.05

WG361975ICB 04/09/14 21:59ICB U -0.00015 0.00015mg/L

WG361557LRB 04/09/14 22:02LRB U -0.00011 0.00011mg/L

WG361557LFB 04/09/14 22:05 96.5LFB MS140331-2 .04832 85 115mg/L.05005

L17433-08LFM 04/09/14 22:18 U 94.5LFM MS140331-2 .0473 70 130mg/L.05005


Page 33 of 60L17433-1404141323


Inorganic QC

Summary




WG361340

WG361340ICV 03/27/14 15:22 98.8ICV II140220-1 1.976 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.12 0.12mg/L

WG361340LFB 03/27/14 15:41 98.9LFB II140317-2 .988 85 115mg/L.999

L17433-01AS 03/27/14 16:44 U 100.2AS II140317-2 1.001 85 115mg/L.999

L17433-01ASD 03/27/14 16:47 U 99.1ASD II140317-2 .99 1.185 115mg/L 20.999



WG361527

WG361527ICV 04/01/14 9:28 100ICV II140228-1 1.999 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.12 0.12mg/L

WG361468LRB 04/01/14 9:47LRB U -0.088 0.088mg/L

WG361468LFB 04/01/14 9:50 102.4LFB II140317-2 1.023 85 115mg/L.999

L17381-01LFM 04/01/14 9:56 U 96.4LFM II140317-2 .963 70 130mg/L.999


L17433-03LFM 04/01/14 10:40 U 101.9LFM II140317-2 1.018 70 130mg/L.999




WG361340

WG361340ICV 03/27/14 15:22 99.6ICV II140220-1 1.992 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.03 0.03mg/L

WG361340LFB 03/27/14 15:41 98.5LFB II140317-2 .493 85 115mg/L.5005

L17433-01AS 03/27/14 16:44 .08 98.3AS II140317-2 .572 85 115mg/L.5005

L17433-01ASD 03/27/14 16:47 .08 98.5ASD II140317-2 .573 0.1785 115mg/L 20.5005



WG361527

WG361527ICV 04/01/14 9:28 98.4ICV II140228-1 1.967 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.03 0.03mg/L

WG361468LRB 04/01/14 9:47LRB U -0.022 0.022mg/L

WG361468LFB 04/01/14 9:50 100.1LFB II140317-2 .501 85 115mg/L.5005

L17381-01LFM 04/01/14 9:56 .07 99.7LFM II140317-2 .569 70 130mg/L.5005

L17381-01LFMD 04/01/14 9:59 .07 100.5LFMD II140317-2 .573 0.770 130mg/L 20.5005

L17433-03LFM 04/01/14 10:40 .07 99.1LFM II140317-2 .566 70 130mg/L.5005

L17433-03LFMD 04/01/14 10:43 .07 97.3LFMD II140317-2 .557 1.670 130mg/L 20.5005

Page 34 of 60L17433-1404141323


Inorganic QC

Summary




WG361971

WG361971ICV 04/09/14 3:41 97.7ICV MS140331-9 .04887 90 110mg/L.05

WG361971ICB 04/09/14 3:44ICB U -0.0003 0.0003mg/L

WG361971LFB 04/09/14 3:47 93LFB MS140331-2 .04657 85 115mg/L.0501

L17399-08AS 04/09/14 4:03 .0001 98.4AS MS140331-2 .04939 70 130mg/L.0501

L17399-08ASD 04/09/14 4:07 .0001 97.9ASD MS140331-2 .04913 0.5370 130mg/L 20.0501

L17475-03AS 04/09/14 5:08 U 98.2AS MS140331-2 .04922 70 130mg/L.0501

L17475-03ASD 04/09/14 5:12 U 100.5ASD MS140331-2 .05036 2.2970 130mg/L 20.0501



WG361760

WG361760ICV 04/03/14 20:59 98.4ICV MS140331-9 .04922 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0003 0.0003mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00022 0.00022mg/L

WG361557LFB 04/03/14 21:09 99.7LFB MS140331-2 .04993 85 115mg/L.0501

L17433-08LFM 04/03/14 22:34 U 97.3LFM MS140331-2 .04877 70 130mg/L.0501




WG361340

WG361340ICV 03/27/14 15:22 98.3ICV II140220-1 98.28 95 105mg/L100

WG361340ICB 03/27/14 15:28ICB U -0.3 0.3mg/L

WG361340LFB 03/27/14 15:41 101LFB II140317-2 68.64 85 115mg/L67.98099

L17433-01AS 03/27/14 16:44 37.9 98AS II140317-2 104.5 85 115mg/L67.98099

L17433-01ASD 03/27/14 16:47 37.9 99.4ASD II140317-2 105.5 0.9585 115mg/L 2067.98099



WG361527

WG361527ICV 04/01/14 9:28 97.7ICV II140228-1 97.69 95 105mg/L100

WG361527ICB 04/01/14 9:34ICB U -0.3 0.3mg/L

WG361468LRB 04/01/14 9:47LRB U -0.22 0.22mg/L

WG361468LFB 04/01/14 9:50 101.7LFB II140317-2 69.12 85 115mg/L67.98099

L17381-01LFM 04/01/14 9:56 117 100LFM II140317-2 185 70 130mg/L67.98099

L17381-01LFMD 04/01/14 9:59 117 99.7LFMD II140317-2 184.8 0.1170 130mg/L 2067.98099

L17433-03LFM 04/01/14 10:40 38.5 100.5LFM II140317-2 106.8 70 130mg/L67.98099

L17433-03LFMD 04/01/14 10:43 38.5 101.4LFMD II140317-2 107.4 0.5670 130mg/L 2067.98099

Page 35 of 60L17433-1404141323


Inorganic QC

Summary




WG360290

WG360290ICV 03/06/14 13:49 101.6ICV WI140226-1 20.3 90 110mg/L19.98

WG360290ICB 03/06/14 14:07ICB U -1.5 1.5mg/L

WG361726

WG361726LFB1 04/03/14 13:31 100.3LFB WI140306-2 30.1 90 110mg/L30

L17370-02DUP RA04/03/14 18:18 94.2DUP 96.7 2.6mg/L 20

L17380-01AS 04/03/14 18:54 1600 101.3AS WI140306-2 4640 90 110mg/L3000

WG361726LFB2 04/03/14 22:11 100.3LFB WI140306-2 30.1 90 110mg/L30



WG361845

WG361845ICV 04/07/14 14:18 92.8ICV MS140331-9 .04641 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.0015 0.0015mg/L

WG361845LFB 04/07/14 14:24 98.4LFB MS140331-2 .04924 85 115mg/L.05005

L17399-08AS 04/07/14 15:23 U 89.5AS MS140331-2 .04479 70 130mg/L.05005

L17399-08ASD 04/07/14 15:26 U 89.5ASD MS140331-2 .04478 0.0270 130mg/L 20.05005



WG361760

WG361760ICV 04/03/14 20:59 98.1ICV MS140331-9 .04907 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0015 0.0015mg/L

WG361557LRB 04/03/14 21:06LRB U -0.0011 0.0011mg/L

WG361557LFB 04/03/14 21:09 97.6LFB MS140331-2 .04887 85 115mg/L.05005

L17433-08LFM 04/03/14 22:34 U 91.8LFM MS140331-2 .04594 70 130mg/L.05005




WG361845

WG361845ICV 04/07/14 14:18 97.6ICV MS140331-9 .04881 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.00015 0.00015mg/L

WG361845LFB 04/07/14 14:24 99LFB MS140331-2 .04955 85 115mg/L.05005

L17399-08AS 04/07/14 15:23 .00027 94.2AS MS140331-2 .04744 70 130mg/L.05005

L17399-08ASD 04/07/14 15:26 .00027 95.4ASD MS140331-2 .04802 1.2270 130mg/L 20.05005



WG361760

WG361760ICV 04/03/14 20:59 98.1ICV MS140331-9 .04905 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.00015 0.00015mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00011 0.00011mg/L

WG361557LFB 04/03/14 21:09 98.5LFB MS140331-2 .04929 85 115mg/L.05005

L17433-08LFM 04/03/14 22:34 .00008 97.5LFM MS140331-2 .04886 70 130mg/L.05005

L17433-08LFMD 04/03/14 22:37 .00008 98.2LFMD MS140331-2 .04923 0.7570 130mg/L 20.05005

Page 36 of 60L17433-1404141323


Inorganic QC

Summary




WG361281




WG361281LCSW11 03/27/14 2:11 100LCSW PCN43577 1409 90 110umhos/cm1408.8

L17433-08DUP 03/27/14 5:14 374DUP 381 1.9umhos/cm 20




WG361845

WG361845ICV 04/07/14 14:18 91.9ICV MS140331-9 .04595 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.0015 0.0015mg/L

WG361845LFB 04/07/14 14:24 97.6LFB MS140331-2 .04884 85 115mg/L.05005

L17399-08AS 04/07/14 15:23 U 86.2AS MS140331-2 .04315 70 130mg/L.05005

L17399-08ASD 04/07/14 15:26 U 86.1ASD MS140331-2 .04308 0.1670 130mg/L 20.05005



WG361760

WG361760ICV 04/03/14 20:59 97.1ICV MS140331-9 .04855 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0015 0.0015mg/L

WG361557LRB 04/03/14 21:06LRB U -0.0011 0.0011mg/L

WG361557LFB 04/03/14 21:09 98.4LFB MS140331-2 .04923 85 115mg/L.05005

L17433-08LFM 04/03/14 22:34 U 88.7LFM MS140331-2 .0444 70 130mg/L.05005




WG361653

WG361653ICV 04/02/14 13:09 98.6ICV WI140322-7 .2957 90 110mg/L.3

WG361653ICB 04/02/14 13:10ICB U -0.003 0.003mg/L

WG361655

WG361602LRB 04/02/14 13:47LRB U -0.003 0.003mg/L

WG361602LFB 04/02/14 13:48 107.5LFB WI140322-4 .215 90 110mg/L.2

L17386-01DUP RA04/02/14 13:50 UDUP U 0mg/L 20

L17392-01LFM 04/02/14 13:52 .064 102.1LFM WI140322-4 .2682 90 110mg/L.2

Page 37 of 60L17433-1404141323


Inorganic QC

Summary




WG361515

WG361515ICV 03/31/14 15:14 97.6ICV WI140322-7 .2928 90 110mg/L.3

WG361515ICB 03/31/14 15:15ICB U -0.003 0.003mg/L

WG361524

WG361496LRB 03/31/14 16:07LRB U -0.003 0.003mg/L

WG361496LFB 03/31/14 16:08 96.2LFB WI140322-6 .1924 90 110mg/L.2

L17387-01DUP RA03/31/14 16:21 .026DUP .0282 8.1mg/L 20

L17388-01LFM 03/31/14 16:23 U 92.7LFM WI140322-6 .1854 90 110mg/L.2

WG361653

WG361653ICV 04/02/14 13:09 98.6ICV WI140322-7 .2957 90 110mg/L.3

WG361653ICB 04/02/14 13:10ICB U -0.003 0.003mg/L

WG361673

WG361626LRB 04/02/14 14:57LRB U -0.003 0.003mg/L

WG361626LFB 04/02/14 14:58 101.8LFB WI140322-6 .2036 90 110mg/L.2

L17433-02LFM 04/02/14 15:00 U 101LFM WI140322-6 .202 90 110mg/L.2

L17433-03DUP RA04/02/14 15:01 UDUP U 0mg/L 20

WG361810

WG361810ICV 04/04/14 15:38 97.8ICV WI140322-7 .2935 90 110mg/L.3

WG361810ICB 04/04/14 15:39ICB U -0.003 0.003mg/L

WG361798LRB 04/04/14 15:40LRB U -0.003 0.003mg/L

WG361798LFB 04/04/14 15:41 95.1LFB WI140322-6 .1902 90 110mg/L.2

L17433-06DUP RA04/04/14 15:43 UDUP U 0mg/L 20

L17466-01LFM 04/04/14 15:44 U 92.7LFM WI140322-6 .1853 90 110mg/L.2



WG360290

WG360290ICV 03/06/14 13:49 103.7ICV WI140226-1 4.17 90 110mg/L4.02

WG360290ICB 03/06/14 14:07ICB U -0.3 0.3mg/L

WG361726

WG361726LFB1 04/03/14 13:31 101.3LFB WI140306-2 1.52 90 110mg/L1.5

L17370-02DUP RA04/03/14 18:18 UDUP U 0mg/L 20

L17380-01AS 04/03/14 18:54 57 103.3AS WI140306-2 212 90 110mg/L150

WG361726LFB2 04/03/14 22:11 100.7LFB WI140306-2 1.51 90 110mg/L1.5



WG361340

WG361340ICV 03/27/14 15:22 98ICV II140220-1 1.96 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.3 0.3mg/L

WG361340LFB 03/27/14 15:41 100.9LFB II140317-2 1.01 85 115mg/L1.001

L17433-01AS 03/27/14 16:44 U 95.9AS II140317-2 .96 85 115mg/L1.001

L17433-01ASD 03/27/14 16:47 U 104.9ASD II140317-2 1.05 8.9685 115mg/L 201.001

Page 38 of 60L17433-1404141323


Inorganic QC

Summary




WG361527

WG361527ICV 04/01/14 9:28 99ICV II140228-1 1.98 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.3 0.3mg/L

WG361468LRB 04/01/14 9:47LRB U -0.22 0.22mg/L

WG361468LFB 04/01/14 9:50 102.9LFB II140317-2 1.03 85 115mg/L1.001

L17381-01LFM 04/01/14 9:56 U 102.9LFM II140317-2 1.03 70 130mg/L1.001


L17433-03LFM 04/01/14 10:40 U 103.9LFM II140317-2 1.04 70 130mg/L1.001




WG361340

WG361340ICV 03/27/14 15:22 98.3ICV II140220-1 1.965 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.06 0.06mg/L

WG361340LFB 03/27/14 15:41 98.6LFB II140317-2 .987 85 115mg/L1.0014

L17433-01AS 03/27/14 16:44 U 98AS II140317-2 .981 85 115mg/L1.0014

L17433-01ASD 03/27/14 16:47 U 99.3ASD II140317-2 .994 1.3285 115mg/L 201.0014



WG361527

WG361527ICV 04/01/14 9:28 97.3ICV II140228-1 1.946 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.06 0.06mg/L

WG361468LRB 04/01/14 9:47LRB U -0.044 0.044mg/L

WG361468LFB 04/01/14 9:50 102.4LFB II140317-2 1.025 85 115mg/L1.0014

L17381-01LFM 04/01/14 9:56 .36 96.1LFM II140317-2 1.322 70 130mg/L1.0014

L17381-01LFMD 04/01/14 9:59 .36 96.5LFMD II140317-2 1.326 0.370 130mg/L 201.0014

L17433-03LFM 04/01/14 10:40 .13 116.3LFM II140317-2 1.285 70 130mg/L1.0014

L17433-03LFMD 04/01/14 10:43 .13 117.6LFMD II140317-2 1.298 1.0170 130mg/L 201.0014



WG361845

WG361845ICV 04/07/14 14:18 93.2ICV MS140331-9 .04661 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.0003 0.0003mg/L

WG361845LFB 04/07/14 14:24 90.2LFB MS140331-2 .04516 85 115mg/L.05005

L17399-08AS 04/07/14 15:23 U 88.6AS MS140331-2 .04432 70 130mg/L.05005

L17399-08ASD 04/07/14 15:26 U 89.1ASD MS140331-2 .0446 0.6370 130mg/L 20.05005

Page 39 of 60L17433-1404141323


Inorganic QC

Summary




WG361760

WG361760ICV 04/03/14 20:59 101ICV MS140331-9 .05052 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0003 0.0003mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00022 0.00022mg/L

WG361557LFB 04/03/14 21:09 96.1LFB MS140331-2 .04808 85 115mg/L.05005

L17433-08LFM 04/03/14 22:34 .0002 97.3LFM MS140331-2 .0489 70 130mg/L.05005

L17433-08LFMD 04/03/14 22:37 .0002 97LFMD MS140331-2 .04873 0.3570 130mg/L 20.05005



WG361340

WG361340ICV 03/27/14 15:22 97.7ICV II140220-1 1.9542 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.024 0.024mg/L

WG361340LFB 03/27/14 15:41 95.6LFB II140317-2 .9555 85 115mg/L1

L17433-01AS 03/27/14 16:44 .038 96.5AS II140317-2 1.003 85 115mg/L1

L17433-01ASD 03/27/14 16:47 .038 97.4ASD II140317-2 1.012 0.8985 115mg/L 201



WG361527

WG361527ICV 04/01/14 9:28 97.9ICV II140228-1 1.9588 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.024 0.024mg/L

WG361468LRB 04/01/14 9:47LRB U -0.0176 0.0176mg/L

WG361468LFB 04/01/14 9:50 98.3LFB II140317-2 .9826 85 115mg/L1

L17381-01LFM 04/01/14 9:56 .141 98LFM II140317-2 1.121 70 130mg/L1

L17381-01LFMD 04/01/14 9:59 .141 98.9LFMD II140317-2 1.13 0.870 130mg/L 201

L17433-03LFM 04/01/14 10:40 .055 100.6LFM II140317-2 1.061 70 130mg/L1

L17433-03LFMD 04/01/14 10:43 .055 100.2LFMD II140317-2 1.057 0.3870 130mg/L 201



WG361340

WG361340ICV 03/27/14 15:22 96.6ICV II140220-1 96.64 95 105mg/L100

WG361340ICB 03/27/14 15:28ICB U -0.6 0.6mg/L

WG361340LFB 03/27/14 15:41 96.9LFB II140317-2 48.44 85 115mg/L50.00131

L17433-01AS 03/27/14 16:44 6.8 96.2AS II140317-2 54.9 85 115mg/L50.00131

L17433-01ASD 03/27/14 16:47 6.8 97.2ASD II140317-2 55.38 0.8785 115mg/L 2050.00131

Page 40 of 60L17433-1404141323


Inorganic QC

Summary




WG361527

WG361527ICV 04/01/14 9:28 96ICV II140228-1 95.98 95 105mg/L100

WG361527ICB 04/01/14 9:34ICB U -0.6 0.6mg/L

WG361468LRB 04/01/14 9:47LRB U -0.44 0.44mg/L

WG361468LFB 04/01/14 9:50 97.2LFB II140317-2 48.6 85 115mg/L50.00131

L17381-01LFM 04/01/14 9:56 52 96.6LFM II140317-2 100.3 70 130mg/L50.00131

L17381-01LFMD 04/01/14 9:59 52 97.2LFMD II140317-2 100.6 0.370 130mg/L 2050.00131

L17433-03LFM 04/01/14 10:40 6.5 97.4LFM II140317-2 55.21 70 130mg/L50.00131

L17433-03LFMD 04/01/14 10:43 6.5 97.7LFMD II140317-2 55.34 0.2470 130mg/L 2050.00131



WG361845

WG361845ICV 04/07/14 14:18 101.9ICV MS140331-9 .05095 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.0015 0.0015mg/L

WG361845LFB 04/07/14 14:24 99.7LFB MS140331-2 .04996 85 115mg/L.0501

L17399-08AS 04/07/14 15:23 .0026 96.5AS MS140331-2 .05095 70 130mg/L.0501

L17399-08ASD 04/07/14 15:26 .0026 97.4ASD MS140331-2 .05138 0.8470 130mg/L 20.0501

WG362063

WG362063ICV 04/10/14 5:36 99.2ICV MS140331-9 .0496 90 110mg/L.05

WG362063ICB 04/10/14 5:39ICB U -0.0015 0.0015mg/L

WG362063LFB 04/10/14 5:43 88LFB MS140331-2 .0441 85 115mg/L.0501

L17282-01AS 04/10/14 5:49 .2043 92.2AS MS140331-2 .2505 70 130mg/L.0501

L17282-01ASD 04/10/14 5:52 .2043 92.6ASD MS140331-2 .2507 0.0870 130mg/L 20.0501



WG361760

WG361760ICV 04/03/14 20:59 102.8ICV MS140331-9 .05138 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0015 0.0015mg/L

WG361557LRB 04/03/14 21:06LRB U -0.0011 0.0011mg/L

WG361557LFB 04/03/14 21:09 97.2LFB MS140331-2 .04872 85 115mg/L.0501

L17433-08LFM 04/03/14 22:34 .0067 97.2LFM MS140331-2 .05542 70 130mg/L.0501

L17433-08LFMD 04/03/14 22:37 .0067 97.7LFMD MS140331-2 .05567 0.4570 130mg/L 20.0501

WG361975

WG361975ICV 04/09/14 21:56 98.8ICV MS140331-9 .04939 90 110mg/L.05

WG361975ICB 04/09/14 21:59ICB U -0.0015 0.0015mg/L

WG361557LRB 04/09/14 22:02LRB U -0.0011 0.0011mg/L

WG361557LFB 04/09/14 22:05 98.4LFB MS140331-2 .04931 85 115mg/L.0501

L17433-08LFM 04/09/14 22:18 .0068 97.8LFM MS140331-2 .0558 70 130mg/L.0501

L17433-08LFMD 04/09/14 22:21 .0068 96.8LFMD MS140331-2 .05532 0.8670 130mg/L 20.0501

Page 41 of 60L17433-1404141323


Inorganic QC

Summary




WG361393

WG361393ICV 03/28/14 15:59 98.7ICV HG140325-4 9.87 79 121ng/L10

WG361393ICB 03/28/14 16:04ICB U -0.5 0.5ng/L

WG361562

WG361562CCV1 04/01/14 15:50 96.8CCV HG140325-4 9.68 76.5 123.4ng/L10

WG361562CCB1 04/01/14 15:55CCB U -0.5 0.5ng/L

WG361562PQV 04/01/14 16:00 86PQV HG140325-6 .43 70 130ng/L.5

WG361562LFB 04/01/14 16:12 75LFB HG140325-5 1.5 71 125ng/L2

L17362-01MS 04/01/14 16:26 U 76MS HG140325-5 1.52 71 125ng/L2

L17362-01MSD 04/01/14 16:31 U 76.5MSD HG140325-5 1.53 0.6671 125ng/L 242

WG361562CCV2 04/01/14 17:01 94.6CCV HG140325-4 9.46 76.5 123.4ng/L10

WG361562CCB2 04/01/14 17:06CCB U -0.5 0.5ng/L

WG361562CCV3 04/01/14 17:47 91.9CCV HG140325-4 9.19 76.5 123.4ng/L10

WG361562CCB3 04/01/14 17:52CCB U -0.5 0.5ng/L

L17433-06MS M204/01/14 18:02 .5 66.5MS HG140325-5 1.83 71 125ng/L2

L17433-06MSD M204/01/14 18:07 .5 66MSD HG140325-5 1.82 0.5571 125ng/L 242

WG361562CCV4 04/01/14 18:22 97.1CCV HG140325-4 9.71 76.5 123.4ng/L10

WG361562CCB4 04/01/14 18:27CCB U -0.5 0.5ng/L



WG361393

WG361393ICV 03/28/14 15:59 98.7ICV HG140325-4 9.87 79 121ng/L10

WG361393ICB 03/28/14 16:04ICB U -0.5 0.5ng/L

WG361711

WG361711CCV1 04/03/14 9:54 95.6CCV HG140403-3 9.56 76.5 123.4ng/L10

WG361711CCB1 04/03/14 9:59CCB U -0.5 0.5ng/L

WG361711PQV 04/03/14 10:04 112PQV HG140403-5 .56 70 130ng/L.5

WG361711LFB 04/03/14 10:09 97.5LFB HG140403-4 1.95 71 125ng/L2

L17433-01MS 04/03/14 10:22 U 95MS HG140403-4 1.9 71 125ng/L2

L17433-01MSD 04/03/14 10:27 U 90.5MSD HG140403-4 1.81 4.8571 125ng/L 242

WG361711CCV2 04/03/14 11:05 94CCV HG140403-3 9.4 76.5 123.4ng/L10

WG361711CCB2 04/03/14 11:10CCB .22 -0.5 0.5ng/L

WG361711CCV3 04/03/14 11:55 94.9CCV HG140403-3 9.49 76.5 123.4ng/L10

WG361711CCB3 04/03/14 12:00CCB .21 -0.5 0.5ng/L

WG361711CCV4 04/03/14 12:48 102CCV HG140403-3 10.2 76.5 123.4ng/L10

WG361711CCB4 04/03/14 12:53CCB U -0.5 0.5ng/L



WG361845

WG361845ICV 04/07/14 14:18 95ICV MS140331-9 .01898 90 110mg/L.01998

WG361845ICB 04/07/14 14:21ICB U -0.0015 0.0015mg/L

WG361845LFB 04/07/14 14:24 94.9LFB MS140331-2 .04743 85 115mg/L.05

L17399-08AS 04/07/14 15:23 .0007 91.6AS MS140331-2 .04651 70 130mg/L.05

L17399-08ASD 04/07/14 15:26 .0007 92.4ASD MS140331-2 .04691 0.8670 130mg/L 20.05

Page 42 of 60L17433-1404141323


Inorganic QC

Summary




WG361760

WG361760ICV 04/03/14 20:59 95.6ICV MS140331-9 .0191 90 110mg/L.01998

WG361760ICB 04/03/14 21:02ICB U -0.0015 0.0015mg/L

WG361557LRB 04/03/14 21:06LRB U -0.0011 0.0011mg/L

WG361557LFB 04/03/14 21:09 95.8LFB MS140331-2 .0479 85 115mg/L.05

L17433-08LFM 04/03/14 22:34 .009 96.6LFM MS140331-2 .05728 70 130mg/L.05

L17433-08LFMD 04/03/14 22:37 .009 98.2LFMD MS140331-2 .05812 1.4670 130mg/L 20.05



WG361845

WG361845ICV 04/07/14 14:18 92.2ICV MS140331-9 .04612 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.0018 0.0018mg/L

WG361845LFB 04/07/14 14:24 95.8LFB MS140331-2 .04789 85 115mg/L.05

L17399-08AS 04/07/14 15:23 U 83.1AS MS140331-2 .04156 70 130mg/L.05

L17399-08ASD 04/07/14 15:26 U 82.3ASD MS140331-2 .04115 0.9970 130mg/L 20.05



WG361760

WG361760ICV 04/03/14 20:59 96.2ICV MS140331-9 .0481 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0018 0.0018mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00132 0.00132mg/L

WG361557LFB 04/03/14 21:09 95.8LFB MS140331-2 .04792 85 115mg/L.05

L17433-08LFM 04/03/14 22:34 U 87.2LFM MS140331-2 .04361 70 130mg/L.05




WG361832

WG361832ICV 04/05/14 13:27 98.8ICV WI140116-3 2.386 90 110mg/L2.416

WG361832ICB 04/05/14 13:28ICB U -0.06 0.06mg/L

WG361834

WG361834LFB1 04/05/14 14:01 101.2LFB WI140215-3 2.024 90 110mg/L2

L17225-02AS 04/05/14 14:03 .04 99.6AS WI140215-3 2.032 90 110mg/L2

L17305-01DUP RA04/05/14 14:05 UDUP U 0mg/L 20

L17433-03AS 04/05/14 14:20 .83 108.3AS WI140215-3 2.996 90 110mg/L2

L17433-06DUP RA04/05/14 14:22 UDUP U 0mg/L 20

WG361834LFB2 04/05/14 14:35 102.5LFB WI140215-3 2.05 90 110mg/L2

Page 43 of 60L17433-1404141323


Inorganic QC

Summary




WG361628

WG361628ICV 04/02/14 10:37 98.2ICV WI131021-1 .985 90 110mg/L1.003

WG361628ICB 04/02/14 10:40ICB U -0.15 0.15mg/L

WG361637

WG361637LFB1 04/02/14 11:42 99.9LFB WI140113-8 .999 90 110mg/L1

WG361637LFB2 04/02/14 12:47 99.4LFB WI140113-8 .994 90 110mg/L1

L17414-19AS 04/02/14 12:49 U 98.8AS WI140113-8 .988 90 110mg/L1

L17433-01DUP RA04/02/14 12:51 UDUP U 0mg/L 20

pH (lab) SM4500H+ B


WG361281





L17433-08DUP 03/27/14 5:14 8.4DUP 8.38 0.2units 20




WG361685

WG361685ICV 04/02/14 18:57 98.1ICV WI140401-5 .64 90 110mg/L.65228

WG361685ICB 04/02/14 18:59ICB U -0.03 0.03mg/L

WG361691

WG361579LRB 04/02/14 23:22LRB U -0.03 0.03mg/L

WG361579LFB 04/02/14 23:23 99.8LFB WI140326-3 .499 90 110mg/L.5

L17305-11LFM M104/02/14 23:41 .07 128.4LFM WI140326-3 .712 90 110mg/L.5

L17305-12DUP 04/02/14 23:43 .1DUP .098 2mg/L 20



WG361340

WG361340ICV 03/27/14 15:22 96.8ICV II140220-1 19.36 95 105mg/L20

WG361340ICB 03/27/14 15:28ICB U -0.6 0.6mg/L

WG361340LFB 03/27/14 15:41 99.1LFB II140317-2 99.14 85 115mg/L99.99364

L17433-01AS 03/27/14 16:44 5.8 99.4AS II140317-2 105.2 85 115mg/L99.99364

L17433-01ASD 03/27/14 16:47 5.8 99.9ASD II140317-2 105.7 0.4785 115mg/L 2099.99364

Page 44 of 60L17433-1404141323


Inorganic QC

Summary




WG361527

WG361527ICV 04/01/14 9:28 97.2ICV II140228-1 19.44 95 105mg/L20

WG361527ICB 04/01/14 9:34ICB U -0.6 0.6mg/L

WG361468LRB 04/01/14 9:47LRB U -0.44 0.44mg/L

WG361468LFB 04/01/14 9:50 100.4LFB II140317-2 100.4 85 115mg/L99.99364

L17381-01LFM 04/01/14 9:56 8.6 100.9LFM II140317-2 109.5 70 130mg/L99.99364

L17381-01LFMD 04/01/14 9:59 8.6 100.9LFMD II140317-2 109.5 070 130mg/L 2099.99364

L17433-03LFM 04/01/14 10:40 7.2 100.9LFM II140317-2 108.1 70 130mg/L99.99364

L17433-03LFMD 04/01/14 10:43 7.2 101.2LFMD II140317-2 108.4 0.2870 130mg/L 2099.99364



WG361441

WG361441PBW 03/28/14 14:22PBW U -20 20mg/L


L17433-02DUP 03/28/14 14:59 280DUP 280 0mg/L 10



WG361444

WG361444PBW 03/28/14 15:00PBW U -15 15mg/L


L17433-08DUP RA03/28/14 15:31 UDUP U 0mg/L 10



WG361340

WG361340ICV 03/27/14 15:22 99.5ICV II140220-1 1.99 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.3 0.3mg/L

WG361340LFB 03/27/14 15:41 103.9LFB II140317-2 1.04 85 115mg/L1.0009

L17433-01AS 03/27/14 16:44 U 103.9AS II140317-2 1.04 85 115mg/L1.0009

L17433-01ASD 03/27/14 16:47 U 104.9ASD II140317-2 1.05 0.9685 115mg/L 201.0009



WG361527

WG361527ICV 04/01/14 9:28 99ICV II140228-1 1.98 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.3 0.3mg/L

WG361468LRB 04/01/14 9:47LRB U -0.22 0.22mg/L

WG361468LFB 04/01/14 9:50 102.9LFB II140317-2 1.03 85 115mg/L1.0009

L17381-01LFM 04/01/14 9:56 U 100.9LFM II140317-2 1.01 70 130mg/L1.0009


L17433-03LFM 04/01/14 10:40 U 105.9LFM II140317-2 1.06 70 130mg/L1.0009


Page 45 of 60L17433-1404141323


Inorganic QC

Summary




WG361971

WG361971ICV 04/09/14 3:41 101.4ICV MS140331-9 .05071 90 110mg/L.05

WG361971ICB 04/09/14 3:44ICB U -0.0003 0.0003mg/L

WG361971LFB 04/09/14 3:47 95.4LFB MS140331-2 .04774 85 115mg/L.05005

L17399-08AS 04/09/14 4:03 .0009 107.4AS MS140331-2 .05465 70 130mg/L.05005

L17399-08ASD 04/09/14 4:07 .0009 106.9ASD MS140331-2 .05438 0.570 130mg/L 20.05005

L17475-03AS 04/09/14 5:08 U 109.9AS MS140331-2 .05501 70 130mg/L.05005

L17475-03ASD 04/09/14 5:12 U 110.8ASD MS140331-2 .05545 0.870 130mg/L 20.05005



WG361760

WG361760ICV 04/03/14 20:59 101.5ICV MS140331-9 .05073 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0003 0.0003mg/L

WG361557LRB 04/03/14 21:06LRB .00019 -0.00022 0.00022mg/L

WG361557LFB 04/03/14 21:09 102.2LFB MS140331-2 .05113 85 115mg/L.05005

L17433-08LFM 04/03/14 22:34 .0004 92.4LFM MS140331-2 .04666 70 130mg/L.05005

L17433-08LFMD 04/03/14 22:37 .0004 94.2LFMD MS140331-2 .04755 1.8970 130mg/L 20.05005

WG361975

WG361975ICV 04/09/14 21:56 100.5ICV MS140331-9 .05023 90 110mg/L.05

WG361975ICB 04/09/14 21:59ICB U -0.0003 0.0003mg/L

WG361557LRB 04/09/14 22:02LRB U -0.00022 0.00022mg/L

WG361557LFB 04/09/14 22:05 108.1LFB MS140331-2 .05411 85 115mg/L.05005

L17433-08LFM 04/09/14 22:18 .0004 94.5LFM MS140331-2 .04771 70 130mg/L.05005

L17433-08LFMD 04/09/14 22:21 .0004 95.4LFMD MS140331-2 .04816 0.9470 130mg/L 20.05005



WG361845

WG361845ICV 04/07/14 14:18 97ICV MS140331-9 .01942 90 110mg/L.02002

WG361845ICB 04/07/14 14:21ICB U -0.00015 0.00015mg/L

WG361845LFB 04/07/14 14:24 94.4LFB MS140331-2 .009461 85 115mg/L.01002

L17399-08AS 04/07/14 15:23 U 88.4AS MS140331-2 .00886 70 130mg/L.01002

L17399-08ASD 04/07/14 15:26 U 89ASD MS140331-2 .008921 0.6970 130mg/L 20.01002



WG361760

WG361760ICV 04/03/14 20:59 99.3ICV MS140331-9 .01988 90 110mg/L.02002

WG361760ICB 04/03/14 21:02ICB U -0.00015 0.00015mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00011 0.00011mg/L

WG361557LFB 04/03/14 21:09 96.7LFB MS140331-2 .009693 85 115mg/L.01002

L17433-08LFM 04/03/14 22:34 U 95LFM MS140331-2 .009514 70 130mg/L.01002


Page 46 of 60L17433-1404141323


Inorganic QC

Summary




WG361340

WG361340ICV 03/27/14 15:22 98.6ICV II140220-1 98.6 95 105mg/L100

WG361340ICB 03/27/14 15:28ICB U -0.6 0.6mg/L

WG361340LFB 03/27/14 15:41 99.2LFB II140317-2 99.21 85 115mg/L100.0393

L17433-01AS 03/27/14 16:44 25.3 98.3AS II140317-2 123.6 85 115mg/L100.0393

L17433-01ASD 03/27/14 16:47 25.3 98.9ASD II140317-2 124.2 0.4885 115mg/L 20100.0393



WG361527

WG361527ICV 04/01/14 9:28 98.2ICV II140228-1 98.2 95 105mg/L100

WG361527ICB 04/01/14 9:34ICB U -0.6 0.6mg/L

WG361468LRB 04/01/14 9:47LRB U -0.44 0.44mg/L

WG361468LFB 04/01/14 9:50 98.6LFB II140317-2 98.68 85 115mg/L100.0393

L17381-01LFM 04/01/14 9:56 48.7 98.8LFM II140317-2 147.5 70 130mg/L100.0393

L17381-01LFMD 04/01/14 9:59 48.7 99.5LFMD II140317-2 148.2 0.4770 130mg/L 20100.0393

L17433-03LFM 04/01/14 10:40 25.6 100.7LFM II140317-2 126.3 70 130mg/L100.0393

L17433-03LFMD 04/01/14 10:43 25.6 101LFMD II140317-2 126.6 0.2470 130mg/L 20100.0393



WG361340

WG361340ICV 03/27/14 15:22 99.4ICV II140220-1 1.9875 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.015 0.015mg/L

WG361340LFB 03/27/14 15:41 97.7LFB II140317-2 .4885 85 115mg/L.5

L17433-01AS 03/27/14 16:44 .196 97.4AS II140317-2 .683 85 115mg/L.5

L17433-01ASD 03/27/14 16:47 .196 98.2ASD II140317-2 .687 0.5885 115mg/L 20.5



WG361527

WG361527ICV 04/01/14 9:28 98.9ICV II140228-1 1.9775 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.015 0.015mg/L

WG361468LRB 04/01/14 9:47LRB U -0.011 0.011mg/L

WG361468LFB 04/01/14 9:50 98.4LFB II140317-2 .492 85 115mg/L.5

L17381-01LFM 04/01/14 9:56 .803 97.6LFM II140317-2 1.291 70 130mg/L.5

L17381-01LFMD 04/01/14 9:59 .803 98.8LFMD II140317-2 1.297 0.4670 130mg/L 20.5

L17433-03LFM 04/01/14 10:40 .253 98.6LFM II140317-2 .7458 70 130mg/L.5

L17433-03LFMD 04/01/14 10:43 .253 98.8LFMD II140317-2 .7472 0.1970 130mg/L 20.5

Page 47 of 60L17433-1404141323


Inorganic QC

Summary




WG360290

WG360290ICV 03/06/14 13:49 102.5ICV WI140226-1 51.2 90 110mg/L49.95

WG360290ICB 03/06/14 14:07ICB U -1.5 1.5mg/L

WG361726

WG361726LFB1 04/03/14 13:31 101.3LFB WI140306-2 30.4 90 110mg/L30

L17370-02DUP RA04/03/14 18:18 10.4DUP U 200mg/L 20

L17380-01AS 04/03/14 18:54 376 100.8AS WI140306-2 3400 90 110mg/L3000

WG361726LFB2 04/03/14 22:11 100LFB WI140306-2 30 90 110mg/L30



WG361845

WG361845ICV 04/07/14 14:18 102.8ICV MS140331-9 .0514 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.0003 0.0003mg/L

WG361845LFB 04/07/14 14:24 98.7LFB MS140331-2 .04954 85 115mg/L.0502

L17399-08AS 04/07/14 15:23 U 91.7AS MS140331-2 .04603 70 130mg/L.0502

L17399-08ASD 04/07/14 15:26 U 92.3ASD MS140331-2 .04632 0.6370 130mg/L 20.0502



WG361760

WG361760ICV 04/03/14 20:59 106.7ICV MS140331-9 .05333 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0003 0.0003mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00022 0.00022mg/L

WG361557LFB 04/03/14 21:09 99.3LFB MS140331-2 .04983 85 115mg/L.0502

L17433-08LFM 04/03/14 22:34 U 101.8LFM MS140331-2 .05108 70 130mg/L.0502




WG361845

WG361845ICV 04/07/14 14:18 99ICV MS140331-9 .04958 90 110mg/L.0501

WG361845ICB 04/07/14 14:21ICB U -0.0003 0.0003mg/L

WG361845LFB 04/07/14 14:24 94.7LFB MS140331-2 .0474 85 115mg/L.05005

L17399-08AS 04/07/14 15:23 U 90.7AS MS140331-2 .04539 70 130mg/L.05005

L17399-08ASD 04/07/14 15:26 U 91.6ASD MS140331-2 .04585 1.0170 130mg/L 20.05005



WG361760

WG361760ICV 04/03/14 20:59 100.3ICV MS140331-9 .05027 90 110mg/L.0501

WG361760ICB 04/03/14 21:02ICB U -0.0003 0.0003mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00022 0.00022mg/L

WG361557LFB 04/03/14 21:09 101LFB MS140331-2 .05057 85 115mg/L.05005

L17433-08LFM 04/03/14 22:34 U 97.2LFM MS140331-2 .04863 70 130mg/L.05005


Page 48 of 60L17433-1404141323


Inorganic QC

Summary




WG361340

WG361340ICV 03/27/14 15:22 96.3ICV II140220-1 1.9268 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.015 0.015mg/L

WG361340LFB 03/27/14 15:41 96.2LFB II140317-2 .9621 85 115mg/L1

L17433-01AS 03/27/14 16:44 U 96.9AS II140317-2 .9693 85 115mg/L1

L17433-01ASD 03/27/14 16:47 U 97.6ASD II140317-2 .9757 0.6685 115mg/L 201



WG361527

WG361527ICV 04/01/14 9:28 97ICV II140228-1 1.9402 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.015 0.015mg/L

WG361468LRB 04/01/14 9:47LRB U -0.011 0.011mg/L

WG361468LFB 04/01/14 9:50 100.3LFB II140317-2 1.003 85 115mg/L1

L17381-01LFM 04/01/14 9:56 U 98.3LFM II140317-2 .9828 70 130mg/L1

L17381-01LFMD 04/01/14 9:59 U 98.8LFMD II140317-2 .9884 0.5770 130mg/L 201

L17433-03LFM 04/01/14 10:40 U 101LFM II140317-2 1.01 70 130mg/L1

L17433-03LFMD 04/01/14 10:43 U 100.9LFMD II140317-2 1.009 0.170 130mg/L 201



WG361845

WG361845ICV 04/07/14 14:18 100.3ICV MS140331-9 .05016 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.0003 0.0003mg/L

WG361845LFB 04/07/14 14:24 100LFB MS140331-2 .04998 85 115mg/L.05

L17399-08AS 04/07/14 15:23 .0012 100.4AS MS140331-2 .05141 70 130mg/L.05

L17399-08ASD 04/07/14 15:26 .0012 100.7ASD MS140331-2 .05153 0.2370 130mg/L 20.05



WG361760

WG361760ICV 04/03/14 20:59 104.4ICV MS140331-9 .05219 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0003 0.0003mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00022 0.00022mg/L

WG361557LFB 04/03/14 21:09 102.4LFB MS140331-2 .05122 85 115mg/L.05

L17433-08LFM 04/03/14 22:34 .0007 104.9LFM MS140331-2 .05317 70 130mg/L.05

L17433-08LFMD 04/03/14 22:37 .0007 104.9LFMD MS140331-2 .05313 0.0870 130mg/L 20.05



WG361845

WG361845ICV 04/07/14 14:18 90.4ICV MS140331-9 .04521 90 110mg/L.05

WG361845ICB 04/07/14 14:21ICB U -0.0006 0.0006mg/L

WG361845LFB 04/07/14 14:24 99.2LFB MS140331-2 .04963 85 115mg/L.05005

L17399-08AS 04/07/14 15:23 .002 93.9AS MS140331-2 .049 70 130mg/L.05005

L17399-08ASD 04/07/14 15:26 .002 92.7ASD MS140331-2 .04841 1.2170 130mg/L 20.05005

Page 49 of 60L17433-1404141323


Inorganic QC

Summary




WG361760

WG361760ICV 04/03/14 20:59 97.3ICV MS140331-9 .04863 90 110mg/L.05

WG361760ICB 04/03/14 21:02ICB U -0.0006 0.0006mg/L

WG361557LRB 04/03/14 21:06LRB U -0.00044 0.00044mg/L

WG361557LFB 04/03/14 21:09 100.2LFB MS140331-2 .05016 85 115mg/L.05005

L17433-08LFM 04/03/14 22:34 .0033 96.3LFM MS140331-2 .0515 70 130mg/L.05005

L17433-08LFMD 04/03/14 22:37 .0033 96.8LFMD MS140331-2 .05176 0.570 130mg/L 20.05005



WG361340

WG361340ICV 03/27/14 15:22 97.7ICV II140220-1 1.954 95 105mg/L2

WG361340ICB 03/27/14 15:28ICB U -0.03 0.03mg/L

WG361340LFB 03/27/14 15:41 99.9LFB II140317-2 .5 85 115mg/L.5005

L17433-01AS 03/27/14 16:44 U 99.7AS II140317-2 .499 85 115mg/L.5005

L17433-01ASD 03/27/14 16:47 U 100.3ASD II140317-2 .502 0.685 115mg/L 20.5005



WG361527

WG361527ICV 04/01/14 9:28 95.7ICV II140228-1 1.913 95 105mg/L2

WG361527ICB 04/01/14 9:34ICB U -0.03 0.03mg/L

WG361468LRB 04/01/14 9:47LRB U -0.022 0.022mg/L

WG361468LFB 04/01/14 9:50 100.1LFB II140317-2 .501 85 115mg/L.5005

L17381-01LFM 04/01/14 9:56 .95 88.7LFM II140317-2 1.374 70 130mg/L.5005

L17381-01LFMD 04/01/14 9:59 .95 89.3LFMD II140317-2 1.377 0.2270 130mg/L 20.5005

L17433-03LFM 04/01/14 10:40 .01 97.5LFM II140317-2 .498 70 130mg/L.5005

L17433-03LFMD 04/01/14 10:43 .01 97.7LFMD II140317-2 .499 0.270 130mg/L 20.5005

Page 50 of 60L17433-1404141323


Inorganic Extended

Qualifier Report
















M353.2 - H2SO4 preservedNitrate/Nitrite as NWG361834









M300.0 - Ion ChromatographySulfateWG361726
























REPAD.15.06.05.01

Page 51 of 60L17433-1404141323


Inorganic Extended

Qualifier Report






M1631, Atomic FluorescenceMercury, dissolvedWG361562































M1631, Atomic FluorescenceMercury, dissolvedL17433-05 WG361562

REPAD.15.06.05.01

Page 52 of 60L17433-1404141323


Inorganic Extended

Qualifier Report







BE Target analyte in continuing calibration blank (CCB) at or above the acceptance criteria. Target analyte was not detected in the sample [< MDL].

M200.8 ICP-MSSelenium, totalWG361760

























REPAD.15.06.05.01

Page 53 of 60L17433-1404141323


Inorganic Extended

Qualifier Report





VC CCV recovery was above the acceptance limits. Target analyte was not detected in the sample [< MDL].

M200.8 ICP-MSBeryllium, totalWG361760














DC Sample required dilution. Non-target analyte exceeded

calibration range.


















REPAD.15.06.05.01

Page 54 of 60L17433-1404141323


Inorganic Extended

Qualifier Report





VC CCV recovery was above the acceptance limits. Target analyte was not detected in the sample [< MDL].

M200.8 ICP-MSBeryllium, totalWG361760




















RO The duplicate originally assigned to this sample was not

used for precision assessment because residue density exceeded the method limits. Another duplicate in the batch was used to assess precision. Method required duplicate frequency was not met.






REPAD.15.06.05.01

Page 55 of 60L17433-1404141323


Certification

Qualifiers


Metals Analysis










REPAD.05.06.05.01

Page 56 of 60L17433-1404141323


Sample

Receipt


ACZ Project ID:

Date Received:

Received By: mtb

03/26/2014 09:38

L17433




NANOYES

X

X

X

X

X

X









NANOYES

X

X

X

X

X

X

X

X

X8) Are all containers intact and with no leaks?











Samples/Containers

X

X

Shipping Containers


Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- ------- -------------NA19354 0.5 13 YesNA19355 0.3 13 Yes

X



REPAD LPII 2012-03

Page 57 of 60L17433-1404141323

Page 58 of 60L17433-1404141323

Page 59 of 60L17433-1404141323

Page 60 of 60L17433-1404141323


Analytical

Report



Boise, ID 83706


Erik Boe:







Erik Boe

April 01, 2014

Project ID: Calico 1st Quarter 2



Boise, ID 83706

Crystal Jensen

Report to: Bill to:

Page 1 of 90L17275-1404011436


Case

Narrative



April 01, 2014

Sample Receipt

Sample Analysis

Holding Times






REPAD.03.06.05.01 Page 2 of 90L17275-1404011436


Sample ID: SAGEBRUSH SPRING






Results

Date Sampled: 03/16/14 09:30



Inorganic Prep

XQDilution




mpb03/27/14 14:36


M200.2 ICP-MS las03/26/14 9:08


M200.2 ICP jjc03/25/14 9:11


Page 3 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 09:30



Metals Analysis

XQDilution


Aluminum, total M200.7 ICP mg/L 0.2U jjc0.03 03/26/14 10:151


Antimony, total M200.8 ICP-MS mg/L 0.002U pmc0.0004 03/28/14 0:281












Cadmium, total M200.8 ICP-MS mg/L 0.0005U pmc0.0001 03/28/14 0:281

Calcium, dissolved M200.7 ICP 45.2 mg/L 0.5 aeb0.1* 03/21/14 11:551



Chromium, total M200.8 ICP-MS 0.0012 mg/L 0.002B pmc0.0005 03/28/14 0:281


Cobalt, total M200.8 ICP-MS 0.00008 mg/L 0.0003B pmc0.00005 03/28/14 0:281


Copper, total M200.8 ICP-MS mg/L 0.003U pmc0.0005 03/28/14 0:281






Lead, total M200.8 ICP-MS mg/L 0.0005U pmc0.0001 03/28/14 0:281






Manganese, total M200.8 ICP-MS mg/L 0.003U pmc0.0005 03/28/14 0:281




Molybdenum, total M200.8 ICP-MS 0.0017 mg/L 0.003B pmc0.0005 03/28/14 0:281


Nickel, total M200.8 ICP-MS mg/L 0.003U pmc0.0006 03/28/14 0:281



Page 4 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 09:30








Silver, total M200.8 ICP-MS mg/L 0.0003U pmc0.00005 03/28/14 0:281






Thallium, total M200.8 ICP-MS mg/L 0.0005U pmc0.0001 03/28/14 0:281


Tin, total M200.8 ICP-MS mg/L 0.0005U pmc0.0001* 03/28/14 0:281




Uranium, total M200.8 ICP-MS 0.0040 mg/L 0.0005 pmc0.0001 03/28/14 0:281


Vanadium, total M200.8 ICP-MS 0.0197 mg/L 0.001 pmc0.0002 03/28/14 0:281




Page 5 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 09:30



Wet Chemistry

XQDilution



128 mg/L 20 abd2 03/24/14 0:001

Carbonate as CaCO3 mg/L 20U abd2 03/24/14 0:001

Hydroxide as CaCO3 mg/L 20U abd2 03/24/14 0:001

Total Alkalinity 128 mg/L 20 abd2 03/24/14 0:001


Conductivity @25C SM2510B 383 umhos/cm 10 abd1 03/24/14 17:051

Cyanide, total M335.4 - Colorimetric w/ distillation mg/L 0.01U bsu0.003* 03/24/14 18:100.5


mg/L 0.01U mpb0.003* 03/27/14 13:320.5





pH (lab) SM4500H+ B

pH 8.2 units 0.1H abd0.1 03/24/14 0:001

pH measured at 19 C 0.1 abd0.1 03/24/14 0:001


mg/L 0.05U pjb0.01* 03/28/14 0:111


SM2540C 270 mg/L 20 id10 03/20/14 12:431


SM2540D mg/L 20U enb5* 03/21/14 12:451



Page 6 of 90L17275-1404011436


Sample ID: GOVERNMENT CORRAL SPRING






Results

Date Sampled: 03/16/14 10:30



Inorganic Prep

XQDilution




mpb03/27/14 14:51


M200.2 ICP-MS las03/26/14 9:18


M200.2 ICP jjc03/25/14 9:46


Page 7 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 10:30



Metals Analysis

XQDilution


Aluminum, total M200.7 ICP 0.05 mg/L 0.2B jjc0.03 03/26/14 10:241










Bismuth, total M200.7 ICP 0.04 mg/L 0.2B jjc0.04* 03/26/14 10:241






















Magnesium, total M200.7 ICP 14 mg/L 1 jjc0.2 03/26/14 10:241






Molybdenum, total M200.8 ICP-MS 0.0017 mg/L 0.003B pmc0.0005 03/28/14 0:311



Potassium, dissolved M200.7 ICP 4 mg/L 1 aeb0.2 03/21/14 11:591


Page 8 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 10:30


Potassium, total M200.7 ICP 4 mg/L 1 jjc0.2 03/26/14 10:241
























Page 9 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 10:30



Wet Chemistry

XQDilution



138 mg/L 20 abd2 03/24/14 0:001








mg/L 0.01U mpb0.003* 03/27/14 13:340.5





pH (lab) SM4500H+ B

pH 8.2 units 0.1H abd0.1 03/24/14 0:001



0.01 mg/L 0.05B pjb0.01* 03/28/14 0:141


SM2540C 280 mg/L 20 id10 03/21/14 9:311


SM2540D mg/L 20U enb5* 03/21/14 12:461



Page 10 of 90L17275-1404011436


Sample ID: POISON SPRING






Results

Date Sampled: 03/16/14 11:45



Inorganic Prep

XQDilution




mpb03/27/14 15:06


M200.2 ICP jjc03/25/14 9:57


M200.2 ICP-MS las03/26/14 9:27


Page 11 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 11:45



Metals Analysis

XQDilution

















Calcium, dissolved M200.7 ICP 1 mg/L 0.5 aeb0.1* 03/21/14 12:021



Chromium, total M200.8 ICP-MS mg/L 0.002U pmc0.0005 03/28/14 0:351

Cobalt, dissolved M200.8 ICP-MS mg/L 0.0003U las0.00005 03/27/14 15:391

Cobalt, total M200.8 ICP-MS mg/L 0.0003U pmc0.00005 03/28/14 0:351









Lithium, dissolved M200.7 ICP mg/L 0.04U aeb0.008 03/21/14 12:021


Magnesium, dissolved M200.7 ICP mg/L 1U aeb0.2 03/21/14 12:021



Manganese, total M200.8 ICP-MS 0.0008 mg/L 0.003B pmc0.0005 03/28/14 0:351




Molybdenum, total M200.8 ICP-MS 0.0155 mg/L 0.003 pmc0.0005 03/28/14 0:351





Page 12 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 11:45






Selenium, total M200.8 ICP-MS mg/L 0.0003U pmc0.0001 03/28/14 0:351





Strontium, dissolved M200.7 ICP mg/L 0.03U aeb0.005 03/21/14 12:021

Strontium, total M200.7 ICP 0.005 mg/L 0.03B jjc0.005 03/26/14 10:271








Uranium, total M200.8 ICP-MS mg/L 0.0005U pmc0.0001 03/28/14 0:351


Vanadium, total M200.8 ICP-MS 0.0004 mg/L 0.001B pmc0.0002 03/28/14 0:351




Page 13 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 11:45



Wet Chemistry

XQDilution



98 mg/L 20 abd2 03/24/14 0:001

Carbonate as CaCO3 43 mg/L 20 abd2 03/24/14 0:001







mg/L 0.01U mpb0.003* 03/27/14 13:350.5


Hardness as CaCO3 SM2340B - Calculation 3 mg/L 7B calc1 04/01/14 12:22



pH (lab) SM4500H+ B

pH 9.1 units 0.1H abd0.1 03/24/14 0:001



0.02 mg/L 0.05B pjb0.01* 03/28/14 0:161


SM2540C 350 mg/L 20 id10 03/21/14 9:331


SM2540D mg/L 20U dcw5* 03/22/14 11:101



Page 14 of 90L17275-1404011436


Sample ID: DEPOSIT STOCK TANK






Results

Date Sampled: 03/16/14 12:35



Inorganic Prep

XQDilution




mpb03/27/14 15:14


M200.2 ICP-MS las03/26/14 9:37


M200.2 ICP jjc03/25/14 10:09


Page 15 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 12:35



Metals Analysis

XQDilution













































Page 16 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 12:35






















Zinc, dissolved M200.7 ICP 0.01 mg/L 0.05B aeb0.01 03/21/14 12:051



Page 17 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 12:35



Wet Chemistry

XQDilution



178 mg/L 20 abd2 03/24/14 0:001




Chloride M300.0 - Ion Chromatography 16.9 mg/L 2.5 tcd0.5 03/25/14 21:521




mg/L 0.01U mpb0.003* 03/27/14 13:350.5





pH (lab) SM4500H+ B

pH 8.2 units 0.1H abd0.1 03/24/14 0:001



0.02 mg/L 0.05B pjb0.01* 03/28/14 0:171


SM2540C 340 mg/L 20 id10 03/21/14 9:351


SM2540D mg/L 20U dcw5* 03/22/14 11:131



Page 18 of 90L17275-1404011436


Sample ID: DEPOSIT DUPLICATE






Results

Date Sampled: 03/16/14 12:45



Inorganic Prep

XQDilution




mpb03/27/14 15:22


M200.2 ICP jjc03/25/14 10:20


M200.2 ICP-MS las03/26/14 9:46


Page 19 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 12:45



Metals Analysis

XQDilution






































Mercury, total M1631, Atomic Fluorescence 1 ng/L 0.5 las0.2* 03/28/14 16:491







Page 20 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 12:45


























Page 21 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 12:45



Wet Chemistry

XQDilution



166 mg/L 20 abd2 03/24/14 0:001








mg/L 0.01U mpb0.003* 03/27/14 13:360.5





pH (lab) SM4500H+ B

pH 8.1 units 0.1H abd0.1 03/24/14 0:001



0.02 mg/L 0.05B pjb0.01* 03/28/14 0:211


SM2540C 340 mg/L 20 id10 03/21/14 9:371


SM2540D mg/L 20U dcw5* 03/22/14 11:151



Page 22 of 90L17275-1404011436


Sample ID: WHISKEY SPRING






Results

Date Sampled: 03/16/14 15:25



Inorganic Prep

XQDilution




mpb03/27/14 15:29


M200.2 ICP-MS las03/26/14 9:56


M200.2 ICP jjc03/25/14 10:32


Page 23 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 15:25



Metals Analysis

XQDilution



Antimony, dissolved M200.8 ICP-MS 0.0008 mg/L 0.002B las0.0004 03/27/14 15:561

Antimony, total M200.8 ICP-MS 0.0007 mg/L 0.002B pmc0.0004 03/28/14 0:511
































Manganese, total M200.8 ICP-MS mg/L 0.003U pmc0.0005 03/28/14 0:511









Page 24 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 15:25















Tin, dissolved M200.8 ICP-MS 0.0002 mg/L 0.0005B las0.0001* 03/27/14 15:561











Page 25 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 15:25



Wet Chemistry

XQDilution



114 mg/L 20 abd2 03/24/14 0:001




Chloride M300.0 - Ion Chromatography 6.53 mg/L 12.5B tcd2.5* 03/25/14 23:395




mg/L 0.01U mpb0.003* 03/27/14 13:390.5

Fluoride M300.0 - Ion Chromatography mg/L 2.5U tcd0.5* 03/25/14 23:395




pH (lab) SM4500H+ B

pH 8.2 units 0.1H abd0.1 03/24/14 0:001



0.03 mg/L 0.05B pjb0.01* 03/28/14 0:221


SM2540C 390 mg/L 20 id10 03/21/14 9:391


SM2540D mg/L 20U dcw5* 03/22/14 11:181

Sulfate M300.0 - Ion Chromatography 119 mg/L 12.5 tcd2.5 03/25/14 23:395


Page 26 of 90L17275-1404011436


Sample ID: MERC TRANSFER/TRIP BLANK






Results

Date Sampled: 03/16/14 17:25



Metals Analysis

XQDilution



REPIN.02.06.05.01

Page 27 of 90L17275-1404011436


Sample ID: TWIN SPRINGS NORTH






Results

Date Sampled: 03/16/14 16:10



Inorganic Prep

XQDilution




mpb03/27/14 15:37


M200.2 ICP jjc03/25/14 10:44


M200.2 ICP-MS las03/26/14 10:06


Page 28 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 16:10



Metals Analysis

XQDilution













































Page 29 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 16:10
















Tin, total M200.8 ICP-MS 0.0002 mg/L 0.0005B pmc0.0001* 03/28/14 0:551










Page 30 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 16:10



Wet Chemistry

XQDilution



140 mg/L 20 abd2 03/24/14 0:001








mg/L 0.01U mpb0.003* 03/27/14 13:400.5





pH (lab) SM4500H+ B

pH 8.2 units 0.1H abd0.1 03/24/14 0:001



0.05 mg/L 0.05 pjb0.01* 03/28/14 0:231


SM2540C 300 mg/L 20 id10 03/21/14 9:401


SM2540D mg/L 20U dcw5* 03/22/14 11:201



Page 31 of 90L17275-1404011436


Sample ID: TWIN SPRINGS SOUTH






Results

Date Sampled: 03/16/14 17:05



Inorganic Prep

XQDilution




mpb03/27/14 15:44


M200.2 ICP-MS las03/26/14 10:34


M200.2 ICP jjc03/25/14 10:55


Page 32 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 17:05



Metals Analysis

XQDilution













































Page 33 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 17:05


























Page 34 of 90L17275-1404011436








Results

Date Sampled: 03/16/14 17:05



Wet Chemistry

XQDilution



136 mg/L 20 abd2 03/24/14 0:001








mg/L 0.01U mpb0.003* 03/27/14 13:410.5





pH (lab) SM4500H+ B

pH 8.2 units 0.1H abd0.1 03/24/14 0:001



0.02 mg/L 0.05B pjb0.01* 03/28/14 0:241


SM2540C 340 mg/L 20 enb10 03/21/14 16:141


SM2540D mg/L 20U dcw5* 03/22/14 11:231



Page 35 of 90L17275-1404011436


Sample ID: SOURDOUGH UPPER






Results

Date Sampled: 03/17/14 11:10



Inorganic Prep

XQDilution




mpb03/27/14 15:52


M200.2 ICP-MS las03/26/14 10:44


M200.2 ICP jjc03/25/14 11:07


Page 36 of 90L17275-1404011436








Results

Date Sampled: 03/17/14 11:10



Metals Analysis

XQDilution























Copper, dissolved M200.8 ICP-MS 0.0009 mg/L 0.003B las0.0005 03/27/14 16:131

Copper, total M200.8 ICP-MS 0.0008 mg/L 0.003B pmc0.0005 03/28/14 1:081









Magnesium, dissolved M200.7 ICP 9 mg/L 1 aeb0.2 03/21/14 12:271



Manganese, total M200.8 ICP-MS mg/L 0.003U pmc0.0005* 03/28/14 1:081

Mercury, dissolved M1631, Atomic Fluorescence 1 ng/L 0.5 las0.2 03/27/14 13:561




Nickel, dissolved M200.8 ICP-MS 0.0006 mg/L 0.003B las0.0006 03/27/14 16:131

Nickel, total M200.8 ICP-MS 0.0006 mg/L 0.003B pmc0.0006 03/28/14 1:081



Page 37 of 90L17275-1404011436








Results

Date Sampled: 03/17/14 11:10























Zinc, dissolved M200.7 ICP 0.10 mg/L 0.05 aeb0.01 03/21/14 12:271

Zinc, total M200.7 ICP 0.10 mg/L 0.05 jjc0.01 03/26/14 10:531


Page 38 of 90L17275-1404011436








Results

Date Sampled: 03/17/14 11:10



Wet Chemistry

XQDilution



131 mg/L 20 abd2 03/24/14 0:001








mg/L 0.01U mpb0.003* 03/27/14 13:410.5





pH (lab) SM4500H+ B

pH 8.1 units 0.1H abd0.1 03/24/14 0:001



0.03 mg/L 0.05B pjb0.01* 03/28/14 0:251


SM2540C 310 mg/L 20 enb10 03/21/14 16:171


SM2540D mg/L 20U dcw5* 03/22/14 11:261



Page 39 of 90L17275-1404011436


Sample ID: SOURDOUGH LOWER






Results

Date Sampled: 03/17/14 12:30



Inorganic Prep

XQDilution




mpb03/27/14 16:00


M200.2 ICP jjc03/25/14 11:18


M200.2 ICP-MS las03/26/14 10:54


Page 40 of 90L17275-1404011436








Results

Date Sampled: 03/17/14 12:30



Metals Analysis

XQDilution




































Manganese, total M200.8 ICP-MS 0.0038 mg/L 0.003 pmc0.0005* 03/28/14 1:121

Mercury, dissolved M1631, Atomic Fluorescence 0.7 ng/L 0.5 las0.2 03/27/14 14:011

Mercury, total M1631, Atomic Fluorescence 1 ng/L 0.5 las0.2 03/28/14 17:301







Page 41 of 90L17275-1404011436








Results

Date Sampled: 03/17/14 12:30























Zinc, dissolved M200.7 ICP 0.01 mg/L 0.05B aeb0.01 03/21/14 12:301



Page 42 of 90L17275-1404011436








Results

Date Sampled: 03/17/14 12:30



Wet Chemistry

XQDilution



112 mg/L 20 abd2 03/24/14 0:001








mg/L 0.01U mpb0.003* 03/27/14 13:420.5





pH (lab) SM4500H+ B

pH 8.2 units 0.1H abd0.1 03/24/14 0:001



0.01 mg/L 0.05B pjb0.01* 03/28/14 0:261


SM2540C 260 mg/L 20 enb10 03/21/14 16:191


SM2540D mg/L 20U dcw5* 03/22/14 11:281



Page 43 of 90L17275-1404011436


Sample ID: EQUIPMENT BLANK






Results

Date Sampled: 03/17/14 13:00



Inorganic Prep

XQDilution




bsu03/28/14 12:50


M200.2 ICP-MS las03/26/14 11:03


M200.2 ICP jjc03/25/14 11:30


Page 44 of 90L17275-1404011436








Results

Date Sampled: 03/17/14 13:00



Metals Analysis

XQDilution





Arsenic, dissolved M200.8 ICP-MS mg/L 0.001U las0.0002 03/27/14 16:201

Arsenic, total M200.8 ICP-MS mg/L 0.001U pmc0.0002 03/28/14 1:151

Barium, dissolved M200.7 ICP mg/L 0.02U aeb0.003 03/21/14 12:331

Barium, total M200.7 ICP mg/L 0.02U jjc0.003 03/26/14 10:591





Boron, dissolved M200.7 ICP mg/L 0.05U aeb0.01 03/21/14 12:331

Boron, total M200.7 ICP 0.01 mg/L 0.05B jjc0.01 03/26/14 10:591



Calcium, dissolved M200.7 ICP mg/L 0.5U aeb0.1 03/21/14 12:331

Calcium, total M200.7 ICP mg/L 0.5U jjc0.1 03/26/14 10:591



Cobalt, dissolved M200.8 ICP-MS mg/L 0.0003U las0.00005 03/27/14 16:201










Lithium, dissolved M200.7 ICP mg/L 0.04U aeb0.008 03/21/14 12:331

Lithium, total M200.7 ICP mg/L 0.04U jjc0.008 03/26/14 10:591

Magnesium, dissolved M200.7 ICP mg/L 1U aeb0.2 03/21/14 12:331



Manganese, total M200.8 ICP-MS 0.0008 mg/L 0.003B pmc0.0005* 03/28/14 1:151



Molybdenum, dissolved M200.8 ICP-MS mg/L 0.003U las0.0005 03/27/14 16:201

Molybdenum, total M200.8 ICP-MS mg/L 0.003U pmc0.0005 03/28/14 1:151



Potassium, dissolved M200.7 ICP mg/L 1U aeb0.2 03/21/14 12:331


Page 45 of 90L17275-1404011436








Results

Date Sampled: 03/17/14 13:00


Potassium, total M200.7 ICP mg/L 1U jjc0.2 03/26/14 10:591







Sodium, dissolved M200.7 ICP mg/L 1U aeb0.2 03/21/14 12:331

Sodium, total M200.7 ICP mg/L 1U jjc0.2 03/26/14 10:591

Strontium, dissolved M200.7 ICP mg/L 0.03U aeb0.005 03/21/14 12:331

Strontium, total M200.7 ICP mg/L 0.03U jjc0.005 03/26/14 10:591










Vanadium, total M200.8 ICP-MS mg/L 0.001U pmc0.0002 03/28/14 1:151




Page 46 of 90L17275-1404011436








Results

Date Sampled: 03/17/14 13:00



Wet Chemistry

XQDilution



mg/L 20U abd2 03/24/14 0:001



Total Alkalinity mg/L 20U abd2 03/24/14 0:001

Chloride M300.0 - Ion Chromatography mg/L 2.5U tcd0.5 03/26/14 1:091

Conductivity @25C SM2510B 1 umhos/cm 10B abd1 03/24/14 18:441



mg/L 0.01U mpb0.003* 03/27/14 13:440.5


Hardness as CaCO3 SM2340B - Calculation mg/L 7U calc1 04/01/14 12:25



pH (lab) SM4500H+ B

pH 6.1 units 0.1H abd0.1 03/24/14 0:001



mg/L 0.05U pjb0.01* 03/28/14 22:001


SM2540C mg/L 20U enb10 03/21/14 16:211


SM2540D mg/L 20U dcw5* 03/22/14 11:341

Sulfate M300.0 - Ion Chromatography mg/L 2.5U tcd0.5 03/26/14 1:091


Page 47 of 90L17275-1404011436


Sample ID: TRANSFER BLANK






Results

Date Sampled: 03/17/14 13:20



Inorganic Prep

XQDilution




bsu03/28/14 13:10


M200.2 ICP-MS las03/26/14 11:13


M200.2 ICP jjc03/25/14 11:42


Metals Analysis

XQDilution



Arsenic, total M200.8 ICP-MS mg/L 0.001U pmc0.0002 03/28/14 1:191




Boron, total M200.7 ICP mg/L 0.05U jjc0.01 03/26/14 11:021


Calcium, total M200.7 ICP mg/L 0.5U jjc0.1 03/26/14 11:021







Lithium, total M200.7 ICP mg/L 0.04U jjc0.008 03/26/14 11:021


Manganese, total M200.8 ICP-MS 0.0006 mg/L 0.003B pmc0.0005* 03/28/14 1:191


Molybdenum, total M200.8 ICP-MS mg/L 0.003U pmc0.0005 03/28/14 1:191


Potassium, total M200.7 ICP mg/L 1U jjc0.2 03/26/14 11:021




Sodium, total M200.7 ICP mg/L 1U jjc0.2 03/26/14 11:021

Strontium, total M200.7 ICP mg/L 0.03U jjc0.005 03/26/14 11:021








Page 48 of 90L17275-1404011436


Sample ID: TRANSFER BLANK






Results

Date Sampled: 03/17/14 13:20



Wet Chemistry

XQDilution



mg/L 20U abd2 03/24/14 0:001



Total Alkalinity mg/L 20U abd2 03/24/14 0:001

Chloride M300.0 - Ion Chromatography mg/L 2.5U tcd0.5 03/26/14 1:271

Conductivity @25C SM2510B umhos/cm 10U abd1 03/24/14 18:511



mg/L 0.01U mpb0.003* 03/27/14 13:460.5




pH (lab) SM4500H+ B

pH 5.9 units 0.1H abd0.1 03/24/14 0:001



mg/L 0.05U pjb0.01* 03/28/14 22:021


SM2540C mg/L 20U enb10 03/21/14 16:231


SM2540D mg/L 20U dcw5* 03/22/14 11:361

Sulfate M300.0 - Ion Chromatography mg/L 2.5U tcd0.5 03/26/14 1:271


Page 49 of 90L17275-1404011436


Sample ID: PROD-1






Results

Date Sampled: 03/16/14 13:20



Inorganic Prep

XQDilution




bsu03/28/14 13:31


M200.2 ICP jjc03/25/14 11:53


M200.2 ICP-MS las03/26/14 11:22


Page 50 of 90L17275-1404011436


Sample ID: PROD-1






Results

Date Sampled: 03/16/14 13:20



Metals Analysis

XQDilution







Barium, dissolved M200.7 ICP mg/L 0.02U aeb0.003 03/21/14 12:361




















Iron, dissolved M200.7 ICP 0.06 mg/L 0.05 aeb0.02 03/21/14 12:361

Iron, total M200.7 ICP 0.04 mg/L 0.05B jjc0.02 03/26/14 11:051





Magnesium, dissolved M200.7 ICP 0.2 mg/L 1B aeb0.2 03/21/14 12:361



Manganese, total M200.8 ICP-MS 0.0471 mg/L 0.003 pmc0.0005* 03/28/14 1:221

Mercury, dissolved M1631, Atomic Fluorescence 0.5 ng/L 0.5 las0.2 03/27/14 14:111






Potassium, dissolved M200.7 ICP 0.5 mg/L 1B aeb0.2 03/21/14 12:361


Page 51 of 90L17275-1404011436


Sample ID: PROD-1






Results

Date Sampled: 03/16/14 13:20


Potassium, total M200.7 ICP 0.4 mg/L 1B jjc0.2 03/26/14 11:051
























Page 52 of 90L17275-1404011436


Sample ID: PROD-1






Results

Date Sampled: 03/16/14 13:20



Wet Chemistry

XQDilution



162 mg/L 20 abd2 03/24/14 0:001

Carbonate as CaCO3 6 mg/L 20B abd2 03/24/14 0:001







mg/L 0.01U mpb0.003* 03/27/14 13:470.5




Nitrogen, ammonia M350.1 - Automated Phenate 0.06 mg/L 0.5B tcd0.05* 03/27/14 13:181

pH (lab) SM4500H+ B

pH 8.4 units 0.1H abd0.1 03/24/14 0:001



0.04 mg/L 0.05B pjb0.01* 03/28/14 22:051


SM2540C 380 mg/L 20 enb10 03/21/14 16:251


SM2540D mg/L 20U dcw5* 03/22/14 11:391



Page 53 of 90L17275-1404011436


Sample ID: MERC. TRANSFER/TRIP BLANK






Results

Date Sampled: 03/17/14 12:45



Metals Analysis

XQDilution



REPIN.02.06.05.01

Page 54 of 90L17275-1404011436















QC Sample Types
























Method References






Comments








REP001.09.12.01

Inorganic

Reference

Page 55 of 90L17275-1404011436



Inorganic QC

Summary




WG361080

WG361080PBW1 03/24/14 13:06PBW 5.8 -20 20mg/L



WG361080PBW2 03/24/14 16:55PBW 2.6 -20 20mg/L

L17275-11DUP 03/24/14 18:37 112DUP 123.6 9.8mg/L 20

L17282-01DUP 03/24/14 20:12 207DUP 205.7 0.6mg/L 20


WG361080PBW3 03/24/14 20:41PBW 2.8 -20 20mg/L

WG361080LCSW12 03/25/14 0:28 103LCSW WC140313- 844.6 90 110mg/L820.0001

WG361080PBW4 03/25/14 0:38PBW 2.5 -20 20mg/L




WG360973

WG360973ICV 03/21/14 11:24 97.1ICV II140220-1 1.941 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.09 0.09mg/L

WG360973LFB 03/21/14 11:43 102.1LFB II140317-2 1.022 85 115mg/L1.0011

L17261-01AS 03/21/14 11:49 U 106AS II140317-2 2.122 85 115mg/L2.0022

L17261-01ASD 03/21/14 11:52 U 107.7ASD II140317-2 2.156 1.5985 115mg/L 202.0022

L17332-01AS 03/21/14 13:01 U 101.4AS II140317-2 1.015 85 115mg/L1.0011

L17332-01ASD 03/21/14 13:04 U 106.2ASD II140317-2 1.063 4.6285 115mg/L 201.0011



WG361188

WG361188ICV 03/26/14 9:50 94.8ICV II140228-1 1.896 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB U -0.09 0.09mg/L

WG361129LRB 03/26/14 10:09LRB U -0.066 0.066mg/L

WG361129LFB 03/26/14 10:12 98.9LFB II140317-2 .99 85 115mg/L1.0011

L17275-01LFM 03/26/14 10:18 U 100.7LFM II140317-2 1.008 70 130mg/L1.0011


L17304-01LFM 03/26/14 11:24 U 97.3LFM II140317-2 .974 70 130mg/L1.0011




WG361239

WG361239ICV 03/27/14 15:22 106.5ICV MS140218-2 .02134 90 110mg/L.02004

WG361239ICB 03/27/14 15:25ICB U -0.0012 0.0012mg/L

WG361239LFB 03/27/14 15:29 99.6LFB MS140320-2 .00996 85 115mg/L.01

L17275-05AS 03/27/14 15:49 U 109.9AS MS140320-2 .01099 70 130mg/L.01

L17275-05ASD 03/27/14 15:53 U 107.8ASD MS140320-2 .01078 1.9370 130mg/L 20.01

L17320-01AS 03/27/14 16:37 U 101.9AS MS140320-2 .01019 70 130mg/L.01

L17320-01ASD 03/27/14 16:47 U 103.9ASD MS140320-2 .01039 1.9470 130mg/L 20.01

Page 56 of 90L17275-1404011436


Inorganic QC

Summary




WG361380

WG361380ICV 03/28/14 0:07 102.2ICV MS140218-2 .02049 90 110mg/L.02004

WG361380ICB 03/28/14 0:11ICB U -0.0012 0.0012mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00088 0.00088mg/L

WG361214LFB 03/28/14 0:18 108.5LFB MS140320-2 .01085 85 115mg/L.01

L17275-08LFM 03/28/14 0:58 U 104.1LFM MS140320-2 .01041 70 130mg/L.01


L17321-02LFM 03/28/14 1:43 U 109.5LFM MS140320-2 .01095 70 130mg/L.01




WG361239

WG361239ICV 03/27/14 15:22 105.1ICV MS140218-2 .05254 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0006 0.0006mg/L

WG361239LFB 03/27/14 15:29 98.5LFB MS140320-2 .04934 85 115mg/L.0501

L17275-05AS 03/27/14 15:49 .0299 128.2AS MS140320-2 .09414 70 130mg/L.0501

L17275-05ASD 03/27/14 15:53 .0299 128.6ASD MS140320-2 .09433 0.270 130mg/L 20.0501

L17320-01AS 03/27/14 16:37 .0003 122AS MS140320-2 .06141 70 130mg/L.0501

L17320-01ASD 03/27/14 16:47 .0003 121.8ASD MS140320-2 .06132 0.1570 130mg/L 20.0501



WG361380

WG361380ICV 03/28/14 0:07 102.8ICV MS140218-2 .05142 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0006 0.0006mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00044 0.00044mg/L

WG361214LFB 03/28/14 0:18 112.2LFB MS140320-2 .05622 85 115mg/L.0501

L17275-08LFM 03/28/14 0:58 .0444 101.8LFM MS140320-2 .0954 70 130mg/L.0501

L17275-08LFMD 03/28/14 1:02 .0444 105.2LFMD MS140320-2 .09711 1.7870 130mg/L 20.0501

L17321-02LFM 03/28/14 1:43 .0011 112.4LFM MS140320-2 .0574 70 130mg/L.0501

L17321-02LFMD 03/28/14 1:46 .0011 114.9LFMD MS140320-2 .05866 2.1770 130mg/L 20.0501



WG360973

WG360973ICV 03/21/14 11:24 97.3ICV II140220-1 1.9458 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB .0031 -0.009 0.009mg/L

WG360973LFB 03/21/14 11:43 97.4LFB II140317-2 .4869 85 115mg/L.5

L17261-01AS 03/21/14 11:49 .014 98AS II140317-2 .9942 85 115mg/L1

L17261-01ASD 03/21/14 11:52 .014 98.3ASD II140317-2 .9968 0.2685 115mg/L 201

L17332-01AS 03/21/14 13:01 .023 96.9AS II140317-2 .5073 85 115mg/L.5

L17332-01ASD 03/21/14 13:04 .023 99.3ASD II140317-2 .5193 2.3485 115mg/L 20.5

Page 57 of 90L17275-1404011436


Inorganic QC

Summary




WG361188

WG361188ICV 03/26/14 9:50 96.5ICV II140228-1 1.9302 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB .0031 -0.009 0.009mg/L

WG361129LRB 03/26/14 10:09LRB U -0.0066 0.0066mg/L

WG361129LFB 03/26/14 10:12 99.4LFB II140317-2 .4971 85 115mg/L.5

L17275-01LFM 03/26/14 10:18 .004 99.5LFM II140317-2 .5014 70 130mg/L.5

L17275-01LFMD 03/26/14 10:21 .004 99.3LFMD II140317-2 .5004 0.270 130mg/L 20.5

L17304-01LFM 03/26/14 11:24 .118 98.3LFM II140317-2 .6093 70 130mg/L.5

L17304-01LFMD 03/26/14 11:27 .118 100.1LFMD II140317-2 .6186 1.5170 130mg/L 20.5



WG361239

WG361239ICV 03/27/14 15:22 97ICV MS140218-2 .04848 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.00015 0.00015mg/L

WG361239LFB 03/27/14 15:29 94.4LFB MS140320-2 .04726 85 115mg/L.05005

L17275-05AS 03/27/14 15:49 U 109.5AS MS140320-2 .0548 70 130mg/L.05005

L17275-05ASD 03/27/14 15:53 U 106.2ASD MS140320-2 .05317 3.0270 130mg/L 20.05005

L17320-01AS 03/27/14 16:37 U 111.8AS MS140320-2 .05598 70 130mg/L.05005

L17320-01ASD 03/27/14 16:47 U 107ASD MS140320-2 .05353 4.4770 130mg/L 20.05005



WG361380

WG361380ICV 03/28/14 0:07 95.4ICV MS140218-2 .04771 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.00015 0.00015mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00011 0.00011mg/L

WG361214LFB 03/28/14 0:18 104.1LFB MS140320-2 .05211 85 115mg/L.05005

L17275-08LFM 03/28/14 0:58 U 103.1LFM MS140320-2 .05159 70 130mg/L.05005


L17321-02LFM 03/28/14 1:43 .0057 96.2LFM MS140320-2 .05386 70 130mg/L.05005

L17321-02LFMD 03/28/14 1:46 .0057 94.8LFMD MS140320-2 .05316 1.3170 130mg/L 20.05005



WG360973

WG360973ICV 03/21/14 11:24 97.9ICV II140220-1 1.957 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.12 0.12mg/L

WG360973LFB 03/21/14 11:43 99.6LFB II140317-2 .995 85 115mg/L.999

L17261-01AS 03/21/14 11:49 U 102.3AS II140317-2 2.044 85 115mg/L1.998

L17261-01ASD 03/21/14 11:52 U 103.7ASD II140317-2 2.072 1.3685 115mg/L 201.998

L17332-01AS 03/21/14 13:01 U 98.8AS II140317-2 .987 85 115mg/L.999

L17332-01ASD 03/21/14 13:04 U 105ASD II140317-2 1.049 6.0985 115mg/L 20.999

Page 58 of 90L17275-1404011436


Inorganic QC

Summary




WG361188

WG361188ICV 03/26/14 9:50 96.7ICV II140228-1 1.934 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB U -0.12 0.12mg/L

WG361129LRB 03/26/14 10:09LRB U -0.088 0.088mg/L

WG361129LFB 03/26/14 10:12 107.6LFB II140317-2 1.075 85 115mg/L.999

L17275-01LFM 03/26/14 10:18 U 104.1LFM II140317-2 1.04 70 130mg/L.999


L17304-01LFM 03/26/14 11:24 .05 102.1LFM II140317-2 1.07 70 130mg/L.999

L17304-01LFMD 03/26/14 11:27 .05 102.8LFMD II140317-2 1.077 0.6570 130mg/L 20.999



WG360973

WG360973ICV 03/21/14 11:24 97.1ICV II140220-1 1.941 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.03 0.03mg/L

WG360973LFB 03/21/14 11:43 99.9LFB II140317-2 .5 85 115mg/L.5005

L17261-01AS 03/21/14 11:49 .11 99.7AS II140317-2 1.108 85 115mg/L1.001

L17261-01ASD 03/21/14 11:52 .11 100.4ASD II140317-2 1.115 0.6385 115mg/L 201.001

L17332-01AS 03/21/14 13:01 .11 97.1AS II140317-2 .596 85 115mg/L.5005

L17332-01ASD 03/21/14 13:04 .11 101.3ASD II140317-2 .617 3.4685 115mg/L 20.5005



WG361188

WG361188ICV 03/26/14 9:50 95.7ICV II140228-1 1.914 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB .013 -0.03 0.03mg/L

WG361129LRB 03/26/14 10:09LRB .012 -0.022 0.022mg/L

WG361129LFB 03/26/14 10:12 97.5LFB II140317-2 .488 85 115mg/L.5005

L17275-01LFM 03/26/14 10:18 .06 95.3LFM II140317-2 .537 70 130mg/L.5005

L17275-01LFMD 03/26/14 10:21 .06 96.3LFMD II140317-2 .542 0.9370 130mg/L 20.5005

L17304-01LFM 03/26/14 11:24 .01 92.1LFM II140317-2 .471 70 130mg/L.5005

L17304-01LFMD 03/26/14 11:27 .01 93.7LFMD II140317-2 .479 1.6870 130mg/L 20.5005



WG361239

WG361239ICV 03/27/14 15:22 96.3ICV MS140218-2 .04814 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0003 0.0003mg/L

WG361239LFB 03/27/14 15:29 94LFB MS140320-2 .04708 85 115mg/L.0501

L17275-05AS 03/27/14 15:49 U 103.8AS MS140320-2 .05202 70 130mg/L.0501

L17275-05ASD 03/27/14 15:53 U 102.6ASD MS140320-2 .05138 1.2470 130mg/L 20.0501

L17320-01AS 03/27/14 16:37 U 101.1AS MS140320-2 .05063 70 130mg/L.0501

L17320-01ASD 03/27/14 16:47 U 101.4ASD MS140320-2 .05079 0.3270 130mg/L 20.0501

Page 59 of 90L17275-1404011436


Inorganic QC

Summary




WG361380

WG361380ICV 03/28/14 0:07 97.7ICV MS140218-2 .04885 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0003 0.0003mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00022 0.00022mg/L

WG361214LFB 03/28/14 0:18 104.5LFB MS140320-2 .05237 85 115mg/L.0501

L17275-08LFM 03/28/14 0:58 U 98.7LFM MS140320-2 .04944 70 130mg/L.0501


L17321-02LFM 03/28/14 1:43 .0022 98.6LFM MS140320-2 .05158 70 130mg/L.0501

L17321-02LFMD 03/28/14 1:46 .0022 98.9LFMD MS140320-2 .05176 0.3570 130mg/L 20.0501



WG360973

WG360973ICV 03/21/14 11:24 97.4ICV II140220-1 97.43 95 105mg/L100

WG360973ICB 03/21/14 11:30ICB U -0.3 0.3mg/L

WG360973LFB 03/21/14 11:43 101.7LFB II140317-2 69.16 85 115mg/L67.98099

L17261-01AS M303/21/14 11:49 959 69.9AS II140317-2 1054 85 115mg/L135.96198

L17261-01ASD M303/21/14 11:52 959 81.8ASD II140317-2 1070.2 1.5385 115mg/L 20135.96198

L17332-01AS 03/21/14 13:01 182 89.9AS II140317-2 243.1 85 115mg/L67.98099

L17332-01ASD 03/21/14 13:04 182 101.6ASD II140317-2 251.1 3.2485 115mg/L 2067.98099



WG361188

WG361188ICV 03/26/14 9:50 98.3ICV II140228-1 98.32 95 105mg/L100

WG361188ICB 03/26/14 9:56ICB U -0.3 0.3mg/L

WG361129LRB 03/26/14 10:09LRB U -0.22 0.22mg/L

WG361129LFB 03/26/14 10:12 103.7LFB II140317-2 70.5 85 115mg/L67.98099

L17275-01LFM 03/26/14 10:18 46 103.7LFM II140317-2 116.5 70 130mg/L67.98099

L17275-01LFMD 03/26/14 10:21 46 103.6LFMD II140317-2 116.4 0.0970 130mg/L 2067.98099

L17304-01LFM 03/26/14 11:24 29.6 102.1LFM II140317-2 99.02 70 130mg/L67.98099

L17304-01LFMD 03/26/14 11:27 29.6 104.9LFMD II140317-2 100.9 1.8870 130mg/L 2067.98099



WG360290

WG360290ICV 03/06/14 13:49 101.6ICV WI140226-1 20.3 90 110mg/L19.98

WG360290ICB 03/06/14 14:07ICB U -1.5 1.5mg/L

WG361148

WG361148LFB1 03/25/14 12:54 101.3LFB WI140306-2 30.4 90 110mg/L30

L17232-03DUP RA03/25/14 17:41 1.7DUP 1.72 1.2mg/L 20

L17232-04AS 03/25/14 18:17 1.48 101.4AS WI140306-2 31.9 90 110mg/L30

WG361148LFB2 03/25/14 21:34 101.7LFB WI140306-2 30.5 90 110mg/L30

L17275-04DUP 03/25/14 22:10 16.9DUP 16.9 0mg/L 20

L17275-05AS 03/25/14 23:21 16.9 100AS WI140306-2 46.9 90 110mg/L30

Page 60 of 90L17275-1404011436


Inorganic QC

Summary




WG361239

WG361239ICV 03/27/14 15:22 98.5ICV MS140218-2 .04923 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0015 0.0015mg/L

WG361239LFB 03/27/14 15:29 96.9LFB MS140320-2 .04848 85 115mg/L.05005

L17275-05AS 03/27/14 15:49 U 108.1AS MS140320-2 .05412 70 130mg/L.05005

L17275-05ASD 03/27/14 15:53 U 108.5ASD MS140320-2 .05429 0.3170 130mg/L 20.05005

L17320-01AS 03/27/14 16:37 U 105.8AS MS140320-2 .05297 70 130mg/L.05005

L17320-01ASD 03/27/14 16:47 U 105.5ASD MS140320-2 .05281 0.370 130mg/L 20.05005



WG361380

WG361380ICV 03/28/14 0:07 99ICV MS140218-2 .04952 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0015 0.0015mg/L

WG361214LRB 03/28/14 0:14LRB U -0.0011 0.0011mg/L

WG361214LFB 03/28/14 0:18 99.5LFB MS140320-2 .04979 85 115mg/L.05005

L17275-08LFM 03/28/14 0:58 .0007 94.7LFM MS140320-2 .04808 70 130mg/L.05005

L17275-08LFMD 03/28/14 1:02 .0007 96.3LFMD MS140320-2 .04891 1.7170 130mg/L 20.05005

L17321-02LFM 03/28/14 1:43 .009 79.7LFM MS140320-2 .0489 70 130mg/L.05005

L17321-02LFMD 03/28/14 1:46 .009 82.1LFMD MS140320-2 .0501 2.4270 130mg/L 20.05005



WG361239

WG361239ICV 03/27/14 15:22 98.1ICV MS140218-2 .04904 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.00015 0.00015mg/L

WG361239LFB 03/27/14 15:29 98LFB MS140320-2 .04906 85 115mg/L.05005

L17275-05AS 03/27/14 15:49 .00016 112.8AS MS140320-2 .05662 70 130mg/L.05005

L17275-05ASD 03/27/14 15:53 .00016 109.9ASD MS140320-2 .05515 2.6370 130mg/L 20.05005

L17320-01AS 03/27/14 16:37 .00055 114.5AS MS140320-2 .05785 70 130mg/L.05005

L17320-01ASD 03/27/14 16:47 .00055 111.8ASD MS140320-2 .05653 2.3170 130mg/L 20.05005



WG361380

WG361380ICV 03/28/14 0:07 96.7ICV MS140218-2 .04833 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.00015 0.00015mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00011 0.00011mg/L

WG361214LFB 03/28/14 0:18 100.5LFB MS140320-2 .05028 85 115mg/L.05005

L17275-08LFM 03/28/14 0:58 .0001 100.6LFM MS140320-2 .05043 70 130mg/L.05005

L17275-08LFMD 03/28/14 1:02 .0001 99.7LFMD MS140320-2 .05001 0.8470 130mg/L 20.05005

L17321-02LFM 03/28/14 1:43 .306 98.7LFM MS140320-2 .3554 70 130mg/L.05005

L17321-02LFMD 03/28/14 1:46 .306 95.9LFMD MS140320-2 .354 0.3970 130mg/L 20.05005

Page 61 of 90L17275-1404011436


Inorganic QC

Summary




WG361080



L17275-11DUP 03/24/14 18:37 352DUP 352 0umhos/cm 20

L17282-01DUP 03/24/14 20:12 583DUP 585 0.3umhos/cm 20

WG361080LCSW8 03/24/14 20:17 100.4LCSW PCN43577 1415 90 110umhos/cm1408.8





WG361239

WG361239ICV 03/27/14 15:22 98.8ICV MS140218-2 .04939 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0015 0.0015mg/L

WG361239LFB 03/27/14 15:29 96.8LFB MS140320-2 .04843 85 115mg/L.05005

L17275-05AS 03/27/14 15:49 U 105.3AS MS140320-2 .05268 70 130mg/L.05005

L17275-05ASD 03/27/14 15:53 U 104.2ASD MS140320-2 .05215 1.0170 130mg/L 20.05005

L17320-01AS 03/27/14 16:37 .0008 99.3AS MS140320-2 .05052 70 130mg/L.05005

L17320-01ASD 03/27/14 16:47 .0008 99ASD MS140320-2 .05035 0.3470 130mg/L 20.05005



WG361380

WG361380ICV 03/28/14 0:07 97.5ICV MS140218-2 .04876 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0015 0.0015mg/L

WG361214LRB 03/28/14 0:14LRB U -0.0011 0.0011mg/L

WG361214LFB 03/28/14 0:18 98.5LFB MS140320-2 .04928 85 115mg/L.05005

L17275-08LFM 03/28/14 0:58 U 91.3LFM MS140320-2 .04568 70 130mg/L.05005


L17321-02LFM 03/28/14 1:43 .003 92.5LFM MS140320-2 .0493 70 130mg/L.05005

L17321-02LFMD 03/28/14 1:46 .003 94.5LFMD MS140320-2 .0503 2.0170 130mg/L 20.05005



WG361114

WG361114ICV 03/24/14 18:07 97.8ICV WI140322-7 .2934 90 110mg/L.3

WG361114ICB 03/24/14 18:08ICB U -0.003 0.003mg/L

WG361087LRB 03/24/14 18:09LRB U -0.003 0.003mg/L

WG361087LFB 03/24/14 18:09 100.8LFB WI140322-4 .2015 90 110mg/L.2

L17275-01DUP RA03/24/14 18:11 UDUP U 0mg/L 20

L17275-02LFM 03/24/14 18:13 U 101.7LFM WI140322-4 .2033 90 110mg/L.2

L17275-12DUP RA03/24/14 18:23 UDUP U 0mg/L 20

L17275-13LFM 03/24/14 18:25 U 105.1LFM WI140322-4 .2102 90 110mg/L.2

Page 62 of 90L17275-1404011436


Inorganic QC

Summary




WG361346

WG361346ICV 03/27/14 11:49 98.1ICV WI140322-7 .2942 90 110mg/L.3

WG361346ICB 03/27/14 11:50ICB U -0.003 0.003mg/L

WG361357

WG361218LRB 03/27/14 13:28LRB U -0.003 0.003mg/L

WG361218LFB 03/27/14 13:29 95.1LFB WI140322-6 .1902 90 110mg/L.2

L17264-03LFM 03/27/14 13:31 U 95.1LFM WI140322-6 .1901 90 110mg/L.2

L17275-01DUP RA03/27/14 13:33 UDUP U 0mg/L 20

L17275-11LFM 03/27/14 13:43 U 95.2LFM WI140322-6 .1903 90 110mg/L.2

L17275-12DUP RA03/27/14 13:45 UDUP U 0mg/L 20



WG360290

WG360290ICV 03/06/14 13:49 103.7ICV WI140226-1 4.17 90 110mg/L4.02

WG360290ICB 03/06/14 14:07ICB U -0.3 0.3mg/L

WG361148

WG361148LFB1 03/25/14 12:54 102LFB WI140306-2 1.53 90 110mg/L1.5

L17232-03DUP RA03/25/14 17:41 UDUP U 0mg/L 20

L17232-04AS 03/25/14 18:17 U 106AS WI140306-2 1.59 90 110mg/L1.5

WG361148LFB2 03/25/14 21:34 102.7LFB WI140306-2 1.54 90 110mg/L1.5

L17275-04DUP RA03/25/14 22:10 .44DUP .45 2.2mg/L 20

L17275-05AS 03/25/14 23:21 .45 103.3AS WI140306-2 2 90 110mg/L1.5



WG360973

WG360973ICV 03/21/14 11:24 98ICV II140220-1 1.96 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.3 0.3mg/L

WG360973LFB 03/21/14 11:43 97.9LFB II140317-2 .98 85 115mg/L1.001

L17261-01AS 03/21/14 11:49 U 100.4AS II140317-2 2.01 85 115mg/L2.002

L17261-01ASD 03/21/14 11:52 U 103.4ASD II140317-2 2.07 2.9485 115mg/L 202.002

L17332-01AS 03/21/14 13:01 U 98.9AS II140317-2 .99 85 115mg/L1.001

L17332-01ASD 03/21/14 13:04 U 104.9ASD II140317-2 1.05 5.8885 115mg/L 201.001



WG361188

WG361188ICV 03/26/14 9:50 96ICV II140228-1 1.92 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB U -0.3 0.3mg/L

WG361129LRB 03/26/14 10:09LRB U -0.22 0.22mg/L

WG361129LFB 03/26/14 10:12 100.9LFB II140317-2 1.01 85 115mg/L1.001

L17275-01LFM 03/26/14 10:18 U 98.9LFM II140317-2 .99 70 130mg/L1.001


L17304-01LFM 03/26/14 11:24 U 99.9LFM II140317-2 1 70 130mg/L1.001


Page 63 of 90L17275-1404011436


Inorganic QC

Summary




WG360973

WG360973ICV 03/21/14 11:24 97.8ICV II140220-1 1.955 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.06 0.06mg/L

WG360973LFB 03/21/14 11:43 100.9LFB II140317-2 1.01 85 115mg/L1.0014

L17261-01AS 03/21/14 11:49 U 98.3AS II140317-2 1.969 85 115mg/L2.0028

L17261-01ASD 03/21/14 11:52 U 99.1ASD II140317-2 1.985 0.8185 115mg/L 202.0028

L17332-01AS 03/21/14 13:01 2.03 91AS II140317-2 2.931 85 115mg/L1.0014

L17332-01ASD 03/21/14 13:04 2.03 99.3ASD II140317-2 3.014 2.7985 115mg/L 201.0014



WG361188

WG361188ICV 03/26/14 9:50 97.7ICV II140228-1 1.953 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB U -0.06 0.06mg/L

WG361129LRB 03/26/14 10:09LRB U -0.044 0.044mg/L

WG361129LFB 03/26/14 10:12 102.7LFB II140317-2 1.028 85 115mg/L1.0014

L17275-01LFM 03/26/14 10:18 U 102.7LFM II140317-2 1.028 70 130mg/L1.0014


L17304-01LFM 03/26/14 11:24 U 100.8LFM II140317-2 1.009 70 130mg/L1.0014




WG361239

WG361239ICV 03/27/14 15:22 101.7ICV MS140218-2 .05084 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0003 0.0003mg/L

WG361239LFB 03/27/14 15:29 96.6LFB MS140320-2 .04833 85 115mg/L.05005

L17275-05AS 03/27/14 15:49 U 105.7AS MS140320-2 .05292 70 130mg/L.05005

L17275-05ASD 03/27/14 15:53 U 103.7ASD MS140320-2 .0519 1.9570 130mg/L 20.05005

L17320-01AS 03/27/14 16:37 U 105.3AS MS140320-2 .05271 70 130mg/L.05005

L17320-01ASD 03/27/14 16:47 U 106ASD MS140320-2 .05303 0.6170 130mg/L 20.05005



WG361380

WG361380ICV 03/28/14 0:07 101.1ICV MS140218-2 .05053 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0003 0.0003mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00022 0.00022mg/L

WG361214LFB 03/28/14 0:18 98.6LFB MS140320-2 .04937 85 115mg/L.05005

L17275-08LFM 03/28/14 0:58 U 101.2LFM MS140320-2 .05063 70 130mg/L.05005


L17321-02LFM 03/28/14 1:43 U 99.3LFM MS140320-2 .04968 70 130mg/L.05005


Page 64 of 90L17275-1404011436


Inorganic QC

Summary




WG360973

WG360973ICV 03/21/14 11:24 97.5ICV II140220-1 1.9495 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.024 0.024mg/L

WG360973LFB 03/21/14 11:43 96.5LFB II140317-2 .9651 85 115mg/L1

L17261-01AS 03/21/14 11:49 .52 97.6AS II140317-2 2.472 85 115mg/L2

L17261-01ASD 03/21/14 11:52 .52 97.9ASD II140317-2 2.478 0.2485 115mg/L 202

L17332-01AS 03/21/14 13:01 .088 96.4AS II140317-2 1.052 85 115mg/L1

L17332-01ASD 03/21/14 13:04 .088 100ASD II140317-2 1.088 3.3685 115mg/L 201



WG361188

WG361188ICV 03/26/14 9:50 96ICV II140228-1 1.9192 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB U -0.024 0.024mg/L

WG361129LRB 03/26/14 10:09LRB U -0.0176 0.0176mg/L

WG361129LFB 03/26/14 10:12 96.3LFB II140317-2 .9627 85 115mg/L1

L17275-01LFM 03/26/14 10:18 .021 96.8LFM II140317-2 .989 70 130mg/L1

L17275-01LFMD 03/26/14 10:21 .021 96.1LFMD II140317-2 .9816 0.7570 130mg/L 201

L17304-01LFM 03/26/14 11:24 .011 93.7LFM II140317-2 .9477 70 130mg/L1

L17304-01LFMD 03/26/14 11:27 .011 95.2LFMD II140317-2 .9631 1.6170 130mg/L 201



WG360973

WG360973ICV 03/21/14 11:24 96ICV II140220-1 95.96 95 105mg/L100

WG360973ICB 03/21/14 11:30ICB U -0.6 0.6mg/L

WG360973LFB 03/21/14 11:43 97.7LFB II140317-2 48.86 85 115mg/L50.00131

L17261-01AS 03/21/14 11:49 162 92.6AS II140317-2 254.6 85 115mg/L100.00262

L17261-01ASD 03/21/14 11:52 162 96.8ASD II140317-2 258.8 1.6485 115mg/L 20100.00262

L17332-01AS 03/21/14 13:01 33.2 93.1AS II140317-2 79.77 85 115mg/L50.00131

L17332-01ASD 03/21/14 13:04 33.2 99.5ASD II140317-2 82.97 3.9385 115mg/L 2050.00131



WG361188

WG361188ICV 03/26/14 9:50 96.3ICV II140228-1 96.26 95 105mg/L100

WG361188ICB 03/26/14 9:56ICB U -0.6 0.6mg/L

WG361129LRB 03/26/14 10:09LRB U -0.44 0.44mg/L

WG361129LFB 03/26/14 10:12 98.9LFB II140317-2 49.46 85 115mg/L50.00131

L17275-01LFM 03/26/14 10:18 9.8 99.1LFM II140317-2 59.37 70 130mg/L50.00131

L17275-01LFMD 03/26/14 10:21 9.8 98.4LFMD II140317-2 59.01 0.6170 130mg/L 2050.00131

L17304-01LFM 03/26/14 11:24 15.6 97LFM II140317-2 64.1 70 130mg/L50.00131

L17304-01LFMD 03/26/14 11:27 15.6 99.2LFMD II140317-2 65.21 1.7270 130mg/L 2050.00131

Page 65 of 90L17275-1404011436


Inorganic QC

Summary




WG361239

WG361239ICV 03/27/14 15:22 102.3ICV MS140218-2 .05113 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0015 0.0015mg/L

WG361239LFB 03/27/14 15:29 99.2LFB MS140320-2 .04971 85 115mg/L.0501

L17275-05AS 03/27/14 15:49 .0032 112.7AS MS140320-2 .05968 70 130mg/L.0501

L17275-05ASD 03/27/14 15:53 .0032 110.7ASD MS140320-2 .05866 1.7270 130mg/L 20.0501

L17320-01AS 03/27/14 16:37 .0114 113.6AS MS140320-2 .06829 70 130mg/L.0501

L17320-01ASD 03/27/14 16:47 .0114 110.9ASD MS140320-2 .06698 1.9470 130mg/L 20.0501



WG361380

WG361380ICV 03/28/14 0:07 102.3ICV MS140218-2 .05117 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0015 0.0015mg/L

WG361214LRB 03/28/14 0:14LRB U -0.0011 0.0011mg/L

WG361214LFB 03/28/14 0:18 100.1LFB MS140320-2 .05014 85 115mg/L.0501

L17275-08LFM 03/28/14 0:58 .02 100.3LFM MS140320-2 .07024 70 130mg/L.0501

L17275-08LFMD 03/28/14 1:02 .02 104.5LFMD MS140320-2 .07237 2.9970 130mg/L 20.0501

L17321-02LFM M303/28/14 1:43 106 2275.4LFM MS140320-2 107.14 70 130mg/L.0501

L17321-02LFMD M303/28/14 1:46 106 1477LFMD MS140320-2 106.74 0.3770 130mg/L 20.0501



WG361308

WG361308ICV 03/27/14 12:34 101ICV HG140325-4 10.1 79 121ng/L10

WG361308ICB 03/27/14 12:39ICB U -0.5 0.5ng/L

WG361308PQV 03/27/14 12:44 104PQV HG140325-6 .52 70 130ng/L.5

WG361308LFB 03/27/14 12:49 99LFB HG140325-5 1.98 71 125ng/L2

L17275-06MS 03/27/14 13:20 U 108MS HG140325-5 2.16 71 125ng/L2

L17275-06MSD 03/27/14 13:25 U 108MSD HG140325-5 2.16 071 125ng/L 242

WG361308CCV1 03/27/14 13:30 103CCV HG140325-4 10.3 76.5 123.4ng/L10

WG361308CCB1 03/27/14 13:35CCB U -0.5 0.5ng/L

WG361308CCV2 03/27/14 14:21 105CCV HG140325-4 10.5 76.5 123.4ng/L10

WG361308CCB2 03/27/14 14:26CCB U -0.5 0.5ng/L

L17284-02MS 03/27/14 14:41 1 104.9MS HG5XPREP 11.8 71 125ng/L50

L17284-02MSD 03/27/14 14:46 1 102.9MSD HG5XPREP 11.6 1.7171 125ng/L 2450

WG361308CCV3 03/27/14 15:17 104CCV HG140325-4 10.4 76.5 123.4ng/L10

WG361308CCB3 03/27/14 15:22CCB U -0.5 0.5ng/L

Page 66 of 90L17275-1404011436


Inorganic QC

Summary




WG361393

WG361393ICV 03/28/14 15:59 98.7ICV HG140325-4 9.87 79 121ng/L10

WG361393ICB 03/28/14 16:04ICB U -0.5 0.5ng/L

WG361393PQV 03/28/14 16:09 112PQV HG140325-6 .56 70 130ng/L.5

WG361393LFB 03/28/14 16:14 100LFB HG140325-5 2 71 125ng/L2

L17275-02MS 03/28/14 16:29 .5 104MS HG140325-5 2.58 71 125ng/L2

L17275-02MSD 03/28/14 16:34 .5 105.5MSD HG140325-5 2.61 1.1671 125ng/L 242

WG361393CCV1 03/28/14 16:59 106CCV HG140325-4 10.6 76.5 123.4ng/L10

WG361393CCB1 03/28/14 17:04CCB U -0.5 0.5ng/L

WG361393CCV2 03/28/14 17:55 104CCV HG140325-4 10.4 76.5 123.4ng/L10

WG361393CCB2 03/28/14 18:00CCB U -0.5 0.5ng/L

L17348-01MS 03/28/14 18:10 9.1 90.5MS HG140325-5 10.9 71 125ng/L2

L17348-01MSD 03/28/14 18:15 9.1 90MSD HG140325-5 10.9 071 125ng/L 242

WG361393CCV3 03/28/14 18:40 104CCV HG140325-4 10.4 76.5 123.4ng/L10

WG361393CCB3 03/28/14 18:46CCB U -0.5 0.5ng/L



WG361239

WG361239ICV 03/27/14 15:22 96.8ICV MS140218-2 .01941 90 110mg/L.02006

WG361239ICB 03/27/14 15:25ICB U -0.0015 0.0015mg/L

WG361239LFB 03/27/14 15:29 91.1LFB MS140320-2 .04556 85 115mg/L.05

L17275-05AS 03/27/14 15:49 .0036 102.7AS MS140320-2 .05495 70 130mg/L.05

L17275-05ASD 03/27/14 15:53 .0036 100.9ASD MS140320-2 .05405 1.6570 130mg/L 20.05

L17320-01AS 03/27/14 16:37 .002 108.1AS MS140320-2 .05604 70 130mg/L.05

L17320-01ASD 03/27/14 16:47 .002 101.7ASD MS140320-2 .05286 5.8470 130mg/L 20.05



WG361380

WG361380ICV 03/28/14 0:07 93.9ICV MS140218-2 .01883 90 110mg/L.02006

WG361380ICB 03/28/14 0:11ICB U -0.0015 0.0015mg/L

WG361214LRB 03/28/14 0:14LRB U -0.0011 0.0011mg/L

WG361214LFB 03/28/14 0:18 92.9LFB MS140320-2 .04644 85 115mg/L.05

L17275-08LFM 03/28/14 0:58 .0108 96.9LFM MS140320-2 .05923 70 130mg/L.05

L17275-08LFMD 03/28/14 1:02 .0108 95.4LFMD MS140320-2 .0585 1.2470 130mg/L 20.05

L17321-02LFM 03/28/14 1:43 U 96.8LFM MS140320-2 .0484 70 130mg/L.05


Page 67 of 90L17275-1404011436


Inorganic QC

Summary




WG361239

WG361239ICV 03/27/14 15:22 97.1ICV MS140218-2 .04856 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0018 0.0018mg/L

WG361239LFB 03/27/14 15:29 93.6LFB MS140320-2 .04679 85 115mg/L.05

L17275-05AS 03/27/14 15:49 U 101.4AS MS140320-2 .0507 70 130mg/L.05

L17275-05ASD 03/27/14 15:53 U 101ASD MS140320-2 .05048 0.4370 130mg/L 20.05

L17320-01AS 03/27/14 16:37 .0018 97.3AS MS140320-2 .05047 70 130mg/L.05

L17320-01ASD 03/27/14 16:47 .0018 97.1ASD MS140320-2 .05033 0.2870 130mg/L 20.05



WG361380

WG361380ICV 03/28/14 0:07 97.7ICV MS140218-2 .04883 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0018 0.0018mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00132 0.00132mg/L

WG361214LFB 03/28/14 0:18 96.2LFB MS140320-2 .04811 85 115mg/L.05

L17275-08LFM 03/28/14 0:58 U 90LFM MS140320-2 .04499 70 130mg/L.05


L17321-02LFM 03/28/14 1:43 .345 106.4LFM MS140320-2 .3982 70 130mg/L.05

L17321-02LFMD 03/28/14 1:46 .345 127.2LFMD MS140320-2 .4086 2.5870 130mg/L 20.05



WG361383

WG361383ICV 03/27/14 20:57 104.9ICV WI140116-3 2.535 90 110mg/L2.416

WG361383ICB 03/27/14 20:59ICB U -0.06 0.06mg/L

WG361387

WG361387LFB1 03/27/14 23:04 105.6LFB WI140215-3 2.112 90 110mg/L2

L17273-08AS 03/27/14 23:23 .05 109AS WI140215-3 2.23 90 110mg/L2

L17273-09DUP 03/27/14 23:26 .64DUP .644 0.6mg/L 20

WG361387LFB2 03/27/14 23:39 104.6LFB WI140215-3 2.092 90 110mg/L2

L17275-05AS 03/27/14 23:41 .07 110.4AS WI140215-3 2.277 90 110mg/L2

L17275-06DUP 03/27/14 23:44 .28DUP .274 2.2mg/L 20

Page 68 of 90L17275-1404011436


Inorganic QC

Summary




WG361341

WG361341ICV 03/27/14 11:36 105.7ICV WI131021-1 1.06 90 110mg/L1.003

WG361341ICB 03/27/14 11:39ICB U -0.15 0.15mg/L

WG361347

WG361347LFB1 03/27/14 11:58 101.7LFB WI140113-8 1.017 90 110mg/L1

WG361347LFB2 03/27/14 12:30 103LFB WI140113-8 1.03 90 110mg/L1

L17274-13AS 03/27/14 12:32 .48 101.1AS WI140113-8 1.491 90 110mg/L1

L17274-14DUP RA03/27/14 12:34 UDUP U 0mg/L 20

WG361354

WG361354LFB1 03/27/14 13:10 108.8LFB WI140113-8 1.088 90 110mg/L1

L17275-10AS 03/27/14 13:12 U 99.5AS WI140113-8 .995 90 110mg/L1

L17275-11DUP RA03/27/14 13:14 UDUP U 0mg/L 20

WG361354LFB2 03/27/14 13:42 109.4LFB WI140113-8 1.094 90 110mg/L1

pH (lab) SM4500H+ B


WG361080



L17275-11DUP 03/24/14 18:37 8.2DUP 8.19 0.1units 20

L17282-01DUP 03/24/14 20:12 8.2DUP 8.19 0.1units 20






WG361388

WG361388ICV 03/27/14 23:01 105.3ICV WI140224-3 .687 90 110mg/L.65228

WG361388ICB 03/27/14 23:04ICB U -0.03 0.03mg/L

WG361389

WG361328LRB 03/27/14 23:53LRB U -0.03 0.03mg/L

WG361328LFB 03/27/14 23:54 103LFB WI140326-3 .515 90 110mg/L.5

L17275-01LFM 03/28/14 0:13 U 105.4LFM WI140326-3 .527 90 110mg/L.5

L17275-02DUP RA03/28/14 0:15 .01DUP U 200mg/L 20

WG361457

WG361457ICV 03/28/14 21:54 107.9ICV WI140224-3 .704 90 110mg/L.65228

WG361457ICB 03/28/14 21:57ICB U -0.03 0.03mg/L

WG361423LRB 03/28/14 21:58LRB U -0.03 0.03mg/L

WG361423LFB 03/28/14 21:59 105.4LFB WI140326-3 .527 90 110mg/L.5

L17275-12LFM 03/28/14 22:01 U 102.2LFM WI140326-3 .511 90 110mg/L.5

L17275-13DUP RA03/28/14 22:03 UDUP U 0mg/L 20

Page 69 of 90L17275-1404011436


Inorganic QC

Summary




WG360973

WG360973ICV 03/21/14 11:24 96.9ICV II140220-1 19.37 95 105mg/L20

WG360973ICB 03/21/14 11:30ICB U -0.6 0.6mg/L

WG360973LFB 03/21/14 11:43 99.5LFB II140317-2 99.5 85 115mg/L99.99364

L17261-01AS 03/21/14 11:49 21.4 103.1AS II140317-2 227.6 85 115mg/L199.98728

L17261-01ASD 03/21/14 11:52 21.4 104.8ASD II140317-2 231 1.4885 115mg/L 20199.98728

L17332-01AS 03/21/14 13:01 4.4 99AS II140317-2 103.4 85 115mg/L99.99364

L17332-01ASD 03/21/14 13:04 4.4 104ASD II140317-2 108.4 4.7285 115mg/L 2099.99364



WG361188

WG361188ICV 03/26/14 9:50 96.2ICV II140228-1 19.24 95 105mg/L20

WG361188ICB 03/26/14 9:56ICB U -0.6 0.6mg/L

WG361129LRB 03/26/14 10:09LRB U -0.44 0.44mg/L

WG361129LFB 03/26/14 10:12 99.2LFB II140317-2 99.15 85 115mg/L99.99364

L17275-01LFM 03/26/14 10:18 4.7 100.3LFM II140317-2 105 70 130mg/L99.99364

L17275-01LFMD 03/26/14 10:21 4.7 99.5LFMD II140317-2 104.2 0.7670 130mg/L 2099.99364

L17304-01LFM 03/26/14 11:24 .9 97.5LFM II140317-2 98.36 70 130mg/L99.99364

L17304-01LFMD 03/26/14 11:27 .9 99.1LFMD II140317-2 99.99 1.6470 130mg/L 2099.99364



WG360922

WG360922PBW 03/20/14 11:46PBW U -20 20mg/L


L17253-02DUP 03/20/14 12:17 790DUP 798 1mg/L 10

WG360981

WG360981PBW 03/21/14 9:00PBW U -20 20mg/L


L17354-01DUP 03/21/14 9:44 160DUP 158 1.3mg/L 10

WG361035

WG361035PBW 03/21/14 15:38PBW U -20 20mg/L


L17275-14DUP 03/21/14 16:27 380DUP 384 1mg/L 10



WG361016

WG361016PBW 03/21/14 12:18PBW U -15 15mg/L


L17354-01DUP RA03/21/14 12:49 UDUP 5 200mg/L 10

WG361048

WG361048PBW 03/22/14 11:00PBW U -15 15mg/L

WG361048LCSW 03/22/14 11:02 95LCSW PCN45340 152 80 120mg/L160

L17275-11DUP RA03/22/14 11:31 UDUP U 0mg/L 10

L17282-01DUP RA03/22/14 12:00 20DUP 19 5.1mg/L 10

Page 70 of 90L17275-1404011436


Inorganic QC

Summary




WG360973

WG360973ICV 03/21/14 11:24 99ICV II140220-1 1.98 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.3 0.3mg/L

WG360973LFB 03/21/14 11:43 104.9LFB II140317-2 1.05 85 115mg/L1.0009

L17261-01AS 03/21/14 11:49 U 104.4AS II140317-2 2.09 85 115mg/L2.0018

L17261-01ASD 03/21/14 11:52 U 104.9ASD II140317-2 2.1 0.4885 115mg/L 202.0018

L17332-01AS 03/21/14 13:01 U 103.9AS II140317-2 1.04 85 115mg/L1.0009

L17332-01ASD 03/21/14 13:04 U 106.9ASD II140317-2 1.07 2.8485 115mg/L 201.0009



WG361188

WG361188ICV 03/26/14 9:50 98.5ICV II140228-1 1.97 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB U -0.3 0.3mg/L

WG361129LRB 03/26/14 10:09LRB U -0.22 0.22mg/L

WG361129LFB 03/26/14 10:12 106.9LFB II140317-2 1.07 85 115mg/L1.0009

L17275-01LFM 03/26/14 10:18 U 107.9LFM II140317-2 1.08 70 130mg/L1.0009


L17304-01LFM 03/26/14 11:24 U 106.9LFM II140317-2 1.07 70 130mg/L1.0009




WG361239

WG361239ICV 03/27/14 15:22 100.7ICV MS140218-2 .05036 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0003 0.0003mg/L

WG361239LFB 03/27/14 15:29 94.4LFB MS140320-2 .04724 85 115mg/L.05005

L17275-05AS 03/27/14 15:49 .0059 115.9AS MS140320-2 .06393 70 130mg/L.05005

L17275-05ASD 03/27/14 15:53 .0059 112.4ASD MS140320-2 .06217 2.7970 130mg/L 20.05005

L17320-01AS 03/27/14 16:37 U 112.2AS MS140320-2 .05615 70 130mg/L.05005

L17320-01ASD 03/27/14 16:47 U 110.6ASD MS140320-2 .05537 1.470 130mg/L 20.05005



WG361380

WG361380ICV 03/28/14 0:07 99.4ICV MS140218-2 .04968 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0003 0.0003mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00022 0.00022mg/L

WG361214LFB 03/28/14 0:18 112LFB MS140320-2 .05604 85 115mg/L.05005

L17275-08LFM 03/28/14 0:58 .0039 88.6LFM MS140320-2 .04826 70 130mg/L.05005

L17275-08LFMD 03/28/14 1:02 .0039 90.1LFMD MS140320-2 .04899 1.570 130mg/L 20.05005

L17321-02LFM 03/28/14 1:43 U 105.1LFM MS140320-2 .05262 70 130mg/L.05005


Page 71 of 90L17275-1404011436


Inorganic QC

Summary




WG361239

WG361239ICV 03/27/14 15:22 99.2ICV MS140218-2 .01986 90 110mg/L.02002

WG361239ICB 03/27/14 15:25ICB U -0.00015 0.00015mg/L

WG361239LFB 03/27/14 15:29 94.8LFB MS140320-2 .009486 85 115mg/L.01001

L17275-05AS 03/27/14 15:49 U 96.2AS MS140320-2 .009627 70 130mg/L.01001

L17275-05ASD 03/27/14 15:53 U 93.5ASD MS140320-2 .009356 2.8670 130mg/L 20.01001

L17320-01AS 03/27/14 16:37 U 89.5AS MS140320-2 .008961 70 130mg/L.01001

L17320-01ASD 03/27/14 16:47 U 88.1ASD MS140320-2 .008818 1.6170 130mg/L 20.01001



WG361380

WG361380ICV 03/28/14 0:07 97.3ICV MS140218-2 .01947 90 110mg/L.02002

WG361380ICB 03/28/14 0:11ICB U -0.00015 0.00015mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00011 0.00011mg/L

WG361214LFB 03/28/14 0:18 98.1LFB MS140320-2 .009822 85 115mg/L.01001

L17275-08LFM 03/28/14 0:58 U 96.4LFM MS140320-2 .00965 70 130mg/L.01001


L17321-02LFM 03/28/14 1:43 U 93.9LFM MS140320-2 .0094 70 130mg/L.01001




WG360973

WG360973ICV 03/21/14 11:24 98.1ICV II140220-1 98.09 95 105mg/L100

WG360973ICB 03/21/14 11:30ICB U -0.6 0.6mg/L

WG360973LFB 03/21/14 11:43 99.6LFB II140317-2 99.63 85 115mg/L100.0393

L17261-01AS 03/21/14 11:49 85.4 101.1AS II140317-2 287.6 85 115mg/L200.0786

L17261-01ASD 03/21/14 11:52 85.4 103.1ASD II140317-2 291.6 1.3885 115mg/L 20200.0786

L17332-01AS 03/21/14 13:01 44.8 97.4AS II140317-2 142.2 85 115mg/L100.0393

L17332-01ASD 03/21/14 13:04 44.8 103.5ASD II140317-2 148.3 4.285 115mg/L 20100.0393



WG361188

WG361188ICV 03/26/14 9:50 98.2ICV II140228-1 98.22 95 105mg/L100

WG361188ICB 03/26/14 9:56ICB U -0.6 0.6mg/L

WG361129LRB 03/26/14 10:09LRB U -0.44 0.44mg/L

WG361129LFB 03/26/14 10:12 101LFB II140317-2 101 85 115mg/L100.0393

L17275-01LFM 03/26/14 10:18 20.5 101.9LFM II140317-2 122.4 70 130mg/L100.0393

L17275-01LFMD 03/26/14 10:21 20.5 101.4LFMD II140317-2 121.9 0.4170 130mg/L 20100.0393

L17304-01LFM 03/26/14 11:24 41.6 100.5LFM II140317-2 142.1 70 130mg/L100.0393

L17304-01LFMD 03/26/14 11:27 41.6 103.3LFMD II140317-2 144.9 1.9570 130mg/L 20100.0393

Page 72 of 90L17275-1404011436


Inorganic QC

Summary




WG360973

WG360973ICV 03/21/14 11:24 99.1ICV II140220-1 1.9822 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.015 0.015mg/L

WG360973LFB 03/21/14 11:43 99.3LFB II140317-2 .4966 85 115mg/L.5

L17261-01AS 03/21/14 11:49 1.62 93.6AS II140317-2 2.556 85 115mg/L1

L17261-01ASD 03/21/14 11:52 1.62 96.2ASD II140317-2 2.582 1.0185 115mg/L 201

L17332-01AS 03/21/14 13:01 1.81 87.2AS II140317-2 2.246 85 115mg/L.5

L17332-01ASD 03/21/14 13:04 1.81 103ASD II140317-2 2.325 3.4685 115mg/L 20.5



WG361188

WG361188ICV 03/26/14 9:50 98.3ICV II140228-1 1.9658 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB U -0.015 0.015mg/L

WG361129LRB 03/26/14 10:09LRB U -0.011 0.011mg/L

WG361129LFB 03/26/14 10:12 97.6LFB II140317-2 .4879 85 115mg/L.5

L17275-01LFM 03/26/14 10:18 .202 97.9LFM II140317-2 .6917 70 130mg/L.5

L17275-01LFMD 03/26/14 10:21 .202 97.3LFMD II140317-2 .6885 0.4670 130mg/L 20.5

L17304-01LFM 03/26/14 11:24 .391 95.2LFM II140317-2 .8672 70 130mg/L.5

L17304-01LFMD 03/26/14 11:27 .391 98.3LFMD II140317-2 .8823 1.7370 130mg/L 20.5



WG360290

WG360290ICV 03/06/14 13:49 102.5ICV WI140226-1 51.2 90 110mg/L49.95

WG360290ICB 03/06/14 14:07ICB U -1.5 1.5mg/L

WG361148

WG361148LFB1 03/25/14 12:54 100.7LFB WI140306-2 30.2 90 110mg/L30

L17232-03DUP 03/25/14 17:41 23.1DUP 23.1 0mg/L 20

L17232-04AS 03/25/14 18:17 19.7 99.7AS WI140306-2 49.6 90 110mg/L30

WG361148LFB2 03/25/14 21:34 100.7LFB WI140306-2 30.2 90 110mg/L30

L17275-04DUP 03/25/14 22:10 47DUP 47 0mg/L 20

L17275-05AS 03/25/14 23:21 47.1 97.7AS WI140306-2 76.4 90 110mg/L30



WG361239

WG361239ICV 03/27/14 15:22 106.3ICV MS140218-2 .05316 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0003 0.0003mg/L

WG361239LFB 03/27/14 15:29 98.9LFB MS140320-2 .04965 85 115mg/L.0502

L17275-05AS 03/27/14 15:49 U 111AS MS140320-2 .05571 70 130mg/L.0502

L17275-05ASD 03/27/14 15:53 U 108.8ASD MS140320-2 .0546 2.0170 130mg/L 20.0502

L17320-01AS 03/27/14 16:37 U 110.9AS MS140320-2 .05566 70 130mg/L.0502

L17320-01ASD 03/27/14 16:47 U 110.6ASD MS140320-2 .05551 0.2770 130mg/L 20.0502

Page 73 of 90L17275-1404011436


Inorganic QC

Summary




WG361380

WG361380ICV 03/28/14 0:07 106.4ICV MS140218-2 .05319 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0003 0.0003mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00022 0.00022mg/L

WG361214LFB 03/28/14 0:18 101.4LFB MS140320-2 .0509 85 115mg/L.0502

L17275-08LFM 03/28/14 0:58 U 105.5LFM MS140320-2 .05296 70 130mg/L.0502


L17321-02LFM 03/28/14 1:43 .0003 101.9LFM MS140320-2 .05146 70 130mg/L.0502

L17321-02LFMD 03/28/14 1:46 .0003 103LFMD MS140320-2 .052 1.0470 130mg/L 20.0502



WG361239

WG361239ICV 03/27/14 15:22 103.5ICV MS140218-2 .05192 90 110mg/L.05015

WG361239ICB 03/27/14 15:25ICB U -0.0003 0.0003mg/L

WG361239LFB 03/27/14 15:29 94.3LFB MS140320-2 .04721 85 115mg/L.05005

L17275-05AS 03/27/14 15:49 U 101.4AS MS140320-2 .05077 70 130mg/L.05005

L17275-05ASD 03/27/14 15:53 U 99.7ASD MS140320-2 .04988 1.7770 130mg/L 20.05005

L17320-01AS 03/27/14 16:37 .0007 103.6AS MS140320-2 .05255 70 130mg/L.05005

L17320-01ASD 03/27/14 16:47 .0007 99.7ASD MS140320-2 .0506 3.7870 130mg/L 20.05005



WG361380

WG361380ICV 03/28/14 0:07 100.5ICV MS140218-2 .0504 90 110mg/L.05015

WG361380ICB 03/28/14 0:11ICB U -0.0003 0.0003mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00022 0.00022mg/L

WG361214LFB 03/28/14 0:18 96.5LFB MS140320-2 .04829 85 115mg/L.05005

L17275-08LFM 03/28/14 0:58 .0002 96.8LFM MS140320-2 .04867 70 130mg/L.05005

L17275-08LFMD 03/28/14 1:02 .0002 95.7LFMD MS140320-2 .04811 1.1670 130mg/L 20.05005

L17321-02LFM 03/28/14 1:43 U 98.1LFM MS140320-2 .0491 70 130mg/L.05005




WG360973

WG360973ICV 03/21/14 11:24 95.2ICV II140220-1 1.9045 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.015 0.015mg/L

WG360973LFB 03/21/14 11:43 96.6LFB II140317-2 .9658 85 115mg/L1

L17261-01AS 03/21/14 11:49 U 96AS II140317-2 1.919 85 115mg/L2

L17261-01ASD 03/21/14 11:52 U 96.6ASD II140317-2 1.931 0.6285 115mg/L 202

L17332-01AS 03/21/14 13:01 .005 95.6AS II140317-2 .9614 85 115mg/L1

L17332-01ASD 03/21/14 13:04 .005 98.8ASD II140317-2 .9926 3.1985 115mg/L 201

Page 74 of 90L17275-1404011436


Inorganic QC

Summary




WG361188

WG361188ICV 03/26/14 9:50 96.6ICV II140228-1 1.9312 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB U -0.015 0.015mg/L

WG361129LRB 03/26/14 10:09LRB U -0.011 0.011mg/L

WG361129LFB 03/26/14 10:12 98.8LFB II140317-2 .9875 85 115mg/L1

L17275-01LFM 03/26/14 10:18 .009 98.9LFM II140317-2 .9982 70 130mg/L1

L17275-01LFMD 03/26/14 10:21 .009 98.3LFMD II140317-2 .9919 0.6370 130mg/L 201

L17304-01LFM 03/26/14 11:24 .007 96.6LFM II140317-2 .9726 70 130mg/L1

L17304-01LFMD 03/26/14 11:27 .007 97.8LFMD II140317-2 .9853 1.370 130mg/L 201



WG361239

WG361239ICV 03/27/14 15:22 102.3ICV MS140218-2 .05115 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0003 0.0003mg/L

WG361239LFB 03/27/14 15:29 101.3LFB MS140320-2 .05064 85 115mg/L.05

L17275-05AS 03/27/14 15:49 .0047 111AS MS140320-2 .0602 70 130mg/L.05

L17275-05ASD 03/27/14 15:53 .0047 109.3ASD MS140320-2 .05935 1.4270 130mg/L 20.05

L17320-01AS 03/27/14 16:37 .0062 112.3AS MS140320-2 .06234 70 130mg/L.05

L17320-01ASD 03/27/14 16:47 .0062 112.3ASD MS140320-2 .06237 0.0570 130mg/L 20.05



WG361380

WG361380ICV 03/28/14 0:07 101.6ICV MS140218-2 .0508 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0003 0.0003mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00022 0.00022mg/L

WG361214LFB 03/28/14 0:18 102.5LFB MS140320-2 .05127 85 115mg/L.05

L17275-08LFM 03/28/14 0:58 .0045 107.8LFM MS140320-2 .05841 70 130mg/L.05

L17275-08LFMD 03/28/14 1:02 .0045 107.1LFMD MS140320-2 .05807 0.5870 130mg/L 20.05

L17321-02LFM 03/28/14 1:43 .004 106LFM MS140320-2 .057 70 130mg/L.05

L17321-02LFMD 03/28/14 1:46 .004 107.8LFMD MS140320-2 .05792 1.670 130mg/L 20.05



WG361239

WG361239ICV 03/27/14 15:22 97.7ICV MS140218-2 .04883 90 110mg/L.05

WG361239ICB 03/27/14 15:25ICB U -0.0006 0.0006mg/L

WG361239LFB 03/27/14 15:29 99.4LFB MS140320-2 .04976 85 115mg/L.05005

L17275-05AS 03/27/14 15:49 .0328 113.6AS MS140320-2 .08965 70 130mg/L.05005

L17275-05ASD 03/27/14 15:53 .0328 113.3ASD MS140320-2 .0895 0.1770 130mg/L 20.05005

L17320-01AS 03/27/14 16:37 U 113.9AS MS140320-2 .057 70 130mg/L.05005

L17320-01ASD 03/27/14 16:47 U 113.1ASD MS140320-2 .05662 0.6770 130mg/L 20.05005

Page 75 of 90L17275-1404011436


Inorganic QC

Summary




WG361380

WG361380ICV 03/28/14 0:07 97.6ICV MS140218-2 .04882 90 110mg/L.05

WG361380ICB 03/28/14 0:11ICB U -0.0006 0.0006mg/L

WG361214LRB 03/28/14 0:14LRB U -0.00044 0.00044mg/L

WG361214LFB 03/28/14 0:18 101.5LFB MS140320-2 .05078 85 115mg/L.05005

L17275-08LFM 03/28/14 0:58 .0422 98.1LFM MS140320-2 .09132 70 130mg/L.05005

L17275-08LFMD 03/28/14 1:02 .0422 99.7LFMD MS140320-2 .09208 0.8370 130mg/L 20.05005

L17321-02LFM 03/28/14 1:43 .0019 102.6LFM MS140320-2 .05324 70 130mg/L.05005

L17321-02LFMD 03/28/14 1:46 .0019 103.5LFMD MS140320-2 .05372 0.970 130mg/L 20.05005



WG360973

WG360973ICV 03/21/14 11:24 97.1ICV II140220-1 1.942 95 105mg/L2

WG360973ICB 03/21/14 11:30ICB U -0.03 0.03mg/L

WG360973LFB 03/21/14 11:43 99.1LFB II140317-2 .496 85 115mg/L.5005

L17261-01AS 03/21/14 11:49 .06 101.1AS II140317-2 1.072 85 115mg/L1.001

L17261-01ASD 03/21/14 11:52 .06 103.7ASD II140317-2 1.098 2.485 115mg/L 201.001

L17332-01AS 03/21/14 13:01 U 99.1AS II140317-2 .496 85 115mg/L.5005

L17332-01ASD 03/21/14 13:04 U 104.1ASD II140317-2 .521 4.9285 115mg/L 20.5005



WG361188

WG361188ICV 03/26/14 9:50 96.7ICV II140228-1 1.933 95 105mg/L2

WG361188ICB 03/26/14 9:56ICB U -0.03 0.03mg/L

WG361129LRB 03/26/14 10:09LRB U -0.022 0.022mg/L

WG361129LFB 03/26/14 10:12 102.1LFB II140317-2 .511 85 115mg/L.5005

L17275-01LFM 03/26/14 10:18 U 103.3LFM II140317-2 .517 70 130mg/L.5005


L17304-01LFM 03/26/14 11:24 .03 103.1LFM II140317-2 .546 70 130mg/L.5005

L17304-01LFMD 03/26/14 11:27 .03 101.9LFMD II140317-2 .54 1.170 130mg/L 20.5005

Page 76 of 90L17275-1404011436


Inorganic Extended

Qualifier Report




M200.7 ICPCalcium, dissolvedL17275-01 WG360973



























SM4500-CN I-Colorimetric w/

distillation








M365.1 - Auto Ascorbic Acid

(digest)




REPAD.15.06.05.01

Page 77 of 90L17275-1404011436


Inorganic Extended

Qualifier Report









































REPAD.15.06.05.01

Page 78 of 90L17275-1404011436


Inorganic Extended

Qualifier Report





Q5 Sample received with inadequate chemical preservation. Additional preservation performed by the laboratory.

M1631, Atomic FluorescenceMercury, totalWG361393





































REPAD.15.06.05.01

Page 79 of 90L17275-1404011436


Inorganic Extended

Qualifier Report

























distillation















REPAD.15.06.05.01

Page 80 of 90L17275-1404011436


Inorganic Extended

Qualifier Report






M200.8 ICP-MSManganese, totalWG361380
















M3 The spike recovery value is unusable since the analyte

concentration in the sample is disproportionate to the spike level. The recovery of the associated control sample (LCS or LFB) was acceptable.

M200.8 ICP-MSManganese, totalL17275-11 WG361380
















REPAD.15.06.05.01

Page 81 of 90L17275-1404011436


Inorganic Extended

Qualifier Report

























distillation















REPAD.15.06.05.01

Page 82 of 90L17275-1404011436


Inorganic Extended

Qualifier Report




















REPAD.15.06.05.01

Page 83 of 90L17275-1404011436


Certification

Qualifiers


Metals Analysis










REPAD.05.06.05.01

Page 84 of 90L17275-1404011436


Sample

Receipt


ACZ Project ID:

Date Received:

Received By: mtb

03/19/2014 10:05

L17275




NANOYES

X

X

X

X

X

X









NANOYES

X

X

X

X

X

X

X

X

X

8) Are all containers intact and with no leaks?











Samples/Containers

X

X

Shipping Containers

L17275-04 Container B1443090 (HG-1631 D): This cont ainer was received broken and the associated analysis were re moved from the project.

Cooler Id Temp (°C) Rad (µR/Hr) Custody Seal Intact?--------- --------- ----------- ------- -------------NA19306 0.2 13 YesNA19307 0.9 13 YesNA19308 1.4 13 YesNA19309 0.9 13 Yes

X



REPAD LPII 2012-03

Page 85 of 90L17275-1404011436


Sample

Receipt


ACZ Project ID:

Date Received:

Received By: mtb

03/19/2014 10:05

L17275



REPAD LPII 2012-03

Page 86 of 90L17275-1404011436

Page 87 of 90L17275-1404011436

Page 88 of 90L17275-1404011436

Page 89 of 90L17275-1404011436

Page 90 of 90L17275-1404011436

Documents

water reports/ACZ Level 2...BD[ Laboratories, Inc. 2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 Analytical Report SPF Water Engineering 300 E. Mallard Drive, Suite