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W A5 Nitric acid Berman, Laura Michelle W A14 N-propanol Bollens, Rachel Ryan W B3 Phosphoric Acid Calhoun, Corinne Sarah W B5 Phosphorous pentoxide Clute-Reinig, Nicholas Michael W B14 Potassium Bromide Crawford, Catherine Rose W C3 Potassium Chloride Cyr, Christina Alene W C14 Potassium dichromate Evarkiou-Kaku, Anatolia Maya W D3 Potassium Iodide Ferguson, Luke Antrim W D5 Potassium Nitrate Fernald, Samuel J. W D14 Potassium Nitrite Folse, Katherine Marie W E3 Potassium oxalate Forrester, William Phillip W E14 Potassium Periodate Ho, Vanessa W F3 Potassium Permanganate Kuo, Linus W F5 Potassium thiocyanate Pitkin, Julia Gabrielle W F14 secondary-butyl alcohol Liu, Melinda W G3 Silver Nitrate Takahashi, Alexis Naoko W G5 Sodium acetate Tarhan, Leyla Yasemin W G14 Sodium bicarbonate Valdez, Stephanie W H3 Sodium Carbonate Vega, Alejandra Dessire W H14 Sodium nitrite Vega, Marvin Marcus W I3 Sodium Sulfite Wang, Kevin Yih Jiun W I14 Sulfuric acid Washington, Shannon Kim W J3 tertiary-butyl alcohol Winninghoff, Hayley Derome W J5 Tetraethylammonium chloride monohydrate Zahedi, Leila Marie

WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

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Page 1: WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

W A5 Nitric acid Berman, Laura Michelle

W A14 N-propanol Bollens, Rachel Ryan

W B3 Phosphoric Acid Calhoun, Corinne Sarah

W B5 Phosphorous pentoxide Clute-Reinig, Nicholas Michael

W B14 Potassium Bromide Crawford, Catherine Rose

W C3 Potassium Chloride Cyr, Christina Alene

W C14 Potassium dichromate Evarkiou-Kaku, Anatolia Maya

W D3 Potassium Iodide Ferguson, Luke Antrim

W D5 Potassium Nitrate Fernald, Samuel J.

W D14 Potassium Nitrite Folse, Katherine Marie

W E3 Potassium oxalate Forrester, William Phillip

W E14 Potassium Periodate Ho, Vanessa

W F3 Potassium Permanganate Kuo, Linus

W F5 Potassium thiocyanate Pitkin, Julia Gabrielle

W F14 secondary-butyl alcohol Liu, Melinda

W G3 Silver Nitrate Takahashi, Alexis Naoko

W G5 Sodium acetate Tarhan, Leyla Yasemin

W G14 Sodium bicarbonate Valdez, Stephanie

W H3 Sodium Carbonate Vega, Alejandra Dessire

W H14 Sodium nitrite Vega, Marvin Marcus

W I3 Sodium Sulfite Wang, Kevin Yih Jiun

W I14 Sulfuric acid Washington, Shannon Kim

W J3 tertiary-butyl alcohol Winninghoff, Hayley Derome

W J5 Tetraethylammonium chloride monohydrate Zahedi, Leila Marie

Page 2: WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

Chemistry 1B Laboratory

Spring 2010

Page 3: WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

Lab Assistants:

Monday – Kori VanDerGeestTuesday – Kelly MurphyWednesday – Jane Xu

Thursday – Connie ClarkeFriday – Albert Liu

Page 4: WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

ExperimentsPOINTS

Excel Exercise 10

Safety and Chemical Resources Worksheets

5

Introduction to Electrochemical Cells

10

Colorimetric Determination of Manganese

15

Gas Chromatography 10

Enthalpy of Reaction 15

Neutron Activation 10

Inorganic Synthesis 30

Molecular Modeling lab 15

Kinetics 10

Total 130

Page 5: WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

Today

REVIEW of Lab Safety

Lab Safety & MSDS worksheets

EXCEL exercises

Safety assignment

Page 6: WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

MSDSMaterial Safety Data Sheet

• properties of a particular substance• procedures for handling, storing, disposing

or working with that substance in a safe manner

• physical data (melting point, boiling point, flash point, etc.), toxicity, health effects, first aid, reactivity,

• format of an MSDS can vary from source to source (click here for an example)

Page 7: WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

MSDS – where do you find them?

• Every chemical supplier (Sigma, Spectrum) must provide an MSDS for each product.

• Consumers can see a copy of MSDS if one knows the compound’s name.

• Available onlinewww.chemistry.pomona.edu has a link to “moldata” and “environmental chemistry”

www.sigma-aldrich.com

Google, Wikipedia

Page 8: WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

Other safety data

• CRC Handbook of Chemistry

• Merck Index

• Library information

Flammability, health hazard, reactivity, special precautions

Page 9: WA5Nitric acid Berman, Laura Michelle WA14N-propanol Bollens, Rachel Ryan WB3Phosphoric Acid Calhoun, Corinne Sarah WB5Phosphorous pentoxide Clute-Reinig,

Specific Hazard- White SectionOxidizers OXY

Acids ACIDAlkali ALK

Corrosives CORUse NO WATER WRadiation HazardNow let’s go into the lab to review safety…

Flammable - RedSusceptibility to Burning4 Deadly - Flash point is below 73°F

- Very Flammable.

3 Danger - Flash point is below 100°F - Can ignites under normal temperature conditions.

2 Hazardous - Flash point is below 200°F - Ignites with moderate heating.

1 Slightly hazardous -Flash point above 200°F - Ignites when preheated.

0 Normal - Will NOT burn.

Reactive - YellowSusceptibility for Energy Release 4 May detonate under normal conditions.3 May detonate with shock or heat.2 Violent chemical change but does not

detonate.1 Not stable if heated, use precautions.0 Normally stable.

Health Hazard- BlueRecommended Protection 4 Special full protective suit and

breathing apparatus must be worn.3 Full protective suit and breathing

apparatus should be worn.2 Breathing apparatus with full face

mask should be worn.1 Breathing apparatus may be worn.0 No precautions necessary.