Varian GC450 User Manual Russian

450

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450

1

P.O. Box 13 Moscow 119311 Russia E-mail: [email protected]

Tel.: +7.495.737.53.67 Fax: +7.495.737.53.69 Homepage: http://www.petrotech.ru/

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, , , : 73/23/ (93/68/) (The Low Voltage Directive) 89/336/ (92/31/ 93/68/) (The EMC Directive) UL 61010-1:2004 R7.05 CSA 22.2. 61010. 1: 2004 EN 61326: 2003 47 CFR 15 J55022: 2002 CISPR 22:1996 (Denan Law) 1.6 : 450-

:

- : G.A. Wassink : Varian B.V. : Hercusweg 8

: : : 23 2005

P.O. Box 8033 4330 EA Middelburg The Netherlands : +31 (0) 118 671 000 : +31 (0) 118 633 118

/ - : Anand Shirur : c: Varian, Inc. 2700 Mitchell drive

: :

Wallnut Creek, California 94598 USA

12



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: 2 2008 : 925-939-2400 : 925-945-2360

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C Varian ............................................................ 3 ......................................................................................................................... 3 ................................................................................................ 3 .............................................................................................. 3 ........................................................................................................... 3 .......................................... 4 .............................................................................................. 5 ........................................................................................................................... 5 .............................................................................................. 5 .......................................................................................... 8 . ......................................................................................................................................................... 8 .................................................................................................... 9 ............................................................................................................ 9 ...................................................................................................... 10 ...................................................................................................... 12 73/23/ (93/68/) ...................................................... 12 .......................................................................................................... 12 - .................................................................................................................. 12 / - ............................................... 12 : 2 2008.................................................................................................................... 1314



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: 925-939-2400 .............................................................................................................. 13 : 925-945-2360 .............................................................................................................. 13

C .............................................................................................................................. 14 ........................................................................................................................... 34 ..................................................................................................................................... 36 450- ........................................................ 36 ....................................................................................................................... 36 450-.................................................................................................... 37 .......................................................................................... 38 ................................................................................................................................... 39 450-............................................. 39 ........................................................................................................ 39 ............................................................................................................................. 39 ......................................................................................................................... 39 ......................................................................................................................... 42 -................................................. 43 .................................................... 44 ........................................................................ 44 .................................................................... 45 .......................................................................................................... 45 -8400/8410.......................................................................... 46 ............................................................................................. 48 ..................................................................... 49 .................................................................. 5115



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................................................. 53 ................................................. 57 ................................................................. 59 .................................................. 59 Varian .................................................................................................. 61 - .................................... 61 .................................................. 63 ................................................................................. 65 - 67 ................................................................................... 67 ........................................................................................ 68 .................................................. 70 .................... 72 .......................................................................... 72 .................................................................................................................. 74 - , . 74 .................................................................................. 77 ........................................................ 77 Varian Varian ............................................................................................................................................... 78 ..................................................................................... 80 .......................................................................................................... 82 .................................................................................... 84 ......................................................................................................... 84 ...................................................................................................... 8616



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.................................................................................................. 86 J504/ J505 S.I.D. 1 2............................................................................................................. 88 J401 ......................................................................................................... 90 J302 ............................................................................................. 92 J45/ J46 1 2 ........................................................................................... 94 J44 (3)................................................................................................................. 95 J42/J43 .................................................................................................... 96 J41 .............................................................................................. 98 ....................................................................................................................... 100 ....................................................................................................... 102 ....................................................... 104 ............................................................................................................... 105 ............................................................................... 106 ........................................................................................................ 106 Error () ............................................................................................. 108 ..................................................................... 109

............................................................. 110

...................................................................................... 111

.................................................................................................... 112 ..................................................................................................................................... 113 ................................................................................................................ 114

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.................................................................................. 115

......................................................................................................... 117 ................................................................................................................ 119 ................................................................................................ 120 .............................................................................................................. 124 .................................................................................................................... 126 ................................................................................................................. 127 / .................................................................................................... 129 ............................................................................................................................. 131 ........................................................................................................ 132 .......................................................................................................... 133 ............................................................................................................ 134 ............................................................................... 134 (-8400) .......................................................................................................... 135 .................................................................................................................. 138 .............................................................................................................. 141 ..................................................................................................................... 143 ................................................................................................................. 144 ................................................................................................................ 146 ...................................................................................................... 148 ................................................................................................................... 149 : ........................................................................................................... 149 : ....................................................................................................................................... 15118



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.................................................................................... 152 .......................................................................................................................... 152 ....................................................................................................................... 152 / ........................................................................ 157 ............................................................................................... 161 .............................................................................................................................. 162 ............................................................................................................................... 162 Ethernet .......................................................................................................... 162 IP Galaxie, BOOTP (DHCP) ............................................................................................. 164 IP 450-..................................................... 168 ............................................................................................................ 169 ............................................................................................................................... 171 ..................................................................................................................... 171 ..................................................................................................... 171 - .................................................................................................................. 173 .................................................................................. 175 ...................................................................................... 177 ................................................................................................ 177 -8400/ 8410 ................................................................................................. 179 ............................................................................................................................... 179 -8400/ 8410 ................................................................................................... 181 ......................................................................................... 189 / .............................................................. 191 ........................................................................................................................... 19319



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........................................................................................ 194 ....................................................................... 199 / ............................................................................................. 204 ......................................................................................... 206 ....................................................................................................................... 207 .......................................................................... 207 ..................................................................................... 208 ............................................................................................... 209 .................................................................................... 211 .......................................................................................... 215 ........................................................................................................... 216 ......................................................................................................... 218 ..................................................................... 220 ............................................................................................................. 224 ...................................................................................................... 225 ..................................................................................................... 227 ................................................................................... 228 (SPME) ............................................................................... 230 (SPME) ................................................................................... 233 ................................................................................ 242 1177................................... 245 1177 .................................................................................... 246 ................................................................................... 246 1177 .................................................................................................... 24620



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1177................................................................................. 247 ................................................................................ 247 ................................................................................ 247 1177......................................................................................................... 249 EFC 1177 ................................ 250 1177 ............................................................................... 254 1177............................................................................................... 254 .......................................................................................................... 254 ....................................................................................... 254 1177 ....................................................... 255 EFC ..................................................................................... 255 ................................................................................. 256 ........................................................................................................... 257 .................................................................................................... 259 ................................................................................... 260 ................................................................................................... 262 ................................................................. 262 1177.......................................................................................................... 263 ................................................................................................ 263 ................................................................................................ 265 1177................................................................. 266 1177...................................................................................................... 267 ............................................................................................. 269 1079 PTV .................................................................................................................. 27321



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1079 PTV ......................................................... 275 ................................................................................... 275 1079 .................................................................................................... 276 1079...................................................................................................... 277 1079 PTV ................................................................................ 278 ........ 278 ..................................................................................... 278 ................................................................... 279 .............................................. 279 ................................................. 279 1079......................................................................................................... 281 EFC 1079 PTV......................... 283 1079 PTV........................................................................ 286 1177............................................................................................... 286 1079 PTV................................................ 287 ....................................................................................................... 290 ................................................................................... 291 ................................................................................................... 293 1079 PTV ............................................................................. 294 ................................................................ 294 ................................................................ 295 ........................ 295 ................................................................... 296 ....................................................................................... 29722



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1079 PTV ......................................................... 299 ............................................................................................. 300 ChromatoProbe .................................................................................................. 303 ChromatoProbe............................................................. 303 ChromatoProbe.................................................................. 307 ........................................................................ 308 ChromatoProbe / ................................................................................................................................. 310 ChromatoProbe ...................... 310 .............................................................................................................................. 312 ........................................................................................ 313 1041 ..................................... 314 ................................................................................... 316 1041 .................................................................................................... 316 .................................................................................. 317 EFC 1041 ................................ 318 EFC ......................................................................................... 321 1041............................................................................................... 324 1041......................................................................................... 325 ............................................................................................. 326 1061.............................................................. 330 ................................................................................... 332 .................................................................................. 333 EFC 1061 ................................ 334 1061 .................................................................................................... 33723



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1061 ....................................................... 338 EFC ......................................................................................... 338 1061 ................................... 341 1061 ............................. 342 ............................................................................................. 343 1093 (SPI) ......................................................... 346 ................................................................................... 349 .................................................................................. 350 1093..................................................................................... 350 EFC 1093 ................................ 352 ............................................................................................................. 355 2 1093.......................................................................... 356 (LN2) 1093 ............................................. 357 1093 ....................................................... 359 EFC ......................................................................................... 359 1093............................................................................................... 360 1093................................................................. 362 ................................................................................... 363 ............................................................................................. 365 (SPT) ................................ 371 .............................................................................................................................. 371 SPT.................................................................................................... 373 ........................................................................................... 375 ...................................................................................... 37524



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............................................................................................................ 377 ................................................................................ 377 ................................................................................. 377 .................................................................................................... 378 ................................................................................... 379 2 (LCO2) ............................................................................ 380 N2 (LN2)................................................................................... 384 SPT ............................................................................................. 388 SPT......................................................................................................... 390 ..................................................................................................... 391 SPT.................................................................................................. 392 ................................................................................................ 397 ............................................................................. 397 ................................................................................................. 398 .......................................................................................... 403 SPT........................................................................................................... 404 ......................................................................................................... 407 ................................................................................................................................. 410 ............................................................................................................................... 410 ............................................................................................................... 411 - () ..................................................................... 415 ............................................................................................. 417 .................................................................................................................................... 419 ..................... 42125



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/ ........................................................................................................ 423 ............................................................................................................ 423 ............................................................................................. 425 .................................................................................................. 426 ............................................................................................. 430 (PDHID)........................................ 432 (PDHID) ........................................................................................ 434 ....................................................................................................... 435 ................................................................................................................ 436 ........................................................................................................... 437 ................................................................................................ 438 ............................................................. 438 ......................................................... 440 .......................................................................... 440 ......................................................................... 441 ................................................................................................................. 442 ()............................................................... 444 ............................................................................................. 446 ....................................................... 447 ...................................................................................................... 455 ................................................................................................. 456 ............................................................................................. 459 () ................................................................................ 461 ............................................................................................. 46226



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.................................................................................................................. 465 ........................................................................................................................ 466 ................................................................................ 471 ................................................................. 472 - ........................................... 472 ............................................................................................. 472 ()............................................................................... 474 ............................................................................................. 476 ................................................................................................ 478 ................................................................................................ 482 / ........................................................................................................ 485 ................................................................................................................ 485 ............................................................................................. 490 - ()................................ 492 .............................................................................................................................. 492 .......................................................................................... 494 ............................................................... 497 .......................................................................................................... 497 ......................................................................................................... 504 ........................................................................................................................... 506 ................................................................................................................... 506 ................................. 508 .............................................................................................................................. 509 ............................................................... 51227



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.................................................................................................................... 520 EFC15............................................... 521 ............................................................................................. 527 ...................................................................................................... 530 - ........................................................................................... 535 ()................................................................ 539 ............................................................................ 544 : ................ 546 : ...... 547 .................................................................................................................. 547 : ............ 548 : . 550 Gate Delay Gate Width.............................................. 551 ............................. 551 .......................................................................................... 552 ......................................... 553 Gate Delay Gate Width .................................................. 555 ..................................................................................................... 559 .............................................................................................. 560 .............................................................................. 562 .................................................................................................................. 562 ........................................................................ 566 ................................................................................ 570 ......................................................................... 57028



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............................................................................ 571 ............................................................................... 573 ....................................................................... 574 ................................................................................. 576 ......................................................................................................... 583 .............................................................................. 588 ........................................................................................................... 589 ............................................................................................................ 590 ............................................................................................................ 591 ........................................................................................................... 592 , ........................................................................ 593 , .................................................................................. 594 ............................................................................. 595 ............................................................................................................................ 595 ......................................................................................................................... 597 ........................................................................................ 600 ........................................................................ 602 ................................................................................................................... 602 ....................... 604 ............................................. 607 .............................................. 607 ........................................................................................................... 608 , ................................................ 610 .................................................................................... 61029



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........................................................................................................ 610 ................................................................................................ 610 ....................................................................................................................... 611 / .......................................................................................... 614 ........................................................................................ 615 ................................................................................................................ 627 ............................................................ 628 !...................................................... 632 2500 ............................................................................................. 632 ................................................................................................. 633 .............................................................................................................................. 635 .................................................................................... 636 ............................................................... 637 ...................................................................................................................... 639 ................................................................................................ 639 ................................................................................................ 640 ................................................................................ 642 (PTV) ...................................... 643 . ................. 645 .................................................................................................................. 645 ............................................................................................................... 646 .............................................................................................. 646 .................................................................................. 647 ........................................................ 64830



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..................................................................... 650 ......................................................................................... 652 . .............................................................................................. 653 . ................................................................................ 680

31



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1: 2: 3: 4: 5: 6: 7: 8: 9: 10: 11: 12: 13: 14: 15: 16: 17: 18: 19: 20: 21: 22: 23: 24: 25: 26: 27: 28: 29: 30: 31: 32: 33: 34: 35: 36: 37: 38: J504-J505 J401 J302 J45/J46 J44 J42/J43 J41 Ethernet 450- - EFC21 1177 EFC21 1177 EFC25 1177 1177 1079 PTV EFC21 1079 EFC25 1079 ChromatoProbe 1041 EFC23 1041 EFC24 1041 1061 EFC23 1061 EFC24 1061 1093 EFC23 1093 EFC24 1093 2 SPT 232



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39: 40: 41: 42: 43: 44: 45: 46: 47: 48: 49: 50: 51: 52: 53: 54: 55: 56: 57: 58: 59: 60: 61: 62: 63: 64: 65:

N2 SPT ( , L2) (PDHID) PDHID PDHID PDHID , , , , , , , , S

33



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1: 2: 3: 4: 5: 6: 7: 8: 9: 10: 11: 12: 13: 14: 15: 16: 17: 18: 19: 20: 21: 22: 23: 24: 25: 26: 27: 28: 29: 30: 31: 32: 33: 34: 35: - 1/16 Varian EFC - Varian 1041 1061 1177 1079 EFC EFC / / 1/16 1177 1/16 1079 34



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36: 37: 38: 39: 40: 41: 42: 43: 44: 45: 46: 47: 48: 49: 50: 51: 52: 53: 54: 55: 56: 57: 58: 59: 60: 61: 62: 63: 64:

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35



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37



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03-92611945 SG092034 03-92543101 03-9261192749



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, . 1 / , 100 / , 100. 100 , , , 100 . 450- EFC VALVE TABLE ( ) (SAPLE DELIVERY) . , . EFC. 1177, 1079 PTV , .

1. FLOW/ PRESSURE (/ ) . 2. INJECTOR () 1177 1079 PTV . 3. EFC , . 4. (ON) 100. 5. COLUMN OVEN ( ). , Turn Oven Power Off ( ). 6. , . , , , 3-5 / . , EFC, .

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SETUP ().

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1.9-1

3,9 9,5 9,7 10,5 11,4 2:

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1.9-1

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1.9-1

Varian Varian. . , , .

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1.9-1

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30 60 360 30 34 209 2 15 32 42 11:

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INJECTOR () , 0 250 . 1177 1079 PTV, , , . , 100 . COLUMN OVEN ( ) 2500. DETECTOR () 300 0. , , 1000 ( 287), , . .

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77



450

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Varian Varian ( ) ( ) 82-005048-01 82-005048-02 82-005048-03 82-005048-04 82-005048-07 82-005048-00 3,00 / 14, 15 16 33,0 / 20,0 / -, , ; 4000 / - 2,00 / , ; 4,00 / 4,00 / 17 30 / 14, 15 16 3 / 14, 15 16

12: Varian : . ma. . 1041 1061 80 1 20 200 5 190 15 80 1 20 200 5 140 15 80 1 20 200 5 140 15

( ) () 0 ( / ) 0 ( ) () 0 ( ) ( ) () ( ) 0 ( ) 0 ( ) ()

0

80 1 20 200 5 175 15

80 1 20 200 5 175 15

220 300 1 On ()

220 300 12 On ()

220 220 0,05 On ()

220 300 12 On () 3,0 0,3

220 b 300 10 On ()

13: 1041 1061 Varian _______________________78



450

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- 20 1 / . b : S 2000, 3000, N 250 0. : 10, Varian.

79



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1177 1079 80 1 20 200 5 220 300 1 On () 80 1 20 200 5 220 300 12 On () 80 1 20 200 5 220 220 0,05 On ()

( ) () 0 ( / ) ( 1) 0 ( ) ( 1) () ( 1) 0 ( ) 0 ( ) () 1 () 1 1 () 1 2

0

80 1 20 200 5

80 1 20 200 5 220 b 300 10 On ()

220 300 12 On () 3,0 0,3 ON () 0,01 OFF () 1,00 ON () 20

14: 1177 1079 Varian _______________________ - 20 1 / . b : S 2000, 3000, N 250 0.

. , , , -8400, 121. . Varian 1:30, . , , . , .80



450

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81



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, . 100% 5% , 95% - -- 50% , 50% - -2 36,1 69,0 80,7 99,3 80,1 110,6 34,6 55,2 39,8 61,2 46,5 77,0 56,5 127,0 81,6 64,7 78,5 82,5 (0)

82



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117,7

15:

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2

3

4

5

6

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1 2 3

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1 ( 8 , 10 , F3)

2 ( 8 , 10 , F3)

3( 8 , 10 , F3)

4 ( 8 , 10 , F3)

5 ( 8 , 10 , F3)

6 ( 8 , 10 , F3)

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24 DC -8 24 DC -9 24 DC -10

24 DC( 1 , )

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24 DC -12 24 DC -13 24 DC -14

24 DC( 1 , )

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Creating () Initialization () Not Ready ( ) Stabilizing () Monitor () PreRun ( ) Sample Prep ( ) Ready () Run ( ) Run/ Not Ready ( /

OFF ()

OFF ()

OFF () OFF ()

ON () OFF ()

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ON ()

OFF ()

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10 11 12 13 14 15 16

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1 2 3 4 5 6 7 8 9 10 11 12 13 14

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Varian GC450 User Manual Russian