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POSIVA OY Working Report-97-34e Ultrasonic inspection of electron beam welded joints in copper Harri Jeskanen Pentti Kauppinen VTT Manufacturing Technology Materials and Structural Integrity August 1997 Mi konkatu 15 A, FIN-001 00 HELSINKI, FINLAND Tel. +358-9-2280 30 Fax +358-9-2280 3719

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POSIVA OY

Working Report-97-34e

Ultrasonic inspection of electron beam

welded joints in copper

Harri Jeskanen

Pentti Kauppinen

VTT Manufacturing Technology

Materials and Structural Integrity

August 1997

M i konkatu 15 A , FIN-001 00 HELSINKI, FINLAND

Tel. +358-9-2280 30

Fax +358-9-2280 3719

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Working Report-97-34e

Ultrasonic inspection of electron beam

welded joints in copper

Harri ..Jeskanen

Pentti Kauppinen

VTT Manufacturing Technology

Materials and Structural Integrity

August 1997

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m MANUFACTURING TECHNOLOGY

A Work report B Public report

C Confidential report x Title of report

Ultrasonic inspection of electron beam welded joints in copper Client/sponsor of project and order

Outokumpu Poricopper Project

Kuparikapselin EB-hitsisauman ultraaanitarkastus Author(s)

Harri Jeskanen, Pentti Kauppinen Keywords

EB-weld, ultrasonic testing, inspection of copper Summary

Report No.

VALC-340 Project No.

V6SU00583 No. of pages/appendices

27 +8 appendices

The copper canisters used for the high active waste disposal are closed by electron beam welding (EB weld­ing) and the integrity of the weld is inspected by using ultrasonic techniques. The main difficulties in the ultra­sonic inspection of copper are the attenuation of the ultrasonic energy due to the large grain size and the ultra­sonic noise caused by the weld. For reliable results the technique used has to be optimized and special care must be taken in the selection of ultrasonic transducers.

In this study the ultrasonic inspection techniques for inspection of EB-welds in copper canisters were devel­oped. In the experimental work both simplified test specimen and a full scale weld specimen were used. The results verify the importance of selection of transducers when small discontinuities are to be detected in mate­rial strongly attenuating ultrasonic waves. For the inspection focussed normal incidence probes and focused angle beam probes are recommended. The focal areas of the probes should cover the complete wall thickness. Based on the experimental results it can be estimated that in EB-weld planar structural discontinuities having diameter larger than 5 mm and locating perpendicular to the sound beam can be reliably detected. With the normal incidence probe the root defects in the weld can be revealed and based on these the depth of weld penetration can be assessed.

Date Espoo _ 21.8.1997

\n_ \(___ c Rauno Rintamaa Research Manager Distribution:

Client, 3 copies

Cf~' it' ' PenttiK~n Project Manager

VTT Manufacturing TechnologyN AL6, 3 copies Authors, 2 copies

VTT Manufacturing Technology Materials and Structural Integrity P.O. Box 1704 FIN -02044 VTT, Finland

Phone: Telefax: E-mail: WWW:

~~ ?w-Checked

+358 9 4561 +358 9 456 7002, +358 9 456 5875 Pentti.Kauppinen @vtt.fi http://www.vtt.fi/manu/

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Working Reports contain information on work in progress

or pending completion.

The conclusions and viewpoints presented in the report

are those of author(s) and do not necessarily coincide

with those of Posiva.

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Contents

Tiivistelma 3

Abstract 4

1. Introduction 5

2. Test programme and the specimens 5

3. Sun1ffiary of literature survey 6

4. Experimental ultrasonic techniques 6 4.1. Mode conversion technique

4.1.1 Creeping wave on the scanning surface 6 4.1.2 Creeping wave on the surface opposite to 7

scanning surface 4.2. Shear wave probes 8

4.2.1 Tandem-technique 8 4.3. Longitudinal wave probes 8

5. Results of experimental measurements 8 5.1. Inspection of welds

5.1.1. Normal incidence probe Panametrics V104 10 5.1.2 Scanning with angle beam probe 10

RTD70°TRL2-Cu 15x22)SA15°FD 5.1.3 Scanning with angle beam probe 11

RTD60°TRL2 Cu2(15x22) SA3°FD 5.2 Reference defects

5.2.1. The normal incidence probe Panametrics V 104

5.2.2 Scanning with angle beam probe RTD70°TRL2-Cu2(15x21)SA15°FD

5.2.3 Scanning with angle beam probe RTD60°TRL2-Cu2(15x22)SA3°FD

5.3. Inspection of the full scale weld sample

11

12

13

14

6. Summary and conclusions 15

7. References 17

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Tiivistelma

Y dinpolttoaineen loppusijoitukseen kaytettavat kuparikapselit suljetaan

elektronisuihkuhitsauksella (EB) ja liitoksen eheys varmistetaan ultraaanitestauksella.

Kuparin ultraaanitarkastusta vaikeuttaa materiaalin suuri raekoko ja hitsin

ultraaanisignaaliin aiheuttama kohina. Luotettavan tarkastustuloksen saavuttamiseksi

tarkastustekniikka on optimoitava ja erityisesti on kiinnitettava huomiota kaytettavien

ultraaaniantureiden valintaan.

Tassa tutkimuksessa kehitettiin EB-hitsin tarkastustekniikkaa kaytUien seka

yksinkertaistettuja koekappaleita etta halkaisijaltaan taysimittaista kuparikapselia.

Koetulokset osoittavat anturien valinnan tarkeyden pyrittaessa havaitsemaan

luotettavasti pienia epajatkuvuuskohtia voimakkaasti ultraaanta vaimentavassa

materiaalissa. Tarkastukseen suositellaan kaytettavan seka fokusoituja

normaaliluotaimia etta fokusoituja kulmaluotaimia, joilla katetaan koko tutkittava

paksuusalue. Koetulosten perusteella EB-hitsista havaitaan halkaisijaltaan 5 mm

ylittavat tasomaiset heijastajat, jotka sijaitsevat kohtisuorassa aanikeilaa vastaan.

N ormaaliluotaimella havaitaan hitsin juuriviat, joiden perusteella voidaan arvioida my os

hitsin tunkeuman syvyytta.

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Abstract

The copper canisters used for the high active waste disposal are closed by electron beam

welding (EB welding) and the integrity of the weld is inspected by using ultrasonic

techniques. The main difficulties in the ultrasonic inspection of copper are the

attenuation of the ultrasonic energy due to the large grain size and the ultrasonic noise

caused by the weld. For reliable results the technique used has to be optimized and

special care must be taken in the selection of ultrasonic transducers.

In this study the ultrasonic inspection techniques for inspection of EB-welds in copper

canisters were developed. In the experimental work both simplified test specimen and a

full scale weld specimen were used. The results verify the importance of selection of

transducers when small discontinuities are to be detected in material strongly attenuating

ultrasonic waves. For the inspection focussed normal incidence probes and focused

angle beam probes are recommended. The focal areas of the probes should cover the

complete wall thickness. Based on the experimental results it can be estimated that in

EB-weld planar structural discontinuities having diameter larger than 5 mm and

locating perpendicular to the sound beam can be reliably detected. With the normal

incidence probe the root defects in the weld can be revealed and based on these the

depth of weld penetration can be assessed.

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1. Introduction

Copper canisters will be used for the high active waste disposal of the Finnish nuclear

power plants. The filled canisters are closed by welding a copper lid to the canister. For

welding a narrow gap welding technique, electron beam (EB) welding has been

proposed. The joint between the canister and the lid has to be inspected after welding in

order to be sure that no significant defects are existing in the weld. There ate two

possible inspection techniques for the welds in thick copper plates: ultrasonic

inspection and radiography /11. The ultrasonic testing of copper is more difficult than

the conventional testing of steel and similarily to steel the weld joints are making the

inspection even more difficult.

The ain1 of the present work was to study the applicability of ultrasonic techniques for

inspection of EB-welds in copper canisters. The practical measurements were performed

with several specimen simulating the real weld geometry in the copper canister. The first

simplified specimen containing artificial reflectors were used to test different ultrasonic

techniques and to optimize the transducers used in later experiments. The final tests

were performed with a specimen representing in full size the EB-weld between the lid

and canister. The results of the experimental measurements and the conclusions from

the work performed are presented in this report.

2. Test programme and the specimens

The ultrasonic measurements were performed using three different test specimens. The

first specimen was a hot rolled copper plate containing an EB-weld. The specimen is

shown in appendix 1.

The other two specimens are shown in appendix 4. The weld geometry simulates the

geometry of real copper canister but the specimen is not curved as the real canister

surface.

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3. Summary of literature survey

A literature survey was performed in order to find usefull hints for practical

measurements. The result of the survey was, however, that only very limited amount of

data has been published about ultrasonic inspection of welds in thick copper products.

The most use full information was given in the report "A study of attenuation and

scattering of ultrasound in polycrystalline copper" published by Swedish Nuclear

Power Inspectorate (SKI) in Sweden /2/. This report summarizes the major difficulties

1net when inspecting copper material. Based on the report one of the main difficulties,

the grain size, is caused by the fact that it is difficult to achieve fine grain sizes in thick

copper forgings. The structure of a rolled thick plate is a mixture of many fine grains

and relatively few coarse or very coarse grains. The recrystallised structures of hot rolled

plate are heavily twinned and these twins can be very effective reflectors of ultrasound.

If suitably oriented the twins in large grains may increase the noise to the ultrasonic

signal.

4. Experimental ultrasonic techniques

4.1 Mode conversion technique

4.1.1 Creeping wave on the scanning surface

The creeping wave propagating along the scanning surface can be used for detection of

surface opening defects and the simultaneously created direct longitudinal wave having

large angle of incidence for detection of defects just below the surface (figure 1).

In the experimental measurements both single crystal and twin crystal probes were used.

The twin crystal probe focused at the depth of 10 mm below the surface and having

separate crystals for transmitting and receiving ultrasonic pulses (SE probe) proved to be

more effective than the single crystal probe.

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Direct longitudinal ~ • .. ":..J.---1'---t-----1---/

30-70-70-wave (K1) ............ . ... >...... I

................... , I

..... 30-70-70-30-wave (~:i Direct shear wave

Creeping wave ID

Figure 1. The principle of mode conversion. The creeping wave propagating along the

surface and the direct longitudinal wave can be used for detection of surface opening

defects and defects close to the scanning surface.

4.1.2 Creeping wave on the surface opposite to scanning surface

The creeping wave propagating along the surface opposite to scanning surface can be

used for detection of incomplete weld penetration. The application of this technique is

restricted only to the base metal of the hotrolled plate because from the interface

between the weld and base metal a metallurgical indication will be recorded due to the

large grain size in the weld material. Furthermore, the large grain size causes strong

attenuation of ultrasonic waves especially in the case of shear wave probes.

The mode conversion 30-70-70 (26-70-70) can be used for rough estimation of flaw

size. If the incident angle of shear wave is 26° the angle for longitudinal wave is 70°.

4.2 Shear wave probes

Due to the strong attenuation of shear waves in the base metal the use of shear wave

probes is impossible in practise. From the different shear wave probes experimentally

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tested the best results were achieved with a composite probe. When measuring the

reference holes in the weld of specimen 1 the signal-to-noise (SIN) ratio was 3-5 dB

with the 2 MHz probe (SWB702).

The use of large incident angles on a perspex-copper interface is for physical reasons not

possible. If large incident angles are necessary the inspection must be performed in . . Immersion.

4.2.1 Tandem-technique

In principle, the tandem-technique would be optimal for detection of planar defects in

the current weld geometry. However, the use of this technique is restricted by the strong

attenuation of shear waves.

4.3 Longitudinal wave probes

In the ultrasonic inspection of copper the longitudinal wave probes are clearly most

effective. The attenuation of longitudinal waves in copper is remarkably lower than the

attenuation of shear waves having same nominal frequency. With shear waves low

frequencies have to be used to overcome the problems caused by attenuation.

5. Results of experimental measurements

In the measurements the automatic ultrasonic inspection system Sumiad Ill has been

used. The logarithmic amplifier used in the measurements allows the measurement of

echo amplitudes having differences up to 80 dB. In the record sheet V65-6353-1

attached in appendix 8 the principle of inspection and the scanning parameters are

presented.

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The defect types detected are root defects in the weld, incomplete penetration and

"craters" on the outside surface. These craters are both surface opening and close to the

surface. In addition, bonding defects (incomplete fusion, lack of fusion) can be expected

when the position of EB-beam is not precisely in the centre of the weld groove.

Specimen 1 was inspected with several shear and longitudinal wave probes that are

normally used for inspection of steel. Based on the results of these measurements the

technique described below was specified and the probes were optimized to inspection of

copper.

The scanning with normal incidence probe is made from the forged side of the specimen

as shown in figure 9. The grain size in the weld and forged base metal limits the

frequency of probe that can be used. In order to have optin1al resolution the diameter of

the sound beam in the weld area should be as small as possible. The probe used in these

measurements was not quite optimal. Defects close to the surface or opening to the

surface are not detected in scanning with normal probe due to the deflection of the

sound beam.

When the scanning is performed from the hot rolled side of the specimen the defects

close to surface or opening to the surface can be detected with creeping wave probe

emitting also longitudinal waves (figure 10).

Both plates I-32 and I-20 have been tested first before cutting the specimen in two

pieces as shown in appendix 4. The reference reflectors machined in the specimen are

shown in appendices 2 and 3.

The cut specimen I-32-1 and I-32-2 have been inspected with acoustic microscope

before machining the reference reflectors. In this inspection a focussed 5 MHz probe

having crystal diameter of 2 inches has been used. The scanning was performed in

immersion from the surfaces shown in appendix 4. The resolution of inspection

performed in immersion is essentially higher due to the higher frequency used and the

shorter sound path in copper. The result of this inspection can be seen in figure 8.

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5.1 Inspection of welds

5 .1.1 Normal incidence probe Panametrics V 104

Figures 2 and 3 show the results of inspection of the welds in specimens I-20 and I-32.

The welding defects in the root area can be clearly seen in the images. It can be also

noticed that that the weld penetration is increasing in the direction of welding.

In specimen I-32 the noise level of the weld is higher (both images are measured at same

level). The difference in noise level is caused by different welding parameters; in this

case the lower voltage used in welding has increased the width of weld.

Results of inspections:

In specimen I-32 the SIN-ratio in weld area is 3-13 dB compared to a 0 3

mm cylindrical hole.

In specimen I-20 the SIN-ratio in weld area is 6-18 dB compared to a 0 3

mm cylindrical hole.

Welding defects were not detected in these specimens .

The weld penetration in specimen I-32 was 46-51 mm and in specimen I-20 46-55 mm.

The depth of weld penetration has been measured by dropping the echo amplitude from

the root defect to 50 o/o from its maximum value.

5.1.2 Scanning with angle beam probe RTD70°TRL2-Cu (15x22)SA15°FD-10

In the inspections performed from the hot rolled sides of the specimens primarily

surface opening defects were detected. The defects were short in X -direction and

therefore the maximum shift of the focussed probe between scannings in X -direction is

3 rrun. The surface contour was not optimal to the relatively large probe. The surface

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quality is an important factor affecting the reliability of inspection and has therefore to

be taken into account in future measurements. Both the surface roughness and the

possible waviness of the surface should be as low as possible to avoid disturbances in

the acoustical coupling between the probe and the material. The requirement for surface

roughness is Ra < 6,3 J.lm. The acceptable waviness is depending on the length of the

contact surface of the probe used in the inspection. In practise unacceptable waviness is

caused by grinding the surface manually.

The figures 4 and 5 show the results of specimens I-20 and I-32.

5.1.3 Scanning with angle beam probe RTD60°TRL2-Cu2(15x22) SA3°FD-40

With the 60° angle beam probe the planar defects can' t be detected. The probe that is

focused at the depth of 40 mm is used for inspection of defects in the weld root area and

to measure the depth of weld penetration.

Figures 6 and 7 show the results of measurement of plates I-20 and I-32 with the 60°

probe.

5.2 Reference defects

5.2.1 The normal incidence probe Panametrics V104, 2.25 MHz, 0 l "

The plate I-32-1 has been tested with the normal probe from the forged side of the joint

as shown in the figure 9. The cylindrical holes both in the front of weld and behind the

weld are clearly detected. The SIN-ratio in the weld area is 7-18 dB compared to the

cylindrical holes.

Most of the flat bottom holes are also detected. The lowest SIN-ratio is 3dB below the

maximum noise when compared to the maximum noise level of the weld. This means in

practise that defects possibly existing in the area of maximum noise level in the weld

would not be detected.

For reliable detection of a flaw the echo amplitude measured from the flaw should

exceed the maximum noise level by at least 6 dB. In the weld of specimen 1-32-1 the

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echo amplitude measured from the flat bottom holes is 2 - 5 dB higher than the

maximum noise level of the weld. From the formula d2 =(HI I H2) d1, where di = 3mm

and the ratio between the heights of echos HI and H2 is (HI I H2 ) = 1.1 - 1.6, the

minimum diameter of the detectable flat bottom hole is d2 = 3.3 - 4.8 mm. On the base

metal side of the joint the minimum diameter of detectable flat bottom hole is 3 mm.

The SIN -ratio of this hole is more than 6 dB both in front of the weld and behind the

weld. The flat bottom holes locating close to the surface are not detected due to the

deflection of the sound beam and due to the adverse effect of the edge of the specimen.

Table 1. Plate 1-32-1; scanning with normal incident probe. The echo amplitudes

measured froJn reference holes shown in figure 9 have been compared to the echo

amplitude from the cylindrical hole C (depth 55 mm, diameter 0 3 mm)

Cylindrical Echo Flat Echo Flat Echo Noise from

hole amplitude bottom amplitude bottom amplitude the weld dB

dB hole dB hole dB

A -1 E2 -12 T2 -10 -7- -18

B -1 E3 -10 T3 -9

c 0 E4 -9 T4 -10

D 0 ES -9

5.2.2 Scanning with angle beam probe RTD70°TRL2-Cu2(15x21)SA15°FD-10

Noise

from

the

base

metal

dB

-16--

20

The specimen I-32-2 was tested with a longitudinal wave angle beam probe as shown in

figure 10. The probe was focused approximately at the depth of 10 mm and thus it can

be used for detection of surface opening defects by the creeping wave component. In

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addition the longitudinal wave component can be used for detection of defects to the

depth 15 mm below the surface.

As presented in table 2 the 03 mm flat bottom hole is detected with SIN-ratio of 2 -9

dB. Correspondingly the cylindrical holes are detected with SIN-ratio of 13 - 23 dB. The

attenuation of ultrasonic in the weld is not remarkable (compared with measurements

performed with cylindrical holes). The difference between results measured in front and

behind the weld is probably mainly caused by differencies in the acoustic coupling of

the probe.

Table 2 Plate 1-32-2; angle beam probe 70 ° SEL. The echo amplitudes of reference

holes shown in figure 10 compared to the echo amplitude from the cylindrical hole A15

(on the base metal side of the joint, distance to surface 15 mm, 0 3 mm)

Cylindrical Echo Flat Echo Notch Echo Noise from Noise from

hole amplitude bottom amplitude depth mm amplitude the weld the base

dB hole dB dB dB metal dB

AS -2 El -17 Ul -19 -23- -30 -30- -33

AlS 0 E2 -17 U2 -16

BS -10 Kl -14

BlS -2 K2 -21

The noise caused by the weld has been measured at the depth of 0 -15 mm and the noise

from the base metal on the hot rolled side of the joint.

5.2.3 Scanning with angle beam probe RTD60°TRL2-Cu2(15x22)SA3°FD-40

The specimen I-32-2 was tested with the 60° longitudinal wave probe as shown in figure

10. The probe is focussed at the depth of 40 mm as can be seen from the results shown

in table 3. As expected planar defects are not detected with this probe. The noise from

the weld is not remarkable. This indicates that the grain structure of the weld has certain

orientation (compare the results with oo and 70°probes).

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Table 3 Plate I-32-2; Angle beam probe 60° SEL. The markings of cylindrical holes

refer to figure 10. The number in the identification shows the depth location of the

cylindrical hole.

Cylindrical Echo amplitude Cylindrical Echo amplitude Noise from the Noise from the

hole dB hole dB weld dB base metal dB

identification

AS -15 B5 -21 - -25 -21 - -25

A15 -6 B15 -10

A25 -2 B25 -6

A35 -1 B35 -5

A45 0 B45 -4

5.3 Inspection of the full scale weld sample

The ultrasonic inspection of the full scale specimen was performed 25.-26.4.1997 in the

facilities of Outokumpu Poricopper Oy in Pori. The test arrangement is shown in the

photographs. The testing was performed by using the technique and transducers

described in 5 .1. In the position where welding process has been started and stopped a

defect having a length of approximatelly 250 mm was detected. It was assessed that

this defect is formed by several individual small defects. The defect is starting from the

inside surface and is propagating gradually to the outside surface thus extending as a

"cloud" through the whole wallthickness. In addition, several defects (crater type) were

detected in areas close to the surface and even at some depth inside the material. The

results of ultrasonic testing with different transducers are shown in figures 11 -16. From

the scannings performed with angle beam probes only the results from scannings on the

side of the hot -rolled plate are presented.

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6. Summary and conclusions

This report describes possible techniques to solve the inspection problem of the EB­

welded copper canister. It is, however, possible that even more suitable techniques could

be developed. The most serious problem in the ultrasonic inspection of the EB-weld in

copper is the strong attenuation of ultrasonic waves in the weld material. The

attenuation is also increased due to the large grain size of the base metal. One solution

to overcome this type of problem would be to use signal processing techniques.

However, the use of e.g. SAFf -algorithm to process the complete measurement data is

not yet possible with current computers. Nevertheless, the main problem is to transmit

sufficient ultrasonic energy into the material and this can be only solved by using a

probe having large piezoelectric crystal.

Also the "kissing bond" -effect where the surfaces are in close contact but there is not

real bonding between the surfaces can cause remarkable problems in inspection.

Only when the problems described here are solved (or the adverse effects minimized)

the reliability of inspection and the minimum size of the detectable defect can approach

the level that is normally achieved in the ultrasonic inspection of steel. There are a few

methods to minimize the adverse effects of weld in inspection:

The ultrasonic noise caused by the weld is decreased when the angle

between the ultrasonic beam and the weld/base metal interface is larger

than 0°.

The transducer used can still be optimized. The normal incidence probe

has to be focussed and the applicability of a twin-crystal transmitter­

receiver (SE) probe should be tested. With the technique used in this

study the volumetric defects are reliably detected but the technique for

detection of planar defects needs improvement.

The normal incidence probe can be improved by following means:

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A transmitter-receiver probe with nominal frequency 2.25 MHz will be

constructed. The piezoelectric element of this probe is formed from

composite crystals having such diameter that the focus of the probe is in

the depth zone to be studied. The angle between the crystals and the

normal of the surface is 10 - 20°. With this type of transducer the noise

caused by the weld will most probably be reduced and smaller defects

could be detected.

Scanning could be performed with several angle beam probes being

focussed at different depths to cover the whole wallthickness.

With the technique described above the planar reflectors having diameter

more than 5 mm and corresponding to a flat bottom hole can be detected

in the EB-weld when the reflectors are located perpendicularly to the

incident bemn (material as in sample I-32/I-20 and grain size 120 J.lm or

less). If the grain size is larger the size of the defect that can be detected is

also remarkably growing.

In the scanning of the full scale specimen performed with normal incidence probes not

even the large craters detected by angle beam probes could be reliably seen. Based on

this it could be assessed that the craters are formed from several smaller reflectors

having diameters less than 5 mm.

The root defects in the weld can be clearly detected with normal incidence probe in the

weld of the full scale specimen. The depth of weld penetration can be evaluated from

the root defect. Also the possible defects caused by wrong positioning of the electron

beam in welding can be detected either as a change of echo amplitude (in the case of a

large reflector) or as a shift of noise area in the cross sectional image (D-scan image). In

angle beam scanning the craters are detected at different depths due to their 3-

dimensional nature.

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7. References

/1/ Aalto, H., Rajainmaki, H., Laakso, L. 1996. Production methods and costs of

oxygen free copper canister for nuclear waste disposal. Report Posiva 96-08, Posiva Oy,

Helsinki.

/2/ Bowyer, W.H. and Crocker, R.L. 1996. A study of attenuation and scattering of

ultrasound in polycrystallinen copper. SKI Report 96:27. Swedish Nuclear Power

Inspectorate, Stockholm. 93 p.

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18

Figure 2 The joint 1-20 has been inspected by scanning with a normal incidence probe (0°)from the forged side of the joint. Welding directionfrom right to left. Weld penetration 45-65 mm. No remarkable welding defects except root defect in the weld can be seen in the images.

Figure 3 The joint 1-32 has been inspected by scanning with a normal incidence probe (0°)from the forged side of the joint. Welding direction from right to left. Weld penetration 46-51 mm. The noise coming from the weld is higher than in figure 2 due to the fact that the width of the weld is larger.

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19

Figure 4 The echo amplitudes of indications detected in joint /-20 are -17- -21 dB when compared to the echo from a diameter 3 mm cylindrical hole at the depth of 10 mm. The scanning of joint has been peiformed from the side of the hotrolled plate with a 70 <YJ'RL-Cu transducer.

Figure 5 The echo amplitudes of indications detected in joint /-32 are -19- -22 dB compared to the echo from a diameter 3 mm cylindrical hole at the depth of 10 mm. The scanning of joint has been peiformed from the side of the hotrolled plate with a 70 <YJ'RL-Cu transducer.

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20

Figure 6 The scanning of joint 1-20 has been performed with a 60° angle probe from the side of the hotrolled plate. The blow-outs in the root area are clearly seen in the image. The weld penetration seems to be approximatelly 40 mm. This value is probably not correct because the focus sing of the probe to 40 mm causes a shift upwards in the location of the indication.

Figure 7 The scanning of joint 1-32 has been performed with a 60° angle beam probe from the side of the hotrolled plate.

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21

Figure 8 Plates 1-32-1 and 1-32-2 were measured also by using a C-mode scanning acoustic microscope. In the upper image a typical "crater" on the surface can be seen. The width of this crater is 3 mm and height 10 mm. The same defect has been detected also in the inspection performed with a 70 o angle probe (figure 5 ).

The scanning of plate 1-32-1 has been performed from the side of the hotrolled plate (grain size 0.120 mm) and scanning of plate I-32-2from the forged side (grain size 0.500 ... 1.500 mm). The increase of grain size clearly causes the increase of the smallest detectable defect size. The scanning directions are presented in appendix 4.

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FBHcp3mm SDHcp3mm Width of the notch - 1 mm

22

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Figure 9 The ultrasonic image of joint 1-32-1. The inspection has been performed with a normal incidence probe. The upper image is the A -scan (time-amplitude) presentation, in the middle the C-scan image (top-view) and the lowest is the D-scan image (side­view). The surfaces used in scanning and scanning directions are shown in the drawing below the images. This drawing is not presenting the sample according to the projection rules of technical drawings. The refelectors shown in red colour in the drawing have been detected in ultrasonic testing and corresponding indications are marked in the images. On the side of the base metal the smallest detectable reflector is a flat bottom hole having the diameter of 3 mm. In the weld area the smallest detectable defect is flat bottom hole having diameter of 5 mm due to the strong noise caused by the weld. The uppermost (El and Tl) holes are not detected due to the adverse effect of the edge of sample and the deflection of the sound beam.

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23

Figure 10 The ultrasonic image of joint /-32-2 inspected with a 70° angle beam probe focus sed at the depth of 10 mm. The direction of scanning is shown in the drawing below the images. The drawing presents the sample in the same way as drawing 9. The reflectors shown in red colour in the drawing have been detected in ultrasonic testing and corresponding indications are marked in the images. Marking "D" is used for welding defects. The acoustical noise from the weld is lower than with normal probe (figure 9 ). The variation of echo amplitudes is mainly caused by differencies in acoustic coupling. The smallest detectable defect with the 70° angle beam probe is less than 0 5 mm in the weld area.

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24

Figure 11. The ultrasonic image of the weld in the full scale specimen. Measurement with normal incidence probe. In the position X=3000 mm, Z=57 mm a 3 mm cylindrical hole is located. The start point of welding is at X-coordinate 276 mm the length of starting area is 102 mm. The slope out area (ending area) is at 378-642 mm. The weld penetration is 50-58 mm.

Figure 12. Magnified image from the defect seen in figure 11 at the end point of welding.

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25

Figure 13. Ultrasonic image measured with a 70°SEL-probe in X-position 0-1531 mm. The defect at the end point of welding is in position X=520- 606 mm. Also crater type defects can be seen in the image.

Figure 14. Ultrasonic image measured with a 70°SEL-probe in X-position 1531 - 3100 mm. The defects seen in the image are craters from which most are opening to the surface.

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26

Figure 15. Ultrasonic image measured with a 60°SEL-probe in X-position 0-1531 mm. The defect at the end point of welding is in position X=410- 600 mm. Also crater type defects and the longitudinal weld of the cylinder (in position X=1200 mm) are seen in the image.

Figure 16. Ultrasonic image measured with a 60°SEL-probe in X-position 1531 - 3100 mm .. Crater type defects and the longitudinal weld of the cylinder (in position X=2750 mm) are seen in the image.

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Appendices

Appendix 1, Plate 1

Appendix 2, Plate I 32-1

Appendix 3, Plate I 32-2

27

Appendix 4, Plate I 32 (similar to I 20)

Appendix 5, Full scale sample

Appendix 6, Macro graphs of specimen I 20

Appendix 7, Fotographs showing the testing arrangement

Appendix 8, Data sheet V 65-6353-1 Examination summary

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APPENDIX 6

Grain size 120 lJ,m Grain size 500-1500 lJ,m

I Hot rolled EB-weld Forged

Hot rolled Weld Forged

Macro graphs showing the grain structure of sample 120 ( x 2 0)

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APPENDIX 7

The arrangement used in ultrasonic testing of the full sca]e smnp1e.

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APPENDIX 8

iiTT . ~

TESTAUKSEN YHTEENVETO V65-6353-1

VALMISTUSTEKNIIKKA Examination summary Sivu/Sheet

Manufacturing Technology 1 (1) T ilaaja/Co n tractor Testausohje/P rocedure

Outokumpu Copper -I UT -laitteisto/equipment

Sumiad Ill v.3.34 Testauspaikka/Test carried out at Testauskohde/Test item

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