Table of Contentslib3.dss.go.th/fulltext/E_content/0003-2700/2012v84n14.pdf · Michael C. Thomas, Simon R. Dunn, Jens Altvater, Sophie G. Dove, and Geoffrey W. Nette pp 5976–5983

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July 17, 2012Volume 84, Issue 14Pages 5833-6276

EDITORIAL LETTERS TO ANALYTICAL CHEMISTRY

ARTICLES

In this issue:

About the Cover: The cover image depicts the active pharmaceutical ingredient (API) within a final dosagby ultraviolet-second order nonlinear optical imaging of chiral crystals (UV-SONICC) andUV fluorescence (TPE-UVF). The incident laser light (green) is shown coming from aboveinteracting with the sample. Chiral crystals, in the presence of intense optical electromfrequency-doubling of the incident light and multi-photon absorption, resulting in the pviolet/blue light to enable selective API localization. Image created by Alyssa P. Cumbearticle.

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EDITORIAL

Metabolomics in Analytical ChemistryJonathan V. Sweedler

pp 5833–5833Publication Date (Web): June 25, 2012 (Editorial)DOI: 10.1021/ac301554c

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LETTERS TO ANALYTICAL CHEMISTRY

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Anal. Chem.

Page 1 of 14Analytical Chemistry: Volume 84, Issue 14 (ACS Publications)

17/7/2555http://pubs.acs.org/toc/ancham/current

Section: Immunochemistry

Homogeneous Assay for Detection of Active Epstein-Barr Nuclear Antigen 1 by Thrombin Activity ModulationGaizka Garai-Ibabe, Ruta Grinyte, Allon Canaan, and Valeri Pavlov

pp 5834–5837Publication Date (Web): June 19, 2012 (Letter)DOI: 10.1021/ac301250f

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TECHNICAL NOTES

Assessment of Compatibility between Extraction Methods for NMR- and LC/MS-Based MetabolomicsAntoni Beltran, Manuel Suarez, Miguel A. Rodríguez, Maria Vinaixa, Sara Samino, Lluís Arola, Xavier Correig, and Oscar Yanes

pp 5838–5844Publication Date (Web): June 14, 2012 (Technical Note)DOI: 10.1021/ac3005567

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QuaMeter: Multivendor Performance Metrics for LC–MS/MS Proteomics InstrumentationZe-Qiang Ma, Kenneth O. Polzin, Surendra Dasari, Matthew C. Chambers, Birgit Schilling, Bradford W. Gibson, Bao Q. Tran, Lorenzo Vega-Montoto, Daniel C. Liebler, and David L. Tabb

pp 5845–5850Publication Date (Web): June 13, 2012 (Technical Note)DOI: 10.1021/ac300629p

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Triple Quad ICPMS (ICPQQQ) as a New Tool for Absolute Quantitative Proteomics and PhosphoproteomicsSilvia Diez Fernández, Naoki Sugishama, Jorge Ruiz Encinar, and Alfredo Sanz-Medel

pp 5851–5857Publication Date (Web): June 18, 2012 (Technical Note)DOI: 10.1021/ac3009516

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Bacterial RNA Extraction and Purification from Whole Human Blood Using IsotachophoresisAnita Rogacs, Yatian Qu, and Juan G. Santiago

pp 5858–5863Publication Date (Web): June 29, 2012 (Technical Note)DOI: 10.1021/ac301021d

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Building Blocks for the Development of an Interface for High-Throughput Thin Layer Chromatography/Ambient Mass Spectrometric Analysis: A Green MethodologySy-Chyi Cheng, Min-Zong Huang, Li-Chieh Wu, Chih-Chiang Chou, Chu-Nian Cheng, Siou-Sian Jhang, and Jentaie Shiea

pp 5864–5868Publication Date (Web): June 15, 2012 (Technical Note)DOI: 10.1021/ac301178w

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ACCELERATED ARTICLES

Selective Imaging of Active Pharmaceutical Ingredients in Powdered Blends with Common Excipients Utilizing Two-Photon Excited Ultraviolet-Fluorescence and Ultraviolet-Second Order Nonlinear Optical Imaging of Chiral CrystalsS. J. Toth, J. T. Madden, L. S. Taylor, P. Marsac, and G. J. Simpson

pp 5869–5875Publication Date (Web): June 8, 2012 (Accelerated Article)DOI: 10.1021/ac300917t

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ARTICLES



Bispecific Antibody-Mediated Detection of the Staphylococcus aureus ThermonucleaseSarah J. Wagstaffe, Katja E. Hill, David W. Williams, Beverley J. Randle, David W. Thomas, Phil Stephens, and D. Jason Riley

pp 5876–5884Publication Date (Web): May 25, 2012 (Article)DOI: 10.1021/ac203403d

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Transglutaminase-Mediated in Situ Hybridization (TransISH) System: A New Methodology for Simplified mRNA DetectionMomoko Kitaoka, Masayuki Mitsumori, Kounosuke Hayashi, Yoshiyuki Hiraishi, Hisao Yoshinaga, Koji Nakano, Katsuyuki Miyawaki, Sumihare Noji, Masahiro Goto, and Noriho Kamiya

pp 5885–5891Publication Date (Web): June 19, 2012 (Article)DOI: 10.1021/ac2034198

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Exciton-Plasmon Interactions between CdS Quantum Dots and Ag Nanoparticles in Photoelectrochemical System and Its Biosensing ApplicationWei-Wei Zhao, Pei-Pei Yu, Yun Shan, Jing Wang, Jing-Juan Xu, and Hong-Yuan Chen

pp 5892–5897Publication Date (Web): June 22, 2012 (Article)DOI: 10.1021/ac300127s

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Section: Biochemical Methods

Cancer Biomarker Detection in Serum Samples Using Surface Plasmon Resonance and Quartz Crystal Microbalance Sensors with Nanoparticle Signal AmplificationYildiz Uludag and Ibtisam E. Tothill

pp 5898–5904Publication Date (Web): June 4, 2012 (Article)DOI: 10.1021/ac300278p

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SubMultiple Precursor Ion Scanning of Gangliosides and Sulfatides with a Reversed-Phase Microfluidic Chip and Quadrupole Time-of-Flight Mass SpectrometryHyeyoung Lee, Larry A. Lerno, Jr., Youngshik Choe, Caroline S. Chu, Laura A. Gillies, Rudolf Grimm, Carlito B. Lebrilla, and J. Bruce German

pp 5905–5912Publication Date (Web): June 14, 2012 (Article)DOI: 10.1021/ac300254d

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Simultaneous Fingerprint and High-Wavenumber Confocal Raman Spectroscopy Enhances Early Detection of Cervical Precancer In VivoShiyamala Duraipandian, Wei Zheng, Joseph Ng, Jeffrey J.H. Low, A. Ilancheran, and Zhiwei Huang

pp 5913–5919Publication Date (Web): June 20, 2012 (Article)DOI: 10.1021/ac300394f

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Reduction of Matrix Effects in Polystyrene/Poly(methylene methacrylate) Blends by Metal-Assisted Secondary Ion Mass SpectrometryNora Becker and Tom Wirtz

pp 5920–5924Publication Date (Web): June 20, 2012 (Article)DOI: 10.1021/ac300433n



Physical Properties of Synthetic High Polymers

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Array-Based Disease Diagnostics Using Lipid/Polydiacetylene Vesicles Encapsulated in a Sol–Gel MatrixS. Kolusheva, R. Yossef, A. Kugel, M. Katz, R. Volinsky, M. Welt, U. Hadad, V. Drory, M. Kliger, E. Rubin, A. Porgador, and R. Jelinek

pp 5925–5931Publication Date (Web): June 19, 2012 (Article)DOI: 10.1021/ac300449u

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Fabrication of Sensitive Glutamate Biosensor Based on Vertically Aligned CNT Nanoelectrode Array and Investigating the Effect of CNTs density on the electrode performanceAzam Gholizadeh, Saeed Shahrokhian, Azam Iraji zad, Shamsoddin Mohajerzadeh, Manouchehr Vosoughi, Sara Darbari, Javad Koohsorkhi, and Mahdiyeh Mehran

pp 5932–5938Publication Date (Web): June 27, 2012 (Article)DOI: 10.1021/ac300463x

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Enzyme-Free and Amplified Fluorescence DNA Detection Using Bimolecular BeaconsJiahao Huang, Xuefen Su, and Zhigang Li


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Phospholipid–Graphene Nanoassembly as a Fluorescence Biosensor for Sensitive Detection of Phospholipase D ActivitySi-Jia Liu, Qian Wen, Li-Juan Tang, and Jian-Hui Jiang


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Detection and Quantification of Bacterial Spoilage in Milk and Pork Meat Using MALDI-TOF-MS and Multivariate AnalysisNicoletta Nicolaou, Yun Xu, and Royston Goodacre

pp 5951–5958Publication Date (Web): May 31, 2012 (Article)DOI: 10.1021/ac300582d

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Clinical Pharmacokinetic Assessment of an Anti-MAdCAM Monoclonal Antibody Therapeutic by LC-MS/MSMireia Fernández Ocaña, Ian T. James, Musarat Kabir, Christopher Grace, Guojun Yuan, Steven W. Martin, and Hendrik Neubert

pp 5959–5967Publication Date (Web): June 18, 2012 (Article)DOI: 10.1021/ac300600f

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Detection of Inflammation in Vivo by Surface-Enhanced Raman Scattering Provides Higher Sensitivity Than Conventional Fluorescence ImagingRoss McQueenie, Ross Stevenson, Robert Benson, Neil MacRitchie, Iain McInnes, Pasquale Maffia, Karen Faulds, Duncan Graham, James Brewer, and Paul Garside


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Rapid Identification of Long-Chain Polyunsaturated Fatty Acids in a Marine Extract by HPLC-MS Using Data-Dependent AcquisitionMichael C. Thomas, Simon R. Dunn, Jens Altvater, Sophie G. Dove, and Geoffrey W. Nette


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SubChemical and Elemental Depth Profiling of Very Thin Organic Layers by Constant Kinetic Energy XPS: A New Synchrotron XPS Analysis StrategyPierre-Luc Girard-Lauriault, Thomas Gross, Andreas Lippitz, and Wolfgang E.S. Unger

pp 5984–5991Publication Date (Web): June 11, 2012 (Article)DOI: 10.1021/ac300585q

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SubIn-Vial Dual Extraction for Direct LC-MS Analysis of Plasma for Comprehensive and Highly Reproducible Metabolic Fingerprinting.Luke Whiley, Joanna Godzien, Francisco J Ruperez, Cristina Legido-Quigley, and Coral Barbas


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High-Performance Liquid Chromatography/High-Resolution Multiple Stage Tandem Mass Spectrometry Using Negative-Ion-Mode Hydroxide-Doped Electrospray Ionization for the Characterization of Lignin Degradation ProductsBenjamin C. Owen, Laura J. Haupert, Tiffany M. Jarrell, Christopher L. Marcum, Trenton H. Parsell, Mahdi M. Abu-Omar, Joseph J. Bozell, Stuart K. Black, and Hilkka I. Kenttämaa

pp 6000–6007Publication Date (Web): June 13, 2012 (Article)DOI: 10.1021/ac300762y

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Enrichment and Detection of Rare Proteins with Aptamer-Conjugated Gold NanorodsEmir Yasun, Basri Gulbakan, Ismail Ocsoy, Quan Yuan, Mohammed Ibrahim Shukoor, Chunmei Li, and Weihong Tan




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Surface-Induced Dissociation of Ion Mobility-Separated Noncovalent Complexes in a Quadrupole/Time-of-Flight Mass SpectrometerMowei Zhou, Chengsi Huang, and Vicki H. Wysocki


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Quantification, Localization, and Speciation of Selenium in Seeds of Canola and Two Mustard Species Compared to Seed-Meals Produced by Hydraulic PressGary S. Bañuelos, Spencer S. Walse, Soo In Yang, Ingrid J. Pickering, Sirine C. Fakra, Matthew A. Marcus, and John L. Freeman

pp 6024–6030Publication Date (Web): June 29, 2012 (Article)DOI: 10.1021/ac300813e

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High-Affinity Binding of Remyelinating Natural Autoantibodies to Myelin-Mimicking Lipid Bilayers Revealed by Nanohole Surface Plasmon ResonanceNathan J. Wittenberg, Hyungsoon Im, Xiaohua Xu, Bharath Wootla, Jens Watzlawik, Arthur E. Warrington, Moses Rodriguez, and Sang-Hyun Oh

pp 6031–6039Publication Date (Web): June 22, 2012 (Article)DOI: 10.1021/ac300819a

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Simultaneous Determination of 143Nd/144Nd and 147Sm/144Nd Ratios and Sm–Nd Contents from the Same Filament Loaded with Purified Sm–Nd Aliquot from Geological Samples by Isotope Dilution Thermal Ionization Mass SpectrometryChao-Feng Li, Xian-Hua Li, Qiu-Li Li, Jing-Hui Guo, Xiang-Hui Li, Lian-Jun Feng, and Zhu-Yin Chu

pp 6040–6047Publication Date (Web): June 19, 2012 (Article)DOI: 10.1021/ac300786x

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Quantification of 8-OxodGuo Lesions in Double-Stranded DNA Using a Photoelectrochemical DNA SensorBintian Zhang, Liang-Hong Guo, and Marc M. Greenberg


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Dual-Function pH and Oxygen Phosphonated Trityl ProbeAndrey A. Bobko, Ilirian Dhimitruka, Denis A. Komarov, and Valery V. Khramtsov


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SubAccurate Determination of Quantity of Material in Thin Films by Rutherford Backscattering SpectrometryC. Jeynes, N. P. Barradas, and E. Szilágyi

pp 6061–6069Publication Date (Web): June 4, 2012 (Article)DOI: 10.1021/ac300904c

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Neutrophil Chemotaxis within a Competing Gradient of ChemoattractantsDonghyuk Kim and Christy L. Haynes

pp 6070–6078Publication Date (Web): June 14, 2012 (Article)DOI: 10.1021/ac3009548 Abstrac

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Exploring Three-Dimensional Matrix-Assisted Laser Desorption/Ionization Imaging Mass Spectrometry Data: Three-Dimensional Spatial Segmentation of Mouse KidneyDennis Trede, Stefan Schiffler, Michael Becker, Stefan Wirtz, Klaus Steinhorst, Jan Strehlow, Michaela Aichler, Jan Hendrik Kobarg, Janina Oetjen, Andrey Dyatlov, Stefan Heldmann, Axel Walch, Herbert Thiele, Peter Maass, and Theodore Alexandrov


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Polydispersity Characterization of Lipid Nanoparticles for siRNA Delivery Using Multiple Detection Size-Exclusion ChromatographyJingtao Zhang, R. Matthew Haas, and Anthony M. Leone


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Sensitive Analyses of Neutral N-Glycans using Anion-Doped Liquid Matrix G3CA by Negative-Ion Matrix-Assisted Laser Desorption/Ionization Mass SpectrometryTakashi Nishikaze, Yuko Fukuyama, Shin-ichirou Kawabata, and Koichi Tanaka



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Enzyme-Linked Small-Molecule Detection Using Split Aptamer LigationAshwani K. Sharma, Alexandra D. Kent, and Jennifer M. Heemstra


Electrochemical Determination of Trihalomethanes in Water by Means of Stripping AnalysisAngela A. Peverly and Dennis G. Peters

pp 6110–6115Publication Date (Web): June 17, 2012 (Article)DOI: 10.1021/ac301005t

Quantitative Multiple Reaction Monitoring of Peptide Abundance Introduced via a Capillary Zone Electrophoresis–Electrospray InterfaceYihan Li, Roza Wojcik, Norman J. Dovichi, and Matthew M. Champion

pp 6116–6121Publication Date (Web): June 11, 2012 (Article)DOI: 10.1021/ac300926h

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Colorimetric Method for Determining Pb2+ Ions in Water Enhanced with Non-Precious-Metal NanoparticlesJeffrey Yan and Erik M. Indra


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MALDI-TOF Mass Spectrometry Analysis of Amphipol-Trapped Membrane ProteinsChérine Bechara, Gérard Bolbach, Paola Bazzaco, K. Shivaji Sharma, Grégory Durand, Jean-Luc Popot, Francesca Zito, and Sandrine Sagan

pp 6128–6135Publication Date (Web): June 14, 2012 (Article)DOI: 10.1021/ac301035r

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Low-Resource Method for Extracting the Malarial Biomarker Histidine-Rich Protein II To Enhance Diagnostic Test PerformanceKeersten M. Davis, Joshua D. Swartz, Frederick R. Haselton, and David W. Wright

pp 6136–6142Publication Date (Web): June 13, 2012 (Article)DOI: 10.1021/ac301030m

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Correlation of Stoichiometries for Rb+ Extraction Determined by Mass Spectrometry and Electrochemistry at Liquid|Liquid InterfacesTom J. Stockmann, Anne-Marie Montgomery, and Zhifeng Ding

pp 6143–6149Publication Date (Web): June 17, 2012 (Article)DOI: 10.1021/ac301051e

Top-Down Study of β2-Microglobulin DeamidationXiaojuan Li, Xiang Yu, Catherine E. Costello, Cheng Lin, and Peter B. O’Connor




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Coulometric Sodium Chloride Removal System with Nafion Membrane for Seawater Sample TreatmentEwa Grygolowicz-Pawlak, Manzar Sohail, Marcin Pawlak, Bastien Neel, Alexey Shvarev, Roland de Marco, and Eric Bakker


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Magnetic Levitation as a Platform for Competitive Protein–Ligand Binding AssaysNathan D. Shapiro, Siowling Soh, Katherine A. Mirica, and George M. Whitesides

pp 6166–6172Publication Date (Web): June 11, 2012 (Article)DOI: 10.1021/ac301121z

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SubRestoration and Spectral Recovery of Mid-Infrared Chemical ImagesEric C. Mattson, Michael J. Nasse, Margaret Rak, Kathleen M. Gough, and Carol J. Hirschmugl

pp 6173–6180Publication Date (Web): June 25, 2012 (Article)DOI: 10.1021/ac301080h

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Microwave-Assisted Protein Solubilization for Mass Spectrometry-Based Shotgun Proteome AnalysisXiaoxia Ye and Liang Li


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Optical Aptasensors for the Analysis of the Vascular Endothelial Growth Factor (VEGF)Ronit Freeman, Julia Girsh, Amily Fang-ju Jou, Ja-an Annie Ho, Thomas Hug, Jens Dernedde, and Itamar Willner


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SubSection: Biochemical Genetics

Sensitive and Label-Free DNA Methylation Detection by Ligation-Mediated Hyperbranched Rolling Circle AmplificationAnping Cao and Chun-yang Zhang

pp 6199–6205Publication Date (Web): June 19, 2012 (Article)DOI: 10.1021/ac301186j



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Probing the Interaction of Cisplatin with Cytochrome c by Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass SpectrometryNingbo Zhang, Yonggang Du, Meng Cui, Junpeng Xing, Zhiqiang Liu, and Shuying Liu

pp 6206–6212Publication Date (Web): June 29, 2012 (Article)DOI: 10.1021/ac301122w


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Section: Organic Analytical Chemistry

Fluorine Speciation Analysis Using Reverse Phase Liquid Chromatography Coupled Off-Line to Continuum Source Molecular Absorption Spectrometry (CS-MAS): Identification and Quantification of Novel Fluorinated Organic Compounds in Environmental and Biological SamplesZhiwei Qin, David McNee, Heike Gleisner, Andrea Raab, Kwaku Kyeremeh, Marcel Jaspars, Eva Krupp, Hai Deng, and Jörg Feldmann


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Polyamine-Functionalized Carbon Quantum Dots as Fluorescent Probes for Selective and Sensitive Detection of Copper IonsYongqiang Dong, Ruixue Wang, Geli Li, Congqiang Chen, Yuwu Chi, and Guonan Chen


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Differentiation of Eight Phenotypes and Discovery of Potential Biomarkers for a Single Plant Organ Class Using Laser Electrospray Mass Spectrometry and Multivariate Statistical AnalysisPaul M. Flanigan, IV, Laine L. Radell, John J. Brady, and Robert J. Levis


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A High-Throughput, Multiplexed Kinase Assay Using a Benchtop Orbitrap Mass Spectrometer To Investigate the Effect of Kinase Inhibitors on Kinase Signaling PathwaysRyan C. Kunz, Fiona E. McAllister, John Rush, and Steven P. Gygi

pp 6233–6239Publication Date (Web): June 19, 2012 (Article)DOI: 10.1021/ac301116z

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Electroanalytical Performance of Nitrogen-Containing Tetrahedral Amorphous Carbon Thin-Film ElectrodesXingyi Yang, Lars Haubold, Gabriel DeVivo, and Greg M. Swain


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Ultrasensitive Detection of Cancer Biomarkers in the Clinic by Use of a Nanostructured Microfluidic ArrayRuchika Malhotra, Vyomesh Patel, Bhaskara V. Chikkaveeraiah, Bernard S. Munge, Sok Ching Cheong, Rosnah B. Zain, Mannil T. Abraham, Dipak K. Dey, J. Silvio Gutkind, and James F. Rusling

pp 6249–6255Publication Date (Web): June 14, 2012 (Article)DOI: 10.1021/ac301392g

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SubDetection of DNA Adducts Originating from 1-Methoxy-3-indolylmethyl Glucosinolate Using Isotope-Dilution UPLC-ESI-MS/MSFabian Schumacher, Wolfram Engst, Bernhard H. Monien, Simone Florian, Anke Schnapper, Lisa Steinhauser, Klaus Albert, Heinz Frank, Albrecht Seidel, and Hansruedi Glatt


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SubMultiplexed Fluorescence Resonance Energy Transfer Aptasensor between Upconversion Nanoparticles and Graphene Oxide for the Simultaneous Determination of MycotoxinsShijia Wu, Nuo Duan, Xiaoyuan Ma, Yu Xia, Hongxin Wang, Zhouping Wang, and Qian Zhang

pp 6263–6270Publication Date (Web): June 25, 2012 (Article)DOI: 10.1021/ac301534w

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SubAn Electrochemically Based Total Organic Carbon Analyzer for Planetary and Terrestrial On-Site ApplicationsShannon T. Stroble and Samuel P. Kounaves

pp 6271–6276Publication Date (Web): June 24, 2012 (Article)DOI: 10.1021/ac301704m

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Table of Contentslib3.dss.go.th/fulltext/E_content/0003-2700/2012v84n14.pdf · Michael C. Thomas, Simon R. Dunn, Jens Altvater, Sophie G. Dove, and Geoffrey W. Nette pp 5976–5983