SYMBIONT - PHASE II ENVIRONMENTAL SITE ASSESSMENT REPORT · 2019. 6. 27. · This report summarizes the results of a Phase II Environmental Site Assessment (ESA) ... As described

October 14, 20 I 0

ARED FOR :

City of Muncie 300 North High Street Muncie, Indiana 47305

REPARED BY :

Symbiont 3850 Priority Way South Drive, Suite I 0 Indianapolis, IN 46240

Phase II Environmental Site Assessment Former Frank Foundries Property 2000- 2100 East 8th Street Muncie, IN 47302

Christine (Tina) A. Reese, P.G. Project Manager

inder, LPG Quality Assurance Manager

Symbiont Project No. WI 03820

Steph nie G. Hinz, .G. Senior Hydrogeologist

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TABLE OF CONTENTS Section Page

1.0 INTRODUCTION .................................................................................................. 1

1.1 Project Identification ................................................................................. 1 1.1.1 Site Name, Facility Identification Number(s),

Mailing Address, ........................................................................... 1 1.1.2 Site Location Map ......................................................................... 1 1.1.3 Current Owner and Operator, and Mailing Address, .................... 1 1.1.4 Site Contact Person or Group Responsible for Investigation ....... 1

1.2 Overview of Current Contamination Conditions ....................................... 2 1.2.1 Current Site Conditions ................................................................ 2 1.2.2 Summary of Phase II ESA Results ............................................... 2

2.0 SITE BACKGROUND AND BASELINE PROJECT ASSESSMENT .................... 4

2.1 Site History ............................................................................................... 4 2.1.1 Current and Past Operations ........................................................ 4 2.1.2 Hazardous Materials Used and Stored on Site ............................ 4 2.1.3 Site Ownership and Operational History ...................................... 5 2.1.4 Site Spill and Contamination History ............................................ 5 2.1.5 Previously Completed Reports, Investigations and Actions ......... 5

2.2 Geographic Information .......................................................................... 11 2.3 Geologic Information .............................................................................. 11 2.4 Ecologic Information ............................................................................... 13 2.5 Preliminary Evaluation of Potentially Susceptible Areas ........................ 13 2.6 Preliminary Evaluation of Possible Chemicals of Concern ..................... 13 2.7 Preliminary Evaluation of Potential Contaminant Transport

Mechanisms ........................................................................................... 13 2.8 Preliminary Evaluation of Potential Human Exposure Pathways ........... 13

3.0 INVESTIGATION METHODS ........................................................................... 15

3.1 Soil Assessment ..................................................................................... 15 3.2 Groundwater Assessment ...................................................................... 15 3.3 Vapor Assessment ................................................................................. 16

4.0 INVESTIGATION RESULTS .............................................................................. 17 4.1 Soil .................................................................................................... 17 4.2 Water Table Depth, Elevation and Flow Directions ................................ 18 4.3 Groundwater .......................................................................................... 18 4.3.1 Field Water Quality .................................................................... 18 4.3.2 Temporary Monitoring Wells ....................................................... 18 4.4 Vapor .................................................................................................... 19

4.4.1 Soil Screening ........................................................................... 19 4.4.2 Groundwater Screening ............................................................. 19 4.4.3 Summary ................................................................................... 19

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5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................. 20 5.1 Conclusions ............................................................................................ 20 5.1.1 Soil .............................................................................................. 20 5.1.2 Groundwater ............................................................................... 20 5.1.3 Vapor ......................................................................................... 21 5.1.4 Potential Risks to Ecological and Human Health ........................ 21 5.2 Recommendations ................................................................................. 22 6.0 LIMITATIONS .................................................................................................... 23 7.0 REFERENCES .................................................................................................. 24

TABLES

1A Soil Sampling Results – Industrial Default Closure Levels 1B Soil Sampling Results – Recreational Nondefault Closure Levels 2 Water Quality and Elevation Data

3 Groundwater Sampling Results

FIGURES

1 Site Location and Local Topography 2 Site Base Map

3 Detected Constituents of Concern in Site Soil Samples – Industrial Default

Closure Levels 4 Detected Constituents of Concern in Site Soil Samples – Recreational Default

Closure Levels 5 Potentiometric Surface Map (09/09/2010)

6 Detected Constituents of Concern in Groundwater

APPENDICES

A Photodocumentation of Field Activities B Laboratory Analytical Data C Soil Boring Logs

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Section 1.0 INTRODUCTION

This report summarizes the results of a Phase II Environmental Site Assessment (ESA) completed by Symbiont on behalf of the City of Muncie at the former Frank Foundries property located at 2000-2100 East 8th Street in the City of Muncie, Indiana hereafter referred to as the “Site”. Based on the information reviewed from the Phase I ESA (Symbiont, 2008), a Phase II ESA was performed in September 2010. The objective of the Phase II ESA was to evaluate current hydrogeologic conditions and document existing soil and groundwater quality. Further detail is provided in the following sections. 1.1 PROJECT IDENTIFICATION 1.1.1 Site Name, Facility Identification Number(s), and Mailing Address The Site is located at 2000-2100 East 8th Street, Muncie, Indiana. The Site is located in Center Township of Delaware County. The Site is located on the north side of East 8th Street, east of the intersection with South Brotherton Street and consists of two parcels of land described as:

Street Address Owner Name

Parcel No. Lot Size (acres)

2000 East 8th Street**

Muncie Castings Specialties, Inc.

11-14-313-007-000 5.5

2100 East 8th Street**

Muncie Warehousing Technologies, Inc.

11-14-328-001-000 4.5

**The Site has the historic address 1324 South Brotherton Avenue

The Site is located in the northwest quarter of Section 14, Township 20 North, and Range 10 East. The approximate latitude of the Site is 40 10’ 56.2” north and the approximate longitude is 85 21’ 50.3” west. 1.1.2 Site Location Map The location and layout of the Site is depicted in Figures 1 and 2. 1.1.3 Current Owner and Operator, and Mailing Address Delaware County records indicate that the property was deeded to Muncie Castings Specialties, Inc. and Muncie Warehousing Technologies, Inc. from Mr. Michael Dunn on April 1, 2004. 1.1.4 Site Contact Person or Group Responsible for the Investigation This Phase II ESA was prepared for the City of Muncie and was funded by a United States Environmental Protection Agency (USEPA) Brownfields Site Assessment grant and monies drawn from the City of Muncie’s general fund.


Contact Information includes:

Mr. Brad Bookout Office of Community Development 300 North High Street Muncie, IN 47305 765-751-9133 [email protected] 1.2 OVERVIEW OF CURRENT CONDITIONS 1.2.1 Current Site Conditions The current layout of the Site is depicted in Figure 2. Photographs of the Site are provided in Appendix A. The Site currently consists of two connected parcels of land. The western parcel is 5.67 acres in size and has multiple interconnected buildings on concrete slab grade that cover the majority of the parcel. The eastern parcel is 4.34 acres in size and contains a grass covered area, a wooded lot, and a grassy and wooded lot containing apparent foundry sand fill materials. The eastern parcel is bisected by an abandoned rail line spur. The Site buildings are in various conditions ranging from severe disrepair to marginal. The Property is currently being used for storage and material salvage operations. Areas of the Site not under roof contain extensive piles of debris and or salvaged materials, or are overgrown with vegetation. As described above, piles of apparent foundry sand are located on the eastern parcel. Miscellaneous debris is scattered throughout the buildings including general refuse, miscellaneous containers and foundry remnants. 1.2.2 Summary of Phase II ESA Results Soil Soil samples were collected from 12 locations across the Site. Select samples were sent to the laboratory and analyzed for polychlorinated biphenyls (PCBs), polynuclear aromatic hydrocarbons (PAHs), volatile organic compounds (VOCs) and/or Resource Conservation and Recovery Act (RCRA) metals. Future Site plans include either re-use as an industrial property or re-purposing as a recreational area or green space. As such, soil concentrations detected in samples collected from the Site were compared to both Indiana Department of Environmental Management (IDEM) Risk Integrated System of Closure (RISC) Industrial Default Closure Levels (IDCLs) and Interim Recreational Nondefault Closure Levels. Exceedances are summarized below. IDEM RISC IDCLs were exceeded at seven sample locations; TW/SB-2, TW/SB-4, SB-8, SB-10, SB-12, SB-13 and TW/SB-16. The RISC IDCL for lead (230 milligrams per kilogram [mg/kg]) was exceeded at TW/SB-2, a soil boring installed adjacent to the former pattern shop. The RISC IDCL for arsenic (5.8 mg/kg) was exceeded at all seven locations; these locations are distributed across the site. The RISC IDCL for benzo(a)pyrene (1.5 mg/kg) was exceeded at


SB-10, a soil boring installed to document the soil quality of a large pile of apparent foundry sand located on the eastern portion of the Site. IDEM RISC Interim Recreational Nondefault Closure Levels were exceeded at three locations; TW/SB-2, SB-8 and SB-10. The RISC Interim Recreational Nondefault Closure Level for arsenic (13 mg/kg) was exceeded at TW/SB-2, a soil boring installed adjacent to the former pattern shop. The RISC Interim Recreational Nondefault Closure Level for Benzo(a)pyrene (0.51 mg/kg) was exceeded at SB-8 and SB-10. The RISC Interim Recreational Nondefault Closure Level for dibenzo(a,h)anthracene (0.51 mg/kg) was exceeded at SB-10. Both SB-8 and SB-10 were installed to document the soil quality of a large pile of apparent foundry sand located on the eastern portion of the site. Groundwater IDEM RISC IDCL exceedances were detected in samples collected at two locations, TW-1 and TW/SB-4, which are monitoring wells located in the west central portion of the property adjacent to the main foundry building, downgradient of a suspected underground storage tank location (TW-1) and adjacent to the former Test Lab (TW/SB-4). The RISC IDCL for lead (0.042 milligrams per liter [mg/L]) was exceeded at TW-1. The RISC IDCL for arsenic (0.01 mg/L) was exceeded at TW-1 and TW/SB-4. These samples appeared slightly turbid in the field indicating that exceedances may be the result of colloidal material present within the groundwater sample, which were unfiltered.


Section 2.0 SITE BACKGROUND AND BASELINE PROJECT ASSESSMENT

2.1 SITE HISTORY 2.1.1 Current and Past Operations During Phase II ESA field activities, the Site was being used for storage and material salvage operations. Details of the Site’s operational history and Phase I ESA (Symbiont 2008) findings are provided below. Foundry Operations The Site was listed as Muncie Foundry and Machine prior to 1911. Between 1911 and 1950, the Frank Foundry Corporation operated until approximately 1996. Foundry operations included a machine shop, core ovens, copulas and drying ovens. Material Storage and Salvage Operations Since 1996, Site owners have stored various materials and wastes on-site. These materials included transformers, capacitors and waste tires. The current owner uses the property to store material from building salvage operations. Additionally, other material stored on the site includes petroleum products, paints, and solvents. USEPA Removal Actions A USEPA Time Critical Removal Action was conducted in June and July of 1999. The action included the identification and removal of more than 300 drums and waste containers. More than 150 drums of transformers, capacitors and PCB-containing oils and soil were also removed during this action. 2.1.2 Hazardous Materials Used or Stored on Site During the Phase I ESA Site inspection conducted in 2008, Symbiont observed numerous chemical containers throughout the Site. Chemical containers identified throughout many facility buildings and the property included paints, solvents, oils, and other petroleum products. Past chemical storage and handling activities are documented in the USEPA Removals Report. One underground storage tank (UST) was identified on the west side of the Site, next to the main foundry building along with its associated pump fixture. Neither the UST nor the pump was in operation during the Site inspection. An above ground storage tank (AST) was located inside the main facility building. The AST was suspended along the top portion of the wall in the walkway area leading to the northern end of the facility, approximately 40 feet high. No markings were present on the AST, and it is not known what material it may have stored.


Observation of several areas was limited due to the structural condition of many site buildings, building debris and vegetative overgrowth of the property. As such, the potential for additional containers containing hazardous materials exists. 2.1.3 Site Ownership and Operational History The Site consists of two parcels. The west parcel is owned by Muncie Warehousing Technologies, Inc. The east parcel is owned by Muncie Casting Specialties, Inc. As part of Phase I ESA activities conducted in 2008, a search of the County Recorders records (including property deeds) was completed; the following information was noted: West Parcel

Deeded to Muncie Warehousing Technologies, Inc. from Mr. Michael Dunn on April 1,

2004.

Deeded to Mr. Michael Dunn from the Delaware County Commissioners on September 22, 2000.

Deeded to the Delaware County Commissioners as a result of delinquent property taxes from Mr. Milton McCarter on September 11, 2000.

East Parcel

Deeded to Muncie Casting Specialties, Inc. from Mr. Michael Dunn on April 1, 2004.

Deeded to Mr. Michael Dunn from the Delaware County Commissioners on September 22, 2000.

Deeded to the Delaware County Commissioners as a result of delinquent property taxes from Mr. Milton McCarter on September 11, 2000.

No environmental liens or activity and use limitations (AULs) were found for either parcel. Note that liens exist due to nonpayment of property taxes. 2.1.4 Site Spill and Contamination History The Site was formerly a generator of RCRA hazardous waste materials. However, the Site is currently not a generator. The waste streams were listed as D001 – Ignitable Wastes and D002 – Corrosive Wastes. The Site had a long list of compliance violations in the 1990s which resulted in a USEPA action being conducted in 1999. On September 10, 2003, USEPA conducted a Site re-inspection and prioritized the site as No Further Remedial Action Planned (NFRAP). 2.1.5 Previously Completed Reports, Investigations and Actions There have been several reports, investigations and actions (including state and federal involvement) historically completed at the Site. The reports, investigations and actions are summarized in the following sections.


2008 - Phase I ESA Symbiont conducted a Phase I ESA in 2008. The findings included the following recognized environmental conditions (RECs) at the Site: REC No.1 – Historic Site Uses/Conditions Foundry Operations The Site was operated as a foundry from prior to 1911 to approximately 1996. Foundry operations included a machine shop, core ovens, cupolas and drying ovens. Sand molds from past foundry operations are located throughout the Site buildings. Foundry sand is also located extensively across the Site. The eastern Site parcel located adjacent to the Cardinal Greenway trail appears to have been used for foundry sand disposal. Foundry sand covers this parcel to depths of up to 20 feet in some areas. Material/Waste Storage and Salvage Operations Following the end of foundry operations at the Site in 1996, owners brought various materials and wastes to the site. These materials included transformers, capacitors and waste tires. REC No. 2 – USTs and ASTs One UST is present on the property, located on the west side of the Site next to the foundry building along with its associated pump fixture. An AST was located inside the main facility building suspended from the ceiling. Former AST support structures were identified in the northern part of the facility and in the former boiler room/building. A potential fill line and AST support structures were identified in the small building located on the east side of the main property entrance. REC No. 3 – IDEM and USEPA Actions IDEM conducted numerous site inspections, a Preliminary Assessment and a Site Investigation at the Site. The inspections and assessments identified the storage of waste materials, petroleum products, PCBs and waste tires. A USEPA Time Critical Removal Action was conducted in June and July 1999. REC No. 4 – Current Property Use The current owners of the parcels, Muncie Casting Specialists, Inc. and Muncie Warehousing Technologies, Inc., use the property to store material from building salvage operations. Materials currently stored on site include petroleum products, paints, and solvents. The Phase I ESA also revealed the following potential environmental concerns (PECs) at the Site:


PEC No. 1 Land Uses/Environmental Conditions on Neighboring Properties Land uses and/or environmental conditions of potential environmental concern were identified at the following properties located north of the Site:

Property owned by Mr. Paul Funkhouser being used to store and repair automotive vehicles.

Impacts, if present at this property, have a possibility of intersecting the Site. PEC No. 2 Former Adjacent Railroad Tracks Railroad tracks ran along the east side of the Site. The track is no longer operational and has been redeveloped as part of the Cardinal Greenway rail trail. The proximity of the Site to the former railroad tracks represents a general PEC of possible undocumented spills or releases of petroleum products or other chemicals that may have been released at the Site and/or migrated onto the Site. PEC No. 3 Unknown/Historic Fill Fill piles on the north side of the Site were noted in the IDEM site inspection trip reports. The potential exists for the presence of undocumented fill materials at numerous other locations at the Site. The potential for undocumented fill materials can be considered a generic PEC in older areas of the City and can include clean fill, construction/demolition debris, foundry sand, slag, ash, cinders, and other materials potentially containing hazardous substances. PEC No. 4 Building/Construction/Demolition Materials It is possible that some asbestos containing materials (ACMs) and lead-based paint or sealers are present in building materials and/or construction/demolition debris present at the Site. An inspection and sampling for ACMs and lead-based paint was not included within the scope of the Phase I ESA conducted by Symbiont in 2008. Previous State and Federal Involvement Symbiont reviewed several other previously completed environmental investigations, reports and other documentation concerning the Site. The findings are summarized below.

According to USEPA reports, the Delaware County Health Department referred the Site to the IDEM in April 1991. IDEM’s Emergency Response Section (ERS) determined it was not an emergency situation and referred it to the Site Investigation Section (SI). IDEM/SI completed a Preliminary Assessment (PA) in June of 1991 and a Site Screening Inspection (SSI) in September of 1992. Due to upgrades to the IDEM File Room, Symbiont was unable to obtain copies of these reports.

On July 29 and 30, 1992, USEPA’s contractor conducted an initial site investigation and returned to the Site on August 13, 1992 to collect additional samples. The Site Assessment Report, dated December 31, 1992, concluded the following threats existed:


A threat of direct contact due to poor site security, and

The presence of hazardous waste in drums and other containers that threaten release, and the potential for fire and/or explosion.

A Removal Action Plan Letter Report was completed on December 31, 1992; however, no USEPA removal action began following that report.

According to IDEM, there was a failed attempt by another party to reopen the facility as a foundry in 1993. Since 1993, the plant had remained idle, except for the authorized and unauthorized salvaging of on-site materials.

On April 30, 1996, IDEM’s Hazardous Waste Compliance Section conducted a Site visit following a complaint alleging the removal of drums from the Site without material characterization or the required manifests needed to ship and dispose of the material. The inspection noted the presence of 244 55-gallon drums, three 30-gallon drums, two containers of sodium pyrophosphate, and one container of methylene blue. IDEM determined that no drums or material had been removed from the site as noted in the complaint. Starting in May 1996, the site owner began characterization activities of potential waste materials identified in the April 30, 1996 inspection and received IDEM approval to dispose of materials as a Special Waste.

On May 29, 1997, the IDEM Hazardous Waste Compliance Section conducted a Site inspection following a complaint. The complaint alleged the site was illegally storing used tires. Approximately 3,500 used tires were present at the Site. The inspection also noted the presence of potentially ACM disposed in a concrete pit in the rear of the facility and the possibility that additional ACM may be buried on-site.

On March 11, 1998, IDEM’s Hazardous Waste Compliance Section conducted a Site visit. The Trip Report for the site visit noted numerous waste containers and potential ACM materials throughout the site.

A follow up inspection was conducted by the IDEM on April 13, 1998. The inspection noted the presence of over 300 tires, over 70 containers (drums and gallon pails) containing oily wastes and other potential hazardous substances and stained soil areas from the spill of oily wastes. Recommendations included the referral of the Site to IDEM’s Office of Environmental Response, Immediate Removal Section.

On behalf of the USEPA, and Ecology and Environment, Inc. (E & E), Superfund Technical Assessment and Response Team (START) assisted the EPA in performing a Site assessment. On May 21, 1998, the USEPA, START Contractor, and IDEM mobilized to conduct a Site assessment of the Property. The following observations were made:

The building is in dilapidated condition. The machine storage building and shed are empty.


Approximately 100 drums are located throughout the Site containing unknown solids and liquids (or empty). The drums are in poor condition.

Southern portion of plant – open pit of debris, a transformer, and approximately 20 drums.

Several pallets of DIa-Carb – a carbonate anhydrase inhibitor, and when heated to decomposition, it emits toxic nitric and sulfuric fumes.

Four leaking transformers located in the outside area between the southern and central plants. Another leaking transformer is located on the western portion of the Site. Six destroyed transformers are present.

Sixty (60) capacitors are located in the central portion of the plant. Thirty (30) capacitors are located in the southwest corner of the Site.

Chemical storage room inside plant with “lab chemicals.”

Two other drums labeled “Poison” are located in the plant.

Five-hundred (500) tires.

Pits containing debris and foundry sand throughout.

The report concluded that the potential threats posed by the Site included:

Exposure to nearby human and animal populations from hazardous substances stored in drums and other containers.

Potential threat of releases from drums, barrels, and other bulk storage containers.

Due to the condition of the Site buildings, hazardous waste on-site is exposed to the weather.

A fire or explosion threat exists from wastes stored on site. The report recommended removal of hazardous wastes from the Site to mitigate the potential threats. This removal action included drums, capacitors, transformers, and the excavation of PCB contaminated soils.

A USEPA Time Critical Removal Action was conducted by the START contractor

from June 28, 1999 to July 29, 1999. Waste characterization and disposal activities including the following:

Identification, sampling and analysis of 136 drums and 96 containers.


Entry into the former Frank Foundries office (owned by Claudine Hoepner) – Inventory of two 5-gallon pails, one drum and an 11,000 pound transformer which contained PCBs over 50 part per million (ppm).

One hundred and three (103) PCB capacitors were identified.

Soil near the capacitors was sampled; results were below the removal standard for PCBs.

Ninety three (93) drums containing liquids (drums were combined).

Stained soil sampled on May 21, 1998 was drummed.

Fifty seven (57) drums were transported to Eltex Chemical Company in Houston for disposal.

Fifty (50) drums were crushed and added to a roll-off box.

The transformer present in the office was moved to the Site. The oil was drained into drums.

Forty seven (47) drums were transported to Eltex Chemical Company in Houston for disposal.

Analytical results of the oil from the smaller transformers indicated 120 ppm of PCBs.

A third shipment of 29 drums containing capacitors, two drums of PCB oil, and one drum of PCB contaminated filters, hoses, and other transformer materials was transported to Chemical Waste, Inc. in Port Arthur, Texas for incineration.

The two large and four smaller transformers were transported to Transformer Decommissioning LLC in Nabb, Indiana. One transformer was transported to U.S. Ecology in Beatty, Nevada.

Two roll-off boxes containing non-hazardous material were shipped to Jay County Landfill in Portland, Indiana for land disposal.

Still present on the Site are the 500 used tires and several pallets of Mississippi Lime and carbonate materials that will not be addressed by the USEPA.

On behalf of the current Site owner, Muncie Warehousing Technologies, Inc., Locus

Technologies prepared a scope of work and budget to complete cleanup activities at the Site (post USEPA activities). The scope of work included asbestos removal, building demolition/stabilization, tire removal, UST removal, and clean and backfill pits, trash, and debris removal and disposal.


2.2 GEOGRAPHIC INFORMATION Information obtained from the Indiana Geologic Survey (IGS) website (http://igs.indiana.edu/), “Indiana Map,” was used to obtain details regarding the physical setting of the Site and surrounding area and is referenced several times in this section. Topography According to the Indiana Geological Survey (IGS) website, the Site is located in the “Bluffton Till Plain” of the “Central Till Plain” natural region. The Site is located in the “New Castle Till Plains and Drainageways” physiographic unit. Ground Surface Elevations on Site Based on the topographic contours on the United States Geological Survey (USGS) topographic map (Figure 1), ground surface at the Site is approximately 952 feet above mean sea level (ft amsl). According to observations made during the Site, the Site is relatively flat and may have a slight slope downward towards the south. However, the eastern portion of the Site contains large piles of foundry sand. Ground Surface Elevations in the Site Vicinity Ground surface elevations within an approximate one-mile radius of the Site range from approximately 972 ft amsl (three-quarters of a mile south of the Site) to 927 ft amsl (at the White River located one-half of a mile north and east of the (Site Figure 1). The general slope of the ground surface is towards the north and west. 2.3 GEOLOGIC INFORMATION Soils A detailed well log for a well located at the Site was obtained on the Indiana Department of Natural Resources (DNR) online well database (http://www.in.gov/gis-dnr-web/website/DNR_WaterWells_II/viewer.htm). According to details provided on the log, subsurface soils at the Site consisted of mixed fill from the surface to five feet bgs underlain by clay to a depth of 67 feet bgs. A 5-foot thick layer of sand and gravel was encountered between 50 and 55 feet bgs. Bedrock was encountered at a depth of 67 feet bgs. According to the EDR Geocheck© Report (EDR, 2008), the predominant soil series in the vicinity of the Site is “Miami.” The surface soil texture is described as silt loam. According to the IGS website, the Site is located within the “Miami-Crosby-Treaty” soil association zone. The Site is located in a zone with 50 to 100 feet of unconsolidated deposits above bedrock. Near surface materials at the property likely consist of reworked native soil and potential fill. Apparent foundry sand is present across the ground surface throughout the Site. The wooded


area on the eastern parcel has apparent foundry sand fill piles up to 20 feet above the ground surface. Geology According to the IGS website, bedrock beneath the Site is anticipated to be dolomite and limestone from the “Pleasant Mills” formation. The depth to bedrock is anticipated to be from 50 to 100 feet bgs. According the well log for the water supply well at the Site (see Section 2.5.2), bedrock was encountered at 67 feet bgs, and was described as limestone and shale to the maximum depth of boring of 246 feet bgs (the maximum depth of boring). Hydrology The nearest surface water body is the White River, which is located approximately one-half mile north and east of the Site. According to the IGS website, the Site is located in the White River/Truitt Ditch Watershed. Hydrogeology According to the IGS website, the Site is located above a carbonate rock aquifer. The following information on three wells located in the vicinity of the Site was obtained:

701 South Burlington Drive (located northwest of the Site) – Static water level – 30 feet bgs; Depth of well 115 feet bgs; Elevation of ground surface – 959 ft amsl.

Layne-Northern Co. (located west-southwest of the Site) Static water level – 19 feet bgs; Depth of well 45 feet bgs; Elevation of ground surface – 960 ft amsl.

1315 Jersey Avenue (located east of the Site) Static water level – 8 feet bgs; Depth of

well 107 feet bgs; Elevation of ground surface – 960 ft amsl. An additional well was listed in the EDR Geocheck© Report (EDR, 2008) that appears to be located on the Site. The following information on the well is provided:

Static water level – 27 feet bgs; Depth of well – 246 feet bgs; Elevation of ground surface – 968 ft amsl.

Based on the information above, it appears as though groundwater at the Site is likely located between 8 and 30 feet bgs. No site-specific information regarding groundwater flow directions was reviewed during the Phase I ESA. Based on the location of the Site relative to the White River, the direction of groundwater flow is anticipated to be north or east towards the White River. Local groundwater flow patterns may also be dominated by constructed features such as permeable backfill materials surrounding building foundations or buried conduits and sumps in the basements of nearby buildings.


2.4 ECOLOGIC INFORMATION Wetlands Information regarding the potential for on-site wetlands was reviewed from the United States Fish and Wildlife Service (FWS) National Wetland Inventory Map HTTP://WWW.FWS.GOV/WETLANDS/DATA/MAPPER.HTML and from Symbiont’s Phase I ESA (2008). The maps indicate there are no wetlands on Site. Flood Zones Based on information provided in the Phase I ESA (Symbiont, 2008), the Site appears to be located outside any defined 100 year or 500-year floodplain. Endangered Species Endangered species were not evaluated as part of the Phase II ESA. 2.5 PRELMINARY EVALUATION OF POTENTIALLY SUSCEPTIBLE AREAS The following potentially susceptible areas were identified as part of the Phase II ESA.

Debris piles located throughout the Site and primarily on the eastern parcel. UST near the northwest property boundary. Former manufacturing areas.

2.6 PRELIMINARY EVALUATION OF POSSIBLE CHEMICALS OF CONCERN Based on a review of historical Site usage PAHs, VOCs, PCBs and RCRA metals all represent chemicals of concern for the Site. 2.7 PRELIMINARY EVALUATION OF POTENTIAL CONTAMINANT TRANSPORT

MECHANISMS The following potential contaminant transport mechanisms were identified as part of the Phase II ESA:

Storm water via infiltration and overland flow, Groundwater migrating off-site, and Vapor migration.

2.8 PRELIMINARY EVALUATION OF POTENTIAL HUMAN EXPOSURE PATHWAYS The following potential exposure pathways were identified as part of the Phase II ESA:


Contact with or ingestion of surface and/or groundwater, Inhalation of vapors, if present, and Construction worker direct contact with soil and groundwater.


Section 3.0 INVESTIGATION METHODS

A Site specific Phase II ESA Sampling and Analysis Plan was developed for the Site and had two main objectives:

1. Evaluate current hydrogeologic conditions at the Site. 2. Evaluate current soil and groundwater quality at the Site based on the RECs and PECs

identified during the Phase I ESA. Details regarding investigation methods are provided in the following sections. Sample location and analysis rational are provided on Table 1. 3.1 SOIL ASSESSMENT Soil samples were collected from twelve boring locations using direct push sampling methods to a depth ranging from approximately 10 to 25 feet below ground surface (bgs). The soil types were described by an on-site hydrogeologist using the unified Soil Classification System (USCS) and Munsell Color Classification System. Soil from each sample interval was split into subsamples for geologic/lithologic classification, field headspace analysis, visual screening and possible laboratory analysis. Soil samples collected for analysis were placed in laboratory supplied sample containers, preserved (as appropriate), sealed, labeled and immediately placed on ice in a cooler for shipment to the laboratory. Select soil samples were analyzed for VOCs, (EPA 8260) PAHs (EPA 8270 by SIM), PCBs (EPA 8082) and RCRA metals (EPA 6010). The sample cooler was submitted under proper chain-of-custody procedures to Pace Analytical, Inc. of Indianapolis, Indiana (Pace). Soil samples were field screened using a photoionization detector (PID). The PID was calibrated daily in the field in accordance with the manufacturer’s specification. The results were reported as instrument units (i.u.) and reported on the soil boring logs. Soil sampling equipment, such as drilling tools, were decontaminated prior to arrival on-site and between soil boring locations. Sampling equipment was decontaminated by washing with a trisodium phosphate substitute solution or equivalent followed by clean tap water or distilled water rinses. Soil borings were decommissioned using hydrated bentonite pellets and gravity feed methods. 3.2 GROUNDWATER ASSESSMENT Temporary monitoring wells were constructed at eight of the 12 boring location (TW-1, TW/SB-2, TW/SB-3, TW/SB-4, TW/SB-5, TW/SB-6, TW-14 and TW/SB16). The wells were constructed by inserting 1-inch diameter polyvinyl chloride (PVC) well screen (0.0010 slot) and riser into the borehole and allowing the formation to collapse onto the screened riser. The wells were completed across the water table.


Prior to well purging and sampling, groundwater levels were measured using a SolinstTM water level probe which was decontaminated between each well location. The wells were purged of 10 well volumes or until water quality parameters (pH, temperature, dissolved oxygen) stabilized prior to sample collection. Following well development, groundwater samples were collected and submitted to Pace. Groundwater samples were collected and analyzed for VOCs, PAHs, and RCRA metals (unfiltered) from the eight groundwater monitoring wells. The wells were sampled using new disposable bailers. Groundwater samples were placed in laboratory-supplied containers and preserved as appropriate. Following purging and sampling, select field water quality parameters were measured using a YSITM water quality meter. Water quality parameters included pH, specific conductivity, temperature, dissolved oxygen (DO), oxidation-reduction potential (ORP), turbidity, and obvious color and odor. The water quality meter was decontaminated between each well location. The top of casing and ground surface elevations at each well location were surveyed to within 0.01 feet. Surveyed elevations and water level measurements were utilized for calculating groundwater elevations and evaluating groundwater flow direction. Each well was properly abandoned using hydrated bentonite pellets and gravity feed methods following sample collection. 3.3 VAPOR ASSESSMENT The IDEM vapor intrusion guidance documents provide a rational, sequential method to determine if the vapor exposure pathway is completed from a source area (contaminated soil or groundwater) to soil gas in the unsaturated zone and to a potential receptor in an occupied building. The first step in the sequential process involves a preliminary screening evaluation which is conducted to determine if contaminant concentrations in the groundwater or the soil are above action levels, if preferential pathways exist and if potential receptors are present. Symbiont utilized this guidance and compared groundwater concentrations to applicable guideline values to determine if further assessment was required.


Section 4.0 INVESTIGATION RESULTS

The following section summarizes investigation results. Photodocumentation of field activities is included in Appendix A. 4.1 SOIL Laboratory analytical results for soil samples are summarized in Table 1A and 1B and contained in Appendix B. Future Site plans include either re-use as an industrial property or re-purposing as a recreational area or green space. As such, Table 1A compares detected soil concentrations to IDEM RISC IDCLs. Table 1B compares detected soil concentrations to IDEM Interim Recreational Nondefault Closure Levels. IDCL exceedances are presented on Figure 3. Recreational Nondefault Closure Levels are presented on Figure 4. Soil boring logs are presented in Appendix C. Soil descriptions (e.g., gross lithology, grain size, moisture content) and field observations (e.g., noted staining or odors) were described on the log for each boring. Industrial Default Closure Exceedances IDEM RISC IDCLs were exceeded at seven sample locations; TW/SB-2, TW/SB-4, SB-8, SB-10, SB-12, SB-13 and TW/SB-16; exceedances are summarized below.

The RISC IDCL for lead was exceeded at sample location TW/SB-2 (360 mg/kg), a boring located adjacent to the former Pattern Shop. The sample result exceeded the Industrial Migration to Groundwater Pathway Closure Level of 230 mg/kg. All soil samples collected at the Site had concentrations reported below the Industrial Soil Direct Contact Closure Level for lead (1300 mg/kg).

The RISC IDCL for arsenic was exceeded at seven locations distributed across the Site; TW/SB-2, TW/SB-4, SB-8, SB-10, SB-12, SB-13 and TW/SB-16, with detected concentrations ranging from 2.9 to 18.5 mg/kg. All seven sample results for arsenic exceeded the Industrial Migration to Groundwater Pathway Closure Level (5.8 mg/kg). All samples collected from the Site were below the Industrial Soil Direct Contact Closure Level for arsenic (20 mg/kg).

The RISC IDCL for benzo(a)pyrene was exceeded at sample location SB-10, a boring installed to document the soil quality of a large pile of apparent foundry sand located on the eastern portion of the property. The sample result exceeded the Industrial Direct Contact Closure Level of 1.5 mg/kg.


Interim Recreational Nondefault Closure Exceedances Because future Site plans may include re-purposing the Site to be a recreational area or greenspace, soil sample results were compared to IDEM’s RISC Interim Recreational Nondefault Closure Levels. IDEM developed these closure levels for a recreational soil direct contact exposure scenario, only. IDEM RISC Interim Recreational Nondefault Closure Levels were exceeded at three locations; TW/SB-2, SB-8 and SB-10; exceedances are summarized below.

The RISC Interim Recreational Nondefault Closure Level for arsenic (13 mg/kg) was exceeded at TW/SB-2, a boring installed adjacent to the former pattern shop.

The RISC Interim Recreational Nondefault Closure Level for benzo(a)pyrene (0.51 mg/kg) was exceeded at sample locations SB-8 and SB-10; borings that were installed to document the soil quality of a large pile of foundry sand located on the eastern portion of the Site.

The RISC Interim Recreational Nondefault Closure Level (0.51 mg/kg) for dibenzo(a,h)anthracene was exceeded at sample location SB-10.

4.2 WATER TABLE DEPTH, ELEVATION AND FLOW DIRECTIONS Water levels were measured on September 9, 2010 at eight temporary monitoring wells installed at the Site. Water level data collected from the wells are summarized in Table 2. The depth to water ranged from 15.32 to 19.71 feet bgs. General groundwater flow at the Site appears to be to the northeast (Figure 5) towards the White River. 4.3 GROUNDWATER 4.3.1 Field Water Quality Water quality field parameters including visual and olfactory observations are summarized in Table 2. All parameters including: temperature, pH, DO, specific conductivity, and ORP appeared typical of ambient groundwater. 4.3.2 Temporary Monitoring Wells Laboratory analytical results for on-site groundwater samples are summarized in Table 3, presented on Figure 6 and included in Appendix B. Groundwater samples were collected from eight temporary well locations and sent to the laboratory for PAH, VOC, and/or RCRA metals analysis. Analytical results were compared to their respective IDEM RISC IDCLs. IDEM RISC IDCL exceedances were detected at two sampling locations; TW-1 (lead and arsenic) and TW/SB-4 (arsenic), which are monitoring wells located in the west central portion of the property adjacent to the main foundry building, downgradient of a suspected UST location and adjacent to the former Test Lab. The samples appeared slightly turbid in the field indicating


that exceedances may be the result of colloidal material present within the groundwater sample (unfiltered). Chromium, 1,2,4-Trimethylbenzene and benzene were also detected in the sample collected from TW-1 at concentrations which exceeded their respective RISC Residential Default Closure Levels, but were below RISC IDCLs. Neither, VOCs or PAHs were detected above RISC IDCLs in any groundwater samples collected from the Site. 4.4 VAPOR As stated above, 1,2,4-trimethylbenzene and benzene were detected in a groundwater sample (TW-1) collected from the Site. In accordance with IDEMs Draft Vapor Intrusion Pilot Program Guidance (2006) and February 4, 2010 Draft Vapor Intrusion Pilot Program Guidance Supplement, the potential for vapor intrusion to impact the air quality in current or future buildings at the Site should be evaluated. 4.4.1 Soil Screening VOCs were not detected in soil samples collected from the Site. As such, the source of VOC detections in a groundwater sample collected from TW-1, remains undefined. 4.4.2 Groundwater Screening 1,2,4-trimethylbenzene, was detected in a groundwater sample collected from TW-1. However, no screening criteria have been established for that analyte in IDEMs Draft Vapor Intrusion Pilot Program Guidance (2006 and 2010). Benzene was detected at the same location at a concentration of 29 microgram per liter (ug/L). The benzene groundwater screening level for industrial/commercial properties with loamy soil and a water table greater than 15 ft bgs, as presented in Appendix V of IDEMs Vapor Guidance, is 2800 g/L. The concentration of benzene detected in groundwater collected from TW-1, 29 g/L, is several orders of magnitude less than the IDEM groundwater screening level for industrial/commercial properties (IDEM, 2006 and 2010). 4.4.3 Summary Based on comparison of groundwater concentrations detected to IDEM Industrial Groundwater Screening Levels, the potential for indoor air samples to exceed Occupational Safety and Health Administration (OSHA) standards for industrial properties is unlikely. Based on IDEMs sequential method, further vapor intrusion assessment does not appear warranted at this time.


Section 5.0 CONCLUSIONS AND RECOMMENDATIONS

The Site specific Phase II ESA Sampling and Analysis Plan was developed for the Site and had two main objectives:

1. Evaluate current hydrogeologic conditions at the Site. 2. Evaluate current soil and groundwater quality at the Site based on the RECs and PECs

identified during the Phase I ESA. 5.1 CONCLUSIONS Based on the results of the Phase II ESA, the following conclusions are made. 5.1.1 Soil Soil samples were collected from 12 locations across the Site. Select soil samples were sent to the laboratory and analyzed for PCBs, PAHs, VOCs and/or RCRA metals. Future Site plans include either re-use as an industrial property or re-purposing as a recreational area or green space. As such, soil concentrations detected at the Site were compared with both IDEM RISC IDCL and Interim Recreational Nondefault Closure Levels. Exceedances are summarized below. Industrial Closure Level Exceedances IDEM RISC IDCLs were exceeded at seven sample locations; TW/SB-2, TW/SB-4, SB-8, SB-10, SB-12, SB-13 and TW/SB-16. The RISC IDCL for lead (230 milligrams per kilogram [mg/kg]) was exceeded at TW/SB-2, a soil boring installed adjacent to the former pattern shop. The RISC IDCL for arsenic (5.8 mg/kg) was exceeded at all seven locations; these locations are distributed across the site. The RISC IDCL for Benzo(a)pyrene (1.5 mg/kg) was exceeded at SB-10, a soil boring installed to document the soil quality of a large pile of apparent foundry sand located on the eastern portion of the Site. Interim Recreational Nondefault Closure Level Exceedances IDEM RISC Interim Recreational Nondefault Closure Levels were exceeded at three locations; TW/SB-2, SB-8 and SB-10. The RISC Interim Recreational Nondefault Closure Level for arsenic (13 mg/kg) was exceeded at TW/SB-2, a soil boring installed adjacent to the former pattern shop. The RISC Interim Recreational Nondefault Closure Level for Benzo(a)pyrene (0.51 mg/kg) was exceeded at SB-8 and SB-10. The RISC Interim Recreational Nondefault Closure Level for dibenzo(a,h)anthracene (0.51 mg/kg) was exceeded at SB-10. Both SB-8 and SB-10 were installed to document the soil quality of a large pile of apparent foundry sand located on the eastern portion of the site. It appears that the majority impacts to soil is a result of past foundry operational activities, disposal of foundry sand.


5.1.2 Groundwater The groundwater flow direction at the Site appears to be to the north/northeast. IDEM RISC IDCL exceedances were detected at two sampling locations, TW-1 and TW/SB-4, monitoring wells located in the west central portion of the property adjacent to the main foundry building, downgradient of a suspected underground storage tank location (TW-1) and adjacent to the former Test Lab (TW/SB-4). The RISC IDCL for lead (0.042 milligrams per liter [mg/L]) was exceeded at TW-1. The RISC IDCL for arsenic (0.01 mg/L) was exceeded at TW-1 and TW/SB-4. These samples appeared slightly turbid in the field indicating that colloidal material may be present within the groundwater sample (unfiltered). It appears that lead impacts to groundwater may be the result of a past release(s) from a historical UST. Arsenic concentrations in groundwater may be biased due to the presence of colloidal material in the sample collected. 5.1.3 Vapor Based on comparison of groundwater concentrations detected at the Site with Industrial Groundwater Screening Levels provided in IDEMs Draft Vapor Intrusion Guidance Documents, the potential for indoor or outdoor air samples to exceed OSHA standards for Industrial properties is unlikely. Based on IDEMs sequential method, further vapor intrusion assessment does not appear warranted at this time. 5.1.4 Potential Risks to Ecological and Human Health The following potential risks to ecological and human health have been identified as part of the Phase II ESA.

If the property is used for industrial purposes, benzo(a)pyrene concentrations in surface samples indicate that direct contact with contaminated soil at the Site may represent a risk to ecological and human health.

If the property is used for recreational purposes arsenic, benzo(a)pyrene and

dibenzo(a,h)anthracene concentrations in surface samples indicate that direct contact with contaminated soil at the Site may represent a risk to ecological and human health.

Contaminated groundwater has the potential to migrate to downgradient receptors. Contact with contaminated groundwater represents a potential risk to ecological and human health.

The apparent foundry waste; slag, cinders, and/or foundry sand, distributed across the eastern portions of the Site presents a potential risk to ecological and human health. In addition, the material represents industrial/solid waste which may require special handling if removed from the site.

The historical Site use included the handling of hazardous substances and petroleum

products. Chemical containers identified throughout the facility and buildings and property included paints, solvents, oils and other petroleum products. One UST were identified. Observation of several areas was limited due to the condition of many site


buildings storing debris and vegetative overgrowth. As such the potential for additional containers containing hazardous materials exists. The potential of a release for existing containers to the environment could present a risk to ecological or human health.

5.2 RECOMMENDATIONS Recommendations for future actions at the Site include, but are not limited to:

Based on future Site use, refine the extent of groundwater and soil impacts as part of a pre-design phase of the selected remediation strategy, as appropriate.

Determine if detected metal impacts in groundwater are due to the presence of colloidal material in the samples.

A formal inventory of miscellaneous containers and structures should be completed. A geophysical survey (e.g., ground penetrating radar, other) may be appropriate to evaluate the potential for additional USTs to be present. Proper characterization and proper removal/decontamination of UST(s), other containers, piping or structures currently present at the site that have the possibility of serving as a source for ongoing or future release to air, sediment, soil, surface water and/or groundwater should be completed.

Proper abandonment and/or rehabilitation of the on-site water supply well.

Proper characterization and handling of structures to include a survey and proper management of ACMs, lead-based paint, mercury and Freon containing equipment and other hazardous substances/materials as part of demolition/deconstruction or renovation of facility structures.

Confirm proper disposition of apparent foundry solid waste materials and debris present on the property with respect to soil quality standards and industrial/solid waste regulations.


Section 6.0 LIMITATIONS

The Phase II ESA for the Frank Foundries property (the Site) was performed in accordance with generally accepted practices for the environmental consulting profession when undertaking similar studies at the same time and in the same geographical area as the work conducted by Symbiont. Symbiont observed the degree of care and skill that are generally exercised by the profession under similar circumstances and conditions. No other warranty is expressed or implied. Symbiont’s observations, findings, and opinions should not be considered as scientific certainties, but only as opinion based upon our professional judgment concerning the significance of the data gathered during the course of this investigation. Specifically, Symbiont does not and cannot guarantee that the property contains no hazardous or toxic materials or other latent conditions beyond that observed by Symbiont during the course of the investigation. Additionally, due to limitations of the investigation process and the necessary use of data furnished by others, Symbiont cannot assume liability if actual conditions differ from the information presented in this report. This report and the findings contained herein shall not, in whole or in part, be disseminated nor used by any other party, in whole or in part, as such action may result in inaccuracies and/or misrepresentations concerning the information obtained by Symbiont.


Section 7.0 REFERENCES

American Society for Testing and Materials, “Standard Practice for Environmental Site

Assessments: Phase I Environmental Site Assessment Process,” ASTM Designation E 1527-05, published September 2006.

Environmental Data Resources, Certified Sanborn Map Report, former Frank Foundries Site –

2000 East 8th Street, Muncie, IN 47302; Inquiry No. 2253666.3s, June 25, 2008. Environmental Data Resources, The EDR Aerial Photo Decade Package, Former Frank

Foundries Site – 2000 East 8th Street, Muncie, IN 47302; Inquiry No. 2253666.5, June 25, 2008.

Environmental Data Resources, The EDR City Directory Abstract, Former Frank Foundries Site

– 2000 East 8th Street, Muncie, IN 47302; Inquiry No. 2253666.6, June 25, 2008. Environmental Data Resources, THE EDR Historical Topographic Map Report, Former Frank

Foundries Site – 2000 East 8th Street, Muncie, IN 47302; Inquiry No. 2253666.4, June 25, 2008.

Environmental Data Resources, The EDR Radius Map with Geocheck©, Former Frank

Foundries Site – 2000 East 8th Street, Muncie, IN 47302; Inquiry No. 2180627.2s, March 28, 2008.

Indiana Department of Environmental Management, 2006, Draft Vapor Intrusion Pilot Program

Guidance, April 26. Symbiont, 2008, Phase I Site Assessment, Former Frank Foundries, 2000/2001 East 8th Street,

Muncie, IN, Symbiont, West Allis, August. Web Sites Indiana Department of Natural Resources – http://www.in.gov/gis-dnr- web/website/DNR_WaterWells_II/viewer.htm Indiana Geological Survey GIS Atlas of Indiana – http://igs.indiana.edu/ National Wetland Inventory Map HTTP://WWW.FWS.GOV/WETLANDS/DATA/MAPPER.HTML

TABLES

TABLE 1ASOIL SAMPLING RESULTS

INDUSTRIAL DEFAULT CLOSURE LEVELSPHASE II ENVIRONMENTAL SITE ASSESSMENT

FORMER FRANK FOUNDRIES PROPERTYSYMBIONT PROJECT NO. W103820

Sample ID

Industrial Soil Direct

Industrial Migration to Groundwater

Industrial Default Closure Level

SB‐1 SB‐1 SB‐2 TW/SB‐2 TW/SB‐2 TW/SB‐3 TW/SB‐4 TW/SB‐4 TW/SB‐5 TW/SB‐6 SB‐7 SB‐7 SB‐8 SB‐10

Sample Date 8/31/2010 8/31/2010 8/31/2010 8/31/2010 8/31/2010 9/1/2010 8/31/2010 8/31/2010 9/9/2010 8/31/2010 8/31/2010 8/31/2010 9/9/2010 9/9/2010Sample Dpeth (ft bgs) 0‐0.5 13.0‐14.0 0.5‐1.0 8.0‐9.0 12.0‐13.0 2.0‐3.0 0.25‐1.0 12.0‐13.0 0.5‐1.0 5.0‐6.0 0‐1.0 5.0‐6.0 4.0‐5.0 4.0‐5.0RCRA MetalsArsenic mg/kg 20 5.8 5.8 4.3 NA 18.5 NA NA 2.9 10.5 NA NA NA NA NA 8.9 8.2Barium mg/kg 230000 17000 10000 15.4 NA 123 NA NA 64.7 66.1 NA NA NA NA NA 868 663Chromium mg/kg 1000000 10000 5.0 NA 15.5 NA NA 12.0 16.2 NA NA NA NA NA 15.9 14.8Lead mg/kg 1300 230 230 9.2 NA 360 NA NA 10.3 17.6 NA NA NA NA NA 171 169PAHs2‐Methylnaphthalene mg/kg 1600 42 42 <0.0281 NA NA 0.0916 NA <0.0293 <0.030 NA <0.0312 NA 0.431 NA 0.198 0.252Acenaphthene mg/kg 24000 1800 1800 <0.0281 NA NA 0.078 NA <0.0294 <0.031 NA <0.0312 NA <0.0261 NA <0.0260 <0.0261Acenaphthylene mg/kg 2800 180 180 <0.0281 NA NA <0.0285 NA <0.0295 <0.032 NA <0.0312 NA 0.152 NA 0.350 0.792Anthracene mg/kg 120000 36000 2000 <0.0281 NA NA 0.0588 NA <0.0296 <0.033 NA <0.0312 NA 0.0763 NA 0.197 0.511Benzo(a)anthracene mg/kg 15 62 15 0.194 NA NA <0.0285 NA <0.0297 <0.034 NA <0.0312 NA 0.098 NA 0.838 2.440Benzo(a)pyrene mg/kg 1.5 16 1.5 0.301 NA NA <0.0285 NA <0.0298 <0.035 NA <0.0312 NA 0.148 NA 0.832 2.270Benzo(b)fluoranthene mg/kg 15 190 15 0.322 NA NA <0.0285 NA <0.0299 <0.036 NA <0.0312 NA 0.155 NA 0.974 2.530Benzo(g,h,i)perylene mg/kg NE NE NE 0.253 NA NA <0.0285 NA <0.0300 <0.037 NA <0.0312 NA 0.291 NA 0.515 1.290Benzo(k)fluoranthene mg/kg 150 1900 150 0.251 NA NA <0.0285 NA <0.0301 <0.038 NA <0.0312 NA 0.163 NA 0.946 2.650Chrysene mg/kg 1500 6200 1500 0.245 NA NA <0.0285 NA <0.0302 <0.039 NA <0.0312 NA 0.280 NA 0.912 2.570Dibenz(a,h)anthracene mg/kg 1.5 60 1.5 0.124 NA NA <0.0285 NA <0.0303 <0.040 NA <0.0312 NA 0.053 NA 0.259 0.673Fluoranthene mg/kg 16000 18000 2000 0.176 NA NA <0.0285 NA <0.0304 <0.041 NA <0.0312 NA 0.44 NA 1.23 2.340Fluorene mg/kg 16000 2300 2000 <0.0281 NA NA 0.190 NA <0.0305 <0.042 NA <0.0312 NA 0.0316 NA 0.0314 0.0547Indeno(1,2,3‐cd)pyrene mg/kg 15 540 15 0.218 NA NA <0.0285 NA <0.0306 <0.043 NA <0.0312 NA 0.138 NA 0.525 1.340Naphthalene mg/kg 8000 170 170 <0.0281 NA NA 0.0396 NA <0.0307 <0.044 NA <0.0312 NA 0.591 NA 0.158 0.198Phenanthrene mg/kg 1200 170 170 0.0467 NA NA 0.376 NA <0.0308 <0.045 NA <0.0312 NA 0.488 NA 0.462 0.666Pyrene mg/kg 12000 13000 2000 0.200 NA NA 0.0357 NA <0.0309 <0.046 NA <0.0312 NA 0.365 NA 1.160 2.61PCB'sPCB‐1242 (Aroclor 1242) mg/kg 5.3 18 5.3 <0.0394 NA NA NA NA NA <0.0421 NA NA NA NA NA NA NAVOCsMultiple mg/kg Varies Varies Varies NA BDL NA NA BDL BDL BDL BDL BDL BDL NA BDL BDL BDL

Notes:PAH = Polycyclic Aromatic Hydrocarbon

VOC's = Volatile Organic CompoundsPCB = Polychlorinated biphenyls

RCRA = Resource Conservation and Recovery Actmg/kg = Milligram per kilogram

NE = Not EstablishedNA = Not AnalyzedBDL = Below Detection Limit

ft bgs = Feet Below Ground SurfaceSB = Soil Boring

1 of 2

TABLE 1ASOIL SAMPLING RESULTS

INDUSTRIAL DEFAULT CLOSURE LEVELSPHASE II ENVIRONMENTAL SITE ASSESSMENT


Sample ID

Industrial Soil Direct

Industrial Migration to Groundwater


Sample DateSample Dpeth (ft bgs)RCRA MetalsArsenic mg/kg 20 5.8 5.8Barium mg/kg 230000 17000 10000Chromium mg/kg 1000000 10000Lead mg/kg 1300 230 230PAHs2‐Methylnaphthalene mg/kg 1600 42 42Acenaphthene mg/kg 24000 1800 1800Acenaphthylene mg/kg 2800 180 180Anthracene mg/kg 120000 36000 2000Benzo(a)anthracene mg/kg 15 62 15Benzo(a)pyrene mg/kg 1.5 16 1.5Benzo(b)fluoranthene mg/kg 15 190 15Benzo(g,h,i)perylene mg/kg NE NE NEBenzo(k)fluoranthene mg/kg 150 1900 150Chrysene mg/kg 1500 6200 1500Dibenz(a,h)anthracene mg/kg 1.5 60 1.5Fluoranthene mg/kg 16000 18000 2000Fluorene mg/kg 16000 2300 2000Indeno(1,2,3‐cd)pyrene mg/kg 15 540 15Naphthalene mg/kg 8000 170 170Phenanthrene mg/kg 1200 170 170Pyrene mg/kg 12000 13000 2000PCB'sPCB‐1242 (Aroclor 1242) mg/kg 5.3 18 5.3VOCsMultiple mg/kg Varies Varies Varies

Notes:PAH = Polycyclic Aromatic Hydrocarbon


RCRA = Resource Conservation and Recovery Actmg/kg = Milligram per kilogram

NE = Not EstablishedNA = Not AnalyzedBDL = Below Detection Limit


SB‐11 SB‐12 SB‐13 SB‐13 SB‐15 TW/SB‐16 TW/SB‐16 TW/SB‐16

9/1/2010 9/1/2010 9/1/2010 9/1/2010 9/1/2010 8/31/2010 8/31/2010 8/31/20100.5‐1.0 0.5‐1.0 0.25‐0.5 4.0‐5.0 0.25‐0.5 0.0‐0.5 0.0‐0.25 4.0‐5.0

3.5 11.3 7.9 NA NA 10.6 NA NA19.9 54.8 69.5 NA NA 65.9 NA NA4.6 13.7 7.8 NA NA 18.7 NA NA10 36.2 19.9 NA NA 42.4 NA NA

0.0309 NA NA NA <0.0323 NA 0.144 NA<0.0302 NA NA NA <0.0323 NA <0.0262 NA<0.0302 NA NA NA <0.0323 NA <0.0262 NA<0.0302 NA NA NA <0.0323 NA <0.0262 NA0.0380 NA NA NA <0.0323 NA 0.0381 NA0.0465 NA NA NA <0.0323 NA 0.0366 NA0.0435 NA NA NA <0.0323 NA 0.0466 NA0.0308 NA NA NA <0.0323 NA 0.0342 NA0.0446 NA NA NA <0.0323 NA 0.0344 NA0.0531 NA NA NA <0.0323 NA 0.0599 NA<0.0302 NA NA NA <0.0323 NA <0.0262 NA0.0377 NA NA NA <0.0323 NA 0.077 NA<0.0302 NA NA NA <0.0323 NA <0.0262 NA<0.0302 NA NA NA <0.0323 NA <0.0262 NA0.0336 NA NA NA <0.0323 NA 0.174 NA<0.0302 NA NA NA <0.0323 NA 0.161 NA0.0440 NA NA NA <0.0323 NA 0.0644 NA

NA NA NA NA NA NA 0.297 NA

NA NA NA BDL BDL NA NA BDL

2 of 2

TABLE 1BSOIL SAMPLING RESULTS

RECREATIONAL NONDEFAULT CLOSURE LEVELSPHASE II ENVIRONMENTAL SITE ASSESSMENT


Sample ID

IDEM RISC Recreational Nondefault Closure Level

SB‐1 SB‐1 SB‐2 TW/SB‐2 TW/SB‐2 TW/SB‐3 TW/SB‐4 TW/SB‐4 TW/SB‐5 TW/SB‐6 SB‐7 SB‐7 SB‐8 SB‐10 SB‐11 SB‐12

Sample Date 8/31/2010 8/31/2010 8/31/2010 8/31/2010 8/31/2010 9/1/2010 8/31/2010 8/31/2010 9/9/2010 8/31/2010 8/31/2010 8/31/2010 9/9/2010 9/9/2010 9/1/2010 9/1/2010Sample Dpeth (ft bgs) 0‐0.5 13.0‐14.0 0.5‐1.0 8.0‐9.0 12.0‐13.0 2.0‐3.0 0.25‐1.0 12.0‐13.0 0.5‐1.0 5.0‐6.0 0‐1.0 5.0‐6.0 4.0‐5.0 4.0‐5.0 0.5‐1.0 0.5‐1.0RCRA MetalsArsenic mg/kg 13 4.3 NA 18.5 NA NA 2.9 10.5 NA NA NA NA NA 8.9 8.2 3.5 11.3Barium mg/kg 10000 15.4 NA 123 NA NA 64.7 66.1 NA NA NA NA NA 868 663 19.9 54.8Chromium mg/kg 10000 5.0 NA 15.5 NA NA 12.0 16.2 NA NA NA NA NA 15.9 14.8 4.6 13.7Lead mg/kg 400 9.2 NA 360 NA NA 10.3 17.6 NA NA NA NA NA 171 169 10 36.2PAHs2‐Methylnaphthalene mg/kg 1600 <0.0281 NA NA 0.0916 NA <0.0293 <0.030 NA <0.0312 NA 0.431 NA 0.198 0.252 0.0309 NAAcenaphthene mg/kg 6000 <0.0281 NA NA 0.078 NA <0.0294 <0.031 NA <0.0312 NA <0.0261 NA <0.0260 <0.0261 <0.0302 NAAcenaphthylene mg/kg 2800 <0.0281 NA NA <0.0285 NA <0.0295 <0.032 NA <0.0312 NA 0.152 NA 0.350 0.792 <0.0302 NAAnthracene mg/kg 6000 <0.0281 NA NA 0.0588 NA <0.0296 <0.033 NA <0.0312 NA 0.0763 NA 0.197 0.511 <0.0302 NABenzo(a)anthracene mg/kg 5.1 0.194 NA NA <0.0285 NA <0.0297 <0.034 NA <0.0312 NA 0.098 NA 0.838 2.440 0.0380 NABenzo(a)pyrene mg/kg 0.51 0.301 NA NA <0.0285 NA <0.0298 <0.035 NA <0.0312 NA 0.148 NA 0.832 2.270 0.0465 NABenzo(b)fluoranthene mg/kg 5.1 0.322 NA NA <0.0285 NA <0.0299 <0.036 NA <0.0312 NA 0.155 NA 0.974 2.530 0.0435 NABenzo(g,h,i)perylene mg/kg NE 0.253 NA NA <0.0285 NA <0.0300 <0.037 NA <0.0312 NA 0.291 NA 0.515 1.290 0.0308 NABenzo(k)fluoranthene mg/kg 51 0.251 NA NA <0.0285 NA <0.0301 <0.038 NA <0.0312 NA 0.163 NA 0.946 2.650 0.0446 NAChrysene mg/kg 510 0.245 NA NA <0.0285 NA <0.0302 <0.039 NA <0.0312 NA 0.280 NA 0.912 2.570 0.0531 NADibenz(a,h)anthracene mg/kg 0.51 0.124 NA NA <0.0285 NA <0.0303 <0.040 NA <0.0312 NA 0.053 NA 0.259 0.673 <0.0302 NAFluoranthene mg/kg 6000 0.176 NA NA <0.0285 NA <0.0304 <0.041 NA <0.0312 NA 0.44 NA 1.23 2.340 0.0377 NAFluorene mg/kg 6000 <0.0281 NA NA 0.190 NA <0.0305 <0.042 NA <0.0312 NA 0.0316 NA 0.0314 0.0547 <0.0302 NAIndeno(1,2,3‐cd)pyrene mg/kg 5.1 0.218 NA NA <0.0285 NA <0.0306 <0.043 NA <0.0312 NA 0.138 NA 0.525 1.340 <0.0302 NANaphthalene mg/kg 6000 <0.0281 NA NA 0.0396 NA <0.0307 <0.044 NA <0.0312 NA 0.591 NA 0.158 0.198 0.0336 NAPhenanthrene mg/kg 1200 0.0467 NA NA 0.376 NA <0.0308 <0.045 NA <0.0312 NA 0.488 NA 0.462 0.666 <0.0302 NAPyrene mg/kg 6000 0.200 NA NA 0.0357 NA <0.0309 <0.046 NA <0.0312 NA 0.365 NA 1.160 2.61 0.0440 NAPCBPCB‐1242 (Aroclor 1242) mg/kg NE <0.0394 NA NA NA NA NA <0.0421 NA NA NA NA NA NA NA NA NAVOCsMultiple mg/kg Varies NA BDL NA NA BDL BDL BDL BDL BDL BDL NA BDL BDL BDL NA NA

NotesPAH = Polycyclic Aromatic Hydrocarbon


RCRA = Resource Conservation & Recovery Act

mg/kg = Milligram per kilogramNE = Not EstablishedNA = Not AnalyzedBDL = Below Detection Limit


1 of 2

TABLE 1BSOIL SAMPLING RESULTS

RECREATIONAL NONDEFAULT CLOSURE LEVELSPHASE II ENVIRONMENTAL SITE ASSESSMENT


Sample ID

IDEM RISC Recreational Nondefault Closure Level

Sample DateSample Dpeth (ft bgs)RCRA MetalsArsenic mg/kg 13Barium mg/kg 10000Chromium mg/kg 10000Lead mg/kg 400PAHs2‐Methylnaphthalene mg/kg 1600Acenaphthene mg/kg 6000Acenaphthylene mg/kg 2800Anthracene mg/kg 6000Benzo(a)anthracene mg/kg 5.1Benzo(a)pyrene mg/kg 0.51Benzo(b)fluoranthene mg/kg 5.1Benzo(g,h,i)perylene mg/kg NEBenzo(k)fluoranthene mg/kg 51Chrysene mg/kg 510Dibenz(a,h)anthracene mg/kg 0.51Fluoranthene mg/kg 6000Fluorene mg/kg 6000Indeno(1,2,3‐cd)pyrene mg/kg 5.1Naphthalene mg/kg 6000Phenanthrene mg/kg 1200Pyrene mg/kg 6000PCBPCB‐1242 (Aroclor 1242) mg/kg NEVOCsMultiple mg/kg Varies

NotesPAH = Polycyclic Aromatic Hydrocarbon


RCRA = Resource Conservation & Recovery Act

mg/kg = Milligram per kilogramNE = Not EstablishedNA = Not AnalyzedBDL = Below Detection Limit


SB‐13 SB‐13 SB‐15 TW/SB‐16 TW/SB‐16 TW/SB‐16

9/1/2010 9/1/2010 9/1/2010 8/31/2010 8/31/2010 8/31/20100.25‐0.5 4.0‐5.0 0.25‐0.5 0.0‐0.5 0.0‐0.25 4.0‐5.0

7.9 NA NA 10.6 NA NA69.5 NA NA 65.9 NA NA7.8 NA NA 18.7 NA NA19.9 NA NA 42.4 NA NA

NA NA <0.0323 NA 0.144 NANA NA <0.0323 NA <0.0262 NANA NA <0.0323 NA <0.0262 NANA NA <0.0323 NA <0.0262 NANA NA <0.0323 NA 0.0381 NANA NA <0.0323 NA 0.0366 NANA NA <0.0323 NA 0.0466 NANA NA <0.0323 NA 0.0342 NANA NA <0.0323 NA 0.0344 NANA NA <0.0323 NA 0.0599 NANA NA <0.0323 NA <0.0262 NANA NA <0.0323 NA 0.077 NANA NA <0.0323 NA <0.0262 NANA NA <0.0323 NA <0.0262 NANA NA <0.0323 NA 0.174 NANA NA <0.0323 NA 0.161 NANA NA <0.0323 NA 0.0644 NA

NA NA NA NA 0.297 NA

NA BDL BDL NA NA BDL

2 of 2

TABLE 2WATER QUALITY AND ELEVAION DATA

PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER FRANK FOUNDRIES PROPERTYSYMBIONT PROJECT NO. W103820

Sample ID TW‐1 TW/SB‐2* TW/SB‐3 TW/SB‐4 TW/SB‐5 TW/SB‐6 TW/SB‐14* TW/SB‐16

Field Measurements2

Top of Casing Elevation1 81.03 80.10 79.53 79.91 80.00 74.24 82.60 83.29

Ground Surface1 80.13 79.79 79.53 79.58 79.61 73.47 80.09 81.48Depth to Water (ft) 18.30 18.17 19.10 18.20 20.10 16.09 20.70 20.50Depth to Bottom (ft) 34.72 34.04 25.62 34.52 34.51 33.77 24.52 29.42

Groundwater Elevation1 62.73 61.93 60.43 61.71 59.90 58.15 61.90 62.79

Field Water Quality Data2

Temperature (oC) 12.93 16.63 13.07 13.75 16.6 15.31 15.2 15.21Specific Conductance (uS/cm) 893 837 900 784 768 878 1127 999Dissolved Oxygen (mg/L) 0.83 0.73 0.23 3.21 0.24 0.2 0.43 1.56pH 7.14 7.23 7.21 7.16 7.37 7.34 7.61 7.16Oxidation Reduction Potential (mV) ‐151.3 ‐242.4 ‐157.8 ‐146.9 ‐173.3 ‐188 ‐207.7 ‐137.8Color Clear Clear Clear Clear Clear Clear Clear Clear

OdorSlight Petroleum

Like OdorNo No No No

Slight Petroleum Like Odor

No No

Turbidity Low Low Low Low Low Low Low Low

Explanation:* Field Measurements made on 9/1/2010 1 Elevations measured to Site‐specific datum (North Rim of manhole located in 8th Street entrance).2 Field Measurements made on 9/9/2010

oC = Degrees CelsiusuS/cm = Microsiemens Per Centimetermg/L = Milligrams Per LitermV = millivoltTW = Temporary WellSB = Soil Boringft = Feet

1 OF 1

TABLE 3GROUNDWATER SAMPLING RESULTSINDUSTRIAL DEFAULT CLOSURE LEVELS

PHASE II ENVIRONMENTAL SITE ASSESSMENTFORMER FRANK FOUNDRIES PROPERTYSYMBIONT PROJECT NO. W103820

RCRA Metals (mg/L)Arsenic 0.01 0.0957 <0.01 NA 0.0112 NA NA <0.01 <0.01Barium 20 0.924 0.227 NA 0.307 NA NA 0.144 <0.1Cadmium 0.051 <0.005 <0.005 NA <0.005 NA NA <0.005 <0.005Chromium 150 0.106 <0.01 NA 0.0178 NA NA <0.01 <0.01Lead 0.042 0.104 <0.01 NA 0.0200 NA NA <0.01 <0.01Mercury 0.031 <0.002 <0.01 NA <0.01 NA NA <0.01 <0.01Selenium 0.51 <0.010 <0.05 NA <0.05 NA NA <0.05 <0.05Silver 0.51 <0.050 <0.002 NA <0.002 NA NA <0.002 <0.002PAHs (µg/L)2‐Methylnaphthalene 410 <1.2 <1.1 <1.1 <1.3 <1.1 <1.1 <1.1 <1.1Acenaphthene 6100 <1.2 <1.1 <1.1 <1.3 <1.1 <1.1 <1.1 <1.1Acenaphthylene 730 <1.2 <1.1 <1.1 <1.3 <1.1 <1.1 <1.1 <1.1Anthracene 31000 <0.12 <0.11 <0.11 <0.13 <0.11 0.37 <0.11 <0.11Benz(a)anthracene 3.9 <0.12 <0.11 <0.11 <0.13 <0.11 0.30 <0.11 <0.11Benzo(a)pyrene 0.39 <0.12 <0.11 <0.11 <0.13 <0.11 0.17 <0.11 <0.11Benzo(b)fluoranthene 3.9 <0.12 <0.11 <0.11 <0.13 <0.11 <0.11 <0.11 <0.11Benzo(g,h,i)perylene NE <0.12 <0.11 <0.11 <0.13 <0.11 0.14 <0.11 <0.11Benzo(k)fluoranthene 39 <0.12 <0.11 <0.11 <0.13 <0.11 <0.11 <0.11 <0.11Chrysene 390 <0.59 <0.56 <0.56 <0.63 <0.54 <0.53 <0.57 <0.57Dibenz(a,h)anthracene 0.39 <0.12 <0.11 <0.11 <0.13 <0.11 <0.11 <0.11 <0.11Fluoranthene 4100 <1.2 <1.1 <1.1 <1.3 <1.1 <1.1 <1.1 <1.1Fluorene 4100 <1.2 <1.1 <1.1 <1.3 <1.1 <1.1 <1.1 <1.1Indeno(1,2,3‐cd)pyrene 3.9 <0.12 <0.11 <0.11 <0.13 <0.11 <0.11 <0.11 <0.11Naphthalene 2000 1.6 <1.1 <1.1 <1.3 <1.1 <1.1 <1.1 <1.1Phenanthrene 310 <1.2 <1.1 <1.1 <1.3 <1.1 2.5 <1.1 <1.1Pyrene 3100 <1.2 <1.1 <1.1 <1.3 <1.1 1.1 <1.1 <1.1VOCs (µg/L)1,2,4‐Trimethylbenzene 5100 23.9 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.001,3,5‐Trimethylbenzene 5100 6.1 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00Benzene 52 29.0 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00Ethylbenzene 10000 24.4 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00n‐Hexane 9500 12.3 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00Toluene 8200 51.5 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00Xylenes, Total 20000 105 < 10.0 < 10.0 < 10.0 < 10.0 < 10.0 < 10.0 < 10.0

Explanation:PAH = Polycyclic Aromatic HydrocarbonVOCs = Volatile Organic CompoundsRCRA = Resource Conservation & Recovery Act

TW/SB = Temporary Wellmg/L = milligrams per liter µg/L = micrograms per liter


9/9/2010 9/9/2010 9/9/2010 9/9/2010

TW/SB‐14TW/SB‐5TW/SB‐3Sample ID

Sample Date

TW‐1 TW/SB‐16

9/9/2010

TW/SB‐6

9/9/2010

TW/SB‐4

9/9/20109/9/2010

TW/SB‐2

1 of 1

FIGURES

MODIFIED FROMU.S.G.S 7.5'

MUNCIE EAST & MUNCIEWEST QUADRANGLES0 0.5 10.25

Miles

0 3,000 6,0001,500Feet

SCALE

CONTOUR INTERVAL 10 FEETNATIONAL GEODETIC VERTICAL

QUADRANGLE LOCATION

INDIANA

Figure 1Site Location and Local TopographyFormer Frank Foundries2000-2100 South 8th St, Muncie, IN, 47302

³

Source:Indiana Spatial Data ServicesDownloaded March, 2008

FORMER FRANK FOUNDRIES2000-2100 SOUTH 8TH STREET

MJM

G:\Pro jects\Muncie, City of\W083470\Map Documents\Site No. 4 – Former Frank Foundries\2- sitebasemap.mxd

CITY OF MUNCIE, INDIANAPHASE II ENVIRONMENTAL

SITE ASSESSMENTFORMER FRANK FOUNDRIES2000-2100 EAST 8TH STREET

MUNCIE, IN, 47302

Figure 2 Site Basemap October 2010

SCALE

DWG

DATE

PROJNO.

6737 West Washington StreetSuite 3440West Allis, Wisconsin 53214414.291.8840FAX 414.291.8841

SGH

DSGN:

DR:

CHK:

APVD:

@A

@A

@A

@A

ED

@A

@A

@A

ED

ED

@A

ED

ED

ED

ED

SB-7

SB-8

TW-1

SB-1

SB-11

SB-10SB-12

SB-13

TW/SB-6

TW/SB-4

TW/SB-2

TW/SB-3

TW/SB-5

TW/SB-16

TW-14/SB-15

³

1 inch = 75 feet

SB-13

TW-1

0 25 50 75 FeetLegend

ED Soil Boring Location

@A Temporary Well Location

Parcel Boundary

Inferred Groundwater Flow Direction

MJM

G:\Pro jects\Muncie, City of\W083470\Map Documents\Site No. 4 – Former Frank Foundries\2.mxd


SITE ASSESSMENTFORMER FRANK FOUNDRIES

2000/2100 EAST 8TH STREETMUNCIE, IN, 47302

Figure 3Detected Constituents

of Concern in Soil Samples - Industrial Default Closure Levels

October 2010

SCALE

DWG

DATE

PROJNO.


SGH

DSGN:

DR:

CHK:

APVD:

@A

@A

@A

@A

ED

@A

@A

@A

ED

ED

@A

ED

ED

ED

ED

SB-7

SB-8

TW-1

SB-1

SB-11

SB-10SB-12

SB-13

TW/SB-6

TW/SB-4

TW/SB-2

TW/SB-3

TW/SB-5

TW/SB-16

TW-14/SB-15

³

1 inch = 75 feet

Sample Depth (ft bgs) 0.25‐1.0 12.0‐13.0

Arsenic 10.5 NABarium 66.1 NAChromium 16.2 NALead 17.6 NA

SB‐4

RCRA Metals (mg/kg)

Sample Depth (ft bgs) 0.5‐1.0

Arsenic 3.5Barium 19.9Chromium 4.6Lead 10

2‐Methylnaphthalene 0.0309Benzo(a)anthracene 0.0380Benzo(a)pyrene 0.0465Benzo(b)fluoranthene 0.0435Benzo(g,h,i)perylene 0.0308Benzo(k)fluoranthene 0.0446Chrysene 0.0531Fluoranthene 0.0377Naphthalene 0.0336Pyrene 0.0440

RCRA Metals (mg/kg)

PAHs (mg/kg)

SB‐11


Arsenic 11.3Barium 54.8Chromium 13.7Lead 36.2

SB‐12

RCRA Metals (mg/kg)Sample Depth (ft bgs) 0.25‐0.5 4.0‐5.0


SB‐13

RCRA Metals (mg/kg)

Sample Depth (ft bgs) 0.0‐0.5 0.0‐0.25 4.0‐5.0

Arsenic 10.6 NA NABarium 65.9 NA NAChromium 18.7 NA NALead 42.4 NA NA

2‐Methylnaphthalene NA 0.1440 NABenzo(a)anthracene NA 0.0381 NABenzo(a)pyrene NA 0.0366 NABenzo(b)fluoranthene NA 0.0466 NABenzo(g,h,i) perylene NA 0.0342 NABenzo(k)fluoranthene NA 0.0344 NAChrysene NA 0.0599 NAFluoranthene NA 0.0770 NANaphthalene NA 0.1740 NAPhenanthrene NA 0.1610 NAPyrene NA 0.0644 NA

PCB‐1242 (Aroclor 1242) NA 0.2970 NAPCBs (mg/kg)

RCRA Metals (mg/kg)

PAHs (mg/kg)

TW/SB‐16

Note:Values highlighted in orange indicateIndustrial Default Closure Level exceedances.

Legend



Parcel Boundary

0 25 50 75 Feet

SB-13

TW-1

Sample Depth (ft bgs) 0‐0.5 13.0‐14.0

Arsenic 4.3 NABarium 15.4 NAChromium 5 NALead 9.2 NA

Benzo(a)anthracene 0.194 NABenzo(a)pyrene 0.301 NABenzo(b)fluoranthene 0.322 NABenzo(g,h,i)perylene 0.253 NABenzo(k)fluoranthene 0.251 NAChrysene 0.245 NADibenz(a,h)anthracene 0.124 NAFluoranthene 0.176 NAIndeno(1,2,3‐cd)pyrene 0.218 NAPhenanthrene 0.467 NAPyrene 0.200 NA

SB‐1

RCRA Metals (mg/kg)

PAHs (mg/kg)

Sample Depth ( ft bgs) 0.5‐1.0 8.0‐9.0 12.0‐13.0

Arsenic 18.5 NA NABarium 123 NA NAChromium 15.5 NA NALead 360 NA NA

2‐Methylnaphthalene NA 0.916 NAAcenaphthene NA 0.708 NAAnthracene NA 0.588 NAFluorene NA 0.19 NANaphthalene NA 0.396 NAPhenanthrene NA 0.376 NAPyrene NA 0.357 NA

PAHs (mg/kg)

TW/SB‐2

RCRA Metals (mg/kg)


Arsenic 2.9Barium 64.7Chromium 12Lead 10.3

TW/SB‐3R

RCRA Metals (mg/kg)


2‐Methylnaphthalene 0.431 NAAcenaphthylene 0.152 NAAnthracene 0.0763 NABenzo(a)anthracene 0.0908 NABenzo(a)pyrene 0.148 NABenzo(b)fluoranthene 0.155 NABenzo(g,h,i)perylene 0.291 NABenzo(k)fluoranthene 0.163 NAChrysene 0.280 NADibenz(a,h)anthracene 0.530 NAFluoranthene 0.440 NAFluorene 0.316 NAIndeno(1,2,3‐cd)pyrene 0.138 NANaphthalene 0.591 NAPhenanthrene 0.488 NAPyrene 0.365 NA

SB‐7

PAHs (mg/kg)


Arsenic 8.9Barium 868Chromium 15.9Lead 171

2‐Methylnaphthalene 0.198Acenaphthylene 0.350Anthracene 0.197Benzo(a)anthracene 0.838Benzo(a)pyrene 0.832Benzo(b)fluoranthene 0.974Benzo(g,h,i)perylene 0.515Benzo(k)fluoranthene 0.946Chrysene 0.912Dibenz(a,h)anthracene 0.259Fluoranthene 1.230Fluorene 0.0314Indeno(1,2,3‐cd)pyrene 0.525Naphthalene 0.158Phenanthrene 0.462Pyrene 1.160

SB‐8

RCRA Metals (mg/kg)

PAHs (mg/kg)




SB‐10

RCRA Metals (mg/kg)

PAHs (mg/kg)

MJM




MUNCIE, IN, 47302

Figure 4Detected Constituents of Concern

in Soil Samples - Recreational Nondefault

Closure LevelsOctober 2010

SCALE

DWG

DATE

PROJNO.


SGH

DSGN:

DR:

CHK:

APVD:

@A

@A

@A

@A

ED

@A

@A

@A

ED

ED

@A

ED

ED

ED

ED

SB-7

SB-8

TW-1

SB-1

SB-11

SB-10SB-12

SB-13

TW/SB-6

TW/SB-4

TW/SB-2

TW/SB-3

TW/SB-5

TW/SB-16

TW-14/SB-15

³

1 inch = 75 feet


Arsenic 3.5Barium 19.9Chromium 4.6Lead 10

2‐Methylnaphthalene 0.0309Benzo(a)anthracene 0.0380Benzo(a)pyrene 0.0465Benzo(b)fluoranthene 0.0435Benzo(g,h,i)perylene 0.0308Benzo(k)fluoranthene 0.0446Chrysene 0.0531Fluoranthene 0.0377Naphthalene 0.0336Pyrene 0.0440

RCRA Metals (mg/kg)

PAHs (mg/kg)

SB‐11

Note:Values highlighted in green indicatesRecreational Nondefault Closure Level exceedances.

Legend



Parcel Boundary

0 25 50 75 Feet

SB-13

TW-1


Arsenic 4.3 NABarium 15.4 NAChromium 5 NALead 9.2 NA

Benzo(a)anthracene 0.194 NABenzo(a)pyrene 0.301 NABenzo(b)fluoranthene 0.322 NABenzo(g,h,i)perylene 0.253 NABenzo(k)fluoranthene 0.251 NAChrysene 0.245 NADibenz(a,h)anthracene 0.124 NAFluoranthene 0.176 NAIndeno(1,2,3‐cd)pyrene 0.218 NAPhenanthrene 0.467 NAPyrene 0.200 NA

SB‐1

RCRA Metals (mg/kg)

PAHs (mg/kg)


Arsenic 2.9Barium 64.7Chromium 12Lead 10.3

TW/SB‐3R

RCRA Metals (mg/kg)


2‐Methylnaphthalene 0.431 NAAcenaphthylene 0.152 NAAnthracene 0.0763 NABenzo(a)anthracene 0.0908 NABenzo(a)pyrene 0.148 NABenzo(b)fluoranthene 0.155 NABenzo(g,h,i)perylene 0.291 NABenzo(k)fluoranthene 0.163 NAChrysene 0.280 NADibenz(a,h)anthracene 0.530 NAFluoranthene 0.440 NAFluorene 0.316 NAIndeno(1,2,3‐cd)pyrene 0.138 NANaphthalene 0.591 NAPhenanthrene 0.488 NAPyrene 0.365 NA

SB‐7

PAHs (mg/kg)


Arsenic 18.5 NA NABarium 123 NA NAChromium 15.5 NA NALead 360 NA NA

2‐Methylnaphthalene NA 0.916 NAAcenaphthene NA 0.708 NAAnthracene NA 0.588 NAFluorene NA 0.19 NANaphthalene NA 0.396 NAPhenanthrene NA 0.376 NAPyrene NA 0.357 NA

TW/SB‐2

RCRA Metals (mg/kg)

PAHs (mg/kg)

Sample Depth (ft bgs) 0.25‐1.0 12.0‐13.0


SB‐4

RCRA Metals (mg/kg)




SB‐8

RCRA Metals (mg/kg)

PAHs (mg/kg)




PAHs (mg/kg)

SB‐10

RCRA Metals (mg/kg)



RCRA Metals (mg/kg)

SB‐12Sample Depth (ft bgs) 0.25‐0.5 4.0‐5.0


SB‐13

RCRA Metals (mg/kg)


Arsenic 10.6 NA NABarium 65.9 NA NAChromium 18.7 NA NALead 42.4 NA NA

2‐Methylnaphthalene NA 0.1440 NABenzo(a)anthracene NA 0.0381 NABenzo(a)pyrene NA 0.0366 NABenzo(b)fluoranthene NA 0.0466 NABenzo(g,h,i)perylene NA 0.0342 NABenzo(k)fluoranthene NA 0.0344 NAChrysene NA 0.0599 NAFluoranthene NA 0.0770 NANaphthalene NA 0.1740 NAPhenanthrene NA 0.1610 NAPyrene NA 0.0644 NA

PCB‐1242 (Aroclor 1242) NA 0.2970 NA

PAHs (mg/kg)

PCBs (mg/kg)

TW/SB‐16

RCRA Metals (mg/kg)

MJM




MUNCIE, IN, 47302

Figure 5Potentiometric Surface Map

(09/09/2010)October 2010

SCALE

DWG

DATE

PROJNO.


SGH

DSGN:

DR:

CHK:

APVD:

@A

@A

@A

@A

ED

@A

@A

@A

ED

ED

@A

ED

ED

ED

ED

61

62

61.5

60

62.5

60.5

SB-7

SB-8

TW-1

SB-1

SB-11

SB-10SB-12

SB-13

TW/SB-6TW/SB-2

TW/SB-3

TW/SB-5

TW/SB-16

TW-14/SB-15

61.9

59.9

58.15

62.79

62.73

61.93

60.43

TW/SB-4

³

1 inch = 75 feet

Note: All Measurements are in feet above mean sea level (AMSL)

SB-13

TW-1

0 25 50 75 FeetLegend



Groundwater Contour - Inferred

Groundwater Contour - Known

Parcel Boundary

Inferred Groundwater Flow Direction

MJM

G:\Pro jects\Muncie, City of\W083470\Map Documents\Site No. 4 – Former Frank Foundries\3-gw.mxd



MUNCIE, IN, 47302

Figure 6Detected Constituents

of Concearn in GroundwaterOctober 2010

SCALE

DWG

DATE

PROJNO.


SGH

DSGN:

DR:

CHK:

APVD:

@A

@A

@A

@A

ED

@A

@A

@A

ED

ED

@A

ED

ED

ED

ED

SB-7

SB-8

TW-1

SB-1

SB-11

SB-10SB-12

SB-13

TW/SB-6

TW/SB-4

TW/SB-2

TW/SB-3

TW/SB-5

TW/SB-16

TW-14/SB-15

³

1 inch = 75 feet

Barium 0.227

TW/SB‐2RCRA Metals (mg/L)

Anthracene 0.37Benz(a)anthracene 0.3Benzo(a)pyrene 0.17Benzo(g,h,i)perylene 0.14Phenanthrene 2.5Pyrene 1.1

TW/SB‐6PAHs (µg/L)

Note:Values highlighted in orange indicatesIndustrial Default Closure Level exceedances.

Legend



Parcel Boundary

SB-13

TW-1

0 25 50 75 Feet

Barium 0.144

TW‐14/SB‐15RCRA Metals (mg/L)


Naphthalene 1.6

1,2,4‐Trimethylbenzene 23.91,3,5‐Trimethylbenzene 6.1Benzene 29.0Ethylbenzene 24.4n‐Hexane 12.3Toluene 51.5Xylenes, Total 105

TW‐1RCRA Metals (mg/L)

PAHs (µg/L)

VOCs (µg/L)


TW/SB‐4RCRA Metals (mg/L)

APPENDICES

APPENDIX A

PHOTODOCUMENTATION OF FIELD ACTIVITIES

Looking N at S site entrance

Looking NE at S side of SE building

SW corner of site looking N along W property line

SW corner of site looking E along S property line

SE corner of site looking W at S property line

From S looking N over RR

From S looking N at start of foundry sand fill piles on Eside of property line

From S site boundary looking N along former S MuckAve

Looking N from E 8th St. at location of water supply

Looking S at location of TW-15

Overhead power at S site entrance

Looking E at small building located E of S site entrance

looking E from site entrance at drilling of TW-15

Drilling at TW-15

Looking SE at SE corner of SE bulding fondation atlocation of SB-13

Looking SE at SE building foundation

Tires on E side of SE building foundation

Looking W at E side of South Center Building

Looking W between main foundry building and S centerbuilding

Looking NW at SE corner of Main foundry building

Looking NE at SW corner of main foundry building

NE corner of Main Foundry building

Looking SW at NW corner of main foundry building

Transformers located on S side of main foundry building

Looking NE at SE corner of S center building

Looking NW from SE corner inside main foundry

Pits inside Main Foundry

Looking SE from NM corner inside main foundry

Remaining structure on NE corner of main foundrybuilding

Remaining structure along N side of main foundrybuilding

Looking E at W side entrance to main foundry building,UST left of entrance

Looking E at location of UST (gasoline)

Looking NE at S side of remaining portions of copula,remaining portions of elevator in background

Looking N from S over N central building foundation

Looking NE at NE corner of N building foundation atdrilling of TW-13

Looking S at N side of N center building

Looking SE at W side of test room

Looking W at SE entrance into pattern room and locationof TW-2

Looking N from SE corner of pattern room

Looking W at former location of AST (10,000 gallonsprinkler system tank)

Looking N at S side of NW building

Common demolition debris found throughout site

APPENDIX B

LABORATORY ANALYTICAL DATA

September 09, 2010

LIMS USE: FR - NICK LOHMANLIMS OBJECT ID: 5040885

5040885Project:Pace Project No.:

RE:

Mr. Nick LohmanSymbiont Science Engineering6737 W Washington StMilwaukee, WI 53214

Frank's Foundry

Dear Mr. Lohman:Enclosed are the analytical results for sample(s) received by the laboratory on September 01, 2010.The results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of thereport.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Mark Davis

[email protected] Manager

Illinois/NELAC Certification #: 100418Indiana Certification #: C-49-06Kansas Certification #: E-10247Kentucky Certification #: 0042Ohio VAP: CL0065Pennsylvania: 68-00791West Virginia Certification #: 330

Enclosures

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Page 1 of 61

Pace Analytical Services, Inc.7726 Moller Road

Indianapolis, IN 46268

(317)875-5894

SAMPLE SUMMARY

Pace Project No.:Project:

5040885Frank's Foundry

Lab ID Sample ID Matrix Date Collected Date Received

5040885001 SB-1 (0-0.5) Solid 08/31/10 10:35 09/01/10 11:48

5040885002 SB-1 (13-14) Solid 08/31/10 10:35 09/01/10 11:48

5040885003 SB-1 (13-14) FD Solid 08/31/10 10:35 09/01/10 11:48

5040885004 SB-2 (0.5-1) Solid 08/31/10 12:30 09/01/10 11:48

5040885005 SB-2 (8-9) Solid 08/31/10 12:30 09/01/10 11:48

5040885006 SB-2 (12-13) Solid 08/31/10 12:30 09/01/10 11:48

5040885007 SB-4 (0.25-1) Solid 08/31/10 11:30 09/01/10 11:48

5040885008 SB-4 (0.25-1) FD Solid 08/31/10 11:30 09/01/10 11:48

5040885009 SB-7 (0-1) Solid 08/31/10 17:30 09/01/10 11:48

5040885010 SB-7 (5-6) Solid 08/31/10 17:30 09/01/10 11:48

5040885011 SB-8 (0.5-1) Solid 08/31/10 17:30 09/01/10 11:48

5040885012 SB-6 (5-6) Solid 08/31/10 17:00 09/01/10 11:48

5040885013 TRIP BLANK Water 08/31/10 08:00 09/01/10 11:48

5040885014 SB-16 (0-0.25) Solid 08/31/10 10:00 09/01/10 11:48

5040885015 SB-16 (0-0.5) Solid 08/31/10 10:00 09/01/10 11:48

5040885016 SB-16 (4-5) Solid 08/31/10 10:00 09/01/10 11:48

5040885017 SB-4 (12-13) Solid 08/31/10 08:00 09/01/10 11:48



Page 2 of 61



(317)875-5894

SAMPLE ANALYTE COUNT



Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts

5040885001 SB-1 (0-0.5) EPA 8082 8 PASI-ILKC

EPA 6010 7 PASI-IFRW

EPA 7471 1 PASI-IRAK

EPA 8270 by SIM 19 PASI-ISRS

ASTM D2974-87 1 PASI-IJTP

5040885002 SB-1 (13-14) EPA 8260 72 PASI-IRSW


5040885003 SB-1 (13-14) FD EPA 8260 72 PASI-IRSW


5040885004 SB-2 (0.5-1) EPA 6010 7 PASI-IFRW



5040885005 SB-2 (8-9) EPA 8270 by SIM 19 PASI-ISRS


5040885006 SB-2 (12-13) EPA 8260 72 PASI-IRSW


5040885007 SB-4 (0.25-1) EPA 8082 8 PASI-ILKC




EPA 8260 72 PASI-IJLF


5040885008 SB-4 (0.25-1) FD EPA 8082 8 PASI-ILKC




EPA 8260 72 PASI-IJLF


5040885009 SB-7 (0-1) EPA 8270 by SIM 19 PASI-ISRS


5040885010 SB-7 (5-6) EPA 8260 72 PASI-IRSW


5040885012 SB-6 (5-6) EPA 8260 72 PASI-IRSW


5040885013 TRIP BLANK EPA 8260 73 PASI-IJLF

5040885014 SB-16 (0-0.25) EPA 8082 8 PASI-ILKC




Page 3 of 61



(317)875-5894






5040885015 SB-16 (0-0.5) EPA 6010 7 PASI-IFRW



5040885016 SB-16 (4-5) EPA 8260 72 PASI-IRSW


5040885017 SB-4 (12-13) EPA 8260 72 PASI-IRSW




Page 4 of 61



(317)875-5894

ANALYTICAL RESULTS



Sample: SB-1 (0-0.5) Lab ID: 5040885001 Collected: 08/31/10 10:35 Received: 09/01/10 11:48 Matrix: SolidResults reported on a "dry-weight" basis

Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit

8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546

PCB-1016 (Aroclor 1016) ND ug/kg 1 09/07/10 17:07 12674-11-208/07/10 00:0539.4PCB-1221 (Aroclor 1221) ND ug/kg 1 09/07/10 17:07 11104-28-208/07/10 00:0539.4PCB-1232 (Aroclor 1232) ND ug/kg 1 09/07/10 17:07 11141-16-508/07/10 00:0539.4PCB-1242 (Aroclor 1242) ND ug/kg 1 09/07/10 17:07 53469-21-908/07/10 00:0539.4PCB-1248 (Aroclor 1248) ND ug/kg 1 09/07/10 17:07 12672-29-608/07/10 00:0539.4PCB-1254 (Aroclor 1254) ND ug/kg 1 09/07/10 17:07 11097-69-108/07/10 00:0539.4PCB-1260 (Aroclor 1260) ND ug/kg 1 09/07/10 17:07 11096-82-508/07/10 00:0539.4Tetrachloro-m-xylene (S) 80 % 1 09/07/10 17:07 877-09-808/07/10 00:0520-130

6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050

Arsenic 4.3 mg/kg 1 09/07/10 12:25 7440-38-209/02/10 00:002.1Barium 15.4 mg/kg 1 09/07/10 12:25 7440-39-309/02/10 00:002.1Cadmium ND mg/kg 1 09/07/10 12:25 7440-43-909/02/10 00:002.1Chromium 5.0 mg/kg 1 09/07/10 12:25 7440-47-309/02/10 00:002.1Lead 9.2 mg/kg 1 09/07/10 12:25 7439-92-109/02/10 00:002.1Selenium ND mg/kg 1 09/07/10 12:25 7782-49-209/02/10 00:002.1Silver ND mg/kg 1 09/07/10 12:25 7440-22-409/02/10 00:002.1

7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471

Mercury ND mg/kg 1 09/08/10 12:56 7439-97-609/03/10 00:000.39

8270 MSSV PAH by SIM 5ML Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3546

Acenaphthene ND ug/kg 1 09/02/10 10:05 83-32-909/01/10 21:4528.1Acenaphthylene ND ug/kg 1 09/02/10 10:05 208-96-809/01/10 21:4528.1Anthracene ND ug/kg 1 09/02/10 10:05 120-12-709/01/10 21:4528.1Benzo(a)anthracene 194 ug/kg 1 09/02/10 10:05 56-55-309/01/10 21:4528.1Benzo(a)pyrene 301 ug/kg 1 09/02/10 10:05 50-32-809/01/10 21:4528.1Benzo(b)fluoranthene 322 ug/kg 1 09/02/10 10:05 205-99-209/01/10 21:4528.1Benzo(g,h,i)perylene 253 ug/kg 1 09/02/10 10:05 191-24-209/01/10 21:4528.1Benzo(k)fluoranthene 251 ug/kg 1 09/02/10 10:05 207-08-909/01/10 21:4528.1Chrysene 245 ug/kg 1 09/02/10 10:05 218-01-909/01/10 21:4528.1Dibenz(a,h)anthracene 124 ug/kg 1 09/02/10 10:05 53-70-309/01/10 21:4528.1Fluoranthene 176 ug/kg 1 09/02/10 10:05 206-44-009/01/10 21:4528.1Fluorene ND ug/kg 1 09/02/10 10:05 86-73-709/01/10 21:4528.1Indeno(1,2,3-cd)pyrene 218 ug/kg 1 09/02/10 10:05 193-39-509/01/10 21:4528.12-Methylnaphthalene ND ug/kg 1 09/02/10 10:05 91-57-609/01/10 21:4528.1Naphthalene ND ug/kg 1 09/02/10 10:05 91-20-309/01/10 21:4528.1Phenanthrene 46.7 ug/kg 1 09/02/10 10:05 85-01-809/01/10 21:4528.1Pyrene 200 ug/kg 1 09/02/10 10:05 129-00-009/01/10 21:4528.12-Fluorobiphenyl (S) 85 % 1 09/02/10 10:05 321-60-809/01/10 21:4545-120Terphenyl-d14 (S) 84 % 1 09/02/10 10:05 1718-51-009/01/10 21:4541-120

Percent Moisture Analytical Method: ASTM D2974-87

Percent Moisture 11.1 % 1 09/03/10 14:300.10



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ANALYTICAL RESULTS



Sample: SB-1 (13-14) Lab ID: 5040885002 Collected: 08/31/10 10:35 Received: 09/01/10 11:48 Matrix: SolidResults reported on a "dry-weight" basis


8260 MSV 5035A VOA Analytical Method: EPA 8260

Acetone ND ug/kg 1 09/07/10 20:50 67-64-192.6Acrolein ND ug/kg 1 09/07/10 20:50 107-02-892.6Acrylonitrile ND ug/kg 1 09/07/10 20:50 107-13-192.6Benzene ND ug/kg 1 09/07/10 20:50 71-43-24.6Bromobenzene ND ug/kg 1 09/07/10 20:50 108-86-14.6Bromochloromethane ND ug/kg 1 09/07/10 20:50 74-97-54.6Bromodichloromethane ND ug/kg 1 09/07/10 20:50 75-27-44.6Bromoform ND ug/kg 1 09/07/10 20:50 75-25-24.6Bromomethane ND ug/kg 1 09/07/10 20:50 74-83-94.62-Butanone (MEK) ND ug/kg 1 09/07/10 20:50 78-93-323.2n-Butylbenzene ND ug/kg 1 09/07/10 20:50 104-51-84.6sec-Butylbenzene ND ug/kg 1 09/07/10 20:50 135-98-84.6tert-Butylbenzene ND ug/kg 1 09/07/10 20:50 98-06-64.6Carbon disulfide ND ug/kg 1 09/07/10 20:50 75-15-09.3Carbon tetrachloride ND ug/kg 1 09/07/10 20:50 56-23-54.6Chlorobenzene ND ug/kg 1 09/07/10 20:50 108-90-74.6Chloroethane ND ug/kg 1 09/07/10 20:50 75-00-34.6Chloroform ND ug/kg 1 09/07/10 20:50 67-66-34.6Chloromethane ND ug/kg 1 09/07/10 20:50 74-87-34.62-Chlorotoluene ND ug/kg 1 09/07/10 20:50 95-49-84.64-Chlorotoluene ND ug/kg 1 09/07/10 20:50 106-43-44.6Dibromochloromethane ND ug/kg 1 09/07/10 20:50 124-48-14.61,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 20:50 106-93-44.6Dibromomethane ND ug/kg 1 09/07/10 20:50 74-95-34.61,2-Dichlorobenzene ND ug/kg 1 09/07/10 20:50 95-50-14.61,3-Dichlorobenzene ND ug/kg 1 09/07/10 20:50 541-73-14.61,4-Dichlorobenzene ND ug/kg 1 09/07/10 20:50 106-46-74.6trans-1,4-Dichloro-2-butene ND ug/kg 1 09/07/10 20:50 110-57-692.6Dichlorodifluoromethane ND ug/kg 1 09/07/10 20:50 75-71-84.61,1-Dichloroethane ND ug/kg 1 09/07/10 20:50 75-34-34.61,2-Dichloroethane ND ug/kg 1 09/07/10 20:50 107-06-24.61,1-Dichloroethene ND ug/kg 1 09/07/10 20:50 75-35-44.6cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 20:50 156-59-24.6trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 20:50 156-60-54.61,2-Dichloropropane ND ug/kg 1 09/07/10 20:50 78-87-54.61,3-Dichloropropane ND ug/kg 1 09/07/10 20:50 142-28-94.62,2-Dichloropropane ND ug/kg 1 09/07/10 20:50 594-20-74.61,1-Dichloropropene ND ug/kg 1 09/07/10 20:50 563-58-64.6cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 20:50 10061-01-54.6trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 20:50 10061-02-64.6Ethylbenzene ND ug/kg 1 09/07/10 20:50 100-41-44.6Ethyl methacrylate ND ug/kg 1 09/07/10 20:50 97-63-29.3Hexachloro-1,3-butadiene ND ug/kg 1 09/07/10 20:50 87-68-34.62-Hexanone ND ug/kg 1 09/07/10 20:50 591-78-692.6Iodomethane ND ug/kg 1 09/07/10 20:50 74-88-492.6Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 20:50 98-82-84.6



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ANALYTICAL RESULTS






p-Isopropyltoluene ND ug/kg 1 09/07/10 20:50 99-87-64.6Methylene chloride ND ug/kg 1 09/07/10 20:50 75-09-218.54-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 20:50 108-10-123.2Methyl-tert-butyl ether ND ug/kg 1 09/07/10 20:50 1634-04-44.6Naphthalene ND ug/kg 1 09/07/10 20:50 91-20-34.6n-Propylbenzene ND ug/kg 1 09/07/10 20:50 103-65-14.6Styrene ND ug/kg 1 09/07/10 20:50 100-42-54.61,1,1,2-Tetrachloroethane ND ug/kg 1 09/07/10 20:50 630-20-64.61,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 20:50 79-34-54.6Tetrachloroethene ND ug/kg 1 09/07/10 20:50 127-18-44.6Toluene ND ug/kg 1 09/07/10 20:50 108-88-34.61,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 20:50 87-61-64.61,2,4-Trichlorobenzene ND ug/kg 1 09/07/10 20:50 120-82-14.61,1,1-Trichloroethane ND ug/kg 1 09/07/10 20:50 71-55-64.61,1,2-Trichloroethane ND ug/kg 1 09/07/10 20:50 79-00-54.6Trichloroethene ND ug/kg 1 09/07/10 20:50 79-01-64.6Trichlorofluoromethane ND ug/kg 1 09/07/10 20:50 75-69-44.61,2,3-Trichloropropane ND ug/kg 1 09/07/10 20:50 96-18-44.61,2,4-Trimethylbenzene ND ug/kg 1 09/07/10 20:50 95-63-64.61,3,5-Trimethylbenzene ND ug/kg 1 09/07/10 20:50 108-67-84.6Vinyl acetate ND ug/kg 1 09/07/10 20:50 108-05-492.6Vinyl chloride ND ug/kg 1 09/07/10 20:50 75-01-44.6Xylene (Total) ND ug/kg 1 09/07/10 20:50 1330-20-79.3Dibromofluoromethane (S) 101 % 1 09/07/10 20:50 1868-53-780-124Toluene-d8 (S) 104 % 1 09/07/10 20:50 2037-26-558-1454-Bromofluorobenzene (S) 103 % 1 09/07/10 20:50 460-00-461-131





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ANALYTICAL RESULTS



Sample: SB-1 (13-14) FD Lab ID: 5040885003 Collected: 08/31/10 10:35 Received: 09/01/10 11:48 Matrix: SolidResults reported on a "dry-weight" basis






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ANALYTICAL RESULTS



Sample: SB-1 (13-14) FD Lab ID: 5040885003 Collected: 08/31/10 10:35 Received: 09/01/10 11:48 Matrix: SolidResults reported on a "dry-weight" basis








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(317)875-5894

ANALYTICAL RESULTS



Sample: SB-2 (0.5-1) Lab ID: 5040885004 Collected: 08/31/10 12:30 Received: 09/01/10 11:48 Matrix: SolidResults reported on a "dry-weight" basis



Arsenic 18.5 mg/kg 1 09/07/10 12:39 7440-38-209/02/10 00:002.2Barium 123 mg/kg 1 09/07/10 12:39 7440-39-309/02/10 00:002.2Cadmium ND mg/kg 1 09/07/10 12:39 7440-43-909/02/10 00:002.2Chromium 15.5 mg/kg 1 09/07/10 12:39 7440-47-309/02/10 00:002.2Lead 360 mg/kg 1 09/07/10 12:39 7439-92-109/02/10 00:002.2Selenium ND mg/kg 1 09/07/10 12:39 7782-49-209/02/10 00:002.2Silver ND mg/kg 1 09/07/10 12:39 7440-22-409/02/10 00:002.2


Mercury ND mg/kg 1 09/08/10 12:57 7439-97-609/03/10 00:000.41





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ANALYTICAL RESULTS






Acenaphthene 70.8 ug/kg 1 09/02/10 10:23 83-32-909/01/10 21:4528.5Acenaphthylene ND ug/kg 1 09/02/10 10:23 208-96-809/01/10 21:4528.5Anthracene 58.8 ug/kg 1 09/02/10 10:23 120-12-709/01/10 21:4528.5Benzo(a)anthracene ND ug/kg 1 09/02/10 10:23 56-55-309/01/10 21:4528.5Benzo(a)pyrene ND ug/kg 1 09/02/10 10:23 50-32-809/01/10 21:4528.5Benzo(b)fluoranthene ND ug/kg 1 09/02/10 10:23 205-99-209/01/10 21:4528.5Benzo(g,h,i)perylene ND ug/kg 1 09/02/10 10:23 191-24-209/01/10 21:4528.5Benzo(k)fluoranthene ND ug/kg 1 09/02/10 10:23 207-08-909/01/10 21:4528.5Chrysene ND ug/kg 1 09/02/10 10:23 218-01-909/01/10 21:4528.5Dibenz(a,h)anthracene ND ug/kg 1 09/02/10 10:23 53-70-309/01/10 21:4528.5Fluoranthene ND ug/kg 1 09/02/10 10:23 206-44-009/01/10 21:4528.5Fluorene 190 ug/kg 1 09/02/10 10:23 86-73-709/01/10 21:4528.5Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/02/10 10:23 193-39-509/01/10 21:4528.52-Methylnaphthalene 91.6 ug/kg 1 09/02/10 10:23 91-57-609/01/10 21:4528.5Naphthalene 39.6 ug/kg 1 09/02/10 10:23 91-20-309/01/10 21:4528.5Phenanthrene 376 ug/kg 1 09/02/10 10:23 85-01-809/01/10 21:4528.5Pyrene 35.7 ug/kg 1 09/02/10 10:23 129-00-009/01/10 21:4528.52-Fluorobiphenyl (S) 83 % 1 09/02/10 10:23 321-60-809/01/10 21:4545-120Terphenyl-d14 (S) 89 % 1 09/02/10 10:23 1718-51-009/01/10 21:4541-120





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Mercury ND mg/kg 1 09/08/10 12:59 7439-97-609/03/10 00:000.39


Acenaphthene ND ug/kg 1 09/02/10 10:41 83-32-909/01/10 21:4530.0Acenaphthylene ND ug/kg 1 09/02/10 10:41 208-96-809/01/10 21:4530.0Anthracene ND ug/kg 1 09/02/10 10:41 120-12-709/01/10 21:4530.0Benzo(a)anthracene ND ug/kg 1 09/02/10 10:41 56-55-309/01/10 21:4530.0Benzo(a)pyrene ND ug/kg 1 09/02/10 10:41 50-32-809/01/10 21:4530.0Benzo(b)fluoranthene ND ug/kg 1 09/02/10 10:41 205-99-209/01/10 21:4530.0Benzo(g,h,i)perylene ND ug/kg 1 09/02/10 10:41 191-24-209/01/10 21:4530.0Benzo(k)fluoranthene ND ug/kg 1 09/02/10 10:41 207-08-909/01/10 21:4530.0Chrysene ND ug/kg 1 09/02/10 10:41 218-01-909/01/10 21:4530.0Dibenz(a,h)anthracene ND ug/kg 1 09/02/10 10:41 53-70-309/01/10 21:4530.0Fluoranthene ND ug/kg 1 09/02/10 10:41 206-44-009/01/10 21:4530.0Fluorene ND ug/kg 1 09/02/10 10:41 86-73-709/01/10 21:4530.0Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/02/10 10:41 193-39-509/01/10 21:4530.02-Methylnaphthalene ND ug/kg 1 09/02/10 10:41 91-57-609/01/10 21:4530.0Naphthalene ND ug/kg 1 09/02/10 10:41 91-20-309/01/10 21:4530.0Phenanthrene ND ug/kg 1 09/02/10 10:41 85-01-809/01/10 21:4530.0Pyrene ND ug/kg 1 09/02/10 10:41 129-00-009/01/10 21:4530.02-Fluorobiphenyl (S) 85 % 1 09/02/10 10:41 321-60-809/01/10 21:4545-120Terphenyl-d14 (S) 77 % 1 09/02/10 10:41 1718-51-009/01/10 21:4541-120

8260 MSV 5030 Low Level Analytical Method: EPA 8260

Acetone ND ug/kg 1 09/07/10 17:53 67-64-1120Acrolein ND ug/kg 1 09/07/10 17:53 107-02-8120



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ANALYTICAL RESULTS






Acrylonitrile ND ug/kg 1 09/07/10 17:53 107-13-1120Benzene ND ug/kg 1 09/07/10 17:53 71-43-26.0Bromobenzene ND ug/kg 1 09/07/10 17:53 108-86-16.0Bromochloromethane ND ug/kg 1 09/07/10 17:53 74-97-56.0Bromodichloromethane ND ug/kg 1 09/07/10 17:53 75-27-46.0Bromoform ND ug/kg 1 09/07/10 17:53 75-25-26.0Bromomethane ND ug/kg 1 09/07/10 17:53 74-83-96.02-Butanone (MEK) ND ug/kg 1 09/07/10 17:53 78-93-330.0n-Butylbenzene ND ug/kg 1 09/07/10 17:53 104-51-86.0sec-Butylbenzene ND ug/kg 1 09/07/10 17:53 135-98-86.0tert-Butylbenzene ND ug/kg 1 09/07/10 17:53 98-06-66.0Carbon disulfide ND ug/kg 1 09/07/10 17:53 75-15-012.0Carbon tetrachloride ND ug/kg 1 09/07/10 17:53 56-23-56.0Chlorobenzene ND ug/kg 1 09/07/10 17:53 108-90-76.0Chloroethane ND ug/kg 1 09/07/10 17:53 75-00-36.0Chloroform ND ug/kg 1 09/07/10 17:53 67-66-36.0Chloromethane ND ug/kg 1 09/07/10 17:53 74-87-36.02-Chlorotoluene ND ug/kg 1 09/07/10 17:53 95-49-86.04-Chlorotoluene ND ug/kg 1 09/07/10 17:53 106-43-46.0Dibromochloromethane ND ug/kg 1 09/07/10 17:53 124-48-16.01,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 17:53 106-93-46.0Dibromomethane ND ug/kg 1 09/07/10 17:53 74-95-36.01,2-Dichlorobenzene ND ug/kg 1 09/07/10 17:53 95-50-16.01,3-Dichlorobenzene ND ug/kg 1 09/07/10 17:53 541-73-16.01,4-Dichlorobenzene ND ug/kg 1 09/07/10 17:53 106-46-76.0trans-1,4-Dichloro-2-butene ND ug/kg 1 09/07/10 17:53 110-57-6120Dichlorodifluoromethane ND ug/kg 1 09/07/10 17:53 75-71-86.01,1-Dichloroethane ND ug/kg 1 09/07/10 17:53 75-34-36.01,2-Dichloroethane ND ug/kg 1 09/07/10 17:53 107-06-26.01,1-Dichloroethene ND ug/kg 1 09/07/10 17:53 75-35-46.0cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 17:53 156-59-26.0trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 17:53 156-60-56.01,2-Dichloropropane ND ug/kg 1 09/07/10 17:53 78-87-56.01,3-Dichloropropane ND ug/kg 1 09/07/10 17:53 142-28-96.02,2-Dichloropropane ND ug/kg 1 09/07/10 17:53 594-20-76.01,1-Dichloropropene ND ug/kg 1 09/07/10 17:53 563-58-66.0cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 17:53 10061-01-56.0trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 17:53 10061-02-66.0Ethylbenzene ND ug/kg 1 09/07/10 17:53 100-41-46.0Ethyl methacrylate ND ug/kg 1 09/07/10 17:53 97-63-212.0Hexachloro-1,3-butadiene ND ug/kg 1 09/07/10 17:53 87-68-36.02-Hexanone ND ug/kg 1 09/07/10 17:53 591-78-6120Iodomethane ND ug/kg 1 09/07/10 17:53 74-88-4120Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 17:53 98-82-86.0p-Isopropyltoluene ND ug/kg 1 09/07/10 17:53 99-87-66.0Methylene chloride ND ug/kg 1 09/07/10 17:53 75-09-224.0



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4-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 17:53 108-10-130.0Methyl-tert-butyl ether ND ug/kg 1 09/07/10 17:53 1634-04-46.0Naphthalene ND ug/kg 1 09/07/10 17:53 91-20-36.0n-Propylbenzene ND ug/kg 1 09/07/10 17:53 103-65-16.0Styrene ND ug/kg 1 09/07/10 17:53 100-42-56.01,1,1,2-Tetrachloroethane ND ug/kg 1 09/07/10 17:53 630-20-66.01,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 17:53 79-34-56.0Tetrachloroethene ND ug/kg 1 09/07/10 17:53 127-18-46.0Toluene ND ug/kg 1 09/07/10 17:53 108-88-36.01,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 17:53 87-61-66.01,2,4-Trichlorobenzene ND ug/kg 1 09/07/10 17:53 120-82-16.01,1,1-Trichloroethane ND ug/kg 1 09/07/10 17:53 71-55-66.01,1,2-Trichloroethane ND ug/kg 1 09/07/10 17:53 79-00-56.0Trichloroethene ND ug/kg 1 09/07/10 17:53 79-01-66.0Trichlorofluoromethane ND ug/kg 1 09/07/10 17:53 75-69-46.01,2,3-Trichloropropane ND ug/kg 1 09/07/10 17:53 96-18-46.01,2,4-Trimethylbenzene ND ug/kg 1 09/07/10 17:53 95-63-66.01,3,5-Trimethylbenzene ND ug/kg 1 09/07/10 17:53 108-67-86.0Vinyl acetate ND ug/kg 1 09/07/10 17:53 108-05-4120Vinyl chloride ND ug/kg 1 09/07/10 17:53 75-01-46.0Xylene (Total) ND ug/kg 1 09/07/10 17:53 1330-20-712.0Dibromofluoromethane (S) 118 % 1 09/07/10 17:53 1868-53-780-124Toluene-d8 (S) 106 % 1 09/07/10 17:53 2037-26-558-1454-Bromofluorobenzene (S) 98 % 1 09/07/10 17:53 460-00-461-131





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Sample: SB-4 (0.25-1) FD Lab ID: 5040885008 Collected: 08/31/10 11:30 Received: 09/01/10 11:48 Matrix: SolidResults reported on a "dry-weight" basis







Mercury ND mg/kg 1 09/08/10 13:00 7439-97-609/03/10 00:000.42




Acetone ND ug/kg 1 09/07/10 18:30 67-64-1121Acrolein ND ug/kg 1 09/07/10 18:30 107-02-8121



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Acrylonitrile ND ug/kg 1 09/07/10 18:30 107-13-1121Benzene ND ug/kg 1 09/07/10 18:30 71-43-26.0Bromobenzene ND ug/kg 1 09/07/10 18:30 108-86-16.0Bromochloromethane ND ug/kg 1 09/07/10 18:30 74-97-56.0Bromodichloromethane ND ug/kg 1 09/07/10 18:30 75-27-46.0Bromoform ND ug/kg 1 09/07/10 18:30 75-25-26.0Bromomethane ND ug/kg 1 09/07/10 18:30 74-83-96.02-Butanone (MEK) ND ug/kg 1 09/07/10 18:30 78-93-330.2n-Butylbenzene ND ug/kg 1 09/07/10 18:30 104-51-86.0sec-Butylbenzene ND ug/kg 1 09/07/10 18:30 135-98-86.0tert-Butylbenzene ND ug/kg 1 09/07/10 18:30 98-06-66.0Carbon disulfide ND ug/kg 1 09/07/10 18:30 75-15-012.1Carbon tetrachloride ND ug/kg 1 09/07/10 18:30 56-23-56.0Chlorobenzene ND ug/kg 1 09/07/10 18:30 108-90-76.0Chloroethane ND ug/kg 1 09/07/10 18:30 75-00-36.0Chloroform ND ug/kg 1 09/07/10 18:30 67-66-36.0Chloromethane ND ug/kg 1 09/07/10 18:30 74-87-36.02-Chlorotoluene ND ug/kg 1 09/07/10 18:30 95-49-86.04-Chlorotoluene ND ug/kg 1 09/07/10 18:30 106-43-46.0Dibromochloromethane ND ug/kg 1 09/07/10 18:30 124-48-16.01,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 18:30 106-93-46.0Dibromomethane ND ug/kg 1 09/07/10 18:30 74-95-36.01,2-Dichlorobenzene ND ug/kg 1 09/07/10 18:30 95-50-16.01,3-Dichlorobenzene ND ug/kg 1 09/07/10 18:30 541-73-16.01,4-Dichlorobenzene ND ug/kg 1 09/07/10 18:30 106-46-76.0trans-1,4-Dichloro-2-butene ND ug/kg 1 09/07/10 18:30 110-57-6121Dichlorodifluoromethane ND ug/kg 1 09/07/10 18:30 75-71-86.01,1-Dichloroethane ND ug/kg 1 09/07/10 18:30 75-34-36.01,2-Dichloroethane ND ug/kg 1 09/07/10 18:30 107-06-26.01,1-Dichloroethene ND ug/kg 1 09/07/10 18:30 75-35-46.0cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 18:30 156-59-26.0trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 18:30 156-60-56.01,2-Dichloropropane ND ug/kg 1 09/07/10 18:30 78-87-56.01,3-Dichloropropane ND ug/kg 1 09/07/10 18:30 142-28-96.02,2-Dichloropropane ND ug/kg 1 09/07/10 18:30 594-20-76.01,1-Dichloropropene ND ug/kg 1 09/07/10 18:30 563-58-66.0cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 18:30 10061-01-56.0trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 18:30 10061-02-66.0Ethylbenzene ND ug/kg 1 09/07/10 18:30 100-41-46.0Ethyl methacrylate ND ug/kg 1 09/07/10 18:30 97-63-212.1Hexachloro-1,3-butadiene ND ug/kg 1 09/07/10 18:30 87-68-36.02-Hexanone ND ug/kg 1 09/07/10 18:30 591-78-6121Iodomethane ND ug/kg 1 09/07/10 18:30 74-88-4121Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 18:30 98-82-86.0p-Isopropyltoluene ND ug/kg 1 09/07/10 18:30 99-87-66.0Methylene chloride ND ug/kg 1 09/07/10 18:30 75-09-224.1



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ANALYTICAL RESULTS






4-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 18:30 108-10-130.2Methyl-tert-butyl ether ND ug/kg 1 09/07/10 18:30 1634-04-46.0Naphthalene ND ug/kg 1 09/07/10 18:30 91-20-36.0n-Propylbenzene ND ug/kg 1 09/07/10 18:30 103-65-16.0Styrene ND ug/kg 1 09/07/10 18:30 100-42-56.01,1,1,2-Tetrachloroethane ND ug/kg 1 09/07/10 18:30 630-20-66.01,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 18:30 79-34-56.0Tetrachloroethene ND ug/kg 1 09/07/10 18:30 127-18-46.0Toluene ND ug/kg 1 09/07/10 18:30 108-88-36.01,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 18:30 87-61-66.01,2,4-Trichlorobenzene ND ug/kg 1 09/07/10 18:30 120-82-16.01,1,1-Trichloroethane ND ug/kg 1 09/07/10 18:30 71-55-66.01,1,2-Trichloroethane ND ug/kg 1 09/07/10 18:30 79-00-56.0Trichloroethene ND ug/kg 1 09/07/10 18:30 79-01-66.0Trichlorofluoromethane ND ug/kg 1 09/07/10 18:30 75-69-46.01,2,3-Trichloropropane ND ug/kg 1 09/07/10 18:30 96-18-46.01,2,4-Trimethylbenzene ND ug/kg 1 09/07/10 18:30 95-63-66.01,3,5-Trimethylbenzene ND ug/kg 1 09/07/10 18:30 108-67-86.0Vinyl acetate ND ug/kg 1 09/07/10 18:30 108-05-4121Vinyl chloride ND ug/kg 1 09/07/10 18:30 75-01-46.0Xylene (Total) ND ug/kg 1 09/07/10 18:30 1330-20-712.1Dibromofluoromethane (S) 112 % 1 09/07/10 18:30 1868-53-780-124Toluene-d8 (S) 98 % 1 09/07/10 18:30 2037-26-558-1454-Bromofluorobenzene (S) 107 % 1 09/07/10 18:30 460-00-461-131





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ANALYTICAL RESULTS






Acenaphthene ND ug/kg 1 09/02/10 11:16 83-32-909/01/10 21:4526.1Acenaphthylene 152 ug/kg 1 09/02/10 11:16 208-96-809/01/10 21:4526.1Anthracene 76.3 ug/kg 1 09/02/10 11:16 120-12-709/01/10 21:4526.1Benzo(a)anthracene 90.8 ug/kg 1 09/02/10 11:16 56-55-309/01/10 21:4526.1Benzo(a)pyrene 148 ug/kg 1 09/02/10 11:16 50-32-809/01/10 21:4526.1Benzo(b)fluoranthene 155 ug/kg 1 09/02/10 11:16 205-99-209/01/10 21:4526.1Benzo(g,h,i)perylene 291 ug/kg 1 09/02/10 11:16 191-24-209/01/10 21:4526.1Benzo(k)fluoranthene 163 ug/kg 1 09/02/10 11:16 207-08-909/01/10 21:4526.1Chrysene 208 ug/kg 1 09/02/10 11:16 218-01-909/01/10 21:4526.1Dibenz(a,h)anthracene 50.3 ug/kg 1 09/02/10 11:16 53-70-309/01/10 21:4526.1Fluoranthene 440 ug/kg 1 09/02/10 11:16 206-44-009/01/10 21:4526.1Fluorene 31.6 ug/kg 1 09/02/10 11:16 86-73-709/01/10 21:4526.1Indeno(1,2,3-cd)pyrene 138 ug/kg 1 09/02/10 11:16 193-39-509/01/10 21:4526.12-Methylnaphthalene 431 ug/kg 1 09/02/10 11:16 91-57-609/01/10 21:4526.1Naphthalene 591 ug/kg 1 09/02/10 11:16 91-20-309/01/10 21:4526.1Phenanthrene 488 ug/kg 1 09/02/10 11:16 85-01-809/01/10 21:4526.1Pyrene 365 ug/kg 1 09/02/10 11:16 129-00-009/01/10 21:4526.12-Fluorobiphenyl (S) 53 % 1 09/02/10 11:16 321-60-809/01/10 21:4545-120Terphenyl-d14 (S) 55 % 1 09/02/10 11:16 1718-51-009/01/10 21:4541-120





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ANALYTICAL RESULTS






Acetone ND ug/kg 1 09/08/10 07:53 67-64-1112Acrolein ND ug/kg 1 09/08/10 07:53 107-02-8112Acrylonitrile ND ug/kg 1 09/08/10 07:53 107-13-1112Benzene ND ug/kg 1 09/08/10 07:53 71-43-25.6Bromobenzene ND ug/kg 1 09/08/10 07:53 108-86-15.6Bromochloromethane ND ug/kg 1 09/08/10 07:53 74-97-55.6Bromodichloromethane ND ug/kg 1 09/08/10 07:53 75-27-45.6Bromoform ND ug/kg 1 09/08/10 07:53 75-25-25.6Bromomethane ND ug/kg 1 09/08/10 07:53 74-83-95.62-Butanone (MEK) ND ug/kg 1 09/08/10 07:53 78-93-328.1n-Butylbenzene ND ug/kg 1 09/08/10 07:53 104-51-85.6sec-Butylbenzene ND ug/kg 1 09/08/10 07:53 135-98-85.6tert-Butylbenzene ND ug/kg 1 09/08/10 07:53 98-06-65.6Carbon disulfide ND ug/kg 1 09/08/10 07:53 75-15-011.2Carbon tetrachloride ND ug/kg 1 09/08/10 07:53 56-23-55.6Chlorobenzene ND ug/kg 1 09/08/10 07:53 108-90-75.6Chloroethane ND ug/kg 1 09/08/10 07:53 75-00-35.6Chloroform ND ug/kg 1 09/08/10 07:53 67-66-35.6Chloromethane ND ug/kg 1 09/08/10 07:53 74-87-35.62-Chlorotoluene ND ug/kg 1 09/08/10 07:53 95-49-85.64-Chlorotoluene ND ug/kg 1 09/08/10 07:53 106-43-45.6Dibromochloromethane ND ug/kg 1 09/08/10 07:53 124-48-15.61,2-Dibromoethane (EDB) ND ug/kg 1 09/08/10 07:53 106-93-45.6Dibromomethane ND ug/kg 1 09/08/10 07:53 74-95-35.61,2-Dichlorobenzene ND ug/kg 1 09/08/10 07:53 95-50-15.61,3-Dichlorobenzene ND ug/kg 1 09/08/10 07:53 541-73-15.61,4-Dichlorobenzene ND ug/kg 1 09/08/10 07:53 106-46-75.6trans-1,4-Dichloro-2-butene ND ug/kg 1 09/08/10 07:53 110-57-6112Dichlorodifluoromethane ND ug/kg 1 09/08/10 07:53 75-71-85.61,1-Dichloroethane ND ug/kg 1 09/08/10 07:53 75-34-35.61,2-Dichloroethane ND ug/kg 1 09/08/10 07:53 107-06-25.61,1-Dichloroethene ND ug/kg 1 09/08/10 07:53 75-35-45.6cis-1,2-Dichloroethene ND ug/kg 1 09/08/10 07:53 156-59-25.6trans-1,2-Dichloroethene ND ug/kg 1 09/08/10 07:53 156-60-55.61,2-Dichloropropane ND ug/kg 1 09/08/10 07:53 78-87-55.61,3-Dichloropropane ND ug/kg 1 09/08/10 07:53 142-28-95.62,2-Dichloropropane ND ug/kg 1 09/08/10 07:53 594-20-75.61,1-Dichloropropene ND ug/kg 1 09/08/10 07:53 563-58-65.6cis-1,3-Dichloropropene ND ug/kg 1 09/08/10 07:53 10061-01-55.6trans-1,3-Dichloropropene ND ug/kg 1 09/08/10 07:53 10061-02-65.6Ethylbenzene ND ug/kg 1 09/08/10 07:53 100-41-45.6Ethyl methacrylate ND ug/kg 1 09/08/10 07:53 97-63-211.2Hexachloro-1,3-butadiene ND ug/kg 1 09/08/10 07:53 87-68-35.62-Hexanone ND ug/kg 1 09/08/10 07:53 591-78-6112Iodomethane ND ug/kg 1 09/08/10 07:53 74-88-4112Isopropylbenzene (Cumene) ND ug/kg 1 09/08/10 07:53 98-82-85.6



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ANALYTICAL RESULTS






p-Isopropyltoluene ND ug/kg 1 09/08/10 07:53 99-87-65.6Methylene chloride ND ug/kg 1 09/08/10 07:53 75-09-222.54-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/08/10 07:53 108-10-128.1Methyl-tert-butyl ether ND ug/kg 1 09/08/10 07:53 1634-04-45.6Naphthalene ND ug/kg 1 09/08/10 07:53 91-20-35.6n-Propylbenzene ND ug/kg 1 09/08/10 07:53 103-65-15.6Styrene ND ug/kg 1 09/08/10 07:53 100-42-55.61,1,1,2-Tetrachloroethane ND ug/kg 1 09/08/10 07:53 630-20-65.61,1,2,2-Tetrachloroethane ND ug/kg 1 09/08/10 07:53 79-34-55.6Tetrachloroethene ND ug/kg 1 09/08/10 07:53 127-18-45.6Toluene ND ug/kg 1 09/08/10 07:53 108-88-35.61,2,3-Trichlorobenzene ND ug/kg 1 09/08/10 07:53 87-61-65.61,2,4-Trichlorobenzene ND ug/kg 1 09/08/10 07:53 120-82-15.61,1,1-Trichloroethane ND ug/kg 1 09/08/10 07:53 71-55-65.61,1,2-Trichloroethane ND ug/kg 1 09/08/10 07:53 79-00-55.6Trichloroethene ND ug/kg 1 09/08/10 07:53 79-01-65.6Trichlorofluoromethane ND ug/kg 1 09/08/10 07:53 75-69-45.61,2,3-Trichloropropane ND ug/kg 1 09/08/10 07:53 96-18-45.61,2,4-Trimethylbenzene ND ug/kg 1 09/08/10 07:53 95-63-65.61,3,5-Trimethylbenzene ND ug/kg 1 09/08/10 07:53 108-67-85.6Vinyl acetate ND ug/kg 1 09/08/10 07:53 108-05-4112Vinyl chloride ND ug/kg 1 09/08/10 07:53 75-01-45.6Xylene (Total) ND ug/kg 1 09/08/10 07:53 1330-20-711.2Dibromofluoromethane (S) 102 % 1 09/08/10 07:53 1868-53-780-124Toluene-d8 (S) 104 % 1 09/08/10 07:53 2037-26-558-1454-Bromofluorobenzene (S) 105 % 1 09/08/10 07:53 460-00-461-131





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Sample: TRIP BLANK Lab ID: 5040885013 Collected: 08/31/10 08:00 Received: 09/01/10 11:48 Matrix: Water


8260 MSV Analytical Method: EPA 8260

Acetone ND ug/L 1 09/07/10 21:56 67-64-1100Acrolein ND ug/L 1 09/07/10 21:56 107-02-850.0Acrylonitrile ND ug/L 1 09/07/10 21:56 107-13-1100Benzene ND ug/L 1 09/07/10 21:56 71-43-25.0Bromobenzene ND ug/L 1 09/07/10 21:56 108-86-15.0Bromochloromethane ND ug/L 1 09/07/10 21:56 74-97-55.0Bromodichloromethane ND ug/L 1 09/07/10 21:56 75-27-45.0Bromoform ND ug/L 1 09/07/10 21:56 75-25-25.0Bromomethane ND ug/L 1 09/07/10 21:56 74-83-95.02-Butanone (MEK) ND ug/L 1 09/07/10 21:56 78-93-325.0n-Butylbenzene ND ug/L 1 09/07/10 21:56 104-51-85.0sec-Butylbenzene ND ug/L 1 09/07/10 21:56 135-98-85.0tert-Butylbenzene ND ug/L 1 09/07/10 21:56 98-06-65.0Carbon disulfide ND ug/L 1 09/07/10 21:56 75-15-010.0Carbon tetrachloride ND ug/L 1 09/07/10 21:56 56-23-55.0Chlorobenzene ND ug/L 1 09/07/10 21:56 108-90-75.0Chloroethane ND ug/L 1 09/07/10 21:56 75-00-35.0Chloroform ND ug/L 1 09/07/10 21:56 67-66-35.0Chloromethane ND ug/L 1 09/07/10 21:56 74-87-35.02-Chlorotoluene ND ug/L 1 09/07/10 21:56 95-49-85.04-Chlorotoluene ND ug/L 1 09/07/10 21:56 106-43-45.0Dibromochloromethane ND ug/L 1 09/07/10 21:56 124-48-15.01,2-Dibromoethane (EDB) ND ug/L 1 09/07/10 21:56 106-93-45.0Dibromomethane ND ug/L 1 09/07/10 21:56 74-95-35.01,2-Dichlorobenzene ND ug/L 1 09/07/10 21:56 95-50-15.01,3-Dichlorobenzene ND ug/L 1 09/07/10 21:56 541-73-15.01,4-Dichlorobenzene ND ug/L 1 09/07/10 21:56 106-46-75.0trans-1,4-Dichloro-2-butene ND ug/L 1 09/07/10 21:56 110-57-6100Dichlorodifluoromethane ND ug/L 1 09/07/10 21:56 75-71-85.01,1-Dichloroethane ND ug/L 1 09/07/10 21:56 75-34-35.01,2-Dichloroethane ND ug/L 1 09/07/10 21:56 107-06-25.01,1-Dichloroethene ND ug/L 1 09/07/10 21:56 75-35-45.0cis-1,2-Dichloroethene ND ug/L 1 09/07/10 21:56 156-59-25.0trans-1,2-Dichloroethene ND ug/L 1 09/07/10 21:56 156-60-55.01,2-Dichloropropane ND ug/L 1 09/07/10 21:56 78-87-55.01,3-Dichloropropane ND ug/L 1 09/07/10 21:56 142-28-95.02,2-Dichloropropane ND ug/L 1 09/07/10 21:56 594-20-75.01,1-Dichloropropene ND ug/L 1 09/07/10 21:56 563-58-65.0cis-1,3-Dichloropropene ND ug/L 1 09/07/10 21:56 10061-01-55.0trans-1,3-Dichloropropene ND ug/L 1 09/07/10 21:56 10061-02-65.0Ethylbenzene ND ug/L 1 09/07/10 21:56 100-41-45.0Ethyl methacrylate ND ug/L 1 09/07/10 21:56 97-63-2100Hexachloro-1,3-butadiene ND ug/L 1 09/07/10 21:56 87-68-35.0n-Hexane ND ug/L 1 09/07/10 21:56 110-54-35.02-Hexanone ND ug/L 1 09/07/10 21:56 591-78-625.0Iodomethane ND ug/L 1 09/07/10 21:56 74-88-410.0Isopropylbenzene (Cumene) ND ug/L 1 09/07/10 21:56 98-82-85.0



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ANALYTICAL RESULTS






p-Isopropyltoluene ND ug/L 1 09/07/10 21:56 99-87-65.0Methylene chloride ND ug/L 1 09/07/10 21:56 75-09-25.04-Methyl-2-pentanone (MIBK) ND ug/L 1 09/07/10 21:56 108-10-125.0Methyl-tert-butyl ether ND ug/L 1 09/07/10 21:56 1634-04-44.0Naphthalene ND ug/L 1 09/07/10 21:56 91-20-35.0n-Propylbenzene ND ug/L 1 09/07/10 21:56 103-65-15.0Styrene ND ug/L 1 09/07/10 21:56 100-42-55.01,1,1,2-Tetrachloroethane ND ug/L 1 09/07/10 21:56 630-20-65.01,1,2,2-Tetrachloroethane ND ug/L 1 09/07/10 21:56 79-34-55.0Tetrachloroethene ND ug/L 1 09/07/10 21:56 127-18-45.0Toluene ND ug/L 1 09/07/10 21:56 108-88-35.01,2,3-Trichlorobenzene ND ug/L 1 09/07/10 21:56 87-61-65.01,2,4-Trichlorobenzene ND ug/L 1 09/07/10 21:56 120-82-15.01,1,1-Trichloroethane ND ug/L 1 09/07/10 21:56 71-55-65.01,1,2-Trichloroethane ND ug/L 1 09/07/10 21:56 79-00-55.0Trichloroethene ND ug/L 1 09/07/10 21:56 79-01-65.0Trichlorofluoromethane ND ug/L 1 09/07/10 21:56 75-69-45.01,2,3-Trichloropropane ND ug/L 1 09/07/10 21:56 96-18-45.01,2,4-Trimethylbenzene ND ug/L 1 09/07/10 21:56 95-63-65.01,3,5-Trimethylbenzene ND ug/L 1 09/07/10 21:56 108-67-85.0Vinyl acetate ND ug/L 1 09/07/10 21:56 108-05-410.0Vinyl chloride ND ug/L 1 09/07/10 21:56 75-01-42.0Xylene (Total) ND ug/L 1 09/07/10 21:56 1330-20-710.0Dibromofluoromethane (S) 101 % 1 09/07/10 21:56 1868-53-780-1234-Bromofluorobenzene (S) 100 % 1 09/07/10 21:56 460-00-470-126Toluene-d8 (S) 102 % 1 09/07/10 21:56 2037-26-580-116



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ANALYTICAL RESULTS






PCB-1016 (Aroclor 1016) ND ug/kg 1 09/08/10 20:19 12674-11-208/07/10 00:0573.4PCB-1221 (Aroclor 1221) ND ug/kg 1 09/08/10 20:19 11104-28-208/07/10 00:0573.4PCB-1232 (Aroclor 1232) ND ug/kg 1 09/08/10 20:19 11141-16-508/07/10 00:0573.4PCB-1242 (Aroclor 1242) 297 ug/kg 1 09/08/10 20:19 53469-21-908/07/10 00:0573.4PCB-1248 (Aroclor 1248) ND ug/kg 1 09/08/10 20:19 12672-29-608/07/10 00:0573.4PCB-1254 (Aroclor 1254) ND ug/kg 1 09/08/10 20:19 11097-69-108/07/10 00:0573.4PCB-1260 (Aroclor 1260) ND ug/kg 1 09/08/10 20:19 11096-82-508/07/10 00:0573.4Tetrachloro-m-xylene (S) 66 % 1 09/08/10 20:19 877-09-808/07/10 00:0520-130


Acenaphthene ND ug/kg 1 09/03/10 10:09 83-32-909/02/10 11:1026.2Acenaphthylene ND ug/kg 1 09/03/10 10:09 208-96-809/02/10 11:1026.2Anthracene ND ug/kg 1 09/03/10 10:09 120-12-709/02/10 11:1026.2Benzo(a)anthracene 38.1 ug/kg 1 09/03/10 10:09 56-55-309/02/10 11:1026.2Benzo(a)pyrene 36.6 ug/kg 1 09/03/10 10:09 50-32-809/02/10 11:1026.2Benzo(b)fluoranthene 46.6 ug/kg 1 09/03/10 10:09 205-99-209/02/10 11:1026.2Benzo(g,h,i)perylene 34.2 ug/kg 1 09/03/10 10:09 191-24-209/02/10 11:1026.2Benzo(k)fluoranthene 34.4 ug/kg 1 09/03/10 10:09 207-08-909/02/10 11:1026.2Chrysene 59.9 ug/kg 1 09/03/10 10:09 218-01-909/02/10 11:1026.2Dibenz(a,h)anthracene ND ug/kg 1 09/03/10 10:09 53-70-309/02/10 11:1026.2Fluoranthene 77.0 ug/kg 1 09/03/10 10:09 206-44-009/02/10 11:1026.2Fluorene ND ug/kg 1 09/03/10 10:09 86-73-709/02/10 11:1026.2Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/03/10 10:09 193-39-509/02/10 11:1026.22-Methylnaphthalene 144 ug/kg 1 09/03/10 10:09 91-57-609/02/10 11:1026.2Naphthalene 174 ug/kg 1 09/03/10 10:09 91-20-309/02/10 11:1026.2Phenanthrene 161 ug/kg 1 09/03/10 10:09 85-01-809/02/10 11:1026.2Pyrene 64.4 ug/kg 1 09/03/10 10:09 129-00-009/02/10 11:1026.22-Fluorobiphenyl (S) 78 % 1 09/03/10 10:09 321-60-809/02/10 11:1045-120Terphenyl-d14 (S) 77 % 1 09/03/10 10:09 1718-51-009/02/10 11:1041-120





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Mercury ND mg/kg 1 09/08/10 13:02 7439-97-609/03/10 00:000.37





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ANALYTICAL RESULTS









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ANALYTICAL RESULTS











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ANALYTICAL RESULTS









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ANALYTICAL RESULTS











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(317)875-5894

QUALITY CONTROL DATA



QC Batch:QC Batch Method:

Analysis Method:Analysis Description:

OEXT/20603EPA 3546

EPA 80828082 GCS PCB

Associated Lab Samples: 5040885001, 5040885007, 5040885008, 5040885014

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 476721


Matrix: Solid

Analyzed

PCB-1016 (Aroclor 1016) ug/kg ND 35.0 09/07/10 09:48PCB-1221 (Aroclor 1221) ug/kg ND 35.0 09/07/10 09:48PCB-1232 (Aroclor 1232) ug/kg ND 35.0 09/07/10 09:48PCB-1242 (Aroclor 1242) ug/kg ND 35.0 09/07/10 09:48PCB-1248 (Aroclor 1248) ug/kg ND 35.0 09/07/10 09:48PCB-1254 (Aroclor 1254) ug/kg ND 35.0 09/07/10 09:48PCB-1260 (Aroclor 1260) ug/kg ND 35.0 09/07/10 09:48Tetrachloro-m-xylene (S) % 80 20-130 09/07/10 09:48

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

476722LABORATORY CONTROL SAMPLE:LCSSpike

PCB-1016 (Aroclor 1016) ug/kg 126167 76 46-129PCB-1260 (Aroclor 1260) ug/kg 131167 78 46-129Tetrachloro-m-xylene (S) % 81 20-130

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

476723MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

5040885001

476724

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

PCB-1016 (Aroclor 1016) ug/kg 188 126 50-150141 11 20188ND 237 264PCB-1260 (Aroclor 1260) ug/kg 188 62 50-15061 2 20188ND 117 114Tetrachloro-m-xylene (S) % 73 20-13072 20

Parameter UnitsMS



MSSpikeResult

4036288035

476927

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

PCB-1016 (Aroclor 1016) ug/kg 192 82 50-15086 4 20192<19.5 158 165PCB-1260 (Aroclor 1260) ug/kg 192 62 50-15060 3 20192<19.5 118 114Tetrachloro-m-xylene (S) % 67 20-13069 20



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MPRP/6247EPA 3050

EPA 60106010 MET

Associated Lab Samples: 5040885001, 5040885004, 5040885007, 5040885008, 5040885015





Matrix: Solid

Analyzed

Arsenic mg/kg ND 2.0 09/07/10 12:18Barium mg/kg ND 2.0 09/07/10 12:18Cadmium mg/kg ND 2.0 09/07/10 12:18Chromium mg/kg ND 2.0 09/07/10 12:18Lead mg/kg ND 2.0 09/07/10 12:18Selenium mg/kg ND 2.0 09/07/10 12:18Silver mg/kg ND 2.0 09/07/10 12:18

Parameter UnitsLCS



Arsenic mg/kg 51.650 103 80-120Barium mg/kg 52.050 104 80-120Cadmium mg/kg 51.450 103 80-120Chromium mg/kg 48.150 96 80-120Lead mg/kg 50.450 101 80-120Selenium mg/kg 50.250 100 80-120Silver mg/kg 24.625 99 80-120

Parameter UnitsMS



MSSpikeResult

5040885001

475036

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic mg/kg 51.7 99 75-12596 4 2051.24.3 55.3 53.3Barium mg/kg 51.7 106 75-125107 .2 2051.215.4 70.3 70.2Cadmium mg/kg 51.7 98 75-12597 2 2051.2ND 50.8 49.6Chromium mg/kg 51.7 90 75-12585 5 2051.25.0 51.2 48.5Lead mg/kg 51.7 95 75-12595 1 2051.29.2 58.4 57.6Selenium mg/kg 51.7 95 75-12593 3 2051.2ND 48.9 47.5Silver mg/kg 25.8 93 75-12590 4 2025.5ND 24.4 23.5



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MERP/2795EPA 7471

EPA 74717471 Mercury






Matrix: Solid

Analyzed

Mercury mg/kg ND 0.33 09/08/10 12:53

Parameter UnitsLCS



Mercury mg/kg 0.50.5 101 80-120

Parameter UnitsMS



MSSpikeResult

5040942034

476342

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .52 104 75-125100 7 20.5ND 0.53 0.50

Parameter UnitsMS



MSSpikeResult

5040967001

476344

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .61 100 75-125105 5 20.61ND 0.61 0.64



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OEXT/20550EPA 3546

EPA 8270 by SIM8270 MSSV PAH by SIM






Matrix: Solid

Analyzed

2-Methylnaphthalene ug/kg ND 25.0 09/02/10 08:54Acenaphthene ug/kg ND 25.0 09/02/10 08:54Acenaphthylene ug/kg ND 25.0 09/02/10 08:54Anthracene ug/kg ND 25.0 09/02/10 08:54Benzo(a)anthracene ug/kg ND 25.0 09/02/10 08:54Benzo(a)pyrene ug/kg ND 25.0 09/02/10 08:54Benzo(b)fluoranthene ug/kg ND 25.0 09/02/10 08:54Benzo(g,h,i)perylene ug/kg ND 25.0 09/02/10 08:54Benzo(k)fluoranthene ug/kg ND 25.0 09/02/10 08:54Chrysene ug/kg ND 25.0 09/02/10 08:54Dibenz(a,h)anthracene ug/kg ND 25.0 09/02/10 08:54Fluoranthene ug/kg ND 25.0 09/02/10 08:54Fluorene ug/kg ND 25.0 09/02/10 08:54Indeno(1,2,3-cd)pyrene ug/kg ND 25.0 09/02/10 08:54Naphthalene ug/kg ND 25.0 09/02/10 08:54Phenanthrene ug/kg ND 25.0 09/02/10 08:54Pyrene ug/kg ND 25.0 09/02/10 08:542-Fluorobiphenyl (S) % 86 45-120 09/02/10 08:54Terphenyl-d14 (S) % 87 41-120 09/02/10 08:54

Parameter UnitsLCS



2-Methylnaphthalene ug/kg 13801670 83 48-120Acenaphthene ug/kg 14201670 85 54-118Acenaphthylene ug/kg 14101670 85 54-129Anthracene ug/kg 13901670 84 46-136Benzo(a)anthracene ug/kg 13801670 83 55-125Benzo(a)pyrene ug/kg 14301670 86 46-140Benzo(b)fluoranthene ug/kg 14001670 84 46-137Benzo(g,h,i)perylene ug/kg 14401670 86 41-124Benzo(k)fluoranthene ug/kg 15101670 91 44-132Chrysene ug/kg 14401670 87 54-121Dibenz(a,h)anthracene ug/kg 14301670 86 44-133Fluoranthene ug/kg 14301670 86 57-131Fluorene ug/kg 14401670 87 56-123Indeno(1,2,3-cd)pyrene ug/kg 14201670 85 42-133Naphthalene ug/kg 13901670 83 48-117Phenanthrene ug/kg 14101670 85 55-120Pyrene ug/kg 14701670 88 56-1242-Fluorobiphenyl (S) % 89 45-120



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Parameter UnitsLCS



Terphenyl-d14 (S) % 87 41-120

Parameter UnitsMS



MSSpikeResult

5040849001

474986

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2-Methylnaphthalene ug/kg 1810 71 25-12368 5 201810ND 1280 1220Acenaphthene ug/kg 1810 74 27-12672 2 201810ND 1330 1300Acenaphthylene ug/kg 1810 75 23-13872 4 201810ND 1350 1300Anthracene ug/kg 1810 75 22-13677 2 201810ND 1360 1380Benzo(a)anthracene ug/kg 1810 72 20-13474 3 201810ND 1290 1330Benzo(a)pyrene ug/kg 1810 70 20-13772 2 201810ND 1270 1290Benzo(b)fluoranthene ug/kg 1810 69 20-13872 4 201810ND 1240 1300Benzo(g,h,i)perylene ug/kg 1810 66 20-11668 3 201810ND 1190 1230Benzo(k)fluoranthene ug/kg 1810 74 15-13674 .2 201810ND 1330 1330Chrysene ug/kg 1810 74 16-13676 2 201810ND 1340 1370Dibenz(a,h)anthracene ug/kg 1810 69 15-12971 3 201810ND 1240 1280Fluoranthene ug/kg 1810 75 11-15577 2 201810ND 1350 1380Fluorene ug/kg 1810 76 20-14175 1 201810ND 1370 1350Indeno(1,2,3-cd)pyrene ug/kg 1810 67 10-12968 2 201810ND 1200 1220Naphthalene ug/kg 1810 72 18-13768 7 201810ND 1310 1220Phenanthrene ug/kg 1810 75 20-18076 2 201810ND 1340 1380Pyrene ug/kg 1810 76 18-14278 3 201810ND 1360 14102-Fluorobiphenyl (S) % 80 45-12069 20Terphenyl-d14 (S) % 78 41-12080 20



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OEXT/20559EPA 3546


Associated Lab Samples: 5040885014





Matrix: Solid

Analyzed


Parameter UnitsLCS






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Parameter UnitsLCS



Terphenyl-d14 (S) % 91 41-120

Parameter UnitsMS



MSSpikeResult

5040871004

475063

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2-Methylnaphthalene ug/kg 1900 76 25-12372 5 201900ND 1440 1370Acenaphthene ug/kg 1900 76 27-12673 4 201900ND 1440 1390Acenaphthylene ug/kg 1900 77 23-13875 3 201900ND 1470 1420Anthracene ug/kg 1900 72 22-13670 3 201900ND 1370 1330Benzo(a)anthracene ug/kg 1900 63 20-13460 5 201900ND 1200 1140Benzo(a)pyrene ug/kg 1900 60 20-13757 6 201900ND 1140 1080Benzo(b)fluoranthene ug/kg 1900 62 20-13859 5 201900ND 1170 1110Benzo(g,h,i)perylene ug/kg 1900 54 20-11650 6 201900ND 1020 958Benzo(k)fluoranthene ug/kg 1900 63 15-13659 6 201900ND 1190 1120Chrysene ug/kg 1900 67 16-13665 3 201900ND 1270 1230Dibenz(a,h)anthracene ug/kg 1900 59 15-12955 7 201900ND 1120 1050Fluoranthene ug/kg 1900 71 11-15569 4 201900ND 1360 1310Fluorene ug/kg 1900 76 20-14173 4 201900ND 1450 1390Indeno(1,2,3-cd)pyrene ug/kg 1900 55 10-12952 7 201900ND 1050 981Naphthalene ug/kg 1900 79 18-13777 2 201900ND 1510 1470Phenanthrene ug/kg 1900 73 20-18071 2 201900ND 1380 1350Pyrene ug/kg 1900 71 18-14267 6 201900ND 1340 12702-Fluorobiphenyl (S) % 84 45-12077 20Terphenyl-d14 (S) % 73 41-12064 20



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MSV/26473EPA 8260

EPA 82608260 MSV 5030 Low

Associated Lab Samples: 5040885007, 5040885008





Matrix: Solid

Analyzed

1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/07/10 14:081,1,1-Trichloroethane ug/kg ND 5.0 09/07/10 14:081,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/07/10 14:081,1,2-Trichloroethane ug/kg ND 5.0 09/07/10 14:081,1-Dichloroethane ug/kg ND 5.0 09/07/10 14:081,1-Dichloroethene ug/kg ND 5.0 09/07/10 14:081,1-Dichloropropene ug/kg ND 5.0 09/07/10 14:081,2,3-Trichlorobenzene ug/kg ND 5.0 09/07/10 14:081,2,3-Trichloropropane ug/kg ND 5.0 09/07/10 14:081,2,4-Trichlorobenzene ug/kg ND 5.0 09/07/10 14:081,2,4-Trimethylbenzene ug/kg ND 5.0 09/07/10 14:081,2-Dibromoethane (EDB) ug/kg ND 5.0 09/07/10 14:081,2-Dichlorobenzene ug/kg ND 5.0 09/07/10 14:081,2-Dichloroethane ug/kg ND 5.0 09/07/10 14:081,2-Dichloropropane ug/kg ND 5.0 09/07/10 14:081,3,5-Trimethylbenzene ug/kg ND 5.0 09/07/10 14:081,3-Dichlorobenzene ug/kg ND 5.0 09/07/10 14:081,3-Dichloropropane ug/kg ND 5.0 09/07/10 14:081,4-Dichlorobenzene ug/kg ND 5.0 09/07/10 14:082,2-Dichloropropane ug/kg ND 5.0 09/07/10 14:082-Butanone (MEK) ug/kg ND 25.0 09/07/10 14:082-Chlorotoluene ug/kg ND 5.0 09/07/10 14:082-Hexanone ug/kg ND 100 09/07/10 14:084-Chlorotoluene ug/kg ND 5.0 09/07/10 14:084-Methyl-2-pentanone (MIBK) ug/kg ND 25.0 09/07/10 14:08Acetone ug/kg ND 100 09/07/10 14:08Acrolein ug/kg ND 100 09/07/10 14:08Acrylonitrile ug/kg ND 100 09/07/10 14:08Benzene ug/kg ND 5.0 09/07/10 14:08Bromobenzene ug/kg ND 5.0 09/07/10 14:08Bromochloromethane ug/kg ND 5.0 09/07/10 14:08Bromodichloromethane ug/kg ND 5.0 09/07/10 14:08Bromoform ug/kg ND 5.0 09/07/10 14:08Bromomethane ug/kg ND 5.0 09/07/10 14:08Carbon disulfide ug/kg ND 10.0 09/07/10 14:08Carbon tetrachloride ug/kg ND 5.0 09/07/10 14:08Chlorobenzene ug/kg ND 5.0 09/07/10 14:08Chloroethane ug/kg ND 5.0 09/07/10 14:08Chloroform ug/kg ND 5.0 09/07/10 14:08Chloromethane ug/kg ND 5.0 09/07/10 14:08cis-1,2-Dichloroethene ug/kg ND 5.0 09/07/10 14:08cis-1,3-Dichloropropene ug/kg ND 5.0 09/07/10 14:08Dibromochloromethane ug/kg ND 5.0 09/07/10 14:08



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Matrix: Solid

Analyzed

Dibromomethane ug/kg ND 5.0 09/07/10 14:08Dichlorodifluoromethane ug/kg ND 5.0 09/07/10 14:08Ethyl methacrylate ug/kg ND 10.0 09/07/10 14:08Ethylbenzene ug/kg ND 5.0 09/07/10 14:08Hexachloro-1,3-butadiene ug/kg ND 5.0 09/07/10 14:08Iodomethane ug/kg ND 100 09/07/10 14:08Isopropylbenzene (Cumene) ug/kg ND 5.0 09/07/10 14:08Methyl-tert-butyl ether ug/kg ND 5.0 09/07/10 14:08Methylene chloride ug/kg ND 20.0 09/07/10 14:08n-Butylbenzene ug/kg ND 5.0 09/07/10 14:08n-Propylbenzene ug/kg ND 5.0 09/07/10 14:08Naphthalene ug/kg ND 5.0 09/07/10 14:08p-Isopropyltoluene ug/kg ND 5.0 09/07/10 14:08sec-Butylbenzene ug/kg ND 5.0 09/07/10 14:08Styrene ug/kg ND 5.0 09/07/10 14:08tert-Butylbenzene ug/kg ND 5.0 09/07/10 14:08Tetrachloroethene ug/kg ND 5.0 09/07/10 14:08Toluene ug/kg ND 5.0 09/07/10 14:08trans-1,2-Dichloroethene ug/kg ND 5.0 09/07/10 14:08trans-1,3-Dichloropropene ug/kg ND 5.0 09/07/10 14:08trans-1,4-Dichloro-2-butene ug/kg ND 100 09/07/10 14:08Trichloroethene ug/kg ND 5.0 09/07/10 14:08Trichlorofluoromethane ug/kg ND 5.0 09/07/10 14:08Vinyl acetate ug/kg ND 100 09/07/10 14:08Vinyl chloride ug/kg ND 5.0 09/07/10 14:08Xylene (Total) ug/kg ND 10.0 09/07/10 14:084-Bromofluorobenzene (S) % 103 61-131 09/07/10 14:08Dibromofluoromethane (S) % 104 80-124 09/07/10 14:08Toluene-d8 (S) % 98 58-145 09/07/10 14:08

Parameter UnitsLCS



1,1,1,2-Tetrachloroethane ug/kg 48.250 96 65-1241,1,1-Trichloroethane ug/kg 49.650 99 61-1351,1,2,2-Tetrachloroethane ug/kg 46.050 92 66-1241,1,2-Trichloroethane ug/kg 52.050 104 74-1271,1-Dichloroethane ug/kg 45.250 90 62-1321,1-Dichloroethene ug/kg 47.450 95 61-1231,1-Dichloropropene ug/kg 51.350 103 74-1281,2,3-Trichlorobenzene ug/kg 44.450 89 60-1251,2,3-Trichloropropane ug/kg 98.0100 98 61-1201,2,4-Trichlorobenzene ug/kg 44.650 89 58-1261,2,4-Trimethylbenzene ug/kg 43.050 86 72-1201,2-Dibromoethane (EDB) ug/kg 52.350 105 74-119



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Parameter UnitsLCS



1,2-Dichlorobenzene ug/kg 45.650 91 75-1171,2-Dichloroethane ug/kg 50.450 101 62-1351,2-Dichloropropane ug/kg 46.750 93 74-1241,3,5-Trimethylbenzene ug/kg 44.550 89 73-1221,3-Dichlorobenzene ug/kg 49.750 99 73-1201,3-Dichloropropane ug/kg 49.550 99 71-1221,4-Dichlorobenzene ug/kg 49.450 99 72-1182,2-Dichloropropane ug/kg 50.050 100 53-1362-Butanone (MEK) ug/kg 343250 137 33-1902-Chlorotoluene ug/kg 48.850 98 72-1222-Hexanone ug/kg 314250 126 44-1684-Chlorotoluene ug/kg 48.650 97 72-1204-Methyl-2-pentanone (MIBK) ug/kg 257250 103 58-126Acetone ug/kg 493 L3250 197 30-190Acrolein ug/kg 12601000 126 30-190Acrylonitrile ug/kg 10801000 108 65-129Benzene ug/kg 50.050 100 76-123Bromobenzene ug/kg 45.350 91 74-116Bromochloromethane ug/kg 50.650 101 56-143Bromodichloromethane ug/kg 46.650 93 67-123Bromoform ug/kg 47.850 96 58-117Bromomethane ug/kg 61.450 123 47-147Carbon disulfide ug/kg 91.1100 91 56-141Carbon tetrachloride ug/kg 52.450 105 54-136Chlorobenzene ug/kg 49.850 100 75-115Chloroethane ug/kg 54.750 109 57-147Chloroform ug/kg 48.650 97 74-123Chloromethane ug/kg 47.050 94 31-155cis-1,2-Dichloroethene ug/kg 47.750 95 76-119cis-1,3-Dichloropropene ug/kg 51.750 103 56-110Dibromochloromethane ug/kg 50.750 101 63-122Dibromomethane ug/kg 45.650 91 70-127Dichlorodifluoromethane ug/kg 63.750 127 30-170Ethyl methacrylate ug/kg 210200 105 58-126Ethylbenzene ug/kg 48.450 97 78-121Hexachloro-1,3-butadiene ug/kg 40.450 81 65-128Iodomethane ug/kg 118100 118 38-173Isopropylbenzene (Cumene) ug/kg 45.450 91 75-128Methyl-tert-butyl ether ug/kg 94.6100 95 59-142Methylene chloride ug/kg 37.150 74 30-170n-Butylbenzene ug/kg 43.550 87 70-123n-Propylbenzene ug/kg 48.950 98 70-126Naphthalene ug/kg 45.750 91 60-128p-Isopropyltoluene ug/kg 42.750 85 65-125sec-Butylbenzene ug/kg 43.850 88 72-125Styrene ug/kg 47.450 95 75-118tert-Butylbenzene ug/kg 35.250 70 61-114Tetrachloroethene ug/kg 49.550 99 63-117



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Parameter UnitsLCS



Toluene ug/kg 50.850 102 72-123trans-1,2-Dichloroethene ug/kg 49.050 98 70-122trans-1,3-Dichloropropene ug/kg 50.250 100 55-107trans-1,4-Dichloro-2-butene ug/kg 167200 83 49-127Trichloroethene ug/kg 49.350 99 74-121Trichlorofluoromethane ug/kg 47.550 95 55-156Vinyl acetate ug/kg 128200 64 46-127Vinyl chloride ug/kg 49.250 98 50-146Xylene (Total) ug/kg 144150 96 77-1204-Bromofluorobenzene (S) % 93 61-131Dibromofluoromethane (S) % 95 80-124Toluene-d8 (S) % 103 58-145

Parameter UnitsMS



MSSpikeResult

5040751002

477232

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1,2-Tetrachloroethane ug/kg 59.2 86 20-133110 24 2059.2ND 51.0 65.11,1,1-Trichloroethane ug/kg 59.2 94 27-142122 27 2059.2ND 55.4 72.51,1,2,2-Tetrachloroethane ug/kg 59.2 83 20-159112 30 2059.2ND 49.1 66.51,1,2-Trichloroethane ug/kg 59.2 93 20-155116 22 2059.2ND 55.1 69.01,1-Dichloroethane ug/kg 59.2 81 31-141110 31 2059.2ND 47.8 65.01,1-Dichloroethene ug/kg 59.2 91 23-132120 27 2059.2ND 53.7 70.81,1-Dichloropropene ug/kg 59.2 94 20-146123 27 2059.2ND 55.5 72.91,2,3-Trichlorobenzene ug/kg 59.2 59 20-14080 31 2059.2ND 34.7 47.61,2,3-Trichloropropane ug/kg 118 82 20-153113 32 20118ND 97.0 1341,2,4-Trichlorobenzene ug/kg 59.2 58 20-12078 29 2059.2ND 34.5 46.21,2,4-Trimethylbenzene ug/kg 59.2 70 20-15691 26 2059.2ND 41.5 53.71,2-Dibromoethane (EDB) ug/kg 59.2 92 20-143114 22 2059.2ND 54.5 67.81,2-Dichlorobenzene ug/kg 59.2 74 20-13399 29 2059.2ND 43.6 58.51,2-Dichloroethane ug/kg 59.2 90 30-143118 27 2059.2ND 53.5 69.91,2-Dichloropropane ug/kg 59.2 85 30-140110 25 2059.2ND 50.6 65.21,3,5-Trimethylbenzene ug/kg 59.2 72 20-14395 27 2059.2ND 42.9 56.21,3-Dichlorobenzene ug/kg 59.2 77 20-136104 29 2059.2ND 45.8 61.61,3-Dichloropropane ug/kg 59.2 89 30-144110 21 2059.2ND 52.9 65.31,4-Dichlorobenzene ug/kg 59.2 76 30-135101 29 2059.2ND 45.1 60.12,2-Dichloropropane ug/kg 59.2 93 30-143121 26 2059.2ND 55.4 71.72-Butanone (MEK) ug/kg 296 102 30-190128 23 20296ND 302 3812-Chlorotoluene ug/kg 59.2 82 30-170105 25 2059.2ND 48.7 62.42-Hexanone ug/kg 296 96 30-170120 22 20296ND 284 3554-Chlorotoluene ug/kg 59.2 80 30-143108 31 2059.2ND 47.2 64.34-Methyl-2-pentanone (MIBK) ug/kg 296 88 30-144108 20 20296ND 261 319Acetone ug/kg 296 129 30-180167 25 20296ND 383 494Acrolein ug/kg 1180 106 30-180140 27 201180ND 1260 1650Acrylonitrile ug/kg 1180 100 30-141129 25 201180ND 1180 1530Benzene ug/kg 59.2 92 50-135119 26 2059.2ND 54.3 70.5Bromobenzene ug/kg 59.2 79 30-125102 26 2059.2ND 46.6 60.5



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Parameter UnitsMS



MSSpikeResult

5040751002

477232

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Bromochloromethane ug/kg 59.2 92 30-159120 26 2059.2ND 54.6 70.9Bromodichloromethane ug/kg 59.2 81 30-141107 28 2059.2ND 48.1 63.6Bromoform ug/kg 59.2 81 30-135110 30 2059.2ND 48.0 65.1Bromomethane ug/kg M059.2 138 30-137242 55 2059.2ND 81.7 143Carbon disulfide ug/kg 118 87 30-156116 28 20118ND 104 137Carbon tetrachloride ug/kg 59.2 97 30-130128 28 2059.2ND 57.2 76.0Chlorobenzene ug/kg 59.2 86 30-137107 22 2059.2ND 50.8 63.7Chloroethane ug/kg 59.2 106 35-143168 46 2059.2ND 62.5 99.6Chloroform ug/kg 59.2 90 30-136119 27 2059.2ND 53.5 70.5Chloromethane ug/kg 59.2 89 28-134121 31 2059.2ND 52.6 71.7cis-1,2-Dichloroethene ug/kg 59.2 88 30-141117 27 2059.2ND 52.4 69.0cis-1,3-Dichloropropene ug/kg 59.2 88 30-126113 24 2059.2ND 52.4 66.9Dibromochloromethane ug/kg 59.2 89 30-129111 23 2059.2ND 52.5 66.0Dibromomethane ug/kg 59.2 80 30-153105 27 2059.2ND 47.3 62.2Dichlorodifluoromethane ug/kg 1d59.2 133 30-150173 26 2059.2ND 78.7 103Ethyl methacrylate ug/kg 237 86 30-170104 19 20237ND 204 247Ethylbenzene ug/kg 59.2 83 50-150104 22 2059.2ND 49.2 61.5Hexachloro-1,3-butadiene ug/kg 59.2 53 30-13860 12 2059.2ND 31.6 35.7Iodomethane ug/kg 118 111 30-180154 32 20118ND 132 183Isopropylbenzene (Cumene) ug/kg 59.2 76 50-15096 24 2059.2ND 44.9 57.1Methyl-tert-butyl ether ug/kg 118 82 40-149107 26 20118ND 97.4 126Methylene chloride ug/kg 59.2 70 30-16398 33 2059.2ND 41.5 58.0n-Butylbenzene ug/kg 59.2 61 40-15277 22 2059.2ND 36.4 45.4n-Propylbenzene ug/kg 59.2 75 40-170102 31 2059.2ND 44.3 60.5Naphthalene ug/kg 59.2 69 50-12895 30 2059.2ND 42.4 57.4p-Isopropyltoluene ug/kg 59.2 65 40-16783 24 2059.2ND 38.7 49.3sec-Butylbenzene ug/kg 59.2 69 40-16889 25 2059.2ND 41.0 52.5Styrene ug/kg 59.2 80 30-141102 24 2059.2ND 47.7 60.4tert-Butylbenzene ug/kg 59.2 58 40-14475 26 2059.2ND 34.2 44.4Tetrachloroethene ug/kg 59.2 84 40-155103 20 2059.2ND 49.6 60.8Toluene ug/kg 59.2 92 50-149114 21 2059.2ND 54.4 67.4trans-1,2-Dichloroethene ug/kg 59.2 92 40-140120 26 2059.2ND 54.7 71.1trans-1,3-Dichloropropene ug/kg 59.2 85 40-130108 24 2059.2ND 50.3 63.9trans-1,4-Dichloro-2-butene ug/kg 237 71 30-15091 25 20237ND 168 216Trichloroethene ug/kg 59.2 88 40-153115 26 2059.2ND 52.1 67.8Trichlorofluoromethane ug/kg 59.2 92 43-140122 28 2059.2ND 54.4 72.2Vinyl acetate ug/kg M0237 23 30-12024 20237ND ND NDVinyl chloride ug/kg 59.2 98 36-137127 26 2059.2ND 58.1 75.2Xylene (Total) ug/kg 178 82 50-143103 23 20178ND 146 1844-Bromofluorobenzene (S) % 94 61-13194 20Dibromofluoromethane (S) % 94 80-12496 20Toluene-d8 (S) % 105 58-14598 20



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MSV/26471EPA 8260

EPA 82608260 MSV






Matrix: Water

Analyzed

1,1,1,2-Tetrachloroethane ug/L ND 5.0 09/07/10 13:501,1,1-Trichloroethane ug/L ND 5.0 09/07/10 13:501,1,2,2-Tetrachloroethane ug/L ND 5.0 09/07/10 13:501,1,2-Trichloroethane ug/L ND 5.0 09/07/10 13:501,1-Dichloroethane ug/L ND 5.0 09/07/10 13:501,1-Dichloroethene ug/L ND 5.0 09/07/10 13:501,1-Dichloropropene ug/L ND 5.0 09/07/10 13:501,2,3-Trichlorobenzene ug/L ND 5.0 09/07/10 13:501,2,3-Trichloropropane ug/L ND 5.0 09/07/10 13:501,2,4-Trichlorobenzene ug/L ND 5.0 09/07/10 13:501,2,4-Trimethylbenzene ug/L ND 5.0 09/07/10 13:501,2-Dibromoethane (EDB) ug/L ND 5.0 09/07/10 13:501,2-Dichlorobenzene ug/L ND 5.0 09/07/10 13:501,2-Dichloroethane ug/L ND 5.0 09/07/10 13:501,2-Dichloropropane ug/L ND 5.0 09/07/10 13:501,3,5-Trimethylbenzene ug/L ND 5.0 09/07/10 13:501,3-Dichlorobenzene ug/L ND 5.0 09/07/10 13:501,3-Dichloropropane ug/L ND 5.0 09/07/10 13:501,4-Dichlorobenzene ug/L ND 5.0 09/07/10 13:502,2-Dichloropropane ug/L ND 5.0 09/07/10 13:502-Butanone (MEK) ug/L ND 25.0 09/07/10 13:502-Chlorotoluene ug/L ND 5.0 09/07/10 13:502-Hexanone ug/L ND 25.0 09/07/10 13:504-Chlorotoluene ug/L ND 5.0 09/07/10 13:504-Methyl-2-pentanone (MIBK) ug/L ND 25.0 09/07/10 13:50Acetone ug/L ND 100 09/07/10 13:50Acrolein ug/L ND 50.0 09/07/10 13:50Acrylonitrile ug/L ND 100 09/07/10 13:50Benzene ug/L ND 5.0 09/07/10 13:50Bromobenzene ug/L ND 5.0 09/07/10 13:50Bromochloromethane ug/L ND 5.0 09/07/10 13:50Bromodichloromethane ug/L ND 5.0 09/07/10 13:50Bromoform ug/L ND 5.0 09/07/10 13:50Bromomethane ug/L ND 5.0 09/07/10 13:50Carbon disulfide ug/L ND 10.0 09/07/10 13:50Carbon tetrachloride ug/L ND 5.0 09/07/10 13:50Chlorobenzene ug/L ND 5.0 09/07/10 13:50Chloroethane ug/L ND 5.0 09/07/10 13:50Chloroform ug/L ND 5.0 09/07/10 13:50Chloromethane ug/L ND 5.0 09/07/10 13:50cis-1,2-Dichloroethene ug/L ND 5.0 09/07/10 13:50cis-1,3-Dichloropropene ug/L ND 5.0 09/07/10 13:50Dibromochloromethane ug/L ND 5.0 09/07/10 13:50



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Matrix: Water

Analyzed

Dibromomethane ug/L ND 5.0 09/07/10 13:50Dichlorodifluoromethane ug/L ND 5.0 09/07/10 13:50Ethyl methacrylate ug/L ND 100 09/07/10 13:50Ethylbenzene ug/L ND 5.0 09/07/10 13:50Hexachloro-1,3-butadiene ug/L ND 5.0 09/07/10 13:50Iodomethane ug/L ND 10.0 09/07/10 13:50Isopropylbenzene (Cumene) ug/L ND 5.0 09/07/10 13:50Methyl-tert-butyl ether ug/L ND 4.0 09/07/10 13:50Methylene chloride ug/L ND 5.0 09/07/10 13:50n-Butylbenzene ug/L ND 5.0 09/07/10 13:50n-Hexane ug/L ND 5.0 09/07/10 13:50n-Propylbenzene ug/L ND 5.0 09/07/10 13:50Naphthalene ug/L ND 5.0 09/07/10 13:50p-Isopropyltoluene ug/L ND 5.0 09/07/10 13:50sec-Butylbenzene ug/L ND 5.0 09/07/10 13:50Styrene ug/L ND 5.0 09/07/10 13:50tert-Butylbenzene ug/L ND 5.0 09/07/10 13:50Tetrachloroethene ug/L ND 5.0 09/07/10 13:50Toluene ug/L ND 5.0 09/07/10 13:50trans-1,2-Dichloroethene ug/L ND 5.0 09/07/10 13:50trans-1,3-Dichloropropene ug/L ND 5.0 09/07/10 13:50trans-1,4-Dichloro-2-butene ug/L ND 100 09/07/10 13:50Trichloroethene ug/L ND 5.0 09/07/10 13:50Trichlorofluoromethane ug/L ND 5.0 09/07/10 13:50Vinyl acetate ug/L ND 10.0 09/07/10 13:50Vinyl chloride ug/L ND 2.0 09/07/10 13:50Xylene (Total) ug/L ND 10.0 09/07/10 13:504-Bromofluorobenzene (S) % 97 70-126 09/07/10 13:50Dibromofluoromethane (S) % 101 80-123 09/07/10 13:50Toluene-d8 (S) % 102 80-116 09/07/10 13:50

Parameter UnitsLCS



1,1,1,2-Tetrachloroethane ug/L 43.450 87 69-1301,1,1-Trichloroethane ug/L 47.150 94 69-1361,1,2,2-Tetrachloroethane ug/L 44.250 88 69-1311,1,2-Trichloroethane ug/L 44.950 90 77-1321,1-Dichloroethane ug/L 44.550 89 67-1331,1-Dichloroethene ug/L 48.650 97 63-1281,1-Dichloropropene ug/L 47.250 94 75-1341,2,3-Trichlorobenzene ug/L 45.150 90 58-1311,2,3-Trichloropropane ug/L 83.2100 83 60-1311,2,4-Trichlorobenzene ug/L 43.450 87 60-1301,2,4-Trimethylbenzene ug/L 41.250 82 73-130



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Parameter UnitsLCS



1,2-Dibromoethane (EDB) ug/L 46.250 92 75-1261,2-Dichlorobenzene ug/L 43.050 86 76-1241,2-Dichloroethane ug/L 46.250 92 69-1391,2-Dichloropropane ug/L 44.750 89 76-1291,3,5-Trimethylbenzene ug/L 42.050 84 74-1301,3-Dichlorobenzene ug/L 43.850 88 76-1251,3-Dichloropropane ug/L 45.450 91 74-1261,4-Dichlorobenzene ug/L 42.950 86 75-1222,2-Dichloropropane ug/L 48.450 97 53-1442-Butanone (MEK) ug/L 281250 112 47-1892-Chlorotoluene ug/L 44.450 89 72-1282-Hexanone ug/L 254250 102 57-1674-Chlorotoluene ug/L 44.450 89 73-1244-Methyl-2-pentanone (MIBK) ug/L 224250 90 61-135Acetone ug/L 397250 159 30-170Acrolein ug/L 10401000 104 30-170Acrylonitrile ug/L 8421000 84 67-136Benzene ug/L 45.250 90 78-127Bromobenzene ug/L 41.650 83 62-139Bromochloromethane ug/L 45.250 90 54-162Bromodichloromethane ug/L 45.350 91 69-133Bromoform ug/L 43.050 86 60-127Bromomethane ug/L 59.150 118 30-170Carbon disulfide ug/L 87.7100 88 58-152Carbon tetrachloride ug/L 48.450 97 62-143Chlorobenzene ug/L 44.550 89 75-123Chloroethane ug/L 62.050 124 56-153Chloroform ug/L 43.750 87 74-131Chloromethane ug/L 48.750 97 35-147cis-1,2-Dichloroethene ug/L 47.350 95 74-128cis-1,3-Dichloropropene ug/L 45.050 90 58-123Dibromochloromethane ug/L 44.650 89 66-131Dibromomethane ug/L 44.350 89 73-133Dichlorodifluoromethane ug/L 71.850 144 30-170Ethyl methacrylate ug/L 179200 89 59-138Ethylbenzene ug/L 42.850 86 81-126Hexachloro-1,3-butadiene ug/L 44.350 89 70-130Iodomethane ug/L 88.8100 89 41-170Isopropylbenzene (Cumene) ug/L 41.450 83 80-130Methyl-tert-butyl ether ug/L 82.4100 82 66-147Methylene chloride ug/L 37.350 75 32-164n-Butylbenzene ug/L 41.550 83 68-135n-Hexane ug/L 46.650 93 69-157n-Propylbenzene ug/L 43.250 86 71-132Naphthalene ug/L 45.650 91 61-135p-Isopropyltoluene ug/L 41.950 84 66-131sec-Butylbenzene ug/L 41.950 84 73-130Styrene ug/L 42.850 86 74-128



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Parameter UnitsLCS



tert-Butylbenzene ug/L 34.250 68 63-117Tetrachloroethene ug/L 42.050 84 60-119Toluene ug/L 45.250 90 75-129trans-1,2-Dichloroethene ug/L 46.850 94 71-126trans-1,3-Dichloropropene ug/L 43.750 87 54-123trans-1,4-Dichloro-2-butene ug/L 158200 79 47-141Trichloroethene ug/L 45.350 91 74-130Trichlorofluoromethane ug/L 51.350 103 62-150Vinyl acetate ug/L 129200 65 41-145Vinyl chloride ug/L 55.050 110 55-141Xylene (Total) ug/L 128150 85 76-1324-Bromofluorobenzene (S) % 97 70-126Dibromofluoromethane (S) % 103 80-123Toluene-d8 (S) % 100 80-116

Parameter UnitsMS



MSSpikeResult

5040690008

477225

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1,2-Tetrachloroethane ug/L 50 99 55-131100 2 2050ND 49.5 50.21,1,1-Trichloroethane ug/L 50 108 64-143116 7 2050ND 54.0 58.01,1,2,2-Tetrachloroethane ug/L 50 102 64-142101 2 2050ND 51.1 50.31,1,2-Trichloroethane ug/L 50 110 71-143108 2 2050ND 55.2 54.01,1-Dichloroethane ug/L 50 106 68-139109 3 2050ND 52.9 54.71,1-Dichloroethene ug/L 50 115 55-140124 7 2050ND 57.7 62.11,1-Dichloropropene ug/L 50 105 66-140115 9 2050ND 52.7 57.51,2,3-Trichlorobenzene ug/L R150 88 33-14055 45 2050ND 43.8 27.61,2,3-Trichloropropane ug/L 100 83 58-13381 2 20100ND 82.8 81.31,2,4-Trichlorobenzene ug/L R150 81 28-14053 42 2050ND 40.6 26.71,2,4-Trimethylbenzene ug/L 50 78 39-14685 8 2050ND 39.2 42.51,2-Dibromoethane (EDB) ug/L 50 105 67-134103 1 2050ND 52.4 51.61,2-Dichlorobenzene ug/L 50 86 48-13780 8 2050ND 43.2 39.81,2-Dichloroethane ug/L 50 107 63-148109 1 2050ND 53.6 54.31,2-Dichloropropane ug/L 50 101 70-136103 2 2050ND 50.7 51.61,3,5-Trimethylbenzene ug/L 50 80 39-14588 10 2050ND 39.9 44.21,3-Dichlorobenzene ug/L 50 85 40-14381 4 2050ND 42.3 40.71,3-Dichloropropane ug/L 50 101 65-133101 .004 2050ND 50.4 50.41,4-Dichlorobenzene ug/L 50 81 38-14278 4 2050ND 40.7 39.22,2-Dichloropropane ug/L 50 110 35-157117 6 2050ND 54.9 58.32-Butanone (MEK) ug/L 250 105 62-132109 4 20250ND 262 2722-Chlorotoluene ug/L 50 88 44-14395 7 2050ND 44.0 47.32-Hexanone ug/L 250 97 61-14198 .8 20250ND 242 2444-Chlorotoluene ug/L 50 88 43-14094 7 2050ND 44.0 47.14-Methyl-2-pentanone (MIBK) ug/L 250 102 57-135102 .2 20250ND 256 256Acetone ug/L 250 112 30-170114 1 20250ND 303 307Acrolein ug/L 1000 113 30-170114 1 201000ND 1130 1140Acrylonitrile ug/L 1000 97 66-137100 3 201000ND 973 1000



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Parameter UnitsMS



MSSpikeResult

5040690008

477225

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Benzene ug/L 50 105 63-141111 6 2050ND 52.3 55.5Bromobenzene ug/L 50 85 57-12883 2 2050ND 42.5 41.7Bromochloromethane ug/L 50 107 65-157108 1 2050ND 53.5 54.2Bromodichloromethane ug/L 50 103 63-135103 .6 2050ND 51.4 51.7Bromoform ug/L 50 91 58-12487 5 2050ND 45.4 43.3Bromomethane ug/L M0,R150 185 30-170232 23 2050ND 92.4 116Carbon disulfide ug/L 100 104 46-162114 9 20100ND 104 114Carbon tetrachloride ug/L 50 110 54-145120 9 2050ND 54.9 59.9Chlorobenzene ug/L 50 93 56-13398 5 2050ND 46.5 48.8Chloroethane ug/L M050 168 54-157187 11 2050ND 84.0 93.4Chloroform ug/L 50 101 67-134105 4 2050ND 50.7 52.6Chloromethane ug/L 50 114 36-137133 16 2050ND 57.0 66.7cis-1,2-Dichloroethene ug/L 50 112 65-132117 4 205012.9 69.1 71.5cis-1,3-Dichloropropene ug/L 50 99 46-12198 .8 2050ND 49.4 48.9Dibromochloromethane ug/L 50 99 64-12495 5 2050ND 49.6 47.3Dibromomethane ug/L 50 104 67-144105 2 2050ND 51.8 52.7Dichlorodifluoromethane ug/L M050 181 30-163190 5 2050ND 90.4 95.0Ethyl methacrylate ug/L 200 99 52-14098 1 20200ND 199 197Ethylbenzene ug/L 50 87 44-15196 10 2050ND 43.4 48.0Hexachloro-1,3-butadiene ug/L 50 67 30-14567 .2 2050ND 33.6 33.6Iodomethane ug/L 100 116 28-168117 .8 20100ND 116 117Isopropylbenzene (Cumene) ug/L 50 84 40-14893 11 2050ND 41.8 46.5Methyl-tert-butyl ether ug/L 100 98 52-15698 .2 20100ND 98.3 98.1Methylene chloride ug/L 50 97 46-15499 2 2050ND 48.4 49.3n-Butylbenzene ug/L 50 69 27-15377 11 2050ND 34.4 38.4n-Hexane ug/L 50 109 32-176121 10 2050ND 54.6 60.6n-Propylbenzene ug/L 50 81 40-14894 14 2050ND 40.6 46.8Naphthalene ug/L R150 97 44-13877 23 2050ND 48.6 38.4p-Isopropyltoluene ug/L 50 75 34-14684 12 2050ND 37.3 41.8sec-Butylbenzene ug/L 50 78 38-15089 13 2050ND 38.9 44.3Styrene ug/L 50 86 38-14188 3 2050ND 42.9 44.1tert-Butylbenzene ug/L 50 66 32-13375 13 2050ND 32.8 37.5Tetrachloroethene ug/L 50 88 25-14699 13 2050ND 43.9 49.7Toluene ug/L 50 101 59-142107 6 2050ND 50.4 53.7trans-1,2-Dichloroethene ug/L 50 112 60-137118 5 2050ND 56.1 59.2trans-1,3-Dichloropropene ug/L 50 92 43-11791 2 2050ND 46.2 45.5trans-1,4-Dichloro-2-butene ug/L 200 77 44-13972 7 20200ND 155 144Trichloroethene ug/L 50 100 61-137115 11 205016.2 66.1 73.7Trichlorofluoromethane ug/L 50 118 53-162126 6 2050ND 59.0 62.8Vinyl acetate ug/L 200 71 24-13268 5 20200ND 142 135Vinyl chloride ug/L 50 133 51-144139 4 2050ND 66.7 69.4Xylene (Total) ug/L 150 87 44-15295 9 20150ND 131 1424-Bromofluorobenzene (S) % 102 70-12697 20Dibromofluoromethane (S) % 103 80-123105 20Toluene-d8 (S) % 100 80-11699 20



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MSV/26478EPA 8260

EPA 82608260 MSV 5035A Volatile Organics






Matrix: Solid

Analyzed




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Matrix: Solid

Analyzed

Dibromomethane ug/kg ND 5.0 09/07/10 20:13Dichlorodifluoromethane ug/kg ND 5.0 09/07/10 20:13Ethyl methacrylate ug/kg ND 10.0 09/07/10 20:13Ethylbenzene ug/kg ND 5.0 09/07/10 20:13Hexachloro-1,3-butadiene ug/kg ND 5.0 09/07/10 20:13Iodomethane ug/kg ND 100 09/07/10 20:13Isopropylbenzene (Cumene) ug/kg ND 5.0 09/07/10 20:13Methyl-tert-butyl ether ug/kg ND 5.0 09/07/10 20:13Methylene chloride ug/kg ND 20.0 09/07/10 20:13n-Butylbenzene ug/kg ND 5.0 09/07/10 20:13n-Hexane ug/kg ND 5.0 09/07/10 20:13n-Propylbenzene ug/kg ND 5.0 09/07/10 20:13Naphthalene ug/kg ND 5.0 09/07/10 20:13p-Isopropyltoluene ug/kg ND 5.0 09/07/10 20:13sec-Butylbenzene ug/kg ND 5.0 09/07/10 20:13Styrene ug/kg ND 5.0 09/07/10 20:13tert-Butylbenzene ug/kg ND 5.0 09/07/10 20:13Tetrachloroethene ug/kg ND 5.0 09/07/10 20:13Toluene ug/kg ND 5.0 09/07/10 20:13trans-1,2-Dichloroethene ug/kg ND 5.0 09/07/10 20:13trans-1,3-Dichloropropene ug/kg ND 5.0 09/07/10 20:13trans-1,4-Dichloro-2-butene ug/kg ND 100 09/07/10 20:13Trichloroethene ug/kg ND 5.0 09/07/10 20:13Trichlorofluoromethane ug/kg ND 5.0 09/07/10 20:13Vinyl acetate ug/kg ND 100 09/07/10 20:13Vinyl chloride ug/kg ND 5.0 09/07/10 20:13Xylene (Total) ug/kg ND 10.0 09/07/10 20:134-Bromofluorobenzene (S) % 99 61-131 09/07/10 20:13Dibromofluoromethane (S) % 95 80-124 09/07/10 20:13Toluene-d8 (S) % 107 58-145 09/07/10 20:13

Parameter UnitsLCS



1,1,1,2-Tetrachloroethane ug/kg 48.950 98 65-1241,1,1-Trichloroethane ug/kg 45.250 90 61-1351,1,2,2-Tetrachloroethane ug/kg 46.550 93 66-1241,1,2-Trichloroethane ug/kg 52.050 104 74-1271,1-Dichloroethane ug/kg 45.050 90 62-1321,1-Dichloroethene ug/kg 45.850 92 61-1231,1-Dichloropropene ug/kg 47.750 95 74-1281,2,3-Trichlorobenzene ug/kg 44.750 89 60-1251,2,3-Trichloropropane ug/kg 81.3100 81 61-1201,2,4-Trichlorobenzene ug/kg 41.950 84 58-1261,2,4-Trimethylbenzene ug/kg 48.150 96 72-120



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Parameter UnitsLCS



1,2-Dibromoethane (EDB) ug/kg 55.150 110 74-1191,2-Dichlorobenzene ug/kg 47.750 95 75-1171,2-Dichloroethane ug/kg 41.150 82 62-1351,2-Dichloropropane ug/kg 48.750 97 74-1241,3,5-Trimethylbenzene ug/kg 47.950 96 73-1221,3-Dichlorobenzene ug/kg 49.350 99 73-1201,3-Dichloropropane ug/kg 52.150 104 71-1221,4-Dichlorobenzene ug/kg 48.650 97 72-1182,2-Dichloropropane ug/kg 47.250 94 53-1362-Butanone (MEK) ug/kg 245250 98 33-1902-Chlorotoluene ug/kg 46.750 93 72-1222-Hexanone ug/kg 278250 111 44-1684-Chlorotoluene ug/kg 45.150 90 72-1204-Methyl-2-pentanone (MIBK) ug/kg 262250 105 58-126Acetone ug/kg 327250 131 30-190Acrolein ug/kg 2010 L31000 201 30-190Acrylonitrile ug/kg 9241000 92 65-129Benzene ug/kg 52.350 105 76-123Bromobenzene ug/kg 51.050 102 74-116Bromochloromethane ug/kg 48.450 97 56-143Bromodichloromethane ug/kg 43.150 86 67-123Bromoform ug/kg 37.550 75 58-117Bromomethane ug/kg 49.650 99 47-147Carbon disulfide ug/kg 85.6100 86 56-141Carbon tetrachloride ug/kg 42.750 85 54-136Chlorobenzene ug/kg 48.750 97 75-115Chloroethane ug/kg 56.750 113 57-147Chloroform ug/kg 41.250 82 74-123Chloromethane ug/kg 49.450 99 31-155cis-1,2-Dichloroethene ug/kg 50.650 101 76-119cis-1,3-Dichloropropene ug/kg 44.550 89 56-110Dibromochloromethane ug/kg 45.750 91 63-122Dibromomethane ug/kg 49.850 100 70-127Dichlorodifluoromethane ug/kg 51.350 103 30-170Ethyl methacrylate ug/kg 186200 93 58-126Ethylbenzene ug/kg 49.150 98 78-121Hexachloro-1,3-butadiene ug/kg 44.550 89 65-128Iodomethane ug/kg 88.2J100 88 38-173Isopropylbenzene (Cumene) ug/kg 51.050 102 75-128Methyl-tert-butyl ether ug/kg 88.9100 89 59-142Methylene chloride ug/kg 45.350 91 30-170n-Butylbenzene ug/kg 51.150 102 70-123n-Hexane ug/kg 49.950 100 76-143n-Propylbenzene ug/kg 46.750 93 70-126Naphthalene ug/kg 45.250 90 60-128p-Isopropyltoluene ug/kg 49.450 99 65-125sec-Butylbenzene ug/kg 49.450 99 72-125Styrene ug/kg 49.350 99 75-118



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Parameter UnitsLCS



tert-Butylbenzene ug/kg 37.550 75 61-114Tetrachloroethene ug/kg 47.850 96 63-117Toluene ug/kg 50.250 100 72-123trans-1,2-Dichloroethene ug/kg 48.250 96 70-122trans-1,3-Dichloropropene ug/kg 40.050 80 55-107trans-1,4-Dichloro-2-butene ug/kg 214200 107 49-127Trichloroethene ug/kg 47.550 95 74-121Trichlorofluoromethane ug/kg 47.350 95 55-156Vinyl acetate ug/kg 167200 83 46-127Vinyl chloride ug/kg 49.450 99 50-146Xylene (Total) ug/kg 148150 98 77-1204-Bromofluorobenzene (S) % 103 61-131Dibromofluoromethane (S) % 92 80-124Toluene-d8 (S) % 101 58-145

Parameter UnitsMS



MSSpikeResult

5040885017

477305

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1,2-Tetrachloroethane ug/kg 36.9 69 20-13351 33 2035.9ND 25.5 18.21,1,1-Trichloroethane ug/kg 36.9 82 27-14287 2 2035.9ND 31.6 32.31,1,2,2-Tetrachloroethane ug/kg 36.9 55 20-15948 17 2035.9ND 20.5 17.21,1,2-Trichloroethane ug/kg 36.9 71 20-15557 25 2035.9ND 26.3 20.61,1-Dichloroethane ug/kg 36.9 82 31-14177 8 2035.9ND 30.2 27.81,1-Dichloroethene ug/kg 36.9 85 23-13284 4 2035.9ND 31.5 30.11,1-Dichloropropene ug/kg 36.9 79 20-14677 5 2035.9ND 29.1 27.71,2,3-Trichlorobenzene ug/kg 36.9 24 20-14020 23 2035.9ND 8.9 7.11,2,3-Trichloropropane ug/kg 74 47 20-15339 22 2071.7ND 34.8 27.91,2,4-Trichlorobenzene ug/kg 36.9 25 20-12021 22 2035.9ND 9.2 7.41,2,4-Trimethylbenzene ug/kg 36.9 52 20-15644 19 2035.9ND 19.2 15.91,2-Dibromoethane (EDB) ug/kg 36.9 72 20-14358 25 2035.9ND 26.8 20.91,2-Dichlorobenzene ug/kg 36.9 41 20-13334 21 2035.9ND 15.2 12.31,2-Dichloroethane ug/kg 36.9 68 30-14365 8 2035.9ND 25.2 23.21,2-Dichloropropane ug/kg 36.9 74 30-14067 12 2035.9ND 27.2 24.01,3,5-Trimethylbenzene ug/kg 36.9 54 20-14349 13 2035.9ND 20.0 17.61,3-Dichlorobenzene ug/kg 36.9 45 20-13637 22 2035.9ND 16.5 13.21,3-Dichloropropane ug/kg 36.9 70 30-14460 18 2035.9ND 25.9 21.71,4-Dichlorobenzene ug/kg 36.9 44 30-13535 24 2035.9ND 16.1 12.62,2-Dichloropropane ug/kg 36.9 79 30-14378 4 2035.9ND 29.1 28.12-Butanone (MEK) ug/kg 185 82 30-19075 11 20179ND 151 1342-Chlorotoluene ug/kg 36.9 54 30-17050 11 2035.9ND 19.8 17.82-Hexanone ug/kg 185 80 30-17076 8 20179ND 149 1374-Chlorotoluene ug/kg 36.9 48 30-14341 18 2035.9ND 17.8 14.94-Methyl-2-pentanone (MIBK) ug/kg 185 80 30-14463 26 20179ND 148 114Acetone ug/kg 185 118 30-180115 6 20179ND 217 206Acrolein ug/kg 740 157 30-180138 16 20717ND 1160 987Acrylonitrile ug/kg 740 72 30-14165 12 20717ND 530 469



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Parameter UnitsMS



MSSpikeResult

5040885017

477305

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Benzene ug/kg 36.9 79 50-13572 13 2035.9ND 29.3 25.7Bromobenzene ug/kg 36.9 59 30-12542 37 2035.9ND 22.0 15.2Bromochloromethane ug/kg 36.9 80 30-15972 13 2035.9ND 29.5 25.8Bromodichloromethane ug/kg 36.9 61 30-14156 12 2035.9ND 22.7 20.2Bromoform ug/kg 36.9 47 30-13543 13 2035.9ND 17.5 15.4Bromomethane ug/kg 36.9 89 30-13788 3 2035.9ND 32.8 31.7Carbon disulfide ug/kg 74 78 30-15676 7 2071.7ND 58.0 54.4Carbon tetrachloride ug/kg 36.9 75 30-13077 .5 2035.9ND 27.6 27.4Chlorobenzene ug/kg 36.9 61 30-13751 20 2035.9ND 22.5 18.4Chloroethane ug/kg 36.9 104 35-143103 4 2035.9ND 38.6 37.0Chloroform ug/kg 36.9 69 30-13665 10 2035.9ND 25.6 23.2Chloromethane ug/kg 36.9 105 28-134101 7 2035.9ND 38.9 36.3cis-1,2-Dichloroethene ug/kg 36.9 82 30-14177 10 2035.9ND 30.4 27.5cis-1,3-Dichloropropene ug/kg 36.9 62 30-12644 37 2035.9ND 22.7 15.6Dibromochloromethane ug/kg 36.9 65 30-12948 34 2035.9ND 24.1 17.1Dibromomethane ug/kg 36.9 71 30-15363 15 2035.9ND 26.2 22.6Dichlorodifluoromethane ug/kg 36.9 132 30-150126 7 2035.9ND 48.7 45.2Ethyl methacrylate ug/kg 147 58 30-17056 6 20143ND 85.6 80.7Ethylbenzene ug/kg 36.9 67 50-15056 20 2035.9ND 24.7 20.1Hexachloro-1,3-butadiene ug/kg 36.9 36 30-13831 19 2035.9ND 13.4 11.1Iodomethane ug/kg 74 75 30-18069 2071.7ND 55.6J 49.4JIsopropylbenzene (Cumene) ug/kg 36.9 67 50-15052 29 2035.9ND 24.8 18.5Methyl-tert-butyl ether ug/kg 74 75 40-14967 14 2071.7ND 55.4 48.0Methylene chloride ug/kg 36.9 76 30-16366 17 2035.9ND 28.1 23.6n-Butylbenzene ug/kg 36.9 47 40-15237 26 2035.9ND 17.4 13.4n-Hexane ug/kg 36.9 89 40-15591 1 2035.9ND 32.9 32.5n-Propylbenzene ug/kg 36.9 56 40-17051 12 2035.9ND 20.8 18.3Naphthalene ug/kg M036.9 31 50-12823 30 2035.9ND 11.3 8.3p-Isopropyltoluene ug/kg 36.9 52 40-16745 17 2035.9ND 19.1 16.1sec-Butylbenzene ug/kg 36.9 55 40-16849 15 2035.9ND 20.4 17.6Styrene ug/kg 36.9 60 30-14147 28 2035.9ND 22.3 16.8tert-Butylbenzene ug/kg 36.9 46 40-14441 13 2035.9ND 16.9 14.8Tetrachloroethene ug/kg 36.9 68 40-15558 19 2035.9ND 25.1 20.8Toluene ug/kg 36.9 80 50-14963 26 2035.9ND 29.4 22.7trans-1,2-Dichloroethene ug/kg 36.9 81 40-14076 9 2035.9ND 29.9 27.3trans-1,3-Dichloropropene ug/kg 36.9 51 40-13040 28 2035.9ND 18.9 14.2trans-1,4-Dichloro-2-butene ug/kg 147 65 30-15040 20143ND 96.0 57.6JTrichloroethene ug/kg 36.9 72 40-15368 8 2035.9ND 26.7 24.5Trichlorofluoromethane ug/kg 36.9 101 43-140101 3 2035.9ND 37.3 36.1Vinyl acetate ug/kg 147 34 30-12029 20143ND 50.1J 41.4JVinyl chloride ug/kg 36.9 97 36-13796 4 2035.9ND 36.0 34.5Xylene (Total) ug/kg 111 66 50-14353 25 20108ND 73.2 56.84-Bromofluorobenzene (S) % 108 61-13197 20Dibromofluoromethane (S) % 2d98 80-124100 20Toluene-d8 (S) % 111 58-14598 20



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MSV/26479EPA 8260







Matrix: Solid

Analyzed




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Matrix: Solid

Analyzed


Parameter UnitsLCS






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Parameter UnitsLCS



1,2-Dichlorobenzene ug/kg 41.050 82 75-1171,2-Dichloroethane ug/kg 44.850 90 62-1351,2-Dichloropropane ug/kg 43.550 87 74-1241,3,5-Trimethylbenzene ug/kg 40.850 82 73-1221,3-Dichlorobenzene ug/kg 41.250 82 73-1201,3-Dichloropropane ug/kg 47.350 95 71-1221,4-Dichlorobenzene ug/kg 40.750 81 72-1182,2-Dichloropropane ug/kg 42.150 84 53-1362-Butanone (MEK) ug/kg 222250 89 33-1902-Chlorotoluene ug/kg 41.350 83 72-1222-Hexanone ug/kg 225250 90 44-1684-Chlorotoluene ug/kg 38.450 77 72-1204-Methyl-2-pentanone (MIBK) ug/kg 225250 90 58-126Acetone ug/kg 230250 92 30-190Acrolein ug/kg 18101000 181 30-190Acrylonitrile ug/kg 8791000 88 65-129Benzene ug/kg 44.250 88 76-123Bromobenzene ug/kg 45.450 91 74-116Bromochloromethane ug/kg 47.650 95 56-143Bromodichloromethane ug/kg 42.650 85 67-123Bromoform ug/kg 36.050 72 58-117Bromomethane ug/kg 47.850 96 47-147Carbon disulfide ug/kg 81.3100 81 56-141Carbon tetrachloride ug/kg 42.550 85 54-136Chlorobenzene ug/kg 42.650 85 75-115Chloroethane ug/kg 52.950 106 57-147Chloroform ug/kg 40.750 81 74-123Chloromethane ug/kg 47.550 95 31-155cis-1,2-Dichloroethene ug/kg 47.550 95 76-119cis-1,3-Dichloropropene ug/kg 38.150 76 56-110Dibromochloromethane ug/kg 42.450 85 63-122Dibromomethane ug/kg 45.450 91 70-127Dichlorodifluoromethane ug/kg 48.250 96 30-170Ethyl methacrylate ug/kg 172200 86 58-126Ethylbenzene ug/kg 43.750 87 78-121Hexachloro-1,3-butadiene ug/kg 39.250 78 65-128Iodomethane ug/kg 79J100 79 38-173Isopropylbenzene (Cumene) ug/kg 45.150 90 75-128Methyl-tert-butyl ether ug/kg 85.4100 85 59-142Methylene chloride ug/kg 42.250 84 30-170n-Butylbenzene ug/kg 43.350 87 70-123n-Propylbenzene ug/kg 41.550 83 70-126Naphthalene ug/kg 40.950 82 60-128p-Isopropyltoluene ug/kg 41.750 83 65-125sec-Butylbenzene ug/kg 42.250 84 72-125Styrene ug/kg 43.950 88 75-118tert-Butylbenzene ug/kg 31.450 63 61-114Tetrachloroethene ug/kg 39.850 80 63-117



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Parameter UnitsLCS






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PMST/5013ASTM D2974-87

ASTM D2974-87Dry Weight/Percent Moisture

Associated Lab Samples: 5040885002, 5040885003, 5040885004, 5040885005, 5040885006, 5040885007, 5040885008, 5040885009,5040885010, 5040885012, 5040885014, 5040885015, 5040885016, 5040885017

Parameter UnitsDup

ResultMaxRPD QualifiersRPDResult

5040885017475588SAMPLE DUPLICATE:

Percent Moisture % 11.9 5 512.5



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Parameter UnitsDup




Parameter UnitsDup



Percent Moisture % 18.7 .7 518.8



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(317)875-5894

QUALIFIERS



DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.S - Surrogate1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.U - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.

LABORATORIES

Pace Analytical Services - IndianapolisPASI-I

ANALYTE QUALIFIERSMultiple compounds are outside acceptance limits due to sample matrix. Refer to LCS for system control and dataacceptability. JLF 09/08/10.

1d

RPD value was outside control limits for several compounds. Refer to batch QC for control. RSW 09/08/102dAnalyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

L3

Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0RPD value was outside control limits.R1



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September 10, 2010



RE:


Frank's Foundry



Sincerely,

Mark Davis



Enclosures



Page 1 of 45



(317)875-5894

SAMPLE SUMMARY




5040967001 SB-3R (2-3) Solid 09/01/10 08:00 09/02/10 11:55

5040967002 SB-11 (0.5-1.0) Solid 09/01/10 08:00 09/02/10 11:55

5040967003 SB-12 (0.5-1.0) Solid 09/01/10 08:00 09/02/10 11:55

5040967004 SB-13 (0.25-0.5) Solid 09/01/10 08:00 09/02/10 11:55

5040967005 SB-15 (0.25-0.5) Solid 09/01/10 08:00 09/02/10 11:55

5040967006 TRIP BLANK Water 09/01/10 08:00 09/02/10 11:55

5040967007 SB-13 (4-5) Solid 09/01/10 08:00 09/02/10 11:55

5040967008 TW-14 Water 09/01/10 11:41 09/02/10 11:55

5040967009 TW-2 Water 09/01/10 14:17 09/02/10 11:55

5040967010 TW-2 FD Water 09/01/10 14:17 09/02/10 11:55



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5040967001 SB-3R (2-3) EPA 6010 7 PASI-IFRW


EPA 8270 by SIM 19 PASI-IRRB

EPA 8260 72 PASI-IRSW


5040967002 SB-11 (0.5-1.0) EPA 6010 7 PASI-IFRW




5040967003 SB-12 (0.5-1.0) EPA 6010 7 PASI-IFRW



5040967004 SB-13 (0.25-0.5) EPA 6010 7 PASI-IFRW



5040967005 SB-15 (0.25-0.5) EPA 8270 by SIM 19 PASI-IRRB



5040967006 TRIP BLANK EPA 8260 73 PASI-IRSW

5040967007 SB-13 (4-5) EPA 8260 72 PASI-IRSW


5040967008 TW-14 EPA 6010 7 PASI-ILLB




5040967009 TW-2 EPA 6010 7 PASI-ILLB




5040967010 TW-2 FD EPA 6010 7 PASI-ILLB






Page 3 of 45



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ANALYTICAL RESULTS



Sample: SB-3R (2-3) Lab ID: 5040967001 Collected: 09/01/10 08:00 Received: 09/02/10 11:55 Matrix: SolidResults reported on a "dry-weight" basis





Mercury ND mg/kg 1 09/08/10 13:15 7439-97-609/03/10 00:000.40




Acetone ND ug/kg 1 09/09/10 22:30 67-64-183.1Acrolein ND ug/kg 1 09/09/10 22:30 107-02-883.1Acrylonitrile ND ug/kg 1 09/09/10 22:30 107-13-183.1Benzene ND ug/kg 1 09/09/10 22:30 71-43-24.2Bromobenzene ND ug/kg 1 09/09/10 22:30 108-86-14.2Bromochloromethane ND ug/kg 1 09/09/10 22:30 74-97-54.2Bromodichloromethane ND ug/kg 1 09/09/10 22:30 75-27-44.2Bromoform ND ug/kg 1 09/09/10 22:30 75-25-24.2Bromomethane ND ug/kg 1 09/09/10 22:30 74-83-94.22-Butanone (MEK) ND ug/kg 1 09/09/10 22:30 78-93-320.8n-Butylbenzene ND ug/kg 1 09/09/10 22:30 104-51-84.2sec-Butylbenzene ND ug/kg 1 09/09/10 22:30 135-98-84.2



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ANALYTICAL RESULTS






tert-Butylbenzene ND ug/kg 1 09/09/10 22:30 98-06-64.2Carbon disulfide ND ug/kg 1 09/09/10 22:30 75-15-08.3Carbon tetrachloride ND ug/kg 1 09/09/10 22:30 56-23-54.2Chlorobenzene ND ug/kg 1 09/09/10 22:30 108-90-74.2Chloroethane ND ug/kg 1 09/09/10 22:30 75-00-34.2Chloroform ND ug/kg 1 09/09/10 22:30 67-66-34.2Chloromethane ND ug/kg 1 09/09/10 22:30 74-87-34.22-Chlorotoluene ND ug/kg 1 09/09/10 22:30 95-49-84.24-Chlorotoluene ND ug/kg 1 09/09/10 22:30 106-43-44.2Dibromochloromethane ND ug/kg 1 09/09/10 22:30 124-48-14.21,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 22:30 106-93-44.2Dibromomethane ND ug/kg 1 09/09/10 22:30 74-95-34.21,2-Dichlorobenzene ND ug/kg 1 09/09/10 22:30 95-50-14.21,3-Dichlorobenzene ND ug/kg 1 09/09/10 22:30 541-73-14.21,4-Dichlorobenzene ND ug/kg 1 09/09/10 22:30 106-46-74.2trans-1,4-Dichloro-2-butene ND ug/kg 1 09/09/10 22:30 110-57-683.1Dichlorodifluoromethane ND ug/kg 1 09/09/10 22:30 75-71-84.21,1-Dichloroethane ND ug/kg 1 09/09/10 22:30 75-34-34.21,2-Dichloroethane ND ug/kg 1 09/09/10 22:30 107-06-24.21,1-Dichloroethene ND ug/kg 1 09/09/10 22:30 75-35-44.2cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 22:30 156-59-24.2trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 22:30 156-60-54.21,2-Dichloropropane ND ug/kg 1 09/09/10 22:30 78-87-54.21,3-Dichloropropane ND ug/kg 1 09/09/10 22:30 142-28-94.22,2-Dichloropropane ND ug/kg 1 09/09/10 22:30 594-20-74.21,1-Dichloropropene ND ug/kg 1 09/09/10 22:30 563-58-64.2cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 22:30 10061-01-54.2trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 22:30 10061-02-64.2Ethylbenzene ND ug/kg 1 09/09/10 22:30 100-41-44.2Ethyl methacrylate ND ug/kg 1 09/09/10 22:30 97-63-28.3Hexachloro-1,3-butadiene ND ug/kg 1 09/09/10 22:30 87-68-34.22-Hexanone ND ug/kg 1 09/09/10 22:30 591-78-683.1Iodomethane ND ug/kg 1 09/09/10 22:30 74-88-483.1Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 22:30 98-82-84.2p-Isopropyltoluene ND ug/kg 1 09/09/10 22:30 99-87-64.2Methylene chloride ND ug/kg 1 09/09/10 22:30 75-09-216.64-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 22:30 108-10-120.8Methyl-tert-butyl ether ND ug/kg 1 09/09/10 22:30 1634-04-44.2Naphthalene ND ug/kg 1 09/09/10 22:30 91-20-34.2n-Propylbenzene ND ug/kg 1 09/09/10 22:30 103-65-14.2Styrene ND ug/kg 1 09/09/10 22:30 100-42-54.21,1,1,2-Tetrachloroethane ND ug/kg 1 09/09/10 22:30 630-20-64.21,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 22:30 79-34-54.2Tetrachloroethene ND ug/kg 1 09/09/10 22:30 127-18-44.2Toluene ND ug/kg 1 09/09/10 22:30 108-88-34.21,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 22:30 87-61-64.2



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ANALYTICAL RESULTS






1,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 22:30 120-82-14.21,1,1-Trichloroethane ND ug/kg 1 09/09/10 22:30 71-55-64.21,1,2-Trichloroethane ND ug/kg 1 09/09/10 22:30 79-00-54.2Trichloroethene ND ug/kg 1 09/09/10 22:30 79-01-64.2Trichlorofluoromethane ND ug/kg 1 09/09/10 22:30 75-69-44.21,2,3-Trichloropropane ND ug/kg 1 09/09/10 22:30 96-18-44.21,2,4-Trimethylbenzene ND ug/kg 1 09/09/10 22:30 95-63-64.21,3,5-Trimethylbenzene ND ug/kg 1 09/09/10 22:30 108-67-84.2Vinyl acetate ND ug/kg 1 09/09/10 22:30 108-05-483.1Vinyl chloride ND ug/kg 1 09/09/10 22:30 75-01-44.2Xylene (Total) ND ug/kg 1 09/09/10 22:30 1330-20-78.3Dibromofluoromethane (S) 91 % 1 09/09/10 22:30 1868-53-780-124Toluene-d8 (S) 96 % 1 09/09/10 22:30 2037-26-558-1454-Bromofluorobenzene (S) 116 % 1 09/09/10 22:30 460-00-461-131





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Sample: SB-11 (0.5-1.0) Lab ID: 5040967002 Collected: 09/01/10 08:00 Received: 09/02/10 11:55 Matrix: SolidResults reported on a "dry-weight" basis





Mercury ND mg/kg 1 09/08/10 13:20 7439-97-609/03/10 00:000.40


Acenaphthene ND ug/kg 1 09/08/10 03:57 83-32-909/03/10 10:4530.2Acenaphthylene ND ug/kg 1 09/08/10 03:57 208-96-809/03/10 10:4530.2Anthracene ND ug/kg 1 09/08/10 03:57 120-12-709/03/10 10:4530.2Benzo(a)anthracene 38.0 ug/kg 1 09/08/10 03:57 56-55-309/03/10 10:4530.2Benzo(a)pyrene 46.5 ug/kg 1 09/08/10 03:57 50-32-809/03/10 10:4530.2Benzo(b)fluoranthene 43.5 ug/kg 1 09/08/10 03:57 205-99-209/03/10 10:4530.2Benzo(g,h,i)perylene 30.8 ug/kg 1 09/08/10 03:57 191-24-209/03/10 10:4530.2Benzo(k)fluoranthene 44.6 ug/kg 1 09/08/10 03:57 207-08-909/03/10 10:4530.2Chrysene 53.1 ug/kg 1 09/08/10 03:57 218-01-909/03/10 10:4530.2Dibenz(a,h)anthracene ND ug/kg 1 09/08/10 03:57 53-70-309/03/10 10:4530.2Fluoranthene 37.7 ug/kg 1 09/08/10 03:57 206-44-009/03/10 10:4530.2Fluorene ND ug/kg 1 09/08/10 03:57 86-73-709/03/10 10:4530.2Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/08/10 03:57 193-39-509/03/10 10:4530.22-Methylnaphthalene 30.9 ug/kg 1 09/08/10 03:57 91-57-609/03/10 10:4530.2Naphthalene 33.6 ug/kg 1 09/08/10 03:57 91-20-309/03/10 10:4530.2Phenanthrene ND ug/kg 1 09/08/10 03:57 85-01-809/03/10 10:4530.2Pyrene 44.0 ug/kg 1 09/08/10 03:57 129-00-009/03/10 10:4530.22-Fluorobiphenyl (S) 73 % 1 09/08/10 03:57 321-60-809/03/10 10:4545-120Terphenyl-d14 (S) 65 % 1 09/08/10 03:57 1718-51-009/03/10 10:4541-120





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Mercury ND mg/kg 1 09/08/10 13:21 7439-97-609/03/10 00:000.42





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Mercury ND mg/kg 1 09/08/10 13:22 7439-97-609/03/10 00:000.38





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Acetone ND ug/kg 1 09/09/10 23:07 67-64-194.4Acrolein ND ug/kg 1 09/09/10 23:07 107-02-894.4Acrylonitrile ND ug/kg 1 09/09/10 23:07 107-13-194.4Benzene ND ug/kg 1 09/09/10 23:07 71-43-24.7Bromobenzene ND ug/kg 1 09/09/10 23:07 108-86-14.7Bromochloromethane ND ug/kg 1 09/09/10 23:07 74-97-54.7Bromodichloromethane ND ug/kg 1 09/09/10 23:07 75-27-44.7Bromoform ND ug/kg 1 09/09/10 23:07 75-25-24.7Bromomethane ND ug/kg 1 09/09/10 23:07 74-83-94.72-Butanone (MEK) ND ug/kg 1 09/09/10 23:07 78-93-323.6n-Butylbenzene ND ug/kg 1 09/09/10 23:07 104-51-84.7sec-Butylbenzene ND ug/kg 1 09/09/10 23:07 135-98-84.7tert-Butylbenzene ND ug/kg 1 09/09/10 23:07 98-06-64.7Carbon disulfide ND ug/kg 1 09/09/10 23:07 75-15-09.4Carbon tetrachloride ND ug/kg 1 09/09/10 23:07 56-23-54.7Chlorobenzene ND ug/kg 1 09/09/10 23:07 108-90-74.7Chloroethane ND ug/kg 1 09/09/10 23:07 75-00-34.7Chloroform ND ug/kg 1 09/09/10 23:07 67-66-34.7Chloromethane ND ug/kg 1 09/09/10 23:07 74-87-34.72-Chlorotoluene ND ug/kg 1 09/09/10 23:07 95-49-84.74-Chlorotoluene ND ug/kg 1 09/09/10 23:07 106-43-44.7Dibromochloromethane ND ug/kg 1 09/09/10 23:07 124-48-14.71,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 23:07 106-93-44.7Dibromomethane ND ug/kg 1 09/09/10 23:07 74-95-34.71,2-Dichlorobenzene ND ug/kg 1 09/09/10 23:07 95-50-14.7



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1,3-Dichlorobenzene ND ug/kg 1 09/09/10 23:07 541-73-14.71,4-Dichlorobenzene ND ug/kg 1 09/09/10 23:07 106-46-74.7trans-1,4-Dichloro-2-butene ND ug/kg 1 09/09/10 23:07 110-57-694.4Dichlorodifluoromethane ND ug/kg 1 09/09/10 23:07 75-71-84.71,1-Dichloroethane ND ug/kg 1 09/09/10 23:07 75-34-34.71,2-Dichloroethane ND ug/kg 1 09/09/10 23:07 107-06-24.71,1-Dichloroethene ND ug/kg 1 09/09/10 23:07 75-35-44.7cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 23:07 156-59-24.7trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 23:07 156-60-54.71,2-Dichloropropane ND ug/kg 1 09/09/10 23:07 78-87-54.71,3-Dichloropropane ND ug/kg 1 09/09/10 23:07 142-28-94.72,2-Dichloropropane ND ug/kg 1 09/09/10 23:07 594-20-74.71,1-Dichloropropene ND ug/kg 1 09/09/10 23:07 563-58-64.7cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 23:07 10061-01-54.7trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 23:07 10061-02-64.7Ethylbenzene ND ug/kg 1 09/09/10 23:07 100-41-44.7Ethyl methacrylate ND ug/kg 1 09/09/10 23:07 97-63-29.4Hexachloro-1,3-butadiene ND ug/kg 1 09/09/10 23:07 87-68-34.72-Hexanone ND ug/kg 1 09/09/10 23:07 591-78-694.4Iodomethane ND ug/kg 1 09/09/10 23:07 74-88-494.4Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 23:07 98-82-84.7p-Isopropyltoluene ND ug/kg 1 09/09/10 23:07 99-87-64.7Methylene chloride ND ug/kg 1 09/09/10 23:07 75-09-218.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 23:07 108-10-123.6Methyl-tert-butyl ether ND ug/kg 1 09/09/10 23:07 1634-04-44.7Naphthalene ND ug/kg 1 09/09/10 23:07 91-20-34.7n-Propylbenzene ND ug/kg 1 09/09/10 23:07 103-65-14.7Styrene ND ug/kg 1 09/09/10 23:07 100-42-54.71,1,1,2-Tetrachloroethane ND ug/kg 1 09/09/10 23:07 630-20-64.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 23:07 79-34-54.7Tetrachloroethene ND ug/kg 1 09/09/10 23:07 127-18-44.7Toluene ND ug/kg 1 09/09/10 23:07 108-88-34.71,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 23:07 87-61-64.71,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 23:07 120-82-14.71,1,1-Trichloroethane ND ug/kg 1 09/09/10 23:07 71-55-64.71,1,2-Trichloroethane ND ug/kg 1 09/09/10 23:07 79-00-54.7Trichloroethene ND ug/kg 1 09/09/10 23:07 79-01-64.7Trichlorofluoromethane ND ug/kg 1 09/09/10 23:07 75-69-44.71,2,3-Trichloropropane ND ug/kg 1 09/09/10 23:07 96-18-44.71,2,4-Trimethylbenzene ND ug/kg 1 09/09/10 23:07 95-63-64.71,3,5-Trimethylbenzene ND ug/kg 1 09/09/10 23:07 108-67-84.7Vinyl acetate ND ug/kg 1 09/09/10 23:07 108-05-494.4Vinyl chloride ND ug/kg 1 09/09/10 23:07 75-01-44.7Xylene (Total) ND ug/kg 1 09/09/10 23:07 1330-20-79.4Dibromofluoromethane (S) 92 % 1 09/09/10 23:07 1868-53-780-124Toluene-d8 (S) 101 % 1 09/09/10 23:07 2037-26-558-145



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4-Bromofluorobenzene (S) 96 % 1 09/09/10 23:07 460-00-461-131





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Sample: TW-14 Lab ID: 5040967008 Collected: 09/01/10 11:41 Received: 09/02/10 11:55 Matrix: Water



Arsenic ND ug/L 1 09/10/10 09:05 7440-38-209/07/10 00:0010.0Barium 144 ug/L 1 09/10/10 09:05 7440-39-309/07/10 00:00100Cadmium ND ug/L 1 09/10/10 09:05 7440-43-909/07/10 00:005.0Chromium ND ug/L 1 09/10/10 09:05 7440-47-309/07/10 00:0010.0Lead ND ug/L 1 09/10/10 09:05 7439-92-109/07/10 00:0010.0Selenium ND ug/L 1 09/10/10 09:05 7782-49-209/07/10 00:0010.0Silver ND ug/L 1 09/10/10 09:05 7440-22-409/07/10 00:0050.0


Mercury ND ug/L 1 09/08/10 11:44 7439-97-609/07/10 00:002.0

8270 MSSV PAH by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510

Acenaphthene ND ug/L 1 09/07/10 16:30 83-32-909/03/10 17:301.1Acenaphthylene ND ug/L 1 09/07/10 16:30 208-96-809/03/10 17:301.1Anthracene ND ug/L 1 09/07/10 16:30 120-12-709/03/10 17:300.11Benzo(a)anthracene ND ug/L 1 09/07/10 16:30 56-55-309/03/10 17:300.11Benzo(a)pyrene ND ug/L 1 09/07/10 16:30 50-32-809/03/10 17:300.11Benzo(b)fluoranthene ND ug/L 1 09/07/10 16:30 205-99-209/03/10 17:300.11Benzo(g,h,i)perylene ND ug/L 1 09/07/10 16:30 191-24-209/03/10 17:300.11Benzo(k)fluoranthene ND ug/L 1 09/07/10 16:30 207-08-909/03/10 17:300.11Chrysene ND ug/L 1 09/07/10 16:30 218-01-909/03/10 17:300.57Dibenz(a,h)anthracene ND ug/L 1 09/07/10 16:30 53-70-309/03/10 17:300.11Fluoranthene ND ug/L 1 09/07/10 16:30 206-44-009/03/10 17:301.1Fluorene ND ug/L 1 09/07/10 16:30 86-73-709/03/10 17:301.1Indeno(1,2,3-cd)pyrene ND ug/L 1 09/07/10 16:30 193-39-509/03/10 17:300.112-Methylnaphthalene ND ug/L 1 09/07/10 16:30 91-57-609/03/10 17:301.1Naphthalene ND ug/L 1 09/07/10 16:30 91-20-309/03/10 17:301.1Phenanthrene ND ug/L 1 09/07/10 16:30 85-01-809/03/10 17:301.1Pyrene ND ug/L 1 09/07/10 16:30 129-00-009/03/10 17:301.12-Fluorobiphenyl (S) 67 % 1 09/07/10 16:30 321-60-809/03/10 17:3035-116Terphenyl-d14 (S) 72 % 1 09/07/10 16:30 1718-51-009/03/10 17:3025-117


Acetone ND ug/L 1 09/09/10 17:17 67-64-1100Acrolein ND ug/L 1 09/09/10 17:17 107-02-850.0Acrylonitrile ND ug/L 1 09/09/10 17:17 107-13-1100Benzene ND ug/L 1 09/09/10 17:17 71-43-25.0Bromobenzene ND ug/L 1 09/09/10 17:17 108-86-15.0Bromochloromethane ND ug/L 1 09/09/10 17:17 74-97-55.0Bromodichloromethane ND ug/L 1 09/09/10 17:17 75-27-45.0Bromoform ND ug/L 1 09/09/10 17:17 75-25-25.0Bromomethane ND ug/L 1 09/09/10 17:17 74-83-95.02-Butanone (MEK) ND ug/L 1 09/09/10 17:17 78-93-325.0n-Butylbenzene ND ug/L 1 09/09/10 17:17 104-51-85.0sec-Butylbenzene ND ug/L 1 09/09/10 17:17 135-98-85.0tert-Butylbenzene ND ug/L 1 09/09/10 17:17 98-06-65.0



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Carbon disulfide ND ug/L 1 09/09/10 17:17 75-15-010.0Carbon tetrachloride ND ug/L 1 09/09/10 17:17 56-23-55.0Chlorobenzene ND ug/L 1 09/09/10 17:17 108-90-75.0Chloroethane ND ug/L 1 09/09/10 17:17 75-00-35.0Chloroform ND ug/L 1 09/09/10 17:17 67-66-35.0Chloromethane ND ug/L 1 09/09/10 17:17 74-87-35.02-Chlorotoluene ND ug/L 1 09/09/10 17:17 95-49-85.04-Chlorotoluene ND ug/L 1 09/09/10 17:17 106-43-45.0Dibromochloromethane ND ug/L 1 09/09/10 17:17 124-48-15.01,2-Dibromoethane (EDB) ND ug/L 1 09/09/10 17:17 106-93-45.0Dibromomethane ND ug/L 1 09/09/10 17:17 74-95-35.01,2-Dichlorobenzene ND ug/L 1 09/09/10 17:17 95-50-15.01,3-Dichlorobenzene ND ug/L 1 09/09/10 17:17 541-73-15.01,4-Dichlorobenzene ND ug/L 1 09/09/10 17:17 106-46-75.0trans-1,4-Dichloro-2-butene ND ug/L 1 09/09/10 17:17 110-57-6100Dichlorodifluoromethane ND ug/L 1 09/09/10 17:17 75-71-85.01,1-Dichloroethane ND ug/L 1 09/09/10 17:17 75-34-35.01,2-Dichloroethane ND ug/L 1 09/09/10 17:17 107-06-25.01,1-Dichloroethene ND ug/L 1 09/09/10 17:17 75-35-45.0cis-1,2-Dichloroethene ND ug/L 1 09/09/10 17:17 156-59-25.0trans-1,2-Dichloroethene ND ug/L 1 09/09/10 17:17 156-60-55.01,2-Dichloropropane ND ug/L 1 09/09/10 17:17 78-87-55.01,3-Dichloropropane ND ug/L 1 09/09/10 17:17 142-28-95.02,2-Dichloropropane ND ug/L 1 09/09/10 17:17 594-20-75.01,1-Dichloropropene ND ug/L 1 09/09/10 17:17 563-58-65.0cis-1,3-Dichloropropene ND ug/L 1 09/09/10 17:17 10061-01-55.0trans-1,3-Dichloropropene ND ug/L 1 09/09/10 17:17 10061-02-65.0Ethylbenzene ND ug/L 1 09/09/10 17:17 100-41-45.0Ethyl methacrylate ND ug/L 1 09/09/10 17:17 97-63-2100Hexachloro-1,3-butadiene ND ug/L 1 09/09/10 17:17 87-68-35.0n-Hexane ND ug/L 1 09/09/10 17:17 110-54-35.02-Hexanone ND ug/L 1 09/09/10 17:17 591-78-625.0Iodomethane ND ug/L 1 09/09/10 17:17 74-88-410.0Isopropylbenzene (Cumene) ND ug/L 1 09/09/10 17:17 98-82-85.0p-Isopropyltoluene ND ug/L 1 09/09/10 17:17 99-87-65.0Methylene chloride ND ug/L 1 09/09/10 17:17 75-09-25.04-Methyl-2-pentanone (MIBK) ND ug/L 1 09/09/10 17:17 108-10-125.0Methyl-tert-butyl ether ND ug/L 1 09/09/10 17:17 1634-04-44.0Naphthalene ND ug/L 1 09/09/10 17:17 91-20-35.0n-Propylbenzene ND ug/L 1 09/09/10 17:17 103-65-15.0Styrene ND ug/L 1 09/09/10 17:17 100-42-55.01,1,1,2-Tetrachloroethane ND ug/L 1 09/09/10 17:17 630-20-65.01,1,2,2-Tetrachloroethane ND ug/L 1 09/09/10 17:17 79-34-55.0Tetrachloroethene ND ug/L 1 09/09/10 17:17 127-18-45.0Toluene ND ug/L 1 09/09/10 17:17 108-88-35.01,2,3-Trichlorobenzene ND ug/L 1 09/09/10 17:17 87-61-65.01,2,4-Trichlorobenzene ND ug/L 1 09/09/10 17:17 120-82-15.0



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ANALYTICAL RESULTS






1,1,1-Trichloroethane ND ug/L 1 09/09/10 17:17 71-55-65.01,1,2-Trichloroethane ND ug/L 1 09/09/10 17:17 79-00-55.0Trichloroethene ND ug/L 1 09/09/10 17:17 79-01-65.0Trichlorofluoromethane ND ug/L 1 09/09/10 17:17 75-69-45.01,2,3-Trichloropropane ND ug/L 1 09/09/10 17:17 96-18-45.01,2,4-Trimethylbenzene ND ug/L 1 09/09/10 17:17 95-63-65.01,3,5-Trimethylbenzene ND ug/L 1 09/09/10 17:17 108-67-85.0Vinyl acetate ND ug/L 1 09/09/10 17:17 108-05-410.0Vinyl chloride ND ug/L 1 09/09/10 17:17 75-01-42.0Xylene (Total) ND ug/L 1 09/09/10 17:17 1330-20-710.0Dibromofluoromethane (S) 98 % 1 09/09/10 17:17 1868-53-780-1234-Bromofluorobenzene (S) 94 % 1 09/09/10 17:17 460-00-470-126Toluene-d8 (S) 97 % 1 09/09/10 17:17 2037-26-580-116



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Mercury ND ug/L 1 09/08/10 11:45 7439-97-609/07/10 00:002.0







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Sample: TW-2 FD Lab ID: 5040967010 Collected: 09/01/10 14:17 Received: 09/02/10 11:55 Matrix: Water





Mercury ND ug/L 1 09/08/10 11:47 7439-97-609/07/10 00:002.0







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(317)875-5894






MPRP/6254EPA 3050

EPA 60106010 MET






Matrix: Solid

Analyzed


Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

5040967001

476022

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic mg/kg 53.7 79 75-12580 .2 2053.22.9 45.3 45.3Barium mg/kg 53.7 100 75-12595 2 2053.264.7 118 115Cadmium mg/kg 53.7 79 75-12580 .3 2053.2ND 42.9 43.0Chromium mg/kg 53.7 81 75-12579 3 2053.212.0 55.6 54.1Lead mg/kg M053.7 75 75-12574 2 2053.210.3 50.6 49.4Selenium mg/kg 53.7 78 75-12579 .1 2053.2ND 41.8 41.8Silver mg/kg 26.8 78 75-12577 2 2026.6ND 21.5 21.0

Parameter UnitsMS



MSSpikeResult

5040942001

476024

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic mg/kg 46.4 85 75-12580 3 2046.438.8 78.4 75.8Barium mg/kg 46.4 102 75-12581 10 2046.456.3 104 93.7Cadmium mg/kg 46.4 90 75-12591 .5 2046.4ND 43.0 43.2



Date: 09/10/2010 03:44 PM Page 26 of 45



(317)875-5894




Parameter UnitsMS



MSSpikeResult

5040942001

476024

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Chromium mg/kg M346.4 74 75-12569 5 2046.418.5 52.9 50.4Lead mg/kg M346.4 64 75-12568 1 2046.4103 133 135Selenium mg/kg 46.4 88 75-12589 .4 2046.4ND 41.4 41.6Silver mg/kg 23.2 83 75-12584 1 2023.2ND 19.9 20.2



Date: 09/10/2010 03:44 PM Page 27 of 45



(317)875-5894






MPRP/6280EPA 3010

EPA 60106010 MET

Associated Lab Samples: 5040967008, 5040967009, 5040967010





Matrix: Water

Analyzed

Arsenic ug/L ND 10.0 09/10/10 08:53Barium ug/L ND 100 09/10/10 08:53Cadmium ug/L ND 5.0 09/10/10 08:53Chromium ug/L ND 10.0 09/10/10 08:53Lead ug/L ND 10.0 09/10/10 08:53Selenium ug/L ND 10.0 09/10/10 08:53Silver ug/L ND 50.0 09/10/10 08:53

Parameter UnitsLCS



Arsenic ug/L 10201000 102 80-120Barium ug/L 10301000 103 80-120Cadmium ug/L 9991000 100 80-120Chromium ug/L 9841000 98 80-120Lead ug/L 10101000 101 80-120Selenium ug/L 10001000 100 80-120Silver ug/L 436500 87 80-120

Parameter UnitsMS



MSSpikeResult

5040950002

477000

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic ug/L 1000 103 75-125101 2 201000ND 1030 1010Barium ug/L 1000 107 75-125106 .5 201000ND 1130 1130Cadmium ug/L 1000 98 75-12596 2 201000ND 978 957Chromium ug/L 1000 98 75-12596 2 201000ND 979 964Lead ug/L 1000 97 75-12595 2 201000ND 971 951Selenium ug/L 1000 101 75-12598 3 201000ND 1010 982Silver ug/L 500 91 75-12598 8 20500ND 455 492



Date: 09/10/2010 03:44 PM Page 28 of 45



(317)875-5894






MERP/2799EPA 7470







Matrix: Water

Analyzed

Mercury ug/L ND 2.0 09/08/10 11:25

Parameter UnitsLCS



Mercury ug/L 4.95 97 80-120

Parameter UnitsMS



MSSpikeResult

5040771002

476837

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L 5 93 75-12594 .9 205ND 4.7 4.7

Parameter UnitsMS



MSSpikeResult

5040767012

476839

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L 5 95 75-12596 1 205ND 4.8 4.8



Date: 09/10/2010 03:44 PM Page 29 of 45



(317)875-5894






MERP/2795EPA 7471







Matrix: Solid

Analyzed

Mercury mg/kg ND 0.33 09/08/10 12:53

Parameter UnitsLCS



Mercury mg/kg 0.50.5 101 80-120

Parameter UnitsMS



MSSpikeResult

5040942034

476342

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .52 104 75-125100 7 20.5ND 0.53 0.50

Parameter UnitsMS



MSSpikeResult

5040967001

476344

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .61 100 75-125105 5 20.61ND 0.61 0.64



Date: 09/10/2010 03:44 PM Page 30 of 45



(317)875-5894






OEXT/20579EPA 3546







Matrix: Solid

Analyzed


Parameter UnitsLCS






Date: 09/10/2010 03:44 PM Page 31 of 45



(317)875-5894




Parameter UnitsLCS



Terphenyl-d14 (S) % 89 41-120

Parameter UnitsMS



MSSpikeResult

5040967001

475982

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2-Methylnaphthalene ug/kg 1950 71 25-12376 6 201950ND 1380 1480Acenaphthene ug/kg 1950 75 27-12682 8 201950ND 1470 1590Acenaphthylene ug/kg 1950 74 23-13879 7 201950ND 1440 1540Anthracene ug/kg 1950 74 22-13677 4 201950ND 1440 1490Benzo(a)anthracene ug/kg 1950 69 20-13471 3 201950ND 1340 1380Benzo(a)pyrene ug/kg 1950 71 20-13771 .4 201950ND 1380 1380Benzo(b)fluoranthene ug/kg 1950 70 20-13870 .2 201950ND 1360 1360Benzo(g,h,i)perylene ug/kg 1950 69 20-11669 .6 201950ND 1350 1350Benzo(k)fluoranthene ug/kg 1950 77 15-13678 1 201950ND 1500 1510Chrysene ug/kg 1950 74 16-13676 2 201950ND 1450 1480Dibenz(a,h)anthracene ug/kg 1950 70 15-12969 .4 201950ND 1360 1350Fluoranthene ug/kg 1950 78 11-15581 4 201950ND 1520 1590Fluorene ug/kg 1950 76 20-14182 7 201950ND 1490 1590Indeno(1,2,3-cd)pyrene ug/kg 1950 69 10-12969 .5 201950ND 1340 1340Naphthalene ug/kg 1950 75 18-13781 8 201950ND 1460 1580Phenanthrene ug/kg 1950 76 20-18080 5 201950ND 1490 1560Pyrene ug/kg 1950 77 18-14280 5 201950ND 1490 15602-Fluorobiphenyl (S) % 74 45-12078 20Terphenyl-d14 (S) % 72 41-12075 20



Date: 09/10/2010 03:44 PM Page 32 of 45



(317)875-5894






OEXT/20588EPA 3510

EPA 8270 by SIM8270 Water PAH by SIM MSSV






Matrix: Water

Analyzed

2-Methylnaphthalene ug/L ND 1.0 09/07/10 15:55Acenaphthene ug/L ND 1.0 09/07/10 15:55Acenaphthylene ug/L ND 1.0 09/07/10 15:55Anthracene ug/L ND 0.10 09/07/10 15:55Benzo(a)anthracene ug/L ND 0.10 09/07/10 15:55Benzo(a)pyrene ug/L ND 0.10 09/07/10 15:55Benzo(b)fluoranthene ug/L ND 0.10 09/07/10 15:55Benzo(g,h,i)perylene ug/L ND 0.10 09/07/10 15:55Benzo(k)fluoranthene ug/L ND 0.10 09/07/10 15:55Chrysene ug/L ND 0.50 09/07/10 15:55Dibenz(a,h)anthracene ug/L ND 0.10 09/07/10 15:55Fluoranthene ug/L ND 1.0 09/07/10 15:55Fluorene ug/L ND 1.0 09/07/10 15:55Indeno(1,2,3-cd)pyrene ug/L ND 0.10 09/07/10 15:55Naphthalene ug/L ND 1.0 09/07/10 15:55Phenanthrene ug/L ND 1.0 09/07/10 15:55Pyrene ug/L ND 1.0 09/07/10 15:552-Fluorobiphenyl (S) % 69 35-116 09/07/10 15:55Terphenyl-d14 (S) % 90 25-117 09/07/10 15:55

Parameter UnitsLCS



2-Methylnaphthalene ug/L 5.910 59 40-110Acenaphthene ug/L 7.410 74 48-117Acenaphthylene ug/L 7.610 76 50-121Anthracene ug/L 8.710 87 53-127Benzo(a)anthracene ug/L 8.610 86 63-122Benzo(a)pyrene ug/L 8.210 82 50-133Benzo(b)fluoranthene ug/L 8.310 83 51-136Benzo(g,h,i)perylene ug/L 7.810 78 39-126Benzo(k)fluoranthene ug/L 8.410 84 49-124Chrysene ug/L 8.810 88 61-116Dibenz(a,h)anthracene ug/L 7.910 79 44-130Fluoranthene ug/L 8.810 88 65-128Fluorene ug/L 8.010 80 54-120Indeno(1,2,3-cd)pyrene ug/L 7.810 78 43-129Naphthalene ug/L 6.710 67 42-120Phenanthrene ug/L 8.210 82 56-120Pyrene ug/L 9.110 91 61-1232-Fluorobiphenyl (S) % 80 35-116



Date: 09/10/2010 03:44 PM Page 33 of 45



(317)875-5894




Parameter UnitsLCS



Terphenyl-d14 (S) % 91 25-117

Parameter UnitsMS



MSSpikeResult

5040962004

476459

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2-Methylnaphthalene ug/L R120 32 27-12253 50 2020ND 6.4 10.6Acenaphthene ug/L R120 48 40-12069 36 2020ND 9.6 13.8Acenaphthylene ug/L R120 49 34-12971 37 2020ND 9.8 14.2Anthracene ug/L R120 60 39-13082 31 2020ND 12.0 16.4Benzo(a)anthracene ug/L R120 53 28-12573 31 2020ND 10.7 14.5Benzo(a)pyrene ug/L R120 34 10-13049 37 2020ND 6.8 9.9Benzo(b)fluoranthene ug/L R120 35 20-12053 41 2020ND 7.0 10.5Benzo(g,h,i)perylene ug/L R120 26 10-13037 35 2020ND 5.2 7.5Benzo(k)fluoranthene ug/L R120 36 20-12550 34 2020ND 7.2 10.1Chrysene ug/L R120 55 30-13075 30 2020ND 11.1 14.9Dibenz(a,h)anthracene ug/L R120 26 10-12537 34 2020ND 5.2 7.4Fluoranthene ug/L R120 64 28-15285 29 2020ND 12.7 17.0Fluorene ug/L R120 53 36-13075 33 2020ND 10.7 14.9Indeno(1,2,3-cd)pyrene ug/L R120 26 10-13037 36 2020ND 5.2 7.5Naphthalene ug/L R120 44 23-12766 40 2020ND 8.8 13.1Phenanthrene ug/L R120 57 43-12579 32 2020ND 11.4 15.7Pyrene ug/L R120 65 28-14087 29 2020ND 13.0 17.52-Fluorobiphenyl (S) % 54 35-11665 20Terphenyl-d14 (S) % 53 25-11760 20



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(317)875-5894






MSV/26546EPA 8260

EPA 82608260 MSV






Matrix: Water

Analyzed




Date: 09/10/2010 03:44 PM Page 35 of 45



(317)875-5894








Matrix: Water

Analyzed

Dibromomethane ug/L ND 5.0 09/09/10 13:37Dichlorodifluoromethane ug/L ND 5.0 09/09/10 13:37Ethyl methacrylate ug/L ND 100 09/09/10 13:37Ethylbenzene ug/L ND 5.0 09/09/10 13:37Hexachloro-1,3-butadiene ug/L ND 5.0 09/09/10 13:37Iodomethane ug/L 11.4 10.0 B-09/09/10 13:37Isopropylbenzene (Cumene) ug/L ND 5.0 09/09/10 13:37Methyl-tert-butyl ether ug/L ND 4.0 09/09/10 13:37Methylene chloride ug/L ND 5.0 09/09/10 13:37n-Butylbenzene ug/L ND 5.0 09/09/10 13:37n-Hexane ug/L ND 5.0 09/09/10 13:37n-Propylbenzene ug/L ND 5.0 09/09/10 13:37Naphthalene ug/L ND 5.0 09/09/10 13:37p-Isopropyltoluene ug/L ND 5.0 09/09/10 13:37sec-Butylbenzene ug/L ND 5.0 09/09/10 13:37Styrene ug/L ND 5.0 09/09/10 13:37tert-Butylbenzene ug/L ND 5.0 09/09/10 13:37Tetrachloroethene ug/L ND 5.0 09/09/10 13:37Toluene ug/L ND 5.0 09/09/10 13:37trans-1,2-Dichloroethene ug/L ND 5.0 09/09/10 13:37trans-1,3-Dichloropropene ug/L ND 5.0 09/09/10 13:37trans-1,4-Dichloro-2-butene ug/L ND 100 09/09/10 13:37Trichloroethene ug/L ND 5.0 09/09/10 13:37Trichlorofluoromethane ug/L ND 5.0 09/09/10 13:37Vinyl acetate ug/L ND 10.0 09/09/10 13:37Vinyl chloride ug/L ND 2.0 09/09/10 13:37Xylene (Total) ug/L ND 10.0 09/09/10 13:374-Bromofluorobenzene (S) % 96 70-126 09/09/10 13:37Dibromofluoromethane (S) % 92 80-123 09/09/10 13:37Toluene-d8 (S) % 96 80-116 09/09/10 13:37

Parameter UnitsLCS






Date: 09/10/2010 03:44 PM Page 36 of 45



(317)875-5894




Parameter UnitsLCS






Date: 09/10/2010 03:44 PM Page 37 of 45



(317)875-5894




Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

5040967008

478552

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1,2-Tetrachloroethane ug/L 50 88 55-13199 12 2050ND 43.9 49.31,1,1-Trichloroethane ug/L 50 88 64-143102 15 2050ND 44.2 51.21,1,2,2-Tetrachloroethane ug/L 50 90 64-14298 9 2050ND 45.1 49.21,1,2-Trichloroethane ug/L 50 91 71-143103 12 2050ND 45.5 51.31,1-Dichloroethane ug/L 50 84 68-13998 15 2050ND 42.0 49.01,1-Dichloroethene ug/L 50 75 55-14087 14 2050ND 37.7 43.31,1-Dichloropropene ug/L 50 90 66-140103 13 2050ND 45.0 51.31,2,3-Trichlorobenzene ug/L 50 88 33-14093 6 2050ND 44.0 46.71,2,3-Trichloropropane ug/L 100 76 58-13384 10 20100ND 75.7 83.81,2,4-Trichlorobenzene ug/L 50 81 28-14084 4 2050ND 40.6 42.11,2,4-Trimethylbenzene ug/L 50 79 39-14688 10 2050ND 39.7 44.01,2-Dibromoethane (EDB) ug/L 50 95 67-134107 12 2050ND 47.5 53.61,2-Dichlorobenzene ug/L 50 84 48-13790 7 2050ND 42.1 45.21,2-Dichloroethane ug/L 50 89 63-148102 14 2050ND 44.4 51.11,2-Dichloropropane ug/L 50 93 70-136107 14 2050ND 46.4 53.41,3,5-Trimethylbenzene ug/L 50 81 39-14590 11 2050ND 40.4 45.11,3-Dichlorobenzene ug/L 50 84 40-14389 7 2050ND 41.9 44.71,3-Dichloropropane ug/L 50 92 65-133106 14 2050ND 46.2 53.21,4-Dichlorobenzene ug/L 50 83 38-14287 5 2050ND 41.4 43.42,2-Dichloropropane ug/L 50 81 35-15798 19 2050ND 40.6 49.12-Butanone (MEK) ug/L 250 79 62-13294 17 20250ND 199 2352-Chlorotoluene ug/L 50 98 44-14395 3 2050ND 48.9 47.52-Hexanone ug/L 250 89 61-141103 15 20250ND 222 2584-Chlorotoluene ug/L 50 96 43-14095 .9 2050ND 48.0 47.64-Methyl-2-pentanone (MIBK) ug/L 250 88 57-135102 15 20250ND 221 256Acetone ug/L 250 85 30-170100 16 20250ND 212 249Acrolein ug/L M01000 154 30-170179 15 201000ND 1540 1790Acrylonitrile ug/L 1000 83 66-13796 15 201000ND 825 962



Date: 09/10/2010 03:44 PM Page 38 of 45



(317)875-5894




Parameter UnitsMS



MSSpikeResult

5040967008

478552

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Benzene ug/L 50 94 63-141106 13 2050ND 46.8 53.1Bromobenzene ug/L 50 90 57-12897 8 2050ND 45.1 48.7Bromochloromethane ug/L 50 88 65-157106 19 2050ND 44.1 53.2Bromodichloromethane ug/L 50 92 63-135105 13 2050ND 46.0 52.5Bromoform ug/L 50 84 58-12488 5 2050ND 41.9 44.2Bromomethane ug/L 50 63 30-17073 14 2050ND 31.4 36.3Carbon disulfide ug/L 100 67 46-16274 10 20100ND 66.5 73.7Carbon tetrachloride ug/L 50 85 54-14596 12 2050ND 42.7 48.0Chlorobenzene ug/L 50 90 56-13397 7 2050ND 45.1 48.5Chloroethane ug/L 50 79 54-15789 13 2050ND 39.3 44.6Chloroform ug/L 50 83 67-13497 15 2050ND 41.6 48.4Chloromethane ug/L 50 57 36-13760 5 2050ND 28.5 30.1cis-1,2-Dichloroethene ug/L 50 90 65-132106 17 2050ND 45.1 53.2cis-1,3-Dichloropropene ug/L 50 83 46-12194 13 2050ND 41.5 47.2Dibromochloromethane ug/L 50 85 64-12495 11 2050ND 42.6 47.4Dibromomethane ug/L 50 93 67-144104 11 2050ND 46.6 51.9Dichlorodifluoromethane ug/L 50 52 30-16354 3 2050ND 26.0 26.9Ethyl methacrylate ug/L 200 93 52-140108 15 20200ND 186 216Ethylbenzene ug/L 50 96 44-15198 2 2050ND 48.0 49.2Hexachloro-1,3-butadiene ug/L 50 78 30-14573 7 2050ND 39.2 36.5Iodomethane ug/L 100 46 28-16855 18 20100ND 45.8 54.9Isopropylbenzene (Cumene) ug/L 50 91 40-14894 3 2050ND 45.7 46.9Methyl-tert-butyl ether ug/L 100 81 52-15692 13 20100ND 81.0 92.1Methylene chloride ug/L 50 86 46-15496 11 2050ND 43.1 48.2n-Butylbenzene ug/L 50 86 27-15381 6 2050ND 43.0 40.4n-Hexane ug/L 50 78 32-17688 12 2050ND 39.0 44.1n-Propylbenzene ug/L 50 97 40-14892 5 2050ND 48.5 46.1Naphthalene ug/L 50 89 44-138100 11 2050ND 44.5 49.9p-Isopropyltoluene ug/L 50 87 34-14685 2 2050ND 43.4 42.3sec-Butylbenzene ug/L 50 89 38-15088 .7 2050ND 44.3 44.0Styrene ug/L 50 91 38-14196 5 2050ND 45.6 47.8tert-Butylbenzene ug/L 50 66 32-13375 12 2050ND 33.0 37.3Tetrachloroethene ug/L 50 83 25-14687 6 2050ND 41.3 43.7Toluene ug/L 50 90 59-142100 10 2050ND 45.0 49.8trans-1,2-Dichloroethene ug/L 50 87 60-13796 9 2050ND 43.7 48.0trans-1,3-Dichloropropene ug/L 50 74 43-11785 13 2050ND 37.1 42.4trans-1,4-Dichloro-2-butene ug/L 200 78 44-13987 11 20200ND 156 174Trichloroethene ug/L 50 89 61-137102 14 2050ND 44.6 51.2Trichlorofluoromethane ug/L 50 78 53-16287 10 2050ND 39.2 43.4Vinyl acetate ug/L 200 79 24-13289 12 20200ND 158 177Vinyl chloride ug/L 50 63 51-14471 12 2050ND 31.5 35.3Xylene (Total) ug/L 150 92 44-15296 4 20150ND 138 1444-Bromofluorobenzene (S) % 103 70-126103 20Dibromofluoromethane (S) % 97 80-12398 20Toluene-d8 (S) % 97 80-11697 20



Date: 09/10/2010 03:44 PM Page 39 of 45



(317)875-5894






MSV/26556EPA 8260







Matrix: Solid

Analyzed




Date: 09/10/2010 03:44 PM Page 40 of 45



(317)875-5894








Matrix: Solid

Analyzed


Parameter UnitsLCS






Date: 09/10/2010 03:44 PM Page 41 of 45



(317)875-5894




Parameter UnitsLCS



1,2-Dichlorobenzene ug/kg 39.350 79 75-1171,2-Dichloroethane ug/kg 42.350 85 62-1351,2-Dichloropropane ug/kg 42.750 85 74-1241,3,5-Trimethylbenzene ug/kg 46.050 92 73-1221,3-Dichlorobenzene ug/kg 46.350 93 73-1201,3-Dichloropropane ug/kg 46.750 93 71-1221,4-Dichlorobenzene ug/kg 45.950 92 72-1182,2-Dichloropropane ug/kg 40.250 80 53-1362-Butanone (MEK) ug/kg 256250 102 33-1902-Chlorotoluene ug/kg 48.550 97 72-1222-Hexanone ug/kg 289250 116 44-1684-Chlorotoluene ug/kg 45.150 90 72-1204-Methyl-2-pentanone (MIBK) ug/kg 233250 93 58-126Acetone ug/kg 351250 140 30-190Acrolein ug/kg 2030 L31000 203 30-190Acrylonitrile ug/kg 8151000 82 65-129Benzene ug/kg 40.350 81 76-123Bromobenzene ug/kg 43.650 87 74-116Bromochloromethane ug/kg 41.450 83 56-143Bromodichloromethane ug/kg 42.750 85 67-123Bromoform ug/kg 39.350 79 58-117Bromomethane ug/kg 62.550 125 47-147Carbon disulfide ug/kg 75.1100 75 56-141Carbon tetrachloride ug/kg 37.750 75 54-136Chlorobenzene ug/kg 45.950 92 75-115Chloroethane ug/kg 75.4 L350 151 57-147Chloroform ug/kg 42.850 86 74-123Chloromethane ug/kg 68.250 136 31-155cis-1,2-Dichloroethene ug/kg 49.150 98 76-119cis-1,3-Dichloropropene ug/kg 38.750 77 56-110Dibromochloromethane ug/kg 38.950 78 63-122Dibromomethane ug/kg 44.850 90 70-127Dichlorodifluoromethane ug/kg 119 L350 238 30-170Ethyl methacrylate ug/kg 212200 106 58-126Ethylbenzene ug/kg 45.150 90 78-121Hexachloro-1,3-butadiene ug/kg 44.750 89 65-128Iodomethane ug/kg 80.1J100 80 38-173Isopropylbenzene (Cumene) ug/kg 43.450 87 75-128Methyl-tert-butyl ether ug/kg 77.6100 78 59-142Methylene chloride ug/kg 40.150 80 30-170n-Butylbenzene ug/kg 40.750 81 70-123n-Propylbenzene ug/kg 48.150 96 70-126Naphthalene ug/kg 45.950 92 60-128p-Isopropyltoluene ug/kg 46.150 92 65-125sec-Butylbenzene ug/kg 47.850 96 72-125Styrene ug/kg 44.350 89 75-118tert-Butylbenzene ug/kg 42.550 85 61-114Tetrachloroethene ug/kg 41.850 84 63-117



Date: 09/10/2010 03:44 PM Page 42 of 45



(317)875-5894




Parameter UnitsLCS






Date: 09/10/2010 03:44 PM Page 43 of 45



(317)875-5894








Associated Lab Samples: 5040967001, 5040967002, 5040967003, 5040967004, 5040967005, 5040967007

Parameter UnitsDup



Percent Moisture % 13.7 R212 512.1

Parameter UnitsDup






Date: 09/10/2010 03:44 PM Page 44 of 45



(317)875-5894

QUALIFIERS



DEFINITIONS


LABORATORIES


ANALYTE QUALIFIERS

Analyte detected in method blank but was not detected in the associated samples.B-Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

L3

Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0Matrix spike recovery was outside laboratory control limits due to matrix interferences.M3RPD value was outside control limits.R1RPD value was outside control limits due to matrix interferenceR2



Date: 09/10/2010 03:44 PM Page 45 of 45



(317)875-5894

September 20, 2010



RE:


Franks Foundry



Sincerely,

Mark Davis



Enclosures



Page 1 of 48



(317)875-5894

SAMPLE SUMMARY


5041216Franks Foundry


5041216001 TW-16 Water 09/09/10 09:31 09/10/10 12:40

5041216002 TW-1 Water 09/09/10 10:02 09/10/10 12:40

5041216003 TW-3 Water 09/09/10 11:02 09/10/10 12:40

5041216004 TW-4 Water 09/09/10 11:32 09/10/10 12:40

5041216005 TW-6 Water 09/09/10 13:21 09/10/10 12:40

5041216006 TW-5 Water 09/09/10 14:14 09/10/10 12:40

5041216007 SB-5_(0.5-1.0) Solid 09/09/10 13:15 09/10/10 12:40

5041216008 SB-8_(4-5) Solid 09/09/10 15:35 09/10/10 12:40

5041216009 SB-10_(4-5) Solid 09/09/10 16:05 09/10/10 12:40

5041216010 TRIP BLANK Water 09/09/10 08:00 09/10/10 12:40



Page 2 of 48



(317)875-5894





5041216001 TW-16 EPA 6010 7 PASI-IFRW



EPA 8260 73 PASI-IALA

5041216002 TW-1 EPA 6010 7 PASI-IFRW




5041216003 TW-3 EPA 8270 by SIM 19 PASI-IRRB


5041216004 TW-4 EPA 6010 7 PASI-IFRW








5041216007 SB-5_(0.5-1.0) EPA 8270 by SIM 19 PASI-IRRB

EPA 8260 72 PASI-IHEB


5041216008 SB-8_(4-5) EPA 6010 7 PASI-IFRW





5041216009 SB-10_(4-5) EPA 6010 7 PASI-IFRW





5041216010 TRIP BLANK EPA 8260 73 PASI-IALA



Page 3 of 48



(317)875-5894

ANALYTICAL RESULTS






Arsenic ND ug/L 1 09/15/10 16:12 7440-38-209/13/10 00:0010.0Barium ND ug/L 1 09/15/10 16:12 7440-39-309/13/10 00:00100Cadmium ND ug/L 1 09/15/10 16:12 7440-43-909/13/10 00:005.0Chromium ND ug/L 1 09/15/10 16:12 7440-47-309/13/10 00:0010.0Lead ND ug/L 1 09/15/10 16:12 7439-92-109/13/10 00:0010.0Selenium ND ug/L 1 09/15/10 16:12 7782-49-209/13/10 00:0010.0Silver ND ug/L 1 09/15/10 16:12 7440-22-409/13/10 00:0050.0


Mercury ND ug/L 1 09/15/10 11:01 7439-97-609/14/10 00:002.0







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(317)875-5894

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(317)875-5894

ANALYTICAL RESULTS






Arsenic 95.7 ug/L 1 09/15/10 16:16 7440-38-209/13/10 00:0010.0Barium 924 ug/L 1 09/15/10 16:16 7440-39-309/13/10 00:00100Cadmium ND ug/L 1 09/15/10 16:16 7440-43-909/13/10 00:005.0Chromium 106 ug/L 1 09/15/10 16:16 7440-47-309/13/10 00:0010.0Lead 104 ug/L 1 09/15/10 16:16 7439-92-109/13/10 00:0010.0Selenium ND ug/L 1 09/15/10 16:16 7782-49-209/13/10 00:0010.0Silver ND ug/L 1 09/15/10 16:16 7440-22-409/13/10 00:0050.0


Mercury ND ug/L 1 09/15/10 11:03 7439-97-609/14/10 00:002.0


Acenaphthene ND ug/L 1 09/13/10 21:14 83-32-909/13/10 10:401.2Acenaphthylene ND ug/L 1 09/13/10 21:14 208-96-809/13/10 10:401.2Anthracene ND ug/L 1 09/13/10 21:14 120-12-709/13/10 10:400.12Benzo(a)anthracene ND ug/L 1 09/13/10 21:14 56-55-309/13/10 10:400.12Benzo(a)pyrene ND ug/L 1 09/13/10 21:14 50-32-809/13/10 10:400.12Benzo(b)fluoranthene ND ug/L 1 09/13/10 21:14 205-99-209/13/10 10:400.12Benzo(g,h,i)perylene ND ug/L 1 09/13/10 21:14 191-24-209/13/10 10:400.12Benzo(k)fluoranthene ND ug/L 1 09/13/10 21:14 207-08-909/13/10 10:400.12Chrysene ND ug/L 1 09/13/10 21:14 218-01-909/13/10 10:400.59Dibenz(a,h)anthracene ND ug/L 1 09/13/10 21:14 53-70-309/13/10 10:400.12Fluoranthene ND ug/L 1 09/13/10 21:14 206-44-009/13/10 10:401.2Fluorene ND ug/L 1 09/13/10 21:14 86-73-709/13/10 10:401.2Indeno(1,2,3-cd)pyrene ND ug/L 1 09/13/10 21:14 193-39-509/13/10 10:400.122-Methylnaphthalene ND ug/L 1 09/13/10 21:14 91-57-609/13/10 10:401.2Naphthalene 1.6 ug/L 1 09/13/10 21:14 91-20-309/13/10 10:401.2Phenanthrene ND ug/L 1 09/13/10 21:14 85-01-809/13/10 10:401.2Pyrene ND ug/L 1 09/13/10 21:14 129-00-009/13/10 10:401.22-Fluorobiphenyl (S) 63 % 1 09/13/10 21:14 321-60-809/13/10 10:4035-94Terphenyl-d14 (S) 70 % 1 09/13/10 21:14 1718-51-009/13/10 10:4019-101


Acetone ND ug/L 1 09/15/10 05:34 67-64-1100Acrolein ND ug/L 1 09/15/10 05:34 107-02-850.0Acrylonitrile ND ug/L 1 09/15/10 05:34 107-13-1100Benzene 29.0 ug/L 1 09/15/10 05:34 71-43-25.0Bromobenzene ND ug/L 1 09/15/10 05:34 108-86-15.0Bromochloromethane ND ug/L 1 09/15/10 05:34 74-97-55.0Bromodichloromethane ND ug/L 1 09/15/10 05:34 75-27-45.0Bromoform ND ug/L 1 09/15/10 05:34 75-25-25.0Bromomethane ND ug/L 1 09/15/10 05:34 74-83-95.02-Butanone (MEK) ND ug/L 1 09/15/10 05:34 78-93-325.0n-Butylbenzene ND ug/L 1 09/15/10 05:34 104-51-85.0sec-Butylbenzene ND ug/L 1 09/15/10 05:34 135-98-85.0tert-Butylbenzene ND ug/L 1 09/15/10 05:34 98-06-65.0



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Carbon disulfide ND ug/L 1 09/15/10 05:34 75-15-010.0Carbon tetrachloride ND ug/L 1 09/15/10 05:34 56-23-55.0Chlorobenzene ND ug/L 1 09/15/10 05:34 108-90-75.0Chloroethane ND ug/L 1 09/15/10 05:34 75-00-35.0Chloroform ND ug/L 1 09/15/10 05:34 67-66-35.0Chloromethane ND ug/L 1 09/15/10 05:34 74-87-35.02-Chlorotoluene ND ug/L 1 09/15/10 05:34 95-49-85.04-Chlorotoluene ND ug/L 1 09/15/10 05:34 106-43-45.0Dibromochloromethane ND ug/L 1 09/15/10 05:34 124-48-15.01,2-Dibromoethane (EDB) ND ug/L 1 09/15/10 05:34 106-93-45.0Dibromomethane ND ug/L 1 09/15/10 05:34 74-95-35.01,2-Dichlorobenzene ND ug/L 1 09/15/10 05:34 95-50-15.01,3-Dichlorobenzene ND ug/L 1 09/15/10 05:34 541-73-15.01,4-Dichlorobenzene ND ug/L 1 09/15/10 05:34 106-46-75.0trans-1,4-Dichloro-2-butene ND ug/L 1 09/15/10 05:34 110-57-6100Dichlorodifluoromethane ND ug/L 1 09/15/10 05:34 75-71-85.01,1-Dichloroethane ND ug/L 1 09/15/10 05:34 75-34-35.01,2-Dichloroethane ND ug/L 1 09/15/10 05:34 107-06-25.01,1-Dichloroethene ND ug/L 1 09/15/10 05:34 75-35-45.0cis-1,2-Dichloroethene ND ug/L 1 09/15/10 05:34 156-59-25.0trans-1,2-Dichloroethene ND ug/L 1 09/15/10 05:34 156-60-55.01,2-Dichloropropane ND ug/L 1 09/15/10 05:34 78-87-55.01,3-Dichloropropane ND ug/L 1 09/15/10 05:34 142-28-95.02,2-Dichloropropane ND ug/L 1 09/15/10 05:34 594-20-75.01,1-Dichloropropene ND ug/L 1 09/15/10 05:34 563-58-65.0cis-1,3-Dichloropropene ND ug/L 1 09/15/10 05:34 10061-01-55.0trans-1,3-Dichloropropene ND ug/L 1 09/15/10 05:34 10061-02-65.0Ethylbenzene 24.4 ug/L 1 09/15/10 05:34 100-41-45.0Ethyl methacrylate ND ug/L 1 09/15/10 05:34 97-63-2100Hexachloro-1,3-butadiene ND ug/L 1 09/15/10 05:34 87-68-35.0n-Hexane 12.3 ug/L 1 09/15/10 05:34 110-54-35.02-Hexanone ND ug/L 1 09/15/10 05:34 591-78-625.0Iodomethane ND ug/L 1 09/15/10 05:34 74-88-410.0Isopropylbenzene (Cumene) ND ug/L 1 09/15/10 05:34 98-82-85.0p-Isopropyltoluene ND ug/L 1 09/15/10 05:34 99-87-65.0Methylene chloride ND ug/L 1 09/15/10 05:34 75-09-25.04-Methyl-2-pentanone (MIBK) ND ug/L 1 09/15/10 05:34 108-10-125.0Methyl-tert-butyl ether ND ug/L 1 09/15/10 05:34 1634-04-44.0Naphthalene ND ug/L 1 09/15/10 05:34 91-20-35.0n-Propylbenzene ND ug/L 1 09/15/10 05:34 103-65-15.0Styrene ND ug/L 1 09/15/10 05:34 100-42-55.01,1,1,2-Tetrachloroethane ND ug/L 1 09/15/10 05:34 630-20-65.01,1,2,2-Tetrachloroethane ND ug/L 1 09/15/10 05:34 79-34-55.0Tetrachloroethene ND ug/L 1 09/15/10 05:34 127-18-45.0Toluene 51.5 ug/L 1 09/15/10 05:34 108-88-35.01,2,3-Trichlorobenzene ND ug/L 1 09/15/10 05:34 87-61-65.01,2,4-Trichlorobenzene ND ug/L 1 09/15/10 05:34 120-82-15.0



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(317)875-5894

ANALYTICAL RESULTS






1,1,1-Trichloroethane ND ug/L 1 09/15/10 05:34 71-55-65.01,1,2-Trichloroethane ND ug/L 1 09/15/10 05:34 79-00-55.0Trichloroethene ND ug/L 1 09/15/10 05:34 79-01-65.0Trichlorofluoromethane ND ug/L 1 09/15/10 05:34 75-69-45.01,2,3-Trichloropropane ND ug/L 1 09/15/10 05:34 96-18-45.01,2,4-Trimethylbenzene 23.9 ug/L 1 09/15/10 05:34 95-63-65.01,3,5-Trimethylbenzene 6.1 ug/L 1 09/15/10 05:34 108-67-85.0Vinyl acetate ND ug/L 1 09/15/10 05:34 108-05-410.0Vinyl chloride ND ug/L 1 09/15/10 05:34 75-01-42.0Xylene (Total) 105 ug/L 1 09/15/10 05:34 1330-20-710.0Dibromofluoromethane (S) 102 % 1 09/15/10 05:34 1868-53-780-1234-Bromofluorobenzene (S) 101 % 1 09/15/10 05:34 460-00-470-126Toluene-d8 (S) 104 % 1 09/15/10 05:34 2037-26-580-116



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Acetone ND ug/L 1 09/15/10 06:06 67-64-1100Acrolein ND ug/L 1 09/15/10 06:06 107-02-850.0Acrylonitrile ND ug/L 1 09/15/10 06:06 107-13-1100Benzene ND ug/L 1 09/15/10 06:06 71-43-25.0Bromobenzene ND ug/L 1 09/15/10 06:06 108-86-15.0Bromochloromethane ND ug/L 1 09/15/10 06:06 74-97-55.0Bromodichloromethane ND ug/L 1 09/15/10 06:06 75-27-45.0Bromoform ND ug/L 1 09/15/10 06:06 75-25-25.0Bromomethane ND ug/L 1 09/15/10 06:06 74-83-95.02-Butanone (MEK) ND ug/L 1 09/15/10 06:06 78-93-325.0n-Butylbenzene ND ug/L 1 09/15/10 06:06 104-51-85.0sec-Butylbenzene ND ug/L 1 09/15/10 06:06 135-98-85.0tert-Butylbenzene ND ug/L 1 09/15/10 06:06 98-06-65.0Carbon disulfide ND ug/L 1 09/15/10 06:06 75-15-010.0Carbon tetrachloride ND ug/L 1 09/15/10 06:06 56-23-55.0Chlorobenzene ND ug/L 1 09/15/10 06:06 108-90-75.0Chloroethane ND ug/L 1 09/15/10 06:06 75-00-35.0Chloroform ND ug/L 1 09/15/10 06:06 67-66-35.0Chloromethane ND ug/L 1 09/15/10 06:06 74-87-35.02-Chlorotoluene ND ug/L 1 09/15/10 06:06 95-49-85.04-Chlorotoluene ND ug/L 1 09/15/10 06:06 106-43-45.0Dibromochloromethane ND ug/L 1 09/15/10 06:06 124-48-15.01,2-Dibromoethane (EDB) ND ug/L 1 09/15/10 06:06 106-93-45.0Dibromomethane ND ug/L 1 09/15/10 06:06 74-95-35.01,2-Dichlorobenzene ND ug/L 1 09/15/10 06:06 95-50-15.01,3-Dichlorobenzene ND ug/L 1 09/15/10 06:06 541-73-15.0



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(317)875-5894

ANALYTICAL RESULTS






1,4-Dichlorobenzene ND ug/L 1 09/15/10 06:06 106-46-75.0trans-1,4-Dichloro-2-butene ND ug/L 1 09/15/10 06:06 110-57-6100Dichlorodifluoromethane ND ug/L 1 09/15/10 06:06 75-71-85.01,1-Dichloroethane ND ug/L 1 09/15/10 06:06 75-34-35.01,2-Dichloroethane ND ug/L 1 09/15/10 06:06 107-06-25.01,1-Dichloroethene ND ug/L 1 09/15/10 06:06 75-35-45.0cis-1,2-Dichloroethene ND ug/L 1 09/15/10 06:06 156-59-25.0trans-1,2-Dichloroethene ND ug/L 1 09/15/10 06:06 156-60-55.01,2-Dichloropropane ND ug/L 1 09/15/10 06:06 78-87-55.01,3-Dichloropropane ND ug/L 1 09/15/10 06:06 142-28-95.02,2-Dichloropropane ND ug/L 1 09/15/10 06:06 594-20-75.01,1-Dichloropropene ND ug/L 1 09/15/10 06:06 563-58-65.0cis-1,3-Dichloropropene ND ug/L 1 09/15/10 06:06 10061-01-55.0trans-1,3-Dichloropropene ND ug/L 1 09/15/10 06:06 10061-02-65.0Ethylbenzene ND ug/L 1 09/15/10 06:06 100-41-45.0Ethyl methacrylate ND ug/L 1 09/15/10 06:06 97-63-2100Hexachloro-1,3-butadiene ND ug/L 1 09/15/10 06:06 87-68-35.0n-Hexane ND ug/L 1 09/15/10 06:06 110-54-35.02-Hexanone ND ug/L 1 09/15/10 06:06 591-78-625.0Iodomethane ND ug/L 1 09/15/10 06:06 74-88-410.0Isopropylbenzene (Cumene) ND ug/L 1 09/15/10 06:06 98-82-85.0p-Isopropyltoluene ND ug/L 1 09/15/10 06:06 99-87-65.0Methylene chloride ND ug/L 1 09/15/10 06:06 75-09-25.04-Methyl-2-pentanone (MIBK) ND ug/L 1 09/15/10 06:06 108-10-125.0Methyl-tert-butyl ether ND ug/L 1 09/15/10 06:06 1634-04-44.0Naphthalene ND ug/L 1 09/15/10 06:06 91-20-35.0n-Propylbenzene ND ug/L 1 09/15/10 06:06 103-65-15.0Styrene ND ug/L 1 09/15/10 06:06 100-42-55.01,1,1,2-Tetrachloroethane ND ug/L 1 09/15/10 06:06 630-20-65.01,1,2,2-Tetrachloroethane ND ug/L 1 09/15/10 06:06 79-34-55.0Tetrachloroethene ND ug/L 1 09/15/10 06:06 127-18-45.0Toluene ND ug/L 1 09/15/10 06:06 108-88-35.01,2,3-Trichlorobenzene ND ug/L 1 09/15/10 06:06 87-61-65.01,2,4-Trichlorobenzene ND ug/L 1 09/15/10 06:06 120-82-15.01,1,1-Trichloroethane ND ug/L 1 09/15/10 06:06 71-55-65.01,1,2-Trichloroethane ND ug/L 1 09/15/10 06:06 79-00-55.0Trichloroethene ND ug/L 1 09/15/10 06:06 79-01-65.0Trichlorofluoromethane ND ug/L 1 09/15/10 06:06 75-69-45.01,2,3-Trichloropropane ND ug/L 1 09/15/10 06:06 96-18-45.01,2,4-Trimethylbenzene ND ug/L 1 09/15/10 06:06 95-63-65.01,3,5-Trimethylbenzene ND ug/L 1 09/15/10 06:06 108-67-85.0Vinyl acetate ND ug/L 1 09/15/10 06:06 108-05-410.0Vinyl chloride ND ug/L 1 09/15/10 06:06 75-01-42.0Xylene (Total) ND ug/L 1 09/15/10 06:06 1330-20-710.0Dibromofluoromethane (S) 98 % 1 09/15/10 06:06 1868-53-780-1234-Bromofluorobenzene (S) 96 % 1 09/15/10 06:06 460-00-470-126Toluene-d8 (S) 97 % 1 09/15/10 06:06 2037-26-580-116



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(317)875-5894

ANALYTICAL RESULTS






Arsenic 11.2 ug/L 1 09/15/10 16:20 7440-38-209/13/10 00:0010.0Barium 307 ug/L 1 09/15/10 16:20 7440-39-309/13/10 00:00100Cadmium ND ug/L 1 09/15/10 16:20 7440-43-909/13/10 00:005.0Chromium 17.8 ug/L 1 09/15/10 16:20 7440-47-309/13/10 00:0010.0Lead 20.0 ug/L 1 09/15/10 16:20 7439-92-109/13/10 00:0010.0Selenium ND ug/L 1 09/15/10 16:20 7782-49-209/13/10 00:0010.0Silver ND ug/L 1 09/15/10 16:20 7440-22-409/13/10 00:0050.0


Mercury ND ug/L 1 09/15/10 11:04 7439-97-609/14/10 00:002.0







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ANALYTICAL RESULTS









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(317)875-5894

ANALYTICAL RESULTS






Acenaphthene ND ug/L 1 09/14/10 13:29 83-32-909/13/10 10:401.1Acenaphthylene ND ug/L 1 09/14/10 13:29 208-96-809/13/10 10:401.1Anthracene 0.37 ug/L 1 09/14/10 13:29 120-12-709/13/10 10:400.11Benzo(a)anthracene 0.30 ug/L 1 09/14/10 13:29 56-55-309/13/10 10:400.11Benzo(a)pyrene 0.17 ug/L 1 09/14/10 13:29 50-32-809/13/10 10:400.11Benzo(b)fluoranthene ND ug/L 1 09/14/10 13:29 205-99-209/13/10 10:400.11Benzo(g,h,i)perylene 0.14 ug/L 1 09/14/10 13:29 191-24-209/13/10 10:400.11Benzo(k)fluoranthene ND ug/L 1 09/14/10 13:29 207-08-909/13/10 10:400.11Chrysene ND ug/L 1 09/14/10 13:29 218-01-909/13/10 10:400.53Dibenz(a,h)anthracene ND ug/L 1 09/14/10 13:29 53-70-309/13/10 10:400.11Fluoranthene ND ug/L 1 09/14/10 13:29 206-44-009/13/10 10:401.1Fluorene ND ug/L 1 09/14/10 13:29 86-73-709/13/10 10:401.1Indeno(1,2,3-cd)pyrene ND ug/L 1 09/14/10 13:29 193-39-509/13/10 10:400.112-Methylnaphthalene ND ug/L 1 09/14/10 13:29 91-57-609/13/10 10:401.1Naphthalene ND ug/L 1 09/14/10 13:29 91-20-309/13/10 10:401.1Phenanthrene 2.5 ug/L 1 09/14/10 13:29 85-01-809/13/10 10:401.1Pyrene 1.1 ug/L 1 09/14/10 13:29 129-00-009/13/10 10:401.12-Fluorobiphenyl (S) 57 % 1 09/14/10 13:29 321-60-809/13/10 10:4035-94Terphenyl-d14 (S) 44 % 1 09/14/10 13:29 1718-51-009/13/10 10:4019-101





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(317)875-5894

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Sample: SB-5_(0.5-1.0) Lab ID: 5041216007 Collected: 09/09/10 13:15 Received: 09/10/10 12:40 Matrix: SolidResults reported on a "dry-weight" basis





Acetone ND ug/kg 1 09/16/10 14:35 67-64-194.4Acrolein ND ug/kg 1 09/16/10 14:35 107-02-894.4Acrylonitrile ND ug/kg 1 09/16/10 14:35 107-13-194.4Benzene ND ug/kg 1 09/16/10 14:35 71-43-24.7Bromobenzene ND ug/kg 1 09/16/10 14:35 108-86-14.7Bromochloromethane ND ug/kg 1 09/16/10 14:35 74-97-54.7Bromodichloromethane ND ug/kg 1 09/16/10 14:35 75-27-44.7Bromoform ND ug/kg 1 09/16/10 14:35 75-25-24.7Bromomethane ND ug/kg 1 09/16/10 14:35 74-83-94.72-Butanone (MEK) ND ug/kg 1 09/16/10 14:35 78-93-323.6n-Butylbenzene ND ug/kg 1 09/16/10 14:35 104-51-84.7sec-Butylbenzene ND ug/kg 1 09/16/10 14:35 135-98-84.7tert-Butylbenzene ND ug/kg 1 09/16/10 14:35 98-06-64.7Carbon disulfide ND ug/kg 1 09/16/10 14:35 75-15-09.4Carbon tetrachloride ND ug/kg 1 09/16/10 14:35 56-23-54.7Chlorobenzene ND ug/kg 1 09/16/10 14:35 108-90-74.7Chloroethane ND ug/kg 1 09/16/10 14:35 75-00-34.7Chloroform ND ug/kg 1 09/16/10 14:35 67-66-34.7Chloromethane ND ug/kg 1 09/16/10 14:35 74-87-34.72-Chlorotoluene ND ug/kg 1 09/16/10 14:35 95-49-84.74-Chlorotoluene ND ug/kg 1 09/16/10 14:35 106-43-44.7Dibromochloromethane ND ug/kg 1 09/16/10 14:35 124-48-14.71,2-Dibromoethane (EDB) ND ug/kg 1 09/16/10 14:35 106-93-44.7Dibromomethane ND ug/kg 1 09/16/10 14:35 74-95-34.71,2-Dichlorobenzene ND ug/kg 1 09/16/10 14:35 95-50-14.7



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(317)875-5894

ANALYTICAL RESULTS






1,3-Dichlorobenzene ND ug/kg 1 09/16/10 14:35 541-73-14.71,4-Dichlorobenzene ND ug/kg 1 09/16/10 14:35 106-46-74.7trans-1,4-Dichloro-2-butene ND ug/kg 1 09/16/10 14:35 110-57-694.4Dichlorodifluoromethane ND ug/kg 1 09/16/10 14:35 75-71-84.71,1-Dichloroethane ND ug/kg 1 09/16/10 14:35 75-34-34.71,2-Dichloroethane ND ug/kg 1 09/16/10 14:35 107-06-24.71,1-Dichloroethene ND ug/kg 1 09/16/10 14:35 75-35-44.7cis-1,2-Dichloroethene ND ug/kg 1 09/16/10 14:35 156-59-24.7trans-1,2-Dichloroethene ND ug/kg 1 09/16/10 14:35 156-60-54.71,2-Dichloropropane ND ug/kg 1 09/16/10 14:35 78-87-54.71,3-Dichloropropane ND ug/kg 1 09/16/10 14:35 142-28-94.72,2-Dichloropropane ND ug/kg 1 09/16/10 14:35 594-20-74.71,1-Dichloropropene ND ug/kg 1 09/16/10 14:35 563-58-64.7cis-1,3-Dichloropropene ND ug/kg 1 09/16/10 14:35 10061-01-54.7trans-1,3-Dichloropropene ND ug/kg 1 09/16/10 14:35 10061-02-64.7Ethylbenzene ND ug/kg 1 09/16/10 14:35 100-41-44.7Ethyl methacrylate ND ug/kg 1 09/16/10 14:35 97-63-29.4Hexachloro-1,3-butadiene ND ug/kg 1 09/16/10 14:35 87-68-34.72-Hexanone ND ug/kg 1 09/16/10 14:35 591-78-694.4Iodomethane ND ug/kg 1 09/16/10 14:35 74-88-494.4Isopropylbenzene (Cumene) ND ug/kg 1 09/16/10 14:35 98-82-84.7p-Isopropyltoluene ND ug/kg 1 09/16/10 14:35 99-87-64.7Methylene chloride ND ug/kg 1 09/16/10 14:35 75-09-218.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/16/10 14:35 108-10-123.6Methyl-tert-butyl ether ND ug/kg 1 09/16/10 14:35 1634-04-44.7Naphthalene ND ug/kg 1 09/16/10 14:35 91-20-34.7n-Propylbenzene ND ug/kg 1 09/16/10 14:35 103-65-14.7Styrene ND ug/kg 1 09/16/10 14:35 100-42-54.71,1,1,2-Tetrachloroethane ND ug/kg 1 09/16/10 14:35 630-20-64.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/16/10 14:35 79-34-54.7Tetrachloroethene ND ug/kg 1 09/16/10 14:35 127-18-44.7Toluene ND ug/kg 1 09/16/10 14:35 108-88-34.71,2,3-Trichlorobenzene ND ug/kg 1 09/16/10 14:35 87-61-64.71,2,4-Trichlorobenzene ND ug/kg 1 09/16/10 14:35 120-82-14.71,1,1-Trichloroethane ND ug/kg 1 09/16/10 14:35 71-55-64.71,1,2-Trichloroethane ND ug/kg 1 09/16/10 14:35 79-00-54.7Trichloroethene ND ug/kg 1 09/16/10 14:35 79-01-64.7Trichlorofluoromethane ND ug/kg 1 09/16/10 14:35 75-69-44.71,2,3-Trichloropropane ND ug/kg 1 09/16/10 14:35 96-18-44.71,2,4-Trimethylbenzene ND ug/kg 1 09/16/10 14:35 95-63-64.71,3,5-Trimethylbenzene ND ug/kg 1 09/16/10 14:35 108-67-84.7Vinyl acetate ND ug/kg 1 09/16/10 14:35 108-05-494.4Vinyl chloride ND ug/kg 1 09/16/10 14:35 75-01-44.7Xylene (Total) ND ug/kg 1 09/16/10 14:35 1330-20-79.4Dibromofluoromethane (S) 100 % 1 09/16/10 14:35 1868-53-780-124Toluene-d8 (S) 109 % 1 09/16/10 14:35 2037-26-558-145



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(317)875-5894

ANALYTICAL RESULTS






4-Bromofluorobenzene (S) 99 % 1 09/16/10 14:35 460-00-461-131





Date: 09/20/2010 04:28 PM Page 21 of 48



(317)875-5894

ANALYTICAL RESULTS



Sample: SB-8_(4-5) Lab ID: 5041216008 Collected: 09/09/10 15:35 Received: 09/10/10 12:40 Matrix: SolidResults reported on a "dry-weight" basis





Mercury ND mg/kg 1 09/15/10 17:38 7439-97-609/14/10 00:000.34


Acenaphthene ND ug/kg 1 09/13/10 14:03 83-32-909/13/10 00:5026.0Acenaphthylene 350 ug/kg 1 09/13/10 14:03 208-96-809/13/10 00:5026.0Anthracene 197 ug/kg 1 09/13/10 14:03 120-12-709/13/10 00:5026.0Benzo(a)anthracene 838 ug/kg 1 09/13/10 14:03 56-55-309/13/10 00:5026.0Benzo(a)pyrene 832 ug/kg 1 09/13/10 14:03 50-32-809/13/10 00:5026.0Benzo(b)fluoranthene 974 ug/kg 1 09/13/10 14:03 205-99-209/13/10 00:5026.0Benzo(g,h,i)perylene 515 ug/kg 1 09/13/10 14:03 191-24-209/13/10 00:5026.0Benzo(k)fluoranthene 946 ug/kg 1 09/13/10 14:03 207-08-909/13/10 00:5026.0Chrysene 912 ug/kg 1 09/13/10 14:03 218-01-909/13/10 00:5026.0Dibenz(a,h)anthracene 259 ug/kg 1 09/13/10 14:03 53-70-309/13/10 00:5026.0Fluoranthene 1230 ug/kg 1 09/13/10 14:03 206-44-009/13/10 00:5026.0Fluorene 31.4 ug/kg 1 09/13/10 14:03 86-73-709/13/10 00:5026.0Indeno(1,2,3-cd)pyrene 525 ug/kg 1 09/13/10 14:03 193-39-509/13/10 00:5026.02-Methylnaphthalene 198 ug/kg 1 09/13/10 14:03 91-57-609/13/10 00:5026.0Naphthalene 158 ug/kg 1 09/13/10 14:03 91-20-309/13/10 00:5026.0Phenanthrene 462 ug/kg 1 09/13/10 14:03 85-01-809/13/10 00:5026.0Pyrene 1160 ug/kg 1 09/13/10 14:03 129-00-009/13/10 00:5026.02-Fluorobiphenyl (S) 56 % 1 09/13/10 14:03 321-60-809/13/10 00:5046-109Terphenyl-d14 (S) 60 % 1 09/13/10 14:03 1718-51-009/13/10 00:5043-107


Acetone ND ug/kg 1 09/16/10 15:03 67-64-1112Acrolein ND ug/kg 1 09/16/10 15:03 107-02-8112Acrylonitrile ND ug/kg 1 09/16/10 15:03 107-13-1112Benzene ND ug/kg 1 09/16/10 15:03 71-43-25.6Bromobenzene ND ug/kg 1 09/16/10 15:03 108-86-15.6Bromochloromethane ND ug/kg 1 09/16/10 15:03 74-97-55.6Bromodichloromethane ND ug/kg 1 09/16/10 15:03 75-27-45.6Bromoform ND ug/kg 1 09/16/10 15:03 75-25-25.6Bromomethane ND ug/kg 1 09/16/10 15:03 74-83-95.62-Butanone (MEK) ND ug/kg 1 09/16/10 15:03 78-93-327.9n-Butylbenzene ND ug/kg 1 09/16/10 15:03 104-51-85.6sec-Butylbenzene ND ug/kg 1 09/16/10 15:03 135-98-85.6



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(317)875-5894

ANALYTICAL RESULTS






tert-Butylbenzene ND ug/kg 1 09/16/10 15:03 98-06-65.6Carbon disulfide ND ug/kg 1 09/16/10 15:03 75-15-011.2Carbon tetrachloride ND ug/kg 1 09/16/10 15:03 56-23-55.6Chlorobenzene ND ug/kg 1 09/16/10 15:03 108-90-75.6Chloroethane ND ug/kg 1 09/16/10 15:03 75-00-35.6Chloroform ND ug/kg 1 09/16/10 15:03 67-66-35.6Chloromethane ND ug/kg 1 09/16/10 15:03 74-87-35.62-Chlorotoluene ND ug/kg 1 09/16/10 15:03 95-49-85.64-Chlorotoluene ND ug/kg 1 09/16/10 15:03 106-43-45.6Dibromochloromethane ND ug/kg 1 09/16/10 15:03 124-48-15.61,2-Dibromoethane (EDB) ND ug/kg 1 09/16/10 15:03 106-93-45.6Dibromomethane ND ug/kg 1 09/16/10 15:03 74-95-35.61,2-Dichlorobenzene ND ug/kg 1 09/16/10 15:03 95-50-15.61,3-Dichlorobenzene ND ug/kg 1 09/16/10 15:03 541-73-15.61,4-Dichlorobenzene ND ug/kg 1 09/16/10 15:03 106-46-75.6trans-1,4-Dichloro-2-butene ND ug/kg 1 09/16/10 15:03 110-57-6112Dichlorodifluoromethane ND ug/kg 1 09/16/10 15:03 75-71-85.61,1-Dichloroethane ND ug/kg 1 09/16/10 15:03 75-34-35.61,2-Dichloroethane ND ug/kg 1 09/16/10 15:03 107-06-25.61,1-Dichloroethene ND ug/kg 1 09/16/10 15:03 75-35-45.6cis-1,2-Dichloroethene ND ug/kg 1 09/16/10 15:03 156-59-25.6trans-1,2-Dichloroethene ND ug/kg 1 09/16/10 15:03 156-60-55.61,2-Dichloropropane ND ug/kg 1 09/16/10 15:03 78-87-55.61,3-Dichloropropane ND ug/kg 1 09/16/10 15:03 142-28-95.62,2-Dichloropropane ND ug/kg 1 09/16/10 15:03 594-20-75.61,1-Dichloropropene ND ug/kg 1 09/16/10 15:03 563-58-65.6cis-1,3-Dichloropropene ND ug/kg 1 09/16/10 15:03 10061-01-55.6trans-1,3-Dichloropropene ND ug/kg 1 09/16/10 15:03 10061-02-65.6Ethylbenzene ND ug/kg 1 09/16/10 15:03 100-41-45.6Ethyl methacrylate ND ug/kg 1 09/16/10 15:03 97-63-211.2Hexachloro-1,3-butadiene ND ug/kg 1 09/16/10 15:03 87-68-35.62-Hexanone ND ug/kg 1 09/16/10 15:03 591-78-6112Iodomethane ND ug/kg 1 09/16/10 15:03 74-88-4112Isopropylbenzene (Cumene) ND ug/kg 1 09/16/10 15:03 98-82-85.6p-Isopropyltoluene ND ug/kg 1 09/16/10 15:03 99-87-65.6Methylene chloride ND ug/kg 1 09/16/10 15:03 75-09-222.34-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/16/10 15:03 108-10-127.9Methyl-tert-butyl ether ND ug/kg 1 09/16/10 15:03 1634-04-45.6Naphthalene ND ug/kg 1 09/16/10 15:03 91-20-35.6n-Propylbenzene ND ug/kg 1 09/16/10 15:03 103-65-15.6Styrene ND ug/kg 1 09/16/10 15:03 100-42-55.61,1,1,2-Tetrachloroethane ND ug/kg 1 09/16/10 15:03 630-20-65.61,1,2,2-Tetrachloroethane ND ug/kg 1 09/16/10 15:03 79-34-55.6Tetrachloroethene ND ug/kg 1 09/16/10 15:03 127-18-45.6Toluene ND ug/kg 1 09/16/10 15:03 108-88-35.61,2,3-Trichlorobenzene ND ug/kg 1 09/16/10 15:03 87-61-65.6



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(317)875-5894

ANALYTICAL RESULTS






1,2,4-Trichlorobenzene ND ug/kg 1 09/16/10 15:03 120-82-15.61,1,1-Trichloroethane ND ug/kg 1 09/16/10 15:03 71-55-65.61,1,2-Trichloroethane ND ug/kg 1 09/16/10 15:03 79-00-55.6Trichloroethene ND ug/kg 1 09/16/10 15:03 79-01-65.6Trichlorofluoromethane ND ug/kg 1 09/16/10 15:03 75-69-45.61,2,3-Trichloropropane ND ug/kg 1 09/16/10 15:03 96-18-45.61,2,4-Trimethylbenzene ND ug/kg 1 09/16/10 15:03 95-63-65.61,3,5-Trimethylbenzene ND ug/kg 1 09/16/10 15:03 108-67-85.6Vinyl acetate ND ug/kg 1 09/16/10 15:03 108-05-4112Vinyl chloride ND ug/kg 1 09/16/10 15:03 75-01-45.6Xylene (Total) ND ug/kg 1 09/16/10 15:03 1330-20-711.2Dibromofluoromethane (S) 99 % 1 09/16/10 15:03 1868-53-780-124Toluene-d8 (S) 105 % 1 09/16/10 15:03 2037-26-558-1454-Bromofluorobenzene (S) 91 % 1 09/16/10 15:03 460-00-461-131





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(317)875-5894

ANALYTICAL RESULTS








Mercury ND mg/kg 1 09/15/10 17:39 7439-97-609/14/10 00:000.34


Acenaphthene ND ug/kg 1 09/13/10 14:20 83-32-909/13/10 00:5026.1Acenaphthylene 792 ug/kg 1 09/13/10 14:20 208-96-809/13/10 00:5026.1Anthracene 511 ug/kg 1 09/13/10 14:20 120-12-709/13/10 00:5026.1Benzo(a)anthracene 2440 ug/kg 1 09/13/10 14:20 56-55-309/13/10 00:5026.1Benzo(a)pyrene 2270 ug/kg 1 09/13/10 14:20 50-32-809/13/10 00:5026.1Benzo(b)fluoranthene 2530 ug/kg 1 09/13/10 14:20 205-99-209/13/10 00:5026.1Benzo(g,h,i)perylene 1290 ug/kg 1 09/13/10 14:20 191-24-209/13/10 00:5026.1Benzo(k)fluoranthene 2650 ug/kg 1 09/13/10 14:20 207-08-909/13/10 00:5026.1Chrysene 2570 ug/kg 1 09/13/10 14:20 218-01-909/13/10 00:5026.1Dibenz(a,h)anthracene 673 ug/kg 1 09/13/10 14:20 53-70-309/13/10 00:5026.1Fluoranthene 2340 ug/kg 1 09/13/10 14:20 206-44-009/13/10 00:5026.1Fluorene 54.7 ug/kg 1 09/13/10 14:20 86-73-709/13/10 00:5026.1Indeno(1,2,3-cd)pyrene 1340 ug/kg 1 09/13/10 14:20 193-39-509/13/10 00:5026.12-Methylnaphthalene 252 ug/kg 1 09/13/10 14:20 91-57-609/13/10 00:5026.1Naphthalene 198 ug/kg 1 09/13/10 14:20 91-20-309/13/10 00:5026.1Phenanthrene 666 ug/kg 1 09/13/10 14:20 85-01-809/13/10 00:5026.1Pyrene 2610 ug/kg 1 09/13/10 14:20 129-00-009/13/10 00:5026.12-Fluorobiphenyl (S) 63 % 1 09/13/10 14:20 321-60-809/13/10 00:5046-109Terphenyl-d14 (S) 66 % 1 09/13/10 14:20 1718-51-009/13/10 00:5043-107


Acetone ND ug/kg 1 09/16/10 15:30 67-64-1120Acrolein ND ug/kg 1 09/16/10 15:30 107-02-8120Acrylonitrile ND ug/kg 1 09/16/10 15:30 107-13-1120Benzene ND ug/kg 1 09/16/10 15:30 71-43-26.0Bromobenzene ND ug/kg 1 09/16/10 15:30 108-86-16.0Bromochloromethane ND ug/kg 1 09/16/10 15:30 74-97-56.0Bromodichloromethane ND ug/kg 1 09/16/10 15:30 75-27-46.0Bromoform ND ug/kg 1 09/16/10 15:30 75-25-26.0Bromomethane ND ug/kg 1 09/16/10 15:30 74-83-96.02-Butanone (MEK) ND ug/kg 1 09/16/10 15:30 78-93-330.0n-Butylbenzene ND ug/kg 1 09/16/10 15:30 104-51-86.0sec-Butylbenzene ND ug/kg 1 09/16/10 15:30 135-98-86.0



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(317)875-5894

ANALYTICAL RESULTS






tert-Butylbenzene ND ug/kg 1 09/16/10 15:30 98-06-66.0Carbon disulfide ND ug/kg 1 09/16/10 15:30 75-15-012.0Carbon tetrachloride ND ug/kg 1 09/16/10 15:30 56-23-56.0Chlorobenzene ND ug/kg 1 09/16/10 15:30 108-90-76.0Chloroethane ND ug/kg 1 09/16/10 15:30 75-00-36.0Chloroform ND ug/kg 1 09/16/10 15:30 67-66-36.0Chloromethane ND ug/kg 1 09/16/10 15:30 74-87-36.02-Chlorotoluene ND ug/kg 1 09/16/10 15:30 95-49-86.04-Chlorotoluene ND ug/kg 1 09/16/10 15:30 106-43-46.0Dibromochloromethane ND ug/kg 1 09/16/10 15:30 124-48-16.01,2-Dibromoethane (EDB) ND ug/kg 1 09/16/10 15:30 106-93-46.0Dibromomethane ND ug/kg 1 09/16/10 15:30 74-95-36.01,2-Dichlorobenzene ND ug/kg 1 09/16/10 15:30 95-50-16.01,3-Dichlorobenzene ND ug/kg 1 09/16/10 15:30 541-73-16.01,4-Dichlorobenzene ND ug/kg 1 09/16/10 15:30 106-46-76.0trans-1,4-Dichloro-2-butene ND ug/kg 1 09/16/10 15:30 110-57-6120Dichlorodifluoromethane ND ug/kg 1 09/16/10 15:30 75-71-86.01,1-Dichloroethane ND ug/kg 1 09/16/10 15:30 75-34-36.01,2-Dichloroethane ND ug/kg 1 09/16/10 15:30 107-06-26.01,1-Dichloroethene ND ug/kg 1 09/16/10 15:30 75-35-46.0cis-1,2-Dichloroethene ND ug/kg 1 09/16/10 15:30 156-59-26.0trans-1,2-Dichloroethene ND ug/kg 1 09/16/10 15:30 156-60-56.01,2-Dichloropropane ND ug/kg 1 09/16/10 15:30 78-87-56.01,3-Dichloropropane ND ug/kg 1 09/16/10 15:30 142-28-96.02,2-Dichloropropane ND ug/kg 1 09/16/10 15:30 594-20-76.01,1-Dichloropropene ND ug/kg 1 09/16/10 15:30 563-58-66.0cis-1,3-Dichloropropene ND ug/kg 1 09/16/10 15:30 10061-01-56.0trans-1,3-Dichloropropene ND ug/kg 1 09/16/10 15:30 10061-02-66.0Ethylbenzene ND ug/kg 1 09/16/10 15:30 100-41-46.0Ethyl methacrylate ND ug/kg 1 09/16/10 15:30 97-63-212.0Hexachloro-1,3-butadiene ND ug/kg 1 09/16/10 15:30 87-68-36.02-Hexanone ND ug/kg 1 09/16/10 15:30 591-78-6120Iodomethane ND ug/kg 1 09/16/10 15:30 74-88-4120Isopropylbenzene (Cumene) ND ug/kg 1 09/16/10 15:30 98-82-86.0p-Isopropyltoluene ND ug/kg 1 09/16/10 15:30 99-87-66.0Methylene chloride ND ug/kg 1 09/16/10 15:30 75-09-224.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/16/10 15:30 108-10-130.0Methyl-tert-butyl ether ND ug/kg 1 09/16/10 15:30 1634-04-46.0Naphthalene ND ug/kg 1 09/16/10 15:30 91-20-36.0n-Propylbenzene ND ug/kg 1 09/16/10 15:30 103-65-16.0Styrene ND ug/kg 1 09/16/10 15:30 100-42-56.01,1,1,2-Tetrachloroethane ND ug/kg 1 09/16/10 15:30 630-20-66.01,1,2,2-Tetrachloroethane ND ug/kg 1 09/16/10 15:30 79-34-56.0Tetrachloroethene ND ug/kg 1 09/16/10 15:30 127-18-46.0Toluene ND ug/kg 1 09/16/10 15:30 108-88-36.01,2,3-Trichlorobenzene ND ug/kg 1 09/16/10 15:30 87-61-66.0



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(317)875-5894

ANALYTICAL RESULTS






1,2,4-Trichlorobenzene ND ug/kg 1 09/16/10 15:30 120-82-16.01,1,1-Trichloroethane ND ug/kg 1 09/16/10 15:30 71-55-66.01,1,2-Trichloroethane ND ug/kg 1 09/16/10 15:30 79-00-56.0Trichloroethene ND ug/kg 1 09/16/10 15:30 79-01-66.0Trichlorofluoromethane ND ug/kg 1 09/16/10 15:30 75-69-46.01,2,3-Trichloropropane ND ug/kg 1 09/16/10 15:30 96-18-46.01,2,4-Trimethylbenzene ND ug/kg 1 09/16/10 15:30 95-63-66.01,3,5-Trimethylbenzene ND ug/kg 1 09/16/10 15:30 108-67-86.0Vinyl acetate ND ug/kg 1 09/16/10 15:30 108-05-4120Vinyl chloride ND ug/kg 1 09/16/10 15:30 75-01-46.0Xylene (Total) ND ug/kg 1 09/16/10 15:30 1330-20-712.0Dibromofluoromethane (S) 100 % 1 09/16/10 15:30 1868-53-780-124Toluene-d8 (S) 105 % 1 09/16/10 15:30 2037-26-558-1454-Bromofluorobenzene (S) 91 % 1 09/16/10 15:30 460-00-461-131





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(317)875-5894

ANALYTICAL RESULTS









Date: 09/20/2010 04:28 PM Page 28 of 48



(317)875-5894

ANALYTICAL RESULTS









Date: 09/20/2010 04:28 PM Page 29 of 48



(317)875-5894






MPRP/6305EPA 3050

EPA 60106010 MET






Matrix: Solid

Analyzed


Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

5041200003

479203

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic mg/kg 79.6 91 75-12591 6 2074.210.1 82.5 77.6Barium mg/kg 79.6 110 75-125105 5 2074.2102 190 180Cadmium mg/kg 79.6 81 75-12579 9 2074.2ND 65.1 59.3Chromium mg/kg 79.6 92 75-12591 7 2074.216.9 90.2 84.4Lead mg/kg 79.6 81 75-12579 8 2074.213.4 78.2 72.0Selenium mg/kg 79.6 87 75-12585 9 2074.2ND 71.3 65.1Silver mg/kg 39.8 78 75-12577 8 2037.1ND 31.0 28.6



Date: 09/20/2010 04:28 PM Page 30 of 48



(317)875-5894






MPRP/6313EPA 3010

EPA 60106010 MET






Matrix: Water

Analyzed

Arsenic ug/L ND 10.0 09/15/10 16:05Barium ug/L ND 100 09/15/10 16:05Cadmium ug/L ND 5.0 09/15/10 16:05Chromium ug/L ND 10.0 09/15/10 16:05Lead ug/L ND 10.0 09/15/10 16:05Selenium ug/L ND 10.0 09/15/10 16:05Silver ug/L ND 50.0 09/15/10 16:05

Parameter UnitsLCS



Arsenic ug/L 9561000 96 80-120Barium ug/L 9431000 94 80-120Cadmium ug/L 9391000 94 80-120Chromium ug/L 9251000 92 80-120Lead ug/L 9201000 92 80-120Selenium ug/L 9391000 94 80-120Silver ug/L 454500 91 80-120

Parameter UnitsMS



MSSpikeResult

5041231002

479389

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic ug/L 1000 98 75-12597 .8 201000ND 978 969Barium ug/L 1000 92 75-12589 3 201000103 1030 996Cadmium ug/L 1000 95 75-12594 1 201000ND 947 938Chromium ug/L 1000 89 75-12588 2 201000ND 896 877Lead ug/L 1000 98 75-125100 1 201000ND 988 1000Selenium ug/L 1000 95 75-12593 2 201000ND 945 930Silver ug/L 500 91 75-12590 2 20500ND 457 449



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(317)875-5894






MERP/2806EPA 7470







Matrix: Water

Analyzed

Mercury ug/L ND 2.0 09/15/10 10:38

Parameter UnitsLCS



Mercury ug/L 5.15 101 80-120

Parameter UnitsMS



MSSpikeResult

5041053001

479622

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L 5 109 75-125108 1 205ND 5.6 5.5



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(317)875-5894






MERP/2808EPA 7471







Matrix: Solid

Analyzed

Mercury mg/kg ND 0.33 09/15/10 17:21

Parameter UnitsLCS



Mercury mg/kg 0.53.5 106 80-120

Parameter UnitsMS



MSSpikeResult

5041136001

480005

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .54 96 75-12599 3 20.54ND 0.61 0.63



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(317)875-5894






OEXT/20717EPA 3546







Matrix: Solid

Analyzed


Parameter UnitsLCS






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(317)875-5894




Parameter UnitsLCS



Terphenyl-d14 (S) % 86 43-107

Parameter UnitsMS



MSSpikeResult

5041208005

479160

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2-Methylnaphthalene ug/kg 2200 79 43-10674 6 202200ND 1740 1630Acenaphthene ug/kg 2200 81 46-10177 5 202200ND 1800 1710Acenaphthylene ug/kg 2200 83 47-10578 6 202200ND 1830 1730Anthracene ug/kg 2200 81 39-11276 6 202200ND 1770 1670Benzo(a)anthracene ug/kg 2200 78 36-10574 6 202200ND 1730 1630Benzo(a)pyrene ug/kg 2200 81 34-11376 7 202200ND 1790 1670Benzo(b)fluoranthene ug/kg 2200 81 33-11178 3 202200ND 1780 1720Benzo(g,h,i)perylene ug/kg 2200 79 26-10973 8 202200ND 1740 1610Benzo(k)fluoranthene ug/kg 2200 86 31-11678 9 202200ND 1880 1720Chrysene ug/kg 2200 83 34-10978 6 202200ND 1820 1710Dibenz(a,h)anthracene ug/kg 2200 80 32-11174 8 202200ND 1760 1630Fluoranthene ug/kg 2200 83 33-11779 5 202200ND 1820 1730Fluorene ug/kg 2200 80 44-10775 5 2022000.034

mg/kg1790 1690

Indeno(1,2,3-cd)pyrene ug/kg 2200 80 27-11374 7 202200ND 1750 1620Naphthalene ug/kg 2200 82 45-10677 6 202200ND 1810 1700Phenanthrene ug/kg 2200 81 42-10376 6 2022000.066

mg/kg1860 1750

Pyrene ug/kg 2200 84 36-11179 7 202200ND 1860 17402-Fluorobiphenyl (S) % 83 46-10979 20Terphenyl-d14 (S) % 82 43-10777 20



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OEXT/20724EPA 3510

EPA 8270 by SIM8270 Water PAH by SIM MSSV






Matrix: Water

Analyzed

2-Methylnaphthalene ug/L ND 1.0 09/13/10 20:22Acenaphthene ug/L ND 1.0 09/13/10 20:22Acenaphthylene ug/L ND 1.0 09/13/10 20:22Anthracene ug/L ND 0.10 09/13/10 20:22Benzo(a)anthracene ug/L ND 0.10 09/13/10 20:22Benzo(a)pyrene ug/L ND 0.10 09/13/10 20:22Benzo(b)fluoranthene ug/L ND 0.10 09/13/10 20:22Benzo(g,h,i)perylene ug/L ND 0.10 09/13/10 20:22Benzo(k)fluoranthene ug/L ND 0.10 09/13/10 20:22Chrysene ug/L ND 0.50 09/13/10 20:22Dibenz(a,h)anthracene ug/L ND 0.10 09/13/10 20:22Fluoranthene ug/L ND 1.0 09/13/10 20:22Fluorene ug/L ND 1.0 09/13/10 20:22Indeno(1,2,3-cd)pyrene ug/L ND 0.10 09/13/10 20:22Naphthalene ug/L ND 1.0 09/13/10 20:22Phenanthrene ug/L ND 1.0 09/13/10 20:22Pyrene ug/L ND 1.0 09/13/10 20:222-Fluorobiphenyl (S) % 61 35-94 09/13/10 20:22Terphenyl-d14 (S) % 92 19-101 09/13/10 20:22

Parameter UnitsLCS



2-Methylnaphthalene ug/L 4.110 41 24-104Acenaphthene ug/L 5.110 51 31-108Acenaphthylene ug/L 5.210 52 33-111Anthracene ug/L 6.910 69 45-120Benzo(a)anthracene ug/L 7.810 78 51-119Benzo(a)pyrene ug/L 7.810 78 52-124Benzo(b)fluoranthene ug/L 8.110 81 51-122Benzo(g,h,i)perylene ug/L 7.610 76 48-112Benzo(k)fluoranthene ug/L 8.410 84 53-123Chrysene ug/L 8.310 83 54-118Dibenz(a,h)anthracene ug/L 7.710 77 49-114Fluoranthene ug/L 8.010 80 52-122Fluorene ug/L 5.610 56 38-113Indeno(1,2,3-cd)pyrene ug/L 7.710 77 49-114Naphthalene ug/L 4.410 44 27-103Phenanthrene ug/L 6.710 67 43-112Pyrene ug/L 8.110 81 51-1202-Fluorobiphenyl (S) % 45 35-94



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Parameter UnitsLCS



Terphenyl-d14 (S) % 78 19-101



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MSV/26660EPA 8260

EPA 82608260 MSV

Associated Lab Samples: 5041216001, 5041216002, 5041216003, 5041216004, 5041216005, 5041216006, 5041216010





Matrix: Water

Analyzed




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Matrix: Water

Analyzed

Dibromomethane ug/L ND 5.0 09/15/10 03:26Dichlorodifluoromethane ug/L ND 5.0 09/15/10 03:26Ethyl methacrylate ug/L ND 100 09/15/10 03:26Ethylbenzene ug/L ND 5.0 09/15/10 03:26Hexachloro-1,3-butadiene ug/L ND 5.0 09/15/10 03:26Iodomethane ug/L ND 10.0 09/15/10 03:26Isopropylbenzene (Cumene) ug/L ND 5.0 09/15/10 03:26Methyl-tert-butyl ether ug/L ND 4.0 09/15/10 03:26Methylene chloride ug/L ND 5.0 09/15/10 03:26n-Butylbenzene ug/L ND 5.0 09/15/10 03:26n-Hexane ug/L ND 5.0 09/15/10 03:26n-Propylbenzene ug/L ND 5.0 09/15/10 03:26Naphthalene ug/L ND 5.0 09/15/10 03:26p-Isopropyltoluene ug/L ND 5.0 09/15/10 03:26sec-Butylbenzene ug/L ND 5.0 09/15/10 03:26Styrene ug/L ND 5.0 09/15/10 03:26tert-Butylbenzene ug/L ND 5.0 09/15/10 03:26Tetrachloroethene ug/L ND 5.0 09/15/10 03:26Toluene ug/L ND 5.0 09/15/10 03:26trans-1,2-Dichloroethene ug/L ND 5.0 09/15/10 03:26trans-1,3-Dichloropropene ug/L ND 5.0 09/15/10 03:26trans-1,4-Dichloro-2-butene ug/L ND 100 09/15/10 03:26Trichloroethene ug/L ND 5.0 09/15/10 03:26Trichlorofluoromethane ug/L ND 5.0 09/15/10 03:26Vinyl acetate ug/L ND 10.0 09/15/10 03:26Vinyl chloride ug/L ND 2.0 09/15/10 03:26Xylene (Total) ug/L ND 10.0 09/15/10 03:264-Bromofluorobenzene (S) % 97 70-126 09/15/10 03:26Dibromofluoromethane (S) % 98 80-123 09/15/10 03:26Toluene-d8 (S) % 101 80-116 09/15/10 03:26

Parameter UnitsLCS






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Parameter UnitsLCS






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Parameter UnitsLCS




Parameter UnitsMS


480574MATRIX SPIKE SAMPLE:MSSpike

Result5041052003

1,1,1,2-Tetrachloroethane ug/L 75.3100 75 55-131ND1,1,1-Trichloroethane ug/L 80.2100 80 64-143ND1,1,2,2-Tetrachloroethane ug/L 82.7100 83 64-142ND1,1,2-Trichloroethane ug/L 78.8100 79 71-143ND1,1-Dichloroethane ug/L 82.4100 82 68-139ND1,1-Dichloroethene ug/L 94.7100 95 55-140ND1,1-Dichloropropene ug/L 88.8100 89 66-140ND1,2,3-Trichlorobenzene ug/L 62.9100 63 33-140ND1,2,3-Trichloropropane ug/L 115200 58 58-133ND1,2,4-Trichlorobenzene ug/L 59.5100 59 28-140ND1,2,4-Trimethylbenzene ug/L 72.4100 72 39-146ND1,2-Dibromoethane (EDB) ug/L 82.8100 83 67-134ND1,2-Dichlorobenzene ug/L 71.2100 71 48-137ND1,2-Dichloroethane ug/L 72.6100 73 63-148ND1,2-Dichloropropane ug/L 81.2100 81 70-136ND1,3,5-Trimethylbenzene ug/L 78.4100 78 39-145ND1,3-Dichlorobenzene ug/L 71.7100 72 40-143ND1,3-Dichloropropane ug/L 82.5100 82 65-133ND1,4-Dichlorobenzene ug/L 70.8100 71 38-142ND2,2-Dichloropropane ug/L 48.2100 48 35-157ND2-Butanone (MEK) ug/L 400500 80 62-132ND2-Chlorotoluene ug/L 75.4100 75 44-143ND2-Hexanone ug/L 436500 87 61-141ND4-Chlorotoluene ug/L 78.2100 78 43-140ND4-Methyl-2-pentanone (MIBK) ug/L 428500 86 57-135NDAcetone ug/L 403500 81 30-170NDAcrolein ug/L 29802000 149 30-170NDAcrylonitrile ug/L 14402000 72 66-137NDBenzene ug/L 85.8100 86 63-141ND



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Parameter UnitsMS


480574MATRIX SPIKE SAMPLE:MSSpike

Result5041052003

Bromobenzene ug/L 74.5100 75 57-128NDBromochloromethane ug/L 91.5100 92 65-157NDBromodichloromethane ug/L 75.6100 76 63-135NDBromoform ug/L 69.3100 69 58-124NDBromomethane ug/L 35.3100 35 30-170NDCarbon disulfide ug/L 170200 85 46-162NDCarbon tetrachloride ug/L 78.8100 79 54-145NDChlorobenzene ug/L 79.1100 79 56-133NDChloroethane ug/L 81.4100 81 54-157NDChloroform ug/L 76.8100 77 67-134NDChloromethane ug/L 52.8100 53 36-137NDcis-1,2-Dichloroethene ug/L 88.9100 89 65-132NDcis-1,3-Dichloropropene ug/L 63.5100 64 46-121NDDibromochloromethane ug/L 71.0100 71 64-124NDDibromomethane ug/L 82.4100 82 67-144NDDichlorodifluoromethane ug/L 106100 106 30-163NDEthyl methacrylate ug/L 323400 81 52-140NDEthylbenzene ug/L 82.2100 82 44-151NDHexachloro-1,3-butadiene ug/L 60.2100 60 30-145NDIodomethane ug/L 137200 69 28-168NDIsopropylbenzene (Cumene) ug/L 78.8100 79 40-148NDMethyl-tert-butyl ether ug/L 164200 82 52-156NDMethylene chloride ug/L 82.8100 83 46-154NDn-Butylbenzene ug/L 64.2100 64 27-153NDn-Hexane ug/L 98.5100 98 32-176NDn-Propylbenzene ug/L 75.4100 75 40-148NDNaphthalene ug/L 75.2100 75 44-138NDp-Isopropyltoluene ug/L 69.5100 69 34-146NDsec-Butylbenzene ug/L 70.5100 71 38-150NDStyrene ug/L 79.0100 79 38-141NDtert-Butylbenzene ug/L 58.4100 58 32-133NDTetrachloroethene ug/L 82.4100 82 25-146NDToluene ug/L 85.1100 85 59-142NDtrans-1,2-Dichloroethene ug/L 96.5100 97 60-137NDtrans-1,3-Dichloropropene ug/L 55.5100 56 43-117NDtrans-1,4-Dichloro-2-butene ug/L 222400 56 44-139NDTrichloroethene ug/L 85.0100 85 61-137NDTrichlorofluoromethane ug/L 88.8100 89 53-162NDVinyl acetate ug/L 270400 68 24-132NDVinyl chloride ug/L 81.1100 81 51-144NDXylene (Total) ug/L 256300 85 44-152ND4-Bromofluorobenzene (S) % 100 70-126Dibromofluoromethane (S) % 106 80-123Toluene-d8 (S) % 101 80-116



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MSV/26709EPA 8260







Matrix: Solid

Analyzed




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Matrix: Solid

Analyzed


Parameter UnitsLCS






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Parameter UnitsLCS



1,2-Dichlorobenzene ug/kg 51.950 104 75-1171,2-Dichloroethane ug/kg 54.050 108 62-1351,2-Dichloropropane ug/kg 54.250 108 74-1241,3,5-Trimethylbenzene ug/kg 55.550 111 73-1221,3-Dichlorobenzene ug/kg 53.550 107 73-1201,3-Dichloropropane ug/kg 60.250 120 71-1221,4-Dichlorobenzene ug/kg 51.250 102 72-1182,2-Dichloropropane ug/kg 48.750 97 53-1362-Butanone (MEK) ug/kg 359250 144 33-1902-Chlorotoluene ug/kg 54.950 110 72-1222-Hexanone ug/kg 377250 151 44-1684-Chlorotoluene ug/kg 56.950 114 72-1204-Methyl-2-pentanone (MIBK) ug/kg 299250 120 58-126Acetone ug/kg 552 L3250 221 30-190Acrolein ug/kg 7941000 79 30-190Acrylonitrile ug/kg 11601000 116 65-129Benzene ug/kg 54.950 110 76-123Bromobenzene ug/kg 48.550 97 74-116Bromochloromethane ug/kg 58.150 116 56-143Bromodichloromethane ug/kg 45.350 91 67-123Bromoform ug/kg 32.550 65 58-117Bromomethane ug/kg 42.250 84 47-147Carbon disulfide ug/kg 112100 112 56-141Carbon tetrachloride ug/kg 36.950 74 54-136Chlorobenzene ug/kg 54.150 108 75-115Chloroethane ug/kg 59.850 120 57-147Chloroform ug/kg 52.650 105 74-123Chloromethane ug/kg 53.950 108 31-155cis-1,2-Dichloroethene ug/kg 53.450 107 76-119cis-1,3-Dichloropropene ug/kg 49.150 98 56-110Dibromochloromethane ug/kg 37.750 75 63-122Dibromomethane ug/kg 51.650 103 70-127Dichlorodifluoromethane ug/kg 52.550 105 30-170Ethyl methacrylate ug/kg 222200 111 58-126Ethylbenzene ug/kg 53.850 108 78-121Hexachloro-1,3-butadiene ug/kg 45.950 92 65-128Iodomethane ug/kg 89.3J100 89 38-173Isopropylbenzene (Cumene) ug/kg 50.950 102 75-128Methyl-tert-butyl ether ug/kg 104100 104 59-142Methylene chloride ug/kg 49.550 99 30-170n-Butylbenzene ug/kg 52.250 104 70-123n-Propylbenzene ug/kg 57.550 115 70-126Naphthalene ug/kg 49.750 99 60-128p-Isopropyltoluene ug/kg 52.950 106 65-125sec-Butylbenzene ug/kg 54.550 109 72-125Styrene ug/kg 52.850 106 75-118tert-Butylbenzene ug/kg 45.450 91 61-114Tetrachloroethene ug/kg 50.250 100 63-117



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Parameter UnitsLCS






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Parameter UnitsDup



Percent Moisture % 17.5 .6 517.6

Parameter UnitsDup






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QUALIFIERS



DEFINITIONS


LABORATORIES


ANALYTE QUALIFIERSAnalyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

L3



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APPENDIX C

SOIL BORING LOGS