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Soil Sampling of Inn at Otter Crest and City of Toledo Biosolids Land Application Sites in the Siletz Watershed DEQ Biosolids Coordinators: Pat Heins-Portland DEQ, Larry Brown-Bend DEQ, Justin Sterger-Bend DEQ, Tim Ruby-Portland DEQ and Paul Kennedy-Eugene DEQ, Site Visit Date: 4/24/19 Report Date: 9/5/2019 Permittee Land Application Site Inn at Otter Crest File #41740; NPDES Permit #101269 EPA #OR0026352 Wyscaver #3 City of Toledo File #89103; NPDES Permit #101713 EPA No. OR0020869 Hughes Introduction On April 24, DEQ regional biosolids coordinators sampled the above biosolids application sites in the Siletz watershed in Lincoln County to: 1) Determine carryover nitrogen; and 2) Assess whether the land application of biosolids increased the soil carryover nitrogen levels at the above sites. Soil Sampling Protocols Attachment 1 provides the approximate locations for soil cores that comprised the representative biosolid amended soils and “control” samples at each site and photos of the sites. Soil samples were collected at the two land application sites specified above using the Oregon State University extension: Farm and Garden Soil Sample guidance (EC 628 Revised Sept 2013) provided in Attachment 2. Samples were collected from Wyscaver #3 and Hughes on April 24, 2019. Three teams collected two random soil samples from each site. Soils were sampled at 0 to 12 inch and 12 to 24 inch depths. Six soil cores from each depth were composited to create a single representative sample. Setback areas were sampled at 0-12 inch and 12-24 inch soil depths as background and labeled as control samples. On the afternoon of April 25, 2019, DEQ delivered the samples to the Oregon State University’s Crops and Soil Central Analytical Laboratory for analysis. Chain of custody procedures were followed and documented through a photo log (available upon request). Overview of Laboratory Results Attachment 3 provides the analytical data for each soil sample as reported by the OSU laboratory.

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Page 1: Soil Sampling of Inn at Otter Crest and City of Toledo

Soil Sampling of Inn at Otter Crest and City of Toledo Biosolids Land Application Sites in the Siletz Watershed

DEQ Biosolids Coordinators: Pat Heins-Portland DEQ, Larry Brown-Bend DEQ, Justin Sterger-Bend DEQ, Tim Ruby-Portland DEQ and Paul Kennedy-Eugene DEQ, Site Visit Date: 4/24/19 Report Date: 9/5/2019

Permittee Land Application Site

Inn at Otter Crest File #41740; NPDES Permit #101269 EPA #OR0026352

Wyscaver #3

City of Toledo File #89103; NPDES Permit #101713 EPA No. OR0020869

Hughes

Introduction On April 24, DEQ regional biosolids coordinators sampled the above biosolids application sites in the Siletz watershed in Lincoln County to: 1) Determine carryover nitrogen; and 2) Assess whether the land application of biosolids increased the soil carryover nitrogen levels at the above sites. Soil Sampling Protocols Attachment 1 provides the approximate locations for soil cores that comprised the representative biosolid amended soils and “control” samples at each site and photos of the sites. Soil samples were collected at the two land application sites specified above using the Oregon State University extension: Farm and Garden Soil Sample guidance (EC 628 Revised Sept 2013) provided in Attachment 2. Samples were collected from Wyscaver #3 and Hughes on April 24, 2019. Three teams collected two random soil samples from each site. Soils were sampled at 0 to 12 inch and 12 to 24 inch depths. Six soil cores from each depth were composited to create a single representative sample. Setback areas were sampled at 0-12 inch and 12-24 inch soil depths as background and labeled as control samples. On the afternoon of April 25, 2019, DEQ delivered the samples to the Oregon State University’s Crops and Soil Central Analytical Laboratory for analysis. Chain of custody procedures were followed and documented through a photo log (available upon request). Overview of Laboratory Results Attachment 3 provides the analytical data for each soil sample as reported by the OSU laboratory.

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Calculation of Soil Carry-Over Nitrogen Using the data provided by the OSU laboratory, DEQ calculated the soil carry over nitrogen concentrations from the ground surface down 24 inches for each site. The results are listed in the table below. Note: The NH4-N results from the OSU laboratory were not utilized in calculating the residual nitrogen in the fields because the soil samples were oven-dried creating an artificially high NH4-N results. The nitrogen associated with NH4-N is accounted for in the NO3-N results as NH4-N readily converts to NO3-N in aerobic soils.

Field / Soil Depth NO3-N (ppm) NO3-N (lbs/acre) Total NO3-N

(lbs./acre) see Note 1

Wyscaver #3 / 0-12” 8.2 33.0 46.3

Wyscaver #3 / 12-24” 3.3 13.3

Hughes / 0-12” 4.9 19.5 31.1

Hughes / 12-24” 2.9 11.6

Note 1: Every 12 inches: NO3-N ppm X 4 = N lbs/ac. Add 12 inch layers together. )

Conclusion OSU’s Crop and Soil Science Central Analytical Laboratory analyzed samples for nitrogen and soil nutrients. DEQ calculated carryover nitrogen and determined that nitrate-nitrogen levels at Wyscaver #3 and Hughes application sites are below what a pasture grass needs for the 2019 growing season and compliant with the DEQ site authorizations in effect for these sites in 2018. For acceptable ranges of carryover nitrogen, see Attachment 4, OSU Extension Service Nutrient Management for Pastures: Western Oregon and Western Washington EM 9224 (January 2019). Dr. Dan Sullivan, a soil scientist at Oregon State University’s Soil and Crop Science Department also reviewed the analytical results on May 29, 2019. He indicated through email that the Hughes and Wyscaver #3 fields could improve their production with the addition of potassium and magnesium amendments (Attachment 5). Report prepared by: Paul Kennedy NRS4, CPSS-REHS DEQ Western Region – Eugene Office 165 SE 7th Avenue, Suite 100 Eugene, OR 97401 541-687-7439

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Attachment 1 Sampling Locations & Photos

Wyscaver #3, Inn at Otter Crest

Biosolids land application soil sample locations Control sample in setback area

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Hughes, City of Toledo

Biosolids land application sample locations Control sample in setback area

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Site Photos

Photo 1: Wyscaver #3, Inn at Otter Crest

Photo 2: Hughes, City of Toledo

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Attachment 2 Oregon State University extension: Farm and Garden Soil Sample guidance

(EC 628 Revised Sept 2013)

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Attachment 3 Oregon State University’s Crops and Soil Central Analytical Laboratory Results

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Attachment 4 OSU Extension Service Nutrient Management for Pastures:

Western Oregon and Western Washington EM 9224 (January 2019)

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Attachment 5 Dr. Dan Sullivan Email Correspondence

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