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Simec AG
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Test report Numb€r C 34812
Obiect ot
Customer:
Batch:
Sublect:
Method(s):
Nandrolone decanoate
Lightbest International Limited Sampl6s: 1
Rec6lpt: 05.08.2015
Assay, ldentification
HPLC
SEmple/Analysls: Method StaluslFäsult Speclflcatlon
Nandrolone decanoate:
ldentificationContent
HPLCHPLC
NN
comPlies'too.7 ./"
comPlies> 98.5 %
yesyes
G = GMP A = accreditated V= generally validat€d P = validat€d on producl N = not validaled
Slgnatur€s: ."^rr.rrU"r...Arf+ I h,u,t-Staff:
20.08.2015page I of '1
Theenclosed resu\s r€,er exclusrcly to the obi€.t ot examinarion descnb€o abow.Tho measunng a6u'acy ßava äbre on requ€si Only händwnrten signatures a€ vatidWithout sritl€n p€mission, t is nor allow€d to pubtish singte parts oi this repon.
Gil"s ...."""," ,",...-lr4as :'i"'illlli.'i"".:..ili.i iilJi'
7. i, ?i t...\?a atr'ttIia
Simec AG Page I of I
Report steroid analysis
HPLC| Nr.5Analysendatum: 19.08.2015 10:39:51 Druckdatum: 20.08.2015 08130:33
Vial: 9 Iniektvolumen: 20
Probenidentifikation: STDNandrolonedecanonateOperator: adminChrom.-Beding. ACN / Wasser, gradientTemperatur: 40'cS.äule Nr, 88, 250 x 4,6, C18Detektion: uV 2,+0nm
0 510 15 20 25 30 35 40 45 50
Channel A
)
I
I
.99,:'
UV ResultsI{ame Time Area Amount Area Percent
Nandrolone decanoate25,140 122545236,593 129156842
0,0000,000
0,94099,060
Totäls130382694 0,000 100.000
Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiveßeSteroideuB,0B,15U9.0B.2015 10-38-37-STD Nandrolone decanonate-Rep1.datI4ethode: c:\Ezchrom Elite\Enterprise\Projects\simec\lvlethod\steroide\Steroide A.met
Simec AG
Report steroid analysis
HPLC:Analysendatum:Vial:Probenidentifikation:Operator:Chrom.-Beding,Temperatur:SäuleDeteKion:
Page I of 1
Nr.519.08.2015 l1:33:239STD Nandrolone decanonateadminACN / Wasser, gradient40 0c
Nr, 88, 250 x 4,6, C18uV 240nm
Druckdatum:Injektvolumen:
20.08.2015 08:31:3220
I
i
- 2Aa
I
6
25
Amount Area PercentTime
Channel A
UV ResultsName
Nändrolone decanoate2s,14736,597
1231937129928198
0,0000,000
0,93999,061
131160135 0,000 100,000
Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroide\18,08,15U9.08.2015 11-32-04-SID Nandrolone decanonate-Rep2.datl4ethode: Cr\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A met
Simec AG Pase l or tReport steroid analysis
HPLC: Nr.5Analysendatum: 19,08,2015 12126t46 Druckdatum: 20.08.2015 08:31:42Vial: 9 Injekwollmen: 20Probenidentifikation: STDNandrolonedecanonateOperatori adminChrom.-Bedin9. ACN / Wasser, gradientTemperatur: 40'C&iule Nr. 88, 250 x 4,6, C18Detektion: UV 240nm
l
9
":i
UV ResultsName
-9
Ii
:*o
I
| +oo
0510r520253035404550
Channel A
Time Area Amount Area Percent
Nändrolone decanoate25.133 122239336,590 129313789
0,0000,000
0,93699,0&
130s36182 0.000 100,000
Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideu8,o8,15U9.08.2015 12-25-31 STD Nandrolone decanonate-Rep3.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A.met
Simec AG
Report steroid analysis
HPLC:Analysendatum:Vial:Probenidentifikation :
Operator:chrom.-Beding.Temperatur:SäuleDetektion:
Nr.519.08.2015 13:20:09ISTD Nandrolone decanonateadminACN / Wasser, gradient40 .cNr. 88, 250 x 4,6, C18uV 240nm
Druckdatum:Injekwolumen:
20.08.2015 08:31:5120
Page 1 of 1
i 600
iaoo
i
200
r0I
600 -
2oo -
l-9
25
Channel A
UV ResultsName Amount Area PencentTime
Nandrolone decanoate25,14336,547
1218188129000992
0,0000,000
0,93599,05s
I Otats130219180 0,000 100,000
Daten File: C:\Ezchrom Elite\Enterprise\Poects\Simec\Data\2015\August 2015\Diverse
Steroide\18,08,15U9,08.2015 13-18-55-STD Nandrolone decanonate-Rep4 datMethode: C:\EZChrom Elite\Enterprise\Proiects\Simec\Method\steroide\Steroide A.met
Simec AG
Repolt steroid analysis
HPLC:
Analysendatum:Nr.519.08.2015 14:13:32 Druckdatum:
Injektvolumen:20.08.2015 08i32:0420
Page 1 of 1
Vial: 9Probenidentifikation; sTDNandrolonedecanonate
adminACN / Wasser, gradient40 0c
Nr. 88, 250 x 4,6, C18UV 240nm
Operator:Chrom.-Beding.Temperatur:SäuleDetektion:
.
| 2aa
I
6
Time Amount Area Percent
Channel A
UV ResultsName
Nandrolone decanoate25,15736,607
D42445131235658
0,0000,000
0,93899,062
132478503 0,000 100,000
Daten File: C:\Ezchrom Elite\Enterprise\Projects\simec\Data\2015\August 2015\DiverseSteroideu8,o8,15U9.0B.2015 14-12-20 STD Nandrolone decanonate-Reps.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\steroide A,met
Simec AG
Report steroid analysis
HPLC:Analysendatum:Vial:Probenidentifikation:Operator:Chrom.-Beding,TemperaturlSäuleDetektion:
Nr.519.08.2015 15:06:569STD Nandrolone decanonateadminACN / Wasser, gradient,t0 "cNr. 88, 250 x 4,6, C18uV 240nm
Druckdatum:Injektvolumen r
20.08.2015 08:36:2220
Page I of 1
i
i
I
:oo:
:
fo
Channel A
UV ResultsName
25
Time Amount Arca Percent
Nandrolone decanoate25,16736,630
1242161130640455
0,0000,000
0,94299,058
Totals131882616 0,000 100.000
Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideU8,08,15U9,08,2015 15-05-42_STD Nandrolone decänonate-Rep6.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\l4ethod\Steroide\Steroide A.met
Simec AG
Report steroid analysis
Page 1 of I
HPLC:AnalysendatumiViäl:Probenidentifikation: Blank
Nr.519.08.2015 16:00:311
20.08.2015 08:36:3220
Druckdatum:Injektvolumen:
Operator:Chrom.-Beding,Temperatur:SäuleDetektion:
adminACN / Wasser, gradient40 "cNr. 88, 250 x 4,6, C18tJV 2.l0nm
'l
-2.
Channel A
UV ResultsI{ame
25
Time Areä Amount Area PercentNandrolone decanoate 0,000 BDL
Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\Diverse
SteroideU8,08, 15\19.08.201s 15-59-11-Blank.datMethode: C:\Ezchrom Elite\Enterprise\Projects\Simec\l\4ethod\Steroide\Steroide A.met
HPLCIAnalysendatum:Vial:Probenidentifikation: C34a12A
Simec AG
Report st€roid analysis
Operator:Chrom.-Beding.TemperaturiSäuleDetektion:
Nr.519.08.2015 16r54:0010
adminACN / Wasser, gradient40 0c
Nr. 88, 250 x 4,6, C18uV 240nm
20,08.2015 08:36r4320
Page 1 of 1
Druckdatum:Injektvolumen:
O_l
II
II
I
i
.
:0
3
6
Channel A
uV ResultsName Time Ämount Ar€a PercentNandrolone decanoate 36,630 151370427 0,000 100,000
Totals1s1370427 0.000 100.000
Daten File: C:\EZChrom Elite\Enterprise\Proiecls\Simec\Data\2015\August 2015\DiverseSteroide\18,08,15\19.08.2015 16-52-44_C34812 A-Rep1.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A.met
HPLC:
Analysendatum:Vial:Probenidentifikation: C34812A
Simec AG
Report steroid analysis
Operatorichrom.-B€ding.Temperatur:SäuleDetektion:
Nr,519,08,2015 17 i47 t2710
20.08.2015 08r36:5220
Page I of 1
Druckdatum:Injektvolumen i
adminACN / Wasser, gradient40 0c
Nr. 88, 250 x 4,6, C18UV 240nm
l
I
zoa )
I
-9
25
llme Area A.nount al€a Percent
| 300
l
| 600
It
i aoo
t
I
| 2oo
I
i
fo
o
channel A
uV ResultsNameNandrolone decanoate 36,600 1s2231615 0,000 100,000
Totals152231615 0,000 100,000
Daten File: C:\EZChrom Elite\Enterprise\Proiects\Simec\Data\2015\August 2015\Diverse
SteroideU8,08,1sU9.08.2015 17-46-12-C34812 A-Rep2.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\lvlethod\Steroide\Steroide A.met
Simec AG
Repod steroid analysis
Päge I of 1
HPLC:
Analysendatum:Vial:
Nr.519.08.2015 18:40:5610
Druckdatum:Injektvolumen:
20.08.2015 08:37:0320
Probenidentifikation: c348124Operator:chrom.-Bedin9.Temperatur:SäuleDetektion:
adminACN / Wasser, gradient40 0c
Nr. 88, 250 x 4,6, c18UV 2,t0nm
:! 600
t2aa
I
3
-sö
15 20
Channel A
UV ResultsName Area Amount Area Percent
Nändrolone decanoate 36,573 151769419 0,000 100,000
Totals151769419 0,000 100.000
Daten File: Cr\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\Djverse
Steroideu8,o8,15U9.0B.2015 18-39-40 C34812 A-Rep3.datl.lethode: Cr\EZChrom Elite\Enterprise\Projects\S'mec\Method\Steroide\Steroide A.met
Simec AG
Report steroid anälysis
HPLCI
Analysendatum:Viäl:
OperatoriChrom.-Beding.Temperatur:SäuleDetektion:
Page I of 1
Nr.519.08.2015 19r34:2211
adminACN / Wasser, gradient40 .cNr. 88, 250 x 4,6, C18UV 240nm
Druckdatum:Injektvolumen :
20,08.2015 08:37:1420
Probenidentifikation: C348128
.600
l.lame
i9
1200I
.
,o
-9I
:
Channel A
UV ResultsName Time Area Amount area PercentNandrolone decanoate 36,U3 123116414 0,000 100,000
123716418 0.000 100,000
Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideu8,08,15U9.08.201s 19-33-0s-C34812 B-Rep1.datl4ethode: C:\EZCh rom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A.met
Simec AG
Report steroid analysis
Page I of 1
HPLC:
Analysendatum:Vial:
Operator:Chrom.-B€ding.Temperatur:SäuleDetektion:
*ls.
Nr,519.08.2015 20127'.4911
Druckdatum:Injektvolumeni
20.08.2015 08:37r2620
Pmbenidentifikation: C348128adminACN / Wasser, gradient40 0c
Nr. 88, 250 x 4,6, C18UV 240nm
3
Channel A
UV ResultsName
t5 25
Time Amount Area PercentNandrolone decanoate 36,590 124222209 0,000 100,000
Totals124222209 0.000 100,000
Daten File: Cr\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideU8,0B, 15U9.08.2015 20-26-30_C34812 B-Rep2.datf4ethode: Cr\EZChrom Elite\Enterprise\Projects\Simec\l4ethod\Steroide\Steroide A,met
Simec AG Pase 1 or 1
Repolt steroid analysis
HPLC: Nr.5Analysendatum: 19.08.2015 21r21i14 Druckdatum: 20.08.2015 08:37:38Vial: 11 Injektvolumen: 20Probenidentifikation: C34a12BOperator: adminChrom.-B€ding. ACN / Wasser, gradientTemperatur: 40 oC
säiule Nr, 88, 250 x 4,6, C18Detektion: UV 2.l0nm
0-
0 510 15 20 25 30 35 1A 45 50
Channel A
UV ResultsName
r 600
i
j2aa -,
:
Time Area Amount Area PercentNandrolone decanoate 36,650 123643516 0,000 100,000
Totals1236r''3516 0,000 100,000
Daten File: Ci \Ezch rom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideu8,08,15U9.08.20l5 21-20-00_C34812 B-Rep3.datl4ethode: C:\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A.met