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Anson Environmental
SDMS Document
112048
I EninronmenUd Audits Hazardous Waste Asbestos Management GrounduxUer Remediation Storage Tank Management Impact Statements Wetlarui Investigations
256 Main Street Northport, NY 11768
516-757-7090 (fax) 516-757-1229
February 4, 1992:
Dorothy Allen, Project Manager United States Environmental Protection Agency, Region II 26 Federal Plaza New York, NY 10278
Re: Administrative Order Index No. II CERCLA-90208 Anchor Chemical Site 500 West John Street, Hicksville, NY
Dear Mrs. Allen:
Enclosed please find copies of the data sheets for the samples taken to date at the above referenced Site. The data for the original sampling of the nine drywells and catch basin and indoor borings 5 & 6 and the re-sampling of drywells 1-4 for mercury and cyanide have been validated and are presented in the validated format from Environmental Standards Inc.
The unvalidated data for the monitoring wells 1D, 4 and 6 and indoor borings 3 & 4 are enclosed from both CEIMIC (inorganics) and Intech Biolabs (organics). The unvalidated data for indoor borings 1 & 2 and the re-sampling of the remaining drywells from CEIMIC Labs is also enclosed. The organic data for the last two borings has not yet been received from Intech Biolabs but we understand it will be available shortly.
We trust this is satisfactory for your purposes, to call.
If you have any questions, please do not hesitate
Very truly yours.
Dean Anson II Co-Facility Coordinator
cc: Richard G. Leiand, Esq. Mr. Arthur D. Sanders
w/out enclosures:
--•• W Printed on
rtecycled Paper
Stanley Sucharski, BB&L Fred Werfel, Spiegel Associates James Doyle, Esq., USEPA Doug Sullivan, Alliance Technologies
300322
m
Validated Data
All Drywells (f irst sampling)
300323
lEXTIIttTttU ODSIMIC MtlYSIS - AMUTICUL liESUlTS
1 • •
lAnseo Envirtmental Saipl i Nuiber
1 llaboratory Saif i l i nuiber
| - • " " • • " " "
1 jReiarks 1 I " • lunits I 1 , - -f
JSEIIIVOIATIIE COKPOUIIDS j Quant.
1 l l i i i t (»q) 1 1
iPhenol 1 11 1 1 1 " - • - • 1 • |bis(2-ChloroeUiyl)ether | I i
|2-Chlcr»|)benol | 11
1 . . . . . -|— |l,3-I)lchlorolienzene | 11 1 . . ,, , t 1 1 |l,l-Dicblorobenzent | 11 1 . , , ., . 1 1 1 lienzyi Alcohol j 11
1 • • 1 |l,2-Dichlorobenzene | I i 1 1 1 1 iH i tdy lpheno l | I i 1 1 1 1 |bis(2-Chloroito|iro|irl)<th«r | I i 1 ) 1 . . . . . . 1 M-Aethylphenol | I t 1 , , . . , 1 1 1 iM l t roso - i f i -n -Propy ls i i n j | I t 1 1 1 • • • 1 iHexachlorcethane | I t
1 1 • •" imt rob inz in i | I t
jlsophorone | I t
r ' 1' |2-«itrophenol j I t 1 , ., , 1 1 1 |2,4-01ieClirlplienol j - I i 1 1 1 1 iBenzoic Acid | Si 1 . . 1 1 — . . 1 — |bi$(2-Cliloroethoxy)ntbane | 11 1 1 1 - " - ~ | -|2,A-01chlorophenol | I t
<JJ)* 11,2,4-Trichlorobenzene | I t ^ 1 1 J ^ . y._ Itaphthalioe j I t
^ O H-Chloroaniline j I t « l i 1 1
iHtxachlorobutadiene It
|4-thli)rs-3-llethylplienol | I t
Quant, l l i i t (Sol)
33i
33t
33i
33t
33i
331
33t
33i
331
33t
331
331
33i
33i
33i
33t
KSt
33i
33t
33t
331
33t
33i
33t
...
- A l l SOIIDS AEPORTED Oil A DRT HEIGHT BASIS ^ ^ ' - ' I i i i I i t
I I I I ^ 1 I I 1 1 I ' I 1 1 P m z 1 outs 1 DUt4 1 Trip Blank | OUtl | M i \ OUfS j OUiT | 0UI8 | 0UI9 | ORAII | 16-1 |Trip Blank j mutS/MSO |
I I 1 Bit 1 i 1 1 1 I I I 1 811 j j 8t9S-i l 1 8I9S-I2 I 8i9S-i3 j 8t9S-l< | 81t3- l l j 81i3-t2 J81i3-I3 | 8113-iA j 81i3-iS j 81i3-t t JBliS-iT | 8 i t 3 - l t j 81 t3 - l l j 81t3-t8 j
Analyzed | Analyzed j Analyzed j j Analyzed j Analyzed j | | Analyzed | | | j JDupllcate of j
Twice 1 Twice j Twice j | Twice j Twice | j ~ j Twice j | j j | OUtl |
U9/Kg 1 u j / rg | u j / t g j ug/l | u j / l g j ug/lg j uj/ l lg j ug/Kg j ug/tg j ug/Kg | ug/rg j ug/l | ug/ l | ug/Kg |
1 1 i 1 1 1 1 1 1 1 1 1 1 Analyzed j
1 j 1 1 j 1 1 j 1 1 1 1 1 Twice 1
1 1 1 KA 1 1 I I 1 I I I 1 tt 1 1
1 1 1 «• 1 1 I I 1 I I I i K* 1 1
1 1 1 M 1 1 I I 1 I I I 1 M 1 1
1 1 1 ** 1 1 I I 1 i l l 1 1* i 1
i i i Kl i i i i i i i i i >* i i
1 1 1 K* 1 1 I I 1 I I I 1 KA 1 1
i i i <• i i i i i i i i i 1* i i
i i 1 ** i i i i i i i i i "* i 1
1 1 1 DA 1 I I I 1 I I I 1 *• 1 1
1 1 1 1* 1 1 I I 1 I I I 1 Kt 1 1
i 1 1 M 1 lU/DJ 1 I I 1 I I I 1 M 1 lU/UJ 1
1 1 1 AA 1 1 I I 1 1 1 1 1 "* 1 1
1 1 1 KA 1 1 I I 1 I I I 1 KA 1 1
1 1 1 AA 1 1 I I 1 1 1 1 1 KA 1 1
1 1 1 KA 1 1 I I 1 I I I 1 KA 1 1
1 1 1 1* 1 1 I I 1 I I I 1 KA 1 1
1 . 1 1 DO 1 1 " Wi J 1 1 1 I I I 1 KA 1 1
1 1 1 KA 1 1 I I 1 I I I 1 KA 1 1
1 1 1 KA 1 1 I I 1 I I I i KA 1 1
1 1 1 KA 1 UJ/U3 1 I I 1 I I I 1 K« 1 II3/U] 1
9Bti/95ii 1 i I KA i 1 1 i i i i i i KA 1 |
1 1 1 KA 1 1 I I 1 1 1 1 1 KA 1 1
1 KA 1 1 KA 1
1 1 1 ll« 1 1 I I 1 I I I 1 KA 1 1
<«a*/^A«i 1 1 1 NK 1 t I I 1 I I I 1 NA 1 t
CO o o
E X T ^ ^ P o R G A A l t AKAlTiilS - 'AJiALmlAI. KtSlilTS
lAnson Environiental Saiple Kuiber
1 llaboratory Saiple Kuiber
1 iBeiarks
1 Units | . . . 1
ISEKIVOIATIIE COKPOUKOS
1 1
1Hexachlorocyclopentadisne 1
|2,l,e-Tricliloropbei)ol
|2,<l,S-Trichlorophenol 1 1 |2-Chioronaphthalene
1 |2-Kitroaniline i lOiiethylphthalate
lAcenaphttiylene
is-Kitroanil ine 1 1 lAcenaphthene 1 1 |2,4-0initrophenol
I " |4-Kitrophenol 1 1 lOlbenzofuran I 1 |2,4-Oinitrctoluene
|2,6-Dinitrotoluene
1 lOiethylplithalate 1 1 14-Chlorophenylphenylether I " •
iFluorene
1 • • •
|4-Kitroanll lne
1 • — •
|4,6-0initro-2-Ketbyiphenoi
1 -K-Kitrosodiphenylaiine
|4-Broiophenylphenylether
iHexachlorobenzene 1 . . -1 iPentachlorophenoi
1 iPhenanthrene 1
Quant, l i i i t (Aq)
It '
It
Si
It
St
It
It
St
It
Si
Si
It
It
It
It
It
It
Si
St
It
It
It
Si
It
Ouant. l i i i t (Sol)
33i
33i
ISSi
33t
ust
33i
33t
i t s t
33i
isst
16Si
33t
33i
33i
33t
33i
33i
les i
16St
33t
33i
33i
les i
33t
' A l l Su'lIOS
0UI2
8t95-t l
Analyzed Twice
^ l ^
t l -
371 J/32t J
EPOBTED O'K A OBT'UElbHl'BASIS '
0UI3 i 0Ut4 i Trip Blank
i i 811 Bt9S-t2 1 8t9S-t3 | 889S-t4
Analyzed | Analyzed | Twice j Twice |
ug/Kg i ug/Hg i ug/l
1 1
1 1 1 1
1 1 K*
1 1 K*
i i KA
1 i **
« / - 1 1 K»
i i H*
1 1 **
1 1 <*
1 i KA
1 1 "*
i i K*
1 1 "*
i 1 >*
1 1 " 1
1 j * 1
1 1 **
i i **
i i ** 1 1 "*
1 KA
i i 1*
1 1 ** 1 1 i i KA
i 2St J/31t } i KA
-#-DUil 1 OUIS
81i3-t l 1 8183-12
Analyzed | Analyzed Twice I Twice
ug/tg i ug/Kg
1
1
DUt( 1 out?
8183-13 1 8183-84
ug/Kg I ug/Kg
1 i B
1
- i ;—
outs
81B3-tS
Analyzed Twice
ug/Kg
B/-
18it } / l S i i J
—1 i 1 ,J \ 1 k-- m
I I I I " ' " ' ' T 0Ut9 i OBAIK i B8-1 i l r i p Blank i DUIIKS/KSO i
i i j 811 1 I 81t3-t6 |81t3-t7 1 8183-18 | 8183-11 | 8183-88 |
I 1 I joupiicate of|
I I 1 1 OUtl 1
ug/Kg 1 ug/Kg j ug/l ' | ug/l j ug/Kg j
I I 1 1 Analyzed | i l l 1 Twice i
i i i K* i ' 1
1 i i ** i 1
I I 1 "* 1 1
i 1 i KA i 1
B 1 B 1 1 KA 1 - / B 1
i i i KA i i
I I 1 >• 1 1
i i i >* i 1
I . I 1 «* 1 1
i i 1 "* i i i i 1 <* i 1
1 1 1 ** 1 1
I I 1 "* 1 1
i i 1 KA i i
i i i *' 1 i I I 1 ** 1 1
i 1 i <* i i i i 1 KA i {
I I 1 "* 1 1 KA
i 1 i <* i i i i 1 K* i i
i i i «* 1 1
i » J 1 19t J i i KA i 71 J/8t ] I
#
CO o o CO
I C A I I ^ ^ ^ I I I I I O J A K A I Y S L - IHAIVTU'
lAnson Environiental Saiple Kuiber
llaboratory Saiple Kuiber
iBeiarks
iunits
isEHIVOlATIlE COKPOUKOS i Quant, i
1 Illiit (Aq)|
lAnthracene | It |
lOi-n-Butylphthalate | It |
JFluoranthene | It |
iPyrene | It |
iButyibenzylphthalate i It i
|3,3'-Dichlorobenzidlne | 2i |
|8enzo(a)anthracene | 18 |
|bis(2-Ethylhexyl)plithalate | It i
IChrysene | It |
ioi-n-Octylphthalate i It i
|8enzo(b)fluoranttiene | 18 |
|Benzo(k)fluoranthene j IB j
|Benzo(a)pyrene | 18 |
|Indeno(t,2,3-cd)pyrene | 18 |
|Oibenz(a,h)anthracene | 18 |
|Benzo(g,h,l)perylene | It |
iouantitation liiit Kultipiier
|Oate of Saiple Collection
|Oate Saiple Beceived by,laboratory
|Oate Saiple Extracted '
|Oate of Saiple Analysis
Instruient Used for Analysis
L IM.»LTS - KLL DUl'IOS
1 DUt2
i 8t9S-ii
i Analyzed
i Twice
1 nlH
Quant. 1
iiit (Sol) 1
33t |24ii 3/2Sti J
33t i 3ti 3/-
33t i 51ti/S2ti
331 |2S,lti/27,itt
33t 1 U3/UJ
33t 1 UJ/U3
33t 1 UJ/U3
33t 1 U3/UJ
33t 1 U3/UJ
33t 1 UJ/U3
33t 1 UJ/UJ
1 8.48
1 8/18/91
1 8/11/91
1 8/14/91
1 8/28 i B/29
KS-5995B
EI UKitu u'il A
DUi3
8895-82
Analyzed Twice
ug/Kg
1188 J/llii 0
26,iti/
21,ttt
UJ/UJ
U3/U3
UJ/UJ
U3/U3
UJ/UJ
UJ/UJ
UJ/UJ
9.i9
8/11/91
8/11/91
8/14/91
8/28 I 8/29
KS-S99SB
Bt'Hcmni'eAS S '' '
0UI4
889S-i3
Analyzed
Twice
ug/Kg
7ti J/81t J
79i J/86i J
-/49t J
7911 U/
9lii U
52i J/S9t J
UJ/UJ
Iiii J/ltti J
set J/Sit J
SBt J/59t J
UJ/UJ
UJ/UJ
UJ/UJ
S.97
8/18/91
8/11/91
8/14/91
8/38 ( 8/31
KS-S995B
Trip Blank
BIB
8i9S-t4
ug/l
KA
KA
KA
KA
KA
KA
KA
KA
NA
NA
KA
KA
KA
KA
KA
KA
KA
KA
KA
KA
KA
KA
OUtl
8183-81
Analyzed
Twice
ug/Kg
9788 U/
11,tit U
UJ/UJ
UJ/UJ
UJ/UJ
UJ/UJ
UJ/UJ
UJ/UJ
UJ/UJ
t.67
8/11/91
8/12/91
8/14/91
8/38 ( 8/31
KS-5995B
U outs
8183-82
Analyzed
Twice
ug/Kg
63 J/72 J
-/34J
64 J/48 J
UJ/-
UJ/-
ISit U/
IttlU
UJ/-
UJ/UJ
UJ/UJ
UJ/UJ
UJ/UJ
B/UJ
R/UJ
R/UJ
l.t3
8/11/91
8/12/91
8/14/91
8/24 S 8/38
KS-599SB
0UI6
Bll3-t3
ug/Kg
.
Slit
26,iti
9.t9
B/11/91
B/12/91
B/14/91
8/27/91
KS-S99SB
;
0Ut7
8183-84
ug/Kg
5988 U
S.4S
8/11/91
8/12/91
B/14/91
8/27/91
BS-S995B
',"; i
0UI8
8183-85
Analyzed Twice
ug/Kg
398 3 1 -
37ti/34lt
37ti/45it
16tt 3 1 -
9Sti U/
12,ttt U
19tl J/2tti J
UJ/UJ
29ti J/27it J
17ti J/17lt J
14ti J/llit J
UJ/lSti J
UJ/UJ
UJ/UJ
9.t9
8/11/91
B/12/91
B/14/91
8/27 S B/29
KS-S99SB
;,
0Ut9
8183-86
ug/Kg
448 J
348 J
371 J
StitU
2St J
6.97
8/11/91
8/12/91
8/14/91
8/27/91
KS-S99S8
1 ii
OBAIK
8183-87
ug/Kg
488 J
418 J
328 J
3tlJ
27ttU
23t J
5.76
8/11/91
8/12/91
8/14/91
8/28/91
KS-S995B
> .1
B8-1
8163-18
ug/l
B
«
B
1.88
8/11/91
8/12/91
8/16/91
B/23/91
KS-599SB
i • i
Trip Blank
811
8183-11
ug/l
KA
NA
NA
NA
NA
NA
NA
NA
NA
KA
HA
KA
NA
NA
NA
NA
NA
KA
HA
NA
NA
NA
'-page J -J
DUIINS/NSO 1
8183-88 i
Duplicate | of OUtl 1
ug/Kg 1
Analyzed |
Twice 1
-/"J 1
118 J/148 J 1
188 J/248 J 1
188 J/178 J 1
w/- 1
UJ/- 1
6388 U/ 1
S988 U i
128 J/116 J 1
168 J/UJ i
118 J/128 J 1
72J/7tJ 1
UJ/UJ i
R/UJ 1
R/UJ 1
R/UJ i
l.t3 1
8/11/91 i
8/12/91 1
8/14/91 1
8/23 S 8/28 1
KS-599SB 1
m
-A
CO o o CO
l u r j ^ B i v c u i l0ENTIFy!Lu .un/ilUKOS ''- ^JlHATEO lunicniXATIOHS- - nif SOlIDS'Mir^ii.lO ON A U I ».<oHT B A S ^ ^ ^ ' i ^ i ^ f i 1 1 1 1 , ; . , j 6 |
lAnsoj) lAyJronwfltai Saiple Kuiber | 0Ut2 | 0U13 | 0UI4 | Trip Blank | OUtl | OUIS J 0Ut6 | DUI7 | GUIS | 0U>9 J DRAIN ) RB-1 jTrip Blank | DUil | 1 1 1 1 1 811 1 1 1 1 1 1 1 1 1 811 1 1 llaboratory Saiple Kuiber | 8 t95- t l j 8895-82 | 8695-83 | 8695-84 | 8183-61 | 8163-62 | 8163-63 |8163-84 | 8183-85 | 8163-66 | 8183-87 j8183-16 | 8183-11 | 8163-68 |
iBeiarks i i i i i i 1 i i i i 1 i i 1
1 lUnits i ug/Kg | ug/Kg | ug/Kg j ug/l j ug/Kg | ug/Kg | ug/Kg | ug/Kg | ug/Kg i ug/Kg j ug/Kg i ug/l i ug/l | ug/Kg {
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
IVOIATIIE COKPOKEKTS | | | 1 - 1 " 1 I ' l l 1 1 | - | - | KA | 1 1 , , , 1 . — , . . 1 1 I I I 1 1 j — " • - - I - - - - 1 |— 1 1 • 1 1 1 1 " 1 1 1 j - 1 1 iHexane | 18,668 J | | | | I I I I I 1 1 1 I 1
lUnknoun Hydrocarbons (Kuiber of Peaks) 1 55,666(5) J |71,S66(18) J 1 I I 1 1 I I I I I I 1 I
IC9K12 Alkylbenzene |446.868(4) J | 6668 J | | | 1 - 1 I I | I I I 1 1 • • •• ' I ' I 1 "" 1 " 1
llaboratory Art i fac ts | | | 16 R | | 1 S R | | 8 R | 18 B | 18 R | 23 R | | | |
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 i 1 1 1 . j . . 1 1 |. 1 1 .. .1.. 1 I I ISEKIVOIATIIE COKPOKEKTS | | | | KA | | | | | | | | - | KA | |
. . |, , ,, , , -ISaturated Hydrocarbon (Kuiber of Peaks)i246,668(13)J/ |96,866(lS)J/ i 4868(3) J / i il2,978(7) J / | | 1568(1) J |916(1) ji67,866(4) J / | 1261(1) J | | | |7226(13)J/ | 1 1351,566(13) J|77,986(15) J j 3446(3) J j |14.266(5) J j | j 161,366(3) J | | j j j l 6 ,286 ( lS ) j j
IC9H12 Alkylbenzenes |29,586(S) 31 |15,666(2j J / | | | I I I I 1 1 1 1 1 1 1 1 92,686(4) J 1 6366 J j j | I I I I i 1 i i i i
- 1 .... , 1 lUnknowns (Kuiber of Peaks) |166,368(4) J/ |12,666(2) J / | 4146(3) J / | | 7378(3) J / |4256(13) J/ |24,S86(3) J | |16,886(8) J / | 9566(5) J |6736(4) J | | |6968(8) J / | i il51,666(5) J i 15,666(4) J j 3428(2) J j | 9266(3) J |3538(13) J | | ilt ,B68(6) J | i i i i 3386(4) J i
lOecahydronaphthalene Isoier | 2886 J / | 4568 J / | 1 1 1 1 1 1 1 1 1 1 1
i i 1 1*1 ^ 1 i i 1 1 1 i 1 i i i i i i
lAlkyl-substituted Cyclobexane | 3186 J / | 13,586 3 / | | | 3366 J / - | | | | | 1 1 1 1 1 i i 13,861 J i 11,186 J i 1 i i i i 1 i i i i i 1
. . - 1 - - - • • 1 1 1 1 1 inexadecanolc Acid | -/179,668 J i i i i i i i i 1 1 i i i 1
lAlkyl-substituted Phenol | | 3686 J / | | | I I I I 1 1 1 1 1 1
lOxygenated PAH | |2766 J/3666 J | | 1 1 1 1 1 1 1 1 1 1 1
IC18H22 Alkylbenzene | | -/2168 J | 1666 J / | | | | j | | I I I 1 I
1 1 1 1 » » J 1 1 I I I I 1 1 1 1 1 1
| l-Phenyl-l,2-propanedione i i i i 1 U » i |Z^^ i \ \ 11S86 J/1566 i 936 J | | | | |
y.- >i
CO o o CO
00
1 tt ' ^ EXTRH^ORGAHIC AKAKSIS
f ^ i
- ANAimCAl BESUITS
lAnson Environiental Saiple Kuiber
1 llaboratory Saiple Nuiber 1 ,.. , 1 IReiarks 1 " lUnits 1 • • • •
IPESTICIOES
1 1 lalpha-BHC 1 Ibsta-BHC j
Idelta-BHC
1 |gaaa-BHC (lindane) 1 • " " • • • "
iHeptachlor
lAldrin
1 •" • ••
IHeptachlor Epoxide
JEndosulfan I 1
iBleldrin
1 |4,4'-D0E 1 •• ' • • "
lEndrin
1 lEndosulfan II 1 •
|t,t'-DB0
i • • • • • • • • • •
lEndosulfan Sulfate 1 |4,4'-DDT 1 1 •• •
iNethoxychlor f
1 lEndrln Ketone 1 1 lalpha-Chlordane 1 1 ••
IgaMa-Chlordane
1 • iToxaphene
Quant, liiit (Aq)
6.6S
6.85
8.65
t.ts
t.ts
t.ts
i.ts
t.ts
t.lt
t.lt
t.lt
t.ll
t.lt
l.lt
t.lt
I.St
l.lt
I.St
I.St
l.t
Quant, liiit (Sol)
8
8
B
8
8
8
8
8
16
16
16
16
16
16
16
86
16
88
88
168
j /
- All SOIIOS
DUI2
8695-61
ug/Kg
183
166 J
146 J
36
22 J
;. i EPOBTED ON A
DUI3
8695-82
ug/Kg
UJ
R
UJ
UJ
UJ
87 J
41 J
R
R
R
UJ
39 J
R
UJ
UJ
i • • ,
IBf UEIGHT SAS
0Ut4
8695-13
ug/Kg
UJ
B
UJ
UJ
UJ
16 J
St J
R
R
R
UJ
126 J
R
UJ
UJ
S
Trip Blank 811
8695-84
ug/l
NA
HA
KA
KA
NA
HA
KA
KA
KA
KA
NA
HA
HA
HA
KA
HA
HA
KA
KA
KA
A w DUil
8113-11
ug/Kg
KA
HA
HA
KA
KA
KA
KA
HA
HA
NA
NA
NA
NA
NA
HA
HA
KA
KA
KA
KA
QMS
8183-12
ug/Kg
UJ
R
UJ
UJ
UJ
UJ
UJ
« R
«
UJ
UJ
R
UJ
UJ
S
0UI6
8163-83
ug/Kg
UJ
R
UJ
UJ
UJ
18 J
75 J
R
R
R
UJ
24 J
R
UJ
UJ
{
0UI7
8163-11
ug/Kg
UJ
R
UJ
UJ
UJ
19 J
11 J
R
R
R
UJ
7.S J
R
UJ
3.4 J
DUIB
81t3-tS
ug/Kg
UJ
«
UJ
UJ
UJ
42 J
48 J
12 J
R
R
R
UJ
52 J
R
UJ
29 J
DUI9
8183-86
ug/Kg
8.2 J
«
UJ
UJ
UJ
UJ
UJ
B
B
B
UJ
14 J
B
UJ
UJ
DRAIK
8183-67
ug/Kg
UJ
B
UJ
UJ
UJ
UJ
UJ
R
R
R
UJ
OJ
R
UJ
OJ
j.
RB-1
8183-16
ug/l
Trip Blank 811
8163-11
ug/l
KA
KA
HA
HA
KA
KA
NA
NA
HA
KA
HA
KA
KA
KA
HA
KA
KA
KA
HA
KA
• X
-page l \ - 1
OUtl 1
8113-18 1
ug/Kg i
1
1 1
1 S.U 1
1
7.7 J 1
6.2 J 1
- •
l E I I ^ ^ P OKEimiC AKAIV^IS - 'AHAIVTIIAI RE^UITS
lAnson Environiental Saiple Kuiber
llaboratory Saiple Huiber
jReiarks
iUnits
ipCBs i Quant. 1 lliiit (Aq)
iAroclor-1616 i 8.5
|Aroclor-l221 i I.S
|Aroclor-1232 i 6.5
iAroclor-1242 | 8.5
|Aroclor-124B i 6.5
|Aroclor-12S4 | 1.6
|Aroclor-1268 | 1.8
iQuantltation liiit Kultipiier
Quant, liiit (Sol)
88
88
88
86
86
166
168
1 • •'
lOate of Snpie Collection
joate Saiple Received by laboratory
ioate Saiple Extracted
ioate of Saiple Analysis
All SOIIOS BEPORTED OK A DRV UEIGHT BASIS
DUI2 1 0UI3 1 DUI4 | Trip Blank i i i 818
8895-61 i 8695-62 | 8895-63 i 8895-64
ug/Kg i ug/Kg i ug/Kg i ug/l
i i i KA
i i i HA
i i i KA
1 1 1 KA
i i i ** i 1 i KA
i i i KA
1.69 i 1.75 i 1.58 1 KA
8/16/91 i 8/18/91 i 8/11/91 i KA
8/11/91 1 8/11/91 1 B/11/91 1 8/11/91
8/14/91 1 8/14/91 1 8/14/91 | 8/14/91
B/27/91 1 8/28/91 | 8/28/91 | 8/28/91
1 1 1
DUil
8183-81
ug/Kg
KA
HA
KA
KA
HA
HA
KA
HA
KA
8/11/91
8/14/91
8/28/91
'
DUI5
8163-62
ug/Kg
6.43
8/11/91
8/11/91
8/14/91
8/28/91
DUIB
8113-13
ug/Kg
1.75
8/11/91
8/12/91
8/14/91
B/28/91
DUI7
8183-64
ug/Kg
6.49
8/11/91
8/12/91
8/14/91
B/28/91
; 1
DUIB
8163-65
ug/Kg
6.74
8/11/91
8/12/91
8/14/91
8/2B/91
"i
DUI9
8163-16
ug/Kg
6.59
8/11/91
8/12/91
8/14/91
8/28/91
:j
ORAIH
8183-87
ug/Kg
6.48
8/11/91
B/12/91
8/14/91
8/28/91
i —
RB-1
8163-16
ug/l
1.66
8/11/91
8/12/91
8/14/91
8/27/91
!*. i '
Trip Blank 811
8163-11
ug/l
KA
KA
KA
HA
KA
HA
KA
KA
KA
HA
HA
KA
-page 8 ^
DUIIKS/KSD 1
8183-88 i
ug/Kg 1
8.54 1
8/11/91 i
B/12/91 1
8/14/91 1
B/27/91 i
BOTES: Coipound was not detected.
U This coipound should be considered 'not-detected' since it was detected in a blank at a siiiiar level.
R Unreliable result - Coipound lay or lay not be present in this saiple. J Quantitation is approxiiate due to liiitations identified during the
quality assurance review (data validation). UJ This coipound was not detected, but the quantitation liiit is probably
higher due to a low bias identified during the quality assurance review.
CO
o CO
r-(•..
CO o o CO CO
o
^ B l E OBBAHIC AHAITSIS - AHAlVTICAl RESUITS'- All SOIIOS'REPOBTEO OK A ORTUEiGHT BASIS ^ ^ ^ B ' " ' ' ' ' . ' ' 1 ' ' ' i ' i'* " ' ^ ^ • " Q " '
(Anson Environiental Saipie Kuiier t m t ! S ' - ! r l m i 3«'-J?'(flfW SUaklmS 35'-37'(5M« 3»'-3J'|7ri(> Slink iFlel i SJ4/?k|JM; W - i l ' l m J «'-47'(ffW7 55'-}7'|lWfH «'-47'ff i(Ji( SJM)Tfl? l l isk |Trip BJM | i i i i 921 1 1 i 822 i 822 i | i i ^ | 823 | 8231 i 8232 i llaboratory Saiple Huiber i 8288-81 i 8266-82 i 8268-63 i 8215-81 i 8215-62 i 8215-83 | 8215-84 i 8224-61 i 8224-t2 i 8224-13 i 8224-84 i 8224-85 i 8224-86 j 8224-17 i
IReiarks l i i i l i l l l i Analyzed |Duplicate of | | | | 1 1 i i i 1 i i i i i Twice J0UI7 4 5 ' T 4 7 ' i j i i
iunits i ug/Kg | ug/Kg j ug/l i ug/Kg | ug/Kg i ug/l i ug/l i ug/Kg i ug/Kg i ug/Kg i ug/Kg { ug/l i ug/l j ug/l | 1 1 . 1 1 1 , . . j . ,,., , 1, ,, . .. „. , .. _. ••
ivOlATIlE CONPOUNOS ^Quantitation iouantitationi { i i i 1 1 i 1 1 i i i i i i i l l i i t (Aq) i l i i i t (Sol) i i i i i 1 1 1 1 1 1 1 i 1 i
jchloroiethane i 16 i 18 i i i i j i i i i i i i i i i
jtroioiethane | 11 | 11 | | | | 1 1 1 1 | j I I 1 1 1
ivinyl Chloride i I t i I t i | | i i 1 i | i i i i i i i
iChloroethane | I t | I t | | | | 1 1 1 | | | -/UJ | | | | |
iKethylene Chloride | 5 | 5 i IStt U i 12tt U i 4 J | I t t t U i 5 U i 4 J i 4 J i 5 U i S U i 6 U/7 U i 5 U i 4 J | 4 J i 5 J i
{Acetone i 16 i 18 i S488 R i 4866 R i 46 J i 4268 8 i 22 R j i SB J i 5 B i 5 B \ i R/11 R { 3 R { 22 J i i i
I'Carbon Disulfide | 5 | 5 | i | j 1 i i i i i i i i i i
il,l-Dichioroetliene i 5 | 5 i i i | i i 1 i i i i i i i i
1 1 1 1 - - 1 1 1 1 1 1 1 1 1 1 |l,l-OichloroeUiane | 5 | 5 | | | | 1 1 1 1 1 1 1 t i l l
iTotal 1,2-Dichloroethene j 5 i 5 j i i i i i i i i i i i i i i
ichlorofon | 5 | S | 1 | 1 1 1 1 1 1 1 1 | | | 1
il,2-0ichloroethane i 5 | 5 i i i i i i i i i i i i i i i
|2-Butanone | 16 i 18 i i | i i i i 1 i i i i i 1 i
|l,l,l-Trichloroethane | S j 5 j i i i i t 1 i i j i 1 j I i
ICarbon Tetrachloride | 5 | S | | | | 1 1 1 | | | | | | | |
ivinyl Acetate i 16 i 16 i i i | i i i i i i i i i i i
ieroiodichloroiethane { 5 i 5 i i i i i i i i i i i i i i i
il,l,2,2-Tetrachloroethane i S i 5 j i | i i i l l i i i i i i i
il,2-Dichloropropane i 5 i S | | i | | I I I 1 i 1 1 1 1 i 1 1 .[._ _] 1 1 I — 1 -- - 1 ,._| 1 .,, I i l l !
|trans-i,3-Dlchloropropene | 5 | 5 | | | | | 1 1 1 1 1 1 1 i l l
iTrichloroeChene | 5 | 5 | I I 1 1 1 1 1 1 1 1 1 j | 1
iDlbroiochloroMthane | 5 | 5 | | | | | | | | | | | | j | |
1,1,2-Trichloroethane | 5 | 5 | | | | 1 1 1 1 I i i i i i
iBenzene | 5 | 5 | | | UJ | | | | | j j i i i i i
. i » ^ ^ i < . « » i . iKAirsis' ' .iimcAi! »u. ..'o - A U » L . J S R E P O L L U UK'A DRT
iAnsoi^nTironiental Saiple Kuiber jouil 25'-27'iouil 36'-32'
1 1 1 llaboratory Saiple Huiber | 8288-61 | 8268-82
IBeiarks | |
1 1 1 1 . ,. , _ . 1 •- 1 1 1 1 -lunits 1 ug/Kg | ug/Kg
1 _ 1 .1 IVOIATIIE COKPOUKOS iouantitatlon iouantitationl i i j liiit (Aq) illiit (Sol) i i
|cis-l,3-Dichloropropene | 5 | 5 | | 1 1 1..,. ,1 1 ••• 1 1 1 1
iSroiofori | 5 | S | |
|2-Hexanone | 18 | 18 | | 1 1 . .,
i4-Kethyl-2-Pentanone | 18 i 18 i i
JTetrachloroetbene | 5 | 5 | |
iloluene j 5 i 5 | |
iChlorobenzene | 5 | 5 | |
JEthylbenzene | 5 | 5 | |
IStyrene | 5 | 5 | |
jTotal Xylenes | S | 5 | |
1 1 1 IQuantltation lUit Kultipiier | 136 | 138
iDate of Saiple Collection | B/21/91 | 8/21/91 1 _. . I " • • 1 1 IDate Saiple Received by laboratory | 8/22/91 | 8/22/91
1 . - -
IDate of Saiple Analysis | B/36/91 | 8/36/91
llnstruient Used for Analysis | KS-5995 C | HS-5995 C 1 1 1
iii«n, iJSIS ' •
Field Blank|DUI6 3S'-37' 821 1
8268-83 i 8215-61
ug/l 1 ug/Kg
UJ 1
UJ i
UJ 1
UJ 1
UJ 1
1.6 i 136
8/21/91 1 8/22/91
8/22/91 1 8/23/91
8/29/91 1 8/36/91
HS-599S 0 1 HS-5995 C
" % DUIB 3l'-32'
8215-62
ug/Kg
1.1
8/22/91
8/23/91
8/29/91
KS-539S A
\ Trip Blank
822 8215-63
ug/l
1.1
8/22/91
8/23/31
8/29/91
HS-5995 0
r 1 Field Blank
822 8215-14
ug/l
l.t
8/22/91
8/23/91
8/29/91
HS-S995 0
1 ;
DUI7 4l'-42'
8224-61
ug/Kg
1.8
8/23/91
8/24/91
8/29/91
HS-5995 A
••
DUI7 45'-47'
8224-82
ug/Kg
1.8
8/23/91
8/24/91
8/29/91
KS-599S A
; I —
DUI7 55'-57'
8224-63
Analyzed Twice
ug/Kg
1.2
8/23/91
8/24/91
8/29 ( 8/38
NS-S995 A
-| j —
0UI7A 45'-47'
8224-64
Duplicate of DIII7 45'-47'
ug/Kg
l.t
B/23/91
B/24/91
8/29/91
NS-5995 A
- t • i-
Field Blank 823
8224-65
ug/l
—
1.8
8/23/91
8/24/91
8/29/91
KS-5995 0
i;
Trip Blank 8231
8224-86
ug/l
1.6
8/23/91
8/24/91
8/29/91
HS-5995 0
# , Trip Blank |
8232 i 8224-67 j
ug/l 1
1.1 i
8/23/91 1
8/24/91 1
B/23/91 i
HS-5995 0 i
BOTES:
CO
- Coipound was not detected. U This coipound should be considered 'not-detected' since it was detected
in a blank at a siiilar level. R Unreliable result - Coipound lay or lay not be present in this saiple. J Quantitation is approxiiate due to liiitations identified during the
quality assurance review (data validation). UJ This coipound was not detected, but the quantitation liiit is probably
higher due to a low bias identified during the quality assurance review.
CO
CO
CO CO
^ ^ i — { i ^ ^ ' ' t ? i " •; • 1 1 - 1 ) j - ~ V i ^ ^ EXTR^^p iRGAKIC AKAlfSIS - AKAlYTICAl BESUITS - , A l l SOIIOS R PORTED OK A DRT UEIGHT BASIS ^ ^ | , ' . . ^ ^ B
iAnsonTiwiromental Saiple Huiber i ou i l 25'-27' iDUIl 3 t ' -32 ' iF ie ld BiankioUIB 3S'-37'ioUt6 3 6 ' i r i T r i p Blank iF ie ld BiankjoUIT 48'-42'iDUI7 45'-47'iDUI7 5S'-57'iDUI7A 45 ' -47 ' iF ie ld B lank i l r ip Blank i l r l p l u n k i 1 1 1 1 821 1 1 1 822 1 822 1 | | | T 823 | 8231 | 8232 | i laboratory Saiple Kuiber i 8266-61 | 8266-62 j 8268-63 | 8215-61 i 8215-62 i 8215-63 i 6215-64 i 8224-61 i 8224-82 i 8224-63 i 8224-64 i 8224-65 i 8224-66 i 8224-67 |
IBeiarks 1 1 1 1 1 1 1 1 1 1 1 i i i i
iuni ts 1 ug/Kg | ug/Kg i ug/ l i ug/Kg i ug/Kg i ug/ l { ug/ l i ug/Kg i ug/Kg { ug/Kg i ug/Kg i ug/ l i ug/ l | ug/ l i
ISEKIVOIATIIE COKPOUKOS IQuantltation |Quant i tat ion| I I I I I I I I I |Dupllcate of | | | | i i l i i i t (Aq) l l i i i t (Sol) i i i i i i i i 1 i iDUI7 45'-47' I | i |
IPhenol 1 11 1 331 1 | | | | 1 K« 1 I | | | | | KA | NA |
ibls(2-Chloroethyl)ether | I t i 331 i i i i i i "« i 1 i i i i i NA | HA i
i2-Chlorophenol i I t i 331 | | i i i i NA | i i { | \ i NA i HA i
ii,3-Dichlorobenzene i 11 { 331 i | i i i j KA i i { | 1 i i KA i KA i
|l,4-Dlchlorobenzene | I t | 331 | | | | | 1 KA | | | i | { i KA | KA |
ioenzyl Alcohol i 16 i 336 i i { i i i HA | j | | i i i KA j HA i
il,2-Dichlorobenzene i 16 J 336 i i i i i i NA | i i i { { i HA i HA i
i2-Kethylphenol i 16 i 338 i | i i i i KA i i i i | | | HA | KA i
|bis(2-Chloroisopropyl)ether i 18 | 336 { i i | i i KA i i | { i i i KA | HA |
|4-Hethylphenol | 18 | 336 | | | | | 1 K« 1 1 | | | | | KA | KA |
iH-Hitroso-di-n-Propylai ins i I t i 331 i i i i i | KA i i i i { { i HA i KA i
iHexachioroothane | I t i 331 i i i 1 i i n * ! i i 1 1 i KA i HA |
iKitrobenzene | I t | 331 | | | | | 1 *• 1 1 1 1 | | KA | HA |
ilsophorona i I t i 331 i i i i i i KA i i i i j i HA i KA |
i2-Kitrophenol i I t i 33t i j i i i i KA i \ \ \ j | M j | t i
|2,4-0i iethylphenol | I t | 33t | | | | | 1 KA | | | | | | KA | KA |
IBenzoic Acid | 56 i 1658 i j i i i i HA i | j { | i HA i KA i
|bis(2-Chloroethoxy)iethane | 18 | 336 | | | | i i «* 1 1 i 1 1 | HA | KA |
|2,4-Dichlorophenol | 18 | 336 | | | | | 1 KA | | | | | | KA | KA |
i l,2,4-Trichlorobenzene i 18 i 336 i i i i | | KA i i i | i i HA i KA i
iKaphthalene | 16 i 336 | | i i | i KA | | j | | HA | KA |
|4-Chloroanil ine | 16 | 336 | | | | | 1 KA | | | | j | HA | KA j
inexachlorobutadiene i 16 i 336 i i i i | | HA i | i { | i KA i HA i
i4-Chloro-3-KethylphenoI \ 16 336 | i KA j | | | u KA | I 1 . 1 _ 1 __ _ . [ . . [ . 1 ..| — 1 — 1 1 1 1 . . [ 1 1 1 1 i2-Hethylnaphthalene i l 8 | 336 | i i | i i KA i i i i { | i HA i KA i
CO o o CO CO
-Wk ^^ iiKAiyn', ilTS "-'
Anson^mromental Saipie Huiber
laboratory Saiple Huiber
Beiarks
lUnits 1 1 1 1 ISEHIVOIATIIE COKPOUKOS
1 1 • • • "
iHexachlorocyclopentadiene 1 |--|2,4,6-Trichlorophenol
1 2,4,5-Trichlorophenoi
|2-Chloronaphthalene
1 ' |2-Kitroaniline 1 lOiiethylphthalate 1 1 lAcenaphthylene t
r |3-Nitroaniline 1 1 " lAcenaphthene 1 1 |2,4-01nltrophenol 1 I " |4-Kitrophenol 1 1 • •
lOlbenzofuran
1 — • • • •
|2,4-0initrotoluene 1 1 |2,6-01nitrotoluene 1 1 iDiethylphthalate 1 1 14-Chlorophenylphenylethir 1 |. , IFluorene 1 1 |4-Kitroaniline 1 |— |4,6-Oinitro-2-Hethylphenol
H-Hltrosodiphenylaiine
|4-Broiophenylphenylether
IHexachlorobenzene
1 •
IPentachlorophenoi
Phenanthrene
1
Quantitation liiit (Aq)
18
11
51
It
St
It
It
St
It
5t
St
It
11
It
It
It
It
51
St
It
It
It
St
It
Quantitation liiit (Sol)
33t
33t
1656
338
1656
338
338
1656
336
lest
1651
331
33t
33t
331
33t
33t
1651
1656
336
336
336
1656
336
.... ..-.IDS Rl
DUil 25'-27'
8268-81
ug/Kg
i w u DUil 3l'-32'
8286-62
ug/Kg
S....:. .i'sAsis'^
Field Blank|DUI6 3S'-37' 821 i
8288-83 i 8215-81
ug/l i ug/Kg
" 1
1
- m DUI6 3 6 ^ ^
8215-82
ug/Kg
) •' ,
W 1 Trip Blank |
822 8215-83
ug/l
HA
HA
HA
KA
KA
KA
KA
KA
KA
KA
HA
HA
HA
KA
KA
KA
KA
HA
HA
KA
HA
HA
KA
KA
; (
Field Blank 1 822
8215-64
ug/l
i J i
DUI7 48'-42'|DUI7 45'-47'
8224-81 i 8224-62
ug/Kg i ug/Kg
1 1
1
-, r^> r---i ,.^-.. m 0UI7 SS'-57'|DUI7A 45'-47'|Field Biank|Trip Blank Trip Hank i
i i 823 i 8231 8232 j 8224-63 i 8224-64 ii 8224-65 i 8224-66 8224-67 i
I I I 1 I I I 1
1 1 ..|..... ,„..| ug/Kg 1 ug/Kg 1 ug/l | ug/l ug/l |
ioupllcate of 1 i i0UI7 45'-47' i i
1 1 HA HA 1
i i HA NA 1
i i HA HA i
1 i KA HA i
1 1 KA KA 1
i i KA KA 1
i i KA KA 1
i i KA KA i
1 1 HA KA 1
1 1 HA HA 1
i 1 KA KA 1
1 1 KA KA 1
1 1 KA KA 1
i 1 KA KA i
1 1 HA HA 1
1 1 KA KA 1
1 i KA KA i
i i KA KA i
i 1 HA HA i
i KA KA i
i i KA KA i
i 1 KA KA i
i i KA KA 1
i 1 KA 1 KA 1
CO
CD CO
E X T ^ ^ ORGAHIC AKAirSIS - 'AKAlTTfcAl Rts'UlTS - A l l SOIIOS REPORTED OK A DRT UEIGnf BASIS' ' ^ ^ ' ^ '' ''''~ . i j ^ B
iAnsonl i iv l ron ienta i Saiple Kuiber ioUl l 25'-27' iDUIl 3 l ' -32 ' iF ie ld BlankiouiB 3S'-37'ioui6 3 6 ' ^ i T r i p Blank iField BiankioUIT 4l'-42'iDUI7 45'-47'ioUI7 55'-57'ioUI7A 45 ' -47 ' iF ie ld BlanklTrip Blank iTr lp lTank i 1 1 1 1 821 1 1 1 822 1 822 1 | | | | 823 | 8231 | 8232 | i laboratory Saiple Huiber | 8268-11 | 8268-62 | 8286-63 | 8215-81 | 8215-62 j 8215-83 | 8215-64 | 8224-61 i 8224-82 i 8224-63 i 8224-84 | 8224-65 i 8224-86 i 8224-67 { 1 . . . _. __ _. 1 _i _ 1 1. 1- - ,. I 1 1 1 ,... I I I I I I 1 •• • 1 1 1 1 1 1 1 1 1 1 1 1 1 — 1 1 iBeurks | | 1 1 1 I I I 1 1 | 1 1 1 i
iun i ts i ug/Kg i ug/Kg i ug/ l i ug/Kg | ug/Kg i ug/l i ug/ l i ug/Kg i ug/Kg j ug/Kg | ug/Kg i ug/ l i ug/ l i ug/ l i
isENIVOlATIlE COHPOUHOS iouant i tat ion iQuant i tat ioni i i i i i i i i i ioupiicate of { i i | i 1 l i i i t (Aq) i l i i i t (Sol) i i i 1 i i i 1 | | |0UI7 45'-47' i j i |
lAnthracene | 11 | 336 | | | 1 | 1 I * 1 1 1 | | | | HA | KA | 1 , . _____ | ._.,,, 1 ,_|...-.,. , 1 ' • • 1 i l l
lOi-n-Butylphthalate | 18 | 336 | | | | 1 1 KA | | | | | | | KA | KA |
iFluoranthene | 18 | 336 | | | | | 1 KA | | j | j | | KA | KA |
IPyrene | 18 | 336 | | | | | 1 KA | | | | I ' I | HA | HA |
IButyibenzylphthalate | 16 | 338 | | 1 | | 1 KA | | | | | | | KA | KA |
|3,3'-Dicblorobenzidine | 26 | 668 | | | | | 1 KA | | | | | | | HA | HA |
iBenzo(a)anthracene i 16 J 331 i i i i i | KA i i i i i i i HA i HA i
|bis(2-Ethylhexyl)phthalate | 16 | 338 | 346 U | 348 U | | 346 U | 2186 U | HA | | | 348 U | | | | KA | KA |
ichrysene i 16 i 336 i i 1 1 i i KA i i i | i { i KA | HA i
iDl-n-Dctylphthalate | 16 | 338 | | | | | 1 « ' 1 1 1 1 1 1 | HA | KA |
|Benzo(b)fluoranthene | I t | 33t | | | | | 1 KA | | | | | | | KA | KA |
|Benzo(k)fluoranthene | I t | 33t i i i i 1 KA i i | | | | | KA | KA |
iBenzo(a)pyrene i 11 | 33t i i i i i i KA i i i i { i i KA i KA i
|Indeno(l,2,3-cd)pyrene | I t | 33t | | 1 | | 1 KA | | | | | | | KA | HA |
|Oibenz(a,h)anthracene | I t | 33t | | | | | 1 *« 1 1 1 | | | | HA | HA |
|Benzo(g,h,i)perylene | I t | 33t | | | | | 1 >* 1 1 1 | | | | KA | KA |
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 IQuantltation l i i i t Ku l t ip i ie r | l . t 3 | 1.13 | l . t t | 1.13 | 1.16 | KA | 1.66 | 1.63 | 1.13 i 1.21 i l . t t j l . t t { KA i NA j
ioate of Saiple Collection i 8/21/91 i 8/21/91 i B/21/91 i 8/22/91 i 8/22/91 i KA i 8/22/91 i 8/23/91 i B/23/91 i 8/23/91 | 8/23/91 | 8/23/91 i HA | KA |
ioate Saiple Beceived by laboratory i 8/22/91 i 8/22/91 i 8/22/91 i 8/23/91 i 8/23/91 i KA i 8/23/91 i 8/24/91 i 8/24/91 { 8/24/91 i 8/24/91 i B/24/91 i KA | HA 1
ioate Saiple Extracted i B/24/91 i 8/24/91 j B/23/91 i 8/26/91 j 8/26/91 i KA { 8/27/91 i 8/26/91 i 8/26/91 i 8/26/91 j 8/26/91 i 8/26/91 i KA i HA i
IDate of Saiple Analysis | 8/36/91 | 8/36/91 | B/27/91 | 8/36/91 | B/36/91 | HA | 8/38/91 | 8/38/91 | 8/38/91 | 8/38/91 | 8/31/91 | 8/36/91 | KA | KA |
l l ns t ru ien t Used for Analysis i KS-5995B i KS-5995B i KS-5995B | KS-5995B i KS-5995B i KA i KS-5995B i IS-5995B j NS-5995B | NS-5995B | KS-5995B | KS-5995B | IA j KA | 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
|CIP ^ V l V E i y IDEKTIFIED COKPOUKOS - ESTIKATED COKCEHTBATIOHS - A l l SOIIOS REPORTED OK A ORT UEIGHT B * S ^ I I ^ W |
lAnson Environiental Saiple Kuiber |0UI1 25'-27'|DUIl 36'-32'|Fieid Blank|DUI6 35'-37'|DUI6 3 l ' -32 ' |Tr ip Blank |Field Blank|DUI7 48'-42'|DUI7 45'-47'|DUI7 55'-57'|DUI7A 45'-47'|Field Blank|Trip Blank |Trip Blank | i i i i 821 i i i 822 i 822 i i { | i i 8 2 3 i 8231 i 8232 i ilaboratory Saiple Kuiber i 828t-t l | 82t l- t2 i 8268-83 i 8215-81 i 8215-62 i 8215-63 | 821S-84 i 8224-11 i B224-t2 i 8224-63 i 8224-64 i 8224-65 i 8224-66 i 8224-87 i
ineiarks i 1 i i i i i i i i i 1 1 i i
1 •• I I I I 1 I I I 1 1 1 1 1 1 1 lunits 1 ug/Kg | ug/Kg | ug/l | ug/Kg | ug/Kg | ug/l | ug/l | ug/Kg | ug/Kg | ug/Kg | ug/Kg | ug/l | ug/l | ug/l |
icOKPOUKOS i j i i i i i i 1 i VOAs iouplicate of i i i i i i i i i i i i i 1 i Twice i0UI7 45'-47' i i i i
IVOIATIIE COKPOKEKTS I | | I 1 - 1 1 1 1 1 1 I ' I 1 1
IHexane | 866 R | 866 R | | 886 R | | | | | | | | | I SJ |
llaboratory Art i facts 1 | 1 i i i 1 1 | 16 R | 16 B | 6 R | 6 R | 14 R/18 R | 18 B | | 9 B | S R |
1 1 1 1 1 1 1 1 1 1 1 1 ' 1 1 1 1
isEHIVOlATIlE COKPOKEKTS i - i - i " i " i i KA i - i - i - i - i - i - i HA i KA |
isulfur (SB) i i 1 i i 456 J i i i i i i { i i i
lUnknowo (Kuiber of Peaks) 1 1 1 1 1 S58(2) J | | | | | | I I I I
KOTES:
- Coipound was not detected. U This coipound should be considered 'not-detected' since it was detected
in a blank at a siiilar level. B Unreliable result - Coipound lay or lay not be present in this saiple. J Quantitation is approxiiate due to liiitations identified during the
quality assurance review (data validation). UJ This coipound was not detected, but the quantitation liiit is probably
higher due to a low bias identified during the quality assurance review.
GO
CO CO cn
CO.-
, j ^ ^ - ^^ ^ ^ E X T R M I F D R G A H I C AKAITSIS - AKAlfTICAl RESUITS - / l l SOIIOS BEPORTED OK A ORT UEIGHT BASIS ^ ^ ^ ' - ^ ^ P
lAnson Environiental Saipie Huiber |OUil 2S'-27'|0U|1 36 ' -32 ' |F ie ld Blank|DUi6 35'-37'|DUI6 38'-32' |Tr ip Blank |Field Blai)k|DU(7 4t'-42'|DUI7 45'-47'|DUt7 5S'-57'|DUi7A 45 ' -47 ' |F ie ld Blank|Trip Blank |Tr ip Blank | i i 1 1 821 1 1 i 822 1 822 i i i i { 823 i 8231 | 8232 | i laboratory Saiple Huiber | 8268-61 { 8266-62 i 8266-13 i 82 iS- t i j 8215-12 j B21S-t3 j 821S-t4 j 8224-11 i 8224-12 i 8224-83 i 8224-84 i 8221-85 i 8224-86 i 8224-87 i
iKeurks | | | | | I I I | | | I I I I
iuni ts i ug/Kg | ug/Kg i ug/ l i ug/Kg i ug/Kg i ug/ l j ug / l i ug/Kg i ug/Kg | ug/Kg | ug/Kg | ug / l { ug/ l { ug/ l i
ipesticides iQuantltat ion |Quant i tat ion! l i i i i i i i i |Duplicate of | | i | 1 i l l i i t (Aq) j l i l i t (Sol) i i i i 1 i i 1 i i ioUl? 45'-47' i i i i
ialpha-BHC i 6.65 { 8 | j i i i j HA j j i i j i i HA i HA i
Ibeta-BHC | t . t S i 8 i i i i i 1 KA | { { i { i i NA j NA {
Idelta-BHC 1 t . t s i s i i i i i i KA 1 | | { i i i NA j HA i
Igava-BHC (lindane) | 6.65 1 8 | | | | | 1 KA | | | | I ' I | KA | HA | 1 1 1 ! - . , . [ ' • .. [ I ' l l 1 1 1 I - ' I 1 1 1
iHepUchlor | 8.65 | 8 | | | | | 1 KA | | | | | | | HA | HA |
jA ld r in 1 1.65 | 8 | | | | | 1 KA | | | | | | | KA | HA |
IHeptachlor Epoxide | 8.85 | 8 | i i i j i KA i i | \ \ \ | KA | HA |
lEndosulfan I | 6.65 | 8 | | | | | 1 KA | | | | | 1 | KA | KA |
iDle ldr in | 6.16 | 16 i i i i | i ' KA { i | { | i i KA | KA i
|4,4'-DDE 1 6.16 | 16 | | | | | 1 KA | | | | | | | KA | NA |
isndrin | 6.16 i 16 i i i i i i HA i { { j i { i NA { NA { 1 1 1 1 •• " • 1 1 1 . . . . |. . . . . 1 . . . 1 1 1 ... . j I 1 1 1 1
lEndosulfan I I | 6.16 | 16 | | | | | 1 KA | | | | | | | KA | HA | 1 1 1 - 1" • 1 1 -•'" I • . . . - - 1 I •-. 1 1 ... . .1 ! „ . , ..,. 1 1 t 1 1
|I,4'-DDD 1 t . l t 1 16 1 1 1 1 1 1 KA 1 | | | | | | KA | HA |
icndoiulfan Sulfate i t . l t j 16 i i | i i | KA i i i i j i i KA i KA {
|4,4'-D0T 1 l . l t 1 16 1 1 1 1 1 1 KA 1 | | | | | | KA | HA |
iKeUloxychlor | t . 5 l | Bt | | | I I 1 KA | | | | | | | KA | HA |
1Endrin Ketone | t . l t | 16 | | | | | | HA | | | | | | | KA | KA |
lalpha-Chlordane | t .S t | 86 | | | | | 1 KA | | | | | | | KA | HA |
Igaaa-Chlordane i 6.56 | 88 i | | i i | KA i i i i i j i NA j HA {
IToxaphene | 1.6 | 166 | | | | | 1 KA | | | j | | | KA | HA |
CO CO
^ M . ......Jc AKAlL. U K A I V T L iuiTS - n. . J I I O S R L . „ , . J O H A O I ^ , .....^BASIS^ ^ ^ t i V i i I I y -i • i ^ J ^ V >
lAnson Environiental Saiple Kuiber |DUI1 2S'-27'iDUIl 38'-32'|Fieid Biankiouie 35'-37'iDUI6 36'-32'iTrip Blank ipield BiankiDUI7 4I'-42'|DUI7 4S'-47'|DUI7 5S'-57'iDUI7A 4S'-47'iField Blankilrip Blank i l r i p Blank i
i i 1 i 821 i i i 822 i 822 i i i i i 823' j 8231 i 8232 j
ilaboratory Saipie Huiber i 8266-61 i 8268-82 | 8266-83 i 8215-61 i 8215-82 i 8215-83 i 8215-84 i 8224-11 { 8224-82 i 8224-83 i 8224-84 i 8224-85 i 8224-66 i 8224-87 i
IBeiarks 1 1 1 1 1 1 1 1 1 1 - 1 1 1 1 1
iunits 1 ug/Kg | ug/Kg | ug/l | ug/Kg i ug/Kg i ug/l j ug/l j ug/Kg j ug/Kg i ug/Kg i ug/Kg i ug/l i ug/l | ug/l i
iPCBs IQuantltation jQuantitation! i i i i i i i i i |Dupiicate of | | | |
i i l i i i t (Aq) i l i i i t (Sol) 1 i i i i i i i i 1 i0UI7 45'-47' i i i i
|Aroclor-1816 | 8.5 | 86 | | | | | | KA .| | | | | | | KA | KA |
|Aroclor-1221 | 6.S | 86 | | | | | | KA | | | | | | | KA | HA |
|Aroclor-1232 i 6.5 i 86 i i | | i i KA | i i 1 i i i KA i KA {
|Aroclor-1242 i 8.5 i BB i i i i i i KA i i i i i - i i KA i HA i
|Arocior-1248 | 6.5 | 86 | | | | | | KA . | | | | | | | KA | HA |
|«roclor-1254 | 1.1 | 166 | | | | | 1 KA | | | | | | | HA | HA |
|Aroclor-126t | l . t | 16t | | | | | 1 KA | | | | | | | KA | HA |
IQuantltation l i i i t Kultipiier | 1.43 | 1.43 { 1.14 | 1.43 | t.43 | KA | 1.12 { t.43 i t.43 | t.St | 1.41 | l . t t | KA i KA i
lOate of Saiple Collection | 8/21/91 | 8/21/91 | 8/21/91 | B/22/91 | 8/22/91 | KA | 8/22/91 | 8/23/91 | 8/23/91 | 6/23/91 | 8/23/91 | 8/23/91 | HA | KA |
IDate Saiple Beceived by laboratory | 8/22/91 | 8/22/91 | 8/22/91 | 8/23/91 | 8/23/91 | KA | 8/23/91 | 8/24/91 | 8/24/91 | 8/24/91 | 8/24/91 | 8/24/91 | HA | HA |
lOate Saiple Extracted | 8/24/91 | 8/24/91 | 8/26/91 | 8/26/91 | 8/26/91 | KA | B/26/91 | 8/26/91 | 8/26/91 | 8/26/91 | 8/26/91 | 8/26/91 | HA | HA |
lOate of Saiple Analysis | 9/13/91 | 9/13/91 | 9/4/91 | 9/5/91 | 9/5/91 | HA | 9/5/91 | 9/5/91 | 9/5/91 | 9/6/91 | 9/6/91 | 9/4/31 | KA | HA |
KOTES: - Coipound was not detected. U This coipound should be considered 'not-detected' since it was detected
in a blank at a siiilar level. R Unreliable result - Coipound lay or u y not be present in this saiple. J Quantitation is approxiiate due to liiitations identified during the
quality assurance review (data validation). UJ This coipound was not detected, but the quantitation lliit is probably
higher due to a low bias identified during the quality assurance review.
CO
CO CO
B. INORGANIC TCL DATA
300338
Ci3 O
CO
7 ^ p - I l«LRESIi • |Al
Al^Pnironientai Saiple Kuiber
laboratory Saiple Kuiber
_ - - -
Percent Solids
lunits 1
i 1 IHORGAKIC ElEKEKTS | Detection
lUilt (Ag) 1 1 lAluiinui P 1 23.6 1 1
1 "1 lAntiiony P | 32.6 J Arsenic F i 4.6 1 1
1 1 iBariui P 1 5.6 1 1 1 " • • • • •- r
iBerylliui P | 1.6
1 |-Itadiiui P 1 4.6 (-• •• 1
ICalciui P 1 77.6 1 1 1 " • |-jChroiiui P 1 5.8
1 1 ICobait P 1 17.t
1 !•• "
ICopper P 1 16.6 1 1 I " - •• • - |
Ilron P 1 95.8 1 1 , 1 • •• 1
Ilead F/P| 1.6,111 1 1
1 1 iNagnesiui P | 118 1 1 1 - j- '• iNanganess P | 2.6 1 1 1 - •!• ••
JHercury CV| 6.28 1 1
1 1 iNickel P j 27.6
1 ipotassiui P i 818 1 1 1 |. .. . IStleniui F I 5.8 1 1 1 1 ISilver P 1 7.1
isodiui P 1 118 1 ,.,.,. 1 ,, 1 1 iThalliui F j 1.8 1 1 1 j-IVanadiui P | 7.6
Zinc P 12.1
{Cyanide AS| 16.1 1 1
.... —
Detection
liiit (Sol)
4.6
6.4
6.86
1.8
8.26
6.86
15.4
l.t
3.4
3.2
19.t
1.21/22.2
23.6
6.46
6.16
5.4
162
1.6
1.4
23.6
8.21
1.4
2.4
2.3
I stj . .on
R8-1 11499-123 BlB3-i6
-
ug/l
Rinse Blank
126
3.6
168
•
R
R
282
R
TEO i I UEIOHTi i ^ ^ ... .. ^^^
FB821 81499-lSS 8268-63
ug/l
Field
Blank
114
3.1
184
5.8
lit
4.1
R
R
375
8(5.3x)
FB822 tl499-18S 8215-64
ug/l
Field
Blank
lie
3.1
198
7,6
2.8
R
R
365
R(7.7x)
FB823
tl499-23S
8224-85
-
ug/l
Field Blank
126
S.t
3.1
145
6.8
278
4.7
7.8
R
R
316
R(5.lx)
O U I ^ ^
11499-tlS
8895-81
63.2»
ig/Kg
7838 J
9.6 J
3.7 J
98.2
1.2 f.
8.7 R
16,386 J
463 J
8.7
266 J
19,568 J
1216
9351 J
152 J
8.21 J
21.5 J
459
R
948 J
8.33
79.1 J
1778 J
438 J
DUI3 86499-125 8195-12
79.8»
ig/Kg
4858 J
UJ
3.8 J
44
t.9 8
2.7 fl
22,988 J
111 J
7.6
49.4 J
11,511 J
617
11,911 J
94.13
R
12.6 3
332
R
474 J
41.1 J
236 J
R
0UI4 lt499-t3S
8895-83
77.18
•g/Kg
2636 J
UJ
1.3 J
34.4
1.8 R
1.5 R
7118 3
31.7 3
18.2 J
6638 J
154
3468 J
55.9 J
R
7.2 3
267
R
293 «
28.5 J
113 3
B
1 S
DUil
H499-I4S
8183-11
86.68
ig/Kg
2638 J
UJ
1.2 J
18.2
6.B1R
2.8 R
9788 J
36.1 J
4.2
17.7 J
6418 3
124
5288 J
54.6 J
B
8.3 J
327
R
262 R
22.6 3
81.3 J
R
• -pagi . 1
DUI5 8I499-85S 1 8183-82
96.78
iq/jQ 1
1586 J 1
OJ 1
8.79 J
9.7 !
8.63 R
1311 J
17.4 J
5.3 J
3818 ]
81.3
951J 1
53.3 J
R
4.7 J
221
K
129 R
5.3 3
24.6 J
R
NOTES: - Elsunt was not detected. U This analyte should be considered 'not-detected' since
it was detected in a blank at a siiilar level. R Unreliable result - Analyte lay or lay not be present
In this saiple. 3 Quantitation is approxiiate due to liiitations identified
during the quality assurance review (data validation). UJ This analyte was not detected, but the quantitation iiiit
is probably higher due to low bias identified during the quality assurance review.
(Ix) This eleient was not analyzed for and not detected; however, due to saiple dilutions, the reported detection iiiit is equal to the 'norial' detection liiit nltiplied by the factor in parentheses.
ANAlfTICAl NETHOO: P - Inductively Coupled Piasia F - Graphite Furnace Atoiic Absorption CV - Cold Vapor Atoiic Absorption AS - Auto Analyzer
CO o o CO
' ^ ' u^^Mnimi
lAnson Environiental llaboratory Saiple N
1 1
- AKAiniCAL RESUlfS - A
Saiple Kuiber uiber
1 iPercent Solids
lUnits 1
IIH0R6AHIC ElEKEHTS
1 1 , 1 1Aluiinui 1 1 lAntiiony
1 Arsenic
1 IBariui 1 IBerylliui 1 j - ••
iCadiiui 1
1 ICalciui 1 1 iChroiiui 1 ICobalt r ICopper 1 ••
Ilron 1
1 Ilead
iHagnesim 1 1 iKanganese
1 iKercury 1 1 iKlckel
ipotassiui 1 1 iSeleniui
ISilver 1 1 ISodiui
IThalliui I IVanadiui 1
J IZinc
ICyanide 1 1 —
1
1 Detection iliiit (Aq)
P 1 23.8
P 1 32.8
F i 4.8
P i 5.8
P 1 1.8
P 1 4.8
P 1 77.8
P 1 5.8
P i 17.8
P i 16.8
P i 95.8
F/Pi 1.8/111
P 1 118
P 1 2.8
Cvi t.2t
P 1 27.t
P 1 818
F 1 S.B -P 1 7.1
P 1 118
F 1 1.8
P 1 7.8
P i 12.8
AS| It.t
Detection liiit (Sol)
4.6
6.4
6.86
1.8
6.28
6.88
1S.4
1.8
3.4
3.2
19.8
6.28/22.2
23.6
8.48
8.18
5.4
162
1.8
1.4
23.6
8.28
1.4
2.4
2.3
; I SOliOS REPOI
DUI6
8183-83
67.68
ig/Kg
9918 J
UJ
(18x)
82.1
1.4 R
6.2 R
9218 J
248 J
11.2
88.2 J
2l,4tt J
112t
6878 J
128 J
B
18.9 J
615
R
993 J
8.28 J
71.2 J
512 J
R
TED OK A DRY 1
DUt7 88499-87S 8183-84
82.48
ig/Kg
3318 J
UJ
1.6 J
15.3
8.91 R
1.3 R
8136 J
54.2 J
3.1
27.8 J
7268 J
157
3758 J
62.8 3
9.3 3
186
B
286 R
18.6 3
78.5 J
2.9 J
EIGHT BASIS
DUIB •1499-185 8183-15
56.68
ig/Kg
11,168 J
9.5 J
3.6 J
S6.8
1.8 R
4.4 R
22,888 J
198 J
11.3
138 3
22.768 J
( U 2 8 ^
14,168 J
162 J
«
28.4 J
548
fl
1248 J
81.8 J
675 J
R
i i
0UI9 86499-89S 8163-86
83.18
ig/Kg
2868 3
UJ
1.2 J
23.3
1.1 B
l.B R
4228 J
37.4 3
5.4
41.7 J
18,988 J
122
2B18 J
189 J
R
11.3 J
268
fl
447 J
28.4 J
138 J
«
~1 DRAIK
68499-16S 8183-87
91.38
ig/Kg
1416 J
UJ
1.5 J
26.8
8.94 R
3.8 R
3658 J
71.6 J
3.4
44.4 J
15,668 J
216
1158 J
13S J
R
17.4 J
215
494 J
17.6 J
254 J
R
> ' DUtlHSD 11499-115 8183-88
79.78
•g/Kg
Duplicate of OUtl
21813
12 J
1.1 J
15.8
8.85 R
1.9 R
6311 J
25.6 J
15.9 3
5888 J
148
3998 J
48.3 3
R
5.9 J
249
R
234 R
IB J
56.5 J
R
I ;
OUIl 25'-27' 11499-135 8268-61
95.88
ig/Kg
1536 J
UJ
5.9
8.56 fl
76.6 fl
2.7 R
2896 J
1.8
225 J
44.4 J
fl
175
R
75.2 fl
2.8 J
4.2 J
R
i !
DUil 3t'-32' tt499-14S 8288-82
96.38
ig/Kg
1336 J
UJ
1.6 J
- .... . 6.3
6.66 R
119 fl
4.1 R
2.6 J
2398 J
2.5
164 J
38.5 J
«
fl
91.6 R
2.6 J
5.4 3
R _
i
i i
-page 2
DUI6 35'-37' i 8I499-16S i 8215-61 i
95.88 1
•9/(9 1
i
list J 1
UJ 1
2.3 J i
4.9 i
t.73 fl 1
51.3 fl i
6.7 3 i
3581 J 1
1.8 i
91.9 J i
31.2 J 1
1 i
K i
129 fl i
3.B J 1
4.5 J i
K 1
,. t
KOTES: - Eleient was not detected. U This analyte should be considered 'not-detected' since
it was detected in a blank at a siiilar level, fl Unreliable result - Analyte u y or lay not be present
in thie saiple. J Quantitation is approxiiate due to liiitations identified
during the quality assurance review (data validation). UJ This analyte was not detected, but the quantitation iiilt
is probably higher due to low bias identified during the quality assurance review,
(ix) This elHent was not analyzed for and not detected; however, due to saiple dilutions, the reported detection liiit is equal to the 'norial' detection liiit lultiplied by the factor in parentheses.
AKAlfTICAl HETHOD: P - Inductively Coupled Plasu F - Graphite Furnace Atoiic Absorption CV - Cold Vapor Atoiic Absorption AS - Auto Analyzer
CO. o-o CO
m - i< - (i. ..lilRESui.. ''Al
Ansonlnviromental Saipie Huiber laboratory Saiple Huiber
,,. , Reurks
lUnits
1 IHORGAKIC ElEKEKTS
1 1 1 lAluiinui P 1 1 [Antiiony P 1 1 lArsenic F 1 ••
IBariui P 1 1 IBerylliui P 1 1 iCadiiui P 1 1 ICalciui P 1 IChroiiui P 1
1 ICobalt P 1 1 ICopper P 1 [Iron P 1
1 Ilead F/ 1 1 iRagnesiui P 1 1 IKanganese P 1 1 IKercury t \ 1 1 IKlckel P
1 iPotassiui P ISeleniui F 1
1 Silver P
Sodiui P
ThalUui F
Vanadiui P
Zinc P
Cyanide A
i Detection iliiit (Aq)
i 23.1
i 32.1
i <•*
1 S.t
1 1-*
1 *•'
i 77.1
i S.t
1 17.t
1 16.8
1 95.8
1 1.8/111
1 118
1 2.8
1 8.28
1 27.8
1 Bit
1 S.t
1 '•'
1 118
1 !•*
i M
i 12.8
S 16.8
•1
Detection liiit (Sol)
4.6
6.4
t.Bt
l.t
t.2t
8.88
15.4
1.8
3.4
3.2
19.8
8.28/22.2
23.6
8.48
8.16
5.4
162
1.8
1.4
23.6
8.28
1.4
2.4
2.3
I soiL..... JI
DUI6 38'-32' 88499-17S 8215-12
96.18
•g/Kg
1578 3
UJ
1.1 J
8.5
8.42 R
163 3
7.6 J
2.4 J
2628 J
6.7
255 J
52.1 J
R
147
R
184 J
3.8 J
18.5 3
fl
TED U .. .... 'i
DUI7 4l'-42' 11499-195 8224-81
95.B8
ig/Kg
1848 J
UJ
8.98 J
8.4
8.46 fl
38.2 R
3.7 R
2798 J
1.8
129 J
21.2 J
R
'
R
88.8 J
2.8 J
S.B J
B
s! i EIGHT'.™... =
0UI7 45'-47' 86499-285 8224-82
97.48
ig/Kg
1688 J
UJ
1.3 J
7.8
6.59 R
37.7 8
3.5 B
2748 J
8.7B
85.9 J
38.3 3
R
R
94.1 J
UJ
2.7 J
3.3 J
fl
\
m i 55'-57' II499-21S 8224-83
84.68
ig/Kg
878 J
UJ
8.96 J
7.3
8.51 8
39.9 R
3.2 R
2528 J
8.84
118 J
1B.9 J
R
R
8B.3 J
2.2 J
3.2 3
R
- p a g ' l ^ l
DUI7A 45'-47'| 88499-22S i 8224-84 i
97.48 1
•9/l!9 1
Duplicate of | DUI7(45'-47')i
655 J i
UJ i
1.7 J 1
6.4 1
8.46 fl 1
37.4 R 1
2.9 R i
2488 J i
1.8 i
51.1 J 1
14.9 J 1
fl i
R 1
87.9 J i
2.8 J 1
3.2 3 1
> 1 1
KOTES: - Eleient was not detected. U This analyte should be considered 'not-detected' since
it was detected in a blank at a siiilar level, fl Unreliable result - Analyte lay or u y not be present
in this.saiple. J Quantitation is approxiute due to liiitations identified
during the quality assurance review (data validation). UJ This analyte was not detected, but the quantitation lliit
is probably higher due to low bias identified during the quality assurance review.
(Ix) This eleient was not analyzed for and not detected; however, due to saiple dilutions, the reported detection lliit is equal to the 'norial' detection liiit lultiplied by the factor in parentheses.
AKAlYTICAl HETHOD: P - Inductively Coupled Plasu F - Graphite Furnace Atoiic Absorption CV - Cold Vapor Atoiic Absorption AS - Auto Analyzer
1 . _ ^ . — . 1 ^ ^ ^ lAHAlYTI, lUlTS -\ .\
iAns^^mroniental Saiple Kuiber i TAKK 16 i {laboratory Saipie Huiber i 911312-tl i
1 Reurks | | 1.,. I t 1 1 1 lUnits 1 ug/l | 1 ,, j 1 ioRGAKIC ElEKEKTS i i 1 1 1
IBenzene | 7 U | 1 1 1 1 I I ICarbon Tetrachloride | 6 U | 1 1 1 1 1 1 IChlorobenzene | 7 U | 1 1 1 1 1 1 IChlorofori 1 S U | 1 .... 1 ..1 1 1 1 |l,2-0ichioroethane | 6 U | 1 1 1 1 1 1 |l,l-Dichloroethylene 1 S U | 1 1 1 1 1 1 iKetbylethylketone | 12 U | I 1 1 •• 1 1
1Tetrachloroethylene | 6 U |
1 r 1 ITrichloroethylene | 6 U |
1 1 1 1 Ivinyl Chloride | 11 U | I 1 . i 1 1 1 jPyridine | 2368 U | 1 .... 1 i 1 1 IDate Saiple Collected | 6/11/91 |
IDate leachate Generated i 6/1B/91 i 1 ..,. 1 ..1 lOate leachate Analyzed i 6/26/91 |
KOTES: - Coipound was not detected. U This coipound was analyzed for but was not detected at or above
the level indicated. R Unreliable result - Coipound u y or lay not be present in this saiple. 3 Quantitation is approxiute due to liiitations identified during
the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation iiiit is
probably higher due to low bias during the quality assurance review.
The reported quantitation liiits are recovery corrected with the exception of toxaphene and chlordane.
CO o o CO
1 1 iTEHTATIVEir IDEKTIFIED COHPOUHOS |
1 lAnson Environiental Saiple Huiber | TAKK 16 | ilaboratory Saiple Kuiber i 911312-11 i
iunits i ug/l i 1 I 1 1 1 1 {Unknown | 8 J | 1 > , .. 1 1 1 ••! {Acetone { 318 R {
inethylent Chloride i 211 J { 1 1 1
j o R l ^ H l l Y S I S - AKAlYTICAl RESUIT
1 Anson Environiental Saipie Huiber {laboratory Saiple Kuiber
{Reurks 1 1 {Units
isEKIVOlATIlE ElEKEHTS
1 1 1 {2,4-Oinitrotoluene 1,. . , . 1 {Hexachlorobenzene 1 . . 1 ' ' {Hexachloro-1,3-butadiene 1 1 {Hexachloroethane
1 {nitrobenzene
{1,4-Dichiorobenzene 1 1 {Kethylphenols (total)
{Pentachlorophenol
{2,4,5-Trichlorophenol
i2,4,6-Trichiorophenol
{Date Saiple Collected 1 ioate leachate 6enerated
1 {Date leachate Extracted 1 1 {Date leachate Analyzed
~-i l-\ S -page 2 {
TAKK 16 { 911312-11 i
ug/l {
i
52 U {
46 U i
46 U 1
59 U 1
38 0 {
52 U {
52 U {
268 0 1
278 U 1
53 U 1
6/11/91 {
6/17/91 {
6/18/91 {
6/28/91 {
KOTES: - Coipound was not detected. 0 This coipound was analyzed for but was not detected at or above
the level indicated. R Unreliable result - Coipound u y or u y not be present in this saiple. J Quantitation is approxiute due to liiitations identified during
the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation liiit is
probably higher due to low bias during the quality assurance review.
The reported quantitation liiits are recovery corrected with the exception of toxaphene and chlordane.
CO o o CO >£» CO
\ ^ ' ' ' I D R G A U V F Y S I S - AKAlYTICAl RESUIT
[Anson Environiental Saiple Kuiber {laboratory Saiple Kuiber
{Reurks
lUnits
ORGAKOCHlOfllHE PESTICIDES
jgaMa-BHC
1 [Heptachlor IHeptachlor Epoxide
1Endrin
IHethoxychlor
IToxaphene
Chlordane
Date Saiple Collected
Date leachate Generated
IDate leachate Extracted
Date Extract Analyzed
f„:P'9'.3 —
TAKK 16 918312-11
ug/l
t.210
t.l7 U
1.17 U
8.33 U
8.19 U
3.3 U
8.16 U
S/11/91
? 1
6/18/91 1
6/21/91 1
1
KOTES: - Coipound was not detected. U This coipound was analyzed for but was not detected at or above
the level indicated. R Unreliable result - Coipound u f or u y not be present in this saiple. J Quantitation Is approxiiate due to liiitations identified during
the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation liiit is
probably higher due to low bias during the quality assurance review.
The reported quantitation liiits are recovery corrected with the exception of toxaphene and chlordane.
CO
o CO
1
, . . . J ^ ^ . . . . . UKAIYTL .JUIT l- P lAnsonrnvironiental Saiple Nuiber {laboratory Saiple Nuiber 1 1 {Reurks 1 1 {Units 1 1 {HERBICIDES
1 1 12.4-0 1 1 12.4.5-TP (Silvex)
ioate Saiple Collected
{Date leachate 6enerated 1 1 {Date leachate Extracted 1 1 {Date Extract Analyzed
1
•V-,- • ' i
TAKK 16 i 918312-81 1
ug/l 1
i
148 UB 1
58 UR i
6/11/91 1
6/2B/91 1
7/2/91 1
7/9/91 {
KOTES: - Coipound was not detected. U This coipound was analyzed for but was not detected at or above
the level indicated, fl Unreliable result - Coipound u y or •ay not be present in this sample. J Quantitation is approxiute due to ILeitations identified during
the quality assurance review (data validation). UJ This compound was not detected, but the quantitation ii^lt is
probably higher due to low bias during the quality assurance review. Ufl This coipound was analyzed for but was not detected; however.
the analysis was deeied unreliable.
The reported quantitation liiits are recovery corrected with the exception of toxaphene and chlordane.
CO
o CO •Cke
1 ^ ^ w • AHAlniinL JlESUlTS' -page's
i_ 1
{Anson Environiental Sample ilaboratory Saiple Kuiber 1
1 1 Kuiber { TAKK 16 {
i 918312-81 j 1 1
1 I I {Reurks | | 1 1 1 1 {Units
{TCIP HETAIS
1 1 1 lA i t tn l t 1 1 {Bariui 1 1 {Cadiiua
{Chroaiu^ 1 1 {lead 1 1 {Hercury 1 1 ISeleniui
1 {Silver 1
1 1 1 u g / l {
i {
1 »t 1 \
{ 2 8 1 {
1 16U 1
{ 18U (
1 1)1 u i
{ 1.8 U {
i 388 U i
i 28U { _ 1
1 1 {CHACTERISTICS i 1 1 1 1 {Flashpoint (at 288 1 1 IpH 1 1 {Reactive Cyanide 1 1 '• {fleactive Sulfide 1
f; 1 1
1 Ko (
1 ' • * 2 1
i S88 u i
1 21110 1
KOTES: - Coipound was not detected. U This coipound was analyzed for but was not detected at or above
the level Micatel. R Unreliable result - Coipound u y or •ay not be present in this sample. J Quantitation is approxiiate due to liiitations Identified during , the quality assurance review (data validation).
UJ This coipound was not detected, but the quantitation iiiit is probably higher due to low bias during the quality assurance review.
The reported quantitation liiits are recovery corrected with the exception of toxaphene and chlordane.
CO o o CO ^
Validated Data
Indoor borings 5 & 6 Re-sampling drywells 1-4
30034?
CO o o CO • ( ^ CO
H i f e ^ --"S'S ' ..'nCAl Ri.vL, J - Air'miu^'REPORTEU 08 A DRY U E l k BASIS ' ^ ^ B -page 1 |
{Anson E l S w e n t a l Saiple Kumber ilB 15 (15-17') ilB 15 (35-37') {iB 16 (31-32') ilB 16 (48-42') { Field Blanks { Field Blanks { Trip Blank { 'laboratory Saaple Kuiber i 12868-84 i 12168-85 i 12168-11 | 12861-12 | 12161-13 i 12861-86 { 12168-17 i f ., ,, , . . . . 1 1 ,1, 1 t 1 I . I
{Reurks { 1 1 1 i Field Blank j Field Blank { Trip Blank {
1 • " ' 1 1 1 ' ' 1 • - | — — " 1 — - 1 — —1 {Units 1 ug/Kg { ug/Kg { ug/Kg { ug/Kg j ug/l | ug/l { ug/l |
ivOLATIlE COHPOUHOS {Quantitation {Quantitationl 1 1 1 1 { i {
{ j l i i i t (Aq) j l i l i t (Sol) j i { i ' i i 1 1
ithloroiethane j I t j I t | i j i ~ i 1 1 {
{Broioiethane { I t { I t { { { { { { | |
{Vinyl Chloride { 18 | 18 { | | { { | { {
{Chloroethane { 18 { 18 { UJ { UJ { UJ | UJ { { | {
{Kethylene Chloride { 5 { 5 j 6 U { 6 U { 5 U j S U { 3 J i 4 J { 4 J {
iAcetone j 11 i I t j 118 U j 118 U j 19 U { 12 U i 9 J i 31 J { 34 J | 1 1 1 j 1 1 1 1 1 1 1 {Carbon Disulfide { 5 | 5 | { | { 1 . j 1 i
{1.1-Dichloroethene | 5 | 5 | | { | | j |
il.l-Oichloroethane j 5 { 5 i j { { j j j 1 I . . . . . . . . 1 | . . 1 . . . I . . 1 , 1 1 — — | . . 1 1 1 1 . | - . . | —1 . . . | {Total 1.2-Oichloroethene { 5 | 5 { { { { { { |
{thlorofori { 5 i 5 i j i j 15 i 15 { {
il.2-Dichloroethane { 5 j 5 j i j { i { {
1 — "" 1 1 1 1 1 ' ' ~l 1 1 1 {2-Butanone { 18 | 18 { { | | { { |
il.l.l-Trichioroethane { 5 j 5 j i j j { j j 1 . 1 - - - - , . - , 1 , -• 1 - - 1 t 1 1 1 1 1 1 1 1 1 1- 1 1 {Carbon Tetrachloride { 5 { 5 { | { | { { {
1 "" " I I I I I 1 1 { 1 {Vinyl Acetate { 18 { 18 | { | | { { {
. . „ 1 1 {Bro^odichioroiethane { S { 5 { | | { j j j
il,1.2.2-Tetrachloroethane ) 5 { 5 i j j j { { { 1 1 1 1 1 1 . I I I I 1 1 1 1 1 1 1 1 1 . . . 1 |l,2-Dlchloropropane | 5 { 5 { { | | { | |
{trans-l.S-Oichioropropene { 5 { 5 { j | j i i j 1 1 j . 1 1 1 1 1 1 {Trichloroetheas j 5 { 5 { { { j j j j
. 1 . , ^ , 1 . . - — . 1 1 1 1
'Dibroiochloroiethane { 5 { 5 { { | { | | j
|l,l,2-Trichioroethane { 5 { 5 { | { { | j j
{Benzene | 6 { 5 { j { | { { {
I. h
KOTES: Coipound uas not detected.
U This coipound should be considered 'not-detected' since it was detected in a blank at a siiilar level.
R Unreliable result - Coipound iay or lay not be present in this saiple.
J Quantitation is approxiiate due to liiitations Identified during the quality assurance review (data validation).
UJ This coipound was not detected, but the quantitation liiit is probably higher due to a lou bias identified during the quality assurance review.
|.L VOIATIIE i nBK AKAIYSIS - AKAlYTICAl RESUITS - All SOIIOS REPORTED ON A DRV UEIGHT BASIS -page 2
1 1 1 1 1 1 1 1 1 {Anson Environiental Saiple Kuiber {IB IS (15-17') {IB 15 (35-37') {IB 16 (38-32') {IB 16 (48-42') { Field Blanks { Field Blanks { Tr ip Blank {
{ laboratory Saiple Kuober { 12868-84 j 12868-65 j 12868-11 j 12868-62 j 12868-83 j 12868-16 i 12861-17 i
{Reurks { I I I I F ie ld Blank { Field Blank { Tr ip Blank {
i un i t s i ug/Kg { ug/Kg { ug/Kg j ug/Kg j u g / l j ug / l { ug / l {
ivOlATIlE COHPOUHOS iouan t i t a t i on JQuanti tat ionj i { i i i { {
i i l i i i t (Aq) i l i i i t (Sol) i { 1 i i i { { | - l i i i l i l l l i {c is- l ,3-Dichloropropene | 5 { 5 { { { { { | { { 1 1 . ' . . _ i . 1 . . . 1 __ 1 1 _ _i 1 . 1 __i 1— 1 1 1 1 1 1 1 — 1 1 — 1 {B ro io fo r i { 5 { 5 { { | { { { { { I 1 . „ i 1 1 1 1 1 1 1 . . . . , 1 1 1 1 1 ..|.. 1 | - 1 1 1 1 {2-Hexanone { 18 { 18 { { | { { { | {
| . . . . . — ] . - — . 1 - 1 1 I I I I 1 1 {4-Kethyl-2-Pentanone { 16 { 16 { { | { { { { {
{Tetrachloroethene { 5 { 5 { | | | { { { {
{Toluene { S { 5 { | { { { { { {
{Chlorobenzene { 5 { 5 { | { { { { { {
{Ethylbenzene { 5 j 5 j j j i i { i i
{Styrene { 5 j 5 i ' j { i i { i j
i l o t a i Xylenes j 5 i 5 { j j { j j { j 1 1 , 1 1 , , 1 , 1 1 1 1 1 , 1 1 1 1 - " — -| 1 1 r - - | 1 - 1 { { { 1 1 1 1 1 1 {Quanti tat ion l i i i t K u l t i p i i e r { 1.2 { 1.2 { 1.8 { l . t { l . t { 1.8 | 1.6 {
{Date of Saiple Co l lec t ion i 12/8/91 i 12/B/91 i 12/7/91 i 12/7/91 ' i 12/7/91 i 12/8/91 i ' HA i
{Date Saipie Received by laboratory | 12/18/91 | 12/18/91 | 12/11/91 | 12/18/91 | 12/11/91 | 12/11/91 | 12/11/91 {
1 - - 1 1 1 1 1 1 r 1 {Date of Saiple Analysis I 12/17/91 { 12/17/91 { 12/17/91 { 12/17/91 { 12/18/91 { 12/18/91 { 12/18/91 {
{ Ins t ru ien t Used for Analysis { GC/HS-5995A { GC/HS-5995A j GC/KS-5995A { GC/NS-5995A { GC/KS-5995A { GC/NS-5995A { GC/KS-5995A { 1 1 1... 1 1 1 1 1 1
BOTES: Coipound was not detected.
U This coipound should he considered 'not-detected' since it was detected in a blank at a siiilar level.
R Unreliable result - Coipound lay or may not be present in this saipie.
J Quantitation is approxiiate due to liiitations identified during the quality assurance review (data validation).
UJ This coipound uas not detected, but the quantitation liiit is probably higher due to a low bias identified during the quality assurance review.
CO;
CO
o o CO C l
o
{EXTRACTABIE 0R6AKIC AKAIYSIS - AKAlYTICAl RESUITS - All SOIIDS REPORTED OK A DRY UEIGHT BASIS
iAnson Environiental Saiple Huiber (IB 15 (15-17') (IB 15 (35-37') ilB 16 (31-32') ilB 16 (48-42') jlahoratory Saiple Kuiber ( 12868-84 | 12868-85 | 12866-11 j 12868-12 1 . . . . . 1 . 1. 1 . , 1 , 1 1 1 1 ~ — 1 (Reurks I I I I
{Units 1 ug/Kg { ug/Xg | ug/Kg | ug/Kg 1 . . . . ! . , . . 1 . . 1 . .1 1 1. 1 .- — — . . | . - . . — 1 . - | . . | 1 — | . ISEKIVOIATIIE COHPOUHOS IQuantltation {Quantitation! { { { j j l i ^ i t (Aq) ( l i i i t (Sol) { i ( j 1 1 1 1 1 1 1 IPhenol ( 18 ( 338 { { | ( i._ . . 1 . .1 1 1 1 1 1 1 1 1 1 1 1 |bis(2-Chloroethyl)ether { 18 ( 331 { | ( (
(2-Chloropbenol | 18 | 338 | | | ( 1. 1 ..1 1 1 .1 _
1 1 1 1 1 1 — 1 (1,3-Oichlorobenzene | 18 ( 338 ( ( ( (
(1,4-Oichlorobenzene | 11 j 331 j | | { i „ , . . . 1 . .1 . , 1 . . , . 1 1 .1 1 1 1 1 — 1 1 1 — {Benzyl Alcohol | I t { 331 { { { { 1 . , . . . .1 1 1 1 , 1 . . 1 1 1 1 1. 1 1 1 {1,2-Dichlorobenzene | I t | 331 | { | ( i „ .1 .1 .1 .1 1 .1 1— 1 1 1 1 1 1 |2-Nethylphenol ( I t { 331 { { | | 1 . , . . . 1 1 1 . ) 1 1 1 1 1 1 1 1 1 {bis(2-ChIoroisopropyl)ether | I t | 33t | ( { { I . . . . . . . 1 1 . 1 . 1 1 . . 1 ; . . . . 1 — 1 1 1 1 1 1 (.. Jiyipbenol { I t | 331 { | ( | 1 . . . . . . - j . . | 1 - : 1 I -1 (H-Nitroso-di-n-Propylaiine i I t | 331 | j j • j 1 ,1 1. . 1 1 1 1 . 1— . | - | . . — 1 1 . 1 . | (Hexachloroethane | I t ( 33t ( | ( (
initrobenzene i It j 331 j i j i 1 1 1 1 1 1 1 1— 1 1 1 1 1 {Uophorou [ I t { 331 { ( { ( 1 1 - 1 1 1 1 1 1 1 1 1 1 1 1 (2-Hitrophenol { It { 331 ( | ( {
i2,4-Diicthylphenol { It ( 331 i ( j i 1„ . , 1 1 1 1 . . . .1 1 | . . . . 1 1 1. 1 . 1 . | (Benzoic Acid { St ( 16S6 ( I I I 1 t 1 1 1 1 1 1 1 1 1 1 1 1 |bis(2-ChloroeChoKy)iethane | 11 { 331 | { ( ( 1 1 1 . 1 1 1 1
|2,4-Dichlorophinol ( 18 { 331 { ( { { ) _ ^ 1 I 1 1 . 1 1 1 " 1 1 1 1 1 1 (1,2,4-Trichiorobenzene { It ( 33t { { { (
(Naphthalene ( I t j 33t j ( | { 1 . , 1.. ..1 1 1 1 1 1 1 1 1 1 1 1 {4~Chloroaniiine { I t ( 331 ( { { { { 1 1 1 1 .1 .1 1 1 1 1 1 1 1 1 1 (HtMchlorobutadiene ( 11 ( 331 | { { {
|4-ciiIoro-3-Nethyipiienoi I 11 | 338 | | | j
jz-Hethyinaphthaiene { It { 331 j { ( j 1 1.. . . | 1 1
'^k •
Field Blanks 12168-13
Field Blank
ug/l
i .-. .
-page 3 |
Field Blanks | Trip Blank {
12861-16 { 12868-17 i
Field Blank { Trip Blank (
ug/l ( NA {
1 ** 1
i *' i i ** i i "* i 1 '* {
i NA {1
i K* [ i
i <* |li
1 ** 1
1 ** i
1 ** 1
i "* i i K* i
i >* i i 1* i
1 «* 1
1 ** 1
i <* i i Kl i
1 "* (
i HA i
i K* i
i ** ( 1 KA 1
i KA i
NOTES:
Compound was not detected.
This coipound should be considered 'not-detected' since
it was detected in a blank at a siiilar level.
Unreliable result - Coipound lay or lay not be present
in this sample.
Quantitation is approxiute due to lUitations identified
during the quality assurance review (data validation).
UJ This compound was not detected, but the quantitation
liiit is probably higher due to a low bias identified
during the quality assurance review.
NA Not analyzed.
-•• i & --i ' 5 ^ k - - !• ~ EXTRACTABIE O f l d ^ H l T S I S - AKAlYTICAl RESUITS - All SOIIOS REPOBTEO OH A DRY UEIGHT 8ASIS ^ B -page 4
iAnson Environiental Saiple Kuiber (IB IS (15-17') (18 15 (35-37') (IB 16 (31-32') (IB 16 (41-42') ( Field Blanks j Field Blanks j Trip Blank
ilaboratory Saiple Kuiber i 12868-84 ( 12868-85 j 12868-81 ( 12868-12 j 12866-13 i 12868-66 i 12868-87
{>.. .,ks ( { { { ( Field Blank ( Field Blank ( Trip Blank
1 • " • • 1 1 1 1 1 1 1 (Units { ug/Kg ( ug/Kg ( ug/Kg ( ug/Kg { ug/l { ug/l { KA
isEKIVOlATIlE COKPOUKOS iouantitation (Quantitationj 1 1 i i i i i ( liiit (Aq) (lliit (Sol) { ( ( { ( i i
iHexachlorocyclopentadiene ( 18 ( 336 ( ( ( ( i i ( H A
(2,4.6-Trichlorophenol ( 18 ( 338 { ( ( ( ( { ( H A
1 - ~ ~ l — "1" 1 1 1 1 1 1 1 (2,4.5-Trichlorophenol ( 5 8 { 1658 ( ( { ( { { ( H A 1. 1 .. 1 .. .1.. . . 1 1 1 1.. .. 1 — 1 1 1 1 1 1 1 1 1 (2-Chioronaphthalene { 18 { 338 ( { { { { ( ( H A
(2-Kitroanliine { 58 ( 1658 { { { { { ( ( H A 1 _ 1 ...|__ 1. ( { { { {
(Oiiethylphthaiate { 18 ( 338 { { ( { ( ( ( KA
(Acenaphthylene { 18 ( 338 { { { { ( ( ( H A 1 1 .1 I-. . 1 1 I-- 1 1 1 1 1 1 • •-- 1 . . 1 . 1 | . 1 . 1 1 |_ 1
(3-Kitroaniline { 58 ( 1658 { { { ( ( ( ( H A
(Acenaphthene { 18 ( 338 { ( ( { - ( i i KA
1 -initrophenol { 58 ( 1658 { ( ( { ( ( ( KA
i4-Kitrophenol { 58 ( 1658 { ( ( { i { i KA
(Dibenzofuran ( 16 ( 336 { ( ( { ( ( ( KA
i2.4-Dinitrotoluene i 18 ( 338 { { ( { i { j KA
i2.6-Oinitrotoluene { 18 ( 338 ( ( ( ( { { ( H A
1" ~1 " 1— " " 1 1""" 1 1 1 1 1 1 (Diethylphthalate { 18 ( 338 ( ( ( ( { { ( H A
i4-Chlorophenylphenylether { 18 ( 338 ( ( ( ( { { i HA 1 I I I I 1 ™ -1- 1 - — 1 — — -1 . _ _l
(Fluorene ( 18 { 338 { { { { ( ( ( HA |
(4-Kitroaniiine ( 58 ( 1658 ( ( { { ( { ( H A
{4,6-0initro-2-HeChylphenol { 58 { 1658 ( ( ( ( { { { KA
(K-Hitrosodiphenylaiine { 18 { 336 ( ( i i { i i KA
(4-Broiophenylphenylether ( 18 ( 338 { ( { ( ( ( ( KA
(Hexachlorobenzene ( 18 ( 336 { { ( ( ( ( ( KA 1 1 1 I 1 .1 1 .
(P....achlorophenol ( 58 ( 1658 { i { i ( i i KA
Phenanthrene 18 338 1 KA
i;.
KOTES:
- Coipound was not detected.
U This coipound should be considered 'not-detected' since
it was detected in a blank at a siiilar level.
B Unreliable result - Coipound u y or u y not be present
in this saipie.
J Quantitation is approxiute due to liiitations identified
during the quality assurance review (data validation).
UJ This coipound was not detected, but the quantitation
liiit is probably higher due to a low bias identified
during the quality assurance review.
HA Hot analyzed.
^ ^ .J^ l u m a m i W K u AKAIYSIS - AKAIYTICAI RESUITS - A H soiios REPORTED OK A DRY UEISHT BASIS ^ ^ -page s (
.. 1 1 |.. 1 1 _ 1 1 JAnson Environiental Sample Kuiber (IB 15 (15-17') jlB IS (35-37') {iS 16 (38-32') {IB 16 (41-42') | Field Blanks i Field Blanks i Trip Blank i llaboratory Saiple Kuiber i 12868-84 j 12868-65 i 12868-81 j 12868-62 i 12868-83 { 12868-86 j 12661-17 j
ifleurks i i { i i Field Slank i Field Blank { Trip Blank {
{Units i ug/Kg i ug/Kg i ug/Kg j ug/Kg { ug/l i ug/l j KA j
isEHIVOlATIlE COKPOUKOS iQuantltation (Quantitationi i { i i i i i i i liiit (Aq) jlilit (Sol) i j i ( i { { i
iAnthracene { 11 { 331 { j i i j i ( KA {
ioi-n-Butylphthalate j 11 j 331 i ( \ \ \ \ j KA {
(Fiuoranthene j It i 331 j j j { j { { KA j
(Pyrene { 11 { 331 { ( ( { { { { HA { 1 . . 1 1 |_ 1 j 1 j 1 1 . .. t
jsutylbenzylphthaiate j 11 { 331 j j j | j j { NA j 1 • 1 |- t • • 1 • I - - |-- - • •• 1 •• '
{3.3'-Dichlorobenzidine j 21 j 666 j j { j { j j HA j
{Benzo(a)anthracene { tt { 331 { { { { { j ( KA {
(bis(2-Ethylhexyl)phthalate { 11 { 331 { { 131 J ( { 411 ( { { HA {
jchrysene i 11 j 338 i { i { { \ { NA i
joi-n-Octylphthalate i 18 j 338 i i j { j \ { HA { !-- I l l 1 1 1 1 1 I I 1 1 1 1 1 1 • 1 1 {Benzo(b)fiuoranthene { 18 ( 338 { ( { { ( { { KA - {
(Benzo(k)fluoranthene { 18 ( 338 { { { { - { ( { HA {
|8enzo(a)pyrene { 18 { 338 { { ( { { ( ( NA { •• { • " { " {
ilndeno(l,2.3-cd)pyrene j 18 { 338 i i { j { { j HA {
{Oibenz(a,h)anthracene j 18 i 338 j { { { j ( ( KA {
{Benzo(g,h.i)perylene { 18 { 338 { { ( { { ( ( NA {
1 1 1 { 1 1 { { { (Quantitation liiit Kultipiier ( 1.18 { I.IB { 1.83 ( 1.83 { 1.88 { 1.86 { KA {
(Date of Saiple Collection { 12/8/91 ( 12/8/91 { 12/7/91 { 12/7/91 { 12/7/91 { 12/8/91 { KA ( 1 _ 1 1 1 ( 1 _ .. 1
1 1 1 1 1 1 1 1 1 (Date Saipie Received by laboratory { 12/11/91 ( 12/16/91 { 12/18/91 { 12/16/91 ( 12/18/91 { 12/18/91 ( NA (
(Date Saiple Extracted { 12/11/91 { 12/11/91 ( 12/11/91 { 12/11/91 { 12/18/91 ( 12/18/91 { KA {
ioate of Saiple Analysis i 12/16/91 i 12/16/91 i 12/16/91 i 12/16/91 i 12/16/91 { 12/16/91 i U \ 1 1 1 1 1 1
(Instruient Used for Analysis { GC/KS-5995B { 6C/KS-5995B { 6C/KS-5995B { 6C/KS-5995B { 6C/HS-5995B ( 6C/KS-5995B ( KA {
KOTES: - Coipound uas not detected. U This coipound should be considered 'not-detected' since
it was detected in a blank at a siiiiar level. R Unreliable result - Coipound u y or lay not be present
in this saiple. J Quantitation is approxiiate due to liiitations identified
during the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation
liiit is probably higher due to a low bias identified during the quality assurance review.
KA Hot analyzed.
ic iP - I £mTTVFiv , i i ) £ | ( i l f j ' " "•."OUKOS r . "•STIKATEI] . ,RATI0K1 i; SOlIOt , , . , ; . > ; E 0 ONfc^mr » U 5 H I B A b ^ ^ B -page 6
( A n s i f l ^ P l n i e n t a l Saiple Kuiber (IS 15 (15-17 ' ) (IB 15 (35-37 ' ) (IB 16 (31-32 ' ) {IB 16 (48-42 ' ) { Field Blanks | Field Blanks | Trip Blank ( ( l abora tory Saiple Nuiber j 12668-14 j 12861-65 j 12868-81 ( 12868-12 i 12861-83 j 12868-86 j 12861-17 j
i f l e u r k s i 1 i i i Field Blank j Field Blank \ Trip Blank j
j u n i t s j ug/Xg j ug/Kg { ug/Xg { ug/Kg j ug/L j ug/ l j ug/L i
icOKPOUNOS i i { i i { 1 1 1 1 1 1 1 1 1 1 1
(VOIATIIE COKPOKEKTS 1 - 1 - 1 - 1 - 1 - 1 - I - I 1 1 . 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
(SEKIVOIATIIE COKPOKEKTS { { | ( 1 - 1 - { KA ( 1 . 1 . 1 1 1 l i l t
1 1 1 1 1 1 1 i 1 ( l abora to ry Ar t i f ac t s (Aldols , e t c . ) { 4688 R { 5811 R ( 4111 R | 4588 R ( | | (
(Unknown ( ( 428 J | ( ( { | { 1 ( 1 1 1 1 .. 1 1 1
KOTES: - Coipound was not detected. U This coipound should be considered 'not-detected' since
it was detected in a blank at a siiilar level. R Unreliable result - Coipound lay or lay not be present
in this saiple. J Quantitation is approxiiate due to liiitations identified
during the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation
liiit is probably higher due to a low bias identified during the quality assurance review. Hot analyzed. HA
CO o o CO
CO o o CO Ul
• J i iORGAHi; i lS - ; [ A l RESi i A l l Sli lORTED 1 . [ UEIGHll . ' S f ^ ^ ! « i i ! -pagii.
n R i Env i ron ienta l Saiple Kuiber i lB 15 (15-17 ' ) j l B IS (35-37 ' ) (IB 16 (38-32') j lB 1 ^ 4 1 - 4 2 ' ) i F ie ld Blanks ( F ie ld Blanks ( Trip Blank ( l labora tory Saiple Nuiber i 12161-14 j 12661-85 i 12161-81 j 12168-82 j 12868-83 j 12 t6 t - t 6 j 12661-17 j
1 1 1 1 1 ' 1 1 '1 1 (Reurks ( { { { { F ie ld Blank { F ie ld Blank { Trip Blank {
jUni ts i ug/Kg { ug/Kg { ug/Kg { ug/Kg | ug / l { u g / l | KA j
jpes t ic ides JQuant i ta t ion JQuant i ta t ion j i J J { j j i j j l i i i t (Aq) j l i l i t (Sol) { j { i { i j j
1 1 1 1 1 1 1 1 1 .| -. 1 (alpha-BHC ( t . t S { 8 { { { { ( { { KA {
jbeta-BHC j 8.85 j 8 j { j j j j { NA j
jdelta-BHC i 8.85 j 8 j j j j { j j HA j
(gaina-BHC ( l indane) j 8.85 i B j j i j j j j KA j
JHeptachlor i 8.15 i 8 j i j j i j j NA j
(A ld r in { 8.85 { 8 { { { { { { { NA {
| . 1 1 1 —1 1 1 1 |— 1 1 (Heptachlor Epoxide { 8.85 { 3 { { ( { { ( { KA (
(Endosulfan I { 8.85 { 8 ( ( { { { { { NA {
{D ie ld r i n { 8.18 ( 16 { { { { | { { NA (
i ( . ( ' -ODE i 8.18 i 16 j j { j j { { HA i 1 . . . • _
(Endrin { 8.18 { 16 ( { ( { { ( ( KA {
iEndosulfan I I { t . l t j 16 j i i j ( j j NA {
{4.4'-DDD i t . l t { 16 i i i { ' i i i NA i
JEndosulfan Sul fate ( t . l t ( 16 { ( { { { ( { NA (
i4,4'-OOT i 8.18 i 16 i i i i i i { HA i 1 1 , 1 .1 1 . . ,1 ,, ,, 1 1 1 ,1 1 1 - 1 1 1 1 I I • . |.. 1 ..|... 1 (Nethoxychior ( 8.58 ( 8 { ( { { { ( ( HA {
(Endrin Ketone { 8.18 ( 16 { { ( ( { { ( NA {
(aipha-Chlordane { 8.51 ( 86 { { ( { { { ( NA ( 1 1 1 ~l 1 1 1 1 1 1 1 (gama-Chiordane ( 8.58 { 88 ( { { { { { { NA (
{Toxaphene { l.t { 161 { ( ( { { ( { NA {
NOTES: - Coipound uas not detected. U This coipound should be considered "not-detected* since
it uas detected in a blank at a siiilar level. R Unreliable result - Coipound lay or lay not be present
in this saiple. J Quantitation is approxiiate due to liiitations identified
during the quality assurance review (data validation). UJ This coipound was not detected, but the quantitation
iiiit is probably higher due to a low bias identified during the quality assurance review.
HA Hot analyzed.
El^^H ( E l ^ ^ K QRGAKIC AKAIYSIS - AKAlYTICAl RESUITS - All SOIIDS REPORTED OH A DRY UEIGHT BASIS -page I
(Anson Environiental Saiple Huiber (IB IS (15-17') ilB 15 (35-37') ilB 16 (31-32'j (IB 16 (48-42') { Field Blanks | Field Blanks { Trip Blank i
(laboratory Saipie Huiber j 12861-14 j 12868-15 j 12861-11 j 12168-82 j 12861-83 j 12868-86 ( 12868-67 j
{Reurks i i i i 1 Field Blank | Field Blank j Trip Blank j
jUnits 1 ug/Kg | ug/Xg | ug/Kg | ug/Xg ( ug/l ( ug/l ( KA j
(PCBs (Quantitation (Quantitation( | 1 1 1 i 1 j
j { liiit (Aq) (liiit (Sol) j { { i ( i j i
JAroclor-lBlB { 8.5 j 88 j { ( { j j ( HA i
{Aroclor-1221 j 8.5 j 86 j { ( j j j ( KA j
(Aroclor-1232 j 8.5 j 88 j ( j { j j ( NA j
iArocior-1242 j 8.5 j 88 ( j j ( j ( j HA j
(Aroclor-1248 ( 8.5 { 88 { { { { | ( { NA |
(Aroclor-1254 ( 1.8 { 168 { { { { { { | NA (
iAroclor-1261 { 1.8 ( 168 ( { j ( j j j KA j
(Quantitation liiit Nultiplier { 1.16 { 1.16 { 1.81 j 1.83 j 1.82 \ 1.82 i HA i
(Date of Saiple Collection { 12/8/91 { 12/8/91 ( 12/7/91 ( 12/7/91 { 12/7/91 { 12/8/91 ( NA (
(Date Saipie Received by labcratory { 12/18/91 { 12/18/91 { 12/16/91 ( 12/16/91 { 12/18/91 { 12/16/91 ( NA {
(Date Saiple Extracted { 12/11/91 i 12/11/91 i 12/11/91 i 12/11/91 i 12/18/91 { 12/18/91 i KA {
(Date of Saiple Analysis { 12/14/91 j 12/13/91 j 12/13/91 j 12/13/91 j 12/13/91 j 12/13/91 j KA j
KOTES:
- Coipound uas not detected.
U This coipound should be considered 'not-detected' since
it uas detected in a blank at a siiilar level.
R Unreliable result - Coipound lay or lay not be present
in this saipie.
J Quantitation is approxiiate due to liiitations identified
during the quality assurance revieu (data validation).
UJ This coipound uas not detected, but the quantitation
iliit is probably higher due to a low bias identified
during the quality assurance review.
HA Hot analyzed.
CO
o CO Ul
B. INORGANIC DATA
300356
CO
o CO
'•j^^^ i ANAl: buiTsi' . ISOLI
j Anson E ^ W n i e n t a l Saiple Nuiber (laboratory Saiple Nuaber
(Percent Solids
junits
(INORGANIC ElENENTS ( Detection 1 { Uiit (Ag) 1 1 . .
(Aluiinui P ( 72.8 I . . , .. .. . 1
(Antiisny P { 45.1 1. .. .1 ..
(Arsenic F ( 2.8
(Bariui P { 3.8 1.. .. _. 1 . .. |.. .. — — — 1 — (Berylliui P ( 1.8
. . . . „i 1 1— (Cadiiui P { 4.8 1 .... 1 . . . . (Calciui P ( 38.1
1 1 (Chroiiui P ( 7.8 1 . 1 ._ 1 1 (Cobalt P ( 18.8 j . . . 1
jcopper P ( 2.8 1 . . 1 - --1 • • 1
(Iron P { 9.8 1.. .. 1 . . 1 — 1 — (lead F ( 1.8 1 , 1 . .__ (Hagnesiui P ( 48.8 1 ... ,1 ... r • ••- 1
(Hanganese P ( l.t
JHercury CV j t.2 1, , . 1 . .. 1 1 (Nickel P ( 12.8 1 .. ... 1 1 1 (Potasslui P ( 2148 1 1 1 1 (Seleniui F ( 4.8 1 1 (Silver P ( 6.8 |.. . . . — 1 — (Sodiui P ( 4458 :.. 1 |.. — — — 1 (Thalliui F ( 2.8 1 — ~ " ~ l — — (Vanadiui P ( 4.8
1 1 (Zinc f ( 2.8 1 1 1 1 (Cyanide A { 16
Detection liiit (Sol)
14.4
9.8
8.4
8.6
6.2
1.8
7.6
1.4
2.8
•
8.4
1.8
8.2
8.8
8.2
6.1
2.4
428
1.8
1.2
898
6.4
8.8
8.4
1.8
DS',.vrua. J ON A U l wctuHT BASl'^ '
IBIS 15-17' (IB 15 35-37' IB 16 31-32' II69I-I5S j 16696-165 j 11691-675
97.48 i 97.48 j 96.68
ig/Kg i ig/Kg i ig/Xg
683 i 1366 i 1111
{ 1.57 { t.75
2.6 ( 4.4 ( 3.7
1.56 U i 1.77 U i 1.51 U
1,1 U j 8.96 0 j 8.68 U • 1
69.6 R ( 21.2 R { 26.5 R
4.6 { 3.8 ( 2.4
1 1
7.4 U ( 5.8 U { 3.7 U
3918 ( 3491 ( 2241
8.74 ( 1.2 ( 8.85
192 ( 148 ( 112
35.8 { 38.2 1 64.3
i 2.3 U {
UJ i UJ 1 UJ
UJ { UJ i UJ
2.6 U i 2.7 U { 3.1 U
5,4 R 1 4.6 R 1 4.2 R
- - ; r-
IB 16 41-42' II698-I8S
96.68
ig/Kg
1181
1.7
1.8
8.68 0
1.4 U
19.7 R
3.8
5.4 U
3311
1.8
lie
47.4
UJ
UJ
2.6 U
8.4 J
• Field Blanks 8869I-I9S
1.18
ug/l
Field Blank
3.8
93.8
14.8
261
1.8
UJ
6.1 J
-page 1 (
Field Blank ( II69I-18S j
l.lt j
ug/i (
Field Blank j
j
3.8 i
5.1 (
78.1 1
j
11.6 (
77.6 {
118 (
j
14.8 i
UJ (
1
6.8 J 1
KOTES: - Eleient was not detected. U This analyte should be considered 'not-detected' since it uas
detected in a blank at a siiilar level. R Unreliable result - Analyte lay or u y not be present in this
saiple. J Quantitation is approxiiate due to liiitations identified during
the quality assurance review (data validation). UJ This analyte uas not detected, but the quantitation liiit is
probably higher due to a low bias identified during the quality assurance review.
ANAlYTICAl NETHOO: f - Inductively Coupled Plasia F - Graphite Furnace Atoiic Absorption CV - Cold Vapor Atoiic Absorption A - Auto Analyzer OS - Oistiilation/Spectrophotoietric
IHORGAKIC AHAl'R
! ! ! J > i ; » i
'AKATYTicirKSii[fP-~Aiilo[iDslEPORfErOHToRYliniiiTlE^^ -page 2 ^ ^
(Anson Environaental Saaple Ruabcr j DU 11 ( DU 12 ( DU 13 ( DU 14 i Field Blank i {> atory Saaple Huiber ( 11691-115 ( 11698-825 { 88698-83S i 88698-845 i 88698-811S i
(Percent Solids ( 84.28 ( 59.88 ( 78.38 j 76.48 i 6.88 i 1 ,. .1 1 - -1 ... |._ 1 1 (Units ( ig/Kg { •g/Kg { ag/Kg ( ag/Kg ( ug/l {
iIHORGAKIC ElEKEHTS i Detection { Detection ( i i i (Field Blank { i . j Halt ( H a l t (Sol) ( j { { j (
JHercury CV ( 8.2 ( 8.1 ( ( ( ( ( (
(Cyanide A ( 18 { 1.8 ( ( ( i ( ( 1 .1 ( ( 1 1 ( 1 1
KOTES: - Eleaent was not detected. U This analyte should be considered 'not-detected' since it was
detected in a blank at a similar level, fl Unreliable result - Analyte u y or aay not be present in this
saaple. J Quantitation is approxiute due to liaitations identified during
the quality aesurance review (data validation). UJ This analyte was not detected, but the quantitation Halt is
probably higher due to a low bias identified during the quality assurance review.
AKAIYTICAI HETHOD: CV - Cold Vapor Atoaic Absorption A - Auto Analyzer
CO o o CO
00
Unvalidated Data
Monitoring Wells 1D, 4 & 6
300359
M'-: • i^Ki'~ni\! CAS<5 N G = ; H i~ B1 1
;AHPL.E I D
r / : : • .1. J . S.^ •••C
F-Bl 1 2 6 M W - 4 ( 7 5 - 7
M l , ! . - !• r,
MW—ID( i 2 0
l-.tl.i 1" ( .-Lj"; / . •
MW-T ( 6 0 - 6 :
L a o ) D i e XiJ :
0 0 6 4 9 - 0 2 s . 0 0 6 4 9 0 4 S
0 0 6 4 9 - 0 8 3
j") r . ,il.,/j. Q _ , ; i I C;
r i •"• A :(i Q •— I •> '^^ Q
. JI
.1C P .1 n t s r s 1 s m s n fc c o r r e c t i o n s a P G 1 .i e ci ' UJers I C P b a c k q r o u , - i d c o r r e c t i o n s a . D o l i e d ?
I f yss—'i- ' jere r a w d a t a , a e n s r - a t s d b B f o r e a D D l i c a t i o n o f b a c k c r o L i n d c o r r s c t i o r " : ; : V .':::i c ; / j^J f
<~. D n d .i. t .i o n s '"! -51 a. D a. c k a. cj f 1 , ' - f = i.',i,;. r i-H !-i-,=, 1 1 • . . ! i e c a r m s a n a
'._ ! ] &? i_ •._' I I <... I -;:.-\ • „ ',. •• !_' t j '.. I ; L t_ •.._ T H E .,•_ "... -r i a. .L y n i i '..i i '_• i U ',_•}If l.j .•_ -i:^ ' - '.zr: : h : vz =;
-i- 1 n n n v
an -ins? conditions data jcopy data package and .ti i.skstts' has been authori
r>ci aoov f? . , t h e d a t < : ; n r a i n e a '...! I•E •,_ '__= < 1!!...''„.i >_ '.t? 1 ! cz ; r . G -n?. i_' J . c r '..J CT. '._•:=*. -.n u i L J f i t ..•_ •_ '.-
...I ;...' V : ne !...aaG l a n a a e r _••. I i •=•. '..J r r • :-• <.j c - := .1 y i f r: © s •:n => v S i i T .1 B D i_' y =._ ; ! fr" i •-_• .L .;. '..J V-f .L. i k U
. a n a t LI r a ; (^^Oi^^JjdL i ^ iad ie;
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.ana t a r e
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: ^ ^ ^
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300360
• I 01
}" C E I M I C
; : C E I M I C C S B B N O ,
s a .11 .'•' w a t e r .) : W A T E R
Q w / m e d ) 3 LOW
^ N b u N
: r a c t : A N S O N
S A S N o , ; 6 i j b N o : , ' r
L a p S a m p . L e
•= . , - , >. i ! - \ ' .
i c e n t r a c i o n u n i - '.—' t ! I ! L J .-• ! •-. ' - I ".J i V w e 1 a n t :
H n a .
.'' -'-r .,:1 '••/ — V V.' - Z J
7440-36-0 7440-3S-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4
7439-96-5 7439-97-6 7440-02-0 7440-09-7 77S2-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6
; H.Lur"inLUT! 1 Antimonv J Arsenic ! BariLiiTi 1 Beryl 1ium i Cadmium i Calcium i Chromium ICobalt i CoDoer ! I ron ! Lead 1Naanesium i Nanc!-an ese 1 Mercurv 1 N i c k -e 1
1 Potassium ': Selenium 1 SiIver i Sodium ;Thai 1ium ;Vanadium 1 Z i n c 1 Cyanide
i t ;
i \
3 , Citj 1 4 , 0 0 I
) ! " E u ( I i i 1
7 „ 0 0 i
! I i
. j , r j a '-J':.* 1
4 0 . 0 0 i
2 . 0 0 I
2 1 4 0 . 0 0 I
4 , 0 0 !
6 . 0 0 !
4 4 5 0 , 0 0 i
y ' i I ' . ' )
H' .. s'ii';
l.jl W
P; i
I p I
' F'
! Cl-
H a - i - ! • - , r - : JLORLESS . a r ; e>; t u r e ;
. o r A -f t e r - O R L E S S C i a r i H-' C L E A R H r r. 1
Tien c s :
300361
INORHAN;
i^^^^Name; CLINIC
L .b Code; CEIMIC
Matrix (soil/water)
L ;vel ( low/med) ;
"/•— S o 1 i id s ;
P31 12
ANSON
WATER
or i^'er'O
\ c a n t r a t i c n Li n i t s ( u q .• • r mq.-'r-..q
• c*. I,.' •.,.' C:'. 11! !_' J. '™ .1 i-' a ^-' -' •—' -T .-•
Da. tEr R e c e i v e d ; 1 1 . / 2 2
w e i g h t ) : (..JG/L
.-H'-z: N a
i 7 4 2 9 ~ - 9 0 - - 5
i 7 4 4 0 - 3 8 - 2
\ 7 4 4 0 - 4 1 - 7 ! 7 4 4 0 - 4 3 - 9 ' 7 - ' ' 4 0 —" !") — '"'
I 7 4 4 0 - 4 8 - 4 I 7 4 4 0 - 5 0 - S
i 7439—92—1 ! 7 4 3 9 - 9 5 - 4
i 7 4 3 9 - 9 7 - 6 I 7 4 4 0 - 0 2 - 0 i 7 4 4 0 - 0 9 - 7 L 7 7 8 2 - 4 9 - 2 I 7 4 4 0 - 2 2 - 4
j -7.440—23—0
I 7 4 4 0 - 6 6 - 6
COLORLESS
COLORLESS
C D n c e n t"" a t i (D r
H.Luminum Antimony I Arsenic E'ariu.m i Beryl 1ium i Cadmium ; Calc.iu.m i Chromium i
f^ r- f-. .-^ ,-^ --• '
I r o n ; L e a d i M a a n e s .i u m \ M - a n g a n e s e i M e r c u r y ! N i c k e l I P o t a s s i u m 1 S e l e n i u m i o 1 .L V <e r i
S o d i u m : T h a i I i u m \ V a n a d i u m ! T .; — — i
.'_ JL n c : C v a n i d e i
1 1 Ci „ 0 0 ! B i
2 . CMj 1 iJ 1 5 , 0 0 i B I
4 . 0 0 ! U i
j . i J i j I 1.
/ , i J U
f^6 . 0 0 i B i 1 . 1 0 i B 1
4 0 . CiC> '. U i 1 (••>, C ) C ) : p. I
2 1 4v.; , Oij ! U i 4 . 0 0 I U I W . ~ T , • • . . " . . '
1 ! E
4 4 5 0 , 0 0 ! U : 2 , 0 0 i U i 4 . 0 0 i U i
14,00 i-B 1 1 Cl *")(") ' i i '
clarity Betors: CLLAR
Claritv A-fter: CLEAR
B -: t
IP ; ! I '.
i ! !
p ;
Texture:
Arti-f-aci
'—/mmenr.:
IN
'.)
300962 ' 03
TNnRF 1-: 1 -H f~l'-... T - . .J . 1 •„_' J„' !-'. S r-* ...J E E E._ E__ ;
Name: CEIMIC
ab Code: CEIMIC
Matrix (soi1/water):
....,5vei ( low/med) :
"" Sol ids :
1 •oni-::en t r- ^
C o n t r a c t : ANSON
C a s e N o , ANSON >3HS N'~ „ N o ,
W.H i t r t L a b S a m o 1 s I D : <I> 0 6
P , - . •!- £-1 Pn= EI r - --1 - \ ' '=i '"< " 1 -i '--
tion Units (ua/L o r (na/ h-.i d r V we .i o in t .
i l o r B e f o r
i o r H - h r e r ;
ICAS No.
: 7429 ; 7440 1 7440 ; 7440 1 7440 i 7440 1 7440 i 7440 1 7440 ! 7440 i 7439 ! 7439 1 7439 1 7439 1 7'-4 3 9 i 7440 1 7440 1 77S2 i 7440 i 7440 i 7440 i 7440 ; 7440
i
i
-90--3^6--38---39--4 1 --43--70--47--48--50--39--92--95--96--97 -02--09--49-_•"?•"?„
^ ' ~ y ~ v .
-23-_ i-; '"7= _
-66-
— "
-0 ".IC
_"T
_"7
-9 _ -7.
_-T
-4 -8 -6 -1 -4 -5 -.6 -0 -~7
_ - ~ y
-4 -5 -0 ~ . t -
-6
! Analyte
1 Aluminum ;Antimony 1 Arsenic i E-iarium 1 Eiery 1 I ium i Cadmium 1 Calcium 1 Chromiufn i Cobalt 1 Copper i I ron 1 Lead 1 Macnesium i M-anqanese 1 Mercury INickel \ P.otassium 1 Selenium !SiIver 1 Sodium i Thai 1ium ; V-an-adium 1 Zinc i Cyanide
I... o Ti C
; i 12, 4 0 ,
4 ,
1
on
00 C'O OC*
OCi 00 OC)
CiC* OCi 00 3C! CiC) 00 2Ci OC) C'O
C'O O'C) CiO C'O C!0 C>CJ
C 1
Bl Ui
1 j •
B ! U 1 Bl Li 1 U l B l B 1 B 1
Ul Bl U l U 1 U! 1 1 '•
U 1 U ; U l Bi B i Ul
COLORLESS
COLORLESS
Clai"-ity &:e-fore: CJLEAR
Clarity After: CLEAR
W
IM
IP I i r
I P I I D I I ! ;
I P - E
IP i I C ' ;'
! !~ (
I ! t
: P I
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H E ' - t i t a c u S \
- j m m e n t . s :
'CRN I IN
300363 04
,!0F<6ANIC
L ^ ^ ^ N a m s : CE I M I C
i . .ase hio,
J G n t r -a c t : A ! l S (.J N
s o i 1 . / w a t e r ) : W A T E R m o l e I D : 0 0 .
vErl ( l-ow./med ) ; I ON
: e n t .r .a r i c n i. J n i • mq./ K. 'v w e i q h t ) : i..JO/
7 4 4 0 - 3 S - 2 7 4 4 0 - 3 9 - 3 7 4 4 0 - 4 1 - 7 7 4 4 0 - 4 3 - 9 7 4 4 0 - 7 0 - 2 7 4 4 0 - 4 7 - 3 7 4 4 0 - 4 5 3 - 4 7 4 4 0 - 5 0 - 8
7 4 3 9 - 9 2 - 1 7 4 3 9 - 9 5 - 4
7 4 3 9 - 9 6 - 5 7 4 3 9 - 9 7 - 6 7 4 4 C-'—C-' 2—C' 7 4 4 0 - 0 9 - 7
7 4 4 0 - 2 2 - 4
7 4 4 0 - 2 8 - 0 7 4 4 0 - 6 2 - 2 7 4 4 0 - 6 6 - 6
P i n a i v t e ? I C o i n c e n t r a t i o n I C
Aluminum I Antimony I Arsenic Barium • Beryl 1iumI Cadmium I
Chromium I Cobalt I Copper I I ron I Lead I MaqnesiumI M-ai-iganese I ! B e r '_ '..l B y !
Nickel ! Potassium 1 Selenium I Silver I Sodium I Thai 1ium I Vanadium I Zinc I Cvanide I
41 . I ) ! ; ; ! i
•.;• n
4 . -1 - ! ~ 7
-7 a
10 .
1 o,. 6 6 .
1 , inrin:; • - - ' • — ' = •
Cj a
• - • 3
1 ••"? J . . ; _ u
2 14Ci . 4 ,
6 . 4 4 5 0 m
u u CiO '") '"
C'Ci
i-i '-.i
'•-••Ci
CiCi
•60
- - • • - '
CiCi
0 0 0 0 0 0 (")0
H
u • - t
u
t.^
B B r i A _ '
( j
f j
u B 1 •—;
u 1 i
9 , C'Ci I B , Ci, OCi 1 U
i r-j K - {-; (za -f. B-^ I*- i;:a 1
. a r H-B-te?
COLORLESS
COLORLESS
.: i a r:
Clarity After: CLEAR
I F 1
P
IF I IP ; ! C B
T e x t u r e ;
A r t i f i
--'-^mmeniis :
300364 OS
Name: CEIMIC
ata Code: CEIMIC
!v|ui--4( 7 5 - 7 -
C a s e N o . : ANSON j H b N o , ; /L7 V-iO a Z I" r o -I 1 I a;
- 9 v e 1 ( l o w / m e d i : LOIAJ
L a b S a m e I s I D : C iCi649 —CiS:
D a t e R e c e i v e d : 1 1 .•'' 2 9 . / 9 1
" j - S o l i d s :
; o n c e n - c r a - J B s E.J ! j . o r Bmq/Kq d r v MR/!•::• R
N o , i -^ .m
I 7429—9Ci—5
i 7 4 4 0 - 3 3 - 2 I 7 4 4 C i - 3 9 - 3
! 7 '440—4^3-9 I 7 4 4 0 - 7 0 - 2 • 7 4 4 0 - 4 7 - 3 I 7 4 4 0 - 4 3 - 4 i 744Ci—5Ci—8 I 7 4 3 9 - S 9 - 6 I 7 4 3 9 - 9 2 - 1 I 7 4 3 9 - 9 5 - 4 : 7 4 3 9 - 9 6 - 5 1 7 4 3 9 - 9 7 - 6 I 744Ci-Ci2-Ci I 7 4 4 i O - C ) 9 - 7
I 7440-22-4
j 7440-23-0 :7440-62-2 17440-66-6
I H ium m u m I Antimonv i Arsenic I Barium i Beryl 1ium I Cadmium I Calcium 1 Chromium I Cobalt I CoDoer I I ron i Lead I Magnesium I Mangaunese ! M s r c v . r v iNickel 1 F-'otassium i Selenium j SiIver 1 Sodium iThailium
L- o n cent r a. t .i o n
;•;.. uu 7.90 0. 74
snadium
Cvan i de
'U H
' •J - / i.i
63 „ 7Ci 3 = 20 1 n 3 0
126Ci .0C> I---, CJ o
^J m Y O
12.50 12.30 Ci. 1 Ci
3 7 7 , OCi
1.10 783.00
0,42 2 . I Ci
U I P, '
Ul
u; U i I ; '•
Ui Ul
3 0 i U i
Color BefoB-e: BROWN
i Dior After: YELLOW
r 1 := B- -i -!- s y t) e — o r E
0 1 a r .i t V A -f t e r ;
I P B B
1 i-
I p
p
T e x t u r e ; MEDIUM
A r t i f a c t :
:immenr_s
FORM I - I N
300365 06
INORGAN: H N H B .
iN-ame ;
n r.ni-i-;^'.
M a t r i x (
CEIMIC
CEIMIC
I / ./ w<=i r e r . '
C CJ n t •'• a c t : A N S U iNi
C a s e N o . : ANSON SAS N o . :
; C I L L a b ;3amp.L(
L-.-,,,Vel t. .1 ow/,med ) : OW
ai=-: i~\
Dncentration Units (uq/L or mo/Kq dr
-„-
*"~
, - • — .
—
..,..
( ^ w —
.-.-
":.olor
..-•lor
'•-•dimmer
B
A
t
e
f
,-
fore:
ter: -
.
B
1 CAS No. i
i 7429-90-5 17440-36-0 17440-33-2 17440-39-3 17440-41-7 \7440-43-9 17440-70-2 !7440-47-3 17440-43-4 I7440-50-S !7439-S9-6 17439-92-1 17439-95-4 i 7439-96-5 17439-97-6 [ 7440'-Ci2-C) ;7440-09-7 17732-49-2 I 7440-22-4 17440-23-5 • 7-44 Ci-23-0 i 7440-62-2 i 7440-66-6
i
BROWN
YELLOW
•
Analyte iC : !
Aluminum 1 Antimonv Arsenic 1 SaB"-ium i Beryl 1ium i iCadmiufTi 1 Calcium 1 Chromiufii 1 Cobalt i Copper i I ron 1 Le^ad i Magnesium 1 Manaanese1 Mercu.ry 1 Nickel 1 Potassium i Selenium 1 Silver i Sodiium 1 Thallium 1 Vanadiu.m i Zinc i Cyanide i
Claritv
Clarity
3ncentration
S 1 1 , CiCi S. 60 Ci. S O 2 , 7Ci (-•. "7 - 7
0.77 •3Ci, CiCi 3 . 40 1 . 90
7 i")
1 96Ci 3 CiCi 2,10
28 , 50 25 . 40
C i . 1 1 2 . 30
409 ,00 0 = 91 1 , 1 Ci
8 5 1 , CiCi
0 .46 2 , 30 2 ., 50 '7 3 C)
Before:
After:
B
C 1
U i Pr !
-0 1
B 1 ! i !
B i
Ui B i
B 1
i..JI Ui Ul Ui Ui Ul Li 1 Bl Bi t j \
1
(--,
*
i.'Vi
IM 1
i F"' i i F' ! 1 F i ! C- '•
i P i • -P '
1P i IF' i IP 1 ! ?~ !
1 P i I F i I P i ; F'
ICV;
B i " B
1 P i
1 F i
IP 1 1 P i I C" '
1 P i
i .-• !
1 1
T 3 ;i
Art
l-R
a t e F s s c e i v e d : 1
w.eiq n't
FORM I
4 )
300366 07
M •a m e : C £ IMIC
i sb Code; CEIMIC
Matri;•; ( soil /vsater ) : SCI
i-,; Vel (low/med ) ; L0W
1 INORGANIC ANALYSIS DATA SHEE'
ANSON 1W-6
a s *=" No,
'r^ Sol ids
D n c e n t r a t i o n Units ( u q / i_ a r m q / K q d
; oLLl NO . ;
Lab Sample ID: OOi
Liate iReceived ; 11.-'
weiqht): MG/KB
B™ H 1 1 '
• 49-1 OS
•
1 CAS No .,
1 7 4 2 9 - 9 0 - 5 1 7 4 4 C i - 3 . 6 - 0 1 7 4 4 0 - 3 8 - 2 i 7 4 4 0 - 3 9 - 3 1 7 4 4 0 - 4 1 - 7 1 7 4 4 0 - 4 3 - 9 i 7 4 4 0 - 7 0 - 2 ; 7 4 4 0 - 4 7 - 3 1 7 4 4 0 - 4 3 - 4 1 7 4 4 C ) - 5 C ! - 3 1 7 4 3 9 - 8 9 - 6 1 7 4 3 9 - 9 2 - 1 1 7 4 3 9 - 9 5 - 4 1 7 4 3 9 - 9 6 - 5 i 7 4 3 9 - 9 7 - 6 1 744C!—Ci2-Ci 1 7 4 4 0 - 0 9 - 7
1 7 7 8 2 - 4 9 - 2 1 7 4 4 0 - 2 2 - 4 1 7 4 4 0 - 2 3 - 5 1 7 4 4 0 - 2 8 - 0 1 7 4 4 0 - 6 2 - 2 1 7 4 4 0 - 6 6 - 6
1 A n a l y t e I f
1 A l u m i n u m i 1 A n t i m o n v 1 i A r s e n i c i i B a r i u m 1 1 B^ery 1 i i u m i iC^admium 1 1 C a l c i u m 1 1 Ch i ' -omium 1 I C o b a l t 1 i i C o P D e r i i I r o n ! I L e a d 1 1 M a q n e s i u m 1 1 i ' i a n o a n e s e i I M e r c L i r y 1 i N i c k e l 1 i P o t a s s i L i m 1 1 S e l e n i u m 1 I S i l v e r i 1 S o d i u m i 1 T h a i l i u m i i V a n a d i u m i I Z i n c 1 1 C y a n i d e 1
j . o n c e n t r a t i ^ o n
5 1 5 , 0 0 9 , 8 0 0 . 8 5 2 . 2 0 1 , 10 0 , 3 7
3 3 , 7 0 3 . 7 0 2 , 2 0 2 . CiCi
1 3 6 0 . 0 0 1 , .3Ci
3 4 . 6 0 1 4 , 8 0
Ci. 1 Ci 2 . 6 0
4 6 5 , 0 0 0 . 3 9 1 , 3 0
9 6 7 , CiCi 0 . 4 4 2 . 4 0 1 , 7 0 2 . 1 Ci
U B B
U B
u g
B
u u u u u u u B B
u
• I < I
Q iM i • i
\ F 1 ; c 1 < 1 1
! !~ 1
i P ; i P 1 IP I IP 1 i P i i p 1 IP i
* i p 1 I F 1 IP 1 IP 1 iCV 1 ! P 1 i P 1
W I F 1 IP i IP i I CT J
IP 1 IP i
• i
Dolor Before: BROWN
.t..p 1Qr After: YELLOW
'"3mmen 15 :
Clarity Before:
Clarity After;
Texture;
Artif-acts
ivi p B-. T i i |-,-|
'ORM I - IN
300367 •^ 08
SAMP f^ C--"'' £-• Q i-i — p "r
MW- .1. u ^iame : C o n t r a c t : ANSON
C a s e N o . : ANSON SAS N o . : B •. B~ I - , - ^ r-B •—, " B ' _ i rB B " E. •• LJ w !._' q ' - - ' a '.-^ ' . - . .1. '. B I ' _ •
M a t r i ;•; ( s o i 1 / w •a t e r ) : •S 011
^•.,^vel ( i o w / m e d ) ; LOW
• ' • - S o l i d s : 8 7 , 1
C o n c e n t r a t . i o n U n i t s (uc!.^''L o r mq. /Kq d r y w e i g h t ) : MO./KB
L a b S a m p l e I D : OOi
D a t e R e c e i v e d : 1 1 /
4 9 - 0 1
2 1 / 9 1
I "7 ''I 4 f i — 7 hi—7
I 7 4 4 0 - 3 9 - 3 I 7 4 4 0 - 4 1 - 7 i 7 4 4 0 - 4 3 - 9 ! 7 4 4 C i - 7 C i - 2 i 7 4 4 0 - 4 7 - 3 i 7 4 4 0 - 4 3 - 4 ; 744Ci—5Ci—8 ' 7 ' ' ' .39 —89—1^,
1 7 4 3 9 - 9 2 - 1 I 7 4 3 9 - 9 5 - 4
I 7439—97—B^
I 7 4 4 0 - 0 9 - 7 i 7 7 8 2 - 4 9 - 2 ; 7 4 4 0 - 2 2 - 4
I 7 4 4 0 - 2 S - 0
1 7 4 4 C i ~ 6 6 - 6
C o l o r B e f o r e : BROWN
i__) lo r A f t e r : YELLOW
P - i m m e n t s :
An .a 1 y t e i CBOTI C e n t r a t i o n
AlLiminum 1
Antimonv i Arsenic i Bariu.BTi i
Beryl liLun i
Cad (Tl ium 1
Calcium 1 Chromium i
Cobalt 1 Copper 1 I ron i
Lead 1
Maa.nesium 1 Manqanese i
Me re Li rv 1 N i ck e1 i
Potassium i
Selenium i Silver i
.S.odium 1
Thailium 1
Vanadium 1 Zinc 1
Cyanide 1
5
14
7
7
1.3
! 0 • ^ '
0 0
31 Ti
1
1
50
0 26 8 (j
2 69
0 1
68 0
1 • ~ ^
•B I
, OCi
. 30
.44 , SO
,52 ,69
. 10
. 10
,70
. 70
, 00 ,80
,30 . 10
,09 .10
. CiC' •7 -i
, CiCi
. 0C>
.35
, 90
, SO
,50
i C L a r i t y B e f o r e ;
C l a r i t y A f t e r :
:v
F P p
C P P F P P F
p
T e ;•; t u r e ;
A r t i f a c t s ;
. i J ± '-J B !
c n p r.i T •ORr
300368
0^* 09
INORGANIC ANALYSIS DATA SHEET
Mi.i.... -r p . .' B -;,,•••,_.. 1 -,--T, -1 B
:£IMir
1 /w^ateB"-)
trac •I- . .••M\ic:;|-f^,i
K-.,? "'e.;. !. low.-'miea.i :
C a s e !Mo, : ANSC'N
SOIL
LOW
8Ci, 7
Concentration '..Jnits (ug/L or mg/Kg dry weight): MG/KG
Lab S'ampl.e ID: 0Ci649-C>3S
Date Received: 11/22/91
.-•HH N o .
7429-•7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-_ — .
-90-—•-< 0 -
-38--39--41--43--70--47--43--50--39--92--95--96--97--02--09--49-_oo.
- •" 7 -
-23--62--66-* " " * " " • " "
„c::
-Ci ~2 _;T
-7 -9 ~.ii!
-"
-4 -8 -6 -1 -4 -5 -6 -Ci -~7
"2 -.4
"••-J
-Ci _ • - • >
-6 "**"*""
AIuminLim Antimony AE"-ssnic Bar iu.m Bervl 1 iu.m CadmiLim Calciij.m Chromiu.m Cobalt Copper I ron Lead MagnesiLim Man0anese Mercurv Nickel Potassium SeleniLim SiIver Sodium Thailium Vanadiu.m Zinc Cyanide
H n a 1 V -i- f jncen t; a tion
OS , 00 3. 1 Ci
Ci, 63
2 , 2Ci
0.54 0,72
24,40 1 ,40 .L a W'J
2.20 36 ,00 1 .30 7, .50
12 ,60 0 , 1 1
34. OCi 0, S3 1 . 1 Ci
99,00 Ci. 41
1 .60 1 ,30 2 , o<:)
Cl
J i
Ul Bl Bi Bl Ul Bl Bl Ui Bi
1
1
Bl i
Ul Ul Ul Ul Ul Ui Ui Bi B 1 Ul
1
.•olor Before: BROWN
L-v lor After: YELLOW
Dmments;
Clarity Before;
Claritv After:
Q
W
p,
F'
c E
P P P o B
p P P F
h
P P F o B
P c
Texture: MEDIUM
Artifacts:
FORM IN
• t
.300369 "" 10
-r;-. B B", C ' E'.-. A B- ,i T E~ A K i A I V' '--- r'—• r-' /'•-. - " /-•. ,:::: i.
MW- I \ a ' : . ' — <Z'y.i
N a m e ; C
I D B . n n f^ : 1.
i ' la.tr .i X ( s o i
. e v e l ( low..-
S o l i d s
'EIMIC
;E IMIC
. 1 /w-ater ) :
'med ) :
C.ase
SOIL
i_,OW
No. • ANSO
in t r a c t : ANSON
SAS No„ : iU N o ,
1 h P. :a m i-j 1 s a m p l e i i j : OCiCj49~OG
.D a t e F\ e c e i v e d : 11./ 2 '6./ 91
C o n c e n t r . a t i c m i J n i t s ' I .-. ^ mg/Kg d r y w e i g h t ) : MG/KG
^
p
Color IBefore:
Color After:
Comm.ents:
1
iCAS No.
17429-90-5 17440-36-0 :7440-38-2 17440-39-3 17440-41-7 17440-43-9 .17440-70-2 i 7440-47-3 17440-4S-4 17440-50-8 i 7439-39-6 17439-92-1 17439-95-4 i 7439-96-5 17439-97-6 i 7440-02-0 ;7440-09-7 i 7782-4-9-2 17440-22-4 i 7440-23-5 17440-28-0 17440-62-2 17440-66-6
BROWN
YELLOW
B
Analyte 1 Con
Aluminum 1 Antiiiionv i Arsenic i BariLim i Beryl lii-im ! Cadmium 1 CalciLim 1 Chromium 1 Cobalt 1 Copper i I ron 1 Lead 1 Maqnesium1 Manqanese i Mercury 1 Nickel 1 F'otassium 1 Selenium i Silver 1 Sod iu.m 1 Thallium 1 Vanadiu.m 1 Zinc i Cyanide i
Clarity B
c
e
Clarity Af
FORM I
entration
717.00 3 , 9Ci 0.53 3. 1 Ci 0,59 0 , 79
•3C!, 5Ci 2.60 2 . OCi 2, 40
1540,00 1 . 1 0
19.70 21 ,20 0.12 2.40
421.00 0.34 1 ,20
876,00 O , 47 2.20 2 = 2Ci 2.60
fore:
ter:
- IN
c
u B B B u B
U B
B
u U U U u u u B B U
Q
*
W
B B
W 1 ! B B
B B
P 1
P 1 F 1 P 1 P 1 P 1 P 1 P 1 P 1 P 1 P ]
F I P 1 P 1 CV 1 P i P 1 F 1 P 1 P 1 F i P 1 P 1 C 1
1 i
Ts/< ture;
.Artifacts:
7
MED
-'88
aoosTO / ' • t t
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
m b Name: INTECH Lab Code: INTECH
59-61' Contract: 68-D9-0048
Case No.: 42-64 SAS No.: SDG J o. : ANSON
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Leve1: (1ow/med) LOW
% Moisture: not dec. 13.
Column: (pack/cap) PACK
CAS NO.
Lab Sample ID: If/|/< 2--'
(g/mL) G Lab File ID: C9759
Date Received: 11/21/91
Date Analyzed: 11/27/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q COMPOUND
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform
107-06-2- 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochlorometharie 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6- 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5— 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene
1330-20-7 Xylene (total)
11. 11. 11. 11. 6.
13. 6. 6. 6. 6. 6. 6.
11. 6. 6.
11. 6. 6. 6. 6. 6. 6. 6. 6. 6.
11. 11. 6. 6. 6. 6. 6. 6. 6.
U U U U B B U U U U U U U U U U U U U u U U U U U u u u u u u u u u
FORM I VOA 1 /87 Rev .
19 3003*rt
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
m b Name: INTECH ab Code: INTECH Case No.
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 13.
Column: (pack/cap) PACK
Number TICs found: 0
59-61' Contract: 68-D9-0048
42-64 SAS No.: SDG No. ANSON
Lab Sample ID: T l ( l ( ' t ^ - /
Lab File ID: C9759
Date Received: 11/21/91
Date Analyzed: 11/27/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER
1. 2. 3. 4. 5. 6. 7. 8.
L ^• 110. "ll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22, 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1/87 Rev .
20 300372
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
^ P D Name: INTECH
Lab Code: INTECH Case No.
Matrix: (soil/water) WATER
Sample wt/vol: 5.0
Level: (low/med) LOW
,3 Moisture: not dec. 100.
.„Column: (pack/cap) PACK
F-BLANK Contract: 68-D9-0048
42-64-85SAS No.: SDG .No.: ANSON
Lab Sample ID: J H f l ^ l - - ^
CAS NO.
(g/mL) ML Lab File ID: A6395
Date Received: 11/21/91
Date Analyzed: 11/30/91
Dilution Factor: l.OO
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q COMPOUND
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-3 5-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dlchloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-4 3-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-b Styrene 1330-20-7 Xylene (total)
10. 10. 10. 10. 3. 9. 5. 5. 5. 5. 16. 5.
10. 5. 5. 10. 5. 5. 5. 5. 5. 5. 5. 5. 5. 10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U BJ J U U U U
U U U U U U U U U U U U U U U U U U u u u u u
FORM I VOA 1 /87 Rev .
25 300373
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Contract: 68-D9-0048
EPA SAMPLE NO.
^ ^ b Name: INTECH
^ E b Code: INTECH Case No.: 42-64-85SAS No.
^-Matrix: (soil/water) WATER
— Sample wt/vol: 5.0 (g/mL) ML
"Level: (low/med) LOW
~~% Moisture: not dec. 100.
Column: (pack/cap) PACK
F-BLANK
: SDG No.: ANSON
Lab Sample ID: J Z/Zf '^
Lab File ID: A6395
Date Received: 11/21/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
Number TICs found: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 2. 3. 4. 5. 6. 7. 8.
t 9. |io. rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1 /87 R e v .
26 300374
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
b Name: INTECH
Lab Code: INTECH Case No
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 23.
Column: (pack/cap) PACK
Contract: 68-D9-0048
. : 42-64 SAS No.: SDGJ^o.: ANSON
Lab Sample ID: J ' / l / t ^ l - ^
(g/mL) G Lab File ID: C9760
Date Received: 11/21/91
Date Analyzed: 11/27/91
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1.00
Q
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform
107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyi-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene
1330-20-7 Xylene (total)
13. 13. 13. 13. 7.
110. 6. 6. 6. 6. 6. 6.
13. 6. 6.
13. 6. 6. 6. 6. 6. 6. 6. 6. 6.
13. 13. 6. 6. 6. 6. 6. 6. 6.
U U u u B B U U U U U U U u u u u u u u u u u u u u u u u u u u u u
m FORM I VOA
32 1/87 Rev.
300375
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
120-122' ^iab Name: INTECH Contract: 68-D9-0048
^Piab Code: INTECH Case No.: 42-64 SAS No.: SDG No
i;:; Matrix: (soil/water) SOIL
(g/mL) G Lab File ID: C9760
Date Received: 11/21/91
Date Analyzed: 11/27/91
ANSON
Lab Sample ID: r////f -V
^Sample wt/vol: 5.0
«Level: (low/med) LOW
- % Moisture: not dec. 23.
-"Column: (pack/cap) PACK
Number TICs found:
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 . 0 0
-
,-.-
.....
1
—
„,.
—
•c-.--.
CAS NUMBER ================
1. 2. 3. 4. 5. 6. 7. 8. 9.
k 10. Pll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC.
II II II lO
II it
FORM I VOA-TIC 1 /87 Rev .
33 300376
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Contract: 68-D9-0048 F-BLANK
fPk Name: INTECH
; Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON
_ Matrix: (soil/water) WATER Lab Sample ID: j : \ l ( ( ^ l - 9
.,5ample wt/vol: 5.0
-Level: (low/med) LOW
-* Moisture: not dec. lOO.
-Column: (pack/cap) PACK
CAS NO.
(g/mL) ML Lab File ID: A6396
Date Received: 11/21/91
Date Analyzed: 11/30/91
Dilution Factor: l.OO
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q COMPOUND
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 12 4-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-4 3-2 Benzene
1UU61-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene i 00-41-4 Ethylbenzene iuu-4 2-b Styrene
1J30-20-7 Xylene (total)
10. 10. 10. 10. 3.
14. 5. 5. 5. 5.
13. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U BJ
U U U U
U U U U U U U U U U U U U U U U U U
u u u u u
FORM I VOA 1 /87 Rev .
38 360377
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Contract: 68-D9-0048
EPA SAMPLE NO.
F-BLANK b Name: INTECH
&b Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON
Matrix: (soil/water) WATER Lab Sample ID: 3:///4/-5
"Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
- Number TICs found: 0
(g/mL) ML Lab File ID: A6396
Date Received: 11/21/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 2. 3. 4. 5. 6. 7. 8.
k ^• |io. rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 2b. 26.
28. 29. 30.
COMPOUND NAME RT EST. CONC.
.
Q
1
FORM I VOA-TIC 1 /87 Rev.
39 300378
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
T-BLANK Fb Name: INTECH Contract: 68-D9-0048
Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON
_.Matrix: (soil/water) WATER Lab Sample ID: j n i i ^ l - ( ?
-Sample wt/vol: 5.0 (g/mL) ML
—Level: (low/med) LOW
—% Moisture: not dec. 100.
—Column: (pack/cap) PACK
CAS NO. COMPOUND
Lab File ID: A6397
Date Received: 11/21/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 7 5-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-!>entanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total)
10. 10. 10. 10. 3. 10. 5. 5. 5. 5. 5. 5. 10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U BJ U U U U U U U U U U U U U U U U U U U U U U U u u u u u u
FORM I VOA 1/87 Rev.
45 300379
«
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Contract: 68-D9-0048
EPA SAMPLE NO.
T-BLANK b Name: INTECH
ab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON
Matrix: (soil/water) WATER Lab Sample ID: Ju((¥i -6
"Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
Number TICs found: 0
(g/mL) ML Lab File ID: A6397
Date Received: 11/21/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 2. 3. 4. 5. 6. 7. 8.
k • iio. ^11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME ============================
RT EST. CONC. Q
FORM I VOA-TIC 1 /87 Rev .
46 300380
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
^ ^ b Name: INTECH
Lab Code: INTECH Case No.: 42-64
Matrix: (soil/water) SOIL
._ Sample wt/vol: 5.0
_ Level: (low/med) LOW
.,..„% Moisture: not dec. 52.
— Column: (pack/cap) PACK
60-62' Contract: 68-D9-0048
SAS No.: SDG.No.: ANSON
Lab Sample ID: J l ( / U ^ ^ (
(g/mL) G Lab File ID: C9761
Date Received: 11/26/91
Date Analyzed: 11/27/91
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1.00
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform
107-06-2 1, 2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 ^Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 • cis-l,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-I»entanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene
1330-20-7 Xylene (total)
21. 21. 21. 21. 14. 54. 10. 10. 10. 10. 10. 10. 21. 10. 10. 21. 10. 10. 10. 10. 10. 10. 10. 10. 10. 21. 21. 10. 10. 10. 10. 10. 10. 10.
u u u u B B U U U U U U U u u u u u u u u u u u u u u u u u u u u u
FORM I VOA 1/87 Rev .
50 300381
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
•
b Name: INTECH
b Code: INTECH Case No.: 42-64
- Matrix: (soil/water) SOIL
"Sample wt/vol: 5.0
"Level: (low/med) LOW
"% Moisture: not dec. 52.
Column: (pack/cap) PACK
.. Number TICs found: 0
60-62' Contract: 68-D9-0048
SAS No.: SDG No.: ANSON
Lab Sample ID: X^///^^~f
(g/mL) G Lab File ID: C9761
Date Received: 11/26/91
Date Analyzed: 11/27/91
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 . 0 0
CAS NUMBER
1. 2. 3. 4. 5. 6. 7. 8.
fe. • •LO.
rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25.
27. 28. 29. 30.
COMPOUND NAME
,
RT EST. CONC. Q
FORM I VOA-TIC 1 /87 Rev .
51 300382
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
^ ^ Name: INTECH
Lab Code: INTECH
75-77' Contract: 68-D9-0048
Case No.: 42-64 SAS No.: SDG Ho.: ANSON
Matrix: (soil/water) SOIL
..Sample wt/vol: 5.0
,._Level: (low/med) LOW
.=.% Moisture: not dec. 23.
--Column: (pack/cap) PACK
(g/mL) G
CAS NO. COMPOUND
Lab Sample ID: JTZ/Z/^f"'^
Lab File ID: C9762
Date Received: 11/26/91
Date Analyzed: 11/27/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride
108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 12 4-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-4 3-2 ' Benzene
10061-02-6 trans-1,3-Dichloropropene 7 5-25-2 Bromof orm 108-10-1 4-Methyl-2-f'entanone 591-78-6 2-Hexanone 127-18-4— Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4—-• Ethylbenzene 100-4 2-5 styrene 1330-20-7 Xylene (total)
13. 13. 13. 13. 7.
39. 6. 6. 6. 6. 6. 6.
13. 6. 6.
13. 6. 6. 6. 6. 6. 6. 6. 6. 6.
13. 13. 6. 6. 6. 6. 6. 6. 6.
U U u u B B U U U U U U U U U u U U U U U U u u u u u u u u u u u u
FORM I VOA 1/87 Rev.
56 300383
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
«
b Name: INTECH
ab Code: INTECH Case No.: 42-64
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 23.
Column: (pack/cap) PACK
Number TICs found: 0
75-77 ' C o n t r a c t : 6 8 - D 9 - 0 0 4 8
SAS N o . : SDG N o . : ANSON
L a b S a m p l e I D : J f i l l ^ ^ - 1
(g /mL) G L a b F i l e I D : C9762
Date Received: 11/26/91
Date Analyzed: 11/27/91
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 . 0 0
CAS NUMBER
1. 2. 3. 4. 5. 6. 7. 8.
k • |io. ^11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22, 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
.
FORM I VOA-TIC 1 /87 Rev .
57 300384
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
Contract: 68-D9-0048
EPA SAMPLE NO,
F-BLANK b Name: INTECH
Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON
Matrix: (soil/water) WATER Lab Sample ID: J|/// f-3
Sample wt/vol: 5,0
Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
(g/mL) ML
CAS NO, COMPOUND
Lab File ID: A6398
Date Received: 11/26/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
-~
--,
• ~ '
m I P
,,.-
^ .
-—
' • " • • •
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane
540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform
107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 1U8-10-1 4-Methyl-2-Pentanone b9i-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane
108-88-3 Toluene 1U8-90-7 Chlorobenzene iuo-41-4 ——Ethylbenzene 100-4 2-5 Styrene 1330-20-7 Xylene (total)
10. 10. 10. 10. 3.
41. 5. 5. 5. 5.
12. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U BJ
U U U U
U U U U U U U U U U U U U U U U U U
u u u u u
FORM I VOA 1 /87 Rev .
g2 300385
«
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Contract: 68-D9-0048
EPA SAMPLE NO.
F-BLANK b Name: INTECH
'ab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON
Matrix: (soil/water) WATER Lab Sample ID: S U H ^ ^ - 1
-Sample wt/vol: 5.0
'Level: (low/med) LOW
"% Moisture: not dec. 100.
"Column: (pack/cap) PACK
„ Number TICs found: 0
(g/mL) ML Lab File ID: A6398
Date Received: 11/2 6/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 2. 3. 4. 5. 6. 7. 8.
i. ^• IlO. rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
•
FORM I VOA-TIC 1/87 Rev .
30038G
63
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
T-BLANK pb Name: INTECH Contract: 68-D9-0048
Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON
Matrix: (soil/water) WATER Lab Sample ID: J U l f y t ' 9
Sample wt/vol: 5.0
Leve1: (1ow/med) LOW
,% Moisture: not dec. 100.
^Column: (pack/cap) PACK
CAS NO.
(g/mL) ML Lab File ID: A6399
Date Received: 11/26/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q COMPOUND
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethehe 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochlorometharie 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-5>entanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene 1330-20-7 Xylene (total)
10. 10. 10. 10. 3.
38. 5. 5. 5. 5. 5. 5.
10. 5. 5. 10. 5. 5. 5. 5. 5. 5. 5. 5. 5. 10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U BJ
U U U U U U U U U U U U U U U U U U U U U U U u u u u u
FORM I VOA 1 /87 Rev.
69 300387
«
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Contract: 68-D9-0048
EPA SAMPLE NO.
T-BLANK b Name: INTECH
ab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON
Matrix: (soil/water) WATER Lab Sample ID: J{( ( (bk- f
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
, Number TICs found: 0
(g/mL) ML Lab File ID: A6399
Date Received: 11/26/91
Date Analyzed: 11/30/91
Dilution Factor: l.OO
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 2. 3. 4. 5. 6. 7. 8.
k. 9-• 10. Fii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME _-
RT EST. CONC. Q
FORM I VOA-TIC 1 /87 Rev .
70 3003Q8
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
#
60-62' b Name: INTECH Contract: 68-D9-0048
Lab Code: INTECH Case No.: 11185 SAS No.: SDG No
Matrix: (soil/water) SOIL
(g/mL) G Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 23.
Column: (pack/cap) PACK
CAS NO. COMPOUND
ANSON
Lab Sample ID: J U I l ^ ^ ' l
Lab File ID: C9877
Date Received: 11/27/91
Date Analyzed: 12/10/91
Dilution Factor: l.OO
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichlor6ethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm 108-10-1 4-Methyl-2-&entanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 styrene 1330-20-7 Xylene (total)
13. 13. 13. 13. 7.
26. 6. 6. 6. 6. 6. 6.
13. 6. 6.
13. 6. 6. 6. 6. 6. 6. 6. 6. 6.
13. 13. 6. 6. 6. 6. 6. 6. 6.
U U U U B B U U U U U U U U U U U U U U U u u u u u u u u u u u u u
FORM I VOA 1/87 Rev.
75 300389
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
^ ^ b Name: INTECH
^ R b Code: INTECH Case No.: 11185
"'••Matrix: (soil/water) SOIL
—Sample wt/vol: 5.0 (g/mL)
'' Leve1: (1ow/med) LOW
*"% Moisture: not dec. 23.
"column: (pack/cap) PACK
-._ Number TICs found: 0
60-62' Contract: 68-D9-0048
SAS No.: SDG No.: ANSON
Lab Sample ID: T(HI^9-\
G Lab File ID: C9877
Date Received: 11/27/91
Date Analyzed: 12/10/91
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 . 0 0
CAS NUMBER
1. 2. 3, 4. 5. 6. 7. 8. 9.
110. Fll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 2b. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1 /87 Rev .
76 300390
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
:.ab Nane: INTECH
Lab Code: INTECH Case No.
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
L,evel: (low/med) LOW
% Moisture: not dec. 18.
rolumn: (pack/cap) PACK
74-76' Contract: 68-D9-0048
11185 SAS No.: SDG No.: ANSON
Lab Sample ID: XUllBf-'^^
Lab File ID: C9878
Date Received: 11/27/91
Date Analyzed: 12/10/91
CAS NO, COMPOUND
Dilution Factor:
CONCENTRATION tJNITS: (ug/L or ug/Kg) UG/KG
1 . 0 0
Q
7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-35-4 1,1-Dichloroethene 7 5-34-3 1,1-Dichloroethane 54 0-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform
107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-4 3-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7 -18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 -Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene iuu-4 2-b Styrene
1330-20-7 Xylene (total)
12. 12. 12. 12. 6.
11. 6. 6. ' 6. 6. 6. 6.
12. 6. 6.
12. 6. 6. 6. 6. 6. 6. 6. 6. 6.
12. 12. 6. 6. 6. 6. 6.
1:
u u u u B BJ U U U U U U U U U U U u u u u u u u u u u u u u u u u u
FORM I VOA 1 /87 R e v .
300391 81
m IE
VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Name: INTECH
::.:jab Code: INTECH
74-76' Contract: 68-D9-0048
Case No.: 11185 SAS No.: SDG No.: ANSON
-Matrix: (soil/water) SOIL
•Sample wt/vol: 5.0
-jevel: (low/med) LOW
"% Moisture: not dec. 18.
"Column: (pack/cap) PACK
Number TICs found: 0
Lab Sample ID: J/Z/Z f-Z
(g/mL) G Lab File ID: C9878
Date Received: 11/27/91
Date Analyzed: 12/10/91
Dilution Factor: l.OO
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER
1. 2. 3. 4. 5. 6. 7,
^ 8 .
P9. • 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 2b. 26. 27.
29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1 /87 Rev .
300392 82
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
F-BLANK Lab Name: INTECH Contract: 68-D9-0048
Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No
Matrix: (soil/water) WATER
ANSON
Lab Sample ID: J Ull^^-^
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 100.
polumn: (pack/cap) PACK
CAS NO.
(g/mL) ML Lab File ID: A6403
Date Received: 11/27/91
Date Analyzed: 12/ 2/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q COMPOUND
74-87-3 Chloromethane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 7 5-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform
107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 7 9-00-5 1,1,2-Trichloroethane 71-4 3-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene /9-34-b 1,1, 2, 2-Tetrachloroethane
108-8 8-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene lOO-42-b Styrene
1330-20-7 Xylene (total)
10. 10. 10. 10. 4. 7. 5. 5. 5. 5.
17. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U u u u BJ J
U U U U
U u u u u u u u u u u u u u u u u u u u u u u
FORM I VOA 1/87 Rev.
300 393^ 87
^Sb
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
lb Name: INTECH
•U.ab Code: INTECH Case No.: 42-64-85SAS No
-Matrix: (soil/water) WATER
"•Sample wt/vol: 5.0
-'-Bevel: (low/med) LOW
"% Moisture: not dec. 100.
~:olumn: (pack/cap) PACK
F-BLANK
(g/mL) ML
Contract: 68-D9-0048
SDG No.: ANSON
Lab Sample ID: Xltil$^~'^
Lab File ID: A6403
Date Received: 11/27/91
Date Analyzed: 12/ 2/91
Dilution Factor: 1.00
Number TICs found; CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
]
CAS NUMBER
1. 2. 3 . 4 . 5. 6.
fc.^-^ 8 . W s . • 10. 11. 12, 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT =======:=
EST. CONC. Q
FORM I VOA-TIC 1 /87 Rev .
300394 88
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
Contract: 68-D9-0048
EPA SAMPLE NO.
T-BLANK ab Name: INTECH
"Lab Code: INTECH Case No.: 42-64-85SAS No.: SDG No.: ANSON
Matrix: (soil/water) WATER Lab Sample ID: Z K l ^ P ' ^
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
CAS NO,
(g/mL) ML Lab File ID: A6404
Date Received: 11/27/91
Date Analyzed: 12/ 2/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q COMPOUND
74-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform
107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 7 5-25-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene
1330-20-7 Xylene (total)
10. 10. 10. 10. 4. 3. 5. 5. 5. 5. 5. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U BJ J
U U U U U U U u u u u u u u u u u u u u u u u u u u u u
FORM I VOA
94
1/87 Rev.
300395
^ib
IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Name: INTECH
Lab Code: INTECH Case No.
" atrix: (soil/water) WATER
'Sample wt/vol: 5.0
"Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
Number TICs found: 0
T-BLANK Contract: 68-D9-0048
42-64-85SAS No.: SDG No.: ANSON
Lab Sample ID: XKI^^S' '
(g/mL) ML Lab File ID: A6404
Date Received: 11/27/91
Date Analyzed: 12/ 2/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 2. 3. 4. 5. 6.
^ V. \ % . P 9 . • 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27.
29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1 /87 R e v .
95 300396
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I 1111142-02
ab Name: INTECH Contract: 68-D9-0048 i
Lab Code: INTECH Case No.:fl-^V-^r SAS No.: SDG No. :/^/<?/
«.a t r 1 X : [soil /water] SOIL
^•ample wt/vol: 30.10 [g/mL] G
Level: [low/med] LOU)
Moisture: />-oTdec. j" eitc • O
Extraction: [SepF/Cont/Sonc] SONC
.OC Cleanup: [Y/N] N pH: 7.5
Lab Sample ID: ff-^J'^
Lab File ID: >BeO30
^ Date Received: IQ'^S 1/91
Date Extracted% #1/25/91
Date Analyzed: 11/30/91
Dilution Factor: \ • \fi
CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108-111-95-
541-106-100-95-95-
108-106-621-67-98-78-88-
105-65-
111-120-120-91-
106-87-59-91-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-•68-3-•50-7-•57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-
-Phenol -bis(2-cl^lo^oetl^yl )ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene - B e n z y l a Icolno 1 -1,2-Dichlorobenzene -2-Methylphenol -bis(2-chloroisopropyl)ether -3&4-MethyIpheno1 -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene -1 sophorone -2-Ni t ropheno1 -2,4-Dimethyl phenol - B e n z o i c acicJ -bis(2-Chloroethoxy)methane -2,4-Dichlorophenol -1,2,4-Tr ichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methylnaphthalene -HexachlorocyclopentacJiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan i1ine -Dimethylphthalate -Acenaphthylene -2,6-Dinitrotoluene
Q
1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 i 380 1 380 1 380 1 380 1 380 1 380 1 1900 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 380 1 360 1 360 1 1900 1 380 1 380 1 . 380
1 i lU 1 lU 1 lU 1 iU 1 lU 1 IU i IU 1 iU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 iU 1 IU 1 IU i IU 1 IU 1 IU 1 iU 1 IU 1 1 r l 3b03S^
FORM I S U - 1 187
IC 5EMI VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I 1111142-02 ab Na-^e: INTECH
„ab Cod?: INTECH Case No.
iatrix: [soil/water] SOIL
Contract: 68-09-0048 I
: ( f l ^ l f ( ( ^ , ^ rS f^S No.: SDG No.: ' ^ ^ / ^ ' ^
lample ut'-vol: 30.10 [g/mL] G
Level: [low/med] LOW
, Moisture: fiat d e c . 0 f t l - |3
Extraction: [SepF/Cont/Sonc] SONC
-PC Cleanup: [Y/N] N pH: 7.5
Lab Sample ID: t^^- (*Y
Lab File ID: >B8030
Date Received: 11/21/91
Date Extracted: 11/25/91
Date Analyzed: 11/30/91
Dilution Factor: \ . 00
CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
99-83-51-
100-132-121-84-
7005-86-
100-534-86-
101-118-87-85-
120-84-
206-129-85-91-56-
218-117-117-205-207-50-
193-53-
191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-•01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-
-3-Ni t roan i1ine -Acenaphthene • 2 , 4 - D i n i t r o p h e n o l - 4 - N i t r o p h e n o 1 •Dibenzofuran -2,4-Dinitrotoluene -Diethylphthalate -4-Chlorophenyl-phenylether -Fluorene -4-Ni t roan i1ine -4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenan threne -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -Butylbenzylphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene -Benzo(g,h,i)perylene
Q
1 1900 1 380 1 380 1 1900 1 380 1 380 1 380 1 380 1 380 1 1900 1 1900 1 380 1 380 1 380 1 1900 1 380 1 380 1 380 1 380 1 380 1 380 1 76 0 1 380 1 380 1 180 1 380 i 380 t 380 1 380 1 360 1 380 1 380
I iU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I : IU IU IU IU IU IU IU I
FORM I SU-2 188
300398
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
tab Name: INTECH
..atrix: f. soil/water) SOIL
-Cample wt-^vol: 30.10 (g/mL) G
Level: (low/med) LOU)
Moisture: /Widec . |' . ied • 1}
Extraction: (SepF/Cont/Sonc) SONC
PC Cleanup: (Y/N) N pH: 7.5
Number TICs found: 1
Contract: 68-D9-0048
EPA SAMPLE NO,
I 1111142-02 I
/ Lab Sample ID: ^^"^3
Lab File ID: >Be030
Date Received: ;iyi/211/9
Date Extracted: 11/25/91
Date Analyzed: 11/30/91
Dilution Factor: | •00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER : = = = = = = s=r = B a
1.
COMPOUND NAME
Unknown
RT E B ^ ^ C3 e
2 . 2 5
EST. CONC.
1 5 0 .
Q
FORM I S U - T I C
189 1/87 Rev.
300399
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111142-03 '~3b Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case No. : 4*'tV^^^ SAS No.: SDG No.: /^^/^/^
atrix: [soil/water] UJATER
Sample wt/vol: 1000 [g/mLl ML
s^evel: [low/med] LOU)
""Moisture: dec 100.
Extraction: [SepF/Cont/Sonc] SERF
=C Cleanup: [Y/N] N pH: 8.0
Lab Sample ID: f - S ^ / ^ l ^
Lab File ID: >B8027
Date Receieved:'^ll'^^l^^l
Date Extracted! 4l/22/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
108-111-95-
541-106-100-95-95-
108-106-621-67-98-78-88-
105-65-
111-120-120-91-106-87-59-91-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-•47-8-•68-3-•50-7-•57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-
-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene •1,4-Dichlorobenzene -Benzyl alcohol •1,2-Dichlorobenzene •2-Methylphenol •bis(2-chloroisopropyl)ether •4-Methyl phenol •N-Nitroso-di-n-propy lamine -Hexachloroe thane -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-Dimethylphenol -Benzoic acid -bis(2-Ch1oroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol •2-Chloronaphthalene •2-Ni t roan i1ine •Dimethylphthalate -Acenaphthylene -2,6-Dinitrotoluene
Q
1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I S U - 1 194 300460
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I I 1111142-03 I
Tab Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case Ho. : S-2-if^'f^ SAS No.: SDG No. : -^/v//^
Iatrix: [soil/water] WATER Lab Sample ID: ^ " 6 ^ 4 ^ ^
Sample wt/vol: 1000 [g/mLl ML Lab File ID: >B8027
.tevel: [low/med] LOW Date Rece i©vedt-*gil/21/91
Mo 1s t u re dec 100,
Extraction: [SepF/Cont/Sonc] SERF
;PC Cleanup: [Y/N] N pH: 8.0
Date Extracted: -11/22/91
Date Analyzed: 11/30/91
Dilution Factor: 1.00
CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
99-83-51-100-132-121-84-
7005-86-
100-534-86-
101-118-87-85-
120-84-
206-129-85-91-56-
218-117-117-205-207-50-
193-53-
191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-•99-2-08-9-32-8-39-5-70-3-24-2-
-3-Ni t roan iIine -Acenaphthene -2,4-Dinitrophenol -4-Ni t ropheno1 -Dibenzofuran -2,4-Dinitrotoluene -Diethylphthalate -4-Chlorophenyl-phenylether -Fluorene -4-Ni t roan i1ine -4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -Butylbenzylphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethy1hexy1)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene -Benzo(g,h,i)perylene
Q
1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 50 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-2 195 300401
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
I I 1111142-03
ib Nam« INTECH Contract: 68-D9-0048
atrix: (soil/water) WATER
Sample wt•vo1: 10 00 (g/mL) ML
a eve 1 : i 1 ow/med ) LOW
^Moisture: dec. 100.
Extraction: (SepF/Cont/Sonc) SERF
PC Cleanup: (Y/N) N pH: 8.0
"fvlumber T ICs f o u n d : 0
Lab Sample ID: f - ^ L A ' ^ ^ ^
Lab File ID: >B8027
Date Received: H'^21/91
Date Extracted: 11/22/91
Date Analyzed: 11/30/91
Di lut ion Factor: ) .00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/ L
-••- 1 I I I CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q
j ' ~ = = = = S S = = = = = S : = B K j S S B B C E S S S B S S S S K S B n s e S S E S S S S S S S K K S : 1 S S B X B K S I S S 1 S S S B S B S B S K B S E | B B S S S
V ' 1 I I I I I
r 1 I I I J. 1 I I I
-,- 1 I I I I I I I I
1 I I I
I I I I I 1 1 I I I
T 1 I I 1 I I I I I
1 1 I I I --• 1 I I I
r 1 I I I I I I I 1 '
- ^ 1 ' I I 1
FORM I SU-TIC
196
1/87 Rev.
300402
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I 1111142-04
"ab Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case No. : 2-^'^5'~SAS No.: SDG No.:^/v/«'«<
atrix: [soil/water] SOIL
^ample wt/vol: 30.52 [g/mLl G
,„evel: [low/med] LOW
" Moisture: / ^ f dec . a; fiV^ • 2 3
Extraction: [SepF/Cont/Sonc] SONC
PC Cleanup: [Y/N] N pH: 8.0
Lab Sample ID: 1 2 M - f * "
Lab File ID: >B8031
Date Received: -4|L/21/91
Date Extracted: 11/25/91
Date Analyzed: 11/30/91
Dilution Factor: }•oO
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108-111-95-
541-106-100-95-95-
108-106-621-67 98-78 88 105 65-
111' 120-120-91-
106^ 87-59^ 91-77-88-95-91-88-
131-208-606-
-95-2--44-4--57-8--73-1--46-7-•51-6-•50-1-•48-7-•60-1--44-5-•64-7--72-1--95-3--58-1--75-5--67-9--85-0--91-1--83-2--82-1-•20-3--47-8--68-3--50-7--57-6--47-8-•06-2--95-4--58-7--74-4-•11-3--96-8-•20-2-
•Phenol •bis(2-chloroethyl)ether •2-Chloropheno1 •1,3-Dichlorobenzene •1,4-Dichlorobenzene -Benzyl alcohol •1,2-Dichlorobenzene -2-Methylphenol •bis(2-chloroisopropyl)ether -3&4-MethyIpheno1 -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-Dimethylphenol -Benzo ic acid -bis(2-Chloroethoxy)methane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene - 4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan i1ine -Dimethylphthalate -Acenaphthylene -2,6-Dinitrotoluene
Q
1 43 0 1 430 1 430 1 43 0 1 430 1 43 0 1 43 0 1 43 0 1 43 0 1 430 1 430 1 430 1 43 0 1 43 0 1 430 1 43 0 1 2100 1 43 0 1 430 1 430 1 430 1 43 0 1 430 1 43 0 1 43 0 1 43 0 1 430 1 430 1 430 1 2100 1 430 1 430 1 43 0
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I S U - 1 HJU
300403
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I 1111142-04
Tab Name: INTECH Contract: 68-D9-0048 I
"tab Code: INTECH Case No.: ^ l - y f ^ f ^ ' SAS No.: SDG No.: < 4 ^ / < ^
Iatrix: [soil/water] SOIL
Sample wt/vol: 30.52 [g/mLl G
,,^evel: [low/med] LOW
't Moisture: /y«f d e c . 11 U t^ . JZ
Extraction: [SepF/Cont/Sonc] SONC
;PC Cleanup: [Y/N] N pH: 8.0
Lab Sample ID: ] 7 c ' \ ' i l
Lab File ID: >B8031
Date Received: i|/'21/91
Date Extracted: 11/25/91
Date Analyzed: 11/30/91
Dilution Factor: l.oo
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
99-83-51-100-132-121-84-
7005-86-
100-534-86-
101-118-87-85-
120-84-
206-129-85-91-56-
218-117-117-205-207-50-
193-53-191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-•01-9-•81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-
•3-Ni t roan i1ine •Acenaphthene •2,4-Dinitrophenol •4-Ni t ropheno1 •Dibenzofuran -2,4-Dinitrotoluene •Diethylphthalate -4-Chlorophenyl-phenyl ether •Fluorene -4-Ni t roan i1i ne -4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromopheny1-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -Butylbenzylphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-EthyIhexy1)phthalate -Di-n-octylphthalate -Benzo(b)fiuoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene •Dibenz(a,h)anthracene -Benzo(g,h,i)perylene
Q
1 2100 1 43 0 1 43 0 1 2100 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 2100 1 2100 1 43 0 1 430 1 43 0 1 2100 1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 850 1 430 1 43 0 1 220 1 43 0 1 430 1 43 0 1 430 1 430 1 430 1 430
IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU
I J IU IU IU IU IU IU IU I
FORM I SU-2 200 300404
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
I I 1111142-04
£ab Name: INTECH Contract: 68-D9-0048
,,„a t r 1 X : i s o i 1 / wa t e r ) SO IL
-ample wt-'vol: 30.52 (g/mL) G
Level: '.low/med) LOW
Moisture: ^ o f d e c . 7-1 . U«^. 2 3
Extraction: (SepF/Cont/Sonc) SONC
PC Cleanup: (Y/N) N pH: 8.0
Number TICs found: 1
Lab Sample ID: ) l< i - i ' i l
Lab File ID: >Be031
Date Received: €i./21/91
Date Extracted: 11/25/91
Date Analyzed: 11/30/91
Dilution Factor: \ . .00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
_ CAS NUMBER 1 COMPOUND NAME
^^^ . - 1 Unknown
1 1 1 1
1 1 1
1 1 -L 1
T" 1 1 1
1 1 1
r 1 1 . 1
-.- \
1 1
^ ^
RT : B B B B a
5 . 04
EST. CONC. E ^ B B B B B B B B
2 1 0 . B B S= B
Q
FORM I S U - T I C 201 1/87 Rev.
300405
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111142-05 .ab Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH _.Case No.: A2'^f-^^rSAS No.: SDG H o . : ^ ^ i ^ * ^
Iatrix: [soil/water] WATER Lab Sample ID: ^ - $ U J < ^
Sample wt/vol: lOOO [g/mLl ML Lab File ID: >B8028
«ievel: [low/medl LOW Date Rece ieved:''|^1/21/91
"•"'. Moisture: dec 100. Date Extracted! 11/22/91
Extraction: [SepF/Cont/Sonc] SERF
;PC Cleanup: [V/N] N pH: 8.0
Date Analyzed: 11/30/91
Dilution Factor: f.OO
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
108-111-95-
541-106-100-95-95-
108-106-621-67-98-78-88-
105-65-
111-120-120-91-
106-87-59-91-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-
-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene -Benzyl alcohol -1,2-Dichlorobenzene -2-Methylphenol -bis(2-chloroisopropyl)ether -4-Methylphenol -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-DimethyIpheno1 -Benzoic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan iIine •Dimethylphthalate •Acenaphthylene •2,6-Dinitrotoluene
Q
1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 90 1 10 1 10 1 10
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU i IU . 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I S U - 1 206 300406
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
1111142-05 ,ab Name: INTECH Contract: 68-D9-0048 . I
Lab Code: INTECH Case No.: f -tV-??' 5^5 ^o. : SDG Ho. :/l^f^fi^
,„,atrix: [soil/water] WATER Lab Sample ID: f — ^ t ^ ^ ^
-example wt/vol: 1000 [g/mL] ML Lab File ID: >B8028
Level: [low/med] LOW Date Rece ievedr^l/21/91
Moisture: dec 100. Date Ext ractedJ'l^ 1/2 2/91
Extraction: [SepF/Cont/Sonc] SERF
PC Cleanup: [Y/N] N pH: 8.0
Date Analyzed: 11/30/91
Dilution Factor: |.00
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
99-83-51-
100-132-121-84-
7005-86-
100-534-86-
101-118-87-85-
120-64-
206-129-85-.91-56-
218-117-117-205-207-50-
193-53-
191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-
•3-Ni t roan iIine •Acenaphthene •2,4-Dinitrophenol •4-Nitropheno1 •Dibenzofuran •2,4-Dinitrotoluene -Diethylphthalate -4-Chlorophenyl-phenylether -Fluorene -4-Ni t roan i1ine -4,6-Dinitro-2-methylphenol -N-Nitrosodiphenyl amine •4-Bromophenyl-phenylether •Hexachlorobenzene •Pentachloropheno1 •Phenanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e
Q
1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 5 0 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 3 1 10 1 10 1 10 1 10 1 10 1 10 1 10
1 i IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 J 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU . 1 IU 1 1 1
FORM I SU-2 207 300407
IF >EMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
I 1111142-05 .ab Nc- INTECH Contract: 68-D9-0048 I
latri.: soil/water) WATER
-Sample ct 'vo1: 10 00 (g/mL) ML
"'iteve 1 : '1 ow/med ) low
~oMoi£ti^re: dec. 100.
Extraction: (SepF/Cont/Sonc) SERF
;PC Cleanup: (Y/N) N pH: 8.0
Number TICs found: 0
Lab Sample ID: ^ - ^ ^ , ^ ^ <
Lab File ID: >B8028
Date Received: 1^/21/91
Date Extracted: 11/22/91
Date Analyzed: 11/30/91
Di lut ion Factor: i.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/ L
CAE NUMBER 1 COMPOUND NAME 1 =: = = = = = =r=: = = = = = = B B | B S B S E B B B B B B B S S B S B B B B B B B S B B B B
1 I
W • 1 1 1
1 1 1
"1 1 1 1
—: 1 1 1
1
1 1 J 1
.... j
1 1
1 1 -1 1
" i ^ ^
RT EST. CONC. S B B S B B B B B B ^ B
Q
FORM I SU-TIC
208 1/87 Rev.
30040&
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
1111164-01 .ab NaT-e: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Ease H o . - A i ' ( A ^ ^ ^ SAS No.: SDG No. :/?/l/c*v
Lab Sample ID: 4<^ ?
Lab File ID: >68065
Date Received: ;r|S i 26/91
I Moisture: .voTdec. ^% o(ti:> 5*2.
Extraction: [SepF/Cont/Sonc] SONC
.PC Cleanup: [Y/N] N pH: 7.5
..Jatrix: [soil/water] SOIL
.Sample wt--vol: 30.25 [g/mL] G
tieve 1 : [low/med] LOW
Date Extractedl!!3.1/27/91
Date Analyzed: 12/03/91
Dilution Factor: ).oo
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108 111 95
541 106 100 95 95
108 106 621 67 98 78 88 105 65'
111. 120. 120. 91. 106 87 59 91 77 88 95 91-88.
131-208-606-
-95-2--44-4--57-8--73-1--46-7--51-6--50-1--48-7--60-1--44-5--64-7--72-1--95-3--58-1--75-5--67-9--85-0--91-1--83-2--82-1--20-3--47-8--68-3--50-7--57-6--47-8--06-2--95-4--58-7--74-4--11-3-•96-8--20-2-
-Pheno I -bis(2-chloroet -2-Chloropheno I -1,3-Dichlorobe -1,4-Dichlorobe -Benzyl alcohol -1,2-Dichlorobe -2-Methylphenol -b is(2-ch loro is -3&4-Methylphen -N-Ni t roso-d i-n -Hexachloroetha -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-Dimethylph -Benzoic acid -bis(2-Chloroet -2,4-Dichloroph -1,2,4-Trichlor •Naphthalene -4-Chloroan i1 in -Hexachlorobuta -4-Chloro-3-met -2-Methylnaphth -Hexachlorocycl -2,4,6-Trichlor -2,4,5-Tr ichlor •2-Chloronaphth -2-Nit roan i1ine -DimethyIphthaI -Acenaphthylene -2,6-Dini troto1
hy1)ether
nzene nzene
nzene
opropyl)ether ol -propylamine ne
eno I
hoxy)methane eno 1 obenzene
e d iene hyIpheno1 a lene opentad iene opheno I opheno 1 a lene
ate
uene
Q
690 690 690 690 690 690 690 690 690 690 690 690 690 690 690 690
3400 690 690 690 690 690 690 690 690 69 0 690 690 690 3400 690 690 690
IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU
I
FORM I SU-1 212 300409
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111164-01
ab Nan-,e: INTECH
Lab Code: INTECH Case No,
Iatrix: [soil/water] SOIL
Contract: 68-D9-0048 I
U t - e ^ ' $ ^ SAS No.: SDG Ho . :/}/\^/(^<^
Sample ut/vol: 30.25 [g/mL] G
•Sevel: [low/med] LOU
~. Moisture: voTdec. f i ^ ^*€ ' ^^
Extraction: [SepF/Cont/Sonc] SONC
PC Cleanup: [Y/N] N pH: 7.5
Lab Sample ID: t ° ' i ^ ^
Lab File ID: >B8065
Date Received: 11/26/91
Date Extracted: 11/27/91
Date Analyzed: 12/03/91
Dilution Factor: |.oo
CAS NO. COMPOUND CONCENTRATION UNITS: lug/L or ug/Kg] UG/KG
99 83 51
100 132 121 84^
7005 86^
100 534 86
101-118 87 85
120 84
206 129 85 91 56
218 117-117. 205^ 207 50
193 53-
191'
-09-2--32-9--28-5--02-7--64-9--14-2-•73-7-•72-3--73-7-•01-6-•52-1-•30-6--55-3-•74-1--86-5--01-8--12-7--74-2--44-0--00-0--68-7--94-1--55-3-•01-9-•81-7--84-0--99-2--08-9--32-8--39-5-•70-3-•24-2-
-3-Ni t roan i1ine -Acenaphthene -2,4-Dinitrophenol -4-Ni t ropheno1 -Dibenzofuran -2,4-Dinitrotoluene -Diethylphthalate -4-Chloropheny1-phenylether •Fluorene •4-Ni t roan i1ine •4,6-Dinitro-2-methylphenol •N-Nitrosodiphenylamine •4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butylphthalate •Fluorant hene -Pyrene -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fiuoranthene -Ben2o(a)pyrene - Indeno(1,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e
Q
3400 690 690
3400 690 690 690 690 690
3400 3400 690 690 690
3400 690 690 690 690 690 690 1400 690 690 690 690 690 690 690 690 690 690
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-2 213 3004tO
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
I 1111164-01 C'ab Name: INTECH
...atrix: tsoil/water) SOIL
'-ample wt/vol: 30.25 (g/mL) G
Level: (low/med) LOW
Moisture: .••'Tdec. f/. . fiiec • f i^
Extraction: (SepF/Cont/Sonc) SONC
. C Cleanup: (Y/N) N pH: 7.5
Number TICs found: 1
Contract: 68-D9-0048
Lab Sample ID: «>-^Z
Lab File ID: >B8065
Date Received: 4^-^26/91
Date Extracted: 11/27/91
Date Analyzed: 12/03/91
Dilution Factor: \.oo
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER
m-
m
COMPOUND NAME 1 RT B B B B B B B B B B B B B B S B B B B B B B B B B B B B | B B B B B B B B
Unknown i 3.62
EST. CONC,
48 0 .
Q
FORM I S U - T I C
214 1/87 Rev. ^ ^.
3004U
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I 1111164-02
•.ab Na-e: INTECH
Tab Cede: INTECH
Contract: 68-D9-0048 I
Case No.: 4'? •'^^"?^ SAS No.: SDG No.: ^o,/<^^
Iatrix: [soil/water] SOIL
Sample wt-vol: 30.21 [g/mLl G
.-...evel: [low/med] LOW
"i Moisture: -^aTdec . a.- c/et • t l
Extraction: [SepF/Cont/Sonc] SONC
PC Cleanup: [Y/N] N pH: 7.5
Lab Sample ID: "75'-?7
Lab File ID: >B8066
Date Received: 11/26/91
Date Extracted: 11/27/91
Date Analyzed: 12/03/91
Dilution Factor: f.oo
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108-111-95-
541-106-100-95-95-
108-106-621-67-98-78-88-
105-65-111-120-120-91-106-87-59-91-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-
-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene -Benzyl alcohol -1,2-Dichlorobenzene -2-Methylphenol -bis(2-chloroisopropyl)ether -3&4-MethyIphenoI -N-Nitroso-di-n-propylamine -Hexachloroethane -Ni t robenzene - Isophorone -2-Ni t ropheno1 -2>4-Dime thy I phenol -Benzoic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -l,2,4-Trichloroben2ene -Naphthalene -4-Chloroani1ine -Hexachlorobutad iene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan i1ine -Dime thyIphthalate -Acenaphthylene -2,6-Dinitrotoluene
Q
1 43 0 1 430 1 430 1 430 1 43 0 1 43 0 1 430 1 43 0 1 430 1 430 1 43 0 1 430 1 43 0 1 43 0 1 430 1 43 0 1 2100 1 430 1 43 0 1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 430 1 43 0 1 430 1 430 1 430 1 2100 1 430 1 430 1 43 0
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-1 218 3004\2'
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111164-02 .ab Name: INTECH
Tab Code: INTECH
Iatrix: [soil/water] SOIL
Sample wt/vol: 30.21 [g/mL] G
.,..eve 1 : [ 1 ow/med ] LOW
Ji Moisture: .yoT dec . ^3 C , 2 3
"Extraction: [SepF/Cont/Sonc] SONC
';PC Cleanup: [Y/N] N pH: 7.5
Contract: 68-D9-0048 I
Case No. : 4-^-^^-^rsAS No.: SDG No . : ^^/c^^
Lab Sample ID: 7f-77
Lab File ID: >B8066
Date Received: -11/26/91
Date Extracted: 3.1/27/91
Date Analyzed: 12/03/91
Dilution Factor: \ . c o
C H S NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
99-83-51-
100-132-121-84-
7005-86-
100-534-86-
101-118-87-85-
120-84-
206-129-85-91-56-
218-117-117-205-207-50-
193-53-
191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-•01-9-•81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-
-3-Ni t roan i1ine -Acenaphthene -2,4-Dinitrophenol -4-Ni t ropheno1 - D i b e n z o f u r a n - 2 , 4 - D i n i t r o t o l u e n e • D i e t h y l p h t h a l a t e • 4 - C h l o r o p h e n y 1 - p h e n y l e t h e r • F l u o r e n e •4-Nitroani1ine •4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromopheny1-phenylether -Hexachlorobenzene -Pentachlorophenol -Phenanthrene -Anthracene -Di-n-butylphthalate -F1uoranthene -Pyrene -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine -Ben2o(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Ben2o(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene •Dibenz(a,h)anthracene •Benzo(g,h,i)perylene
Q
1 2100 1 43 0 1 430 1 2100 1 430 1 43 0 1 43 0 1 43 0 1 43 0 1 2100 1 2100 1 43 0 1 43 0 1 43 0 1 2100 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 860 1 43 0 1 430 1 43 0 1 430 1 430 1 43 0 1 430 1 430 1 430 1 430
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-2 219 30041^'
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
1111164-02 Ilab Name: INTECH
..Jatriv: (soil/water) SOIL
"ample wt/vol: 30.21 (g/mL) G
"Level: (low/med) LOW
i Moisture: ..-ordec. i'j . fl^<', 2 3
Extraction: (SepF/Cont/Sonc) SONC
• PC Cleanup: (Y/N) N pH: 7.5
Number TICs found: 1
Contract: 68-D9-0048
Lab Sample ID: 75'-77
Lab F i l e ID : >B8066 •?*••
Date R e c e i v e d : 3 ^ / 2 6 / 9 1
Date Extracted; 11/27/91
Date Analyzed: 12/03/91
Dilution Factor: ( . 0
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME
Unknown
RT : ^ ^ B s
3.61
EST. CONC. E B B B B S B S B B B
520.
Q
FORM I SU-TIC 220 1/87 Rev,
300414
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I I I111164-02RE I
I .ab Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case No. : 2-^^-^T SAS No.: SDG Ho. : ^'^i^f*-
J a t n x : [soil/water] SOIL Lab Sample ID: 1 ^ ~ ^ 7
Sample wt/vol: 30.21 [g/mL] G Lab File ID: >B80e4
Tleve 1 : [ low/med ] LOW
; Moisture: /voT'dec. 7" ifitc 2 3
Extraction: [SepF/Cont/Sonc] SONC
.;PC Cleanup: [Y/N] N pH: 7 .3
Date Received: "tl/26/91
Date Extracted: 11/27/91
Date Analyzed: 12/04/91
Dilution Factor: ).oo
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108-111-95-
541-106-100-95-95-
108-106-621-67-98-78-88-
105-65-
111-120-120-91-106-87-59-91-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-
-Phenol -bis(2-chloroethyl)ether •2 -Ch lo ropheno1 - 1 , 3 - D i c h l o r o b e n z e n e • 1 , 4 - D i c h l o r o b e n z e n e •Benzyl a l c o h o l • 1 , 2 - D i c h l o r o b e n z e n e •2-Me t h y I p h e n o 1 •bis(2-chloroisopropyl)ether •3&4-MethyIpheno1 •N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene - I sophorone -2-Ni t ropheno1 -2,4-Dimethylphenol -Benzo ic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methy 1 naphtha Iene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan i1ine •Dime thyIphthalate •Acenaphthylene •2,6-Dinitrotoluene
Q
^ i-
43 0 43 0 43 0 43 0 43 0 43 0 43 0 43 0 430 43 0 43 0 43 0 43 0 43 0 430 43 0
2100 43 0 43 0 43 0 43 0 43 0 43 0 43 0 430 43 0 43 0 430 430
2100 430 43 0 430
1 1 IU I IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 ,, A 3<i04l5
FORM I S U - 1
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I111164-02RE I .ab Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case Ho. : ^ 2 - ( f ^ - f ^ Sf^S No.: SDG No. : A i ^ '
.Jatnx: [soil/water] SOIL Lab Sample ID: 7S^ 7 7
-Sample wt/vol: 30.21 [g/mLl G
Tevel: [low/medl LOW
. Moisture: ,voT dec. M / i f - 5 3
Extraction: [SepF/Cont/Sonc] SONC
:PC Cleanup: [Y/N] N pH: 7.5
CAS NO. COMPOUND
Lab File ID: >B8064
Date Received: ;^/26/91
Date Extracted: 11/27/91
Date Analyzed: 12/04/91
Dilution Factor: .<jo
CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG Q
99-83-51-100-132-121-84-
7005-86-
100-534-86-
101-118-87-85-
120-84-
206-129-85-91-56-
218-117-117-205-207-50-
193-53-
191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-
-3-Ni t roan i1ine -Acenaphthene • 2 , 4 - D i n i t r o p h e n o l - 4 - N i t r o p h e n o I •Dibenzofuran -2,4-Dinitrotoluene -DiethyIphthalate -4-Chlorophenyl-phenylet her •Fluorene •4-Ni t roan i1ine •4,6-Dinitro-2-methyIpheno1 •N-Nitrosodiphenylamine •4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene •Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene •ButyIbenzyIphtha late -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-EthylhexyI)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)py'~ene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e
1 2100 1 43 0 1 430 1 2100 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 2100 1 2100 1 43 0 1 430 1 43 0 1 2100 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 860 1 430 1 430 1 43 0 1 43 0 1 43 0 1 430 1 430 1 43 0 1 430 1 43 0
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-2 225 300416
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
I111164-02RE Lab Name: INTECH
liatri-;: i soil/water) SOIL
"":.ample wt/vol: 30.21 (g/mL) G
Level: (low/med) LOW
b Moisture: .yoT d e c . 23 • ^ ^ • 2.1
Extraction: (SepF/Cont/Sonc) SONC
-oPC Cleanup: (Y/N) N pH: 7.5
Number TICs found: 1
Contract: 68-D9-0048
Lab Sample ID: 75^-77
Lab File ID: >B8084
Date Received: Jt!4/26/91
Date Extracted: 11/27/91
Date Analyzed: 12/04/91
Dilution Factor: \-oo
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q j = = = = s: = = = = s= = B B B B B ( ts = x = m K m m K ^ = ^ B X s = a s B = a s s = a = a x | B B B B S B B S | B B B B B B B B B B B B B | = s i — s s
^ 1 . - - [Unknown 1 3 .58 1 600. 1 J
I I I I I
I I I I I 1 1 I I I
, 1 I I I 1 1 - I I I
1 1 I I I 1 1 I I 1
i 1 I I I I I I I I
1 1 I I 1 ~ 1 I I I
1 1 I I 1 I I I I I
. ^ 1 . I I 1 B 1 I I I
FORM I SU-TIC 226 1/87 Rev. 3064it
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I I 1111164-03 I
_ab Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case Ho. : ' ^ ^ - t f ^ ' ^ SAS No.: SDG No.: t^^J^^
-Matrix: [soil/water] WATER
Sample wt/vol: 1000 [g/mL] ML
Level: [low/med] LOW
yi Moisture: dec 100.
Extraction: [SepF/Cont/Sonc] SERF
SPC Cleanup: [Y/N] N pH: 7.5
Lab Sample ID: r - $ t / i ^ K
Lab File ID: >B8083
Date Receieved: il/26/91
Date Extracted: 11/27/91
Date Analyzed: 12/04/91
Di lut ion Factor: ).00
CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
108-111-95-
541-106-100-95-95-
108-106-621-67-98-78-88-
105-65-
111-120-120-91-
106-87-59-91-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-•50-7-•57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-
-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene -Benzyl aIcoho 1 •1,2-Dichlorobenzene -2-Methylphenol -bis(2-chloroisopropyl)ether -4-Methylphenol -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene -1 sophorone -2-Nitropheno1 -2,4-Dimethylphenol -Benzo ic acid -bis(2-Chloroethoxy)me thane -2,4-Dichloropheno1 -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutad iene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-Trichlorophenol -2,4,5-Tr ichloropheno1 -2-Chloronaphthalene -2-Ni t roan i1ine -Dimethylphthalate •Acenaphthylene -2,6-Dinitrotoluene
Q
1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 ^1
FORM I S U - 1 230 3'0041B
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111164-03 ab Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case No. : ^'^*''?^ SAS No.: SDG No.: ^ ^ i < > ^
,. atriv: [soil/water] WATER
—ample wt/vol: 1000 [g/mLl ML
H'evel: [low/med] LOW
Mo ISt ure: dec 100.
Extraction: [SepF/Cont/Sonc] SERF
PC Cleanup: [Y/N] N pH: 7.5
CAS NO, COMPOUND
Lab Sample ID: r - $ L ^ ^ ^
Lab File ID: >B8083
Date Receieved: :ll/26/91
Date Extracted: il/27/91
Date Analyzed: 12/04/91
Di lut ion Factor: |.00
CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L Q
99-83-51-100-172-121-84-
7005-86-
100-534-86-
101-118-87-85-
120-84-
206-129-85-91-56-
218-117-117-205-207-50-193-53-
191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-•44-0-•00-0-68-7-•94-1-55-3-01-9-81-7-84-0-99-2-•08-9-•32-8-•39-5-70-3-24-2-
-3-Ni t roan iIine •Acenaphthene •2,4-Dinitrophenol •4-Ni t ropheno1 •Dibenzofuran •2,4-Dinitrotoluene •Diethylphthalate •4-Chloropheny1-phenylether •Fluorene •4-Ni t roan i1i ne •4,6-Dinitro-2-methylphenol •N-Nitrosodiphenylamine •4-Bromopheny1-phenylether -Hexachlorobenzene -Pentachloropheno1 - Ph enanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e
1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 50 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU . 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-2 231 300419
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
I 1111164-03 •tab Name: INTECH Contract: 68-D9-0048
..'-.atri>: (soil/water) WATER
^ample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
Mo ISt ure: dec. 100.
Extraction: CSepF/Cont/Sonc) SERF
PC Cleanup: (Y/N) N pH: 7.5
Number TICs found: 0
Lab Sample ID: lf-'SLi^»'K
Lab File ID: >B6083
Date Received: .^/26/91
Date Extracted: 11/27/91
Date Analyzed: 12/04/91
Di lut ion Factor: /.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/ L
•... CAS NUMBER COMPOUND NAME B S S B B B B B :
RT EST. CONC, Q
FORM I S U - T I C
232 1/87 Rev.
300420
m IB
E.EMIUOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I 1111185-01 .ab Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case No. : f/-^*'-^f~ SAS No.: SDG No.: ' ' A''
iatrix: [soil/water] SOIL
^Sample wt/vol: 30.40 [g/mLl G
„^eve 1 : [low/medl LOW
""' Moisture: /VoTdec. 1 1 ffec- 1 \
Extraction: [SepF/Cont/Sonc] SONC
PC Cleanup: [Y/N] N pH: 8.0
Lab Sample ID: ( jO^y i
Lab File ID: >B8095
Date Received: 11/27/91
Date Extracted: 12/03/91
Date Analyzed: 12/06/91
Dilution Factor: l.oO
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108^ 111 95
541-106^ 100-95-95-
108-106-621-67-98-78 88.
105' 65
111-120-120-91-106' 87 59 91 77 88-95-91-88-
131-208-606-
-95-2--44-4--57-8--73-1--46-7--51-6-•50-1--48-7--60-1--44-5--64-7--72-1--95-3--58-1--75-5--67-9--85-0-•91-1-•83-2-•82-1--20-3--47-8--68-3--50-7--57-6--47-8-•06-2-•95-4-58-7-•74-4-•11-3-•96-8-20-2-
-Phenol -bis(2-chloroethyl)ether -2-Chloropheno1 - 1 , 3 - D i c h l o r o b e n z e n e - 1 , 4 - D i c h l o r o b e n z e n e - B e n z y l a l c o h o l - 1 , 2 - D i c h l o r o b e n z e n e - 2 - M e t h y l p h e n o l - b i s ( 2 - c h l o r o i s o p r o p y l ) e t h e r - 3 & 4 - M e t h y I p h e n o 1 -N-Nitroso-di-n-propylamine -Hexachloroethane -Nit robenzene - Isophorone -2-Ni t ropheno1 -2,4-Dime thyIpheno1 -Benzo ic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1 ,2,4-Tr ichlorobenzene -Naphthalene -4-Chloroani1ine - He xachlorobutadiene -4-Chloro-3-methyIpheno1 -2-Methylnaphthalene - Hexach1orocycI open tadiene -2,4,6-Trichlorophenol -2,4,5-Trichlorophenol •2-Chloronaphthalene •2-Ni t roan i1ine •Dimethylphthalate •Acenaphthylene •2,6-Dinitrotoluene
Q
1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 430 1 43 0 1 430 1 43 0 1 430 1 43 0 1 2100 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 430 1 43 0 1 43 0 1 430 1 43 0 1 430 1 2100 1 430 1 430 1 430 1 r»o tr
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-1 300421
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111185-01 ab Narr.e: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case No. : 42-irV'^5 SAS No.: SDG No.: -^V^^
atrix: [soil/water] SOIL
.Sample wt/vol: 30.40 [g/mL] G
-evel: [low/med] LOW
""'Moisture: /v^Tdec. f^ ^t^. 13
Extraction: [SepF/Cont/Sonc] SONC
PC Cleanup: [Y/N] N pH: 8.0
Lab Sample I D : ^ - ^ ? '
Lab File ID: >B8095
Date Received: 11/27/91
Date Extracted: 12/03/91
Date Analyzed: 12/06/91
Dilution Factor: \.(jo
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
99' 83^ 51-
100-132-121-84-
7005-86-
100-534-86^
101-118-87^ 85
120^ 84
206^ 129 85 91 56
218 117. 117. 205^ 207. 50-
193 53-
191-
•09-2-•32-9-•28-5-•02-7-•64-9-•14-2-73-7-•72-3-73-7--01-6-•52-1--30-6--55-3--74-1-•86-5--01-8--12-7-•74-2--44-0--00-0--68-7--94-1--55-3--01-9-•81-7--84-0--99-2--08-9-•32-8--39-5-•70-3-•24-2-
•3-Ni t roan i1ine •Acenapht hene •2,4-Dinitrophenol •4-Ni t ropheno1 •D ibenzo furan •2,4-Dinitrotoluene •Diethylphthalate •4-Chloropheny1-phenylether •Fluorene •4-Ni t roan i1ine -4,6-Dinitro-2-methylphenol •N-Nitrosodiphenyl amine •4-Bromopheny1-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butylphthalate •Fluoranthene -Pyrene - B u t y l b e n z y l p h t h a l a t e - 3 , 3 ' - D i c h l o r o b e n z id i n e - B e n z o ( a ) a n t h r a c e n e - C h r y s e n e -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)fluoranthene • B e n z o ( a ) p y r e n e - I n d e n o ( l , 2 , 3 - c d ) p y r e n e • D i b e n z ( a , h ) a n t h r a c e n e - B e n z o ( g , h , i ) p e r y l e n e
Q
1 2100 1 43 0 1 430 1 2100 1 43 0 1 43 0 1 43 0 1 43 0 1 43 0 1 2100 1 2100 1 43 0 1 43 0 1 43 0 1 2100 1 43 0 1 430 1 43 0 1 430 1 43 0 1 43 0 1 850 1 430 1 430 1 36 1 43 0 1 430 1 430 1 430 1 430 1 430 1 43 0
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 J 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-2 23G 300422
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
"tab Name: INTECH Contract: 68-D9-0048
EPA SAMPLE NO.
I I I 1111185-01 1 I _l
• atrix: (soil/water) SO IL
""ample wt--vol: 30.40 (g/mL) G
Level: Clow/med) LOU
Mo 1 s t u r e : .'>6t"dec . j 3 . (/((:, 2 I
Extraction: (SepF/Cont/Sonc) SONC
,.PC Cleanup: (Y/N) N pH: 8.0
Number TICs found: 2
Lab Sample ID: j, _^2
Lab File ID: >B8095
Date Received: lPl/27/91
Date Extracted: 12/03/91
Date Analyzed: 12/06/91
Dilution Factor: \ . o o
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER 1 COMPOUND NAME 1 RT 1 E S T . CONC. 1 Q { = B S : = = =:=: = =: = = S B B S B \ = S S X K t S ^ B S = = = = ^ S S = ^ m a S S S S i = aSXSS | B B B B S B B S 1 B B B B B B B B B B B B B J B B B B S
i l ^ l . 1 4 1 - 7 9 - 7 l 3 - P e n t e n - 2 - o n e , 4 - m e t h y l - ( 8 1 2 . 6 7 1 1 7 0 . 1 J ^ ^ 2 . . - - l A l d o l C o n d e n s a t i o n 1 3 . 5 5 1 8 5 0 0 . 1 3
1 1 I I I
i 1 I I '
1 1 I I 1
I I I I I '- 1 I I I
1 1 I I I I I I I I
1 1 I I I 1 I I 1
I I I I I j. 1 I I I
T" 1 I I I I I i l l
^ ^
FORM I SU-TIC 1/87 Rev.
237 300423'
IB Z.EMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I 1111185-02 .at \ < f ' f - INTECH Contract: 68-D9-0048 I
ab Core: INTECH Case No. : ^ 2 - ^ ^ ' ?^'SAS No.: SDG No . :/?/v/^/^
riatri,-: [soil/water] SOIL
• ample .. t • WQ 1 : 30.51 [g/mL] G
Level: Llow/med] LOW
J Mo 1 5 • _ - e : ,'j'ot dec . |g siic- \%
-E:xtrac';cn: [ SepF/Con t/Sonc ] SONC
CiPC Cleanup: [Y/N] N pH: 7.3
COMPOUND
Lab Sample ID: 7f- 76.'
Lab File ID: >B8096
Date Received: 11/27/91
Date Extracted: 12/03/91
Date Analyzed: 12/06/91
Dilution Factor: \ .00
CHS NO.
1 106-1 ill-1 ''? -! - 4 1 -1 10 6-i 100-i 95-i 95-i 108-1 106-i 621-i 67-i 98-1 78-1 86-1 105-1 65-i 111-1 12 0-1 120-t 91-1 106-i 87-1 59-i 91-i 77-i 88-i 95-1 91-i 88-i 131-1 208-1 606-
-95--44--57--73--46--51--50--48--60--44--64--72--95--58--75--67--85--91--83--82--20--47--68--50--57--47--06--95--58--74--11--96--20-
-2 -4 -8 -1 -7 -6 -1 .7 •1
-5 -7 •1
•3
-1 -5 .9 •0
-1 -2 -1 -3 -8 -3 -7 -6 -8 -2 -4 -7 -4 -3 -8 •2
CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
-Pheno 1 -bis(2-chloroethyl)ether -2-Chloropheno1 -1,3-Dichlorobenzene -1,4-Dichlorobenzene -Benzyl alcohol -1,2-Dichlorobenzene -2-Methylpheno 1 •bis(2-chloroisopropyl)ether •3&4-MethyI phenol •N-Nitroso-di-n-propylamine •Hexachloroethane -Nit robenzene • Isophorone -2-Ni t ropheno 1 -2,4-DimethyIpheno 1 -Benzoic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-me t hy1pheno 1 -2-Methylnaphthalene -Hexachloroeyclopentad iene -2,4,6-Trichlorophenol -2,4,5-Tr1chloropheno 1 -2-Chloronaphthalene -2-Ni t roan i1i ne -DimethyIphthalate -Acenaphthylene -2,6-Dinitrotoluene
Q
1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 2000 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 2000 1 400 i 400 1 400
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU i IU 1 IU 1 IU i IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1
1 ^ 1
FORM I SU-1 •2T3 ^00424
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111185-02 ,ab Name: INTECH Contract: 68-D9-0048 I
• ab Code: INTECH Case No. : /^Z-t'^-^r SAS No.: SDG No.:rfxK/*>'
itatrix: [soil/water] SOIL Lab Sample ID: l ^ - f k /
ample wt/vol: 30.51 [g/mLl G
Level: [low/med] LOW
Moisture: «yol dec . \% o u t - l ^ :
Fxtraction: [SepF/Cont/Sonc] SONC
..-.-C Cleanup: [Y/N] N pH: 7.3
COMPOUND CAS NO.
i 99-1 83-i 51-1 100-i- 172-i 121-i 84-i 7005-i 86-1 100-1 534-1 86-i 101-1 118-i 87-i 85-1 120-1 84-i 206-1 129-i 85-1 91-i 56-1 218-1 117-1 117-1 205-1 207-1 50 1 193 1 53-1 191-
-09--32--28--02--64--14--73--72--73--01--52--30--55--74--86--01--12--74--44--00--68--94--55--01--81--84--99--08--32--39--70--24-
-2 -9 -5-•7
-9 -2 -7 -3 -7--6 -1--6--3 -1 -5 -8 -7 -2 -0 -0 -7 -1 -3 -9 -7 -0 -2 -9 -8 -5 -3 -2
Lab File ID: >B8096
Date Received: ,11/27/91
Date Extracted: 12/03/91
Date Analyzed: 12/06/91
Dilution Factor: |.ofl
CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG Q
• 3 - N i t r o a n i 1 i ne • A c e n a p h t h e n e • 2 , 4 - D i n i t r o p h e n o l - 4 - N i t r o p h e n o 1 • D i b e n z o f u r a n - 2 , 4 - D i n i t r o t o l u e n e • D i e t h y l p h t h a l a t e • 4 - C h l o r o p h e n y 1 - p h e n y l e t h e r • F l u o r e n e • 4 - N i t r o a n i 1 i n e • 4 , 6 - D i n i t r o - 2 - m e t h y l p h e n o l -N -N i t r o s o d i p h e n y l a m i n e - 4 - B r o m o p h e n y 1 - p h e n y l e t h e r - H e x a c h l o r o b e n z e n e • P e n t a c h l o r o p h e n o 1 • P h e n a n t h r e n e • A n t h r a c e n e • D i - n - b u t y l p h t h a l a t e •F l u o r a n t h e n e • P y r e n e -ButyIbenzyIphthalate -3,3'-Dichlorobenzidine - Be nzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene - Benzo(k)fiuoranthene -Benzo(&)pyrene -lndeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene -Benzo(g,h,i)perylene
1 2000 1 400 1 400 1 ' 2000 1 400 1 400 1 400 1 400 1 400 1 2000 1 2000 1 400 1 400 1 400 1 2000 1 400 1 400 1 400 1 400 1 400 1 400 1 800 1 400 i 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400 1 400
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU ! IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-2 244 300425
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE HO.
I 1111185-02 'Lab Name: INTECH Contract: 68-D9-0048
.iatrix: ( s o i 1 / wa t e r ) SO IL
ample wt/vol: 30.51 (g/mL) G
Level: (low/med) LOW
. Moisture: ,>oTdec. j^ . (/ c. (g
Extraction: (SepF/Cont/Sonc) SONC
-:.PC Cleanup: (Y/N) N pH: 7.3
Number TICs found: 3
Lab Sample ID: 7 ^- '^ ("
Lab File ID: >B8096
Date Received:>iJC4/27/91
Date Extracted: 12/03/91
Date Analyzed: 12/06/91
Dilution Factor: ).C0
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER
3 .
4127-47 -3
COMPOUND NAME 1 RT B B B B B B B B B B B B S B B B B S B B B S a S B S B B | B B B B B B B B
Cyclopropane, 1,1,2,2-tetram 1 2.66 Aldol Condenset ion (/'/vkfo'o**-/'-J 1 3.55 Unknown Alkane 1 24.35
EST. CONC,
2 0 0 . 7 6 0 0 .
5 6 0 .
Q
J J 3
FORM I S U - T I C
245 1/87 Rev.
300426
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I 1111185-03
Lab Name: INTECH Contract: 68-D9-0048 I
ab Code: INTECH Case No. : f l" ^-^r SAS No.: SDG Ho.-./J^jf'
Matrix: [soil/water] WATER
...ample wt/vol: 1000 [g/mLl ML
~eve1: [low/med] LOW
SMoisture: dec 100.
xtraction: [SepF/Cont/Sonc] SERF
GPC Cleanup: [Y/N] N pH: 7.0
COMPOUND
Lab Sample ID: F- C/f/VK
Lab File ID: >B8C70
Date Receieved: 11/27/91
Date Extracted: 12/01/91
Date Analyzed: 12/03/91
Di lut ion Factor: | .00
CAS t
i 108-i 111-i 95-i. 541-i 106-i 100-1 95-i 95-1 108-1 106-1 621-1 67-i 98-i 78-i 88-i 105-i 65-i 111-1 120-i 120-1 91-i 106-i 87-1 59-1 91-1 77-1 88-1 95-1 91-1 88-i 131-1 208-i 606-
-10.
-95--44--57--73--46--51--50--48--60--44--64--72--95--58--75--67--85--91--83--82--20--47--68--50--57--47--06--95--58--74--11--96--20-
-2 -4 -8 -1 -7 -6 -1 -7 -1 -5 -7 -1 -3 -1 -5 -9 -0 -1 -2 -1 -3 -8 -3 -7 -6 -8 -2 -4 -7 -4 -3 -8 •2
CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
-Phenol -b i s(2-ch 1 oroe -2-Chloropheno -1,3-DichIorob -1,4-Dichlorob -Benzyl a Icoho -1,2-Dichlorob -2-Methylpheno •b is(2-ch loro 1 •4-Methylpheno •N-Ni t roso-d i-•Hexachloroeth •N i t robenzene • I sophorone -2-Ni t ropheno1 -2,4-Dimethylp -Benzoic ac id -b i s(2-Ch1oroe -2,4-Dichlo rop -1,2,4-Trich lo -Naphthalene -4-Ch1o roan i 1 i -Hexach1orobu t -4-Chloro-3-me -2-Methylnapht -Hexachlorocyc -2,4,6-Trich lo -2,4,5-Tr ich1o •2-Ch1oronaph t •2-N11 roan i1 in -D1 me thyIphtha -Acenapht hy1 en -2,6-DinItroto
thy 1)ether 1 enzene enzene 1 enzene 1 sopropy1)ether 1 n-p ropylamine ane
heno 1
thoxy)methane heno 1 robenzene
ne ad iene t hy1pheno1 ha lene 1 open t ad i ene ropheno 1 ropheno 1 halene e late e luene
Q
1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 i 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 O C 4
dXai
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 -IU 1 IU 1 IU i IU 1 IU i IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 1 1
300427
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I I 1111185-03
Lab Name: INTECH Contract: 68-09-0048 I
.ab Code: INTECH Case No.:^2-^f'^r SAS No.: SDG No. : , , /'v
_Matri,.: [soil/water] WATER Lab Sample ID: ^•'/f ^^^
Sample wt/vol: 1000 [g/mL] ML Lab File ID: >BM70
"".evel: [low/med] LOW
% Mo 1 St ure: dec 100.
Date Receieved: :\l/27/91
Date Extracted: 12/01/91
extraction: [SepF/Cont/Sonc] SERF
G.PC Cleanup: [Y/N] N pH: 7.0
Date Analyzed: 12/03/91
Di lut ion Factor : |. 00
CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
99-83-51-
100-132-121-84-
7005-86-
100-534-86-
101-118-87-85-
120-84-
206-129-85-91-56-
218-117-117-205-207-50-
193-53-
191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-Sl-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-
-3-Ni t roan i1ine -Acenaphthene •2,4-Dinitrophenol •4-Ni t ropheno1 •Di benzofuran •2,4-Dinitrotoluene -Diethylphthalate •4-Chloropheny1-phenylether •Fluorene •4-Ni t roan i1ine •4,6-Dinitro-2-methylphenol •N-Ni trosodiphenylamine •4-Bromophenyl-phenylether -Hexachlorobenzene •Pentachloropheno1 •Phenanth rene •Anth racene • D i - n - b u t y l p h t h a l a t e •F1uo r a n t h e n e • P y r e n e • B u t y l b e n z y l p h t h a l a t e • 3 , 3 ' - D i c h l o r o b e n z i d i n e • B e n z o ( a ) a n t h r a c e n e • C h r y s e n e •bis(2-Ethylhexyl)phthalate •Di-n-octyIphthalate •Benzo(b)fiuoranthene •Benzo(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd)pyrene -Dibenz(a,h)anthracene - B e n z o ( g , h , i ) p e r y l e n e
Q
1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 50 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
FORM I SU-2 252 300428
IF ;.EMIUQLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
I 1111185-03 XI a b N 6 -: e : NTECH Contract: 68-D9-0048
,.„atri": soil/water) WATER
-•-ample i-.' vol: 1000 (g/mL) ML
Teve1: 'low/med) LOW
Moi?'_re: dec. 100.
Extraction: (SepF/Cont/Sonc) SERF
PC Cleanup: (Y/N) N pH: 7.0
Number TICs found: 1
Lab Sample ID: f - ^ ^ t ^ ^ K
Lab File ID: >B8070
Date Received: 11/27/91
Date Extracted: 12/01/91
Date Analyzed: 12/03/91
Dilut ion Factor: j.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/ L
CAS NUMBER 1 COMPOUND NAME 1 RT 1 E S T . CONC. 1 Q
^ ^ 1 . - - l U n k n o w n 1 5 . 08 1 1 2 . 1 J
" ' I I I I I I I I
1 ' 1 1 1
i 1 I I I " 1 I I I
I I I I I X 1 I I I
r 1 I I I
i 1 I I I
I I I I I
i~ 1 I I I
.1. 1 i 1 1
-,- 1 I I I
I I I I I 1 ' 1 1 1
^ ^ I I I
FORM I SU-TIC 1/87 Rev,
253 300429
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
..ab Name: INTECH
Lab Code: INTECH Case No.
Iatrix: (soil/water) SOIL
Sample wt/vol: 30. (g/mL) G
jevel: (low/med) LOW
% Moisture: not dec. 13. dec. 13.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 7.5
EPA SAMPLE NO.
59-63' Contract: 68-D9-0048
42-64 SAS No.: SDG No.: ANSON
Lab Sample ID:
Lab File ID: GP1134
Date Received: iU/21/91
Date Extracted:>!11/25/91
Date Analyzed: 11/29/91
CAS NO, COMPOUND
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 . 0 0
Q
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 76-44-8 Heptachlor
3 09-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4 , 4 ' -DDE 72-20-8 Endrin
33213-65-9 Endosulfan II 72-54-8 4 , 4 ' -DDD
1031-07-8 Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-4 3-5 Methoxychlor
53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-35-2 Toxaphene
12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-12 32 53 4 69-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260
9.2 9.2 9.2 9.2 9.2 9.2 9.2 9.2 18. 18. 18. 18. 18. 18. 18. 92. 18. 92. 92. 180. 92. 92. 92. 92. 92.
180. 180.
U U U U U U U U U U U U U U U U U U U U U U U U U U u
FORM I PEST 1 /87 R e v .
347 300430
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
.ab Name: INTECH
Lab Code: INTECH
F-BLANK Contract: 68-D9-0048
Case No.: 42-64 SAS No.: SDG No.: ANSON
"matrix: (soil/water) WATER
Sample wt/vol: 1000. (g/mL)ML
.evel: (low/med) LOW
% Moisture: not dec.100. dec. 0.
extraction: (SepF/Cont/Sonc) SERF
GPC Cleanup: (Y/N) N pH: 8.0
CAS NO. COMPOUND
Lab Sample ID: J l l f / ^ l ~ 3
Lab File ID: GP1138
Date Received: 11/21/91
Date Extracted: 11/22/91
Date Analyzed: 11/29/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC 76-44-8 Heptachlor 3 09-00-2 Aldrin 1024-57-3 Heptachlor 9 59-98-8 Endosulfan 60-57-1 Dieldrin 72-55-9 4 , 4 '-DDE 72-20-8 Endrin
3 3213-65-9 Endosulfan 72-54-8 4 , 4 ' -DDD
1031-07-8 Endosulfan 50-29-3 4 , 4 '^DDT
(Lindane)
epoxide I
II
sulfate
7 2-4 3-5 Methoxychlor 53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-35-2 Toxaphene
12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12 67 2-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 1109 6-82-5 Aroclor-1260
.050
.050
.050
.050
.050
.050
.050
.050 .10 .10 .10 .10 .10 .10 .10 .50 .10 .50 .50 1.0 .50 .50 .50 .50 .50 1.0 1.0
U U U U U U U U U U U u u u u u u u u u u u u u u u u
FORM I PEST 1/87 Rev.
351 300431
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
,ab Name: INTECH
Lab Code: INTECH Case No.: 42-64
Iatrix: (soil/water) SOIL
Sample wt/vol: 31. (g/mL) G
_,evel: (low/med) LOW
% Moisture: not dec. 23. dec. 23.
..xtraction: (SepF/Cont/Sonc) SONC
r.-pc Cleanup: (Y/N) N pH: 8.0
120-122' Contract: 68-D9-0048
SAS No.: SDG No.: ANSON
Lab Sample ID:
Lab File ID: GP1135
Date Received: 11/21/91
Date Extracted: 11/25/91
Date Analyzed: 11/29/91
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 . 0 0
Q
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 76-44-8 Heptachlor
3 09-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4 , 4 ' -DDE 72-20-8 Endrin
33213-65-9 Endosulfan II 72-54-8 4 , 4 ' -DDD
1031-07-8 Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-4 3-5 Methoxychlor
53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-3 5-2 Toxaphene
12674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12 67 2-29-6 Aroclor-1248 11097-69-1 Aroclor-12 54 11096-82-5 Aroclor-1260
10. 10. 10. 10. 10. 10. 10. 10. 20. 20. 20. 20. 20. 20. 20.
100. 20.
100. 100. 200. 100. 100. 100. 100. 100. 200. 200.
U U U U U U U U U U u u u u u u u u u u u u u u u u u
FORM I PEST
354
1 /87 R e v .
300432
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
..ab Name: INTECH
Lab Code: INTECH
F-BLANK Contract: 68-D9-0048
Case No.: 42-64 SAS No.: SDG No.: ANSON
Matrix: (soil/water) WATER
Sample wt/vol: 1000. (g/mL)ML
jevel: (low/med) LOW
% Moisture: not dec.100. dec. 0.
Jxtraction: (SepF/Cont/Sonc) SERF
GPC Cleanup: (Y/N) N pH: 8.0
CAS NO. COMPOUND
Lab Sample ID: Jj/f/^-^-^
Lab File ID: GP1139
Date Received: 11/21/91
Date Extracted: 11/22/91
Date Analyzed: 11/29/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 76-44-8 Heptachlor
3 09-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4 , 4 ' -DDE 72-20-8 Endrin
33213-65-9 Endosulfan II 72-54-8 4 , 4 ' -DDD
1031-07-8 Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-43-5 Methoxychlor
53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-35-2 Toxaphene
12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 53469-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-12 60
.050
.050
.050
.050
.050
.050
.050
.050 .10 .10 .10 .10 .10 .10 .10 .50 .10 .50 .50 1.0 .50 .50 .50 .50 .50 1.0 1.0
U U U U U U U U U U U U U U U U U U u u u u u u u u u
FORM I PEST 1/87 Rev.
300433
358
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
,ab Name: INTECH
Lab Code: INTECH
60-62' Contract: 68-D9-0048
Case No.: 42-64 SAS No.: SDG No.: ANSON
atrix: (soil/water) SOIL
Sample wt/vol: 30. (g/mL) G
evel: (low/med) LOW
% Moisture: not dec. 52. dec. 52.
xtraction: (SepF/Cont/Sonc) SONC
QPC Cleanup: (Y/N) N pH: 7.5
CAS NO. COMPOUND
Lab Sample ID: J'/z/Z f-/
Lab File ID: GP1147
Date Received: 11/26/91
Date Extracted: 11/27/91
Date Analyzed: 11/29/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 7 6-44-8 Heptachlor
3 09-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4, 4'-DDE 72-20-8 Endrin
33213-65-9 Endosulfan II 72-54-8 4 , 4 ' -DDD
1031-07-8 -Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-43-5 Methoxychlor
53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 510 3-74-2 gamma-Chlordane 8 001-35-2 Toxaphene
12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-12 32 534 69-21-9 Aroclor-1242 12 67 2-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260
17. 17. 17. 17. 17. 17. 17. 17. 33. 33. 33. 33. 33. 33. 33.
170. 33.
170. 170. 330. 170. 170. 170. 170. 170. 330. 330.
U U U U U U U U U U U U U U U U U U U U U U U U U U U
FORM I PEST 1 /87 R e v .
300434
361
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
,ab Name: INTECH
Lab Code: INTECH
75-77' Contract: 68-D9-0048
Case No.: 42-64 SAS No.: SDG No.: ANSON
atrix: (soil/water) SOIL
Sample wt/vol: 30. (g/mL) G
.evel: (low/med) LOW
% Moisture: not dec. 23. dec. 23.
xtraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 7.5
CAS NO. COMPOUND
Lab Sample ID: J l / / l l r^-2^
Lab File ID: GP1149
Date Received: 11/26/91
Date Extracted: 11/27/91
Date Analyzed: 11/29/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 76-44-8 Heptachlor
3 09-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4 , 4 ' -DDE 72-20-8 Endrin
33213-65-9 Endosulfan II 72-54-8 4,4'-DDD
1031-07-8 Endosulfan sulfate 50-29-3 4, 4'-DDT 72-43-5 Methoxychlor
53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8 001-35-2 Toxaphene
12674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-12 32 534 69-21-9 Aroclor-1242 12 67 2-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-12 60
10. 10. 10. 10. 10. 10. 10. 10. 21. 21. 21. 21. 21. 21. 21.
100. 21.
100. 100. 210. 100. 100. 100. 100. 100. 210. 210.
U U U U U U U U U U U U U u u u u u u u u u u u u u u
FORM I PEST 1 /87 R e v .
365 300435'
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
ab Name: INTECH
'Lab Code: INTECH
F-BLANK Contract: 68-D9-0048
Case No.: 42-64 SAS No.: SDG No.: ANSON
'atrix: (soil/water) WATER
Sample wt/vol: 1000. (g/mL)ML
evel: (low/med) LOW
% Moisture: not dec.100. dec. 0.
xtraction: (SepF/Cont/Sonc) SERF
GPC Cleanup: (Y/N) N pH: 7.5
CAS NO, COMPOUND
Lab Sample ID: 7//// -
Lab File ID: GP1143
Date Received: 11/26/91
Date Extracted: 11/27/91
Date Analyzed: 11/29/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 76-44-8 Heptachlor
309-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4 , 4 ' -DDE 72-20-8 Endrin
33213-65-9 Endosulfan II 72-54-8 4,4'-DDD
1031-07-8 Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-4 3-5 Methoxychlor
53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-3 5-2 Toxaphene
12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260
.050
.050
.050
.050
.050
.050
.050
.050 .10 .10 .10 .10 .10 .10 .10 .50 .10 .50 .50 1.0 .50 .50 .50 .50 .50 1.0 1.0
U U U U U U U U U U u u u u u u u u u u u u u u u u u
FORM I PEST 1/87 Rev.
369 300436
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
...ab Name: INTECH
Lab Code: INTECH
Contract: 68-D9-0048 60-62'
Case No.: 85-2060 SAS No.:
"Iatrix: (soil/water) SOIL
Sample wt/vol: 30. (g/mL) G
..evel: (low/med) LOW
% Moisture: not dec. 23. dec. 23.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 8.0
CAS NO. COMPOUND
SDG No.: ANSON
Lab Sample ID: J7////^$^- I
Lab File ID: GP2240
Date Received: 11/27/91
Date Extracted: 12/ 3/91
Date Analyzed: 12/14/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 76-44-8 Heptachlor
3 09-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4 , 4 ' -DDE 72-20-8 Endrin
33213-65-9 Endosulfan II 72-54-8 4 , 4 ' -DDD
1031-07-8 Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-43-5 Methoxychlor
53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8 001-35-2 Toxaphene
12674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260
10. 10. 10. 10. 10. 10. 10. 10. 21. 21. 21. 21. 21. 21. 21.
100. 21.
100. 100. 210. 100. 100. 100. 100. 100. 210. 210.
U U U U U U U U U U U U u u u u u u u u u u u u u u u
FORM I PEST 1 /87 Rev .
300437
372
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
.ab Name: INTECH
Lab Code: INTECH Case No.: 85-2060 SAS No
Iatrix: (soil/water) SOIL
Sample wt/vol: 31. (g/mL) G
.evel: (low/med) LOW
% Moisture: not dec. 18. dec. 18.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 7.3
74-76' Contract: 68-D9-0048
SDG No.: ANSON
Lab Sample ID: J//r/ r-Z-
Lab File ID: GP2241
Date Received: 11/27/91
Date Extracted: 12/ 3/91
Date Analyzed: 12/14/91
Dilution Factor: 1.00
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 76-44-8 Heptachlor
3 09-00-2 Aldrin 1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 4 , 4 ' -DDE 72-20-8 Endrin
33213-65-9 Endosulfan II 72-54-8 4,4'-DDD
1031-07-8 Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-43-5 Methoxychlor
53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8001-35-2 Toxaphene
12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 53469-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 11097-69-1 Aroclor-1254 11096-82-5 Aroclor-1260
9.6 9.6 9.6 9.6 9.6 9.6 9.6 9.6 19. 19. 19. 19. 19. 19. 19. 96. 19. 96. 96. 190. 96. 96. 96. 96. 96.
190. 190.
U U U u u u u u u u u u u u u u u u u u u u u u u u u
FORM I PEST
378
1/87 Rev.
300438
^ b
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
ib Name: INTECH
•Lab Code: INTECH
F-BLANK Contract: 68-D9-0048
Case No.: 85-2060 SAS No.: SDG No.: ANSON
•Iatrix: (soil/water) WATER
"Sample wt/vol: 940. (g/mL)ML
l,evel: (low/med) LOW
% Moisture: not dec.100. dec. 0.
Extraction: (SepF/Cont/Sonc) SERF
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
Lab Sample ID: J U i ] ^ f ^ 3
Lab File ID: GP2221
Date Received: 11/27/91
Date Extracted: 12/ 3/91
Date Analyzed: 12/13/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
319-84-6 alpha-BHC 319-85-7 beta-BHC 319-86-8 delta-BHC 58-89-9 gamma-BHC (Lindane) 7 6-44-8 Heptachlor 3 09-00-2 Aldrin
1024-57-3 Heptachlor epoxide 959-98-8 Endosulfan I 60-57-1 Dieldrin 72-55-9 -4 , 4 ' -DDE 72-20-8 Endrin
33213-65-9 Endosulfan II 72-54-8 4 , 4 ' -DDD
1031-07-8 Endosulfan sulfate 50-29-3 4 , 4 ' -DDT 72-43-5 Methoxychlor
53494-70-5 Endrin ketone 5103-71-9 alpha-Chlordane 5103-74-2 gamma-Chlordane 8 001-35-2 Toxaphene
12 674-11-2 Aroclor-1016 11104-28-2 Aroclor-1221 11141-16-5 Aroclor-1232 534 69-21-9 Aroclor-1242 12 672-29-6 Aroclor-1248 iio::7-69-i Aroclor-1254 1109 6-82-5 -Aroclor-1260
.053
.053
.053
.053
.053
.053
.053
.053 .11 .11 .11 .11 .11 .11 .11 .53 .11 .53 .53 1.1 .53 .53 .53 .53 .53 1.1 1.1
U U U U U U U U U U U U U U U U U U U U U U U U U U U
FORM I PEST 1/87 Rev.
300439 382
Unvalidated Data
Indoor borings 3 & 4
300440
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
}h Name: INTECH
Lab Code: INTECH
10-12' Contract: 68-D9-0048
Case No.: 61-68 SAS No.: SDG No.: ANSON
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
..Level: (low/med) LOW
„% Moisture: not dec. 1.
-Column: (pack/cap) PACK
CAS NO.
Lab Sample ID:
(g/mL) G Lab File ID: C9640
Date Received: 11/11/91
Date Analyzed: 11/19/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q COMPOUND
7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1, 1-Dichloroethene 75-34-3 1,1-Dichloroethane
540-59-0 1,2-Dichloroethene (total) 67-6 6-3 Chloroform
107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1, 1,1-Trichloroethane 5 6-23-5 Carbon Tetrachloride
108-05-4 Vinyl Acetate 7 5-2 7-4 Bromodichloromethane 7 8-87-5 1, 2-Dichloropropane
10 0 61-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 7 9-00-5 1, 1, 2-Trichloroethane 71-4 3-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane
108-8 8-3 Toluene 108-9 0-7 Chlorobenzene 10 0-41-4 Ethylbenzene 100-4 2-5 Styrene
lJ-JO-20-7 Xylene (total)
10. 10. 10. 10. 6.
25. 5. 5. 5. 5. 5. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5, 5. 5. 5. 5.
U U U U B
U U U U U U U U U U U U U U U U U U U U U
u u u u u
FORM I VOA 1 / 8 7 R e v ,
IS
300441
IE VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
b Name: INTECH
ab Code: INTECH Case No.
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 1.
Column: (pack/cap) PACK
Number TICs found: 1
10-12' Contract: 68-D9-0048
61-68 SAS No.: SDG No.: ANSON
Lab Sample ID:
(g/mL) G Lab File ID: C9640
Date Received: 11/11/91
Date Analyzed: 11/19/91
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 .00
CAS NUMBER
1. 110-54-3 2 . 3 . 4 . 5. 6. 7 . 8.
L ^• klG. • l l . 12. 13. 14 . 15. 16. 17. 18. 19. 20. 21. 22. 23 . 24 . 25. 26. 27. 28. 29. 30.
COMPOUND NAME
Hexane
RT
18.83
EST. CONC.
5.
Q
J
FORM I VOA-TIC 1/87 R e v .
- 19 30044?
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
ib Name: INTECH
Lab Code: INTECH
Contract: 68-D9-0048
Case No.: 61-68 SAS No.: SDG No
15-17'
ANSON
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 2.
Column: (pack/cap) PACK
CAS NO.
Lab Sample ID:
(g/mL) G Lab File ID: C9641
Date Received: 11/11/91
Date Analyzed: 11/19/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q COMPOUND
7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1,1-Dichloroethene 7 5-3 4-3 1,1-Dichloroethane 54 0-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene 1330-20-7 Xylene (total)
10. 10. 10. 10. 6.
19. 5. 5. 5. 5. 5. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U B
U U U U U U U U U U U U U U U U U U U U U U U U U u U u
FORM I VOA 1/87 Rev.
r, —
300443
IE VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
m b Name: INTECH ab Code: INTECH Case No
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 2.
Column: (pack/cap) PACK
Number TICs found: 1
EPA SAMPLE NO,
15-17' J (n«Ai~oZ
ANSON
Contract: 68-D9-0048
.: 61-68 SAS No.: SDG No.
Lab Sample ID:
(g/mL) G Lab File ID: C9641
Date Received: 11/11/91
Date Analyzed: 11/19/91
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1.00
- ^ J ^
---
CAS NUMBER
1. 1 1 0 - 5 4 - 3 2 . 3 . 4 . 5 . 6 . 7 . 8 .
k ^• | i o . F l l .
1 2 . 1 3 . 1 4 . 1 5 . 1 6 . 1 7 . 1 8 . 1 9 . 2 0 . 2 1 . 2 2 . 2 3 . 2 4 . 2 5 . 2 6 .
2 8 . 2 9 . 3 0 .
COMPOUND NAME
H e x a n e (DOT)(8CI9CI )
RT
1 8 . 8 2
EST. CONC,
5 .
FORM I VOA-TIC 1/87 Rev .
r. n
300444
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
b Name: INTECH
Lab Code: INTECH Case No,
Matrix: (soil/water) WATER
F-BLANK Contract: 68-D9-0048
61-68 SAS No.: SDG No.: ANSON
Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
CAS NO. COMPOUND
Lab File ID: C9558
Date Received: 11/11/91
Date Analyzed: 11/13/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1,1-Dichloroethene 75-34-3 1, 1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-6 6-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-9 3-3 2-Butanone 71-55-6 1,1, 1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 7 8-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-3 4-5 1,1, 2 , 2-Tetrachloroethane 108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 10 0-4 2-5 Styrene 1330-20-7 Xylene (total)
10. 10. 10. 10. 5.
68. 5. 5. 5. 5.
26. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 4. 5. 5. 5. 5.
U U U U B
U U U U
u u u u u U . U u u u u u U U u u u u J U U U U
FORM I VOA 1 / 8 7 R e v .
r-. o
30044^
IE VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
Name: INTECH
::ab Code: INTECH Case No,
'Matrix: (soil/water) WATER
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
' Number TICs found: 0
Contract: 68-D9-0048
61-68 SAS No.: SDG No
Lab Sample ID:
F-BLANK
ANSON
(g/mL) ML Lab File ID: C9558
Date Received: 11/11/91
Date Analyzed: 11/13/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 2 . 3. 4 . 5. 6. 7. 8.
^ ^ • lf°-PLI. 12. 13 . 14 . 15. 16. 17. 18. 19. 20. 21. 22 . 23. 24 . 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1 / 8 7 R e v ,
\J v
300446
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
m b Name: INTECH Contract: 68-D9-0048
Lab Code: INTECH Case No.: 61-68 SAS No.: SDG No
Matrix: (soil/water) SOIL
(g/mL) G
IB#3 ^ f . Z 7
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 2.
Column: (pack/cap) PACK
CAS NO. COMPOUND
ANSON
Lab Sample ID: Xlllo^^-?
Lab File ID: C9686
Date Received: 11/12/91
Date Analyzed: 11/23/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q
7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1,1-Dichloroethene 7 5-34-3 1,1-Dichloroethane
540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform
107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 5 6-23-5-^ Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene
100 61-02-6 trans-1, 3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-7 8-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1, 2, 2-Tetrachloroethane 108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene
1330-20-7 Xylene (total)
10. 10. 10. 10. 5.
26. 5. 5. 5. 5. 5. c 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U BJ B U U U U u u U u u u u u U u u u U U U u U u U u u u u u
FORM I VOA 1 / 8 7 R e v .
. -iO 300447
IE VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
^kab Name: INTECH Contract: 68-D9-0048
^ ^ b Code: INTECH Case No.: 61-68 SAS No.: SDG No.
-Matrix: (soil/water) SOIL
(g/mL) G
EPA SAMPLE NO.
IB#3 2.5--Z7
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 2.
Column: (pack/cap) PACK
Number TICs found: 0
ANSON
Lab Sample 10:3(1'°^*"^
Lab File ID: C9686
Date Received: 11/12/91
Date Analyzed: 11/23/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER
1. 2. 3 . 4 . 5. 6. 7. 8. 9.
|10. Fll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27 . 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1/87 Rev .
4x
3O044&'
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Fb Name: INTECH Contract: 68-D9-0048
Lab Code: INTECH Case No.: 61-68 SAS No.: SDG No
Matrix: (soil/water) SOIL
(g/mL) G
30-32'
Sample wt/vol: 5.0
Level: (low/med) LOW
.% Moisture: not dec. 2.
Column: (pack/cap) PACK
CAS NO, COMPOUND
ANSON
Lab Sample ID: i W l o i S ' ^
Lab File ID: C9668
Date Received: 11/12/91
Date Analyzed: 11/22/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q
7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1,1-Dichloroethene 7 5-3 4-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-6 6-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 5 6-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene
100 61-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-8 8-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene 1330-20-7 Xylene (total)
10. 10. 10.
' I : 15. 5. 5. 5. 5. 5. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U B B U U U U U U U U U U U U U U U U U U U U u u U U U U u U
FORM I VOA 1/87 Rev,
4v>
300449
IE VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
•. b Name: INTECH ab Code: INTECH Case No.
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 2.
Column: (pack/cap) PACK
Number TICs found: 0
30-32 Contract: 68-D9-0048
61-68 SAS No.: SDG No.: ANSON
Lab Sample ID: T\\\o(,$-<t'
Lab File ID: C9668
Date Received: 11/12/91
Date Analyzed: 11/22/91
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 .00
CAS NUMBER
1. 2 . 3. 4. 5. 6. 7. 8.
L ^• IlO. "ll. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 2b. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1/87 Rev .
300450
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
# b Name: INTECH Contract: 68-D9-0048
Lab Code: INTECH Case No.: 61-68 SAS No.: SDG No
Matrix: (soil/water) SOIL
5.0 (g/mL) G
35-37'
Sample wt/vol:
Level: (low/med) LOW
% Moisture: not dec. 3
Column: (pack/cap) PACK
CAS NO, COMPOUND
ANSON
Lab Sample ID: J i \ io( i r$-4
Lab File ID: C9669
Date Received: 11/12/91
Daite Analyzed: 11/22/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q
7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-35-4 1,1-Dichloroethene 7 5-3 4-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 78-9 3-3 2-Butanone 71-55-6 1, 1, 1-Trichloroethane 56-23-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 7 8-87-5 1,2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 12 4-4 8-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-7 8-6 2-Hexanone 12 7-18-4 Tetrachloroethene /9-34-b 1,1, 2, 2-Tetrachloroethane
108-88-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 Ethylbenzene 100-4 2-5 Styrene
1330-20-7 Xylene (total)
10. 10. 10. 10. 6.
15. 5. 5. 5. 5. 5. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U B B U U U U U U U U U U U u u u u u u u u u u u u u u u u u
FORM I VOA 1/87 Rev,
J 2
300451
IE VOLATILE ORGANICS ANALYSIS DATA SHEET - TENTATIVELY IDENTIFIED COMPOUNDS
«
b Name: INTECH
ab Code: INTECH
EPA SAMPLE NO,
35-37 Contract: 68-D9-0048
Case No.: 61-68 SAS No.: SDG No.: ANSON
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 3.
Column: (pack/cap) PACK
Number TICs found; 0
Lab Sample ID: J(//o < -
(g/mL) G Lab File ID: C9669
Date Received: 11/12/91
Date Analyzed: 11/22/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER
1. 2 . 3. 4. 5. 6. 7. 8.
L ^• kio. ^ 1 1 . 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22 . 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1/87 R e v .
r •"I
300452
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
Ib Name: INTECH
Lab Code: INTECH Case No.
Matrix: (soil/water) WATER
F-BLANK Contract: 68-D9-0048
61-68 SAS No.: SDG No.: ANSON
Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
CAS NO, COMPOUND
Lab File ID: C9564
Date Received: 11/12/91
Date Analyzed: 11/13/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
74-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 7 5-3 5-4 1, 1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-6 6-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene
100 61-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1,2, 2-Tetrachloroethane 108-8 8-3 Toluene 108-9 0-7 Chlorobenzene 100-41-4 —Ethylbenzene 10 0-42-5 Styrene
1330-20-7 Xylene (total)
10. 10. 10. 10. 5.
33. 5. 5. 5. 5.
20. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5.
I : 5 . 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U B
U U U U
U u U U U U U U U u u u u u u u u u u u u u u
FORM I VOA 1/87 Rev,
300453
IE VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
^tob Name: INTECH
^ R b Code: INTECH Case No,
-••Matrix: (soil/water) WATER
'Sample wt/vol: 5.0
•"Level: (low/med) LOW
"% Moisture: not dec. 100.
"Column: (pack/cap) PACK
Number TICs found: 0
EPA SAMPLE NO,
F-BLANK
61-68
(g/mL) ML
Contract: 68-D9-0048
SAS No.: SDG No.: ANSON
Lab Sample ID:
Lab File ID: C9564
Date Received: 11/12/91
Date Analyzed: 11/13/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 2. 3. 4 . 5. 6. 7. 8.
. 9-|10. Wii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1/87 Rev.
300454
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: INTECH
Lab Code: INTECH Case No.
Matrix: (soil/water) WATER
EPA SAMPLE NO.
T-BLANK Contract: 68-D9-0048
61-68 SAS No.: SDG No.: ANSON
Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML
..Level: (low/med) LOW
..% Moisture: not dec. 100.
Column: (pack/cap) PACK
CAS NO. COMPOUND
Lab File ID: C9565
Date Received: 11/12/91
Date Analyzed: 11/13/91
Dilution Factor: 1.00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
""
•
7 4-87-3 Chloromethane 7 4-83-9 Bromomethane 75-01-4 Vinyl Chloride 7 5-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1, 1-Dichloroethene 75-34-3 1, 1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1, 2-Dichloroethane 7 8-93-3 2-Butanone 71-55-6 1, 1,1-Trichloroethane 56-2 3-5 Carbon Tetrachloride 108-05-4 Vinyl Acetate 7 5-27-4 Bromodichloromethane 7 8-87-5 1, 2-Dichloropropane
10061-01-5 cis-l, 3-Dichloropropene 7 9-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1, 2-Trichloroethane 71-4 3-2 Benzene
10061-02-6 trans-1,3-Dichloropropene 7 5-2 5-2 Bromof orm 108-10-1 4-Methyl-2-Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 7S-34-5 1,1, 2, 2-Tetrachloroethane 108-8 8-3 Toluene 108-9 0-7 Chlorobenzene
• 100-41-4 Ethylbenzene 10 0-4 2-5 Styrene 1330-20-7 Xylene (total)
10. 10. 10. 10. 4.
330. 5. 5. 5. 5. 5. 5.
10. 5. 5.
10. 5. 5. 5. 5. 5. 5. 5. 5. 5.
10. 10. 5. 5. 5. 5. 5. 5. 5.
U U U U BJ
E u u U u u u u u u u u u u u u u u u u u u u u u u u u u
FORM I VOA 1 / 8 7 R e v .
300456
I IE VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
fab Name: INTECH
ab Code: INTECH Case No.: 61-68
"Matrix: (soil/water) WATER
Contract: 68-D9-0048
SAS No.: SDG No,
Lab Sample ID:
T-BLANK Xli
ANSON
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dec. 100.
Column: (pack/cap) PACK
Number TICs found: 0
(g/mL) ML Lab File ID: C9565
Date Received: 11/12/91
Date Analyzed: 11/13/91
Dilution Factor: l.oo
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 2. 3. 4 . 5. 6. 7. 8. 9.
|io. rii. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22 . 23. 24 . 25. 26. 27. 28. 29. 30.
COMPOUND NAME RT
.
EST. CONC. Q
FORM I VOA-TIC 1/87 Rev.
G8
300456
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111061-01 Lab Name: INTECH Contract: 68-09-0048 I
\h CocJe: INTECH Case Ho. : ^) - ( fh SAS No.: SDG No.: /^/vSo.t/
Matrix: [soiI/water] SOIL
-Sample wt/vol: 30.00 [g/mLl G
Level: [low/meidl LOU)
'% Moisture: j, dec. I.
Extraction: [SepF/Cont/Sonc] SONC
GPC Cleanup: [Y/Nl N pH: 7.0
Lab Sample ID:
Lab File ID: >B7957
Date Received: 11/11/91
Date Extracted: 11/15/91
Date Analyze(d: 11/20/91
Dilut ion Factor : \ .00
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108-111-95-
541-106-100-95-95-
108-106-621-67-98-78-88-
105-€ ^ -
111-120-120-91-
106-87-59-91-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-
-Phenol -bis(2-chloroet -2-Chloropheno1 -1,3-Dichlorobe •1,4-Dichlorobe •Benzy1 a Icoho1 -1,2-Dichlorobe •2-Methylpheno1 •bis(2-chIorois -3&4-MethyIphen -N-Nitroso-di-n •Hexachloroetha •Nit robenzene - Isophorone •2-Ni t ropheno1 -2,4-DimethyIph -Benzoic acid •b is(2-Chloroet -2,4-Dichloroph -1,2,4-Trichlor -Naphthalene •4-Chloroan i1 in •Hexachlorobuta •4-Chloro-3-met •2-Methylnaphth •Hexach1oroeycl •2,4,6-Tr ichlor -2,4,5-Tr ichlor •2-Chloronaphth •2-Ni t roan i1ine •Dime thyIphtha1 •Acenaphthylene •2,6-DinItroto1
hy1)ether
nzene nzene
nzene
opropyl)ether ol -propylamine ne
eno 1
hoxy)methane eno I obenzene
e d iene hy1pheno1 a lene opentad iene opheno I opheno 1 a 1 ene
ate
uene
FORM I SU-1
Q
340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 340
1700 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
•^ -«t •J^v
30045?:
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111061-01
#
Lab Name: INTECH Contract: 68-D9-0048 I
b Code: INTECH Case No.: /-^S . SAS No.: SDG No.: / i ^ ^ o ^
Matrix: [soil/water] SOIL
Sample wt/vol: 30.00 [g/mL] G
Level: [low/med] LOW
„ - \ Moisture: I, dec. |.
Extraction: [SepF/Cont/Sonc] SONC
"GPC Cleanup: [Y/N] N pH: 7.0
Lab Sample ID:
Lab File ID: >B7957
Date Received: 11/11/91
Date Extracted: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor: (.00
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
99 83 51-
100-132 121-84-
7005 86 100 534 86 101 118 87-85-
120-84-
206-129-85-91-56
218' 117 117 205 207-50-
193-53
191.
-09-2--32-9--28-5--02-7--64-9-•14-2-•73-7--72-3--73-7--01-6--52-1--30-6--55-3--74-1--86-5--01-8--12-7--74-2--44-0--00-0-•68-7-•94-1--55-3--01-9--81-7--84-0--99-2-•08-9--32-8--39-5--70-3--24-2-
•3-Ni t roan i1 -Acenaphthen •2,4-Dinit ro •4-Ni t rophen •D ibenzofura -2,4-Dini tro •Diethylphth -4-Chlorophe -F1uorene -4-Ni t roan i1 -4,6-Din i t ro -N-Ni t rosod i -4-Bromophen -Hexachlorob •Pent achloro •Phenanthren •An thracene •Di-n-butyIp •Fluoranthen •Pyrene •ButyIbenzy1 -3,3'-Dichlo •Benzo(a)ant -Chrysene -bis(2-Ethyl -Di-n-octyIp •Benzo(b)flu •Benzo(k)f lu -Benzo(a)pyr - Indeno(1,2, -Dibenz(a,h) -Benzo(g ,h , i
1 ne e pheno1 ol n to luene a late ny1-phenylether
ine -2-methylphenol phenylam ine y 1 -phenylether enzene pheno1
htha late e
phthalate robenz id i ne hracene
hexyl)phthalate htha la te oran thene oran t hene ene 3-cd)pyrene anth racene )pe rylene
1700 340 340 1700 340 340 340 340 340 1700 1700 340 340 340
1700 340 340 340 340 340 340 670 340 340 190 340 340 340 340 340 340 340
Q
IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I 3 IU IU IU IU iU IU IU
FORM I SU-2 1 ' - ' Xuvj
300458
f, IF
SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
I 1111061-01 ab Name: INTECH Contract: 68-D9-0048 I
..Matrix: (soil/water) SOIL
-Sample wt/vol: 30.00 (g/mL) G
Level: (low/med) LOU)
% Mo ISture: |. dec. |.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 7.0
Number TICs found: 3
Lab Sample ID:
Lab File ID: >B7957
Date Received: 11/11/91
Date Extracted: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor: \ .oo
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER
1. 2. 3.
4127-47-3
COMPOUND NAME
Cyclopropane, 1,1,2 ,2-tetram Aldol Condensation t"y / i/ Aj) Unknown
RT
2.71 3.64
27.86
EST. CONC,
300. 9800. 170.
Q
J J J
FORM I SU-TIC 1/87 Rev
lo7 .. 300459
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I 1111061-02 Lab Name: INTECH
ib Code: INTECH
Matrix: [soil/water] SOIL
Sample wt/vol: 3 0.00 [g/mL] G
.Level: [low/med] LOU
-% Moisture: Z. dec. 2- .
"Extraction: [SepF/Cont/Sonc] SONC
'GPC Cleanup: [Y/N] N pH: 7.1
Contract: 68-D9-0048 I
Case No.: ^I '^B' SAS No.: SDG Ho. : / ^ ^ t'^'^
Lab Samp 1e ID:
Lab File ID: >B7958
Date Received: 11/11/91
Date Extracted: 11/15-'91
Date Analyzed: 11/20/91
CAS NO. COMPOUND
Di lut ion Factor:
CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108-95-2 Phenol 111-44-4 bis (2-ch loroethyl )ether 95-57-8 2-Ch loropheno 1
541-73-1 1,3-Dich lorobenzene 106-46-7 1,4-Dichlorobenzene 100-51-6 Benzyl alcohol 95-50-1 1,2-Dich lorobenzene 95-48-7 2-Methylphenol 108-60-1 b is(2-chloroisopropyl)ether 106-44-5 3&4-Me thy I phenol 621-64-7 N-Nitroso-d1-n-propy lamine 67-72-1 Hexach loroethane 98-95-3 Nit robenzene 78-58-1 Isophorone 88-75-5 2-N It ropheno I 105-67-9 2,4-Dimethylphenol 65-35-0 Benzoic acid 111-91-1 bis(2-Chloroethoxy) me thane 12 0-83-2 2,4-Dichlorophenol 120-82-1 1,2,4-Inch lorobenzene 91-2 0-3 Naphthalene
106-47-8 4-Chloroani 1 ine 87-68-3 He xach lorobutad iene 59-5 0-7-^ 4-Chloro-3-methylphenol 91-57-6 2-Methylnaphthalene 77-47-8 Hexach lorocyc lopentad iene 88-06-2 2,4,6-Tr ich loropheno I 95-95-4 2,4,5-Trichlorophenol 91-58-7 2-Ch loronaphtha lene 88-74-4 2-Ni t roam I ine 131-11-3 Dimethylphthalate 208-96-8 Acenaphthylene 606-20-2 2,6-Dinitrotoluene
FORM I SU-1
\ 0</
Q
340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340
IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU tu IU IU IU IU IU IU IU IU IU IU IU 1
3G. 300460
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I 1111061-02
#
Lab Name: INTECH Contract: 68-D9-0048 I
b Code: INTECH Case No.: ^|-^S SAS No.: SDG No.: ^^.-/o^
Matrix: [soil/water] SOIL
Sample wt/vol: 30.00 [g/mLl G
.-Level: [low/med] LOW
% Moisture: 2.- dec. 2..
"Extraction: [SepF/Cont/Sonc] SONC
GPC Cleanup: [Y/N] N pH: 7.1
Lab Sample ID:
Lab Flle ID: >B7958
Date Received: 11/11/91
Date Extracted: 11/15/91
Date Analyzed: 11/20/91
Dilution Factor: \,o<)
CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG Q
99-83-51-100-132-121-84-
7005-86-
100-534-86-101-118-87-85-120-84-
206-129-85-91-56-
218-117-117-205-2 07-50-
193-53-
191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-•44-0-00-0-68-7-94-1-55-3-01-9-•81-7-•84-0-•99-2-08-9-32-8-39-5-70-3-24-2-
-3-Ni t roan i1ine -Acenaphthene -2 ,4-Din i t ropheno1 -4-Ni t ropheno1 -D ibenzofuran -2,4-Dinitrotoluene •Diethylphthalate •4-Chlorophenyl-phenylether -Fluorene •4-Ni t roan i1i ne •4,6-Dinitro-2-methylphenol -N-Nitrosodiphenylamine -4-Bromophenyl-phenylether -Hexachlorobenzene -Pentachloropheno1 -Phenanthrene -Anthracene -Di-n-butyIphthalate -Fluoranthene -Pyrene -ButylbenzyIphtha late -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene -bis(2-Ethylhexyl)phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Be n z o(k)fluoranthene -Benzo(a)pyrene -Indeno(l,2,3-cd;vyrene - D i b e n z ( a , h ) a n t h r a c e n e - B e n z o ( g , h , i ) p e r y l e n e
FORM I SU-2
1 1700 1 340 1 340 1 1700 1 340 1 340 1 340 1 340 1 340 1 1700 1 1700 1 340 1 340 1 340 1 1700 1 340 1 340 1 340 1 340 1 340 1 340 1 680 1 340 1 340 1 320 1 340 1 340 1 340 1 340 1 340 1 340 1 340
1 IU iU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU 1 J IU IU IU IU IU IU IU 1
IG J
300461
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
1 1111061-02 Lab Name: INTECH Contract: 68-D9-0048
Matrix: (soil/water) SOIL
Sample wt/vol: 30.00 (g/mL) G
Level: (low/med) LOU)
.% Moisture: 2-. dec. 2. .
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 7.1
- Number TICs found: 3
Lab Sample ID:
Lab File ID: >B7958
Date Received: 11/11/91
Date Extracted: 11/15/91
Date Analyzed: 11/20/91
Dilut ion Factor: 1-^0
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
I I I I I 1 CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q
1 1 . - - lUnknown 1 2 . 7 1 1 3 1 0 . 1 J ^ 2 . - - 1 A l d o l - C o n d e n s a t ionfvo(/L-c-r(ivK-v».^ 3 . 6 4 1 1 1 0 0 0 . 1 3 P 3 . - - lUnknown 1 2 7 . 8 6 1 1 7 0 . 1 3
1 * 1 1 1 1
FORM I S U - T I C 1/87 Rev,
iG.:>
30046e
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I 1111061-03 Lab Name: INTECH Contract: 68-D9-0048 I
sb Code: INTECH Case No.: ^ \ ' ( ?^ SAS No.: SDG No.: I^^^<^H
Matrix: [soil/water] WATER Lab Sample ID:
Sample wt/vol: 1000 [g/mL] ML Lab File ID: >B7949
Level: [low/med] LOW Date Receieved: 11/11/91
% Moisture: dec 100. Date Extracted: 11/14/91
Extraction: [SepF/Cont/Sonc] SERF
GPC Cleanup: [Y/N] N pH: 7.0
COMPOUND ,
Date Analyzed: 11/20/91
Dilution Factor: f.OO
CAS NO.
1 108-1 111-1 95-1 541-1 106-l 100-1 95-1 95-1 108-1 106-1 621-1 67-1 98-1 78-1 88-1 105-1 65-1 111-1 120-1 120-1 91-1 106-1 87-1 59-1 91-1 77-1 88-1 95-1 91-1 88-1 131 1 208 i 606
•95-•44-•57-•73-•46-•51-•50--48--60--44-•64--72--95--58--75--67--85--91--83--82--20--47--68--50--57--47--06^ -95--58--74. -11 -96 -20
2-4-•8-1-•7-•6-•1-
• 7
-1-•5-
• 7 -
•1-
-3-•1
•5-
-9 -0-•1-
-2 -1 -3 -8 -3 -7 -6 -8 -2 -4 -7 -4 -3 -8 -2
CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
Pheno 1 bis(2-chloroethyl)ether 2-Chloropheno 1 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl alcohol 1,2-Dichlorobenzene 2-Methylphenol bis(2-chloroisopropyl)ether 4-MethylphenoI N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene I sophorone 2-NitrophenoI 2,4-Dimethylphenol Benzoic acid bis(2-Chloroethoxy)me thane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroani1ine Hexachlorobutadiene 4-Chloro-3-methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene
----2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-NitroaniIine Dimethylphthalate Acenaphthy Iene 2,6-Dinitrotoluene
FORM I SU-1
Q
1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 10
10 1 10 1 10 1 10 1 10 1 50 1 10 1 10 1 10
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 IU 1 IU \ IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU IU 1 1
IV.:;
300463
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
1111061-03 Lab Name: INTECH
fb Code: INTECH Case No.
Matrix: [soil/water] WATER
Sample wt/vol: 1000 [g/mL] ML
Level: [low/medl LOW
% Moisture: dec 100.
Extraction: [SepF/Cont/Sonc] SERF
GPC Cleanup: [Y/N] N pH: 7.0
Contract: 68-D9-0048 I
I P ) ' ( J ^ SAS No.: SDG No.: /}A-i<5'
Lab Sample ID:
Lab File ID: >B7949
Date Receieved: 11/11/91
Date Extracted: 11/14/91
Date Analyzed: 11/20/91
Di lut ion Factor: | .00
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
99-83-51-100-132-121-84-
7005-86-
100-534-86-101-118-87-85-120-84-
206-129-85-91-56-
218-117-117-205-207-50-193-53-191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-
-3-Ni t roan iii -Acenaphthene -2,4-Dinitrop -4-Ni t ropheno -Dibenzofuran -2 ,4-Dini trot •Die thyIphtha •4-Chlorophen •Fluorene •4-Nit roan i1i •4,6-Din i t ro--N-Ni t rosod i p •4-Bromopheny •Hexachlorobe -Pentachlorop -Phenanthrene -Anthracene -Di-n-butyIph -Fluoranthene -Pyrene -ButyIbenzyIp -3,3'-Dichlor -Benzo(a)anth -Chrysene •bis(2-Ethylh -Di-n-octyIph •Benzo(b)fluo •Benzo(k)fluo -Benzo(a)pyre - Indeno(1,2,3 •Dibenz(a ,h )a -Benzo(g ,h , i )
ne
heno 1 1
0 luene late y1-phenylether
ne 2-me thyIpheno1 heny1 ami ne 1 -phenylet her nzene heno 1
tha late
htha late obenz id ine racene
exy1)phtha 1 ate tha la te ranthene rant hene ne -cd)pyrene n thracene perylene
50 10 10 50 10 10 10 10 10 50 50 10 10 10 50 10 10 10 10 10 10 20 10 10 3 10 10 10 10 10 10 10
FORM I SU-2
Q
IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I J IU IU IU IU IU IU IU
IV; 300464
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
I 1111061-03 Lab Name: INTECH Contract: 68-D9-0048
• . Tatrix: (soil/water) WATER
"Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
?6 Moisture: dec. 100.
Extraction: (SepF/Cont/Sonc) SERF
GPC Cleanup: (Y/N) N pH: 7.0
Number TICs found: 1
Lab Samp 1e ID:
Lab File ID: >B7949
Date Received: 11/11/91
Date Extracted: 11/14/91
Date Analyzed: 11/2 0/91
Di lut ion Factor: | .00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/ L
1 CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q 1
1 1 . - - lUnknown 1 5 . 1 3 1 1 2 . 1 J f i 1
"' 1 1 1 1 I I
. t 1 1 1 I I
A I I I I W I I I I
- 1 1 I I I I
- 1 1 I I I I
- - 1 1 I I I I
- 1 1 I I I I
1 1 I I I I
FORM I SU-T IC 1 / 8 7 Rev
IV,}
300465
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I 1111068-03 Lab Name: INTECH Contract: 68-D9-0048 I
b Code: INTECH Case No.: U'lp9' SAS No.: SDG No. : JV; /*
Lab Sample ID:
Lab File I D : >B7965
Date Received: 11/12/91
Date Extracted: 11/15/91
Date Analyzed: 11/21/91
Dilution Factor: \.oo
Matrix: [soil/water] SOIL
Sample wt/vol: 30.17 [g/mL] G
Level: [low/medl LOW
% Moisture: 2-. dec. 2..
Extraction: [SepF/Cont/Sonc] SONC
GPC Cleanup: [Y/N] N pH: 8.0
CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108-111-95-
541-106-100-95-95-
108-106-621-67-98-78-88-
105-65-
111-120-120-91-106-87-59-91-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-50-7-57-6-47-8-06-2-•95-4-58-7-74-4-11-3-96-8-20-2-
•Pheno1 -bis(2-chloroethyl)ether •2-Chloropheno1 •1,3-Dichlorobenzene •1,4-Dichlorobenzene •Benzyl a Icoho1 •1,2-Dichlorobenzene •2-Methylphenol •bis(2-chloroisopropyl)ether •3&4-Methylpheno1 -N-Nitroso-di-n-propylamine -Hexachloroethane •Nit robenzene • Isophorone -2-Ni t rophenoI -2,4-Dime thy IphenoI -Benzoic acid -bis(2-Chloroethoxy)me thane -2,4-Dichlorophenol -1,2,4-Trichlorobenzene -Naphthalene -4-Chloroani1ine -Hexachlorobutadiene -4-Chloro-3-methylphenol -2-Methylnaphthalene -Hexachlorocyclopentadiene -2,4,6-TrichlorophenoI -2,4,5-Trichlorophenol -2-Chloronaphthalene -2-Ni t roan iIine -Dimethylphthalate -Acenaphthylene -2,6-Dinitrotoluene
FORM I SU-1
Q
340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340 340 340 340 340 340 340 340 340 340 1700 340 340 340
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU - 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
IGO,, 30046iB
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
Lab Name: INTECH
l^b Code: INTECH Case No.: 6/- ^
Matrix: [soil/water] SOIL
Sample wt/vol: 30.17 [g/mL] G
Level: [low/med] LOW
-% Mo isture : 2. dec . .
Extraction: [SepF/Cont/Sonc] SONC
GPC Cleanup: [Y/N] N pH: 8.0
I I 1111068-03
Contract: 68-D9-0048 I
SAS No.: SDG No.: /^ /y io^
Lab Sample ID:
Lab File ID: >B7965
Date Received: 11/12/91
Date Extracted: 11/15/91
Date Analyzed: 11/21/91
Dilution Factor: l.OO
CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
99-83-51-10 0-132-121-84-
7005-86-10 0-534-86-
101-118-87-85-
120-84-
206-129-85-91-56-
218-117-117-205-207-50-
193-53-191-
09-2-32-9-28-5-02-7-64-9-14-2-73-7-72-3-73-7-01-6-52-1-30-6-55-3-74-1-86-5-01-8-12-7-74-2-44-0-00-0-68-7-94-1-55-3-01-9-81-7-84-0-99-2-08-9-32-8-39-5-70-3-24-2-
-3-Ni t roa -Acenapht -2,4-Dini -4-Ni t rop -Dibenzof -2,4-Dini -Die thyIp •4-Chloro •Fluorene •4-Ni t roa -4,6-Dini •N-Ni t ros •4-Bromop •Hexachlo •Pent achI -Phenanth -An thrace •Di-n-but -Fluorant •Pyrene -ButyIben -3,3'-Dic -Benzo(a ) -Chrysene -bis(2-Et -Di-n-oct -Benzo(b) •Benzo(k ) -Benzo(a ) - Indeno (1 •D ibenz (a •Benzo(g ,
n iIine hene t ropheno 1 heno 1 uran t roto luene htha late phenyl-phenylether
n i I ine tro-2-methy I phenol odiphenyI amine henyl-phenylet her robenzene oropheno I rene ne y Iphtha late hene
zyIphthalate h I orobenz i d ine anthracene
hyIhexyI)phthalate y Iphtha late f luo ran thene f luoranthene pyrene ,2 ,3-cd)pyrene ,h )anth racene h,i)pe ry1ene
1700 340 340 1700 340 340 340 340 340 1700 1700 340 340 340 1700 340 340 340 340 340 340 680 340 340 320 340 340 340 340 340 340 340
FORM I SU-2
Q
IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I 3 IU IU IU IU IU IU IU
300467
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
I 1111068-03 Lab Name: INTECH Contract: 68-D9-0048
Matrix: (soil/water) SOIL
Sample wt/vol: 30.17 (g/mL) G
.Level: (low/med) LOW
% Moisture: 2. dec. 2-.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 8.C
Number TICs found: 4
Lab Sample ID:
Lab File ID: >B7965
Date Received: 11/12/91
Date Extracted: 11/15/91
Date Analyzed: 11/21/91
Dilution Factor: ). oo
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 CAS NUMBER 1 COMPOUND NAME 1 RT ( ss = s5=:s: = 35 = =: = 3=a»3sss= | =s = = = = = = = = = = = as = =i = = = = = = = = = = = = = | s= = ss = » = = =
1 1 . - - lUnknown 1 1.70 ^ 2 . - - 1 Aldol Condensat ion-Pro/ycr(/» «V«i#'/K,) 3.6 0 P 3. - - lUnknown 1 5.19 1 4 . - - lUnknown 1 7.52
EST. CONC,
2 0 0 . 3 7 0 0 .
1 4 0 . 2 7 0 .
FORM 1 S U - T I C
Q
3 3 3 3
1 /87 Re^-t f - o
300488
ib SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111068-05 Lab Name: INTECH
kb Code: INTECH Case No ( ? l - l , ^
Matrix: [soil/water] SOIL
Sample wt/vol: 30.21 [g/mL] G
Level: [low/med] LOW
C c - i t r a c t : 6 8 - D 9 - 0 0 4 8 I
SAS N o . : SDG N o . : / iA^So/V
Lab Sample I D :
Lab F i l e I D : >B7966
D a t e R e c e i v e d : 1 1 / 1 2 / 9 1
% M o i s t u r e : 2 . d e c . 2 .
Extraction: [SepF/Cont/Sonc] SONC
GPC Cleanup: [Y/N] N pH: 7.5
CAS NO. COMPOUND
Date Extracted: 11/15/91
Date Analyzed: 11/21/91
Di lut ion Factor
CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
1 108-1 111-1 95-1 541-1 106-1 100-1 95-1 95-1 108-1 106-1 621-1 67-1 98-1 78-1 88-1 105-1 65-1 111-1 120-1 120-1 91-1 106-1 87-1 59-1 91-1 77-1 88-1 95-1 91-1 86-1 131-1 208-1 606-
-95--44--57--73--46--51--50--48--60--44--64--72--95--58--75--67--85--91--83--82--20--47--68--50--57--47--06--95--58--74--11--96--20-
•2 • 4 -8 -1 -7 -6 •1 -7 •1 -5 -7 -1 -3 -1 -5 -9 -0 -1 -2 -1 -3 -8 -3 -7 -6 -8 -2 -4 -7 -4 -3 -8 -2
Phenol bis(2-chloroethyl)ether 2-Chloropheno1 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzyl alcohol 1,2-Dichlorobenzene 2-Methylphenol bis(2-chloroisopropyl)ether 3&4-Methylphenol N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-NitrophenoI 2,4-Dime thy I phenol Benzoic acid bis(2-Chloroethoxy)me thane 2,4-DichlorophenoI 1,2,4-Trichlorobenzene Naphthalene 4-Chloroani1ine Hexachlorobutadiene 4-Chloro-3-methylphenol 2-Methylnaphthalene HexachlorocycI open tadiene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroani1ine Dime thyIphthalate Acenaphthylene 2,6-Dinitrotoluene
FORM I SU-1
\ . o O
1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 1700 i 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 330 1 1700 1 330 1 330 1 330
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 1 1
300469
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I I 1111068-05
Lab Name: INTECH Contract: 68-D9-0048 I
lb Code: INTECH Case No.: 6/-^^ SAS No.: SDG No.: A ' ^ i O i v
Matrix: [soil/water] SOIL
Sample wt/vol: 30.21 [g/mLl G
Level: [low/med] LOW
% Moisture: 2. dec. 2 -
Extraction: [SepF/Cont/Sonc] SONC
GPC Cleanup: [Y/N] N pH: 7.5
Lab Sample ID:
Lab File ID: >B7966
Date Received: 11/12/91
Date Extracted: 11/15/91
Date Analyzed: 11/21/91
Dilution Factor: l.oo
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
99-09-2 3-Ni t roan il ine 83-32-9 Acenaphthene 51-28-5 — 2,4-Dinitrophenol 100-02-7 4-Nit ropheno 1 132-64-9 Dibenzofuran 121-14-2 2,4-Din it roto luene 84-73-7 Diethylphthalate
7005-72-3 4-Chlorophenyl-phenylet her 86-73-7 Fluorene 100-01-6 4-Nit roan i 1 ine 534-52-1 4,6-Dinitro-2-methylphenol 86-30-6 N-Nitrosodiphenylamine 101-55-3 4-Bro mo phenyl-phenylether 118-74-1 Hexach lorobenzene 87-86-5 Pentach loropheno 1 85-01-8 Phenanthrene 12 0-12-7 Anthracene 84-74-2 Di-n-butylphthalate
2 06-44-0 Fiuoranthene 129-0 0-0 Pyrene 85-68-7 Butylbenzylphthalate 91-94-1 3,3'-Dich lorobenz id ine 56-55-3 Benzo (a )anthracene
218-01-9 Chrysene 117-81-7 bis(2-Ethylhexyl)phthalate 117-84-0 Di-n-octylphthalate 2 05-99-2 Benzo (b)f luoranthene 207-08-9 Be nzo (k)f luoranthene 5 0-32-8 Benzo(a)pyrene 193-39-5 Indeno (1,2, 3-cd) pyrene 53-70-3 D ibenz ( a, h) an thracene 191-24-2 Benzo (g,h, I ) perylene
1700 330 330 1700 330 330 330 330 330 1700 1700 330 330 330 1700 330 330 330 330 330 330 670 330 330 240 330 330 330 330 330 330 330
FORM I SU-2
Q
IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I J IU IU IU IU IU IU IU
13i
300470
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
I 1111068-05 Lab Name: INTECH Contract: 68-D9-0048 I
Matrix: (soil/water) SOIL
Sample wt/vol: 30.21 (g/mL) G
Level: (low/med) LOU
% Moisture: 2.. dec. Z-
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 7.5
Number TICs found: 3
Lab Sample ID:
Lab File ID: >B7966
Date Received: 11/12/91
Date Extracted: 11/15/91
Date Analyzed: 11/21/91
Dilution Factor: \ . o v
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
1 1 I I I 1 CAS NUMBER 1 COMPOUND NAME 1 RT 1 E S T . CONC. 1 Q 1 = = = s s s = : s s z = = B S S S = | ==5 = = = = = = = = =s = = = = = = = = = = = = = = = s== | = = = = = = = = | = = = = = = = = = = = = = ' j = = = = =
1 1 . - - l A l d o l C o n d e n s e t ion-/' i^o<^f^t//»«^'^j 3 . 6 1 1 43 0 0 . 1 J ^ L 2 . - - lUnknown 1 7 . 5 3 1 3 0 0 . 1 J ^ B 3 . - - lUnknown 1 1 2 . 3 8 1 1 3 0 . 1 J
I I I I I I I I I I 1 1 I I I I I I I I
' 1 1 I I I I I I I I 1 1 I I ' I I I I I I I I I I 1 1 I I 1 I I I I I I I I I I I t I i i 1 1 I I I 1 1 I I ! I I I I I
- 1 1 I I ' I ' I I I I
1 1 I I I I I I I I
"" i 1 I I I I I 1 1 1
FORM I S U - T I C 1/8 7 . I-}
300471
IB SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
1111068-07 Lab Name: INTECH Contract: 68-D9-0048 I
kb Code: INTECH Case No.: i)l-(?2^ SAS No.: SDG No.: A / ^ J O ^
Matrix: [soil/water] SOIL
Sample wt/vol: 30.21 [g/mL] G
Leve1: [low/med] LOW
% Moisture: 2. dec. 2-.
Extraction: [SepF/Cont/Sonc] SONC
GPC Cleanup: [Y/N] N pH: 7.5
Lab Sample ID:
Lab File ID: >B7962
Date Received: 11/12/91
Date Extracted: 11/15/91
Date Analyzed: 11/21/91
Dilution Factor: l.oo
CAS NO, COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/KG
108-111-95-
541-106-100-95-95-
108-106-621-67-98-78-88-
105-65-
111-120-120-91-106-87-59-93-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-•83-2-82-1-20-3-47-8-•68-3-50-7-57-6-•47-8-•06-2-95-4-58-7-74-4-11-3-96-8-20-2-
•Phenol -b is(2-chloroet -2-Chloropheno1 -1,3-Dichlorobe -1,4-Dichlorobe -Benzyl alcohol -1,2-Dichlorobe -2-MethylphenoI -bis(2-ch loro is -3&4-Methylphen -N-Nitroso-d i-n -Hexachloroetha -Nit robenzene -1 sophorone -2-Ni t rophenoI -2,4-Dimethylph -Benzo ic acid -bis(2-Chloroet -2,4-Dichloroph -1,2,4-Trichlor -Naphthalene -4-Chloroan i1 in -Hexachlorobuta -4-Chloro-3-me t -2-Methylnaphth -HexachlorocycI -2,4,6-Trichlor -2,4,5-Tr ichlor -2-Chloronaphth -2-Ni t roan i1ine -Dimethylphthal -Acenaphthy Iene -2,6-Dinitrotol
hyl)ether
nzene nzene
nzene
opropyl)et her ol -propyl am i ne ne
eno I
hoxy)methane eno I obenzene
e d iene hylphenoI a lene opent ad iene opheno1 opheno I a lene
a t e
u e n e
FORM I SU-1
Q
300472
IC
S E M I U O L A T I L E O R G A N I C S A N A L Y S I S DATA SHEET EPA SAMPLE NO.
I 1111068-07
Lab Name: INTECH C o n t r a c t : 6 8 - D 9 - 0 0 4 8 I
i ^ ^ C o d e : INTECH Case N o . : ( f l ' i r ^ SAS N o . : SDG N o . : ^ ^ J c ^
Matrix: [soil/water] SOIL
Sample w t / v o l : 30.21 [g/mLl G
-Level: [low/med] LOW
-% M o i s t u r e : 1 . d e c . 1,
'Extraction: [SepF/Cont/Sonc] SONC
GPC Cleanup: [Y/N] N pH: 7.5
Lab Sample ID:
Lab Flle ID: >B7962
Date Received: 11/12/91
Date Extracted: 11/15/91
Date Analyzed: 11/21/91
Dilution F a c t o r : \.0<^
CAS NO, COMPOUND
C O N C E N T R A T I O N U N I T S :
[ug/L or ug/Kg] UG/KG
99-83-51-
100-
132-121-84-
7005-86-
100-534-86-
101-118-
87-
85-120-84-
206-129-85-91-
218-117^ 117^ 205-207-
50-193-
53-191-
•09-2-•32-9-•28-5-•02-7-•64-9-•14-2-•73-7-•72-3-•73-7-•01-6-•52-1-•30-6-•55-3-•74-1-•86-5-•01-8-•12-7-•74-2-•44-0-•00-0-•68-7-•94-1-•55-3-•01-9--81-7--84-0--99-2-•08-9-•32-8-•39-5-•70-3-•24-2-
-3-Ni t roan i1ine
- Ac enaphthene •2,4-Dinitrophenol -4-Ni t rophenoI -Dibenzofuran -2,4-Dinitrotoluene •Diethylphthalate -4-Chlorophenyl-phenylet her -Fluorene -4-Nitroani1ine •4,6-Dinitro-2-me thyIphenoI -N-Nitrosodiphenyl amine •4-Bromophenyl-phenylet her -Hexachlorobenzene -Pentachloropheno1
- Ph enanthrene -Anthracene -Di-n-butylphthalate -Fluoranthene -Pyrene -Butylbenzylphthalate -3,3'-Dichlorobenzidine -Benzo(a)anthracene -Chrysene
-bis(2-Ethylhexyl )phthalate -Di-n-octylphthalate -Benzo(b)fluoranthene -Benzo(k)f luoranthene -Benzo(a)pyrene
- Indeno(1,2,3-cd)pyrene -Dibenz(a,h)anthracene •Benzo(g,h,i)perylene
Q
1 1700 1 340 1 340 1 1700 1 340 1 340 1 340 1 340 1 340 1 1700 1 1700 1 340 1 340 1 340 1 1700 1 340 1 340 1 340 1 340 1 340 1 340 1 680 1 340 1 340 1 220 1 340 1 340 1 340 1 340 1 340 1 340 1 340
1 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU 1 IU I IU 1 IU 1 IU 1 IU 1 IU 1 IU i IU 1 IU 1 IU 1 IU 1 IU 1 1 J 1 IU 1 IU 1 IU 1 IU i IU 1 IU 1 IU 1 1 ' 1
FORM I SU-2
300473
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
Lab Name: INTECH Contract: 68-D9-0048
EPA SAMPLE NO,
I 1111068-07 I
Matrix: (soil/water) SOIL
Sample wt/vol: 30.21 (g/mL) G
Level: (low/med) LOU
% Moisture: X . dec. 2-.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) N pH: 7.5
Number TICs found: 3
Lab Sample ID:
Lab File ID: >B7962
Date Received: 11/12/91
Date Extracted: 11/15/91
Date Analyzed: 11/21/91
Di lut ion Factor : I. "S ®
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
CAS NUMBER 1 COMPOUND NAME 1 RT 1 EST. CONC. 1 Q
1. - - lAldol C o n d e n s e t ion-Piro(/ieT ((/*«6<Diif ) 3.62 1 3 7 0 0. 1 3 2. - - lUnknown 1 5.22 1 170. 1 J
k 3 . - - lUnknown 1 7.56 1 240. 1 J
' 1 I I I
FORM I SU-TIC 1/87 Rev.
C u X
300474
IB SEMIUOLATILE 'ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
I 1111068-08 Lab Name: INTECH Contract: 68-D9-0048 I
.Lab Code: INTECH Case No.: ^1-^g SAS No.: SDG No.:/?/^/<^^
Matrix: [soil/water] WATER
"Sample wt/vol: 1000 [g/mL] ML
Level: [low/medl LOW
H Moisture: dec 100.
Extraction: [SepF/Cont/Sonc] SERF
_GPC Cleanup: [Y/N] N pH: 7.0
Lab Sample ID:
Lab File ID: >B7950
Date Receieved: 11/12/91
Date Extracted: 11/14/91
Date Analyzed: 11/20/91
Di lut ion Factor: | .00
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L
108-111-95-
541-106-100-95-95-108-106-621-67-98-78-88-
105-65-
111-120-120-91-106-87-59-91-77-88-95-91-88-
131-208-606-
95-2-44-4-57-8-73-1-46-7-51-6-50-1-48-7-60-1-44-5-64-7-72-1-95-3-58-1-75-5-67-9-85-0-91-1-83-2-82-1-20-3-47-8-68-3-5 0-7-57-6-47-8-06-2-95-4-58-7-74-4-11-3-96-8-20-2-
-Phen -bis( -2-Ch -1,3-•1,4--Benz -1,2--2-Me -bis( -4-Me -N-Ni -Hexa -Nit r - Isop -2-Ni -2,4--Benz -bis( -2,4-•1,2, -Naph -4-Ch •Hexa •4-Ch -2-Me -Hexa •2,4, -2,4, -2-Ch -2-Ni -D ime -Acen -2,6-
ol 2-ch 1 oroet lorophenoI Di ch 1 orobe Dich lorobe yI a 1 echo 1 Dichlorobe thyIpheno1 2-ch 1 oro i s thy Ipheno1 t roso-d i-n chloroe tha obenzene horone t ropheno 1 Dime thyIph 0 ic ac id 2-Chloroet Dichlo roph 4-Tr ich 1 or thalene loroan i 1 i n ch lorobu t a loro-3-met thylnaphth chlorocyc1 6-Tr ichlor 5-Tr i chlor 1 oronaph t h t roan i I ine thyIphtha1 aphthy1ene D in 11 rot o 1
hyl)e ther
nzene nzene
nzene
opropyI)ether
-propylamine ne
eno I
hoxy)me thane eno I obenzene
e d iene hyIpheno1 a 1 ene opent ad i ene opheno 1 opheno 1 a 1 ene
ate
uene
10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 50 10 10 10 10 10 10 10 10 10 10 10 10 50 10 10 10
Q
IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU < . \ j >J
FORM I SU-1 300475'
IC SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I 1 I 1111068-08 I
Lab Name: INTECH Contract: 68-D9-0048 I
Lab Code: INTECH Case No.: ^|-^0 SAS No.: SDG No. : ,/??/v/(?
Matrix: [soil/water] WATER Lab Sample ID:
Sample wt/vol: 1000 [g/mL] ML Lab File ID: >B7950
Level: [low/med] LOW Date Receieved: 11/12/91
% Mo Isture: dec 100.
Extraction: [SepF/Cont/Sonc] SERF
GPC Cleanup: [Y/N] N pH: 7.0
Date Extracted: 11/14/91
Date Analyzed: 11/20/91
Di lut ion Factor: | .00
CAS NO. COMPOUND CONCENTRATION UNITS: [ug/L or ug/Kg] UG/L Q
99-09-2- 3-NitroaniIine 83-32-9 Acenaphthene 51-28-5 2,4-Din it ropheno 1 100-02-7 4-Ni t ropheno 1 132-64-9 Dibenzofuran 121-14-2 2,4-Din it roto luene 84-73-7 •--Diethylphthalate
7005-72-3 4-Chlorophenyl-phenylether 86-73-7 Fluorene 100-01-6 4-Nitroaniline 534-52-1 4,6-Dinitro-2-me thylphenol 86-30-6 N-Nitrosodi pheny I am ine 101-55-3 4-Bromophenyl-phenylether 118-74-1 Hexach lorobenzene 87-86-5 -. Pent ach loropheno 1 85-01-8 Phenanthrene 120-12-7 Anthracene 84-74-2 Di-n-butylphthalate
2 06-44-0 Fiuoranthene 129-00-0 Pyrene 85-68-7 Butylbenzylphthalate 91-94-1 -3,3'-Dichlorobenzidine 56-55-3 Be nzo (a )an thracene
218-01-9; Chrysene 117-81-7 bis(2-Ethylhexyl)phthalate 117-84-0 Di-n-octylphthalate 205-99-2 Be nzo (b)f luoranthene 2 07-08-9 Benzo (k)f luoranthene 50-32-8 Benzo(a)pyrene 193-39-5 Indeno (1,2,3-cd )pyrene 53-70-3 D 1 benz ( a, h) an thracene 191-24-2 Benzo(g,h, i )perylene
1 50 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 50 1 50 1 10 1 10 1 10 1 50 1 10 1 10 1 10 1 10 1 10 1 10 1 20 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10 1 10
1 IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU IU I
^ 200
FORM I SU-2 300476
IF SEMIUOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIUELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
I 1111068-08 Lab Name: INTECH Contract: 68-D9-0048
Matrix: (501 I/water) WATER
Sample wt/vol: 1000 (g/mL) ML
^Level: (low/med) LOW
% Moisture: dec. 100.
Extraction: (SepF/Cont/Sonc) SERF
GPC Cleanup: (Y/N) N pH: 7.0
' Number TICs found: 0
Lab Samp 1e ID:
Lab Flle ID: >B7950
Date Received: 11/12/91
Date Extracted: 11/14/91
Date Analyzed: 11/20/91
Dilut ion Factor: | .00
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/ L
CAS NUMBER 1 COMPOUND NAME 1 RT — = — — — — — — s = = = = = = = 1 s = = s s B s s s 3 B = s = m s = ass = s = s = sss = r: | a;ss=!as = = tt =
i 1
EST. CONC. Q
FORM I S U - T I C 1 /87 Rev .
210 300477
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
L a b Name:
m rmecU C o n t r a c t
ab code: l U f f C ) ) Case No.: ^i~^^ SAS No.:
Matrix: (soil/vater) "jfVi TEi
Sample wt/vol: / 0 ^ (q/nL)/^^
Level: (low/med) L O W
% Moisture: not dec. /tV dec. 0
Extraction: (SepF/Cont/Sonc) . " ^ u F
GPC Cleanup: ( Y / N ) ^ PH; 7t^
EPA SAMPLE NO.
SDG NO.: f^l/U^nJ
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted: > ' y ^ j ^ l
Date Analyzed: /I Mo / 9 f
M i / / j ) M I
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITSJ (ug/L or ug/Kg)
NITS;
LO.
1 319-84-6 alPha-BHC 1 .0-6 1 L 1 1 319-85-7 beta-BHC 1 . C ^ \ ' 1 1 319-86-8 delta-BHC I , a^ 1 U 1 1 58-89-9 qamma-BHC (Lindane) | ,0"^ 1 V \ 1 76-44-8 Heptachlor 1 ,t'>f 1 \J 1 1 309-00-2 Aldrin 1 •O'i 1 i; 1 1 1024-57-3 Heptachlor epoxide | 'trf \ U 1 1 959-98-8 Endosulfan I \ .Of 1 ./ 1 1 60-57-1 Dieldrin 1 .f './O 1 1 1 72-55-9 4.4'-DDE 1 ./O 1 , 1 1 72-20-8 Endrin | </C 1 (' 1 1 33213-65-9 Endosulfan II 1 .jO | o 1 1 72-54-8 4.4'-DDD I /c? 1 ,/ 1 1 1031-07-8 Endosulfan sulfate | ./O | j 1 50-29-3 4.4'-DDT 1 -lO | | 1 72-43-5 Methoxychlor 1 ,SO 1 ; 1 1 53 4 94-70-5 Endrin Ketone \ . lO 1 ' 1 1 5103-71-9 alpha-Chlordane I , ^ \ j \ 1 5103-74-2 gamma-Chlordane | . S O \ <J j 1 8001-35-2 Toxaphene 1 /,0 1 i/ 1 1 12674-11-2 Aroclor-1016 1 -^ 1 j \ \ 11104-28-2 Aroclor-1221 1 - S 1 1 1 11141-16-5 Aroclor-1232 1 ' ^ 1 ; 1 1 53469-21-9 Aroclor-1242 1 ,5" 1 ^ 1 1 12 672-29-6 Aroclor-1248 1 , >' 1 1 1 11097-69-1 Aroclor-1254 1 h O \ ^ \ 1 11096-82-5 Aroclor-1260 I A 9 | j |
FORM I PEST 1/87 Rev.
2V7 300478
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: I A/TEC P
EPA SAMPLE NO.
I f=)c]6 6 L M K
'Lab Code: I U T E ' C ) ) Case No.: ^^'^^ SAS No.:
Matrix: (soil/water) Wf JEf
Sample wt/vol: / (Wl^ (q/nL) t /IL
Leve 1: (1 ow/med) L O W
% Moisture: not dec. /?/// dec. C?
Extraction: (SepF/Cont/Sonc) V 5 E V ^
GPC Cleanup: ( Y / N ) ^ pH:7(y
Contract: ftJll^^/U j )35-(K?fc$'-c? rQ
SDG NO.: ^)L/^/l/
Lab Saaple ID:
Lab File ID:
Date Received:
Date Extracted; / / / / 4 / 9 /
Date Analyzed: //
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITS/ ( u g / L o r uq /Kq) i l h / L -
3 1 9 - 8 4 - 6 3 1 9 - 8 5 - 7 3 1 9 - 8 6 - 8 5 8 - 8 9 - 9 7 6 - 4 4 - 8 3 0 9 - 0 0 - 2 1 0 2 4 - 5 7 - 3 9 5 9 - 9 8 - 8 6 0 - 5 7 - 1 7 2 - 5 5 - 9 72-20-8 3 3 2 1 3 - 6 5 - 9 72-54-8 1 0 3 1 - 0 7 - 8 5 0 - 2 9 - 3 7 2 - 4 3 - 5 5 3 4 9 4 - 7 0 - 5 5 1 0 3 - 7 1 - 9 5 1 0 3 - 7 4 - 2 8 0 0 1 - 3 5 - 2 1 2 6 7 4 - 1 1 - 2 1 1 1 0 4 - 2 8 - 2 1 1 1 4 1 - 1 6 - 5 5 3 4 6 9 - 2 1 - 9 1 2 6 7 2 - 2 9 - 6 1 1 0 9 7 - 6 9 - 1 1 1 0 9 6 - 8 2 - 5
-a lpha-BHC -beta-BHC " • d e l t a - B H C -gamma-BHC ( L i n d a n e ) - H e p t a c h l o r \ - A l d r i n -Heptachlor epoxide^ -Endosulfan I ^ -Dieldrin •4, 4 • -DDE -Endrin -Endosulfan .XI -4,4" -DDD -Endosulfan sulfate -4 ,4 • -DDT Methoxychlor_ Endrin ketone -alpha-Chlordane_ -gamma-Chlordane' -Toxaphene_ -Aroclor-1016 -Aroclor-1221' -Aroclor-1232' - A r o c l o r - 1 2 4 2 ] - A r o c l o r - 1 2 4 8 ' -Aroc lor -1254]^ - A r o c l o r - l 2 6 0 '
/ g ^ . ^ r . !££ 'CS •J2£
.J21. <cr • CS-
'M. to
-JC_ _d f . / ( / J0_
t a Q
'JO-ro
, r j - o
mU-
J i .
u_
^
iZ.
z iJ
Jj_
if
FORM I PEST 1/87 Rev.
300479
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: r/lTTFCH Contract : M^^/1/ Lab Code: j j l / n f C n Case No.: ^ '"^^ SAS No.
Matrix: (soil/water) O Q J ^
Sample wt/vol: .S<0'P (q/mL) W
Level: (low/med) L O W
% Moisture: not dec. I. dec. I»
Extraction: (SepF/Cont/Sonc) .bO/^L
GPC Cleanup: ( Y / N ) ^ PH: 7 - ^
SDG
EPA SAMPLE NO.
j r6 *^ 'C'-)P' I
I H^h/mi ' l
NO.: 2ZM
5H A
Lab Sample ID:
Lab File ID: _
Date Received:
Date Extracted: H J / ^ n ^
Date Analyzed: )l j ' ^ ^ T ^
Dilution Factor: \ > 0
CAS NO. COMPOUND CONCENTRATION UNITSX (ug/L or ug/Kg) I jJz/klZ
1 319-84-6 alPha-BHC 1 € . 0 1 U 1 1 319-85-7 beta-BHC 1 xD 1 J 1 1 319-86-8 delta-BHC 1 ^ 0 I U | 1 58-89-9 qamma-BHC (Lindane) I ^ 0 1 (/ 1 1 76-44-8 Heptachlor 1 )^€ 1 J 1 1 309-00-2 Aldrin 1 fc \ U \ 1 1024-57-3 Heptachlor epoxide I l$-V | J | 1 959-98-8 Endosulfan I \ 2i-0 \ U \ 1 60-57-1 Dieldrin 1 /(, \ J \ 1 72-55-9 4.4'-DDE 1 /(, 1 ;/ 1 1 72-20-8 Endrin 1 / 1 U | 1 33213-65-9 Endosulfan II 1 /<- 1 ; 1 1 72-54-8 4.4'-DDD 1 / 1 o 1 1 1031-07-8 Endosulfan sulfate 1 / 1 J 1 1 50-29-3 4.4'-DDT 1 / (, I , .' 1 1 72-43-5 Methoxychlor 1 ^-Q I i,' 1 1 53494-70-5 Endrin Ketone I /A 1 // 1 1 5103-71-9 alpha-Chlordane I l?p 1 ly 1 1 5103-74-2 qamma-Chlordane j ^ 0 1 ,/ 1 1 8001-35-2 Toxaphene 1 /^ C 1 i M 1 12674-11-2 Aroclor-1016 1 ^0 | U 1 1 11104-28-2 Aroclor-1221 1 ^ 0 1 J 1 1 11141-16-5 Aroclor-1232 1 fC 1 J 1 1 53469-21-9 Aroclor-1242 1 <5'i 1 >.; 1 1 12672-29-6 Aroclor-1248 1 '^0 1 J, 1 1 11097-69-1 Aroclor-1254 1 /^C'' | ^ | 1 11096-82-5 Aroclor-1260 1 /^(P 1 'J 1
FORM I PEST 1/87 Rev.
300480
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name; rmjzU Contract •.MtM iLab code: J I U T T C H Case No.: ^'~^^ SAS No.:
Matrix: ( so i l /water ) SClTt.
Sample wt /vol : 3 0 - 0 (q/mL) ^
Level: (low/med) L O W
% Moisture: not dec. 2. dec. >
Extraction: (SepF/Cont/Sonc) ^ t W ^
GPC Cleanup: (Y/N)J^ pH: 7- ^
EPA SAMPLE NO.
I JXh^H IS -17 ' I
SDG NO.: M ^
Lab Sample ID:
Lab File ID:
Date Received:
Date Ext rac ted : //'Iio 91
Date Analyzed: / / / ^ J ' ^ l
Dilution Factor:
CAS NO. COMPOUND CONCENTRATION UNZTSl , (ug/L or uq/Kq) (/b/C (7
319-84-6 319-85-7 319-86-8 58-89-9 76-44-8 309-00-2 1024-57-3 959-98-8 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8 50-29-3 72-43-5 53494-70-5 5103-71-9 5103-74-2 8001-35-2 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5
-alpha-BHC -beta-BHC -delta-BHC -gamma-BHC (Lindane) -Hept achl or \ -Aldrin -Heptachlor epoxide^ -Endosulfan I '_ -Dieldrin -4,4'-DDE -Endrin -Endosulfan LI -4,4'-DDD -Endosulfan sulfate -4,4' -DDT • Methoxychlor__ Endrin Ketone -alpha-Chlordane_ -gamma-Chlordane] -Toxaphene '_ -Aroclor-1016_ -Aroclor-1221' -Aroclor-1232' -Aroclor-1242] -Aroclor-1248] -Aroclor-1254] -Aroclor-1260'
XO. S£L .£>£.
Jj l
u W
JL
± /o
f J.
i O. ^
) 0
u
j i .
-Ll
.LL
-iA-^
± ±
FORM I PEST 1/87 Rev.
239 300481
I D EPA SAMPLE NO. P E S T I C I D E ORGANICS ANALYSIS DATA SHEET
I J 6 # 3 A S ' ^ ' 1
ryl/lK^ contract: J | ! 5 M L I _2 l iL£££ :L . I
.WLab Code: '3^(1?^ Case No.: ^ 1 - ^ ^ SAS No.: SDG No.: U K U ^ A J
Lab Name:
Matrix: (soil/water)_5_^XL
Sample wt/vol: S O J ^ (g/v^) \7
Level: (low/med) L O W
% Moisture: not dec. ,y- dec. < '
Extraction: (SepF/Cont/Sonc) S ^ ^ ^
GPC Cleanup: (Y/N).^ pH: 8'-fP
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:,
Date Analyzed:
<A)
lj)5]9\
JlJM^ QI
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITSl . (ug/L or uq/Kq) (;(7/r(7
iO
1 3 1 9 - 8 4 - 6 a lpha-BHC 1 }f£) \ U \ 1 3 1 9 - 8 5 - 7 beta-BHC 1 le 0 1 ^ 1 1 3 1 9 - 8 6 - 8 d e l t a - B H C 1 ^ . 0 1 L' 1 1 58-89-9 qamma-BHC (Lindane) I g'.D 1 (/ 1 1 76-44-8 Heptach lor 1 g\C> 1 'J 1 1 309-00-2 A l d r i n 1 ^.p 1 i; \ 1 1024-57-3 Heptach lor epox ide I < .0 1 u' 1 1 9 5 9 - 9 8 - 8 - Endosulfan I 1 ^ . 1 .' 1 1 60-57-1 D i e l d r i n 1 /A I I 1 72-55-9 4.4'-DDE 1 Jb 1 r 1 1 72-20-8 Endrin 1 /I. 1 ,,' 1 1 33213-65-9 Endosulfan .11 I /i, 1 . t 1 72-54-8 4,4'-DDD \ JC I I 1 1031-07-8 Endosulfan s u l f a t e 1 / 6 1 . 1 1 50-29-3 4,4'-DDT I /C 1 \J I 1 72-43-5 Methoxychlor 1 y?0 I -j 1 1 53494-70-5 Endrin Ketone 1 //, I , i 1 5103-71-9 a lpha -Ch lo rdane 1 jfo 1 ^ 1 I 5103-74-2 qamma-Chlordane I jU 1 i, 1 1 8001-3 5-2 Toxaphene 1 j/^O I 1 1 12674-11-2 Aroclor -1016 1 %o 1 1 1 11104-28-2 Aroc lo r -1221 1 iC 1 ; 1 1 11141-16-5 Aroclor -1232 1 KP \ o> \ 1 534 6 9 - 2 1 - 9 A r o c l o r - 1 2 4 2 i hV 1 ' 1 1 1 2 6 7 2 - 2 9 - 6 A r o c l o r - 1 2 4 8 1 S'/l 1 •.' 1 1 11097-69-1 Aroclor-1254 1 /hO \ 1 1 1 1 0 9 6 - 8 2 - 5 A r o c l o r - 1 2 6 0 I / l [ J | J j
FORM I PEST 1/87 Rev. ^ ' ( y r^> ' ^
300482
Lab
^FLab
Mat:
Samj
Lev*
% M<
Extl
GPC
--
•
--.
-
— •
ID PESTICIDE ORGANICS ANALYSIS DATA
Name: i A / ) t C ) ^ Contract
Code: J U I ^ C ) ) Case No.: ^ t - i > i SAS No.
rix: (soil/water) OT'L
3le wt/vol: 3 0 . ^ \ (q/mL) L7
il: (low/med) L Q W
sisture: not dec. ^- dec. 2 .
raction: rSenF/Cont/Sonc) ^ ^ C
Cleanup: (Y/N) Kj PH: 7 5
CONGE] CAS NO. COmOUND (ug/L
1 319-84-6 alpha-BHC 1 319-85-7 beta-BHC 1 319-86-8 delta-BHC 1 58-89-9 qamma-BHC (Lindane) 1 76-44-8 Heptachlor 1 309-00-2 Aldrin I 1024-57-3 Heptachlor epoxide 1 959-98-8 Endosulfan I 1 60-57-1 Dieldrin 1 72-55-9 4.4'-DDE 1 72-20-8 Endrin 1 33213-65-9 Endosulfan .11 1 72-54-8 4, 4'-DDD 1 1031-07-8 Endosulfan sulfate 1 50-29-3 4, 4'-DDT 1 72-43-5 Methoxychlor 1 53494-70-5 Endrin Ketone 1 5103-71-9 alpha-Chlordane 1 5103-74-2 qamma-Chlordane 1 8001-35-2 Toxaphene 1 12674-11-2 Aroclor-1016 1 11104-28-2 Aroclor-1221 1 11141-16-5 Aroclor-1232 1 53469-21-9 Aroclor-1242 1 12672-29-6 Aroclor-1248 1 11097-69-1 Aroclor-1254 1 11096-82-5 Aroclor-1260
EPA SHEET
1 X6«
: SDG No.:
Lab Sample ID:
Lab File ID:
Date Received: //
Date Extracted: //^
Date Analyzod: / J j
Dilution Factor:
1TRATI0N UNITS;i , or uq/Kq) (7(7/ r(7
1 £.0
1 j : . Q
1 2-c 1 6.0 ' ^-^ 1 r^o 1 Co 1 u 1 / / 1 //, 1 /^ 1 /y 1 J 1 /6 1 ??o 1 )C 1 ^ D 1 ^ D 1 /U-> 1 S" 1 SO 1 ^ ( ? 1 K D
1 ^u 1 /Jiip 1 /If?
SAMPLE NO.
Ml tU
Q
1 iJ 1 1 0 1 1 L 1 1 f 1 1 I.' 1 1 -J 1 1 / 1 1 ^ 1
1 '' 1 1 ./ 1 1 '.' i 1 _„ Ji i t 1 1
' i. ) , ' 1 ^ 1
1 ^ 1
1 1,' 1 1 u' 1 1 1 1 1 V 1 1 ' ' 1 1 \'! 1 1 U 1
1 -. I 1 ^' 1
FORM I PEST 1/87 Rev.
C O i
300483
ID PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: JM£Ci Contract •.MbML 'Lab Code: J^ tV^Cn Case No.: L)-^'^ SAS No.:
Matrix: ( so i l /water ) SOd-L
Sample wt /vol : S 0 ( ^ (g/nL) W
Level: (low/med) L O W
% Moisture: not dec, c - dec. <?<•
Ext rac t ion : (SepF/Cont/Sonc) 5^/VC
GPC Cleanup: ( Y / N ) ^ pH: / ^ ^
EPA SAMPLE NO.
_ I t / ^ / ' j / p ^ - 7
SDG NO.: ^ H j m j
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted
Date Analyzed:
Dilution Factor:
CAS NO. COMPOUND CONCENTRATION UNITS (ug/L or ug/Kg)
HITS;, /
319-84-6 319-85-7 319-86-8 58-89-9 76-44-8 309-00-2 1024-57-3 959-98-8 60-57-1 72-55-9 72-20-8 33213-65-9 72-54-8 1031-07-8 50-29-3 72-43-5 53494-70-5 5103-71-9 5103-74-2 8001-35-2 12674-11-2 11104-28-2 11141-16-5 53469-21-9 12672-29-6 11097-69-1 11096-82-5
-alpha-BHC -beta-BHC ~ -delta-BHC -gamma-BHC (Lindane) -Heptachlor [ -Aldrin -Heptachlor epoxide_ -Endosulfan I ] -Dieldrin -4,4* -DDE -Endrin -Endosulfan II •4,4' -DDD -Endosulfan sulfate •4 ,4 • -DDT ] Methoxychlor_ Endrin Ketone -alpha-Chlordane_ -gamma-Chlordane] -Toxaphene -Aroclor-1016 -Aroclor-1221] -Aroclor-1232' -Aroclor-1242] -Aroclor-1248] -Aroclor-1254] -Aroclor-12 6 o'
• O
. 0 £JL. JLD-
z± Q_
(7
AL
J J L mLU
.LL
-"nfr
i L -W-
^ L
FORM I PEST 1/87 Rev, o ^ -
300484
TOTAL ME:TAI...S &. CYANIDE COVER F'AGE - INORGANIC ANALYSES DATA PACKAGi;;:
;ib Name;
I^Pcode:
. : :M V\O „ ;;
.-,
; CEI11IC
; CEIMIC C a s e No.,;!
7 / 8 8
SAMPLE ID F.lEf.1.109 FBi.:i.: IB»*3 IB*43 I B n 3 IB*^3 IB** 3 IBM- I I B « 4
1.0 2 5 - • 2 7 3 0 - - 3 4 3 5 - 3 9 3 5 - 3 9 D 3 5 - - 3 9 S 1 0 - 1 2 .15-.1.7
Contract:: ANSON
SAS No,.;; SDG No., s FB;H09
_.ab Samp>Ie I D , 006 : l .9 -08S 006:l.9--04S 0 0 6 1 9 •0.1.S 0061 .9 -02S 0061.9^^03S 0061.9--03S2 006. I .9-03DS 0061 .9 -06S 0 0 6 1 9 - 0 7 S
Wi^^ ' ICP i n t e r e l e m e n t c o r r e c t i o n s a p p l i e d ? Y e s / N o NG Were ICF' b a c k g r o u n d c o r r e c ^ t i o n s a p p l i e d ? Y e s / N o YES
I f y e s - w e r e raw da ' ta g e n e r a t e d b e - f o r e aI:JP:1. i ca l.:i.on o-f hacI'-.g r o u i i d c:or r e c t i o n s 7 Y e s / N o N0
r jmrnen i-ss
I certi-fy that this dat-a package is in compliance with the terms and jnditions of the contract., both technically and for comp le ten (ess., for Uier than the conditions detailed above,. Release of the data contained
in this hardcopy data package and in the computer-readable data submitted I-'I floppy diskette has been authorized by the Laboratory Manager or the I \naqer's designee,, as verified by the following signaturo?,,
.Signature;; ..O...m.Uf<i.:...^kM<::r. H mis;; ..^Btlk.lil.'S. S.h..LLk..^.
_.ni(f.A.}_ .._ •;...•i-.ie;; .._.J^/]o/;H(A^.n±,<L, .5y.j?.?.'!;.. /.?c) „ Late;;
COVER PAGE •• IN Rev,. 6/89
300485
TOTAL I1ETAI...S &. CYANIDE
INORGANIC ANALYSIS DATA SHEET SAMPLE ID
: FB;L:L09 ab Name;; CEII1IC Contract;: ANSON I.._
Lab Code;: CEIMIC Case No.. :: ANSON SAS No„:: SDG No„:: FBI 109
jitrix (soil/water):: WATER Lab Sample ID:: 00619-08S
•evel (low/med):: LOW Date Received s 11/12/91
;r Solids;; 0,.0
("on cen tra ti on Un i ts (uq/L or mg / Kci d r y we iq ht) s UG/L
: j l o r B e f o r e : ; C
C o l o r A f t e r ; : COLGRLESJii
CAS No. An a 1 y t e I Con c&^n t r a t i on
7429-7440-7440-7440-7440-7440-7440-7440" 7440-7440" 7439" 7439-7439-7439" 7439" 7440-7440" 7782-7440-7440" 7440" 7440" 7440" 7440-
•90-" 5 -36-0 •3S--2 •39-3 -41-7 -43-9 •70-2 -47-3 •48-4 -50-8 •89-6 •92-1 -95-4 •96-5 •97-6 •02-0 •09-7 •49-2 -22-4
I Aluminum I Antimony lArsenic 1 E-iarium I .Beryllium I Cadmium [Calcium I Chromium ICobalt ICopper I Iron ; Lead I Magnesium !Manganese I Mercury INickel ! Po (..assium I Selenium ISilver :
D Ibodium -28-0 -31-5
•C)(-.>~i>
I Thallium ITin I Vanadium I Z i ri c I Cyanide
102 ,.00 45„00 2»00 3.00 6 „ 00 4.. 00
108„00 7.. 00
10,. 00 8„00
74,. 00 1.00
61..00 1,. 00 0.. 20 12,00
2140 ..00 4 .00 6.. 00
4450„00 2.. 00
4., 00 2.. 00
10.. 00
C1 a ri ty Before:: CLEAR
Clarity After;: CLEAR
Q
W
M
p"~
F-' F F' F' F' F-F' P F' F' F" F' P CV P F' I"' P P F NR !=•
F' C
Textures
Artifacts
...•c.;>mmen l..r
FOr:;M I - I N 3
300486
TOTAL METAL &. CYANIDE
INORGAhllC ANALYSIS DATA SHEET
ab Name;; CEIMIC
.ab Code;: CEIMIC
Contracts ANSON
Case NO..S ANSON SAS No.
SAMPLE ID
FBlllO
SDG No„= FBI109
vvtrix (soil/water);: WATER
»vel (low./med)s LOW
Solids;; 0..0
Lab Sample ID:; 00619-04G
Date Received:: 11/12/91
Con cen t I'a t i on Un i ts (ug /L o i" mg /Kg d r y we i g h t) s UG/L
Before:;
ICAS No..
I 7429-90-5'" 17440-36-0 I 7440-38-2 17440-39-3 17440-41-7 ;7440-43-9 ;7440-70-2 ;7440-47-3 17440-48-4 17440-50-8 I 7439-89-6 17439-92-1 ;7439-95-4 17439-96-5 17439-97-6 ;7440-02-0 17440-09-7 I 7782-49-2 I 7440-22-4 17440-23-5 17440-28-0 17440-31-5 I 7440-62-2 I 7440-66-6 [
coiloRLiss
1 Analyte
1 Aluminum 1 Antimony 1 Arsenic 1 E<arium I Beryllium' 1 Cadmium I 1 Calcium I I Chromium I ICobalt I ICopper I 1 Iron I I Lead I I Magnesium,' 1 Manganese 1 1 Mercury I INickel 1 1 F'otassium 1 |So:-?lenium I ISilver I 1 Sodium 1 1 Thallium I ITin 1 [Vanadium 1 I Z i ri c 1 ICyanide I
"'"Cla'ri-l
1 1
Concentration IC 1
_______ _...
45«O0IU 2„001U 3.00 IU 6,00 1 4,00 IU
131..00 IB 7„00|U
10.00IU 5„00 IB
62-00 IB 1« 401B
48..00 IB 1.. 00 1 B 0„20|U
12-OOIU 2140 ..00 I U
4„001U 6.. 00 I U
4450„00 IU 2..00IU
I 1
4„00|U 7^00 IB
10„00|U 1
.y""Befores CLEAR
1 1
Q IM 1
1 P ' IP IF IP 11"' IP IP IP IP IP IP IF I F' IP ICV IP IP IF IP IP IF I NR IP IP IC
"" Ter < ture-( ) I o r
C o l o r A f t e r : : COLORLESS
(.5\.:immeri •Ls;
C l a r i t y A f t e r : : CLEAR A r t i f a c t s : ;
300487
•ORI' I K / 8 8
roTAi... Mi;;:TALS &. C Y A N I D E
INORGANIC ANALYSIS DATA SHEET SAMPLE ID
I
I IBi*3 25-27 VIb Name;; CEIMIC Contracts ANSON I_
ab Code;: CEIMIC Case No„s ANSON SAS No.s SDG No,, s FBI 109
.fttrix (soil/water)s SOIL Lab Sample IDs 00619-0IS
-;o v e 1 (1 o w / m e d ) ;: L.. 0 W D a t e R e c e i v e d s 11 /12/91
l:i.d-: 97., 9
Concentration Units (ug./l... or mg./|<g dry weight) s MG/KG
ICAS No.
M.?....
I 7440 I 7440 I 7440 I 7440 I 7440 I 7440 I 7440 I 7440 I 7439 I 7439 I 7439 I 7439 I 7439 I 7440 I 7440 I 7782 I 7440 I 7440 I 7440
9 0 - 5 - 3 6 - 0 - 3 8 - 2 - 3 9 - 3 - 4 1 - 7 - 4 3 - 9 - 7 0 - 2 • 4 7 - 3 ••48-4 - 5 0 - 8 •89 -6 • 9 2 - 1 • 9 5 - 4 •96 -5 •97 -6 - 0 2 - 0 - 0 9 - 7 •49 -2 X.. A.. '-T
28-0 7440-31-5
K.I .<.. A. .
/ • . - . . • < - .
•7440. 7440- ' . - , < : > • •
An a 1 y te I Con cG-?n l-. rat i on
Hlum m u m ; Antimony I Arsenic I Eiarium 1 Beryllium I Cadmium I Calcium I Chromium | Cobalt I Copper I Iron I Lead I Magnesium I Manganese I Mercury I Nickel I F'otassium I Selenium I Silver I Sodium I Thallium I Tin I Vanadium I Zinc I Cyanide I
15 50 ..00 4.. 00 0 „ 86 5,00 0. 0, 36
37.. 30 3„00 0.89 1,. 50
lllOuOO 1.. 20
127 ..00 26,. 90 0.. 09 1„10
191„00 0 „ 40 0.. 54
397.00 0.. 20
2 „ 00 2.. 80 2.. 00
C Q
'*E"
N*
*
N N
*
M
CV F" P F P P F NR
f jlor Before;; BLACK C1 a !'• i •[. y B e i ' a r e :; Texture FINE
C'-ilor After; YELLOW Clarity After Artifacts
tummen 'I;.
300488
FORM I ^7/BB
lames CEIMIC
:ode;: CEIMIC
TOTAL METAI...S &. CYANIDE
1 [NGRGANIC ANALYSIS DATA SHEET
Contracts ANSON
SAMPLE ID
I IBn3 30-34
Lab Code;: UhlMlU Case NOi, s ANSOh
VI t !'• i X (;; o i ]. / w a t e !'•) s S O I I...
Bve]. (low/me?d) s
SAS No,,;; SDG No„:; FBI 109
Lab Sample IDs 00619-02S
Date Receiveds 11/12/91 LOW
.ids;; 97.7
Concentration Units (ug./|... or mg/Kg dry weight) s MG/KG
^ ^ ^ # -^•^
( >loi-' Befoi-es
C o l o r A f t e r s
Ci.:immen ts;;
-—-»- — — .—— .-.-- —-
I C A S No..
1 7429-90-5"" I 7440-36-0 17440-38-2 I 7440-39-3 ; 7440.-41-. 7 ;7440-43-9 I 7440-70-2 I 7440-47-3 I 7440-48-4 17440-50-8 17439-89-6 17439-92-1 17439-95-4 17439-96-5 17439-97-6 I 7440-02-0 I 7440-09-7 I 7782-49-2 I 7440-22-4 17440-23-5 I 7440-28-0 17440-31-5 17440-62-2 !7440-66-6 I -
BLACK
YELLOW
__......_..»__»..._.... -
Analyte I C(
Aluminum ! Antimony 1 Arsenic 1 Barium I Bei'yilium I Cadmium I Calcium I ChromiLim I Cobalt I Copper I I I'on 1 Lead 1 Magnesium 1 Manganese 1 Mercury I Nickel I F'o Lass ium 1 Selenium I Silver I Sodium I Thallium I Tin I Vanadium I Z :i. ri c I Cyanide 1
Clarity
Clarity
incentration I C
2140700 I"" 3 .. 80 I U 0..45IB
12„30 IB 0.. 34 I B 0,. 59 1
74.. 00 I B 6 „ 0 0 I 1.. 6 0 I B 3 „ 50 I
6360.. 00 1 0.. 94 1
473.. 00 I 93.30 1 0,.10IU 1.. 50 1 B
228 ..00 IB 0.34 1 U 0.. 51 IU
375.,001U 0.. 17IU
6.00 I 8., 90 1 2.. 00 1 Ll
Befores
Afters
. » _ . ..M — M — « •—• ~
Q
...._..-
N>fi
;{•:
NW N
*
—..«...«. _ ..„ ™
"***"""
M I
-;-,
F' 1 F" I F' 1 I"' I P-' 1 F' I F' 1 P I P I I"' I F 1 F' 1 F' I C V I F' I F' I F 1 P I F' I F I NR 1 F' I P I C 1
Textures
Artifacts
FINE
300489
"ORM I IN
TOTAL METALS &. CYANIDE
INORGANIC ANALYSIS DATA SHEET SAMPLE ID
I
I IB**3 35-39 I ' — -_„„_ . ab Mame;; CEIMIC Contracts ANSON
Lab Code:; CEIMIC Case No., s ANSON SAS No„s SDG No., s FBI 109
..atrix (soil/water) s SOIL Lab Sample IDs 00619-03S
-evel (low/med)s LOW Date Receiveds 11/12/91
97.. 8
Con cen tration Uni ts (ug/L or mg/Kg dry weight)s MG/KG
.-:: bo.I, Ids;;
y.\.ov- Bef ores BLACK
' o lo i flT'ters
commen t s s
CAS No..
74'29-90-5~ 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6
LACK
ELLOW
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium ' Chromium I Cobalt I Coppo?r I Iron 1 Lead I Maqnox'sium ' Manganese Mojrcury Nickel F'otassium ' Selenium Silver Sodium Thallium Tin Vanadium Z :i. n c Cyanide
„.„„..._.
Clari1
C o n c e ri t ration
1520700 4.60 0.,80 7,. 60 0..41 0.92
32.. 10 9.. 60 1.. 00 2„20
9140 ..00 1.. 00
152.. 00 47.. 90 0..10 1..20
219.. 00 0 „ 37 0..61
455.00 0.. 18
6.10 12.90 1„90
•.y Be fores
•.y Afters
C
—
I..I B B B
B
U B
B
1..1 U U U U U U
U
""
Q
" " * E
N*
*
NW N
>!•:
M
p~
F' F F-F' F' P F' F' P F' F F' F' CV F-' P F P P F NR F-F' C
Te;
Ar-
<tures
:ifact
FINE
300490
l-ORM I IN
TOTAL METALS «; CYAhllDE
INORGANIC ANALYSIS DATA SHEET SAMF'LE ID
I IB**4 10-12 ab Names CEIMIC Contracts ANSON I
Lab Codes CEIMIC Case No-s ANSON SAS No., s SDG No„s FBI 109
atrix (soil/water)s SOIL Lab Sample IDs 00619-06S
!-eveI (low/med )s LOW Date Received s 11/12/91
>;; Sol ids s 98 ..7
Con cen t ra t i on Un i ts (ug/L oi- mq./Kg d r y wo?i g h t) s MG/KG
Dior Be fores
Color A-f ter s
tommen ts s
CAS No..
7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-
90-5 36-0 38-2 39-3 41-7 43-9 70-2 47-3 48-4 50-8 89-6 -92-1 -95-4 -96-5 -97-6 -02-0 -09-7 "49-2 -22-4 7440
7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6
BLACK
YELLOW
Analyte
Aluminum Antimony Arseni c Barium Beryl1ium Cadmium Calcium Chromium Cobalt Copper I ron Lead Magnesium Manganese Mercury Nickel F'otassium Selenium Silver Sodium Thallium Tin Vanadium Z :i. n c Cyanide
C' 1 a !'• i
Con c e n t r a •!: i o n
94 5. 4. 0. 3. O. 0.
O,. 4- u
8410. 1.
179.. 49. O.. 1.
196.. 0. 0-
403, O,
00 10 57 90 28 92 60 70 92 50 00 90 00 80 10 10 00
00 18
3.. 40 5.80 1.90
C
Ll
Q
"*E"
M*
*
NW
*
/ Before s
Clarity After:
M
F' I"' F' F' F-F' F' F-F F' F' CV F' F' F F' F' F NR I"' F' C
T e x t u r e s FINE
A r t i f a c t s s
300491
FOR IN / . ' \ . j I.? 8
TOTAL METALS & CYANIDE
1 INORGANIC ANALYSIS DATA SHEET
SAMPLE ID
I IB#4 15-17 \ \b Names CEIMIC Contracts ANSON I _ _
Lab Code;; CEIMIC Case No., s ANSON SAS No,, s SDG No.s FBI 109
Ldtrix (soil/water)s SOIL Lab Sample IDs 00619-078
r;vel (low/med)s LOW Date Receiveds 11/12/91
^ Sol idss 98.4
Con cen t ra t i on Un i ts (ug/L o r mg/Kg d ry we ig h t)s MG/KG
7429" 7440" 7440-7440" 7440" 7440" 7440" 7440-7440" 7440-7439-7439" 7439" 7439" 7439" 7440-7440" 7782" 7440-7440" 7440-7440-7440-7440
^lo „
9 0 - 5 " •36-0 •38-2 •39-3 •41-7 4 3 - 9
" 7 0 - 2 - 4 7 - 3 - 4 8 - 4 - 5 0 - 8 - 8 9 - 6 - 9 2 - 1 - 9 5 - 4 " 9 6 - 5 - 9 7 - 6 " 0 2 - 0 - 0 9 - 7
'•t .•• A . .
"22-4 -23-5 "28-0 -31-5 .. /. '-:•... o \..' X.. I I . .
-66-6
( )lor Befores BLACK
r-)lor After;: YELLOW
Commen 'Ls s
Analyte
Aluminum An'timony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt CoppOlM'-I ron Lead Magnesium Manganese Mercury Nickel F'otassium Selenium Sils.'er Sodium Thallium Tin Vanadium Z i 11 c Cyanide
C1 a r i
tration
••349755
4.. 50 0..24 3.. 10 0.. 30 0.40
73.. 60 2,. 90 0 „ 99 1.80
3160.00 0,. 83
154„00 33.20 0.. 10 1 „ 20
212.. 00 0,. 39 0.. 59
441.00 0., 19
1.. 90 4,. 10 2 „ 00
Cl — '
UI BI BI Bl Ul Bl
Ul Bl
BI
Ul UI Ul Ul Ul Ul Ul
B"
UI
Q
">KE"
^i*•
-"IW N
*
E<ef ore;
C 1 a I" :i. t ••/ A f t (•>? i"
M
F P P CV P P F P P F NR I"' F' C
Tex
Art
tures FINlii
ifactss
300492
•OR Ih 7 / 3 8
Unvalidated Data
Indoor borings 1 & 2 Re-sampling drywells 5-9, catch basin
300493
TOTAL METALS &. CYANIDE: COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name;; CEIMIC Contracts ANSON
i^ Code;; CEIMIC Case No.s ANSON SAS No.s SDG No., s CATCH.._BA
' No„ :; 7/88 SAMPLE ID CATCHB DW5 DW6 DW7 DW8 DU)9 FB0104 FB0105 IBllO IBllOD IBllOS IB115 IB210 IB215
I'
ll
II
I!
i >
I
i
II
I!
II
I!
ti
ll
i !
! i
i i
i I
1
Lab Sami 00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-00006-
Dle ID. -OlS -02S -03S -•04S ••05S -06S - U S -12S -07S -07S2 -07DS -08S -09S -lOS
ICF' interelement corrections applied? Yes/No HO ICF' background corrections applied? Yes./No YES If y(-?s-were raw data generated before-? application of background corrections? Yes/No NO
i.,ommer] ts
cerl:.ify thai:, this data package is in compliance with the terms and conditions of the contract., both technically and for completeness,, for * other than the conditions detailed above.. FU-?leaso? of the data contained n this hardcopy data package and in the computer-readable data submitted ..j-i floppy diskette has been authorized by the Laboratory Manager or the Manager's designee^ as verifi(-?d by the following signature.
iqnaturei
' ^^-^^ ' ' '^^ ' ..-.^a^.Mc RhA,.^. COVER PAGE - IN Rev..6/89
300494
3
I ^ ^ Names CEIMIC
TOTAL METALS ,S-: CYANIDE
5A ;;5F'IKE SAMF'LE REiCOVERY
Contracts ANSON
SAMPLE ID
IBllOS
SDG No.. T. CATCH_BA
Level (low./med)s LOW
Lab Codes CEIMIC Case No.s ANSON SAS No.s
L,.\trixs SOIL
"-Solids for Samples 99.0
Concentration Units (ug/L or mg/kg dry weight)s MG/KG
i '"
Analyte
'Iluminum In timony
I Arsenic I.Bar ium •ieryllium
,oadmium 1 Calcium ^l^omium ^^^alt I Copper ' ': ron .ead
; riagnesium I M a n g a n e s e lercury
...lickel 1 Potassium ">elenium •: i .1 ve r
1 Sodium '.Thallium Vanadium
(•Zinc 1 Cyanide
Control L i m i t
;\;R
75-125 75-125 75-125 75-125 75-125
75-125 75-125 75-125
75-125
75-125 .75-125 75-125
75-125 75-125
75-125 75-125 75-125 75-125
Spiked Sample Result (SSR) f
-«--»-„.—.„__....,.„....„_--„_____„
80.8080 1 7.19011
357.35981 8„6300 I 9.8068 1
37.26581 87 ..4767 I 47.0726 1
6„0698 i
145.5329 1 0.37961
89„63421
1.7723 i 12.1604 1
9.1644 1 91.5955 1 90.2226 I 14.43431
1 Sample :i Result (SR)
I 9.61071 I 1.4869 I 1 7.2570 1 I 0.78451 I 1.17681
I 11.5720 1 I . 1.7652 1
4.31501
1 1„96361
1 66.8824 1 1 0.09621 I 2.3536 1
1 0.48481 1 0„9307 I
I 0.1616 1 1 8.04161 I 7„6493 I I 1.2500 1
u
S p :i. ke Added (SA)
98,. 07 7.35
>92„27 9.81 9.81
39 „ 23 98.07 49 „ 03
3.67
98 „ 07 0.40
98.07
1.84 9.81
9.18 98 ,.07 98 „ 07 16.67
ZP.
B:
89. 80. 88.
oo,. 89. 87.
111.
80. 94. 89.
96. 114.
99, 85. 84. 86.
IQ _ • _ .
41 6 1 3 1 01 01
5IN
O 1 A- t
91
X.. 1
91 01
3 1 01
81 X . . 1
^~ 1
61
Ml
NRl F' 1 F 1 F' 1 P I F' I NR I F' I P 1 F- I NRI F 1 N R t F' 1 CVI P I NR I F 1 F' I NR I F ' P I F' 1 C 1
Comments s
FORM V (PART 1) - IN 7/88
300495 4
!re Names CEIMIC
Lab Codes CEIMIC
.vatrixs SOIL
TOTAL.. METALS &. CYANIDE
5B. POST DIGEST SPIKE SAMPLE RECOVERY
Contracts ANSON
Case No„s ANSON lo „ s
SAMPLE ID
IBllOA
SDG No „ s CATCH._BA
Level (low/med)s LOW
Concentration Unitss ug/L
—— — —
i ^ '
1 Analyte
, Aluminum 1 Antimony iirsenic Barium
1 Beryllium 'Cadmium I^alcium
,Chromium ICobalt ^^^p('?r
1 Lead ' 'lagnesium 'langanese
1 Mercury INickel -'otassium
, ..Selenium ISilver • .Sodium Thallium
I Vanadium 'Zinc i. yan ide
t _„„._„.„
.., ™. . . . ..._ ™ . . . . - » . . . . .
Control 1.. .1. m i t
rv.R
( MnrncvM"! tii>::
"""'"
S p i ked Sam p1e Result (SSR) C
161.00
«.
** "*•• "* -* **— — * " ~ " ~ — • -*" •*** •*" ••** •
Sample Result (SR)
59 „ 00
_. _—
C
_„„, _-,-.-- — - . . ™ ™ ™ -
Spike Added (SA)
100.0
ZR
102.0
— —
* • • • * " "
Q
—-—
I'i
NR NR NR NR NR NR NR F' NR NR NR NR NR NR NR NR NR NR NR NR NR Hfl HR hIR
FORM V (PART 2) - IN 7/88
300496 5
TO'TAL ME:'IAL;B &: CYANIDE
SAMPLE ID DUF'LICATES
IBllOD
lames CEIMIC Contracts ANSON
.sb Codes CEIMIC Case No.;; ANSON SAS No.s SDG No.s CATCH....BA
Ma 11- i X ( so i 1 / wa ter ) s SO IL Leve 1 (1 ow/med ) s LOW
:v Solids for Samples 99.0 Z Solids for Duplicates 99.1
Concentration Units (ug./L or mg/kg dry weight) s MG/KG
Analyte
Aluminum An timony Ai'sen i c Barium .Beryllium Cadmium Calcium Chromium Cobalt Copper Iron ead
Magnesium Manganese Mercury Nickel F'otassium Selenium Silvo^r Sodium Thallium 'vV an ad ium 'Z. i n c Cyanide
Control L i m :i. t
1.0 980.7
2.0
0.5
;.9
Sample (S) C
1609. 9. 1. 7. 0. 1.
911. 11. 1. 4.
5641. 1.
.<;;w;7i
66 0 X . . <
163 0 0
173. 0 8 7 1
8843 6107 4869 2570 7845 1768 0517 5720 7652 3150 8520 9636 1817 8824 0962 3536 3813 4848 9807 7765 1616 0416 6493 2500
Duplicate (D) C
1741. 9. 0. 7. 0. 0.
1020. 5. X., n
4. 4778.
A.. H
344. 71. 0.
219. 0. 1.
148. 0. 4. 8.
1741 8010 8784 4007 6001 8001 9021 4005 0002 6005 8778 3891 0344 4071 0878 4003 4219 5270 OOOl 4148 1757 4004 0008 5572
RF'D
-•-•-
51.5 2.0
26.6 38 „ 1 11.4 72.7
200.0 6.4 16.6 19.6 18.7 6.5
36.4 29 „ 3
2.0 15.7
58 „ 5 4.5
Q
*
Ml
P~\ P 1 F 1 F' 1 P I P 1 P 1 F' I F- 1 F' 1 P I F I F' I P 1 CVI P 1 P 1 F 1 F' 1 F' 1 F 1 F' 1 F' 1 C I
300497 FORM VI - I N V 8 8
TOTAL MEiTALS & CYANIDE
9 ICP SERIAL DILUTIONS
SAMF'LE ID
IBllOL Names CEIMIC Contracts ANSON _ .
ab Codes CEIMIC Case No.s ANSON SAS No.s. SDG No.s CATCH._.BA
Matrix (soil/water)s SOIL Level (low/med)s LOW
C^on cen 1: r a t i on l.Jii i ts s uq /I...
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese ni?>rc.K.\ry Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Initial Sample F;esul t (I)
„ _ „ _ _ „ . „ . . .
49.00
37 „ 00 4 „ 00 6.00
4645.00 59.00 9.00
22 „ 00 28765.00
1454.00 341.00
12.00 833.00
5.00 886.00
41-00 ,39.00
B
'r.-ji~>r-xa.l Dilution
Result (S) C
siiiTooT"" 245.00 IU
20.00 IB 20.00 IB 20.00 IU
4780.00 IB 75.001 45.00 IU 25.00 IB
29560.00 1
1465.00 IB 355.001
65.00 IB 1535.00 IB
15.001B 820.00 IB
45.00 IB 45.00 IB
Difference
1.1
45.9 400 „ 0 100.0
2.9 A . . / I* x
13.6 2.8
0.8 4.1
441.7 84.3
200.0 7 „ 4
9.8 15.4
Q M
P~ P NR P P F-F' P P P P NR P P NR P P NR F' P NR P P
•ORM IX - IN
30049S'
TOTAL. METAI..S & CYANiLDE
SAMPLE ID INORGANIC ANALYSIS DATA SHEET
CATCHB Name;; CEIMIC Contracts ANSON I
,...ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH_.BA
••-atrix (soil/water) s SOIL Lata Sample IDs 00006~01S
l._evel (low/med )s LOW Date Received s 01/07/92
Sol idss 92.1
Concentration Unilis (ug/L or mg/Kg dry weight) s MG/KG
CAS No.
7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-
90-5 36-0 38-2 39-3 41-7 43-9 70-2 47-3 48-4 50-8 89-6 92-1 95-4 96-5 97-6 02-0 09-7 49-2 22-4 23-5 28-0 60 o
66—6
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mo? r cury Nic ke1 F'otassium Selenium Silver Sodium Thallium Vanadium Z i n c Cyanide
Con cen t nx t i 011
0.09
.00
C
U
U
Q
Color Befores BROWN
fco1o r Af te r s YELLOW
I Dmmei^i tn;. s
Clari ty Before s
C1 a r i ty Af "te r s
M
NR hIR NR NR NR NR NR NR NR NR NR NR NR NR CV NR NR NR NR NR NR NR NR C
Textures MEDIUM
Ar^tif actss
•ORM - IN 7 /88
8 300499
TOTAL METALS &: CYANIDE
1 INORGANIC ANALYSIS DATA SHEET
SAMPLE ID
DW5 lame s CE IMIC Con t r<- c t s ANSON
•b-ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No-s CATCH_BA
'a t r i x (so i1/wa te r)s SOIL La b Sam p1e IDs 00006-028
C'evel (low/med )s L_OW Date Received s 01/07/92
Sol idss 95.9
Concentration Units (ug/L or mg/Kg dry weight) s MG./KG
CAS No.
•7429-7440" 7440-7440" 7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-
• 90 -5 • 3 6 - 0 •38 -2 •39 -3 •41 -7 •43 -9 •70 -2 •47 -3 4 8 - 4 •50 -8 8 9 - 6 •92 -1 9 5 - 4 •96 -5 9 7 - 6 0 2 - 0 0 9 - 7 •49-2 2 2 - 4 •23 -5 •28 -0 O.C. .^.
•66-6
A n a l y t e
Aluminum Antimony A r s e n i c Barium B e r y l l i u m Cadmium Calcium C h r o m i u m C o b a l t C o p p e r I r o n l._ead M a g n e s i u m Manganese M e r c u r y N i c k e 1 F ' o t a s s i u m Selen ium S i l v e r Sodium T h a l l i u m Vanadium Z inc C y a n i d e
C o n c e n t r a t i o n
0 . 0 9
1 „ 9 0
U
LJ
Q
• ^ ' o l o r B e f o r e s BROWN
u o l o r A f t e r s YELLOW
o m m e n t s s
C 1 a !'• i t y B B f o r e ;
C l a r i t y A f t e r s
M
NR NR NR' hIR hlR NR NR NR HR NR NR NR NR NR CV NR NR NR NR NR NR NR NR C
Textures MEDIUM
Artifactss
•0R:M I - IN 7 / 8 8
300500
TOTAL.. METALS & CYANIDE
INORGANIC ANALYSIS DATA SHEET SAMF'LE ID
1 DW6 Name;; CEIMIC Contracts ANSON 1
,.ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH_.BA
" vitrix (soil/water) s SOIL Lab Sample IDs 00006-038
Level (low/med )s LOW Date F\'eceiveds 01/07/92
84.7 SolIdss
Concentration Units (ug/l._ or mg/Kg dry weight) s MG/KG
CAS No.
7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-
•90-5 •36-0 •38-2 •39-3 •41-7 •43-9 •70-2 •47-3 48-4 •50-8 89-6 92-1 95-4 96-5 97-6 02-0 09-7 49-2 22-4 23-5 28-0 6 r-i r y
<.. .C
66-6
Analyte
Aluminum Ant.imony Arsenic E<arium Beryllium Cadmium Calcium Chromium Cobalt Co p pe r Iron Lead Magnesium Manganese Mercury N i c ke 1 Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide
Con CBn t ra. -tion
0.09
2.30
U
Ll
f' olor Bef ores BROWN
color Afters YELLOW
C1 a r :L t y B e fore;
Clarity Afters
Q M
NR NR' NR NR NF,' NR NR NR NR NR NR hIR NR NR CV NR NR NR NR hIR NR NR NR C
Textures MEDIUM
Artifactss
ommen '..s s
FORM I - I 7 /88
10 300501
TOTAL METALS &. CYANIDE
INORGANIC ANALYSIS DATA SHEET SAMPLE ID
DW7 i Names CEIMIC Contracts ANSON 1
:;ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH__BA
atrix (soil/water)s SOIL Lab Sample IDs 00006-04S
..e'-.'el (low/med) s L.OW Date Received s 01/07/92
Sol idss 87.0
Concentration Units (ug/L. or mg/Kg dry weight) s MG/KG
CAS No.
7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-
•90 -5 •36 -0 •38 -2 - 3 9 - 3 - 41 -7 - 43 -9 •70 -2 •47 -3 •43 -4 •50 -8 •89 -6 •92 -1 9 5 - 4 •96-5 9 7 - 6 •02-0 0 9 - 7 •49-2 A.. A.. ' 'T
A..\.> \ . '
•28-0 •62-2 •66-6
•-"olor Befores BROWN
Color Afters YELLOW
omments s
Analyte
Aluminum Antimony Arsenic Barium E<eryllium Cadmium Calcium Chromium Cobalt Copposr I ron Le^ad Magnesium Manganese Mercury Nickel F'otassium Se1en i um Silvo^r Sodium Thallium Vanadium Z i n c Cyanide
Con cen t ra t i on
0.34
1.90
C
U
Q
Clari•ty Before:
C .1 a r i 1: y A f l'. e r:;
M
NR NR NR NR NR NR NR NR NR NR NR NR NR NR CV NR NR NR NR NR NR NR NR C
Textures MEDIUM
Artifactss
FORM I IN 1 j_7/8S
300502
TOTAL METALS &: CYANIDE
INORGANIC ANALYSIS DATA SHEET SAMPLE IT!
DW8 lames CEIMIC Contracts ANSON I„
ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH_.BA
atrix (soil/water)s SOIL Lab Sample IDs 00006-05S
..evel (low/med )s LOW Date Received s 01/07/92
Sol idss 89.2
Concentration Units (ug/L. or mg/Kg dry weight) s MG/KG
CAS No.
7429-7440-7440-7440-7440-7440-7440-7440-7440-7440-7439" 7439-7439-7439-7439-7440^ 7440-7782-7440-7440-7440-7440-7440-
90-5 36-0 38-2 39-3 41-7 43-9 70-2 47-3 -48-4 -50-8 -89-6 -92-1 -95-4 -96-5 -97-6 -02-0 -09-7 -49-2 -22-4 -23-5 -28-0 6'_.'-.'> X . . X . .
-66-6
Analyte
Aluminum Antimony Arsenic Ba r i um Beryllium Cadmium Calcium Chromium Cobalt Copper I I'on L_ead Magnesium Manganese Mercury N i c l'-.e 1 Potassium Selenium S i1ve r Sodium Thallium Vanadium Z i n c Cyanide
Con cen tra ti on
0.26
,00 U
Q
c^olor Befores BROWN
Color Afters YELLOW
.•)mmen ts s
C1 a r i t y B e f o r • e;
Clarity Afters
M
NR NR NR NR NR NR NR NR NR NR NR NR NR NR CV NR NR NR NR NR NR NR NR C
Textures MEDIUM
Artifactss
FORM I 7 / 8 8
300503
TOTAL METALS &. CYANIDE
INORGAhllC ANALYSIS DATA SHEET SAMPLE ID
• I I i
I DW9 I Names CEIMIC Contracts ANSON 1 1
-...ata Codes CEIMIC Case No.s ANSON SAS No.s SDG No-s CATCH__BA
Tutrix (soil/water)s SOIL Lata Sample IDs 00006-068
Level (low/med )s LOW Date Received s 01./07/92
76 „ 7 bolIds s
Concentration Units (ug./L or mg/Kg dry weight) s MG/KG
CAS No.
7429-7440 7440 7440 7440 7440 7440 7440 7440 7440 7439 7439 7439 7439 7439' 7440 7440 7782 7440' 7440 7440' 7440 7440
90-5 -36-0 -38-2 -39-3 -41-7 -43-9 -70-2 -47-3 -48-4 -50-8 -89-6 -92-1 -95-4 -96-5 -97-6 -02-0 -09-7 -49-2 -22-4 -23-5 -28-0
—66-6
C - i l o r B e f o r e s BROWN
C o l o r A f t e r s YELLOW
( »mmo>?n t s s
Analyte
Aluminum Antimony Arsenic Barium Eie ry 11 i um Cadmium Calcium Chromium Cotaalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyan i do?
Con cen tration
0.12
2.20
C
*•"
U
Ll
Q M
NR NR NR NR NR NR NR NR NR NR NR NR NR NR CV NR NR NR NR NR NR NR NR C
Clarity Before;
Clarity Afters
Textures MEDIUM
Artifactss
FORi'i I - :I:N
30050*
TOTAL. METALS &. C Y A N I D E
>AMF'LE I D INORGANIC ANALYSIS DATA SHEET
. # . "BO 104
Contracts ANSON I._ 1
Case No. s ANSON SAS hlo - s SDG No. s CATCH._BA
Lata Sample IDs 00006-1IS
Date Receiveds 01/07/92
L^WF Names CEIMIC
Cab Codes CEIMIC
I Atrix (soil/water)s WATER
l._evel (low/med )s LOW
: Sol idss 0.0
Concentration Units (ug/L_ or mg/Kg dry weight) s UG/L
CAS No.
7429 7440 7440 7440-7440-7440-7440-7440-7440-7440-7439-7439-7439-7439-7439-7440-7440-7782-7440-7440-7440-7440-7440-
-90-5 -36-0 -38-2 -39-3 -41-7 -43-9 -70-2 -47--48--50-8 -89-6 -92--95--96-5 97-6 02-0 09-7 49-2 22-4 23-5 28-0 A O — O
6 6 - 6
-4
-1 -4
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury N i c l--.e 1 F'otassium Selenium Silver Sodium Thallium Vanadium 2!i nc Cyan i do?
Con co?n t r a t i on
84. 49.
r ^ J i - ,
3 . 4. 4.
6. 9.
13. 37. 1.
41., A. . K
0. 10.
290. 3, 9.
70. 1. 6. 5.
10,
on
00 00 00 00 00 00 00 00 00 00 00 00 00 00 20 00 00 00 00 00 00 00 00 00
1
CI 1
ui UI UI UI BI Ul UI UI Ul BI UI UI UI Ul UI Bl UI Ul Bl UI Ul Ul Ul Ul
1
r Jlor Befores YELLOW
Co1o r Af te r s COLORLESS
( )mmen ts s
Clarity Befores CLEAR
Clarity Afters CLEIAR
Q M
F' F F' P P F' P P P F' F F' F' CV P P F P F'
C
T e x t u r o ? s
A r t i f a c t s ;
FORM I I h-l
14 300505'
TOTAL MEIALS & CYAhllDE
1 INORGANIC ANALYSIS DATA SHEET
SAMPLE ID
I l~B0105 I Names CEIMIC Contracts ANSON I I
_ab Codes CEIMIC Case No.s ANSON SAS No.s SDG No.s CATCH_.BA
'"'atrix (soil/water) s WATER Lab Sample IDs 00006-128
Level (low/med)s LOW Date Receiveds 01/07/92
Sol idss 0.0
Con CErnt trati on Un i ts (ug/L or mg/Kg d r y wei g ht) s UG/L
CAS No.
7429^' 7440-7440-7440-7440-7440^ 7440-7440-7440-7440-7439-7439-7439-7439-7439-7440^ 7440-7782-7440-7440-7440-7440-7440-— .............
-90--36--38--39--41--43-• • " / O -
-47--48--50--89--92--95--96--97--02--09--49" -22--23--28--62--66-" "" "" "
-'•5 -0 „ r y
A-
-3 -7 -9
J i . ,
-3 -4 -8 -6 -1 -4 -5 -6 •0 •7 I
A., 1
•4 I -5 -0 ' " .C.
-6 " • " ' " • "
Analyte
Aluminum Antimony Arsenic Barium Bt?ryllium Cadmium Calcium Chromium Cotaalt Copper I ron Lead Magnesium Manganese Mo? r cury Nickel F'otassium So? 1 en ium Silvo?r Sodium Thallium Vanadium Z .1. n c Cyanide
Con co?n t r a t i on
84.00 49.00 2.00 3.00 4.00 4.00
7-,6 „ 0 0 9.00 9-00 6-00
220-00 1 „ 00
41.00 8.00 0.20 10.00
290-00 3.00 3.00
84.00 1.00 6 „ 00 5.00
10.00
1
CI Q 1 I
UI UI UI UI Bl UI Ul BI UI Bl
1
Ul Ul BI UI UI Ul Ul W UI BI UI UI UI Ul
I , 1 , ,,. , „,,
M
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•ORM I I hi 7 /88
15 300506
TOTAL METALS & CYANIDE
(Names CEIMIC
i.ab Codes CEIMIC
1 INORGANIC ANALYSIS DATA SHEET
Contracts ANSON
Case No„s ANSON SAS No„s
^.MPLE ID
IBllO
SDG No -s CATCH BA
atrix (soil./wato?r) s SOIL,
.evel (low/med)s LOW
Solidss 99.0
\» v.. 1 1 \ , t CV \. .1. V^ • 1 V
1
;CAS No. 1
17429~90~5~ I 7440-36-0 17440-38-2 I 7440-39-3 17440-41-7 17440-43-9 17440-70-2 I 7440-47-3 I 7440-48-4 17440-50-8 I 7439-89-6 17439-92-1 17439-95-4 17439-96-5 17439-97-6 17440-02-0 17440-09-7 I 7782-49-2 17440-22-4 17440-23-5 17440-28-0 17440-62-2 17440-66-6
1 1
^ 1 1 .1. v. i.f \, V,\ \J ^ 1
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cotaalt Copper Iron Lead Magnesium Manganese Me r cu ry Nickel Potassium Selenium Silvo?r Sodium Thallium Vanadium Zinc Cyanide
v./ I "*V.< ' ' ^ y ^ » * / *"»V.. a. U| 1 1 ^ / M
Con cen t ra t i on ,' C ,' Q
l6io7oo1~1 9„601UI 1. 50 I B I 7-30IBI 0 - 78 IB1 1 - 201 1
911-00 IB 1 11.601 I N* 1 - 80 IUI 4 - 301B1
5640.00 1 I 2.001 I
285.00 IBI 66-901 1 0-lOIUI 2-40 IB I
163-00 IB I 0 - 48 IUI 0„981BI
174.001B1 0.16IU1 8.001B1 7.601 I 1.201UI
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n I
p~l F' I F I F" I P I F- 1 P I F- I F' I F' I P I F I P I F- I CVI p : p 1 F 1 p 1 p 1 F I F' I P 1 C I
Lab Sample IDs 00006-078
Date Receiveds 01/07/92
MG/KG
r-"-)lor Before s BROWN
Color Afters YELLOW
:)mmo?n ts s
Clarity E<eforo?;
Clarity Afters
Textures MEDIUM
Artifactss
m •ORM I IN 7 / 8 8
16 300507
TOTAL METALS .?,; CYANIDE
INORGANIC ANALYSIS DATA SHEET SAMPLE ID
IB115 Names CEIMIC Contracts ANSON 1
rab Codes CEIMIC Case No.s ANSON SAS No-s SDG No-s CATCH_E<A
atrix (soil/water)s SOIL Lab Sample IDs 00006-08S
..evel (1 ow./m(:?d) 3 LOW Date F«;eceiveds 01/07/92
Sol idss 97-4
Concentration Units (ug/L. or mg/Kg dry weight) s MG/KG
CAS No.
7'429-90-5"" 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-B 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6 „_.„.„ — ».„..-_„...
Analyte
Aluminum An timony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc Cyanide
Con cen t ra t i on
liooToo 8.10 1.90 6.50 0-50 0.83
160.00 4.50 1.50 2.80
5350.00 1.20
243.00 54.30 0.09 2.50
198.00 0.57 0.50
164.00 0.19 3.30 6-50 1 „ 90
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w •ORM I IN
300508
TOTAL METALS &. CYANIDE
SAMPLE ID INORGANIC ANALYSIS DATA SHEET
IB210 Names CEIMIC
--ab Codes CEIMIC
Contracts ANSON
Case No-s ANSON SAS No. SDG No-s CATCH BA
atrix (soil/water): SOIL
Level (low./mo?d)s LOW
Lab Sample IDs 00006-09S
Date Receiveds 01/07/92
Solids 98-4
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
1 1
ICAS No-1 ' ,...•.... ,1
I 7429-90-5 17440-36-0 17440-38-2 I 7440-39-3 17440-41-7 17440-43-9 I 7440-70-2 I 7440-47-3 ;7440-48-4 1 7440-50-8 I 7439-89-6 1-7439-92-1 • 174,39-95-4 ' 17439-96-5 17439-97-6 I 17440-02-0 17440-09-7 I I 7782-49-2 17440-22-4 I 17440-23-5 17440-28-0 I 17440-62-2 17440-66-6 , ' ....,,
* . » . M . . « » . . ~ _ . » - _ « . '
Analyte
Aluminum Antimony Arsenic E<ar ium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury , Nickel Potassium I Selenium Silver Sodium Thallium I Vanadium Zinc Cyanide ,
Concentration _______
9.30 1.00 6.50 0.76 0-76
134-00 5-30 1-70 2.80
4300.00 2.30
305.00 53-00 0-09 2-50
207.00 0.54 0.57
132-00 0-18 3.40 8-70 1-30
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m FORM IH
300509
TOTAL METALS &. CYANIDE
1 INORGANIC ANALYSIS DATA SHEET
SAMF'LE ID
IB215 Contracts ANSON
Case No. s ANSOhl SAS No. s
^amB^ CEIMIC
:;:.;ab Codes CEIMIC
atriX (soi1/water)s SOIL
Level (Iow./med)s LOW
Solidss 97.2
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
SDG No.s CATCH_BA
Lata Sample IDs 00006-108
Date Received: 01/07/92
CAS No,
7429 7440 7440-7440 7440-7440 7440-7440^ 7440^ 7440^ 7439^ 7439-7439-7439^ 7439-7440-7440-7782-7440-7440-7440-7440-7440-
90-5 36-0 38-2 39-3 41-7 43-9 70-2 47-3 48-4 50-8 89-6 92-1 95-4 96-5 -97-6 02-0 09-7 49-2 22-4 23-5 28-0
J C J i -
66—6
^olor Before?s E<ROWN
color Afters YELLOW
ommentss
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cotaalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium S :L 1 ve r Sodium Thallium Vanadium Z i n c Cyan i do?
Concentration
784. 9. 0. 3. 0. 0.
34 . A.. I
1 . A.. I
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1 4 8 .
0. * A ^ m
9 1 . 0 . 0.
84 . 0 . A. . II
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