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001955
001956
ENVIRONMENT • PROTECTtON AGENCY
Ott i t , Entoicenifni' A r\ / ' /• r K ' "A r: \
CHAIN OF CUSTODY RECORD
R C G I O N i ^
Fi lS t l l i I r i [ i J ! i i > H t i l E i l i l t l Jl C i l l l Sl.______l')..ll.f,. I . - K J S 7^270
PROJ NO PROJECT NAME
\
STA NO D A T f c
•73"S I A I f O N I I H A I h.iN
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001957
CHAIN OF CUSTODY RECORD
i was su'-'ow «Fifit [ [ i t f [ [ )Jt i (>nal Hldf). 1 E!m St.
D.iiLr., T.-x.is 75^/0
PRO.) NO ^ P R O J E C T NAME
w?^^'^SAMPLERS i .,r,,—
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S T A Ni^ I OATF; i TiMF S T A T H I M ( (X A rH)M
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001958
c- A "\ i C - t taterf 4 3 l » ^^^,
r. 4 ^ 1 C - ^ "'erF I-''1!-? , \ O A ?
F 4 5 1 S - tt terIntractable)
r 4 5 Q 4 - ^ aler• ' J l-' I i \ UA t
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1. 4 ^ 0 " \\'lt''r1 ;ih' u «W\»\«
001959
i EnwfowwitI P'ot»ci>o" Afl»ftcv. CL^ S*"^ Mtn»gewm OHic*.
i? C 6««91B AK«»ftdfi»Vira«M,t223U 703/557.2A90
S«mpl« Number
F ^ e i S 'Organics Analysis Data Sheet
(Page 1 »
UiboraiorvNarne To^con Laboratories, Inc.
ili/ .LAb Sample ID No
Sample Mainx _
Daia Release Authorized B^/?
Case NoQC Repon No
Conrad No
Date Sample Received
VotatilflL^ompounds/ }Conceniraron ( Low/ Medium (Circle 0"et
Date Extracted/Prepared ^J? ^..'P.^UL-/1-2-)^ ^S ^'<Date Analyzed 0 ^ I •> •>.
Conc/Dil Factor ____—————pH——. » {7
Perce^il Moisture - —'" .I—.
'ed - i,.^ •^ o" / g ^
^ 3511^--^1^/^A5
D«n "•ao- •'; ^^« ' » i
^ •to^" "g • * » - • • * :c E"* ff 'c"o'*. - j -» i . " ia^ i ' < - i » ' » ^*#<l<>A1 • I".* ' *.-l i- '00•^-'0^»^ ••i; ( - •'s •H_ •I >•* t'V3.'•;?•; "0"
a»f ft ' l lo- ';• *• '- ' ty •—ui' a» •IJ' ;••
to. •fy " g ' t i ^ ' t ^ E " * '•'f 'f-io*. -• j ' t i . " ia^l • t - l « - » ^t#<l ' S ' ^ * ' 1 " f A / "' f\ f\ l^dd •i".* ' *-^ i- 'w-'o'*\ ».,; * - •'6 •n- •i »•• t-va.'•;?•; "O'-T-T- !''• ^ ' C '" U 0 . L' U ^4
- - - - . - . » f .„ w,.,i a^ ,,J, ;.,
V«lu» W lUt 'n^'' I t lai^ g'. >•»' ""••" "• H]^»' 'c '"<a<irc'i0- ''"" '•oo" •"» •*'^<"
U I'^diC*1*! ;ri"'&o""d .mi •-•'fnifl ','• Bn' "n' aai»'*'?ci**lltW' I"* —' "•'^^•~ A»i1^'.-3' 1 '" ' 'C>' '•'» l^'^O ' * "
«»K u n a 'O'-1! Mt*<l o" "•oin'. ; o^c »-'••'•o"fl.l^'.Ci"tC'.0"* I'''-.! 1 '%&• •'»<»tr'-i* t"« .nt" a •"»'••
d»r:' o" '•'•'.t i "f 'oofoif t'-i.-iii •«o UCo'^'oo"'^ ivi ••'• ii«^ *o' o^' •'"T (*iiri. i»d T''»"^"•(w •t i~"r " ." •"-— •"• -»'-•» 'ir'*'" !•»'• i--" • ' i '
i ' ' r u""c'1*
••vl •'•i n- •i —••*<i •• -.»•"''»'• * t - • • ' ' Q » .;1-»" I •r
•tl»",'''»iJ •..•]"-.[M-.^--iH o 'f • '
&• •u*'*- '10 •"»n ti l: " * 1 * I
C '^•1 'ItM •3C *t 'C M*!"-1^ M'*"-"*'*'* —^•" '"*id^-'n.cJi' 3'- ••»i a^f co"ti"^**<i tTv .";- MS S'"9'»'co'r 'oo' l-'•3»l l.£'Mi"0'^o u''" (*" ••n '*1 f'flr'
fo^' i •)» ..i-' •--co o. GC MS
8 ^"•'t ' •^ •i uw3 *^»' 1'^ •'\»<»i» '* ta-'••<l '•' '"» n'»"-•t •*'*• «i • •K'^'O'* n •"d-c^r* &o<i "•• o'iMHO''Bl»"« i:0"l»'-'.n»!,o" •' «W-"t '*'• d* * "**• 'C !•*'
>00' on'.t'y aci'o"
O'*'*' O'"*' »[><• < . ( "rfli •• i '[xi'-ic'n '"•' '** '•<" '*•' 1 0
P'or—", (**' -^ i-'» . •1^ ,111 i ..wa •"'»• "" •1 ' 3*'""'»»»> • .(?*(! ••-rf- I ^.-~ Mt- •.D>'"" • ' !<^ '' 1 1- '''•' d""
t^-in-l, , ••yn'"
tf •i •ki , - • -,^, p »i* > ' . - , 3 . < ? 8 A 0 6 9 i ^ 2t
001960
loborolories, inc.
June 20, 1985
USEPAContract LaboratoryprogramSMO'P. 0. Box 8L8zOexandria, VA 22313
USP:P^^LP. 0. Box 15027Las Veqas, W 89114a,ttn: Oata audit
Staff
US^P^ Region viPnvironmental ServicesDivision6609 Hornwood Drive'^ont^rrey Park Plaza,Buildi' g C?\ttn:Dr. William Langley
oe: contract ^o. 68-01-7026; Case "to. 3984; QC report No. 3984
Enclosed are thc^ resubmitted mdterial for Case \o. 3984 received fromUSEP^ Region VT on March 23 and 26. 1985. The sample identificationand analyses requested are as follo^-s:
Toxicon Number
2978/022978/C32978/04
USEP^ Tdentification
F 4518 Low WaterF 4594 :^- WaterF 4600 Low Water
Pull HSLF-Jll H^LF'Jll HSL
Contract Mo. 68-01-6809 was inadvertently employed on the data packageand SLimrary pdCKdt.Je cover letLers. Cov^r" iett^rs A,t.'n the correctionare enclosed.
Sincerely,' f- '' ' ^ <"^ i
Z/ i J^ x^ . Lik^ y.-^^Charlie t?. Westerrran, Ph.D.Technical Director
CEW/jwF.nclosures
001961
^ f •
laboratories, inc
/^-r s^.n, y /tl.^ti ^^J-
C L / - C / ^
^.^^< //-Ta^--••-'•••
May 22, 199S
'JSEP^Contract LaboratorypL'oycamSN1;P. 0. Box 8^8Mexandri-a, ' 7\ 2231-3
US^P'"-.WSLp. 0. Box 1-5027r-as Veqas, NV 89114^ttn: Data ^udit
StAff
USRP'\ Reqi-on VTEnvironmental ServicesDivision6608 Hornwood DriveNfcintfirrey park pLaza,Building CMtn: Dr. William l inqley
Re: Contract No. 68-01-6809; Case No. 3984; QC Report No. 3984
Enclosed are the analytical data and quality assurance for Case No,3984 received from USEPA Region VT on ^-irch 23 and 26, 1985. ThesaJiple identification and analyses requested are as follows:
Tax icon N'Jmber ys^PA Identification ?^nalysis Tasks
2978/022978/032978 '04
FFF
45L845944600
LewLowLow
WaterWaterWater
FullF-ollFall
HSLHSLHSL
v\1 \-U^ //'ha:-Li->? r';. ^st-er-.'3.-,, p;i.?.
3 9 P '-» 0 6 1 C 0 1
001962
fc - s. i
loborolohes. inc
May 22, 1985
USE PAContract LaboratoryProgramSWP, 0. Box 81-8Alexandria, VA 22313
US^PA?MSLP. 0. Box 15027IA3 Vegas, W 89114Attn: &3ta Audit
Staff
US^PA Regl-on VIEnvironmental ServicesDivision6608 Hornwood DriveMonterrey Park Plaza,Building CAttn:Dr.William Langley
Re: contract No. 68-01-^809: -Case No. 3984; 2C Report No. 3984
Enclosed are tne analytical data and quality assurance for Case No.3984 received from US^PA Region VI on March 23 and 26, 1985. Thesample identification and analyses req'Jestsd are as follows:
Toxicon Numbe;
2978 -022978 '0329"^ '04
USEPA Identification
F 4518 LCTA- Wa^rF 4594 Low Wa^r-F 4600 Low Water
Analysis Tasks
Full HSL1M11 HSLFull HSL
Sin.-er-'i-y,
•^'A '-<1 '-•t--^ //v'' • \^'' x < . t—^-C nar 1 i Q '•:'. ' s ie r v^ n, ? n. D.Tl--•lc".-''• i-c^ •- ^ir-^-^tor
. "7'% '" '*('
3 9 8 4 0 6 9 2 0 3
001963
N° 1 2 9 0S A M P L E M A N A G E M E N T OFFICE r»C
I n v o i c e n i s r - r f n a n r - v R ^ n o r t - 0 'k. ^I n v o i c e D i s c r e p a n c y R e p o r t^
Invoice Number:Lab:Invoice Date:Cost Lot: /?
.' r rContract Number: C f - C :' - 7- i ^^Case Number:r v y j ^ ) m
r~-r-'3-o
k <_ ^ < -^.•/^'/^..^1^^ ^^ U}^ ^ // /^i^_.. A^/.7-' ^./n/n/^..Reason:1 . I • ' • I . J Is^ • /' i •l^—L^w. ^L . . . Ut /U^' t7 ^^ i^\ . ' \i. ^- ^^-L ^P,•^ ' / ^ . ^ ^6( f\-i.(:' / - _ . _ ^ J ^ f . C T ^ .L, ^. .^---^-L ^^i___ Q
'pi^ .^ r ' L L \ H^ ^. Z> ^/ '..-^. y^- ^^ /^-' ^ ^ h c^ ot' . € _ __p^-—————,—^——
.•^<<.;-,/^r:.
^
/L- - ; ^
• / - 1 ' ^ ^/f^/ /^.-.^^^^^ .•; .__^ ; ;—^c, ' " / / ^ 7 ^/ /^^^^.'.7/ ^ / ' 7 • f -
! - ' : - :>• (: '•-f 7* • / ;•,' ' Reported by: FTS/703 557-2490Direct inquiries to: Marta Meixner Reynene Barrett Anna Payne Marge Galloway
3 o 8 A 0 6 ( - - ^ ^
001964
-1 t
loborotories, inc
Mav 22. 1^16
'JSE?r\'oniract I^i-or^tory">Y- •i"' r' :l''"i1. - •J-J L di i.
SMOP. 0. Box 81.8Mexandri-a, VA 22313
US^P^PMSLP. 0. Box L5027Las Vegas, W 89L14Attn: O.^ta i\udit
Staff
UWP^ ^.^ i-on V:Rnvi-roruT^^ntaL cervicesDi. vision6608 Hornwod DriveMonterrey Park Pla7.a,Buildirtq CAtt.nrOr.WillicL'n LarK^l^y
P-^: Contract So. 68-01-6809; Case No. 398.1; QC Report N'o. 393-1
Er>,Jlosed are the analyticaL data and q-JdIity assurance £or Case No,3984 received from USEPA Region VI on M^rch 23 and 26, 1985. The'- mple identification and analyses requested are as CoUows:
^•^'~ ^ 03< ' -i / 0 4
US^P^ Identification
F 4518F 4594[••' 4600
now Water"TJOW Water''..OA' Water
.^n.^l-ysis Ta3<s
Full :{SLF\ii'- -L3L
^^T.
/ \_^\ \ .i.. ^-•^-A1 ^^r
i :-": :e T-;. ^ - :' •rT.'i:,, Ph.D.
r*. -^
.- Q 0 1
001965
E^, o^ma".*! ProftKI.O" Agt-Cv CL^ SBT'0't^ftat'T'Tll 0".C»
P .: B o . B ' a Alefxjm Vi'g.".< ; 3 3 1 3 703-'557 2490Sample Nurnbof
^S/,y
Organics Analysis Data Sheet(Page 1 »
U»t.:--a!orv\ame Toxicon Laboratories, Inc. Case No __
Lac Sample 10 No ^9 '•'l/0^_________ QC flepon Noi/J^< Sa-.oleMa:'ix ^——J^JL-tC—___________ Contract No 68-C1-7Q26^ ^ ^
Daia Release Authorized B<^ UXJ^uA±kLAaA. Date Sarnpte Received
VolalilfiLCompounds
Concentration ( Low// Medium (Cn-cle One)
Date Extracted^repared ^ 5 v J^
Dale Analyzed
Cone/Oil Factor
Percent Moisture
Percent Moislure (Decanted)~—^
^uo / '9 '"Q / t<0 CAS'-——fdrclaOne) Numbef
CASNu-'ibar7-S .9 7 - 3
^S^ 9 "}75- ' l -475. CC 375 i 767-£.; 1
75 * S 075 3; 47^ 3.: 3' -::- c,*:' 6; 3T' :" ?7^ 9: 37 ' 5^ ••,C. .- ' -. £
1 -. Q - ( ;)
7^ : - .
————————u—————————— , ,. , .Chlo'-o^e"~'d^e j /i; Bfoi-"o ethaneVmv' Chlof'acC^>'0^&<!ha-^eMefiv'fc^< C^lo^deAce'cneCa'tio'-' D's-.-'ide1 1 -Dic^lc.'oftihen^1 1 -D'crifci'c^ihd'-'e''"I'A'^S 1 ? ^ l ; t^la^^f l•1e f 'e""'o's'^"^' 2 3.r'';,J'3e:*',aie? •G.i'-s'^-f^f' 1 t •Tf..:^.3foc"'.a'-pCa'^'3" 'T'f'.i:'"o-i';''. "»' A;f I - "5 •3"^ '><:•: '•''•.'.-)•-'?•- 9 '•'-
/L-1 y
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79 3-1 678 87 -5lOQo-i -02-67 9 . 0 1 - 6'l as l
79.X £7 ' 43 21006' 0' 5' i ; ^S e
76 ^ :59' "= <-,1 ? ^ 1 - •' 2 7 1 5 41 0 - •:'" 31 3 5 5: 'i '>; j • d
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Organics Analysis Data Sheet(Page 3)
Sample Number
T ^7
Pesticide/PCBsConccnirat'o'-' (Lo^y Medium
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fug ' ibf ug 'KgTC'rcle One
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Organics Analysis Data Sheet(Page4»
Sample Number
c- <4 <. 1 ^1 J 1 ^
Tentatively Identified Compounds
CASNumtxr
1
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1
4
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22
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29
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001969
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Sample Numlxir
^.59<7Organics Analysis Data Sheet
(Page 1 )
Labc-BiorvName T^con Laboratories,Inc^'' 0 *>( 3- //^ "•<Lab S s-nple ID No ^ J J '. / ^-^
Sa.^ceMair .x 1/^:4 k; ^Sa.^ceMair .x 1/^:4 k' ^ ______
Data ^clease Aulhon^ed By ^-e \v\ L^A^.'^YY\
Case No
QC Repon N;
Contact No 69-01-7026
Date Sample Received 03 I ^ 3 / ^^
Votatilfi-pompounds/'^ i
Concentration / Low/ Mediu"-1 (Circle One)
Date Exiracied/'Pfepared vt ^ "-C'3^^Date Analyzed
Conc/Dtl Factor
Percent Moisture
Percent Moisture (Decanted)^—-^ug/ loruo /Kg CAS
.ircle 0"a) NumberCASMu—Sir
7d c"^7-i S3 975 - :< -d
75 :•: 375 267.6.; 1
75 ' £ 375 3 ^ - 4
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Organics Analysis Data Sheet(Page 2)
Sampla lumbar
i^us^
Semivolatifo Compounds
Concentration ( Low )
Oate Extracted/Prepared
Dale Analysed
Medium (Circle One)c ^Si S
Conc/Di! Factor
'uu/l^t/ ug/Kflircia Ortel
CASNu'nb«f6: 75-9
10S 95-2
62 53-31 1 1 - 4 4 - 4
95 57-B
& d 1 . 7 3 1106 <l6-7
1C':- 5 1 - 6
96 S? 195 •lg 7
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1 2 1 - 1 4 . 2
606.20-2
84.65-2
7005-72-3
86 73 -7
100 01 -6
534 5 2 - 186-30-6
1 0 1 - 5 5 - 3
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8 7 - 6 5 - 5
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94 7 4 . 2
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E", :>'••,-(^;< '''• 01 »:!';>'•' A^fcy CLf S«"-'p'« M«i»3»nioni O+ficcP ; B o « B ' 6 Ai t .&^a'r V.'e'^t 2 2 3 1 3 703-557-2490
Orgamcs Analysis Data Sheet(Page 3»
Sample Number
r' 4r_f4-
Pesticide/PCBsConcenua'ion (Low.)
Dale Extracted/Prepared
Dale Analysed ____'
Cone/Oil Faci&r ____/_ ^
Medium (Ctfde One)
lAl/ :
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(iJg^r ug g'-it.rcleOne)
3 1 9 - 8 4 - 63 1 9 - 9 S 73 1 9 86-858 89 976-A4-8339-00 21 0 2 4 57.3959-98 860 57-172-55 972 20-83 3 2 1 3 - 6 5 972-54.87d2 l .93 -4
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Sample Number
F '/Organics Analysis Data Sheet
(Page 4)
Tentatively Identified Compounds
CAS..imtxif
1
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3
4
5
6 . ....
7
a
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1 2
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1 4
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24
25
26
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29
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Sample Numtxr
F ^ G ooOrganics Analysis Data Sheet
(Page 1 »
U^o-aio^Na-ne Ig«ico i bgcatgr,ies, Irc_
Lab Ss-nple ID No _ ^^.L/0^.
Case No
QC Repo^ No
Conuac<N= 69-01-7026SaTiple Mai f 'x .————" —- - i___r-/——.=?=——————Sa-nole Mainx ..
Data Release Authonted B \^^^\U^ •sAC- iJ. -rt . Oa.e Sample Received -. 2-L?-llilS
Volatilfi.^ompounds
Concentration ( Low/^ Mediurn (Cirde One)
Dale Extractcd/Preparert ^L2-£^JL5-
Oate Analyzed ______G ^ S^
Cone/Oil Factor
Perceni Moisture
Percent Mois tu re (Decaniecj ;y—•\
( l J O / . t9 f u o / K Q'-—^Circia Onol
CASN'Limbar
7 4 - S 7 - 374.63 97 5 - 0 1 - 4
75-00 .175-09 257 64 •7S 1 5 - 0
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l^b0^
Organics Analysis Data Sheet
(Page 4;
Tentatively Identified Compounds
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001975
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Organics Analysis Data Sheet(Page 2)
Semivolalile Compounds
C3ncentfai>on ( Low y Medium (Circle One)
Date ExTacred/PreptKed — ^ ^^JLyA,
Date Analyzed
CASf^u'-nbar
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Organics Analysis Data Sheet(Page 31
Sample Number
±^°
Pesticide /PCBs
Concenirai'on n.ow_) Mcdum
Date £>clfa^ed/Pfepa''ed
Datp Analyzed
(Cifcie One)
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3 1 9 84 63 1 9 8S 73 1 9 66 8S8 89 976-^-8339.00 2102d 57 3959 98 S60 5 7 - 172 S5 972.20-83 3 2 1 3 - 6 5 972 .54 -874;' 93 -41 0 3 - - 0 7 . 850 29 37:.43 553494 72 55 7 - 7 4 99:>0' 35 21 2 6 7 4 1 ' -2
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WATER SURROGATE PERCENT RECOVERY SUMMARYContract Laboratory TtKJcon L^bor^torie^ Inc.___ Contract No. ^-01-^026
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Caic No.
WATER MATRIX SPIKE/MATH.,. ;>PIKE DUPLICATE RECOVERY
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REAGENT BLA. K SUMMARY
Cas9 No.6B-01-7026Contractor T^ icon Labor ft tori eg. Inc. Contract No.
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001980
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Sample Numtxr
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Organics Analysis Lata Sheet(Pdje 1 J
La';':"a!onr Na^e
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O a - a Release Au^o^ed 8^ J^/'^ i/U^^-^
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OC Repon No 3 j' Y
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Votatilfi^ompornds
Concentration / Low/ Med'u^n (Circle One)^— '/^ - T -ir. <., <•
Oate Exiracted^Prepared __—ii_^
Date Analyzed ________^2_?
Conc/0.l Pacio' ——J_____pH
Percent Moisture
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Orgamcs Analysis Data Sheel(Page2»
Sample Number
M B i
Semivofatile Compounds
Concentration ( Low ) Medium (Circle One)
Date Extracied^Prepared
Dale Analyzed
Conc/Dil Factor
<UO/l>rug/Kg.ircl* One|
CASNumb»f62 75-9108 95-2
6 2 - 5 3 - 31 t 1.44.4
95 57-8
5 4 1 . 7 3 - 11:^ 45.7
1 0 0 . 5 1 - 695 5:/ l9s 48 7
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87.68 359 50 7
9' 57 67 7 4 7 4
98 36 ?
96 9'- 4* 9 I 5S 7
99 7-1 41 3 1 n •)
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Tentatively Identified Compounds
Strnple Number
MR l
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ORGANICS tRATnC^^^^^ScropleNurabT
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LAB FILE COPY
001987
ScRnpleNumbar
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^ I
loborotories. inc
^y 22, 1965
US^?^Contract LaboratoryprogramSWP. 0. Box 818Alexandria, VA 22313
US^PAWLP. 0. Box 1.5027Las Vegas, W 89114Attn: Data Audit
Staff
USEPA Re9i-on VCRnvironniental ServicesDivi.si.on6608 Hornwood DriveMontzrrey park P-lasa,Building CAttn:Dr.Willi.-yn Langley
Re: Contract No. 68-01-6809: Case No. 3984; QC Report No. 3984
Enclosed are tne analytical data an5 quality assurance for Case No.3934 received from USEPA Region vl on M^rch 23 and 26, 1985. Thesair '-le identificf.ti-on and analysca req'^st3d are as follows:
Toxicon ^arnb r
2978 '022976 0329'c 04
USSP^ Identification
F 4518 Low WaterF 4594 Lcr/-- WaterF 460'; Low water
'Vi-alyais Tasks
?Jll HSLF'Jll HSLFUL1- KSL
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001992
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(Page 1 )
Labc'aiory Na-ne Tox^-con laboratories, Inc
Lftb Sample (0 N3 ^ 9 S 7-/c>^
Sample Matrix lA^+^ ______
Data Release Authorised f^ QV ^AL^?T.I L \
Case NoOC Report r4c _______3^S^
Contract No l8^01^7026.
Date Sairiple Receded
VolatjJe-^ompounds
Concentration // Low/ Medium (Circle One}
Dale Extracted/Prepared ...... ° -J • ^ i s^
Date Analyzed
Cone/Oil Pactor
Percent Moisture
,PH
Percent Moisture (Decanied)
u f l ' ' t o r u g / K g CAS,ircla One) Nufnbe r
CASNumbar74.87.374-83-97 5 - 0 1 - 475-OC 375-09 267-64 17 6 - 1 5 - 075 35 -475 34 31 5 6 53 56 - - 6 £ 3107-06 :76.93 37 1 - 6 5 656 . : 3 -5106 05 475 7 7 . 4
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fts^Organics Analysis Data Sheet
(Page 2)
Semivotatile Compounds
Conceniralion ( L o w y Medium (Circle One)
Dale Extracted/Prepared t '6 :>
Date Analysed
Conc/Oi! Factor
ug-'l^fug/Kgrcle Ona}
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CASNumber
62 75-9
10S 95-262 S3.31 1 1 - 4 4 . 4
95-67-85 4 1 - 7 3 - 1 ''06 45.7
1 0 0 - 5 1 . 69 5 . 5 3 . 195-43 7
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83-32-95 1 . 2 8 . 5100-02-7132-64-9
1 2 1 - 1 4 - 2606-20-284-66-2
7005-72-386-73-7
1 0 0 - 0 1 - 65 3 4 . 5 2 - 186-30.6
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56 55 3 11 1 7 . e i 72 1 6 01 9i T7.e ' i o205.99 2207-08 950 3 2 - 81 9 3 39 553 70 3l9 i 24 2
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2, d-Omnrophenol
4-NtirophenolOtb«n;o(ufan2. 4 Oinitroioiuene
2, 6-Oiniiroio'uencOie;hytphthalaie
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Orgsnics Anatysis Data Sheet(Page 3»
Pesticide/PCBsConcentration (Low) Medium
Dale E'ctraci&d/Prepared y /
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Cone ''Dit Pacior - - - / -P
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3 1 9 - 6 4 - 63 1 9 - 8 5 - 73 1 9 - 8 6 - 858-89 976-^-8309-00-21024-57.3959-98 860 57.172-55-972 20-83 3 2 1 3 - 6 S 972 54.67421 93-41 0 3 1 - 0 ^ " - 65^ 29 37 2 - 4 3 . 553^94 70-557 74 98.^1 3 5 - 21 2 6 7 4 1 1 . 2n i C W . 2 8 - 2n 1 4 1 . 1 6 553469 2 ' - 9•2672 29 61 1 0 9 7 . 6 9 1i 1 0 9 6 82 5
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f ^ S l ?Org?nics Analysis Daic* Sheet
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Sample Numtxir
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Organics Analysis Data Sheet(Page 1 )
Labo-aioryNsme TcKicon Labor atories. inc. Case No
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Cone/Oil Factor
Percent Moisture
Percent Moisture (Decanted)
/'ug/lorufi^g"——tCirclflOna) '
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Stmp(» Number
1=-4^Organics Analyst's Data Sheet
(Page 2)
Semivolatile Compounds
Medium (Circle One)c^a f c - ^S
Concentration ( Low )
Date Extracted/Prepared,
Dale Analyzed ^ f$
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l 3 t u 32 OR 9-3 R99 09 ;
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Pestid'de/PCBs
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Conc^Dtl Fad&f
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3 1 9 84.6319.85-73 1 9 fl5-858-89 976-44.8m 00-21024 57-3959 98 860 5 7 - 172-55 972-20.83 3 2 1 3 - 6 5 972 54.8"4^ 93-4' 0 3 1 07-850 29 37: 43 5S,3d94 70-55'? 74 99:^1 35 2l 2 6 7 d . 1 1 . 21 * 1 0 4 26 21 1 1 4 1 . 1 6 - 553469 2 1 - 91 2 6 7 2 29 6i 1097 69 1H096 82 5
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Sampla Number
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Sample Numbar
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(Page 1 )
Labo-aioryName Toodcon Laboratories. Inc.
Lab Sample ID No ^9 ^ V^ <_________
Case NoOC Report No
Samc-e Matrix ____tA^t ^ , /'__r_______ ^..,.^. .../ _____Contract No 68-01-7026
Data release Authored By ^/ 'JL^T t ^^^v''" Date Sample Received
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Date Analyzed
Medium (Circle One)
C^M^
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Sample Number
M B (
Semiyolaiile Compounds
Concentration ( Low ) Medium (Circle One)
Date Extracted/Prepared — .liJii
Date Anafy^ed
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CASNuTtbaf
62 75-9'OS 95-2
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Sample Ni.mber
M^ i
Tentatively Identified Compounds
CASH^mber
1
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Sample Number
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Semivolatile CompoundsConcentration Low Medium (Circle One)
^ate Extracted/Prepared __„___________
Date Analy7ed _1. •v"2l^-^•
Conc/Dil Factor
ug^lorug /Kg(Circle One)
CASNuTiber62 75.910£ 95 -262 S 3 - 3' 1 I-44-495-57.85 4 ^ . 7 3 - 1105 .46 -71 0 C - S 1 - 6SS-^- l95-< ia .739638 32 -9106-44.5b2 ' - o4 .76 7 . 7 , ? . 19S 95 376 59 186 75 605 67.9
66.S5.01 1 91 1
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83-32-95 1 . 2 8 - 5100-02-7132-64 91 2 1 - 1 4 - 2606-20-284-66-27005-72-306-73-7100-01-6534.52-186-30-61 0 1 - 5 5 - 31 1 8 - 7 4 . 187.86.585-0 1 -81 2 0 - 1 2 - 784.74 2206-44-092-97 5129-00-085-60 791 - 9 4 - 156 55 31 1 7 - 6 1 - 72 1 8 - 0 1 - 9U 7-84 0205-99 2207-08 9S0.32 81 9 3 39 553 70 31 9 1 24 ?
AcenaDhihene2. 4-Dinilropheno'4-Nnrop^eno'Diben2ofuran2, 4-Dinilroto'uenc2, S-OinitrorolueneDiethylptithalaleA-Chlorophenyl-ohenvleth^fFluorene4-Nnroaniiine4. 6-Di^l!^^o-2-^^e' t"'vlph 'eno !
N-NiirosodiDhenyldTiine ( 1 !4-6^omoo^er^v^-Dh6 r 'V le t ' '^e'HexachlorobenrenePentachiciroDhenolPhenariihrerieAnthraceneDi-n-BulviphihalaicPtiJOfantherieBenndmePyre^eOutvibefwvip^ala'e3, 3'-D'chioroben?idineBen;o<atAnihrai:cneC»is(2-£ihvlheKvt|Prn-iaiaipChryseneDi-n-Ociv' PmhaialeBen;o(b»F!uor»nlherieBenJ'o<i()FiuorantheneBarucMalPyfeneIndenoil 2, 3 cdlPyene3ibentia hiAninracenpBeri;o<g h tiPefvif-'p
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Pesticide/PCBsConcenlration: (^L^w Medium (Qircle One)
Dale Extracted/Prepared __/>-^/
Date Analysed ^ / f
Conc/Dil Factor I C
Sampiy Number
^t^-c/^p
CASNumber319 -84 -6319-85-7319-86-850-89 976-44-8309-00-21034.57.3959-98-860 57-172-55-&72-20-833213-65-972• ti4•87421-93 .41031.07-850-29 372-43-553494-70-557-74 98001-35.21 2 6 7 4 - 1 1 - 21 1 104.28-2! 1 1 4 1 1 6 - 553469 2 1 - 912672 29 61 1 0 9 7 6 9 - 11 1 0 9 6 32 -5
Atpha-BHCBeta-SueDflita-BHCGamwa-BHC (Lindane)HeotachlorAldnnHoptachlof EpoxideEndosutfan 1OfetdJ-in4.4 -ODEEndrinEndosutfan 1 14. 4'-DDDEndnn AldehydeEndosulfan Sulfate4, 4'.DOTMethoxvcn'orEndnn KeioneChlo'daneToxa&hent*A roc l o^ -1016A r o c i o r - 1 2 2 1Aroclor-1232Afoclor 1242Acoc lo r -1248A^oclol••1?.54Aroclo ' -1260
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Tentatively Identified Compounds
CASNumb*r
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Sampla Number
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(Page 2)
I!11111
1
111
SeConcentration
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Dale Analysed
Conc/Dil Factor
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Organics Analysis Data Sheet(Page 3»
Sample Number
-^4^crA>>
Concentration
Dale Exiiacied/P
Dale Analyzed
Cone/Oil Factor.CASNumbar
Pesticide/PCBs^—"i\.Low./ Medium
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(Circle
WOnet
319-84-6319 -65 -7319-86-858 89 976-44-8309-00.21024-57-3959.98-860-57-172-55-972-20-83 3 2 1 3 - 6 5 - 972 -54 -87 4 2 1 - 9 3 - 41 0 3 1 - 0 7 - 850-29-372-43.553494 70.657.74-98001-35 21 2 6 7 4 - 1 1 . 21 1 104.28 21 1 1 4 1 - 1 6 553469 2 1 91 2 6 7 2 - 2 9 61 1097 69 11 1 0 9 6 82 6
Alpha-BHCBeta-BHCDef:a BHCGamwa-BHC (LindaneiHeptachlorAldrinHeptachlor EpOKideEndosu^an iDieldnn4. 4 -ODEEndrinEndosulfan (ld 4'-DDDEnd'in AldehydeE^dosuHan Suifate4 4 -DDTMeihoKyc'-.io''£nd*'i^ Ke'o~'eC'^io''daneToxas^eneAroclo^-IO^Arodo^ 1 2 2 1Arocio ' ' -1 232Arocio ' . 1 242A'-ocio' 1 2 4 3A r o c t o 1 ' - 1 254A r o d o r - 1 2 6 0
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Tentatively Identified Compounds
Sample Number
^ fcc^M S,
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Labc'alorv Name
Lab Sample ID No
Sarnie Mainx
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Contract No .68-01-7026
Data Release Authorised By Dale Sample Received
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Conc/Dil Factor
Percent Moisture
Percent Moisture (Decanted)
u g ^ o r u g ^ g(Ctrctfl Onol
CASNumbar
74.87-374.83.975-01 -47S-OC 375.09 267-64 17 5 - 1 5 - 075 -35 -476-34 3156-60 -567 -66 -3107-06 278 93 37 1 - 5 5 65 6 - 2 3 - 5108-05 475 -27 .4
Oio'o'Tie thaneBfOTiomeiha^eV'nv1 ChlorideChioroeihaneMethane ChforidcAceioneCarbon Oisul^ide1 1 -Dichloroeihe^e1 , 1 -DichloroethaneTrans-1 . 2-OichioroeT^eneChlorofofrn
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100 42 5
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Organics Analysis Data Sheet(Page 3)
Pesticide/PCBsConcentration ^ow) Medium (Circle One)
Dale Extracted/Prepared
Dale Analysed _/1- ^ f • c——^~?^
Sample Number
EA^^ ^^
Conc/Dil Factor
CASNumber
(uo^^ug^rTCircle One)
3 1 9 8 - 1 63 1 9 8 5 •?319-86-858-89-9
176-44.8309-00-21024-57-3959-98-860-57-172-55-972 20-63 3 2 1 3 - 6 5 972 54-87 4 2 1 - 9 3 - 41 0 3 1 - 0 7 - 8''0 29 3-2-43 5•'3494 70-5•.7 74-9P.Y31-35 2' ;674-H-2
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Organics Analysis Data Sheet(Page 4»
Tentatively Identified Compounds
Sample Number
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Sample Number
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Semivolatile Compounds
Concentration Low Medium (Circle One)
Dale Extracted/Prepared „___
OoteAna.'^ed /t < -^ . .o
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CAS
62 75.910° 95 -262 53-31 1 1 - 4 4 - 4
95-57-65- : - .73-1106.46-71 0 0 - S 1 - 6o^-S^. I95-48 739636 32-9106-44-562 - .64 -767 72 195 95 378 59 18£ 75 5105 67.965 B5-0IT 9 1 . 11 2 3 83 21 2 0 82 '9' 20 31(X 47 687-68 359 50 791 S7.677.47.4B8 06 295 9S 491 S8 788 74 41 3 1 1 1 3208 96 699 09 ; 3 ^n^.in.i^.f ( . .
N'AiifoscsJiTiet^vla'TTneP'-ieno'An.l'nebiSl-2-C^i^rcwihvOEthef2-ChloroD^pnol1 , 3-D'chiotoben^ene1 , 4-Dichi^robenteneBen?v1 AI;:I»IO)1 2-Dic^i^'i>hen;ene
2-Me;nvt.3->rno'bis(2-chlo''^Kiop'-opvl!E!^cf4 - ^e tnv lo^p^o fN-Niiroso ^>. n.Pfoov'a'^i^':'He«3chio'r'r".ane^ii-oben/e -'(•iSODhO''Or'P
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( 1 1 Cannot t)r iffoafaiei-l ffo'r- clip'-n*nvta'-"i"e
83 32.951 28-5100-02-71 3 2 - 6 4 - 91 2 1 - 1 4 - 260G.20.284.66-27005-72-386 73-7100-01-6534 .52-186-30-61 0 1 - 5 5 - 31 1 8 7 4 - 167 -86 -58 5 - 0 1 - 81 2 0 1 2 - 784 ,74-2206-44-092-87.51 2 9 00-085 68 79 1 - 9 4 156 55 31 1 7 - 8 1 72 1 8 01 91 1 7 - 8 4 - 0205 99 2207-08 9•>0 32-893 39 63 70 39 1 24 2
Acenap^thene2. 4-Oini'rophenol4-^iTrophenolDiberizofuran2. 4-Dinitrotoluenc2, 6-OiniirorolueneDiethylphihaiaic4-C^loroDhe'-ivl-phenvlethc1-Fluorene4-Niiroaniline4, 6-Diniiro-2-Mer'-ivicieno'N-NllfosodlD^e^v!a'r'lr'e P !4-B'•o^r]ODhenvl•Dhe^v le' t^e'HexachiorobenienePentacfTofo^henoiPhenarithreneAnibraceneD'-n-fiuivlp^i^aiateFfJoraniheneBefi;idinePyreneBuivlbenrv'P^i^aiatp3. 3 -Dic^iloroben^d.ne9enrcKa)Anihracenebis(2-Eihv'^eKvl)PMthaia'pCh'vseneD'-n-Ocivf Phtha'aieSentofbfF'uorarithcneBcn?o<n>?fuoranthen<ienio<a|Pvfanendericw' 2 3 cd^vrcrie)itien;(a hiAnthfacpne
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Sample Number
^ 5liM^>Orgamcs Analysis Data Sheet
(Page 1 »
LAbc'aiorvName Toxicon Laboratories, Inc.
Lab Sample ID No __^9^/^3AT<.p
l/J^-t-^/________Sample Mar ' ix
Case No
QC Repon No .
Contract No ,66-01-7026
Data Release Authorized By ^ / 0^ JA^us^Lyv. Dale Sample Received 03/^3/^^
Vo)ati!fL(:ompouxds
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Date Analyzed
Conc/Dil Factor
Percent Moisture
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/'ug7!^ UB''Kg i<—fC^rdeOnat i
CASNur-iber
74-87.374-83-975-01 .475-00-375-09-26 7 - 6 4 - 175 - ' 5 -07 5 - 3 5 - 475 34-31 5 6 - 6 3 - 567.6f 3w-oe :76 53 37- £5 65e ;3.51 0 8 - 0 5 - 475 27 4
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002023
Cr>-."onrn*ntaf Pf&iecno" Agency, CLP Sample Management OHice.P 0 Box 818 Alexandria V.rg.n.a 22313 703,'557-2490
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
Sample Number
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CASNumber
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002024
Eiw'onme^ia! Protectio'"' AB^-ICV. CU* Sample MBrTgement OHice.P, C SoxSlB. Alexandria Virginia 22313 703/557-24&0
Sample Number
^q^4M<.Organics Analysis Data Sheet
(Page 3»
Pesticide/PCBs
Concentration Low Medium (Circle One)
Dale Extracted/Prepared ______________
Dale Analyzed A/^ -^ 'a-^'^\- (l-^-^^ ?^
Cone ^'Ott Factor
CASNumbar
ug 'lorug 'Kg(Circle Onet
1 9 85 7119-84-6
19-86-88-89 96-44-8
J09-00-21024.57.3959 98 86 0 5 7 - 172 55 972-20-833213-65 972-54-87421 93-41 0 3 1 - 0 7 - 850 29 372-43 553494 70 557 74.98001 35 2^2674 1 1 - 2• 1 1 0 4 28 21 1 1 4 1 - 1 6 - 553469 21 912672 29 61 1 0 9 7 69 1^096 82 5
Alpha-BHCBeia-BHCDelia BHCGamma-BHC (Lmdane)HepiachlorAldrmHep'a^hfor EpoxideEndosulfan 1Dield'-m4,4 -DOEEndnnEndos^ilfan 1 14 ,4 -ODDEnd'-in AldehydeEndosulfa^ Sulfale4.4 -DDTMethoxychlorEndfi^ KsioneChfcrdaneToxap^eneA r o c l O f - 1 0 1 6A r o c i o r - 1 2 2 1
A^oc lo ^ -1232Aroc!o- - -1242Arocfor -1248Aroclor 1254
Arocfo ' - l260
V = VolJ^e of exi'-act injected (ul)
V = Volume of ift-aier extracted Irril)
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ofW. V.
PofH 1
002025
Env>r-:nni(ni»l Proiec: o.-' Agancv CLPSa'^'P1* Vaiaoe-^e-r 0*<.ceP 0 abc-fl iB A)t»t-*d'a Virgin 223 1 3 703 S5724&0
Sample Number^^.6 7 IM^
Organics Analysis Data Sheet(Page 1 »
Labc-aioryName Tcecicon Laboratories, Inc.
Lab Sample ID No —_J9 ^ /^ J A?S
Samc^e Matrix
Case No
QC Report No
ComraciNo i8^01^7026_
Daia Release Authorized By-jy ^J^^^^L^v - s-. Dale Sample Received ^[ ^_3]^
VolalJJfi^ompounds
Concentration / Low/-^ Medium (Circle One)
CASNum^flf
Dale Extracted/Prepared
Dafo Ai-alyyp^
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002026
Cnvir'o^m«nrl Prorciio" Agency CLP Sample Ma-'»a»w"i OMiceP 0 •o>6'6 Afia^O-.t V^g'"- 2 2 3 1 3 703'5572*9C
Organics Analysis Data Sheet(Page 4)
TenUtr/ely Identified Compounds
Sample Number
f-US/^^IS^
CASNufnb«r
1
2 ———————
3A
R
A
7
10
1 1
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161-7
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FractionRT of Scan
Number6»ltm»ted
Conc«nlrat«o"(ug 't or ug 'kg
CO—————[^,
fT~>
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0r-i
Form ] Pan B 4 84
002027
Prot»:T'o- Agency CLP Sample M»^«g«m»oi OM'CBAlc>«r.(lr.« Virc.n.a 22313 703 /5572490
Organics Analysis Data Sheet(Page 3)
Peslicide/PCBs
Concentration Low Medium (Circle One)
Date Eirtracied 'Prepared ——————————————
Date Analyzed ——^ •••" ' < •—./••'•j •'-• •-V-^
Con^Dil Faciw
Sample Numberr 4 ^ / s /-.i ^
CASNumb«r
ug lorug 'Kg(Circle One i
3 1 9 84 63 1 9 85 73 1 9 86058 89 976-44 830900 21024 57-3959 98 860 57 172 55 972 20 63 3 2 1 3 65 972 54 874?i 93-4W31 07-850 29 372.43 553494 70 557 74 9B30' 35 21 2 6 7 4 1 1 21 1 1 0 4 ;e 21 1 1 4 1 1 6 55346<* ;i 91 2 6 7 ? 29 61 1 0 9 7 69 1i 109f B: 5
Alpia BHCBciaBHCDena-B^CGa'^'-na-BHC •:i^3a"eHeoiac'^o''Aldn^Hepta-^io- Eooi'tleEidoSJi'an lDiC'O'."4 4 -DDEEnd'inE1l3cSJ'fa- l!4 4 -DDDEnd-'r- A;3e'-»3e
?ndcsu"a" SJ^ale4 4 - D O T
^e'^oxvc'iic-E'^O'''" Ke'oneC^'o'daneTo»33^e".eA-o:to- 1 0 1 6A'Q-.-Q' 1 2 2 1
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V = Volume of exracr inje;;eff lui)
V^ = Vo'ume o* wrc- e»"a;Ted c-nn
W :: We 3^; o^ sa^o'e exTra^ied (g
V = Votume o< loiat exiraci iul'
cy^CO• -
0r^
Form 1 a s-i
002028
E iwifOfl"1*^!*! P'oiect.oft Ag«^cv CtP Stmpf* M«rrg«m«ni OM*cc.» 0 Bo«Bl8. Af».*^dfn V^o-"'* 2 2 3 1 3 703/557-2490
Organics Analysis Data Sheet(Page 2)
Stmpta Numbar
i^Sf 8 MS^
Semivotatilfl Compounds
Concentration (Tow,) Medium (Circle Onei
Date Exiracied/Prepared
Dale Analyzed .
Cone/Oil Factor
CASfrifTlbar
l iO^/Ofug/Kg(Circle Onet
CASNumber Ong)
6: 75-9lC-e95.26; 63-31 •1.44.495-57.854* .73 -1'C-5-46-71 0 C - 5 1 . 696 53 195 48 739=38 32-9*0€-44.56:- 6<l 767 ^: 195 ?5 37B £9 18£ 75 5'05 6 7 - 965 0; 01 1 1 9 1 l1 2 C S3 2' 5 C 82 19 ' - 2 ^ 3106 47-8B7-68 359 &0 79 t . S 7 - 677 47.488 06 295 95 491 59 788 74 ai3i * 1 - 3206 96 B99 09 2
r^-\iirosodiwei^vfa-"f"ePhenolAn'l'nebn, 2-CMorwhvllEthe'2-CMoroo^enol1 3 Oichtofoben2?ne1 4 D>chlofobeitf*neBe^ryf Alcohol1 2 Dichlorobt";e"eZ-Meihyip^enolb's-2-chiofo'&OD'ODvi!£i"e'4-Meihylphc^oiN-N.iro'SO-Di-n-PfOov'an-.ineHeid;hloroe'naneNifoDen^e-ietsoo^o'one2 Sifop^'e'^oi2 4•D"^^e' l^»lchenol9e-;o'c Acidb'^.' 2-C^lofo?'hol'•-^•1^'ha f te2 4 O.C^IO'OD^?''Ol
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AcenaohThe-ie2. 4-Omiiroohenol4-NuroDheriolOitxi-irofuran2, 4.0ini(toio)uene2 6-OinitroiolueneDieihylohihaiate4-C t^fo^ODhenv^-3>^enylet^^e^Fluorene4-Nitfoaniline4. 6-Dinitro-2-Mel^ylo^eric'N.NitrosodiD^envia^ine ( 1 14-B^o-•nophenv(•D'1env fc•^e'•Hetac^'oro&entenePentachiorooheioiPnena'-'i^reneAni*i^ceneD'-n-BuTvlo'".'iaiaieFluoranneneBenzidinoPyreneBuiviSe'^tvfD^^'Hale3. 3 •D-cr'iorobenJiGineBenJo(a)Aninracenett 'a^-EthvfheKyfiPhihaia'eChryieneDt-n-Octvl PhthalarBento<b|Piuoraninene8enio(ii)Fiuoranfhen<Ban/oialPyreneindp.-'ml 2 3cdiPye"<?Dib*-i/ia hiAninraceneBe'-r^q n oPervipne
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002029
| r^Sf^-^st-Organics Analysis Data Sheet
(Page 1 )
Cafip Nn
QC Report No
31S^
^1
Labo-aiory Name Toflcicon Laboratories, Inc.y^w/^Lab Sample ID NoSample Matrix Contract No 68-01-7026
Date Sample Received ^3 y3 ° ->Daia Release Authorized By <* 04' ^T t ,
Volatile Compounds
Concentration Low Medium (Circle One(Dale Extracted 'Prepared
/ ''DateAna'yzed -i/u^i' / '"••I f A-C //(ti- f^ 'f. a-^t^, 7
^Conc/Dil factor
Percent Moisture.PH
Percent Moisture (Decanted)CASNumber
ug/lorug 'Kg{Circle One)
74-8'. 374-83 975-0 ' -475 00 375-09-267-64-17 5 - 1 5 - 075 35 475 34-315S-60 567-66 3107.06 278 93 371 .55 -656 2 3 - 5108 35-475 27.4
C^'u^o'^ythaneBro"nomcifiaf,e
Vinyl ChfOfiflc
Chio^oeiiflnpMe:^v'enc ChionaeAce'o^eCa'bon Di».iitide1 1 -Dichioffipthene1 'i -DfChiofiiBthaneT r a ^ s - 1 , 2 D.rhiofoetheneChlofofo^^1 2-0'c^'o',iefhanB2-Buta^onB1 1 i •Tri<-hi,irr>BthaneCa^bc^ ^e'ffii n'e'ld^V.n/i Aceiatn
B'o'^&dici!(>t,,^p,hanp
Daia fle[>or-i"g Q^a' '-e's
79-34 5 ' 1 2 2 Tetrac^ioroei^ane78-87 &10061-02 679-01-6124-48 179-00 57 1 - 4 3 2
looei.oi^1 1 0 75 875 2S 2591 78 6108 i0 \1 2 7 1 8 4108 88 3108 90 •'100-1' 4
100-4: 5
To'a ^.p'-'es
1 2 DiCh!orOD''ODane |Trans 1 3-D'chlo''opropeneT''[(;^io''oether-eDib''3'^oc^io''o^e*^ane1 1 2 TnchloroethaneBe^-^e''ec's 1 3 D!C:MofOD''QDene2-CF'>o'oeif-'vlvi"v!ethe''B'o'^'oto'Tn
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002030
Efw-on'-TtMal Pf0lec'lo•• Agency CLP Sample Management Otiice.f» 0 Box BIB Ale«a-a'ia Vt/fiinr 22313 703/557.2490
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
[ Sample Number| _ F ^ S / § ^ 5
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002031
£ri, -sinie-nia1 Pfoie:lion Agency CLP Sample MBriBflemar'iCW'ceP C 8011 9 1 8 A'eMa-<dna Virginit 22313 703'557-24&0
Organics Analysis Data Sheet(Page 3»
Pesticide/PCBs
Concenlratton Low Medium (Circle One)
Date Extracted ''Prepared ___.__________
Dale Analy/ed r '' • • ^~~ ^-^ ^'^^ ?
Conc^'Ott FaciwCASNumber
ug ^ or ug g(Circle One!
3 1 9 - 6 4 - 6319-85-7319-86-856-39 976-A4-8309-00-21024 57-3959-96 860 57 172-55 972-20.83 3 2 1 3 - 6 5 - 972-54-87421 93--11 0 3 1 - 0 7 - 850.29 372.43 5 1
53494 70.557 74 98301 35 2'2674 • 1 2
' 1 1 0 4 28 21 1 1 4 1 16 .553469 2' 912672 29 6U097 69 11 * 0 9 6 82 5
Alpha-B^CBeia-BHCDelia 94CGa~iT-a'6HC (Lmdane1
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002032
Envifoi^fnenisi Protection Agency CLP Sample Mgnanernant OHiceP 0 SiOiBIB Alexandria Virg^ia 22313 703-'557-2490
Organics Analysis Data Sheet(Page^)
Sample Number
FVs/y^s"
Labc'-aiorv^ame Taxicon Laboratories, Inc.
Lab Sample ID No ^^A^________
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Case No
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Contract No 68-01-7026
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r •'i .-c. L., ..i/ 0-'
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ug^orug'Kg i(Circle One) 1
7 4 - 8 - 374-83 97S-0- .475-OC 375-09-267-64-1
r /5-15-075-35-475-34-3156-60-567.66-3107-06-278-&3-37 1 - 5 5 - 656-23.5108-05.47 5 - 2 7 - 4
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79-34 578-87 51006' ")2 679-0^ 61 2 4 . 4 6 179-GC57 1 - 4 3 21006' 31 51 1 0 75 876 26 ;5 9 1 . 7 6 6108 ':• 11 2 7 . 1 6 4108 8» 3108 9: --100 4' 4
100-4; 5
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Organics Anafysi's Data Sheet(Page 2»
SemivolatilConceniradon (Tow.)
Date Extracted/Prepared:
Date Analyzed .
Conc/Dif Factor.
5 Compounds
Medium (Circle One)<-/^ i.^
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002034
Envi'onmenia' ProierliO" Agency CLPSarnpteManaoeTKiiiCWiceP 0 Bo«8l8 Alanano^a Virgm,< 22313 703'55?249C
Organics Analysis Data Sheet(Page 4)
Sample Number
M ^ \
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CASNunnb«r
1
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002035
E" •f/ifonfnen\6< Proi»cro" Agency CLP Sample Manage-nani QMiccP 0 Box 8 1 6 A)a««'>dfia. Virgin 2 2 3 1 3 703^557-2490
Sample Number
^f MB{
Organics Analysis Data Sheet(Page 1 »
TcMicon laboratories, I1^- case NoLfl&o''alorv Name
Las Sample ID No
Sample Matrix lA^-t- ^ /
Data Release Authorized By ^y S ''',. . '
QC Repon No „_
Contract No 18-01-7026
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Votaijifi^ompoundsConcentration , Low/ Medium (Circle One)
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Conc/Dit Factor
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t.'.? ^^^S
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7d.67-374.33-97 5 - 0 1 - 475-00-375-09 7.67-64- !7 5 - t 5 - 075 35-<175-3^ 31 5 6 - 5 3 567-66 310- ' - :3-576 93 37 1 - 5 5 656 23 5106 35 d75 27.4 T
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'£ftvifonw/tf»l PiotpCT.on AflB^cv, Ci-P S^mpit Ma'Tgamem QMicey 0 Boxfilfi. Al«>*^(lri< Virg'ni* 2 Z 3 1 3 703 /557•24&0
Organics Analysis Data Sheet(Page 2)
Sampla Nurnbar
,M B |
SernivolatUe CompoundsConcen(ra;ion ( L o w . ) Medium fCirde One}
'——--' , -7 -. ( ^L CDale Extracted/Prepared, • ^3 ' o J
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'ug^Arug/KgCASNi-rnbaf .ircle One'6; 75-910*? 95-26; S3.31 ^ *-A4-495 £7.65 - 1 - 7 3 - 1W 46-710C 5 1 . 695 S3-195 •*9 739=38-32-910€ A4-562 - -64 .767 -t; 199 3^ 378 5- 186 75 5-.05 c? 966 ?; 0m 3 1 - 1120 93 21 2 0 S: 19 1 - 2 ; 3(06 * "-887 68 359 SO 791 5? 677 47 488 06 795 9S ^91 68 788 74 4< 3 ' n 3?0fi 96 »99 09 ;
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E"» •o"-neni*' Protect.o'. Agei^cv CL.PSl^pllMa'vge'ndtO^'c*P C Box8l8 Alexi-^on. Vir^o.i 22313 703'667 2490
Sample Number^1
Organics Analysis Data Sheet(Page 3)
Pesticide/PCBt
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Con^OtI Factw
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CASNumber
>r ug'KgJrcta On<)
3 1 9 84-6319-65 73 1 9 8 6 - 85889 976-4^-8309-00-21 0 2 4 - 5 7 - 3959 98 66057.1
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US. ENVIRONMENTAL PROITCnON AGENCY HW Sample Monageipeni'POBoxSiaAJ-^^imVu-^ii^.'1!^ 703 W ITS bb? 2-190 "
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002039
n0| U S, ENVIRONMENTAL PROTCCTION AGENCY HWlSompleM ragemeni O&oe ~M^ M^K
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Semiyolatile Compounds
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Organics Analysis Data Sheet(Page 3)
Scrnple Number
I 4J^f
Concenirai'c
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Date Analy2(Conc^DilFa<
CASNumber
31984 .6319-85-73 1 9 86 85889 976-A4-830900 21024 .57-3S599B 6>0 57.1
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Organics Analysis Data Sheet(Page 4)
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Organics Analysis Data Sheet(Page 1 »
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002049
Organics Analysis Data Sheet(Page 2)
Semivotatile Compounds
Concentratton [ Low.) Medium (Circle One)
Dale Extracted/Prepared c^^^^
Dale Analyzed .
Conc/Dil Factor
/ug/f^rug/KgCASNumber '—fOccle One]6: 75.91 0 8 - 9 5 - 262 .53 -3m.44-495-57-8541 -73 .1106-46-71 0 0 - 5 1 - 69 5 - 5 0 - 195-48 7'39538 3 2 - 9106-4,4.56 2 1 - 6 A 75 7 . 7 2 - 195 95-376 59 189 75 51 0 5 . 6 7 - 965 65.01 n 91 11 2 0 83 21 2 0 - B 2 ••9 ^ . 2 0 2106-47 B87-68 359 &0 791 57 677 47 488 06 ?'9^ 95 491 58 785 74 41 3 ' 1 1 3?08 ft99 09 /
N-Vifosodi'T'etnytarninePhenolAnilinebiSl-2-C'^croeihvlieiher^•Chlorophenol1 . 3-OicNofober.;?ne1 . 4-0'chtofoben»eneBenrvt Alcohol1 S-O-chtorobpn/p-nR2-Meihyfohenolbi >'2 chrOrofsop'opvOEl^'4-Veihvfoheno:N-^'fc^o-D'-n-f ' foDvia'T'lneHetar.ht^'oei^fl'-iB^ irottpn/e^s'soD^riro^e
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CASNumber
83-32-95 1 - 2 8 - 5100-02-7132-64-91 2 1 - 1 4 - 2606-20-264-66-27005-72-386-73-7100.01-6534-52-166-30-61 0 1 - 5 5 - 31 1 8 - 7 4 - 187 -86-585-01 -81 2 0 - 1 2 - 784.74-2206-44-092-87-5123-00-085-68- '*9 1 - 9 4 - 156 55 31 1 7 . 8 1 - 72 1 8 - 0 1 - 91 1 7 - 8 4 - 0205 99 2207-08 950 32-81 9 3 39 553 70 3' 9 1 24 2
AcenaDhthene2, 4-Oi'tilroE: icnoi4-NnrophenolDibanzo^uran2, 4-Di"itroio(uene2, C-Oi'TfoiolueneDiethylphthatate4-C l^lo^ODhe^^Y!-phenv^ethe^Fluorene4-Nilroaftihne4. 6-D[nitro-2-Meinylphen.->lN-Nl^rosodlo^ef'v^amlne ( 1 )4-BromoD^'e^lv(-P^cn^'f6the'Hexachlofobar.tenePeniachlorooheno'Prie^anthreneAnthraceneDi-n-BuTvfphthaiale^fuoraniheneBenrid'nePyrerieBulvlbenrvfDhthaiaic3 3 -O'chiofobcnJ'id'ne9en^o(a)Anihraccn«*b $(2-Ethvlhe"vf|PhlhalaicChrvscneD.-n-Ocivf PhihaialeBento<[)^!uorarnheneSenrtMktFiLioranthariC8en(o<alPyf8n«lr.deno<1, 2 3 cdlPv^"^i^iben-na hiAnthfacc"eBen/CMg h iiPervfene
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002050
Organics Analyst's Data Sheet(P&ge 3»
Pesticide/PCBs
Conceniralion /Low) Medium (Circle One)
Dale Exiraded/'Prepared - ^A 9 /S^
Dai&Anafyzed 4/^/W
Cone i'Factor f c1
CA5Number
^B^ug'Ks:ircle One)
3 1 9 - 8 4 - 63 1 9 - B 5 - 7319-86-858-89-976-44-8309 00-21024-57.3959.96-&60.57-172-55-972 20-83 3 2 1 3 - 6 5 - 972-54-87421 93-41 0 3 1 - 0 7 - 850 2 9 372.43-553494 70 557-74 98001 35 21 2 6 7 4 . 1 1 - 2' 1 1 0 4 28 2I 1 1 4 * 1 6 - 553469 2 1 - 9'2672 25 6H097 69 11 1 0 9 6 82 5
Alpha.BHCBeia-BHCDelia-BUCGa-ima-BMC (L'nda''elHepiachlorAidnn
MeDtac^lo' EpoxideEndosL;lfan lD'e'd''^4 4 -DDEEndnnE"d;SJlfan 1 14. 4 .ODDE^d^r AldehydeEr*d;s J' far- S..''*aie4 4 .DDTMei^oxychlorEnd'i" Ke;o^eChlo'daneTona^^eneA r O C i O f - 1 0 1 6
A r o c i o ' - 1 2 2 1Arodor -1232A'-oc io ' -1242Afocio ' -1248Afoc io r -1254Aroc io ' -1260
G <?SH
ff-^fuft.ffSi{ J
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V =' Vo'uT-ie of Sxi fact injecied (ul)
V» = VoiuTie o^ wsier exiracied (ml)
W- = We.ghi o^ »amisle exiracied {gt
V. « Vo'ume of twe'' exfact (Jl)
Of W. V. V.
002051
USEP^ Case Number _3^Ji
Category
USEP^ Region
Numbers
Data Report
Data Sunrmary Report
Laboratory DataLog BooksBench SheetsRaw DataCalculationsCorrections
Sample Loggin RecordsSarftple Traffic RecordsToKicon Sam[^le RecordsAl-rbill RecordsCastody RecordsSampt.e Tags
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10012001300140015001
6001
70017101720173017401
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002052
Organics Analysis Data Sheet(Page 4»
Tentatively Identified Compounds
CASNumber
1
2 ........ .....
3
A
5fi7
ft
Q
10
1 1 . -'-"' / *-
1 7
in
14 ..
1 R
1f i
1 7
1 a1 S ....
2021 ......
22
21 .
34 .........
25 - . .?fi
* / , i
2820
30————^1
Compound Name
^, (,r!M-^ ("^ ^^^v^/uk l<^^-f^•
'
.. --. ^ /. ti < 1 1 . . 1 , /i
Fraction
s,«^-./J
BT or ScanNumber
[ ' ' ' ' f ? .
EstimatedGtincentration
^ug^of ug 'kg
- " ~ " " " " — • " "• "——
-—————-———
—————————^
J.
^000^t0....... ,. ,„,
1 T - -——— . ^ ^ - '
Fof^i 1 Pari B
002053
^' 1985
USBPAContract r^^^o?ra^ ^^torySMO
• ot Box 8_[D
^^ ^ .3
USRPAENSLP. C. Bcoc 15027r^s Vegas, w 89114Att^: Data Audit
Staff
^PA R ion vi^^oniitentai .^^sion ^vices
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-' ^^se No. 39g,closed t-^ Repol't No. 300,984 ^ece^l^^ytica, ., „. 84S°^^T ,, , ' ; " "" -•
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F 45^3P 4594 Low wclte^^ 4600 Low ter
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002054
002055
002056
002057
