•- - - -""'- > •••

First Year Course in Chemical EnCineeringSemester I

Candidates will be examined in the subject as indicated inthe following tables :

Papers

TotalMarks

PeriodicTeatHarks

No.of Examinationpapera Hra Marks

Subject---------------------------------------------------------------------S"No,

-------------------------------------------------------------------CH' El""lrical En!:ineerin," 1 3 eo 10 100101 • Electronics

CHE Inorganic Chemistry 1 3 eo 10 100102

,"E Physics 1 3 eo 10 100103

CHe PhYsical Chemistry_I 1 eo 10 100I 101

CHe Mechanical Engineering_I 1 2 ,30 20 00105

t-.......,~HE EngineerLnll Graphics 1 , 60 10 100! 106

-----------------------------------, , 330 ", 500" -----------------------------------Prseticals and Orals

Marks for TotalClass work

603030

ExaminationMrs Marks

----------------------------------------------------------------------------------------------------------------------------------------CHEI17- Physics 6CHEI18- Inorganic Chemistry 3CHEl19- Electrical EnCineerin~ 3

& Electronics Laboratory

•

---------------------------------Total Marks---------------------------------750

1

1 _. '---- --'=-'-'~ . ._-~--'.---'-' - - -'

•

Alternator: Working principle and regulation.

reGulation

of generatorscontrol, and

working, t~'pesHotora speed

motors Working principles of synchronous Bndmotora, their characteristics and starting method6.h,p. meter. Choice of motors for different duties.

D.C. generators: Principle ofand their characteristics, D.C.starting methods.

Single phs.se transformer: Principle of warlllng.efficiency. Three phase and instrument transformers.

A.C.inductionPractical

CAE-lOt: Electrical Engineering and Electronics:Three phase. system of e.m.fs. snd currents. Star and deltaconnections. Three phase power measurements.

ConVersion of A.C. to D.C. - various methods. Used and theirspecific applications.

Electrical hearing methods.Electrical Tariff and p.f.improvement.

I

•Illustrations for the above named applications to be givenwith the help of block diagrams only,

Characteristics of tranaistors and transistor amplifier.Multistage amplifiers, Cathode Ray OscillOscope.Electronic timing and control devices.Introduction to integrated circuits.

Reference Book

Electrical Technology - E. Hughes (E.L.B. Publication JBasic Electrical Enllineerlng - Fitzerald and HiggnhothamApplied Electricity - A.W, Hisrt (Blackie and Sons)Electrical Technology - H. Cotton, 7th Edition .Fundalllentaisof Electrical Engineering Vol. I A IIIS.D.Bhide H.N.Navale)

Electronics Use of electronic valves as rectifier,detector, amplifier and oscillator. Two and three stageamplifiera. Digital circuits, operational amplifier.Photoelectric devicas and their applications. Transducers.

L2 •5.••5.

CHE-I02: Inorganic Chemistry:

Development of the nuclear theory of the atom. Bohr's theoryof the atomic epectra of hydrogen. De Broglie's particle waveduality principle. Heisenberg's uncertainty principle. TheSchrodinger equation. Qualitative account of the solution or theSchrodinger equation for the hydrogen atom. The quantum numbers,atomio orbitals, electronic configuration of the elements.

2

---~._--_..-

Reference Book

CHE-I03: Physics:

---- - -:-- -'--- - .•.. ' ..

Diffraction

InterferenceFabry-Perot

concentration

Light: Interference-Michelson interferometer,involving multiple reflections in thin .films,interferometer, Measurement of refractive index andof soiution.

Diffraction-Fresnel, Fraunhoffer diffraction.grating, Resolving power of optical instruments.

Hest: Conduction-Conductivity of Metals, insulators, liquidsand gases, Electronic theory of conductivity, Radiation-Blackbod}'radiation, Kirchoff's lsw, Stefan-Bolt:::mannlaw, Wien'g law,Planck'••law.

,The long form of the periodic table, types of elements,

periodic trends in atomic and ionic radii, inni'.Hilion potential,electronic affinities, electronegativities, oxidation states,ma~netic susceptibilities of atoma and ions.

Ionic, covalent and coordinate bonds, bond properties, bondpolarity, The ionic model, lattice energy, appLications oflattice energetics. Bonding in metals, The covalent bond, thevalence bond and molecular-orbital theories of the covalent bond,hybridization and resonance. The valence shell electron pairrepulsion theory. Hydrogen bond, Van del' Wall's forces.

Temperature measurement and control-Resistance thermometer,thermo e.m.f., high and low temperature measurement, thermistors.Application of thermostatic and other temperature controldevices.

2. Introduction to valency theory: Jean Worall and I.J.Worall, Macdonald technical and scientific; London

1. Concise inorganic chemistry: J.D. Lee, D. Van Nostrand Co.,2nd Edition

General sspect~ of the chemistry of the non-transitionelements including the study of one representative element ofeach group. Study of SOlDeindustrially important compounds of thenon~transition metals. Oxides and oxyacids of nitrogen,phosphorous, sulphur and halogens. Hydrogen and hydrides. Noblegases and their compounds.

,

Electricity, Magnetism: Laws of electromaJ;:neticinduction,self and mutual induction inductiVe circuit. Time-varYingmagnetic field, Magnetization CUrve Hysteresis, Magneticcircui~, leakage and reluctance. Motio~ of char~ed particles inelectr~c and mag~etic fields, Mullikan's experiment, Thomaon's;7periment, Capac~ty. energy in condenser, capacitation circuit~nusoidal ".m.f., R.M.S. value: graphical representation'current and power of RC and RCL cirCuit. '

Sound: Ultrasonic-Production,applications. detection, velocity nnd

CHE-I01 : Physical Chemistry :

Theories of reaction rates lcollision, modified collision,Lindmann's hypothesis, activated complex}.

H2

of

temperature,order and

reaction,

Reference Book

1

brief details and applications

•

Rate of reaction, Effect ofon rate of reaction,

of deter~ination of order oforder reaction.

reactions.-) 2HCI)

Complex reactions, Side reaction, Reversible reaction,consecutive reaction, Rate equation for complex reaction,catal~tical reactions, Homogeneous and heterogeneous catalyticreact~on, Acid, base reactions, Enzyme reactions Photochemicalreact~ons, Laws of photochemsitry, Chain reaction~, free radicalreact~ons, Mechanism of [2NO tF -) 2NO F, CI t H 2HCI)

2 2 2 2reactions, Mechanism of (2ND t F -) 2NDF, CI +

, 2reactions.

Chemical Kinetics:concentration etc.Illolecularity, MethodsPseudo molecular, Zero

Element ot Physical Chemistry: Glasston & Lewis.Text~ook of Physical Chemistry : A Pindaly.Phys~cal Chemistry: A.J. Mee.Principsles of Physical Chemistry : Prutton, Maron.

CHE-I05 : Mechanical Engineering - I:

1-2.3.1.

Basic principles,followinC:

Relationship between molecular structure and properties auchas surface tension, viscosity, refractivity, optical activity anddipole mOlllents.

Gaseous State: Real gases,-Deviation from idealbehaviour-Reduced equation of atate-Thermal properties of ~asesspecific heat of gsses~oritical phenomenon and criticalconstants-Principle of continuity of states-liquification of~ases.

Liquid State' Nature of intermolecular forces-Vapourpressure of liquid, Effect of temperature, Vapour pressure ofsolutiona, Roult's law of lowering of vapour pressure, Boilincpoint elevation and free zinC point depresaion, Idealsolutions, solubility, Nernst distribution law, Association anddissociation in solution, chemical equilibria in ideal and realsolution, osmosis. Determination of molecular weicht based oncolli~ative properties.

Lasers' Principles and applications He-Ne and Ruby lasers.Free electron theory and bond theory and their electricalproperties, Semiconductors and types, diodes, transistors.

,Modern Physics: Photoelectric emission, use of photocell,

photo~ultiplier, photoconductivity, Thermionic emission,Richardson equation, Contact potential, coated cathodes, Vacuumtubes, Cathode ray tubes, thyratorons.

_.Processes and tools-Patten making. sand moulding and castine. diecasting, centrifugal castinll. Proces('ling of plastics. Rolling.forging. drawing, stampingand punching processes. Metalcuttine hand tools, drille, hamlller, taps and dies. Lathe,drilling, planing, shaping and milling machines. Machining ofplastics. Grinding machine •• and grindinG wheels, lappig, honinsand super!!n!"h!n;. RivettinC', soldering, brazinr;:, welding-gasand electric, and metsl spraying. Welding of ~ast!ca.

eRE-106 : Engineering Graphics - 1Solid Geometry Projectione of solids like prism, pyramids,

cylinders and cones, Sections of solids. Developments of solida.Interpenetration of simple solids including cone and cylinder.Isowetric scales and projection ••.

Machine dr.••.wing-Orthographic projections, First Angle andThird Angle methods of projection ••, Conventions in dimensioningand in sections, Forms and proportions of ScreW threads, bolts,nuts, locking device", for nuts, studs, set-screws, hanllers andbrackets. Free hand sketches of the above parts,

Reference Book

Electricity and Magnetism: Hyateresis B-Hof Magnetic susceptibility-Quinck' M th d curve, MeasurementSensitivity and Reduction fa'. 'ds e ? Galvanometer'.0 i ~~or an COmparl.son of . i~" c rcuit. Mechanical equivalent f h • J 1 capaCl.t es.o ea~- -E ectrical Method.

1. Engineering Drawings, Voi. I - N.D. Bhatt.2. Principles of Solid Geometry - Gunda and Arvikar3. Engineering Drawing French.1. Engineering Drawinll Zozora.5. Engineering Drawing Luzzader.

Methods.

Radiation-Metallic

Method.Elllmissivity of

Tens ion-Jaeger' s

of Diode, Triode, CrystalThermister, Experiments on

Matter, SurfaceMeasurement.

Interference using Bi-Prism. Newton', • "., r r ,,'-n••8. Cornu's'-ner erence or determination of Young's Modulus.Gratings, Spectrometer-Dispersive power of .at straight edge. Particle size Illeasureme~~,-smb:of light. •

CHE-117 : Physics Laboratory:

Heatl Thermal conductivity Lee'sDetermination of Stefan's constantsurface.

Light:Method ofDiffractionDiffractiondiffraction

. Modern Physics, Characteristicsdl.ode and Transistors. Resistance ofHe-He laser.

Properties ofUlt~asonic velocity

- ..••...--•..------------- ------------------"--_.

Fe-Ni alloy.

eHE-IIS : Inorcanic Chemistry Laboratory:Volumetric analysi'" Preparation and standardization of

volumetric solutions. Acid base reactions, titrationa of amixture ot (al hydrochloric and acetic acid (b) sulphuric andphosphoric acid (0) Carbonate and bicarbonate. Oxidationreduction titrationa involvin~ pemancanate dichromate, ceriesulphate, iodine llriiodidel potassium bromate. Precipitationtitration: Mohr'" and Volhard'" titration". Compleximetrictitrationa involvinC EDTA: Determination of water hardness.Determination of Maneanes •• in pyrolusite. Oravimetrlc anaiysisGravimetric determination of Fe, Ni, SO and Cl. Analysis of a,

Reference Book

Willard, Furman,

Vocel.

A Short Course in Qualitative AnalysisBeacon.Practical Inoranic Chemistry2.

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,~'

0' , !•, ,<m ",g!~ T.~ i" "'~>5>0 ..,z

itl"- ..,,...,

shunt

amplifier.Study of

Transiator

triode. Triode lISRectifier circuits.oscillators and

lead teats on transformer,ahunt generator.

A.

CHE-1l9 , Electrical and Electronice LaboratoryElectrical EnCineerinc Laboratories ,

Study of 3 phase circuits,motor, induction motor and D.C.

,

B. Electronics Laboratory.

Characteristics of diode andTransducer!!. Photoelectric tubes.C.R.O. and ita Uaes. Stud fcharacteristics. y 0

- 0------:'::"

---------------------------------------------------------------

in

<50

TotalMarks

'60

100

180

PeriodicTestMarks

as indic"ted

'"

II

Examination Marks for TotalBra Marks Class work

---------------------------------

Papers

examined in the subjects

Total Marks

Subjects

Candidat~s will befollowing tables

---------------------------------

Practical ••and Orals-----------------------------------

, 3 60 10 '60CHE-20l- Applied Mechanics

Mathematicl'l-I 1 3 60 10 100CHE-202-Organic Ch~lIIistry-I 1 3 60 10 100CBE-203-

CHE-201- M~chanical Engineerinll- 1 3 60 10 100u.60CHE-205- Computer Programming 1 2 30 20

• applications •

----------------------------------------------------------------CHE-216- Tutorials on Computer 3 30 20 "ProgrammingCHE-217- Physical &; Organic 6 60 10 100Chemistry. LaboratoryCHE-218- Engineerin!,:Laboratory , 60 10 100• workshop Practice

--------------------------------------------------------------------- No.of ExaminationSr. Subject papers Brs MarksNo. --------------------------------------------------------------------

,<.No.

,

Reference Book

CHE-202 : Hathematics - I :

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of

second

mass and

of

Conditions

and journal friction).

-.'"-------

of general equationsReductionequations.

Kinematics of particles and rigid bodies.Kinetics of particles and rigid bodies Force,acceleration.Kinetics of particl ••s and rigid bodies Work and Energy.Kinetics of particles and rigid bodies Impulse andmomentulll.

.,",o ,d'.,

Dynamics

(b) Cslculus.

(it) Geometrydegree and polar

1. Methods of virtual work.Friction IExcluding rolling pivot5.

1. Applied Mechanics and Strength of Materials I.B.Prasad.2. A text Book of Applied Mechanics: I.B.Prasad.3. Collection of Problems in Theoretic .••.l Mechanics : Meshersky1. Engineering Mechanics: Higdon and Stilea.

(i) Algebra: Complex numbers, De Hoivere's Theorem, hyperbolicfunctions, separation of a complex number into real and imaginaryparts.

(a) Algebra and Geometry.

,.,.

Applied Mechanicsforces. Equivalent

1 Coplanar "tatilltica.e~uilibrium,Graphic b .Conditions of "quill r~um.

f Equivalent systems.Space orc"S,

for determine hearns,Reactions f 1 joined plane true"S .Forces in members 0 .F n in joined plane true ••s.R ctions for deterrnLne PF~~ces in cables and simple mechanisms.Centroid and centre of gravity .

CKE-201----~------"

8

Integral Calculus: Simple reduction formulae for integration.Beta and Ga&~a functions. Determination of area and length ofcruves. Double and triple integrationll and application to findmoment of inertIa and centre of gravity.

Differential Calculus: Curvature. Higherof functions and Leibnitz's rule for thetheorem. Taylor and MaClaurin's theorems,

order differentiationderivative. Mean valueIndeterminate forms.

t 2Alkyl halides SN and SN reactions-effects of temperature

reactants, solvents, elc., Elimination reactiolls-El and E2mechanism. Say-tzarf and Hofmann rules, GrignaI'd reagents andtheir general reactions.

....,--~--.

stereochemistry ofWalden inversion,conformations ofof cycloalkanee,

Stereochemiatry : Absolute configuration,compounds having two asymmetric carbon atoma,Separation of enantiomers, diastereomers,ethane, n-butane, cyclohexane, structuresAsymmetric synthesis.

Electronic theory : Types of bond. hybridization, bo:~O• intermediates-formation and structurefission, types • , • ,h't., .nd

h i ion carbanion and free radicals, eL:c~ro •car on um , t f aC1ds and baaes,nucleophiles, types of re"c:tion, coneep 0 Addition reactionsAlkanes' Geometrical iaomer1sm, E-Z isomers,of alkenes-Harkownikoff'a rule, ozonolysis, types of diene" andtheir characteristic reactions, Diels-tllder reaction,Polyllleri" ••t ion.

Carboxylic acids' Strenl:th of carboxylic acids, H-bondinl:,Mechanism of esterification and hydrolysis, Tautomerism,Preparation of ethyl acetoacetic ester and diethyl malonate,synthesis through acetoscetic ester and diethyl malonate.

Aminea : Basicity of a.ines.

Reactions and Rearran~ements : Aldol reaction, Cannizzaroreaction, Stobbe condenaation, Dareen glycidic ester synthesis,Perkin reaction, Reformatsky reaction, Michael Addition.Dieckmann condensation, Pinacol-plnocolone rearrangement,Benzil-benzilic acid rearrangement, Beckmann rearrangement,{synthetic applicationa and mechanisms of these reactionsl.

Carbohydrstes : Structures of glucose, fructose, starch andcellulose reactions and interconversions of glucose and fructoae,Oxidation snd reduction of glucose.

Oxidation and Reduction : Mechanisms and applications ofoxidizing and reducing agents like, dillllolvingmetal reductionscatalytic hydrogenations. Meer~in-Ponndorf-Verley reduction.NaBR ,LiAla, Sodium dicromate, hydrogen peroxide, catalytic

1 ,oxidation, 01'0 peracids (Baeyer villager oxidation), Oppenser

1oxidation,

Reference Book1. Text book of Organic Chemistry: Horrison & Boyd2. Orcanic Chemistry Vol. II : I.L.Flnar

CHE-204 : Mechanical Engineerinc -II:

Introduction to the laws of thermodynamics, entropy conceptas a consequence cf the second law of thermodynamics, Study ofair cycles. Otto, Diesel, semi-Diesel, and Brayton cycle.Representation of these on P.V. and T.S. diagrams. Calculationsof ~ork and po~er.

9

z"I

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"I~•> "• ;z• •> •••••c. ,,~, ,~ ,,"",~•~ I," ""'l~>5 ' ,>0 "Iz

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••

stationary

Rererence Book

CHE-205 , Co.puter PrograBDing and Applications.

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highpoweratealll

cells,power

CHE-216 :Tutorials On Computer Prograa.iing:-~hia will be based on programming excercises Carried out by

the candidate based On the ayllabus.

1. Basic Engineering Thermodynamics: T. Roy Chaudhari2. TherillalEngineering (S,l.Units) , P,L. Ballaney3. Engineering Thermodynamics, Gupta & Prakash

Selected examples from Chemical Engineering.

Bearings to withstand end thrust. Shafts and couplings.

History and organisation of Computers problems solving onComputer, Algorithms and flow charts. Introduction to numericalmethods, Interpolation and extrapolation solution ofdifferential equations partial differential equationa, Elamentsof BASIC/FORTRAN/PASCAL.

Control and input - output statements subscripted variables,Punctions and Subroutines Writing simple Computer programs inBASIC/FORTRAN,

Study of bearings: (Journal, ball and roller bearings),sturfing box, keys and bolts, mechanical seals.

Solar, wind and tidal ener~y. Applications and allocations.

Transmissions: Types of drives, group and indivual drives,their merita and demerita. Belta, chain and gear drives.

Calculations of pulley sizes and gear trains for speedreduction.

Measurements oC surCace tension by drop wei~ht methodand torsion balance method-Molecular weight determination of

----------._-,

CHE-217 : Physical and Organic Chemistry LaboratoryA. Phyaical Chemistry :

Elementry study of other types of power plants,and mobile plants.

Direct energy conversion devices such ss fuelthermoelectric generation and MHD : their principles andlimitations.

Steam EnCineerinc, Study of the properties of ste~m,and low pressure boilers. Steam power plants an fcalculationa usin~ steam tables and Mollier ChB:t, types 0of tUrbines. Cogeneration of steam and electric1ty.

~---- ---_. ~~~-

polymer by viscosity measurement a-Lowering of freezing point andelevation of boiling point method-Heat of neutralization andsolution-Verification of Ostwsld's dilution law by conductivitymeasurements-specific rotation of Cane sugar by polarity.Percentage composition of mixture by refractive indexmeaeurements. Measurement of diffusivity in :as phase\acetone-air) ,

Hydrolysis of methyl acetate-Relative strength of twoacids-Rate constant with varying cone, of ester-Order of reactionbetween (K S +KI){KBrO +K!l -Saponification of ehtyl acetate in

2 2 3presence of base-Adsorption of acid by charcosl-Partitioncoefficient of I CCI and Benzoic acid in Benzene Determination

2 1of energy of activation and other thermodynamic functions.

B. Organic Chemistry

Identifications of an organic compound throughelemental analysis, group detection, physical constant(m,p./b.p.) and derivatisation. Estimations of selected organiccompounds like, aniline/phenol, formaldehyde/acetone, glucose,glycerol, Neutral equivalents of acids and, bases, Sap value ofan oil

CHE-218 : EnUineeriD4 Laboratory and Workshop Practice :

A. Engineering Laboratory :

(a) Study of petrol and Diesel en~ines. Trial on Diesel engine.Study of types of drives,

TeBt DemonBtration: \i) Tension Te:!'.tlii) HardnesB Teat and/orImpsct TeBt.

Power plant visit.

B. Workshop:

Practice in taper metal turning. Practice in Boldering, brazingand welding. use of dies for cutting pipe-threads. Joining andfitting of pipes, Visit to workshops,

11

....~••... ,.,,-,,

-------------~------------------------------------------------------

Practical" and Orals

•

z ;)0•~z ...,•>z>• ~>•z~ ,'"-~ ••••.~• •••c0>0 •••z

itI.1-' .'"'

i.

100100100

'00

Harks for TotalClass work

,as indicated

ENGINEERING

605060

subjects

soo

----------

6,,

ExaminationMrs Marks

------------------------------------------------------------------

----------~--TotalMarks

Papers

COURSE IN CHEKICALSemester I

examln..,d in the

•

be

Total Marks

--,_. ~ "1.' _

Subjects

Candidates willfollowing table.

SECOND yEl\ll

, 60 10 100Mathematics 12 iCHE-301-

Chemistry-II 1 , 60 10 100CME-302-Orllanic

Physical Chemistry- I r 1 , 60 '10 100CHE-303-

CME-301-Structural Mechanics 1 , 60 10 100CHE-305- Process Calculation 1 ~.3 60 10 100----~------------------------'00 200 500--------------------------------------------------------------------------------------------------'e,No,

--------------------------------------------------------------------CHE-316_Organic ChemistryCHE-317_Physical ChemiatryCHE-3l8_ Structural Mechanics

"& --~ -- ' .•

12

'.

CHE-301 : Mathematics - II :

~HE-302 : Organic CheRietry :

Partial differentiation: Function of two or more variableunits. Differentiation under the integral sign.

vector,s Dot andtriple products.three di~ensiona.

Integration: Differentiation of an integral with variableunits. !)ifferentiat.ionunder the int"llrsl....-sign.,.

Vectors: Scalars and Vectors ~dclitionofcross product of vectors. Scalar and vectorSimple application of vectors to geo~etry ofIolatrices. - ~

Oifferential Equations: Ordinary differential equations ofthe first order. Equations of the first order and higher degreesLinear differential equations of with constant coefficients.Homogeneous linear differential equations, Simultaneousequations. Curve fitting.

Halobenzenes: Nitration reaction, reagents and conditioneused, uses of nitrocompounds.

Aromaticity and aromatic Character. Properties of aromaticcompounds, Huckel's rule, Resonance, resonance energy, structureof benzene and benzenoids, non-benezenoid aromatic compounds.

Orienting influence of different substituents-ohangedistribution method and stability of the intermediate method.Mechanism of aromatic electrophilic substitution reaction.Friedel-Crafts alkylation and acyiation, fires rearrangementFormulation reactions. Gattermann-koch, Gattermann, Vilsmeier,Reimer tiemann.

Aromatic amines : Introduction of-NH group in an aromatic2

rin~, basicity correlations, Diazotisation or aromatic primaryamines, Reactions of aryl diazonium aalts-Sandmeyer, Gettermann,Azocouplini reaction, Ullmsnn reaction, reduction, deaminationreaction, Azo dyes, benzidine rearrangement.

z. ~o.~-,z "'"< ,>• ">• !"i> ~j'••• ,> ;J,0 •• ,~.

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!.til_. ,.,

ManuichBlanks chlromethylation reaction, Kolbe reaction,reaction, Claisen rearran~em.nt.

,

13

: Sulphonation reaction-mechanismsnd thermodynamic control of aa blockinc Croup, as solubilising

Phenols: Acidity of phenols, preparations of phenols,condensation polymerization and phenol-formaldehyde resins.Heterocyclic compounds: Nomenclature, structure, aromaticity,preparation and reactions of pyridine, pyrrole, furan andthiophene. Preparations of quinoline and isoquinoline.Spectroscopy. Ultraviolet spectroscopy. Basic principleschromphore-auxo-chrame concept, effect of conjugation and'solventon peak position, applications.

Aromatic sulphonic acidsand reagents used, Kineticreaction, uaes SO H group as

3acidic group and its conversion to-OH group.

Laws of crystallography. X-ray diffraction by crystals,Bragg's eguation, Determination of crystal structure (NaCL, KCI),Defects in crystals, space groups, Brsvais Lattices, Applicationof group theory, Crystal structure of metale and semi-conductors.

Two component system, solid-liquid system (Eutectic.compound solid solution formation), liquid-liquid ,.yatem(miscible and imJlliaciblej,solvent extraction, fractionaldistillation, Distillation (azeotrope and zeotropic systems).

Thermodynamics: First law of thermodynamics, application tocompression and expansion of gases. Second law of thermodynamicsConcept of entropy. Third law of thermodynamics. Entropy changein compression expansion, chemical reactions and mixing.

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rule,

shift,

Boltzmanenergy

definition)(water and

nndsystem

Simple three co~ponentslid-liquid and liquid-

(,.tatementoomponent

Basic principles, selectiongroups, applications.

ruleto one

Oibb's phase rule,of phase rule to

spectroscopy.of funct.ional

rule Pha,.eof phase rule

Solid State l Crystalline state.

Infraredidentification

Reference Book

NMR spectroscopy Basic principles, chemicalspin-spin splittin~, anisotropic affects, applications.

1. Basic Engineering Thermodynamics' T. Roy Chaudhari2. Thermal Engineering (S.I.Units) : P.L. Ballaney3. Engineering Thermodynamics; Gupta & Prakash

CHE-303 : Physical Cheaistry - II l

Pha,.eApplicationsulphur).

Derivation ofSystem, Applicationliquid systems.

Introduction to statistical thermodynamics, Maxwelldistribution, partition functions-Entropy and freefunction. Sackur-Tetrode equation.

Concept of free energy, Criterion for spontaneity ofreaction, Gibbs-Helmholtz equation. Partial molal properties.Chemical potential, concept of activity and fugacity. Criterionfor phase equilibrium, Gibbs,-Duhem equation.

Equilibrium in homogeneous system: Homogeneous equilibria.Law of mass action Equilibrium in gaseous system, Equilibrium inliquid system. Effect of addition one of the products onequilibrium, Effect of temperature, Effect of pressure, LeChatelier's principle, Application to practical system.

VsriouB' types of stress and strains. Relation betweenelastic constant.sIntroduction to temperature stress. Problems onsimple and composite sections Concept of shear stress,distribution.

Short snd long columns snd struts. Standard cases with axiallosd. Euler's snd Rsnl<ine's formulse. (without Derivstions).Bebsviour of thin and thick cylinders. Problems on thin cylinderssnd spheres. •

.i Standard free"andard heat of formaL on,Thermochemaitry, L • h' of reaction and free energyf tion variatIon eaLenergy of orma i •. th temperature and pressure.chanSe of a react On Wl: Laws of electrolysis, electrol~tic

Electrochemistry nt and application ofol'.:a.n,sport'n,n.~~o'n"i;conduction, meaeure~,e 1 t ~L L LL ¥

Ionic lIlobility, "tronll and weak e e~ rcept of pH, buffertheo~y. Debye-Huckeltheor~. onattraction of acidity and basiCIty.'l:solutions, Concept

1 t'" and galvanic cells, types- Electromotive force. electro iY 1 d termination of standardof electrodes and els7trode rea~t ~~si ;eversible electrode andE.M.P., eleclrodie oXl.dationpo ~'.' a ~otentiollletric tit1'"tlo06,half cell reaction. Hernst equa~lon,th"rmodynalllicsof cell reactions.

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andof

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diagram.trusses.

solids. Lawsfriction,

Standsrd csses ofsnd msthemsticsl

free bodyframes and

----- -_._--

\15.

and simple proble~s on centroid and second moment of

Reference BookEl"ment of Physicsl Chemistry Glasston & Lewis.Textbook of Physical Chemistry' A Findaly.Physicsl Chemistry: A.J. Me~.Principales of Physical Chemlstry : Pruttan, Maron.

L2 •3 •1.

CHE-301 : Structural Mechanics :Concept of loads, supports and

Equilibrium of rigid bodles such as beams,Problems on anslysis of besms and trusses.

Friction-slidin~ friction b"t,,"en dryfriction. Probl"m on block friction, ,,'ad~efriction and oth"r rigid bodies under friction.

Conceptsres (M.I.)

Shear force and Bending moment diagrams for cantileversimply supported beams (with or without overhang). Theorybending: Concept snd problema.

Toraion~of a circulsr shaft. Trsnsmission of Power-Closecoiled Helicsl '.sprin~. Concept snd derivstion only. Simpleproblems.

Concept of slope snd deflection of beam.slope snd deflectio~ by Moment-area Methodmetbod. Simple probl",ms.

,.

Units and dimension:

Reference Book

CHE-305 : Frocess Calculations

real gassolutions

Idealmixtures

Psychrometric chart,

gases, liquids and solidsproperties, properties of

Basic concept : Humidity and saturation,solubility diagrams.

Propertil'" oflaws, criticaland equilibria.

Basic and derived units, dimensional analysis, dimensionaland empirical equaticns, Different ways of expresaing units ofquantities and physical constants.

1. Strength of Material: L.B.Prasad2. Advanced Strength of Haterials : K.T.Krishna Swamy3. Strength of Ha~erials : Junnarkar

Less conventional separation processes.

Typical industrial applications.

Therlllochemistry Heats of formation, combustion, solution,dilution, etc., and the effects of pressure and temperature onthem. Temperature of reaction. Energy balance for systems withand without ch~mical reset ion. Process efficiency, ,

.j~

-~

•

of the type:liquid-solid

0.11.. Hougen, K.M. Watson,R.A.Regalz.W.K.Levie A.H.Rsdaah,H.C. Lewis.Durl:apraasd Rao,n.v.s. Murthy

energy balances. Energy balancesphotochemical and biochemical

Reference Book

Concept of and calculations involving energy,enthalpy of reversible and irreversible processes.

atate material andelectrochemical,

Chemical Proess Principles

Industrial StoichiometryProcess Calculations forChemical Engineering

Unsteadyfor nuclear,processes.

I.

Thermophysic.sheat, work and

2.

Material balance: Concepts of limiting and excess rescatns, tieelement, recycle, purging, bypass etc., in batch, stagewise andcontinuous operations, in systems with and without chemicalreaction, and in unit operations.

,.

Separation and purification of binary mixturesWater soluble, water insoluble, both water soluble,liquid-liquid.

CHE-3l6 : Organic Che.iatry Laboratory :

--------------------.~ -'-"'--=---,"",--' •.

CHE-311 : Physical Chemistry Laboratory:

Preparations of simple organic compounds like acatanilide,m-dinitrobenze, methyl salicylate, benzamide, o-chlorobenzonicacid, tribromophenoI, p-nitrobenzomic acid and an azo dye.

Determination of equivalent conductivity of strongelectrolyte at infinite dilution, Solubility of sparingly solubleaalt by conductometric and potentiometric measurement,Conductometric-titration, Determination of standard redoxpotential of FE ++ IFe +++ system, Saponifaction of ahtyl acetateby conductivity method, Potentiometric titrations, Evaluation ofH, Sand G for eleetrochemcial reactions by E.M.F.meaaurements. Verification of Lamber-Beer'g la~, Adsorption of adye on solid surface by colourimetry.

hydroxyl, carboxyl,primary amino group,

",

Estimation of functional groups like,ester, amide, unsaturation, nitro, aromaticetc.

DeterminatIon of transport number by Hittorff method and bythe movin~ boundary method, Dissociation constant of acid byusing pH meter, Determination of pRa of an acid. Determination ofrate constant for inversion of cane sugar by polarimetry.

eHE-3IB : Structural Mechanics Laboratory

Univeral Force Table, roof truas apparatus fractionalplane. Reactions in beam, both simply supported and 'overhanging.Link polygon, B.M. apparatus. Simple machine like Screw Jack orWhel and axle.

z ..;0

~ :;<>z~.t>z ..Ii~z

;I ,> c!c ,z ,<m "Z J,• i~" ...A>c •">0z ..;

~I,": ...J

Determination ofof vapour-liquid

or Na 0 study of2 2

Determination ofDecomposition of

by distributiondyn"mic adsorption

forlll"tion"re" by

Study of rate of decomposition of H 02 2

method,of N ,

2t-butanol by ion e~change resin catalysts,solubility of a gas in liquid, Determinationequilibrium and activity coefficient.

complexsurface

------ __ c_ - •...... '. - -..-

Papers

Semester II

---------------------------------------------------------------------

100

100

TotalHarks

10

PeriodicTestHarks

,

No.of Examinationpapers Hrs Harks

----------- -------------------_~: 120 80 200

Total Harks ----------------------

Subject

-------- ---------------------------------Sr. Subjects ---------------------------No. Examination Marks for Total___________________________ Hrs Harks Class workCHE-116- Heat Transfer --------------------------------------

Laboratory. 6 60 10 100

CHE-117- Momentum TransferLaboratory

CHE-101- Homentum transfer 1 3 60 10 100

CHE-102- Haterial TechnolOGY 1 3 60 10 100

CHE-103- Introduction 10 1 1 60 10 100Chelll.EngG.

CHE-101- Economic • Ind . Mgt. 1 , 60 10 100

CHE-105- He"t Transfer 1 3 60 10 100----------------------- ------------300 200 500----------------------- ------------

Practical", and Orals

---------------------------------------------------------------------

Candidates will be eKamined in the subjects as indicated in thefollowing tables :

'u

18

-----~--_.

~. .

<~z .:-J~

~.li• ..J.', \, .

LG. 5:Katz D.L.

Types of fluids,and Non-Newtonian,three dimensional

,_.. - ~.__.---_. ---------

Analysis, fundamentalused in fluid mechanics.numbers, application to

"

Reference BookHeat Transfer ~ KundsenOperations : Gupta

Definition of fluid,incompressible, Newtoniansteady-unsteady, two and

Transfer :

"' •.~ -~-----_._-~ .••••••.,~< •. -

Layer Theory: Boundary Layer growth along flat plate,and turbulent flow in boundary laver. The thickness oflayer (definition and formulae only). Boundary layer intubes.

•Fluid DynalllicaandMomentum Transport

otindary:~.Jinarjiundarytraillht

~o phase co-current and~c9u'nt~~9urrent flow: Liquid-liquid andtS liquid systellls.FIOW"~j,~,t.(no mathematical treatment).ow &. Pressure MeasureOlel)tJ.,"i]- Principle and "T~pes of

anometers. The flot "~thBrough nozzles, or~f!cemeter,"nturimeter!l, pitot t{;b~r,Rota';'eter,notch or weir, other flow,:.a!luringdevices. 'Ii. "'''~~I~~'''',,','J'~'-imensional Analysis ';,''.)liRlehsionslimensions, units of various quantitiesuckinghanis Pi theorem. Dimensionlessluid flow problems.,

fluids , Pumping equipments for liquid. Thepump, positive displacement, Rotary pumps,

entrifugal pumps, design and operating Characteristics, NPSHalculations, Air lift pump.mping Equipment for,gases : Reciprocating piston compressors,6toy blowers and co~pressor, Centrifugal blowers and Compressor'~cluding turbo Comp;essor, Vacuum producing Equipmenta.~.t:er :required for Compression .0:£gasses : Clearance volume,

Cf' . Tho ,~W.- re"uirelllent forulti-stage COlllpressar e c~ency. u. ~~mping through pipe line liquids and gasea.,.,.

'i ,tHE';'~Ol-, :Ho_ntu.

;i~ld';'Propertles:C~mpressible lindLaminar-turbulent,

'flows.

'_~'lciWof Fluids Natur" and mechanism of fluid flow t.he~ontinuity equation, Bernoullis equation, Euler's equation of:motion along stream line, Bernoulli's equation as inte~ration of,Euler's equation, Momentum changes in fluid. The energy of a fuid~n motion, pressure and fluid head, pressure volume relationships~9r incompressible and compressible fuids, Reynold's number,~1..'b.llinarand tubulent flow in close conduit, velocity profile,~tiction factor for smooth and rough pipes, Hau~en Poiseu!lle

~

'qi.lation. velocity distribution in turbulent flow. The reiationbetween maximum and aversge velocity. Friction factor chart, Drageduction in tUrbulent flow, Effect of heat transfer on friction

~actor, friction factor in flow through channels of non-circular~rbss section. The friction loss from sudden expansion and~ntraction. Effect of fitting snd valves. Distribution oflowing fluids through branched pipes. Measurement of viscacity,arcy's Law lna derivation).

CHE-102 : Material TechnolouyClassification of engineering materIals, crystal structure,

che~ical bonding and structure of solids. Phase diagrams ofimportant alloy systems such as steels, brasses, cupronickel etc.and the applications of phase diagrams. Heat treatment of steels.Crystal defects and mechanical properties of solids such asplastic deformation, creep, fracture, fatigue.

Thermosetting and thermoplastics, structure-propertyrelationships in polymers, elastomers, Inorganic classes., "ood,graphite and ceramics. Composite materials.

Corrosion : Electrochemical principles, forms, mechanisms,prevention and control. Protective coatings. Corrosion behaviourof important alloys. Criteria for selection of materials forchemical industries.

Reference Book

Definition and scope of.unit operations in chemical engineeing.

Dryin~ : Tray dryers, rotary dryers, Vacuum dryers spray dryers,Fluidized bed dryers.

Size separationsl Equipments for mechanical separation, hydraulicspearation.

flaah,

TankWalker

<\ framefilters

such as Ja'"& VI trafine

S.P,Nay3k

PlateVaccume

such asSwenson

----_ .. ~",.•.•.•..._--- -.. _ .•-----~----

crystallizer'Scrystallizer,

for size reductionHammer mill, Ball mill

ofbatch

- . _.- ------~~-~~

for filtration such asfilter, Rotary filter,

Material Scienc : G.B.S. NarangEngineering Metallurgy and Material Science

20

Distillation: He~hods of distillation such as simple,steam distillation.

Crystallization: Typescrystallizer, AGitatedcn'stallizer.

Size reduction: Equipmentscruaher, Gyratory cursher,grinders.

Filtration: Equipment"filter press, Sweetlsndsuch as leaf filters.

The subject deals with the basics of Chemical Engineering & isintroduction of various topics listed below, hence there shouldbe no m3thematical treatment & derivation. The stress should beCiven only On the working ~rinciples « construction details ofvarious equipments.

Mixing and ACitation: Mixing in liquid - liquid « liquid - solidsystem. Types and selection of Agitators.

I.,.'CHE-103 : Introduction to Chemical Fngg,:

A, Economics Nature and signific"nce of economics. Basicecono~ic concepts. Demand and supply, elasticity of demand andsupply.

Heat Exchangers & Evaporators: Types of Heat Exchangers:Construction of Shell & tube heat exchanger 1n detail. T~pes ofevaporators. Evaporator accessories, construction de~ails.

Econo.ics and Industrial HanaCement

alteastwill be

liquid extraction,extractor and spray

submit the detail drawings ofabove topics. The theory paperincludes 50% DrawinS work.

Types of packing, differnet types of absorption

CHE-404 :

Note: The student has toEight equipments from theof duration 4 hours which

Absorption:equiplllents.Extraction: Solid liquid, liquidequipments such as Basket extractor, Rotocet& packed extraction tower.

functions of money.of foreign exchange and

Introduction to ~icro and macrO economics and price theory.

Honey, Real and opportunity cost. Concepts of profit and revenue,tax tariff and subsidies, wants and utilities.

z. ..Jc~ -z ..I•>z •> '.' ~• ,J'>m ~Z'iI ,> .J'c ,z ,<m '--~D • ...••~~,

.< i" ,> ..Jir0>0z• ..J

~l'l- ...J

capitalism,

of IndiaRole of at;:riculture in

Concepts of equilibrium and margin economic systems,socialism and mixed economy.

Economic development of India. Structure and featureseconomy. Growth of public sector in India.Indian economy.

Honey banking and trade. Nature andCo~mercial and central banking. Problemsimplicationa of currency devaluation.

F"ctors of product.

Meaning and tools of economic planning. Five year plans of India.:. Industrial Management Introduction: Management principles.anagement and enGineering studies. Heani-management. Concept of scien"f" "g and type of~. 1C management.

Financial and Accounting Mana erne .firm. Management of sales andS nt. The sales organization of aadvertisement. Mark.'~ research.

-.

organization.organizing,

.•. .•.... _ .•.••..

Functional areas of bu~'".~~. FTL Q-'- QQ O~m~of bu-I~.-~"eo~y and practice • Q Q •• Q~t ffi of management, planningsang, coordinating and cont~ol. 'Production Management . ltdproductivl." . n ro uction to work stud" Co-~.p' of~" wages and in t. " ••~ Lcontrol, Scheduling f j cen 1ves, production planning andcontrol and preventlvO p:o.ects, Haterials management, nuali~"e ma1nLenance. " ~.

-----_.-.._ .•..

Reference Book

and0'

Single

dilDension.••.1

processes.

basic equations,

transfer to vapori~ationevaporations.

Heat Transfer Laboratory:

of heat transfer,

Heat transfer through fluidised beds.

CHE-116

Reference Book

1. Engineering Heat Transfer Gupta & Prakash2. Problem on Heat Transfer P.Chattopadhya3. Heat Transfer ~ Champan1. h text book of Heat Transfer ~ Sukhatme S.P.

Heat Exchangers: Basic type~, LMTD in single pass, parallelcounter flow arrangements, cross-flow arrangements. I Usecorrection factor. Design principles of heat exchangers.

!

IRadiation Stefan-Boltzman'" law, Black-body radiation,radiation from aolid surfaces. Heat exchange by radiation betweentwo finite black surfaces, between two infinite I parallelsurfaces, ahape factor.

Evaporation: Helltand multiple effect

Modesanalysis,Conduction: Thermal conductivity of materials: Steady andunstesdy atate conditions. Steady atate conditions, equation ofplanes, cyl~nders, hollow spheres and problems related to thesecaSes. Lagglng of Pipes and other equipments; optimum laggingthickness. Heat transfer from extended surfaces (fins}.'

Convection : Individual and overall heat transfer coefficients.Natural and forced convection, laminar and turbulent flow, Heattransfer inside and outside the tubes. Natural convection heattransfer to wall and q'linder. Filmwiae and I dropwisecondensation. Heat transfer to boiling, correlations in boilingheat transfer.

Coat Engg. in P I drocess n ustries : Chilton C.H.

CHE-105 : Hest Transfer :

thermal conduct1vity of metal bar.thermal conduvtiv1ty of an insulating material.heat transfer coefficient by natural and forced

.~- ,.•

lube

heat

I;. •..--- ..

•

. _ ..~ _ .•.•. ' ,

efficiencY of pin f1n.the critical heat flux.Stefan' Boltzaman's constant.the emissivity of alum1nium plste.

_.'

To deter",ineTo determineTo determineconvection.To determine heat transfer coefficient 1n shell landtype heat exchanger.To determine heat transfer coefficient in double ,pipeexchenger.To determineTo determineTo determineTo determine

5 •

6.7 •6.9.

1.

L,.,.

~~------.~-~---.~.•~.----~--------10. To study droI»<ise and filmwise condensaton.11. Study of evaporatorl!l.12. Study of different types of heat. exchancers.

(Minimum eight experiments)

CHE-117 , Momentum Transfer Laboratory(I) Determination viscocity(2) Study of different. types of manometers.(3) Verification of Bernoullis Theorem(1) Venturimeter(5) Orificemet.er(6) Notch or Weirs(7) Study of flow throuch pipe tittincs(8) Verificstion of Darcy's law(91 Characteristics of Centrifugal pump(10) Flow of gases through pipes (Study of Friction factor

versus Reynold's number)(11) Reynold'" Experiment(12) Study of different types of Compressors

(Minimum Eight experiment ••).

23

.~-~---------------~.-'" - ..

________________________________________________________ ~k_~~~ __ ~ _

Candidates will be examined in the subjects as indicated inthe following table.

CHE-516- Mass Transfer-I 6 " 10 '"Laboratory

CHE-.5l7- Mechanical Operations 6 60 " '"--------------------------------~

z oJ0•~z ,.J<>z ,~ .:> ,.J'• !z;I ,> ....•!0• ,<m ,.A•~ ~- .J~>r •0>0z .;'I.,.J

TotalHark"

200

Marlts for TotalClass work

PeriodicTest IHarks

ExaminationHra Marks

No.of Examinationpapers Hrs Harks

Papers

Semester I

Practica!" and Orals

THIRD YEAR COURSE IN CHEHICAL ENGINEERING

SubJect"

Subjects

CHE-501- Ha"s Transfer , , 3 " " '"CHE-502- Mechanical Operation , 3 " " '"CHE-503- Cnemical Engineering , 3 60 10 >00

Thermodynamic"

CHE-501- Chemical React.ion , 3 " 10 '"Engineering ,CHE-505- Industrial • , 3 60 10 '"Engineering Chemi"try, ~-~--~--------~------------------300 200 600

s.,No,

s.,No,

Total Harks 700________________________ k ~ _

21

--------------------------------------.-----------.--

• .J0

"~• .J<>• ,>" ,J'> ,• ,•;I ,> •-'c ,~

,~,.J~

-~ ~

" ...A>c ,0>0• .J

~J,.J

and

masswallwith

lInits,

factor.

drier,

,transfer

drum

Iabsorption I,of",aplates bl'absorption.

Ref"rence Book

offo<

Tray drier, rotary drier,Vacuullldrier.

in packed towers: Height of columns,curve.

1. Hass Transfer Operation,,:Treybal R.E.2. Unit Operations of Chemical Engineering: McCabe3. Principles of Unit Operations' Foust A.S.1. Chemical Engineering Vol.II : Coulson J.M and

Richardson, J.P.

Th;i.rd

Absorptionequilibrium

Maas transfer Analogies' Heat, mass and momentum transfer.,

Gaa absorption: Mechanism of absorption and application oftransfer theories, values of transfer coefficients in wettedcolumns. packed towers, "'pray tower". The abllorptionchelrlicalreaction. !

CHE-501- Hass Transfer I

Semester I

Principles of diffusion and mass transfer betweenphases, Equimolecular counter diffusion, diffusion I throughstationary gas, Maxwell's law of diffusion, Diffusion in vapours,Diffusion in liquid, Diffusion in solids, unsteady state masstransfer.

Interphase .ase transfer: Theories of mass transfer, masstransfer coefficients, counter current mass transfer, andtransfer units, Concept of Mass transfer with chemical reaction.

Drying equipaents:Fluidized bed drier,

Plate towers: No.Different equipmenls

Drying: General principles, Rate of drying,moisture movement during drying. Diffusion andclassification snd selection of dryer".

Solids: Properties of solids, screening, screening equipmenteffectiveness of screens, screen Analysis, Average diameters andaverage specific Burface, shape factors etc. Size reduction ofsolids, Types of equipment on the various stages of reduclion,power requirement, Laws of crushing. Handling of solids, Designof belt conveyors, screw Conveyors, flight conveyors, pneumatic

,Humidification and Dehumidification: Principle and equipment,Definitions for Adiabatic saturation temperature, wet bulbtemperature, Humidity charts, Cooling tower: Height of 'packing,humidifying towers. Systems other than Air-water. I

Ithe Illechanie:mofcapillary theory

CHE-502- Mechanical Operation

----------------------------~.~.~

Fluid solid aysteG: Fixed bed, spouted bed, Fluidized bed systemand appllcation~.

maximumsettling velocity,I

Iequipment, mixing characteristics,index calculation~.

conveyors.

Fluids: Flo•• of solids through fluids,free and hindered settling conditions.

Filtration: Equipments for filtration, constant pressure andconstant rate filtration, filter calculations optimum cycle,Handling of compressible cakes snd use of filter aida, washing ofcake. Centrifugation equipment and calculations.Mixing • Agitation: Types ofpower consumption, Uniformity

Classification: Equipment", for clas6ification, principles ofJig~ing. Tabling, Haganetic snd electrostatic separations,sedimentation, laboratory batch sedimentation, Calculation ofareS snd depth for continuacus thickeners. Cyclone separators andtheir design.

Reference Book

CHE-503- Che~ical Eng~neering The~odyna.ics

Partial molal quantities, Gibbs Duhem equation in multicomponentsystem, phase rule, single component phase equilibria.

,,J,

",,

non idealRegular

chemicalreactionroultipte

and 2nd law of thermodynamics,Brief revision or 1stHaxwell's relationships.

.I, Mechanical Operations for Chemical Engineers: Naraynan &Bhattacharya I

2. Unit Operations of Chemical Enqineering Vo. I &, II.:P.Chart topadhya,

Thermodynamics of solution. electrolytes, ideal andsolution, Determination of activity coefficients.~olution theory, high pressure vapour equilibria,reaction equilibria. Homogeneous and hetrogeneous8~'stem. Equilibrium constants and composition inreaction phase rule.

Reference Book

26

,Review of chemical reaction equilibrium, classificat~on of

chelRical reaction, homogenous systems, rates of reaction, 'orderof reaction, and rate constant.

Pandey. ChaudhariChemical Engineering Thermodynamics

CHE-501- Che.ical Reaction Engineering I

, ""

Prnciples of reactor stablity and optimization:

Thermal characteristics of rectors: Isothermal, adibatic and nonadiabatic conditions.

Collection and interpretation of kinetic data, rate ofco~plex reactions, parallel series and other cases, heterogenousreaction kinetics,

".,Th.0'

Simulified objective functions.

Ideal reactions: Concept of ideality, Development of designexpression for batch, tubular and stirred tank reactors. Combinedreaotor aystem. comparision between mixed and plug flow reactoradvantges and limitation in application.

Residence time distribution Reaidence time functionrelation amongst there application to ideal reactors.modelling of real systms. Non-ideality parameters, predictlonreactor performance. Concept of mlcro and WacrO mixing.

Reference Book

27

z ,J0

"~z J•>z ,>" •••••>• !z~ ,"> ..•• ,t<, ,<m-.J~"~

.< •" .A>" ,0>0z ,J

~",J

-

of basicsoda and

Irefining.

Engineering aspects of lhe manufacturechemic~ls such as sulphuric acid, causticsods ash, ammonia, nitric acid and ures.

Outlines of operations and proceses in petroleum

- - ._------ -._"_. '.- .' - - .

Salient features of manufacture of commodity chemicals;status of chemical industry in India.

,1. Chemical Technology Vol. I to IV, Chem. Engg. Centre,

1:1.T. ,Madras.2. Unit Processes in Organic5 Synthesis: Oroggins

Reference Book

1. Chemical Reaction Engineering: Leven-piel O.2. Chemical Engineering Kinetics: Smith J.M.3. Chemical Reactor Theory: Denbingh R.O. & Turner K.O.

Engineering aspects of the manufacture, with considerationfor alternative routea, of basic organic chemicals,' such asethylene, propylene and other olefins. Acetylene, butadiene,benzene and alkyl benzenes, vinyl chloride, styrene, phenoia,aminI'S, alcohols, sldehydes, ketones, corbo:'l'ylicscids; esters,ethylene oxide, phthalic anh)'drideand terpthalic acid. I

Classification, sampling. snalysis and selection of coal.Csrbonisation and complete gasification of coal. Fuel oilspecifications. Combustion of solid, liquid and gaseous fuels.

Utilities: treatment of water for industrial use.

inorganicchlorine,

CHE-505- Industrial ~ Engineering Chemistry.

CHE-617- Mechanical Operations

CHE-516- Haas Transfer laboratory -I

Fat thIndustrial Chemi.cals

,,E~periments based on Grinding efficiency, Laws of

crushing, sieve analysis, efficiency of screening, sedimentation,filtration, cyclone separators, Fluidization, Mixing etc.lll\inimum 8 experiments)

,Experiments based on diffusion in still sir; diffusion

coefficients, wetted wall column. absorption ill packed tower,cooling tower, Tray direr, Ratars dirier, Fuidized bed drier,solid dissolution, interphSBe maSStransfer etc. !Minimum ei~htexperiments)

,.

• (.;0 ,~• J<>z ,>• ~~,>~ j ,

, ~ • •> l.,j~e ,• ,",m U~•• i~" ,.J~>r •0>0z J

iD,lJ

• ..J

" 0~z J<>•~ I~-"• U':D. ,:l'l ,.I;e ,• ,, ,m -1••~,< , .S">. J,r i0>0• J

~1'•••~ l.,j

\",I.,II

II_ ' ••••••• 0

)28

~-,.----------,-------,

------------------------------------------------------~--------------TotalHarks

Marks for Totalelaes work

PeriodicT""tHarks

II

60 10 100,60 10 100

I30 30 50

60 10 100

60 10 160,30 30 60

3

2

3

31

1

1

1

No.of Examinationpapers Hrs Marks

ExaminationMrs .• Harks

Papers

Semester

:;:, _. ,.•

Subjects

Subject

•,

'I

-----------------------------------Practical" and Orals

------------------,------------c!--300 200 500"

CHE-606- Elective I

CHE-601- Mathematics III

Candidates will be examined in the subjects as indicated in .th~-.following tables :

CHE-605- Hass Transfer II

CHE-602- Instrumentation &Instrumental analysis

CHE-601- Machine Oesil:1I & Drawing 1 3

CHE-503- Communication Skill & 1Tech. Report Writing

eIlE-617- Mass Transfer , 60 10 100Laboratory n

eHE-618- InstrUlllentat ion , 60 10 100Methods of analysis

CHE-618- Machine Drawing 60 50

----------------------------------------------------------------------------------------------------------------------------------------

,..No.

29

"'. --'

260

'.,

130120

'60-----------------------~------------------------------------------

12

•.-- .•._~_.~..••••,_.."'._...

Total Marks

~ -<--

---------------------------------

CHE-602- Instrumentation & Instrumental analysie

CHE-601- Mathematics IIIStatistics' Elementary treatment of probability and

mathematical expectation. Measurea of central tendencis, momentsand moment generating function. Frequency distributions1Binomial , Poission snd Normal distributions). I

Differentiation and intellration of vectors. ,The vectoroperator, curl and divergence of a raetor, Line snd surfaceintellrals. Gauss and Stokes's theorems. Complex ,I 'Variables.Regular Function, CaucheyRiemann differential equations, Cauchy'stheorem, Taylor's theorem. Cuntour.integration. Simple confermalmapping. Fourier series and integrals. 'I

Laplace transforms. Simple partial differential

Solu'tion of differential equations byDifferential equations:series method.

Transformsequaitons.

L Measuring instruments

iii. Measurement of Head and Level- Direct and indirect methods

Elements of measruing instrumentsStatic and dynamic characteristics of measuring instrumentsDynsmic characteristics of 1st order and 2nd order type measuringinstruments.

i. Temperature Heasurement:Temperature scalesExpanaion thermo~etersThermocouples, Thermistors, R.T.D.Radiation based temperature measuring instruments.

foilowingfalling in theinstrumentsof the2. Detailscategories:

ii. Pressure and Vacuum Measurement'ManometersMeasuring elements for gauge pressure and vacUumIndicatin~ elements for pressure and vaCuum gau;esMeasurement of absolute pressure etc.

iv. Flowmetering- Variable area meter. varisble head meter.

v. Measurement of Chemical Composition:- Spectroscopic analysis : Absorption spectrosocopy.emission spectroscopy, mass spectroscopy, x-raydiffraction. colour measurment by spectrometers'ldetailSof N.M.H.

I

30

"..Jz

0

~ ..Jf ,> ,> ....If•> ,•> ,;I> .J~c~

,•m .I'•

.~,~• .I'>

0>0 ..;z••~.- ..;

,

1

I

II

sulfide,

including:

------~-----~-~--------

Control Valv••"'

Gas analysis by thermal conductivityMoisture (humidity) analyaisPH measrementChromatography - a.L.C., H.p.L.e.Other special methods of analysis

Heat of combustion methodChemical methods for analysis of hydrogenorbon diOxide etcMagnetic susceptibility methodPolarizing cell methodDilatometerInterferometer

3.

1. Introduction to single loop feedback control:Block diagram and a brief introduction to PID controllers

6. Introduction to Digitial Control Systems:(Hatter under this heading should he presented without goinginto the details of constructional features and electroniccircuitry)

Digital control systemsIGeneralized data acqUisition system consisting of transducers.

aignal conditioners, multiplexer, analog to digital converters,data processing and handling systems, Conversion of Idigitalsignal to analos signals used in chemicRI' industries: r

1

,current to pressure converters

practice of communication.

Process Instrumentation :

Principles '"

Digital to analog converters,etc.,.

2.

1.

Recording. indicating and signalling instruments,transmission of instrument readinS. instrumentation in' moderncontrol plants, instrumentation diagrams etc. ICHE-603 - Coamunication Skill and Technical Report Writing,

\Professional communication: Forms of Technical writing.

3 • Reference work'" data collection

Techical corrospondence

Mechanics of presenting

Note takins II

setup.present day industrial

31

technical information

reports in the

ContentLangua!,:eForm

Importane of

••b.o.

5.

5.1,

. 7 •

_... ".-J~-------.-~." •• , .,._ •••..,.........,--.#0- _. _.,

-'

._-~

Liq-Liq Extraction : Calculation with and without reflux forimmiscible and partly mi'lciblesystems.

%0•;! J

I •,..;1~

> ,~ .J!il•0 ,J~m•• •~ ,-. ..;i,"~•0 ..)•~ILl' ..J

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free

wise,

stage

'lelection ofsafety, stre""

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stresses, selection of ball

Equilibria principles,and ion - exchange,

King

32

Reference Book

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exchanse ;adsorption

Prnciple, rate of cyrstal growth.

and ioncontact

and bearings, shaft design on the basis of rigidity,of keys and coupling, Belt, chain and Ilear drives (inAdvantages and disadvantages.

Separation Process

8. Classificstion of reports9. Writing of reports

a. Formatb. Mechanics of Language

CHE-601- Machine Design & Drawing.Design Mechn.'-.l -op,' f~~ p. er es 0 material,material, theories of failure, factor ofconcentration, fluctuatinllstresses.

Bolted, rivetted"••nd welded joints,and roller bearings.

Shaftsdesignbrief)•

Distillation:CRE-605- Mass Transfer II

Vapour liquid equilibria ideal non ideal systems, relativevolatality, Methods of distillation, Differential, flash,a:i\eotropicand extrative distillation. Low pressure di'ltlilatlon,steam distillation.

New separation techniques.

1.

Adsorptionand counter

Methods of Me Cabe - Thiele, Ponchon - Savarit, Reflux ratio.Number of plates, Plate efficiencies, Franske equation. Plate andpacked colu~s for distillation. Types of trays, Bubble captrays, sieve trays, Packed column for distillation. Continuouscontact equipment, concept "ofmulticomponent system,

Leaching : Single and multistage operations baaed on lowestcoordinates.CryatallizationTher~al balances, eguipment.

eHE-606 Elective Ia) Fuel and Combustion

,

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m ..J~•~ !• .,J~>r ,0>0 .Iz

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inand

liquidcolumn,

of H.T.U.

I

1,,grates

'I,

"I,':;,

,

and reinforcements for polymers, plasticizers,flame retardants. Introduction to polymer

fibres, elastomers, adhesives and foams.

Fuels as source of Energy and Chemicals,Conventional (commercialand non-commercial) and renewable sources of energy, Reserves,production, origin properties and classification andgassification of coal and biomass, petroleum refining. Types andproperties of gaseous fuels. Combustion calculations. Flametemperature. TyPes of combustion processes. Ignition temperature.Velocity of flame propagation.Limits of inflammability. Combustion of coal onpulverised state. Oil and gas burners.b) Particulate Technology : Particulate I systems,characteri~ation of particulate system trough ahaper" size andsurface. Generation of particulate system. Change of sizedistribution by size reduction, agglomeratIon and ,growth inBuspension. Hixin!: characteristica. Separation of particulatematter from liquids and gases. Storage, flow and discharge ofpowers. Metering of particulate systems. I

c} Polymer Chemistry Natural and synthetic, polymers.Principles of addition polymerization and polycondensation.Polymerization of monomers in bulk, aolution, emulsion andsuspension.. Molecular weight of polymers. Testing andcharacterization of polymers. Degradation of polymers.Copolymerization. Inorganic polymers.

Fillersstabili>:ers,technology :

Id) Energy Resources and Utilisation: Forms of energy andenergy conversion. New coal conversion processes. Biochemical(renewable) sources of energy. Hydrogen energy. Nuclear energy.Solar energy-collection and utilisation, wind and wave energy,geothermal energy. Energy storage systems. Energy auditing andeconomics. Concept of total energy system.

I,el Catalysis: Basic principles of heterogeneous catalYsis,chemisorption phenomena, correlation between the structure andcatalytic propertiea- present status. Basic principles ofhomogeneous catalysis, acid-base catalysis, liquid phaseoxidation, Walker process, hydroformylation-oxo I process,carbonylation reactions, polymeric catalysts, polymer bounden~yme and homogeneous catalysts,

Experiments based on Distlilation. solidextraction, Liquid Liquid extraction, spraycryatallization, adsorption, ionicchange, determinationand N.T.U., H.E.T.P. (any eight experiments). I

CHE-618- Instrumentation Hethoda of Analysis :11,

CHE-617- Hass Transfer Laboratory II

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Callibration of instruments such as, thermocouples, RTD sensors,rotameter ••, pressure gauges, orifice meter etc.

Valve characteristics, Dynamic response of in~trumentssuch sa, thermometers, thermocouples, manometers, control valves,pressure regulating valves etc.

Chromatography (Any eight experiments based on above

valves

methode

topics),,,

,other

Stuffing box, Icoupling,design Calculations),

using refractometer and

- globe, gate, needle, check relief

drive Componentsbearing, pulley (with

measurementsanalyais.

of valve avalves,

Typessafely

Compost tionfor chemical

2. Mechanicalgearassemblies,

CHE-619- Hachine Drawing

3. Process flow and Control diagrams.

1-.nd

I

Not" ,- Duration of paper '1hrs ..SO marks Theory. 30 Mll.krsdesisnand drawins.

I

Sear,

Drawin!l'ssketches

duplex,,

four.nd

plunser,- piston.types of pumpsreciprocating.

Each candidate shall submit at leastNo. 1,3,1 and two Design Calculations

No.2.

Work:topic

topoic

I,"II

,

I

1. VariousCentrifugal &.Term.fromfrom

•.,

--------------------------------------------------------------------

Semester IFco'U.rthYea.r

TotatMarks forCtass work

ExaminationHI's Marks

Subjectss.,'0,

,--------------------------------------------------------------------

CHE-701- Process Equipment 3 " 10 100DesignCHE-702- Chemical Engineering 3 " 10 '00MathemsticsCHE-703- Trsnsport Phenomena 3 60 10 '00

CHE-701- Numerical Analysis 3 " 10 '00Hodelling • SimulstionCHE-706 , Elective H 2 30 30 "------------------------------------------

------------------------------------------------------------------------------------------------------------------------------------

'00

50

'00

'00

350

600

'50

I

60

'"

60

60

'".-

Tot••l

Practical and Orals

CHE-718- Process Equipment Design --i. Drawing{Orsl)

CHE-719- Seminar

CHE.717_ Industrial Training 5:Educstional tour

CHE-716- Modelling 5:Sillluistion 6

III

35

,.CHE-101- Process Equip.ent Design

Mechanical properties of Materiels, selection of materials,protective costing, corroaoin - Causes and prevention. Theoriesof failures, factor of Safety. The material behaviour understresses, Fabrication- Design of Following Equipments:-Atmospheric storage vessels, unfired pressure vessel subjected tointernal and external pressure, vessels tor high pressureoperations. Agitated vessels, Tall column, supports for pressurevsssel, process design for evaporators. (Calendria type ofevaporator in detail). "

Eigen valus, eiSen vectors,Sylvester's formula,

Design of rotary dryer and crystalliser.The proportionating of pressure vessels.Selection of LID Ratio, optimization.Safety devices used in process industries,

CHE-102- Chemical Engineering Mathematics

Hamilton,,'.

Caley theorem ond

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PART-I MOMENTUM TRANSPORT

CHE-103- Transport Pheno.ena

36 'j

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HASS TRANSPORT

II : ENERGY TRANSPORTPART

PART - III :

Applications in distillation, transient analysis ofabsorber, unsteady atate analYsis in reactor system,Prater's method of estimation of the kinetics of complexschemes.

- .'-"".' ;,.-

Mathematical Technique essentia! for optimisation such as linearprogramming and dynamic programming, and application toequipment catalyst optimisation and overali process optimisation.,

Viscosity and the mechanism of momentum transport.Velocity distribution in laminsr flow.The equations of change for isoth,rmal systems.Velocity distributions with more than one independent variable.

Thermal conductivity and the nee han ism of energy transport.Temperature distributions in solids and in laminar lowThe equations of chanSe for Nonisothermal systmes.Temperature distributions with more then Onevariable.

Diffusivity and the mechanisms of mass transport.Concentration distributios in solid and in laminar flow.The equations of change of Multicomponent systems,Concentration dislributions with more than one independentvariable,

Examples of Mathematical Models:

Numerical Analysis:CHE-101- NUMERICAL ANALYSIS MODELLING A SIMULATION

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Newton-Rsphson

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Bennet - Myers

rule, Weddle's rule,by Sterling's formula.

37

Gauss-Siedel method

•

IApplications of ~athematical modelin~ Fundamental Laws:,ContinuitT equations, ener~y equation, equations

transport equations, equations of state, phaseequilibrium, chemical Kinetics

Reference BookTransport Phenomena : BirdMomontum, Heat and Mass Transfer

Solution of Simultaneous Linear Equations:Gauss elimination,Solution of Ordinary Differential Equations:

1.,.

Root Finding Methods:Bisection method, successive approximation,

method, MulIers's method.Numerical Inte~ration:

Trapezoidal rule, Simpson'sGregory-Newton formula, interpretation

Introduction:Process Modeling and Si~ulation:

motion,chemical

Taylor's series method, Euler's method, Kanga-Kutta method,Piccard's method.

1Mathematical models of chemical engineering systemssuch as CSTRs, PFRs, batch rsactors, distillation columns,Computer Simulation:Digitel simulation of chemical engineeringconsidered above.

CHE - 706 : ELECTIVE - IIa) Environmental Engineering

Nature of pollutants, their Sources and sinks.Meteorology and problems associated with dispersion •. Samplingmethods. Control techniques for gaseous and particulate

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to ,z ••

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Biochemicals reactors including treatment of aqueouswaste streams.

d) Multiphase reactionsMass transfer with chemical reaction in gas-liquid and

liquid-liquid systems. Three-phase reactors, Fixed bed and slurryreactors.

Scope of biochemical engineering in mQdern industry.Characteristics of biological materials, Enzyme kinetics.Isolation and application of enzymes. Immobilised enzymes. Cellstructure and metabolism. Kinetics of microbial ~ growth.Sterilization of liquids and gases. Design and control ofindusrial bio-resctor. Product recovery snd purification.Elementary aspects of genetics and biomedical engineering.Applications in the manufacture of foods and beverages,pharmaceuticals, chemicals and agro chemicals.

Water Pallulin : Characterisation of industrial wastewaters. Permissible limite of pollutants. Primary, secondary andtertiary treatment methods. Recovery methods for pollutants.Solid waste treatment.

cJ Biochemical Engineering

pollutants.

Introduction to electrochemical engineering.Theoretical aspects and special features of electrochemicalprocess. Role of mass transfer in a variety of electrochemicalproceesea. Some aspects of electrochemical reactor' design.Scale-up and optimization of reactors. I

Illustrative examples, particularly production ofcaustic soda, aluminium, sdiponitrile and speciality orcanicchemicals: recovery of metal valUes from waste atreams.,'

b) Electrochemical Engineering

e} Petroleum EngineeringCharacteristics of Indian and Foreign crudes. Basic

features of on-shore and off-shore oil and gas I fields.Characteristics of associated Cas. Exploration and development.Secondary and tertiary recovery of oils. Piping from the oilfield. Oil field chemicals.Trsnsporation of oil products.

CHE-716- Modelling & SimulationDigital Simulation of Chemical Engineering Systems.

3B

II

Students will be required to prepare a critical reviewsof selected topics in Chemical EnGineering and Bllied I aubjectsBnd submit in the form of B stBndard typed report. The studentwill alBo be required to make an oral presentation of the review.

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,jof at least five equipments.

Indu~trial Training and Educational TourCHE-717

39

a} Tour and training reportb) Seminarc) Vivo-voced) certificate from conmcerned organisation.

Process design snd drawing

Every atudent has to undergo 6 weeks summer training at renownedindustrial organisation (related to respective branch of study).The COnCern department should organise eductlonal tour comprisinCvisit to different reputed industrial organisation. Aftersuccessful completion of industrial training and educationaltour, the Btudent ••ill have to deliver B seminar and I submit atyped report based on his critical study of dlfferent,Bspets ofthe concenred organisation. Evaluation will be based on

CHE-119- Seminar

CHE-118- Proce~s Equip.ont Design & Drawing(Orsl)

Tot.alMarks forClass ,",ork

Examinat.ionHI'S Marks

----------------------------------------

Semester II

Subject.s--------------------------------------------------------------------S"No,

--------------------------------------------------------------------ClIE-801- Process Dynamics , , 60 10 100ControlCHE-802- Chemical Reaction , 60 10 100Engineering nCHE-803- Plant Design , , 60 10 '00Project EngineeringCllE-801- Process Engineering ,, 60 10 '00EconOlnic>:,Costing

•CHE-805- Elective HI 2 20 20 50

150

---------------------------------------------------------._---------

250600

Marks for 1 TotalClass work'

'20

ExaminationHI'S Marks

----------------------------------------

------------------------------------------------------------------------------------------------------------------------Total

Practical and Orals

Subjects",No,--------------------------------------------------------------------

CHE-816- Process Contt-ol • 60 10 '00Labot-atoryCHE-811- Plant Design" 60 " '00Drawing (Oral)CHE-818- Project work '00 " '"

J~•~

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Root Locus analysis

Stability analysis: notion of stability, Routh-Hurwitz I criterionfor stability

,Solution of linear differential equations using 'laplaceTransform, Transfer functions and input-output models Dynamicbehaviour of firat order, second order and higher order systems.

I controlled,derivative

I,control

,

Dynamic behaviour of feedbackof proportionla, intergal and

CHE-SOl- P~oce68 DYnamics & Control

Introduction : Characteristics of chameisl proceaMathematical modelling of a chemical process:State variables and state equationsInput-output model

Linearization of nonlinear systems

Feedback controlprocesses, effectaction.

Feedback controller design: performance criteria, selection typeof feedback controller,

Feedback control of systems with lar~e dead time/inverse responseIFeedforward control, ratio control, feedforward feed-back

control, cascade control, selective control, splil-range control.

Digitsl computer control: sampling continuous time Ireconstruction of continuous time signal from discreteconversion of continuous time to discrete time models.

of

plota,

singal,values,

design,,,

,contacting,,

etc.) criteria.,I

Bode

Ifrequency response

K ,C

processes:

, ,D

Tuning of Controllers (Selection of J ,r

Frequency reponse analysi~ of linearNyquists plots.

Design of feedback control systems usingtechniques.

CHE-802- ehe.ical Reaction EnCineering II

a. Hetrogeneous Reacting Systema:-

Rate equations for heterogeneous reaction,patterns for two phase systema.

b. Fluid - Particle ReactionBi-

Z-transfor, discrete time response of dynamic systms,di~ital feedback controllers.

(Introduction to Digital Control Principles;

,I

Selection of model, Unreacted core model for sphericalparticles of unchanllinll size, Rate' of reaction for lIhrinkingspherical particles, Determination of the rate controlling steps,~pplication to design - particles of single size, plug flowsolids. uniforms cas composition. MiXedflow of particle" ofsingle unchanging size. Mixed flow of size mixture of particlesof unchanginG size. Applications to fluidized bed withentrainment of solid fines. Instantaneous reaction.c. Fluid - Fluid ReactiOll:-

Rate equations, for instantaneous, fast, intermediatesand for ••low reaction. Slurry reaction kinetics, Rate equationfor infinitely "low reaction, film conversion parameter, Aerobicfermentations, Application to design - Towers for fast and slowreactions, Mixer settlers, Semi-batch contacting patterns.Reactive distillation and extractive reactions.d. Catslysis:-

Concept of catalyst Selection, classification andcharacteriatics of catalyst, Preparation of a catslyst 'and itsd"activation, Poeisioning of catalyst and regeneration.

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",

CHE-803- Plant Design & Project Engineering

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Fans

fixed bedreactors,

reactors.

Compreners,Pump,

Staged adiabatic pack ••d bedFluid - solid catalytic fixed

IDesign -

reactors,,.

bod

Process auxiliaries, piping design leyout, supports,insulation, pipe fittings, types of valves, selection ofproceee cotnrol and Instrumentation, control I system

,

Adsorption and its clsssificatio,isotherms, Determination of catalyst Surfaceo.

Applicationr••actors and fludized- bed reactors.

f.

different types ofarea by BET method.,

Solid - Catalyzed Reaction:- I

Rate equations, diffusion within Porous catalyst,experimental methods for finding rates, Product diatrib~tion inIllultipler"actions. 'j

Transportation of fluidsBlowers, Selection.

Design of Heterogenous Catalytic Re&ctors:-Fixed bed Reactors, Isotermal and adiabtio

reactor Nonisothermal, Non adiabatic fixed bedFluidized bed reactors, Slurry reactors, Trickle _ bed

12

Introduction: Basic considerations in Chemical Eng;; PlantDesign, Project identification, Preliminary techno-economicfeasibility. 'I

Process design aspects, Selection of proces, factorsaffecting proess selection, importance of laboratory developmentto pilot plant, scal ••-up ~ethods. Types flow sheets, Selection ofprocess Equipmnet; Development of process flow sheet from procesainformation.

pipingvales,design.

.- ..-""""

--------~-------------~---------

CHE-805- Elective III,

J~I~,

"..J!~,

water,heating

Iindul'ltrial

reedCoil

ProblelllS

inapplictionanalyais.

Use of PERT(CPH techniques.and assessment of project profitability.

Project Scheduling,Project evaluation

Process utilities, process water, boilerwater treatment, waste treati~ent of disposal,system, Chiiling plant, Compressed air and vacuum.

Safely measures in Plant Equipment.standardization and Commissioning.

Cash flow statement, project evaluation, discount cashflow, pay back period, br~ak-even point, introduction to marketsurvay, preliminary analysis of balance sheet, minimum: economicplant capacity, technological obsolence, need for expansion anddiversification, concept of marginal additional investment, roleof research and development. Indian Chemical Industry, currentstate and trends.

CHE-B01- Process Engineering Economics • Coating

Estimation of investment. 6/10 factor rule Icost ofinfrastructure, estimate of investment for the same, ~atimatingcost of productioin, principle of costing, Estimating workingcapital requairments, estimating financial cost by iway ofinterset charges and depriciation. Methods for detrmination ofdepriciation, profitability of project.

Phase equilibria and itssystems. Chemical reaction equilibria

b) Newer Separation Process

Plant location and layout-factors affecting bothplanning and layouts, Drawings of Plant layout, Use of scale upmethods. Plant elevtion drawings and complete engineering flowsheet drawings,

a) Industrial Thermodynamics

Basic concepts and definitIons, simple and compositesystem, thermodynamic process. Energy concepts and consequences,work and heat interactions. Application of laws of tyermodynamicsto opan and closed systems. Meat energies and heat pumps,reversibility and entropy and their applications to indusrialprohelsm. Heat exchanga network deai~n for distillation and powersystems.

Need for newer separation proceSlles. Characterizationof separation processes. Discussion of new separation methods,such as, adsorption on molecular sives; cas-liquidchromatoCraphYI extractive and addative crystallization.Extraction with reaction. Extraction with supercritical fluids.Separation of racemic mixtures. Separation by merobrancea lIuch as,reverse osmosis, pervaporation, etc. Separation of Cases byme.branes. Liquid membrane permeation. Separations viaaublimation/desublimation.

e) Applied Catalysisi. Catalytic aspects of industrially important processes.

Procesa in petroleum refining. Catalytic crackig, hydrocracking,reforming hydro desulphurieation.

,

-

,

reforminC ofmethanation.

autoxidation of

industry. Steamshift reaction,

iii. Processes fertilisernaphtha, low temperature water cas

iv. Catalytic h;rdrogenation.

ii. Partial oxidation of hydrocarbons,prcpylene.

oj Polymer Engineering, .._,Char~cteristic8 of polymeri~ation reactions. Polymerization

reactor ~eaicn and control. Heat transfer to solid and moltenpolymers~' Hixing of polymers, Processing of polymers byccmpreaalon, injection and extrusion techniques. Lamination,castins~~tbamins, blow moulding, vacUUm forming, calendering etc.'; ;"

" 10d} Opti~ization, Computer Aided Design & Project Engineering,r~i"hOptimising: Statistical methods in data eolection andoorI:"81&t1'O:n.Analytical methods for locating opt.imal conditionsfor univariable and multivariable unconstrained and constrainedsystems .;\.Dtrect-aellrch techniques, Linear Programming.

. ,',';<:ii, ".\.?omputer:Aided Destcn : Use of digital computers in

flowsheet:icalculations. Modular approach to desicn. Comput;rgraphics;'~_:{ 'I

,. ;~,iii~ Project Encineerinc Concept of s project as

conglomeration of multiple technical and non-technicaldiscipline~. Stages in a project such as process licence, processenCineerin~, detailed engineering, procurement, construction,commissioing, project planning and coat control. Briefintroduction to individual enCineering discriplines and theirscope of work in the project. CPM/PERT notwork methods:identification of critical path and critical activities.Contractual of reimbusement for contractors. Legal aspects suchas !::uarantees,liabilites, insurance, patent indenity. etc.

CHE-817- Plant Design & DrawinC (Oral)

Practicals based on theory subject processand control.

CHE-816- Procesa Control LaboratoryDynamics

I

flow sheets,seheduling.

2 processof project

Four drawincs ofsystem. Problell'ls

work:piping

Termplantlayout and

The project work on the topic will consiat I of eithersome investigational work, or design problem or experimentalsetup of some development work or prototype equipment Ordissertation related to the field of chemical engineering.

Every student will be required to submit a projectreport in a typed form, on a topic from the field of chemicalengineering which may be either selected by the studnet butepecifically approved by the faculty member who will guide theetudent, or on a topic to be.asaiged by one Or more facultyIllemb••ra.

the topicarea of

examined inthe relat",d

CRE-818- Project work

Every student will be orallyincorporated in the project and inspecial isation.

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