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S OVEREIGN C ONSULTING I NC . July 11, 2017 Via E-mail Ms. Shauna Little U.S. Environmental Protection Agency EPA-Region 1 5 Post Office Square Boston, MA 02109-3912 Re: NPDES Remediation General Permit Application Shell-Branded Service Station 140 Sharon Street Stoughton, Massachusetts 02072 RTN 4-15064 Ms. Little: Sovereign Consulting Inc. (Sovereign), on behalf of Colbea Enterprises LLC (Colbea), has prepared this National Pollutant Discharge Elimination System (NPDES) Remediation General Permit (RGP) – Notice of Intent (NOI) for the above referenced disposal site. This RGP – NOI pertains to Category I – Petroleum Related Site Remediation, Category III – Contaminated Site Dewatering, Sub-Category F - Fuels Parameters. The NPDES RGP permit application was prepared to allow for discharge of groundwater during dewatering for underground storage tank installation activities. The groundwater will require pre-treatment prior to discharging into the municipal storm sewer located on Sharon Street in Stoughton, Massachusetts and will be discharged in accordance with NPDES regulations. The project is also regulated under the Massachusetts Contingency Plan 310 CMR 40.0000 under Release Tracking Number (RTN) 4-15064. If you have any questions regarding this submittal, please feel free to contact the undersigned. Sincerely, SOVEREIGN CONSULTING INC. James M. Smith Senior Project Manager Attachments: NPDES RGP Application cc: With Attachments: Marc Oler, SOPUS Town of Canton MassDEP-SERO Mass DOR– 21J Sovereign File – 2P764

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Page 1: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

S O V E R E I G N C O N S U L T I N G I N C . July 11, 2017 Via E-mail Ms. Shauna Little U.S. Environmental Protection Agency EPA-Region 1 5 Post Office Square Boston, MA 02109-3912 Re: NPDES Remediation General Permit Application

Shell-Branded Service Station 140 Sharon Street Stoughton, Massachusetts 02072 RTN 4-15064

Ms. Little: Sovereign Consulting Inc. (Sovereign), on behalf of Colbea Enterprises LLC (Colbea), has prepared this National Pollutant Discharge Elimination System (NPDES) Remediation General Permit (RGP) – Notice of Intent (NOI) for the above referenced disposal site. This RGP – NOI pertains to Category I – Petroleum Related Site Remediation, Category III – Contaminated Site Dewatering, Sub-Category F - Fuels Parameters. The NPDES RGP permit application was prepared to allow for discharge of groundwater during dewatering for underground storage tank installation activities. The groundwater will require pre-treatment prior to discharging into the municipal storm sewer located on Sharon Street in Stoughton, Massachusetts and will be discharged in accordance with NPDES regulations. The project is also regulated under the Massachusetts Contingency Plan 310 CMR 40.0000 under Release Tracking Number (RTN) 4-15064. If you have any questions regarding this submittal, please feel free to contact the undersigned. Sincerely, SOVEREIGN CONSULTING INC.

James M. Smith Senior Project Manager Attachments: NPDES RGP Application cc: With Attachments:

Marc Oler, SOPUS Town of Canton MassDEP-SERO Mass DOR– 21J

Sovereign File – 2P764

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S O V E R E I G N C O N S U L T I N G I N C . S c i e n c e . S e r v i c e . S o l u t i o n s .

NPDES REMEDIATION GENERAL PERMIT APPLICATION

Shell-branded Gasoline Station 140 Sharon Street

Stoughton, Massachusetts

MassDEP RTN 4-15064

July 11, 2017

Project Number: 2P764

Prepared for:

Equilon Enterprises LLC dba

Shell Oil Products US 20954 S. Wilmington Avenue

Carson, CA 90810

Prepared by:

Sovereign Consulting Inc. 16 Chestnut Street, Suite 520

Foxborough, Massachusetts 02035

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TABLE OF CONTENTS

1.0 INTRODUCTION......................................................................................................................................................1

2.0 PROJECT SUMMARY..............................................................................................................................................1

2.1 SITE DESCRIPTION...........................................................................................................................................................................1

3.0 DISCHARGE INFORMATION.............................................................................................................................2

3.1 INFLUENT AND RECEIVING WATER SAMPLING...................................................................................................................23.1.1 Influent Sample Results..........................................................................................................................................................33.1. Dilution Factor...........................................................................................................................................................................3

4.0 TREATMENT SYSTEM INFORMATION.........................................................................................................4

4.1 SYSTEM DESIGN................................................................................................................................................................................4

5.0 RECEIVING SURFACE WATER...........................................................................................................................4

5.1 RECEIVING WATER INFORMATION...........................................................................................................................................45.2 RECEIVING WATER CLASSIFICATION.......................................................................................................................................5

6.0 ESA AND NHPA ELIGIBILITY.............................................................................................................................5

6.1 ENDANGERED SPECIES ACT GUIDANCE.................................................................................................................................56.2 NATIONAL HISTORIC PRESERVATION ACT...........................................................................................................................5

FIGURES Figure 1 Site Locus Map Figure 2 Site Plan with Drainage Details Figure 3 Typical Groundwater Dewatering Installation Diagram Figure 4 Waterbody Assessment and TMDL Status Raynham, MA Figure 5 MassDEP BWSC Phase 1 Site Assessment Map ATTACHMENTS Attachment A Notice of Intent Form Attachment B Laboratory Analytical Data Attachment C Dilution Factor and Effluent Limitation Calculations for Massachusetts Attachment D Town of Canton Discharge Notification Letters Attachment E US Fish and Wildlife Service Species Determination Attachment F MACRIS Database Search Results

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1.0 INTRODUCTION Sovereign Consulting Inc. (Sovereign) prepared this National Pollutant Discharge Elimination System (NPDES) Remediation General Permit (RGP) application on behalf of Shell Oil Products US (SOPUS) to manage treated groundwater which will be discharged into the municipal storm catch basin located on Sharon Street in Stoughton, Massachusetts. The residually impacted groundwater will be generated from dewatering during underground storage tank (UST) system installation. This site is identified by the Massachusetts Department of Environmental Protection (MassDEP) as Release Tracking Number (RTN) 4-15064 and is regulated in accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.0000. Accordingly, discharges subject to the MCP do not require the completion of a state application form BRPWM 12 or state fee payment. A Site Location Map and discharge location is provided as Figure 1 and a Site Plan, depicting relevant site features including the municipal storm system location, is attached as Figure 2. Figure 3 presents a Typical Groundwater Dewatering Installation Diagram. A Waterbody Assessment and TMDL Status for Canton, Massachusetts (the discharge location for the storm drain outfall) is provided as Figure 4. The MassDEP Bureau of Waste Site Cleanup Phase I Site Assessment Map, dated July 5, 2017, is provided as Figure 5. For the purpose of this investigation, the “facility” is defined as the area located within the property boundaries of 140 Sharon Street, Stoughton, Massachusetts. The “disposal site” is defined as the property and other properties where oil and/or hazardous material (OHM) has come to be located as a result of the release from the property. Relevant Contacts: Facility/Facility Owner: Colbea Enterprises LLC 2050 Plainfield Pike Cranston, Rhode Island 02921 Contact: Thomas Breckel Tel: (401) 943-0005 Facility Operator: Colbea Enterprises LLC 2050 Plainfield Pike Cranston, Rhode Island 02921 Contact: Thomas Breckel Tel: (401) 943-0005 2.0 PROJECT SUMMARY 2.1 Site Description The facility is located in a mixed commercial/residential area of Stoughton, Massachusetts and has operated as a gasoline station since at least the 1960s. This Shell-branded station is currently owned by Colbea Enterprises LLC (Colbea). A one-story building with a convenience store and a car wash are located on the southern portion of the property. Two 10,000-gallon gasoline and

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one 8,000-gallon gasoline underground storage tanks (USTs) are located on the northwest portion of the facility. The existing USTs are constructed of single-walled, fiberglass-reinforced plastic with product line leak detection and an in-tank monitor. The station and carwash buildings are heated via electric, forced hot-air systems. Electricity and telephone services enter the property via overhead lines from a utility pole at the eastern property corner. Electric and telephone service lines continue underground to the facility building. Natural gas, water, and sewer are supplied to the facility via underground utility lines entering the property from the east. The areas surrounding the structures are paved with asphalt. Entrances to the property are located on Sharon Street and Bay Road. Colbea anticipates removing the entire UST system, demolishing the site building, installing a new UST system, and constructing a new site building in the near future. The disposal site is a commercial property and does not have a NPDES permit or prior application. Dewatering activities associated with this RGP application are associated with excavation for the installation of replacement USTs. 2.2 Sensitive Receptors According to data obtained from the MassDEP Bureau of Waste Site Cleanup (BWSC) Phase 1 Site Assessment Map, dated July 5, 2017, Figure 5, the disposal site is not located within a Current or Potential Drinking Water Source Area, Zone II or Interim Wellhead Protection Area (IWPAs). No other potentially sensitive environmental receptors have been identified within a 500-foot radius of the disposal site. A residential property, identified as 2351 Central Street in Stoughton, is located adjacent to the southeastern corner of the subject property and utilizes a private water supply well for drinking water purposes. The private drinking water supply well on that property is located approximately 300 feet southeast of the disposal site in the inferred upgradient direction. No schools, hospitals, daycare centers, or long-term health care facilities were identified within 500 feet of the disposal site. There are no IWPAs, surface water supply Zone A areas, Potentially Productive Aquifers, Non-Potentially Productive Aquifers, wetlands, Protected Open Spaces, Priority Habitats of Rare Species, vernal pools, or Areas of Critical Environmental Concern (ACEC) identified within 500 feet of the disposal site. The nearest surface water bodies are Shephard Pond and Massapoag Brook, approximately 1,600 feet northwest of the disposal site boundary. Wetlands are located within ½ mile of the disposal site in the southwest, east and northeast directions. The nearest wetlands are located approximately 625 feet downgradient, in the northwest direction of the facility. A potential vernal pool is located approximately ½ mile from the disposal site boundary. A FEMA 100-year floodplain and protected open space are located within ½ mile radius of the disposal site. A non-potential drinking water source area of medium yield and a medium yield aquifer are located approximately 1,125 feet southeast of the disposal site. 3.0 DISCHARGE INFORMATION 3.1 Influent and Receiving Water Sampling An influent sample was collected from groundwater at monitoring well MW-1, which is located within the area where construction dewatering will be required. A receiving water sample was

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collected from the nearest accessible surface water location in Massapoag Brook. Both groundwater samples were collected on June 1, 2017 and analyzed by a State of Massachusetts certified laboratory for the parameters required by the RGP Permit. The sample results, laboratory methods, laboratory method detection limits, and the total maximum daily mass of contaminants of concert (COCs) anticipated to be discharged have been summarized in the Notice of Intent form provided as Attachment A, and the laboratory analytical report included as Attachment B.

3.1.1 Influent Sample Results The influent sample results from groundwater collected at monitoring well MW-1 chloride and hardness parameters, below the effluent limit listed in Section D of the NOI form. Effluent samples were not collected at the time of sampling because the dewatering treatment system is not installed. On the NOI form, all analytes detected above the laboratory detections limits from the June 1, 2017 sampling event were recorded as “Known or Believed Present” and all analytes detected below the laboratory detections limits were recorded as “Known or Believed Absent”. The two exceptions were tert-butyl alcohol (TBA) and tertiary-amyl methyl ether (TAME), which have historically been detected at this location, but have not been detected in recent years. These two analytes have been conservatively categorized as “Known or Believed Present.”

3.1. Dilution Factor SOPUS evaluated the potential concentration considering a dilution factor (DF) using the formula below: Dilution Factor (DF) Calculation: DF = (Qs + Qd) / Qd

Where:

DF = Dilution Factor Qd = Maximum flow rate of the discharge in cubic feet per second (cfs) (1.0

gpm =0.002676 cfs) Qs = Receiving water 7Q10 flow (cfs) where 7Q10 is the minimum flow (cfs) for 7

consecutive days with a recurrence interval of 10 years Estimated flow rates are based on the maximum flow rate of 50 gpm and the United States Geological Society 7Q10 flow data for Massapoag Brook, the dilution factor is as follows:

DF = (Qs + Qd) / Qd Qd = .0.072 MGD Qs = 0.275 DF = (0.275 +0.072)/ 0.072 DF= 4.82

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SOPUS anticipates that the treatment system will remove the majority of dissolved iron from the effluent water stream prior to discharge to the storm water drain which discharges to Dam Lot Brook. If needed, a modification to the system may be required which will include the incorporation of a sequestering agent to keep iron in solution. Any modifications to the system will be submitted for approval by a Notice of Change (NOC). The calculated dilution factor and effluent limitation calculations are included as Attachment C. 4.0 TREATMENT SYSTEM INFORMATION 4.1 System Design The sump water treatment system will be located in on the disposal site, located at 140 Sharon Street in Stoughton, Massachusetts. The system will be composed of the following: one submersible sump pump locate within each sub-grade sump, a pre-treatment holding tank, two bag filters piped in parallel to filter out particulates, two influent 200-pound or greater liquid phase granular activated carbon (LGAC) units piped in parallel and two effluent 200-pound or greater LGAC units piped in parallel, and a post-treatment holding tank. The flow rate of the system is designed to pump, treat, and discharge up to 50 gpm, but is expected to range from 1 to 20 gpm. The component of the system with the most limited flow will be the LGACs. The proposed discharge location for treated groundwater is a municipal storm drain catch basin located adjacent to the property line, on Sharon Street adjacent to the disposal site as depicted on Figure 2. This storm drain discharges to a wetland that feeds Massapoag Brook. Refer to Figure 4 for a typical Groundwater Dewatering Installation Diagram. 5.0 RECEIVING SURFACE WATER The proposed discharge location for treated groundwater is a municipal storm drain catch basin located adjacent to the property line, on Sharon Street as depicted on Figure 2. This storm drain discharges to a wetland that feeds Massapoag Brook. The discharge point to the wetland is located 350 feet to the northwest of the disposal site. The Town of Canton Town Engineer and Conservation Commission were both notified in writing of the planned discharge of treated groundwater to the wetland feeding Massapoag Brook. Both departments will be contacted again following submittal of the RGP application. Copies of the notification letters are included as Attachment D. 5.1 Receiving Water Information The receiving water for the indirect discharge of the treated groundwater discharge is Massapoag Brook. On June 19, 2017, Sovereign consulted the online United States Geological Survey (USGS) Streamstats program to determine the 7Q10 flow rate at the discharge location. Data obtained from the online resource indicated that the 7Q10 flow rate for Massapoag Brook at USGS station #01105270 is 0.426 cubic feet per second (cfs). Based on data available, Sovereign calculated a 7Q10 flow rate for this area to be approximately 0.275 million gallons per day (mgd).

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Per the Waterbody Assessment and TMDL Status Map for Canton, Massachusetts, Massapoag Brook is listed as a Category 5 impaired or threatened water body. Category 5 is water that is impaired or threatened for one of more uses and required a TMDL. A copy of the Waterbody Assessment and TMDL Status Map for Canton, Massachusetts is included as Figure 4. 5.2 Receiving Water Classification Sovereign consulted the MassDEP Division of Water Pollution Control to determine the classification for the receiving waters. Massapoag Brook, segment MA73-21, is listed as Class B. 6.0 ESA AND NHPA ELIGIBILITY 6.1 Endangered Species Act Guidance In accordance with Appendix I and II of the RGP regulations, Sovereign personnel reviewed the regulations to determine if the proposed discharge to the storm drain on Sharon Street, which discharges to a wetland that feeds Massapoag Brook, is in compliance with the Endangered Species Act (ESA) eligibility criteria. Based on the ESA Eligibility Criteria, the applicable criterion is “Criterion B”. Criterion B states that a formal or informal consultation with the Fish and Wildlife Service (FWS) under section 7 of the ESA resulted in either a no jeopardy opinion (formal consultation) or a written concurrence by FWS on a finding that the discharges and related activities are “not likely to adversely affect” listed species or critical habitat (informal consultation). While one threatened species (the northern long eared bat) exists within this portion of the Massapoag Brook and wetland area, the planned discharge of treated groundwater is considered not likely to adversely affect this species. In addition, there are no critical habitats located in the vicinity of the project area. Correspondence with the FWS is included as Attachment E. 6.2 National Historic Preservation Act In accordance with Appendix III of the RGP regulations, Sovereign personal reviewed electronic listings to determine if any historic properties, or properties eligible for listing on the National Register of Historic Places, are within the path of the discharge or discharge related activities. Listings of Historic Places within the Town of Canton, in the vicinity of the proposed discharge area of Massapoag Brook and associated wetland were obtained from the Massachusetts Cultural Resources Information System (MACRIS) online database, accessed July 6, 2017). A copy of the MACRIS report is provided as Attachment F. The database indicated that Massapoag Brook and its associated wetland are not registered as historic properties. There are several historic places located in proximity to the proposed discharge area. Upon review of the listed locations, It has been determined that the listed properties are located upgradient from Massapoag Brook and its associated wetland area, and are unlikely to be impacted from the planned discharge of treated groundwater to the wetland area. In accordance with Part IIC of Appendix III of the RGP regulations, Permit Eligibility Criterion B is applicable. Criterion B states that “Historic properties are present. Discharges and discharge related activities do not have the potential to cause effects on historic properties.” This project does not involve the demolition or rehabilitation of existing buildings or other

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structures or facilities and historic properties are not affected by the discharge or identified in the path of the discharges regulated by this permit.

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NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA

FIGURES

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SOVEREIGN CONSULTING INC.

Sovereign Scale (approx.)Job No.2R

1" = 1000'764

UTM 19 322408E, 4667315N

Reference: Stoughton, MA Quadrangle - USGS 1989Contour Interval = 3 meters

140 Sharon Street, Stoughton, MA

FIGURE 1SITE LOCUS MAP

Shell-branded Gasoline Station

SITE LOCATION

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M A 73 -32_ 2008U n nam ed T r ibu ta ry (5 )

M A 73 -05_ 2008 E as t B ran ch (5 ) (T M D L )

MA73-02_2008 Neponset River (5) (TMDL)

MA73-05_2008East Branch (5) (TMDL)

M A 73 -24_ 2008 P u rg a to ry B rook (4a ) (T M D L )

M A 73 -05_ 2008 E as t B ran ch (5 ) (T M D L )

MA73-24_2008Purgatory Brook (4a) (TMDL)

M A 73 -20_ 2008Be av e r M e ado w B rook (5 ) (T M D L)

MA73-27_2008Ponkapog Brook (4a) (TMDL)

M A 73 -20_ 2008 B ea ve r M ea dow B roo k (5 ) (T M D L)

MA73-21_2008Massapoag Brook (5)

MA73-29_2008Pine Tree Brook (5) (TMDL)

MA73-19_2008Beaver Brook (5)

MA 73-18_2008Steep H ill B rook (2)

MA73-22_2008Pequid Brook (5) (TMDL)

M A 73 -17_ 2008Trap ho le B roo k (4 a ) (T M D L )

M A 73 -01_ 2008 N epo nse t R iv e r (5 ) (T M D L)

M A73 -01_2 008 N epon set R iver (5) (TM DL)

MA73-02_2008Neponset River (5) (TMDL)

MA73-25_2008Pecunit Brook (2)

24

27

139

28

138

BolivarBolivarPondPond

GlenGlenEchoEchoPondPond

LakeLake

ReservoirReservoirPondPond

PonkapoagPonkapoagPondPond

HoughtonsHoughtonsPondPond

Saw Mill PondSaw Mill Pond

CarCarWorksWorksPondPond

LakeLake

Forge PondForge Pond

Dedham

Boston

Stoughton

Avon

Randolph

Canton

Milton

Westwood

Norwood

Sharon

Quincy

MA73053_2008Sprague Pond (3)

MA74015_2008Hoosicwhisick Pond (3)

MA73005_2008Bolivar Pond (5)

MA73022_2008Glen Echo Pond (3)MA73020_2008

Forge Pond (5)

MA73048_2008Reservoir Pond (4c)

MA73043_2008Ponkapoag Pond (4c)

95

93

95

Beech RunBeech Run

Nepo

nset

River

Nepo

nset

River

Pecunit Brook

Pecunit Brook

Ponkapoag BrookPonkapoag Brook

Steep Hill BrookSteep Hill Brook

Balster BrookBalster Brook

Pequ

id Br

ook

Pequ

id Br

ook

Massapoag Brook

Massapoag Brook

Redwing Brook

Redwing Brook

York Brook

York Brook

Pequit Brook

Pequit Brook

Neponset RiverNeponset River

Blue Hill RiverBlue Hill River

Pine Tree BrookPine Tree Brook

Lowder BrookLowder Brook

Beaver Brook

Beaver Brook

Waterbody Assessment and TMDL Status 0 0.5Miles

Map produced by E PA Region I G IS CenterMap Tracker ID 6678, F ebruary 25, 2010

Data Sources: TeleAtlas, Census B ureau,US G S, M assDEP

Canton, MAWaterbodies

MS4 Urbanized Areas (2000 Census)Municipal Boundaries

Swamp/MarshState ID,Waterbody Nam e (Category)(T MDL(s) approved for th is waterbody)

Waterbody Label Assessment of Waterbody SegmentCategory 2: Attaining some uses; other usesnot assessedCategory 3: Insufficient information to make assessments for any use.See companion table for a listing of pollutants,non-pollutants, and TMDLs for each waterbody

Notes:1) A da pte d f rom Fina l M assachu se tts Yea r 20 08 In teg rated List of Wa te rs;availab le at http ://w w w.m ass.go v/d ep /w ater/r esou rce s/08l is t2 .pd f2) W a terb od ie s sho w n w ith ou t a n ide nti fie d ca teg ory a re a ss ig ne d as C atego ry 3 by de fin it ion .3) F or a dd ition al in form a tio n o n T MD L s and to v ie w rep orts, se e: http ://w w w.m ass.go v/d ep /w ater/r esou rce s/ tmd ls .h tm4) F or M assachu se tts Su rfa ce W ate r Q ua li ty S ta nd ard s, an d w a terb od y classe sand u se s, se e: http ://w w w.m ass.go v/d ep /serv ice/r egu la tio ns /3 14 cm r04 .p df

Category 4a: TMDL is completed and approved for one or more pollutantsCategory 4c: Impairment not caused by a pollutant.Category 5: Impaired or threatened for one or moreuses and requiring a TMDL.

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MassDEP - Bureau of Waste Site CleanupPhase 1 Site Assessment Map: 500 feet & 0.5 Mile RadiiSite Information:

140 SHARON STREET, STOUGHTON MA140 SHARON STREET STOUGHTON, MA4-000015064NAD83 UTM Meters: 4667328mN , 322397mE (Zone: 19)July 5, 2017

The information shown is the best available at the date of printing. However, it may be incomplete. The responsible party and LSP are ultimately responsible for ascertaining the true conditions surrounding the site. Metadata for data layers shown on this map can be found at:http://www.mass.gov/mgis/.

500 m1000 ft

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NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA

ATTACHMENT A

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MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 14 of 24

II. Suggested Format for the Remediation General Permit Notice of Intent (NOI)

A. General site information: 1. Name of site:

Site address:

Street: City:

State:

Zip:

2. Site owner

Owner is (check one): Federal State/Tribal Private

Other; if so, specify:

Contact Person:

Telephone: Email:

Mailing address:

Street: City:

State:

Zip:

3. Site operator, if different than owner

Contact Person:

Telephone: Email:

Mailing address:

Street: City:

State:

Zip:

4. NPDES permit number assigned by EPA:

NPDES permit is (check all that apply: RGP DGP CGP

MSGP Individual NPDES permit Other; if so, specify:

5. Other regulatory program(s) that apply to the site (check all that apply):

MA Chapter 21e; list RTN(s):

NH Groundwater Management Permit or

Groundwater Release Detection Permit:

CERCLA

UIC Program

POTW Pretreatment

CWA Section 404

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MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 15 of 24

B. Receiving water information: 1. Name of receiving water(s):

Waterbody identification of receiving water(s):

Classification of receiving water(s):

Receiving water is (check any that apply): Outstanding Resource Water Ocean Sanctuary territorial sea Wild and Scenic River

2. Has the operator attached a location map in accordance with the instructions in B, above? (check one): Yes No

Are sensitive receptors present near the site? (check one): Yes No

If yes, specify:

3. Indicate if the receiving water(s) is listed in the State’s Integrated List of Waters (i.e., CWA Section 303(d)). Include which designated uses are impaired, and any

pollutants indicated. Also, indicate if a final TMDL is available for any of the indicated pollutants. For more information, contact the appropriate State as noted in Part

4.6 of the RGP.

4. Indicate the seven day-ten-year low flow (7Q10) of the receiving water determined in accordance with the instructions in

Appendix V for sites located in Massachusetts and Appendix VI for sites located in New Hampshire.

5. Indicate the requested dilution factor for the calculation of water quality-based effluent limitations (WQBELs) determined in

accordance with the instructions in Appendix V for sites in Massachusetts and Appendix VI for sites in New Hampshire.

6. Has the operator received confirmation from the appropriate State for the 7Q10and dilution factor indicated? (check one): Yes No

If yes, indicate date confirmation received:

7. Has the operator attached a summary of receiving water sampling results as required in Part 4.2 of the RGP in accordance with the instruction in Appendix VIII?

(check one): Yes No

C. Source water information:

1. Source water(s) is (check any that apply):

Contaminated groundwater

Has the operator attached a summary of influent

sampling results as required in Part 4.2 of the RGP

in accordance with the instruction in Appendix

VIII? (check one):

Yes No

Contaminated surface water

Has the operator attached a summary of influent

sampling results as required in Part 4.2 of the

RGP in accordance with the instruction in

Appendix VIII? (check one):

Yes No

The receiving water

Potable water; if so, indicate

municipality or origin:

A surface water other

than the receiving water; if

so, indicate waterbody: Other; if so, specify:

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MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 16 of 24

2. Source water contaminants:

a. For source waters that are contaminated groundwater or contaminated

surface water, indicate are any contaminants present that are not included in

the RGP? (check one): Yes No If yes, indicate the contaminant(s) and

the maximum concentration present in accordance with the instructions in

Appendix VIII.

b. For a source water that is a surface water other than the receiving water, potable water

or other, indicate any contaminants present at the maximum concentration in accordance

with the instructions in Appendix VIII? (check one): Yes No

3. Has the source water been previously chlorinated or otherwise contains residual chlorine? (check one): Yes No

D. Discharge information

1.The discharge(s) is a(n) (check any that apply): Existing discharge New discharge New source

Outfall(s): Outfall location(s): (Latitude, Longitude)

Discharges enter the receiving water(s) via (check any that apply): Direct discharge to the receiving water Indirect discharge, if so, specify:

A private storm sewer system A municipal storm sewer system

If the discharge enters the receiving water via a private or municipal storm sewer system:

Has notification been provided to the owner of this system? (check one): Yes No

Has the operator has received permission from the owner to use such system for discharges? (check one): Yes No, if so, explain, with an estimated timeframe for

obtaining permission:

Has the operator attached a summary of any additional requirements the owner of this system has specified? (check one): Yes No

Provide the expected start and end dates of discharge(s) (month/year):

Indicate if the discharge is expected to occur over a duration of: less than 12 months 12 months or more is an emergency discharge

Has the operator attached a site plan in accordance with the instructions in D, above? (check one): Yes No

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MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 17 of 24

2. Activity Category: (check all that apply) 3. Contamination Type Category: (check all that apply)

I – Petroleum-Related Site Remediation

II – Non-Petroleum-Related Site Remediation

III – Contaminated Site Dewatering

IV – Dewatering of Pipelines and Tanks

V – Aquifer Pump Testing

VI – Well Development/Rehabilitation

VII – Collection Structure Dewatering/Remediation

VIII – Dredge-Related Dewatering

a. If Activity Category I or II: (check all that apply)

A. Inorganics

B. Non-Halogenated Volatile Organic Compounds

C. Halogenated Volatile Organic Compounds

D. Non-Halogenated Semi-Volatile Organic Compounds

E. Halogenated Semi-Volatile Organic Compounds

F. Fuels Parameters

b. If Activity Category III, IV, V, VI, VII or VIII: (check either G or H)

G. Sites with Known

Contamination H. Sites with Unknown Contamination

c. If Category III-G, IV-G, V-G, VI-G,

VII-G or VIII-G: (check all that apply)

A. Inorganics

B. Non-Halogenated Volatile

Organic Compounds

C. Halogenated Volatile Organic

Compounds

D. Non-Halogenated Semi-Volatile

Organic Compounds

E. Halogenated Semi-Volatile

Organic Compounds

F. Fuels Parameters

d. If Category III-H, IV-H, V-H, VI-H, VII-H or

VIII-H Contamination Type Categories A through

F apply

Page 21: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 18 of 24

4. Influent and Effluent Characteristics

Parameter

Known

or

believed

absent

Known

or

believed

present

# of

samples

Test

method

(#)

Detection

limit

(µg/l)

Influent Effluent Limitations

Daily

maximum

(µg/l)

Daily

average

(µg/l)

TBEL WQBEL

A. Inorganics

Ammonia Report mg/L ---

Chloride Report µg/l ---

Total Residual Chlorine 0.2 mg/L

Total Suspended Solids 30 mg/L

Antimony 206 µg/L

Arsenic 104 µg/L

Cadmium 10.2 µg/L

Chromium III 323 µg/L

Chromium VI 323 µg/L

Copper 242 µg/L

Iron 5,000 µg/L

Lead 160 µg/L

Mercury 0.739 µg/L

Nickel 1,450 µg/L

Selenium 235.8 µg/L

Silver 35.1 µg/L

Zinc 420 µg/L

Cyanide 178 mg/L

B. Non-Halogenated VOCs

Total BTEX 100 µg/L ---

Benzene 5.0 µg/L ---

1,4 Dioxane 200 µg/L ---

Acetone 7.97 mg/L ---

Phenol 1,080 µg/L

Shauna
Typewritten Text
---
Page 22: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 19 of 24

Parameter

Known

or

believed

absent

Known

or

believed

present

# of

samples

Test

method

(#)

Detection

limit

(µg/l)

Influent Effluent Limitations

Daily

maximum

(µg/l)

Daily

average

(µg/l)

TBEL WQBEL

C. Halogenated VOCs

Carbon Tetrachloride 4.4 µg/L

1,2 Dichlorobenzene 600 µg/L ---

1,3 Dichlorobenzene 320 µg/L ---

1,4 Dichlorobenzene 5.0 µg/L ---

Total dichlorobenzene 763 µg/L in NH ---

1,1 Dichloroethane 70 µg/L ---

1,2 Dichloroethane 5.0 µg/L ---

1,1 Dichloroethylene 3.2 µg/L ---

Ethylene Dibromide 0.05 µg/L ---

Methylene Chloride 4.6 µg/L ---

1,1,1 Trichloroethane 200 µg/L ---

1,1,2 Trichloroethane 5.0 µg/L ---

Trichloroethylene 5.0 µg/L ---

Tetrachloroethylene 5.0 µg/L

cis-1,2 Dichloroethylene 70 µg/L ---

Vinyl Chloride 2.0 µg/L ---

D. Non-Halogenated SVOCs

Total Phthalates 190 µg/L

Diethylhexyl phthalate 101 µg/L

Total Group I PAHs 1.0 µg/L ---

Benzo(a)anthracene

As Total PAHs

Benzo(a)pyrene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Chrysene

Dibenzo(a,h)anthracene

Indeno(1,2,3-cd)pyrene

Page 23: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 20 of 24

Parameter

Known

or

believed

absent

Known

or

believed

present

# of

samples

Test

method

(#)

Detection

limit

(µg/l)

Influent Effluent Limitations

Daily

maximum

(µg/l)

Daily

average

(µg/l)

TBEL WQBEL

Total Group II PAHs 100 µg/L ---

Naphthalene 20 µg/L ---

E. Halogenated SVOCs

Total PCBs 0.000064 µg/L ---

Pentachlorophenol 1.0 µg/L ---

F. Fuels Parameters

Total Petroleum

Hydrocarbons 5.0 mg/L ---

Ethanol Report mg/L ---

Methyl-tert-Butyl Ether 70 µg/L

tert-Butyl Alcohol

120 µg/L in MA

40 µg/L in NH ---

tert-Amyl Methyl Ether

90 µg/L in MA

140 µg/L in NH ---

Other (i.e., pH, temperature, hardness, salinity, LC50, additional pollutants present); if so, specify:

Page 24: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 21 of 24

E. Treatment system information

1. 1. Indicate the type(s) of treatment that will be applied to effluent prior to discharge: (check all that apply)

Adsorption/Absorption Advanced Oxidation Processes Air Stripping Granulated Activated Carbon (“GAC”)/Liquid Phase Carbon Adsorption

Ion Exchange Precipitation/Coagulation/Flocculation Separation/Filtration Other; if so, specify:

2. 2. Provide a written description of all treatment system(s) or processes that will be applied to the effluent prior to discharge.

Identify each major treatment component (check any that apply):

Fractionation tanks Equalization tank Oil/water separator Mechanical filter Media filter

Chemical feed tank Air stripping unit Bag filter Other; if so, specify:

Indicate if either of the following will occur (check any that apply):

Chlorination De-chlorination

3. Provide the design flow capacity in gallons per minute (gpm) of the most limiting component.

Indicate the most limiting component:

Is use of a flow meter feasible? (check one): Yes No, if so, provide justification:

Provide the proposed maximum effluent flow in gpm.

Provide the average effluent flow in gpm.

If Activity Category IV applies, indicate the estimated total volume of water that will be discharged:

4. Has the operator attached a schematic of flow in accordance with the instructions in E, above? (check one): Yes No

Page 25: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 22 of 24

F. Chemical and additive information 1. Indicate the type(s) of chemical or additive that will be applied to effluent prior to discharge or that may otherwise be present in the discharge(s): (check all that apply)

Algaecides/biocides Antifoams Coagulants Corrosion/scale inhibitors Disinfectants Flocculants Neutralizing agents Oxidants Oxygen

scavengers pH conditioners Bioremedial agents, including microbes Chlorine or chemicals containing chlorine Other; if so, specify:

2. Provide the following information for each chemical/additive, using attachments, if necessary:

a. Product name, chemical formula, and manufacturer of the chemical/additive;

b. Purpose or use of the chemical/additive or remedial agent;

c. Material Safety Data Sheet (MSDS) and Chemical Abstracts Service (CAS) Registry number for each chemical/additive;

d. The frequency (hourly, daily, etc.), duration (hours, days), quantity (maximum and average), and method of application for the chemical/additive;

e. Any material compatibility risks for storage and/or use including the control measures used to minimize such risks; and

f. If available, the vendor's reported aquatic toxicity (NOAEL and/or LC50 in percent for aquatic organism(s)).

3. Has the operator attached an explanation which demonstrates that the addition of such chemicals/additives may be authorized under this general permit in accordance

with the instructions in F, above? (check one): Yes No; if no, has the operator attached data that demonstrates each of the 126 priority pollutants in CWA Section

307(a) and 40 CFR Part 423.15(j)(1) are non-detect in discharges with the addition of the proposed chemical/additive?

(check one): Yes No

G. Endangered Species Act eligibility determination 1. Indicate under which criterion the discharge(s) is eligible for coverage under this general permit:

FWS Criterion A: No endangered or threatened species or critical habitat are in proximity to the discharges or related activities or come in contact with the

“action area”.

FWS Criterion B: Formal or informal consultation with the FWS under section 7 of the ESA resulted in either a no jeopardy opinion (formal consultation)

or a written concurrence by FWS on a finding that the discharges and related activities are “not likely to adversely affect” listed species or critical habitat

(informal consultation). Has the operator completed consultation with FWS? (check one): Yes No; if no, is consultation underway? (check one):

Yes No

FWS Criterion C: Using the best scientific and commercial data available, the effect of the discharges and related activities on listed species and critical

habitat have been evaluated. Based on those evaluations, a determination is made by EPA, or by the operator and affirmed by EPA, that the discharges and

related activities will have “no effect” on any federally threatened or endangered listed species or designated critical habitat under the jurisdiction of the

FWS. This determination was made by: (check one) the operator EPA Other; if so, specify:

Page 26: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 23 of 24

NMFS Criterion: A determination made by EPA is affirmed by the operator that the discharges and related activities will have “no effect” or are “not likely

to adversely affect” any federally threatened or endangered listed species or critical habitat under the jurisdiction of NMFS and will not result in any take of

listed species. Has the operator previously completed consultation with NMFS? (check one): Yes No

2. Has the operator attached supporting documentation of ESA eligibility in accordance with the instructions in Appendix I, and G, above? (check one): Yes No

Does the supporting documentation include any written concurrence or finding provided by the Services? (check one): Yes No; if yes, attach.

H. National Historic Preservation Act eligibility determination 1. Indicate under which criterion the discharge(s) is eligible for coverage under this general permit:

Criterion A: No historic properties are present. The discharges and discharge-related activities (e.g., BMPs) do not have the potential to cause effects on

historic properties.

Criterion B: Historic properties are present. Discharges and discharge related activities do not have the potential to cause effects on historic properties.

Criterion C: Historic properties are present. The discharges and discharge-related activities have the potential to have an effect or will have an adverse

effect on historic properties.

2. Has the operator attached supporting documentation of NHPA eligibility in accordance with the instructions in H, above? (check one): Yes No

Does the supporting documentation include any written agreement with the State Historic Preservation Officer (SHPO), Tribal Historic Preservation Officer (TPHO), or

other tribal representative that outlines measures the operator will carry out to mitigate or prevent any adverse effects on historic properties? (check one): Yes No

I. Supplemental information Describe any supplemental information being provided with the NOI. Include attachments if required or otherwise necessary.

Has the operator attached data, including any laboratory case narrative and chain of custody used to support the application? (check one): Yes No

Has the operator attached the certification requirement for the Best Management Practices Plan (BMPP)? (check one): Yes No

Page 27: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

MAG910000 Appendix IV – Part 1 – NOI

NHG910000 Page 24 of 24

J. Certification requirement

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure

that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those

persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I have

no personal knowledge that the information submitted is other than true, accurate, and complete. I am aware that there are significant penalties for submitting false

information, including the possibility of fine and imprisonment for knowing violations.

BMPP certification statement:

Notification provided to the appropriate State, including a copy of this NOI, if required. Check one: Yes No

Notification provided to the municipality in which the discharge is located, including a copy of this NOI, if requested. Check one: Yes No

Notification provided to the owner of a private or municipal storm sewer system, if such system is used for site

discharges, including a copy of this NOI, if requested.

Permission obtained from the owner of a private or municipal storm sewer system, if such system is used for site

discharges. If yes, attach additional conditions. If no, attach explanation and timeframe for obtaining permission.

Check one: Yes No NA

Check one: Yes No NA Notification provided to the owner/operator of the area associated with activities covered by an additional discharge

permit(s). Additional discharge permit is (check one): RGP DGP CGP MSGP Individual NPDES permit

Other; if so, specify:

Check one: Yes No NA

Signature: Date:

Print Name and Title:

JSmith
Stamp
Page 28: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA

ATTACHMENT B

Page 29: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Buffalo10 Hazelwood DriveAmherst, NY 14228-2298Tel: (716)691-2600

TestAmerica Job ID: 480-118849-1Client Project/Site: Shell--Stoughton MA

For:Sovereign Consulting Inc.16 Chestnut StreetFoxborough, Massachusetts 02035

Attn: James Smith

Authorized for release by:6/15/2017 1:35:54 PMDenise Giglia, Project Management Assistant [email protected]

Designee for

Becky Mason, Project Manager II(413)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Page 30: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Table of Contents

Client: Sovereign Consulting Inc.Project/Site: Shell--Stoughton MA

TestAmerica Job ID: 480-118849-1

Page 2 of 31TestAmerica Buffalo

6/15/2017

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

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Page 31: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Definitions/GlossaryTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Qualifiers

General Chemistry

Qualifier Description

HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.

Qualifier

F1 MS and/or MSD Recovery is outside acceptance limits.

E Result exceeded calibration range.

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Buffalo

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Page 32: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Case NarrativeClient: Sovereign Consulting Inc. TestAmerica Job ID: 480-118849-1Project/Site: Shell--Stoughton MA

Job ID: 480-118849-1

Laboratory: TestAmerica Buffalo

Narrative

Job Narrative480-118849-1

Receipt

The samples were received on 6/2/2017 2:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 1.3º C.

Receipt Exceptions

The following sample was activated for Total Hardness analysis by the client on 6/6/17: MASSAPOAG BROOK (480-118849-3). This

analysis was not originally requested on the chain-of-custody (COC).

The following sample was activated for Total Hardness analysis by the client on 6/7/17: MW-1 (480-118849-1). This analysis was not originally requested on the chain-of-custody (COC).

GC/MS VOA Method 8260C: The continuing calibration verification (CCV) associated with batch 480-361004 recovered outside acceptance criteria, low biased, for Ethanol. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the associated samples were non-detect for this analyte, the data have been reported. The following sample is impacted: MW-1 (480-118849-1) and MASSAPOAG BROOK (480-118849-3).

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC/MS Semi VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

HPLC/IC Method 300.0: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW-1 (480-118849-1). Elevated reporting limits (RLs) are provided.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

General Chemistry

Method SM 4500 Cl G: This analysis is normally performed in the field and has a method-defined holding time of 15 minutes. The following sample has been qualified with the "HF" flag to indicate analysis was performed in the laboratory outside the 15 minute

timeframe: MW-1 (480-118849-1) and MASSAPOAG BROOK (480-118849-3).

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Organic Prep

Method 625: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 480-360259.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

TestAmerica BuffaloPage 4 of 31 6/15/2017

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Page 33: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Detection SummaryTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Client Sample ID: MW-1 Lab Sample ID: 480-118849-1

Hardness

RL

0.50 mg/L

MDLAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1200 SM 2340B

Chloride 10000 ug/L Total/NA20580000 300.0

Client Sample ID: TRIP BLANK Lab Sample ID: 480-118849-2

No Detections.

Client Sample ID: MASSAPOAG BROOK Lab Sample ID: 480-118849-3

Iron

RL

50 ug/L

MDLAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total

Recoverable

1580 200.7 Rev 4.4

Hardness 0.50 mg/L Total/NA145 SM 2340B

Chloride 500 ug/L Total/NA179000 F1 300.0

Ammonia 0.020 mg/L Total/NA10.052 350.1

Chlorine, Total Residual 0.020 mg/L Total/NA10.020 HF SM 4500 Cl G

TestAmerica Buffalo

This Detection Summary does not include radiochemical test results.

Page 5 of 31 6/15/2017

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Page 34: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Client Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Lab Sample ID: 480-118849-1Client Sample ID: MW-1Matrix: WaterDate Collected: 06/01/17 08:45

Date Received: 06/02/17 02:00

Method: 8260C - Volatile Organic Compounds by GC/MSRL MDL

1,4-Dioxane ND 40 ug/L 06/07/17 22:14 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.010 mg/L 06/07/17 22:14 1Acetone ND

1.0 ug/L 06/07/17 22:14 1Benzene ND

1.0 ug/L 06/07/17 22:14 1Ethylbenzene ND

2.0 ug/L 06/07/17 22:14 1m,p-Xylene ND

1.0 ug/L 06/07/17 22:14 1Methyl tert-butyl ether ND

1.0 ug/L 06/07/17 22:14 1o-Xylene ND

1.0 ug/L 06/07/17 22:14 1Toluene ND

10 ug/L 06/07/17 22:14 1t-Butyl alcohol ND

50 ug/L 06/07/17 22:14 1Ethanol ND

1,2-Dichloroethane-d4 (Surr) 105 77 - 120 06/07/17 22:14 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene (Surr) 107 06/07/17 22:14 173 - 120

Toluene-d8 (Surr) 96 06/07/17 22:14 180 - 120

Method: 625 - Semivolatile Organic Compounds (GC/MS)RL MDL

2,4,5-Trichlorophenol ND 5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 12,4,6-Trichlorophenol ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 12,4-Dichlorophenol ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 12,4-Dimethylphenol ND

10 ug/L 06/02/17 14:08 06/06/17 23:54 12,4-Dinitrophenol ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 12-Chlorophenol ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 12-Methylphenol ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 12-Nitrophenol ND

10 ug/L 06/02/17 14:08 06/06/17 23:54 13 & 4 Methylphenol ND

15 ug/L 06/02/17 14:08 06/06/17 23:54 14-Nitrophenol ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Acenaphthene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Acenaphthylene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Anthracene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Benzo(a)anthracene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Benzo(a)pyrene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Benzo(b)fluoranthene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Benzo(g,h,i) perylene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Benzo(k)fluoranthene ND

10 ug/L 06/02/17 14:08 06/06/17 23:54 1Diethylhexyl phthalate ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Butyl benzyl phthalate ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Chrysene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Di-n-butyl phthalate ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Di-n-octyl phthalate ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Dibenz(a,h)anthracene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Diethyl phthalate ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Dimethyl phthalate ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Fluoranthene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Fluorene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Indeno(1,2,3-cd)pyrene ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Naphthalene ND

10 ug/L 06/02/17 14:08 06/06/17 23:54 1Pentachlorophenol ND

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Phenanthrene ND

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Page 35: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Client Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Lab Sample ID: 480-118849-1Client Sample ID: MW-1Matrix: WaterDate Collected: 06/01/17 08:45

Date Received: 06/02/17 02:00

Method: 625 - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL

Phenol ND 5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

5.1 ug/L 06/02/17 14:08 06/06/17 23:54 1Pyrene ND

2,4,6-Tribromophenol (Surr) 84 52 - 151 06/02/17 14:08 06/06/17 23:54 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

2-Fluorophenol (Surr) 51 06/02/17 14:08 06/06/17 23:54 117 - 120

Nitrobenzene-d5 (Surr) 78 06/02/17 14:08 06/06/17 23:54 142 - 120

p-Terphenyl-d14 83 06/02/17 14:08 06/06/17 23:54 122 - 125

Phenol-d5 (Surr) 36 06/02/17 14:08 06/06/17 23:54 110 - 120

Method: 200.7 Rev 4.4 - Metals (ICP) - Total RecoverableRL MDL

Antimony ND 20 ug/L 06/09/17 11:10 06/12/17 23:12 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

15 ug/L 06/09/17 11:10 06/12/17 23:12 1Arsenic ND

50 ug/L 06/09/17 11:10 06/12/17 23:12 1Iron ND

Method: 200.7 Rev 4.4 - Metals (ICP) - DissolvedRL MDL

Cadmium ND 2.0 ug/L 06/08/17 11:03 06/09/17 13:57 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

4.0 ug/L 06/08/17 11:03 06/09/17 13:57 1Chromium ND

10 ug/L 06/08/17 11:03 06/09/17 13:57 1Copper ND

10 ug/L 06/08/17 11:03 06/09/17 13:57 1Lead ND

10 ug/L 06/08/17 11:03 06/09/17 13:57 1Nickel ND

25 ug/L 06/08/17 11:03 06/09/17 13:57 1Selenium ND

6.0 ug/L 06/08/17 11:03 06/09/17 13:57 1Silver ND

10 ug/L 06/08/17 11:03 06/09/17 13:57 1Zinc ND

Method: 245.1 - Mercury (CVAA) - DissolvedRL MDL

Mercury ND 0.00020 mg/L 06/08/17 09:30 06/08/17 14:30 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

Method: SM 2340B - Total Hardness (as CaCO3) by calculationRL MDL

Hardness 200 0.50 mg/L 06/15/17 10:20 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

General ChemistryRL MDL

TPH ND 5.0 mg/L 06/07/17 09:06 06/07/17 09:06 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

10000 ug/L 06/09/17 11:44 20Chloride 580000

0.020 mg/L 06/03/17 17:54 1Ammonia ND

10 ug/L 06/15/17 10:26 1Cr (III) ND

0.020 mg/L 06/07/17 19:00 1Chlorine, Total Residual ND HF

RL RL

Total Suspended Solids ND 4.0 mg/L 06/05/17 00:54 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

General Chemistry - DissolvedRL MDL

Chromium, hexavalent ND 10 ug/L 06/02/17 05:56 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

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Page 36: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Client Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Lab Sample ID: 480-118849-2Client Sample ID: TRIP BLANKMatrix: WaterDate Collected: 06/01/17 06:00

Date Received: 06/02/17 02:00

Method: 8260C - Volatile Organic Compounds by GC/MSRL MDL

1,4-Dioxane ND 40 ug/L 06/06/17 02:52 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.010 mg/L 06/06/17 02:52 1Acetone ND

1.0 ug/L 06/06/17 02:52 1Benzene ND

1.0 ug/L 06/06/17 02:52 1Ethylbenzene ND

2.0 ug/L 06/06/17 02:52 1m,p-Xylene ND

1.0 ug/L 06/06/17 02:52 1Methyl tert-butyl ether ND

1.0 ug/L 06/06/17 02:52 1o-Xylene ND

1.0 ug/L 06/06/17 02:52 1Toluene ND

10 ug/L 06/06/17 02:52 1t-Butyl alcohol ND

50 ug/L 06/06/17 02:52 1Ethanol ND

1,2-Dichloroethane-d4 (Surr) 111 77 - 120 06/06/17 02:52 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene (Surr) 101 06/06/17 02:52 173 - 120

Toluene-d8 (Surr) 95 06/06/17 02:52 180 - 120

Lab Sample ID: 480-118849-3Client Sample ID: MASSAPOAG BROOKMatrix: WaterDate Collected: 06/01/17 11:20

Date Received: 06/02/17 02:00

Method: 8260C - Volatile Organic Compounds by GC/MSRL MDL

1,4-Dioxane ND 40 ug/L 06/07/17 22:37 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.010 mg/L 06/07/17 22:37 1Acetone ND

1.0 ug/L 06/07/17 22:37 1Benzene ND

1.0 ug/L 06/07/17 22:37 1Ethylbenzene ND

2.0 ug/L 06/07/17 22:37 1m,p-Xylene ND

1.0 ug/L 06/07/17 22:37 1Methyl tert-butyl ether ND

1.0 ug/L 06/07/17 22:37 1o-Xylene ND

1.0 ug/L 06/07/17 22:37 1Toluene ND

10 ug/L 06/07/17 22:37 1t-Butyl alcohol ND

50 ug/L 06/07/17 22:37 1Ethanol ND

1,2-Dichloroethane-d4 (Surr) 108 77 - 120 06/07/17 22:37 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene (Surr) 109 06/07/17 22:37 173 - 120

Toluene-d8 (Surr) 95 06/07/17 22:37 180 - 120

Method: 625 - Semivolatile Organic Compounds (GC/MS)RL MDL

2,4,5-Trichlorophenol ND 5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 12,4,6-Trichlorophenol ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 12,4-Dichlorophenol ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 12,4-Dimethylphenol ND

10 ug/L 06/02/17 14:08 06/07/17 00:20 12,4-Dinitrophenol ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 12-Chlorophenol ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 12-Methylphenol ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 12-Nitrophenol ND

10 ug/L 06/02/17 14:08 06/07/17 00:20 13 & 4 Methylphenol ND

15 ug/L 06/02/17 14:08 06/07/17 00:20 14-Nitrophenol ND

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Page 37: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Client Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Lab Sample ID: 480-118849-3Client Sample ID: MASSAPOAG BROOKMatrix: WaterDate Collected: 06/01/17 11:20

Date Received: 06/02/17 02:00

Method: 625 - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL

Acenaphthene ND 5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Acenaphthylene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Anthracene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Benzo(a)anthracene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Benzo(a)pyrene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Benzo(b)fluoranthene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Benzo(g,h,i) perylene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Benzo(k)fluoranthene ND

10 ug/L 06/02/17 14:08 06/07/17 00:20 1Diethylhexyl phthalate ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Butyl benzyl phthalate ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Chrysene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Di-n-butyl phthalate ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Di-n-octyl phthalate ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Dibenz(a,h)anthracene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Diethyl phthalate ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Dimethyl phthalate ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Fluoranthene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Fluorene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Indeno(1,2,3-cd)pyrene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Naphthalene ND

10 ug/L 06/02/17 14:08 06/07/17 00:20 1Pentachlorophenol ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Phenanthrene ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Phenol ND

5.2 ug/L 06/02/17 14:08 06/07/17 00:20 1Pyrene ND

2,4,6-Tribromophenol (Surr) 83 52 - 151 06/02/17 14:08 06/07/17 00:20 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

2-Fluorophenol (Surr) 48 06/02/17 14:08 06/07/17 00:20 117 - 120

Nitrobenzene-d5 (Surr) 80 06/02/17 14:08 06/07/17 00:20 142 - 120

p-Terphenyl-d14 83 06/02/17 14:08 06/07/17 00:20 122 - 125

Phenol-d5 (Surr) 33 06/02/17 14:08 06/07/17 00:20 110 - 120

Method: 200.7 Rev 4.4 - Metals (ICP) - Total RecoverableRL MDL

Antimony ND 20 ug/L 06/09/17 11:10 06/12/17 23:15 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

15 ug/L 06/09/17 11:10 06/12/17 23:15 1Arsenic ND

50 ug/L 06/09/17 11:10 06/12/17 23:15 1Iron 580

Method: 200.7 Rev 4.4 - Metals (ICP) - DissolvedRL MDL

Cadmium ND 2.0 ug/L 06/08/17 11:03 06/09/17 14:01 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

4.0 ug/L 06/08/17 11:03 06/09/17 14:01 1Chromium ND

10 ug/L 06/08/17 11:03 06/09/17 14:01 1Copper ND

10 ug/L 06/08/17 11:03 06/09/17 14:01 1Lead ND

10 ug/L 06/08/17 11:03 06/09/17 14:01 1Nickel ND

25 ug/L 06/08/17 11:03 06/09/17 14:01 1Selenium ND

6.0 ug/L 06/08/17 11:03 06/09/17 14:01 1Silver ND

10 ug/L 06/08/17 11:03 06/09/17 14:01 1Zinc ND

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Page 38: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Client Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Lab Sample ID: 480-118849-3Client Sample ID: MASSAPOAG BROOKMatrix: WaterDate Collected: 06/01/17 11:20

Date Received: 06/02/17 02:00

Method: 245.1 - Mercury (CVAA) - DissolvedRL MDL

Mercury ND 0.00020 mg/L 06/08/17 09:30 06/08/17 14:32 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

Method: SM 2340B - Total Hardness (as CaCO3) by calculationRL MDL

Hardness 45 0.50 mg/L 06/15/17 10:22 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

General ChemistryRL MDL

TPH ND 4.7 mg/L 06/07/17 09:06 06/07/17 09:06 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

500 ug/L 06/08/17 00:17 1Chloride 79000 F1

0.020 mg/L 06/07/17 17:31 1Ammonia 0.052

10 ug/L 06/15/17 10:26 1Cr (III) ND

0.020 mg/L 06/07/17 19:00 1Chlorine, Total Residual 0.020 HF

RL RL

Total Suspended Solids ND 4.0 mg/L 06/05/17 00:54 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

General Chemistry - DissolvedRL MDL

Chromium, hexavalent ND 10 ug/L 06/02/17 05:56 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

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Page 39: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Surrogate SummaryTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: 8260C - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (77-120) (73-120) (80-120)

12DCE BFB TOL

105 107 96480-118849-1

Percent Surrogate Recovery (Acceptance Limits)

MW-1

111 101 95480-118849-2 TRIP BLANK

108 109 95480-118849-3 MASSAPOAG BROOK

109 111 97LCS 480-360557/4 Lab Control Sample

107 112 97LCS 480-361004/4 Lab Control Sample

114 108 96MB 480-360557/6 Method Blank

106 110 97MB 480-361004/6 Method Blank

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

TOL = Toluene-d8 (Surr)

Method: 625 - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (52-151) (17-120) (42-120) (22-125) (10-120)

TBP 2FP NBZ TPH PHL

84 51 78 83 36480-118849-1

Percent Surrogate Recovery (Acceptance Limits)

MW-1

83 48 80 3383480-118849-3 MASSAPOAG BROOK

91 54 84 3992LCS 480-360259/2-A Lab Control Sample

88 52 84 3889LCSD 480-360259/3-A Lab Control Sample Dup

63 48 82 3792MB 480-360259/1-A Method Blank

Surrogate Legend

TBP = 2,4,6-Tribromophenol (Surr)

2FP = 2-Fluorophenol (Surr)

NBZ = Nitrobenzene-d5 (Surr)

TPH = p-Terphenyl-d14

PHL = Phenol-d5 (Surr)

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Page 40: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: 8260C - Volatile Organic Compounds by GC/MS

Client Sample ID: Method BlankLab Sample ID: MB 480-360557/6Matrix: Water Prep Type: Total/NAAnalysis Batch: 360557

RL MDL

1,4-Dioxane ND 40 ug/L 06/05/17 23:27 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 0.010 mg/L 06/05/17 23:27 1Acetone

ND 1.0 ug/L 06/05/17 23:27 1Benzene

ND 1.0 ug/L 06/05/17 23:27 1Ethylbenzene

ND 2.0 ug/L 06/05/17 23:27 1m,p-Xylene

ND 1.0 ug/L 06/05/17 23:27 1Methyl tert-butyl ether

ND 1.0 ug/L 06/05/17 23:27 1o-Xylene

ND 1.0 ug/L 06/05/17 23:27 1Toluene

ND 10 ug/L 06/05/17 23:27 1t-Butyl alcohol

ND 50 ug/L 06/05/17 23:27 1Ethanol

1,2-Dichloroethane-d4 (Surr) 114 77 - 120 06/05/17 23:27 1

MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

108 06/05/17 23:27 14-Bromofluorobenzene (Surr) 73 - 120

96 06/05/17 23:27 1Toluene-d8 (Surr) 80 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-360557/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 360557

1,4-Dioxane 500 469 ug/L 94 50 - 150

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Acetone 0.125 0.165 mg/L 132 56 - 142

Benzene 25.0 23.6 ug/L 94 71 - 124

Ethylbenzene 25.0 23.2 ug/L 93 77 - 123

m,p-Xylene 25.0 23.0 ug/L 92 76 - 122

Methyl tert-butyl ether 25.0 25.3 ug/L 101 77 - 120

o-Xylene 25.0 23.5 ug/L 94 76 - 122

Toluene 25.0 22.7 ug/L 91 80 - 122

t-Butyl alcohol 250 291 ug/L 117 75 - 125

1,2-Dichloroethane-d4 (Surr) 77 - 120

Surrogate

109

LCS LCS

Qualifier Limits%Recovery

1114-Bromofluorobenzene (Surr) 73 - 120

97Toluene-d8 (Surr) 80 - 120

Client Sample ID: Method BlankLab Sample ID: MB 480-361004/6Matrix: Water Prep Type: Total/NAAnalysis Batch: 361004

RL MDL

1,4-Dioxane ND 40 ug/L 06/07/17 21:17 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 0.010 mg/L 06/07/17 21:17 1Acetone

ND 1.0 ug/L 06/07/17 21:17 1Benzene

ND 1.0 ug/L 06/07/17 21:17 1Ethylbenzene

ND 2.0 ug/L 06/07/17 21:17 1m,p-Xylene

ND 1.0 ug/L 06/07/17 21:17 1Methyl tert-butyl ether

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Page 41: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)

Client Sample ID: Method BlankLab Sample ID: MB 480-361004/6Matrix: Water Prep Type: Total/NAAnalysis Batch: 361004

RL MDL

o-Xylene ND 1.0 ug/L 06/07/17 21:17 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 1.0 ug/L 06/07/17 21:17 1Toluene

ND 10 ug/L 06/07/17 21:17 1t-Butyl alcohol

ND 50 ug/L 06/07/17 21:17 1Ethanol

1,2-Dichloroethane-d4 (Surr) 106 77 - 120 06/07/17 21:17 1

MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

110 06/07/17 21:17 14-Bromofluorobenzene (Surr) 73 - 120

97 06/07/17 21:17 1Toluene-d8 (Surr) 80 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-361004/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 361004

1,4-Dioxane 500 424 ug/L 85 50 - 150

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Acetone 0.125 0.134 mg/L 107 56 - 142

Benzene 25.0 21.8 ug/L 87 71 - 124

Ethylbenzene 25.0 22.2 ug/L 89 77 - 123

m,p-Xylene 25.0 22.1 ug/L 88 76 - 122

Methyl tert-butyl ether 25.0 24.1 ug/L 96 77 - 120

o-Xylene 25.0 21.8 ug/L 87 76 - 122

Toluene 25.0 21.3 ug/L 85 80 - 122

t-Butyl alcohol 250 255 ug/L 102 75 - 125

1,2-Dichloroethane-d4 (Surr) 77 - 120

Surrogate

107

LCS LCS

Qualifier Limits%Recovery

1124-Bromofluorobenzene (Surr) 73 - 120

97Toluene-d8 (Surr) 80 - 120

Method: 625 - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 480-360259/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360707 Prep Batch: 360259

RL MDL

2,4,5-Trichlorophenol ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 12,4,6-Trichlorophenol

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 12,4-Dichlorophenol

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 12,4-Dimethylphenol

ND 10 ug/L 06/02/17 14:08 06/06/17 21:16 12,4-Dinitrophenol

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 12-Chlorophenol

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 12-Methylphenol

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 12-Nitrophenol

ND 10 ug/L 06/02/17 14:08 06/06/17 21:16 13 & 4 Methylphenol

ND 15 ug/L 06/02/17 14:08 06/06/17 21:16 14-Nitrophenol

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Page 42: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: 625 - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Method BlankLab Sample ID: MB 480-360259/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360707 Prep Batch: 360259

RL MDL

Acenaphthene ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Acenaphthylene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Anthracene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Benzo(a)anthracene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Benzo(a)pyrene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Benzo(b)fluoranthene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Benzo(g,h,i) perylene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Benzo(k)fluoranthene

ND 10 ug/L 06/02/17 14:08 06/06/17 21:16 1Diethylhexyl phthalate

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Butyl benzyl phthalate

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Chrysene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Di-n-butyl phthalate

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Di-n-octyl phthalate

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Dibenz(a,h)anthracene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Diethyl phthalate

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Dimethyl phthalate

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Fluoranthene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Fluorene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Indeno(1,2,3-cd)pyrene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Naphthalene

ND 10 ug/L 06/02/17 14:08 06/06/17 21:16 1Pentachlorophenol

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Phenanthrene

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Phenol

ND 5.0 ug/L 06/02/17 14:08 06/06/17 21:16 1Pyrene

2,4,6-Tribromophenol (Surr) 63 52 - 151 06/06/17 21:16 1

MB MB

Surrogate

06/02/17 14:08

Dil FacPrepared AnalyzedQualifier Limits%Recovery

48 06/02/17 14:08 06/06/17 21:16 12-Fluorophenol (Surr) 17 - 120

82 06/02/17 14:08 06/06/17 21:16 1Nitrobenzene-d5 (Surr) 42 - 120

92 06/02/17 14:08 06/06/17 21:16 1p-Terphenyl-d14 22 - 125

37 06/02/17 14:08 06/06/17 21:16 1Phenol-d5 (Surr) 10 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-360259/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360707 Prep Batch: 360259

2,4,5-Trichlorophenol 50.0 46.4 ug/L 93 45 - 132

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

2,4,6-Trichlorophenol 50.0 43.0 ug/L 86 37 - 144

2,4-Dichlorophenol 50.0 44.6 ug/L 89 39 - 135

2,4-Dimethylphenol 50.0 43.8 ug/L 88 32 - 119

2,4-Dinitrophenol 100 97.8 ug/L 98 1 - 191

2-Chlorophenol 50.0 38.6 ug/L 77 23 - 134

2-Methylphenol 50.0 37.0 ug/L 74 45 - 120

2-Nitrophenol 50.0 41.7 ug/L 83 29 - 182

3 & 4 Methylphenol 50.0 35.7 ug/L 71 48 - 120

4-Nitrophenol 100 51.2 ug/L 51 1 - 132

Acenaphthene 50.0 43.8 ug/L 88 47 - 145

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Page 43: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: 625 - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-360259/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360707 Prep Batch: 360259

Acenaphthylene 50.0 44.8 ug/L 90 33 - 145

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Anthracene 50.0 47.8 ug/L 96 27 - 133

Benzo(a)anthracene 50.0 49.1 ug/L 98 33 - 143

Benzo(a)pyrene 50.0 48.5 ug/L 97 17 - 163

Benzo(b)fluoranthene 50.0 48.4 ug/L 97 24 - 159

Benzo(g,h,i) perylene 50.0 45.2 ug/L 90 1 - 219

Benzo(k)fluoranthene 50.0 49.7 ug/L 99 11 - 162

Diethylhexyl phthalate 50.0 48.0 ug/L 96 8 - 158

Butyl benzyl phthalate 50.0 47.9 ug/L 96 1 - 152

Chrysene 50.0 47.7 ug/L 95 17 - 168

Di-n-butyl phthalate 50.0 48.7 ug/L 97 1 - 118

Di-n-octyl phthalate 50.0 50.2 ug/L 100 4 - 146

Dibenz(a,h)anthracene 50.0 47.1 ug/L 94 1 - 227

Diethyl phthalate 50.0 46.7 ug/L 93 1 - 114

Dimethyl phthalate 50.0 46.3 ug/L 93 1 - 112

Fluoranthene 50.0 49.6 ug/L 99 26 - 137

Fluorene 50.0 44.4 ug/L 89 59 - 121

Indeno(1,2,3-cd)pyrene 50.0 46.6 ug/L 93 1 - 171

Naphthalene 50.0 39.7 ug/L 79 21 - 133

Pentachlorophenol 100 94.2 ug/L 94 14 - 176

Phenanthrene 50.0 48.6 ug/L 97 54 - 120

Phenol 50.0 22.1 ug/L 44 5 - 112

Pyrene 50.0 48.3 ug/L 97 52 - 115

2,4,6-Tribromophenol (Surr) 52 - 151

Surrogate

91

LCS LCS

Qualifier Limits%Recovery

542-Fluorophenol (Surr) 17 - 120

84Nitrobenzene-d5 (Surr) 42 - 120

92p-Terphenyl-d14 22 - 125

39Phenol-d5 (Surr) 10 - 120

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 480-360259/3-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360707 Prep Batch: 360259

2,4,5-Trichlorophenol 50.0 42.2 ug/L 84 45 - 132 10 21

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

2,4,6-Trichlorophenol 50.0 41.5 ug/L 83 37 - 144 4 20

2,4-Dichlorophenol 50.0 43.3 ug/L 87 39 - 135 3 23

2,4-Dimethylphenol 50.0 42.6 ug/L 85 32 - 119 3 18

2,4-Dinitrophenol 100 95.8 ug/L 96 1 - 191 2 29

2-Chlorophenol 50.0 36.9 ug/L 74 23 - 134 4 26

2-Methylphenol 50.0 37.0 ug/L 74 45 - 120 0 30

2-Nitrophenol 50.0 41.9 ug/L 84 29 - 182 1 28

3 & 4 Methylphenol 50.0 34.6 ug/L 69 48 - 120 3 30

4-Nitrophenol 100 48.0 ug/L 48 1 - 132 6 24

Acenaphthene 50.0 42.2 ug/L 84 47 - 145 4 25

Acenaphthylene 50.0 42.9 ug/L 86 33 - 145 4 22

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Page 44: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: 625 - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 480-360259/3-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360707 Prep Batch: 360259

Anthracene 50.0 45.8 ug/L 92 27 - 133 4 15

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

Benzo(a)anthracene 50.0 46.7 ug/L 93 33 - 143 5 15

Benzo(a)pyrene 50.0 45.9 ug/L 92 17 - 163 6 15

Benzo(b)fluoranthene 50.0 45.4 ug/L 91 24 - 159 6 17

Benzo(g,h,i) perylene 50.0 45.1 ug/L 90 1 - 219 0 19

Benzo(k)fluoranthene 50.0 44.7 ug/L 89 11 - 162 11 19

Diethylhexyl phthalate 50.0 47.1 ug/L 94 8 - 158 2 15

Butyl benzyl phthalate 50.0 46.1 ug/L 92 1 - 152 4 15

Chrysene 50.0 45.7 ug/L 91 17 - 168 4 15

Di-n-butyl phthalate 50.0 47.6 ug/L 95 1 - 118 2 15

Di-n-octyl phthalate 50.0 46.6 ug/L 93 4 - 146 7 15

Dibenz(a,h)anthracene 50.0 44.4 ug/L 89 1 - 227 6 18

Diethyl phthalate 50.0 44.7 ug/L 89 1 - 114 4 15

Dimethyl phthalate 50.0 45.4 ug/L 91 1 - 112 2 15

Fluoranthene 50.0 47.2 ug/L 94 26 - 137 5 15

Fluorene 50.0 43.1 ug/L 86 59 - 121 3 18

Indeno(1,2,3-cd)pyrene 50.0 44.9 ug/L 90 1 - 171 4 17

Naphthalene 50.0 38.7 ug/L 77 21 - 133 3 31

Pentachlorophenol 100 91.3 ug/L 91 14 - 176 3 21

Phenanthrene 50.0 46.7 ug/L 93 54 - 120 4 16

Phenol 50.0 21.1 ug/L 42 5 - 112 5 36

Pyrene 50.0 46.6 ug/L 93 52 - 115 4 15

2,4,6-Tribromophenol (Surr) 52 - 151

Surrogate

88

LCSD LCSD

Qualifier Limits%Recovery

522-Fluorophenol (Surr) 17 - 120

84Nitrobenzene-d5 (Surr) 42 - 120

89p-Terphenyl-d14 22 - 125

38Phenol-d5 (Surr) 10 - 120

Method: 200.7 Rev 4.4 - Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: MB 480-361115/1-AMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 361604 Prep Batch: 361115

RL MDL

Cadmium ND 2.0 ug/L 06/08/17 11:03 06/09/17 13:10 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 4.0 ug/L 06/08/17 11:03 06/09/17 13:10 1Chromium

ND 10 ug/L 06/08/17 11:03 06/09/17 13:10 1Copper

ND 10 ug/L 06/08/17 11:03 06/09/17 13:10 1Lead

ND 10 ug/L 06/08/17 11:03 06/09/17 13:10 1Nickel

ND 25 ug/L 06/08/17 11:03 06/09/17 13:10 1Selenium

ND 6.0 ug/L 06/08/17 11:03 06/09/17 13:10 1Silver

ND 10 ug/L 06/08/17 11:03 06/09/17 13:10 1Zinc

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Page 45: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: 200.7 Rev 4.4 - Metals (ICP) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-361115/2-AMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 361604 Prep Batch: 361115

Cadmium 200 206 ug/L 103 85 - 115

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Chromium 200 206 ug/L 103 85 - 115

Copper 200 206 ug/L 103 85 - 115

Lead 200 206 ug/L 103 85 - 115

Nickel 200 196 ug/L 98 85 - 115

Selenium 200 203 ug/L 102 85 - 115

Silver 50.0 49.1 ug/L 98 85 - 115

Zinc 200 210 ug/L 105 85 - 115

Client Sample ID: Method BlankLab Sample ID: MB 480-361305/1-AMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 361793 Prep Batch: 361305

RL MDL

Antimony ND 20 ug/L 06/09/17 11:10 06/12/17 22:11 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 15 ug/L 06/09/17 11:10 06/12/17 22:11 1Arsenic

ND 50 ug/L 06/09/17 11:10 06/12/17 22:11 1Iron

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-361305/2-AMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 361793 Prep Batch: 361305

Antimony 200 211 ug/L 106 85 - 115

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Arsenic 200 206 ug/L 103 85 - 115

Iron 10000 10300 ug/L 103 85 - 115

Method: 245.1 - Mercury (CVAA)

Client Sample ID: Method BlankLab Sample ID: MB 480-361074/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 361228 Prep Batch: 361074

RL MDL

Mercury ND 0.00020 mg/L 06/08/17 09:30 06/08/17 13:44 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-361074/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 361228 Prep Batch: 361074

Mercury 0.00667 0.00645 mg/L 97 85 - 115

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

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Page 46: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: 1664A - HEM and SGT-HEM

Client Sample ID: Method BlankLab Sample ID: MB 480-360840/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360951 Prep Batch: 360840

RL MDL

TPH ND 5.0 mg/L 06/07/17 09:06 06/07/17 09:06 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-360840/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360951 Prep Batch: 360840

TPH 19.9 15.0 mg/L 75 64 - 132

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Method: 300.0 - Anions, Ion Chromatography

Client Sample ID: Method BlankLab Sample ID: MB 480-360953/28Matrix: Water Prep Type: Total/NAAnalysis Batch: 360953

RL MDL

Chloride ND 500 ug/L 06/07/17 21:42 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-360953/27Matrix: Water Prep Type: Total/NAAnalysis Batch: 360953

Chloride 50000 50500 ug/L 101 90 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: MASSAPOAG BROOKLab Sample ID: 480-118849-3 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 360953

Chloride 79000 F1 50000 113000 E F1 ug/L 67 81 - 120

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Method BlankLab Sample ID: MB 480-361248/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 361248

RL MDL

Chloride ND 500 ug/L 06/09/17 09:59 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-361248/3Matrix: Water Prep Type: Total/NAAnalysis Batch: 361248

Chloride 50000 50700 ug/L 101 90 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

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Page 47: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: 350.1 - Nitrogen, Ammonia

Client Sample ID: Method BlankLab Sample ID: MB 480-360366/27Matrix: Water Prep Type: Total/NAAnalysis Batch: 360366

RL MDL

Ammonia ND 0.020 mg/L 06/03/17 17:50 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Method BlankLab Sample ID: MB 480-360366/50Matrix: Water Prep Type: Total/NAAnalysis Batch: 360366

RL MDL

Ammonia ND 0.020 mg/L 06/03/17 18:10 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-360366/28Matrix: Water Prep Type: Total/NAAnalysis Batch: 360366

Ammonia 1.00 1.05 mg/L 105 90 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-360366/51Matrix: Water Prep Type: Total/NAAnalysis Batch: 360366

Ammonia 1.00 1.04 mg/L 104 90 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: Method BlankLab Sample ID: MB 480-361013/27Matrix: Water Prep Type: Total/NAAnalysis Batch: 361013

RL MDL

Ammonia ND 0.020 mg/L 06/07/17 17:39 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Method BlankLab Sample ID: MB 480-361013/3Matrix: Water Prep Type: Total/NAAnalysis Batch: 361013

RL MDL

Ammonia ND 0.020 mg/L 06/07/17 17:18 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Method BlankLab Sample ID: MB 480-361013/75Matrix: Water Prep Type: Total/NAAnalysis Batch: 361013

RL MDL

Ammonia ND 0.020 mg/L 06/07/17 18:21 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-361013/28Matrix: Water Prep Type: Total/NAAnalysis Batch: 361013

Ammonia 1.00 1.04 mg/L 104 90 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

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Page 48: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-361013/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 361013

Ammonia 1.00 1.05 mg/L 105 90 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-361013/76Matrix: Water Prep Type: Total/NAAnalysis Batch: 361013

Ammonia 1.00 1.04 mg/L 104 90 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Method: SM 2540D - Solids, Total Suspended (TSS)

Client Sample ID: Method BlankLab Sample ID: MB 480-360405/1Matrix: Water Prep Type: Total/NAAnalysis Batch: 360405

RL RL

Total Suspended Solids ND 1.0 mg/L 06/05/17 00:54 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-360405/2Matrix: Water Prep Type: Total/NAAnalysis Batch: 360405

Total Suspended Solids 279 276 mg/L 99 88 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Method: SM 3500 CR D - Chromium, Hexavalent

Client Sample ID: Method BlankLab Sample ID: MB 480-360135/3Matrix: Water Prep Type: Total/NAAnalysis Batch: 360135

RL MDL

Chromium, hexavalent ND 10 ug/L 06/02/17 05:56 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-360135/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 360135

Chromium, hexavalent 50.0 56.8 ug/L 114 85 - 115

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Method: SM 4500 Cl G - Chlorine, Residual

Client Sample ID: Method BlankLab Sample ID: MB 480-361021/3Matrix: Water Prep Type: Total/NAAnalysis Batch: 361021

RL MDL

Chlorine, Total Residual ND 0.020 mg/L 06/07/17 19:00 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

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Page 49: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Sample ResultsTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method: SM 4500 Cl G - Chlorine, Residual (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-361021/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 361021

Chlorine, Total Residual 0.930 0.940 mg/L 101 90 - 110

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: MW-1Lab Sample ID: 480-118849-1 DUMatrix: Water Prep Type: Total/NAAnalysis Batch: 361021

Chlorine, Total Residual ND HF ND mg/L NC 20

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

TestAmerica Buffalo

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Page 50: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Association SummaryTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

GC/MS VOA

Analysis Batch: 360557

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 8260C480-118849-2 TRIP BLANK Total/NA

Water 8260CMB 480-360557/6 Method Blank Total/NA

Water 8260CLCS 480-360557/4 Lab Control Sample Total/NA

Analysis Batch: 361004

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 8260C480-118849-1 MW-1 Total/NA

Water 8260C480-118849-3 MASSAPOAG BROOK Total/NA

Water 8260CMB 480-361004/6 Method Blank Total/NA

Water 8260CLCS 480-361004/4 Lab Control Sample Total/NA

GC/MS Semi VOA

Prep Batch: 360259

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 625480-118849-1 MW-1 Total/NA

Water 625480-118849-3 MASSAPOAG BROOK Total/NA

Water 625MB 480-360259/1-A Method Blank Total/NA

Water 625LCS 480-360259/2-A Lab Control Sample Total/NA

Water 625LCSD 480-360259/3-A Lab Control Sample Dup Total/NA

Analysis Batch: 360707

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 625 360259480-118849-1 MW-1 Total/NA

Water 625 360259480-118849-3 MASSAPOAG BROOK Total/NA

Water 625 360259MB 480-360259/1-A Method Blank Total/NA

Water 625 360259LCS 480-360259/2-A Lab Control Sample Total/NA

Water 625 360259LCSD 480-360259/3-A Lab Control Sample Dup Total/NA

Metals

Prep Batch: 361074

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 245.1480-118849-1 MW-1 Dissolved

Water 245.1480-118849-3 MASSAPOAG BROOK Dissolved

Water 245.1MB 480-361074/1-A Method Blank Total/NA

Water 245.1LCS 480-361074/2-A Lab Control Sample Total/NA

Prep Batch: 361115

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 200.7480-118849-1 MW-1 Dissolved

Water 200.7480-118849-3 MASSAPOAG BROOK Dissolved

Water 200.7MB 480-361115/1-A Method Blank Total Recoverable

Water 200.7LCS 480-361115/2-A Lab Control Sample Total Recoverable

Analysis Batch: 361228

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 245.1 361074480-118849-1 MW-1 Dissolved

Water 245.1 361074480-118849-3 MASSAPOAG BROOK Dissolved

Water 245.1 361074MB 480-361074/1-A Method Blank Total/NA

TestAmerica Buffalo

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Page 51: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Association SummaryTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Metals (Continued)

Analysis Batch: 361228 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 245.1 361074LCS 480-361074/2-A Lab Control Sample Total/NA

Prep Batch: 361305

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 200.7480-118849-1 MW-1 Total Recoverable

Water 200.7480-118849-3 MASSAPOAG BROOK Total Recoverable

Water 200.7MB 480-361305/1-A Method Blank Total Recoverable

Water 200.7LCS 480-361305/2-A Lab Control Sample Total Recoverable

Analysis Batch: 361604

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 200.7 Rev 4.4 361115480-118849-1 MW-1 Dissolved

Water 200.7 Rev 4.4 361115480-118849-3 MASSAPOAG BROOK Dissolved

Water 200.7 Rev 4.4 361115MB 480-361115/1-A Method Blank Total Recoverable

Water 200.7 Rev 4.4 361115LCS 480-361115/2-A Lab Control Sample Total Recoverable

Analysis Batch: 361793

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 200.7 Rev 4.4 361305480-118849-1 MW-1 Total Recoverable

Water 200.7 Rev 4.4 361305480-118849-3 MASSAPOAG BROOK Total Recoverable

Water 200.7 Rev 4.4 361305MB 480-361305/1-A Method Blank Total Recoverable

Water 200.7 Rev 4.4 361305LCS 480-361305/2-A Lab Control Sample Total Recoverable

Analysis Batch: 362174

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water SM 2340B480-118849-1 MW-1 Total/NA

Water SM 2340B480-118849-3 MASSAPOAG BROOK Total/NA

General Chemistry

Analysis Batch: 360135

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water SM 3500 CR D480-118849-1 MW-1 Dissolved

Water SM 3500 CR D480-118849-3 MASSAPOAG BROOK Dissolved

Water SM 3500 CR DMB 480-360135/3 Method Blank Total/NA

Water SM 3500 CR DLCS 480-360135/4 Lab Control Sample Total/NA

Analysis Batch: 360366

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 350.1480-118849-1 MW-1 Total/NA

Water 350.1MB 480-360366/27 Method Blank Total/NA

Water 350.1MB 480-360366/50 Method Blank Total/NA

Water 350.1LCS 480-360366/28 Lab Control Sample Total/NA

Water 350.1LCS 480-360366/51 Lab Control Sample Total/NA

Analysis Batch: 360405

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water SM 2540D480-118849-1 MW-1 Total/NA

Water SM 2540D480-118849-3 MASSAPOAG BROOK Total/NA

Water SM 2540DMB 480-360405/1 Method Blank Total/NA

TestAmerica Buffalo

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Page 52: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

QC Association SummaryTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

General Chemistry (Continued)

Analysis Batch: 360405 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water SM 2540DLCS 480-360405/2 Lab Control Sample Total/NA

Prep Batch: 360840

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 1664A480-118849-1 MW-1 Total/NA

Water 1664A480-118849-3 MASSAPOAG BROOK Total/NA

Water 1664AMB 480-360840/1-A Method Blank Total/NA

Water 1664ALCS 480-360840/2-A Lab Control Sample Total/NA

Analysis Batch: 360951

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 1664A 360840480-118849-1 MW-1 Total/NA

Water 1664A 360840480-118849-3 MASSAPOAG BROOK Total/NA

Water 1664A 360840MB 480-360840/1-A Method Blank Total/NA

Water 1664A 360840LCS 480-360840/2-A Lab Control Sample Total/NA

Analysis Batch: 360953

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 300.0480-118849-3 MASSAPOAG BROOK Total/NA

Water 300.0MB 480-360953/28 Method Blank Total/NA

Water 300.0LCS 480-360953/27 Lab Control Sample Total/NA

Water 300.0480-118849-3 MS MASSAPOAG BROOK Total/NA

Analysis Batch: 361013

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 350.1480-118849-3 MASSAPOAG BROOK Total/NA

Water 350.1MB 480-361013/27 Method Blank Total/NA

Water 350.1MB 480-361013/3 Method Blank Total/NA

Water 350.1MB 480-361013/75 Method Blank Total/NA

Water 350.1LCS 480-361013/28 Lab Control Sample Total/NA

Water 350.1LCS 480-361013/4 Lab Control Sample Total/NA

Water 350.1LCS 480-361013/76 Lab Control Sample Total/NA

Analysis Batch: 361021

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water SM 4500 Cl G480-118849-1 MW-1 Total/NA

Water SM 4500 Cl G480-118849-3 MASSAPOAG BROOK Total/NA

Water SM 4500 Cl GMB 480-361021/3 Method Blank Total/NA

Water SM 4500 Cl GLCS 480-361021/4 Lab Control Sample Total/NA

Water SM 4500 Cl G480-118849-1 DU MW-1 Total/NA

Analysis Batch: 361248

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 300.0480-118849-1 MW-1 Total/NA

Water 300.0MB 480-361248/4 Method Blank Total/NA

Water 300.0LCS 480-361248/3 Lab Control Sample Total/NA

Analysis Batch: 362229

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water SM 3500 CR D480-118849-1 MW-1 Total/NA

Water SM 3500 CR D480-118849-3 MASSAPOAG BROOK Total/NA

TestAmerica Buffalo

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Page 53: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Lab ChronicleClient: Sovereign Consulting Inc. TestAmerica Job ID: 480-118849-1Project/Site: Shell--Stoughton MA

Client Sample ID: MW-1 Lab Sample ID: 480-118849-1Matrix: WaterDate Collected: 06/01/17 08:45

Date Received: 06/02/17 02:00

Analysis 8260C 06/07/17 22:14 JAS1 361004 TAL BUF

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 625 360259 06/02/17 14:08 SMP TAL BUFTotal/NA

Analysis 625 1 360707 06/06/17 23:54 PJQ TAL BUFTotal/NA

Prep 200.7 361115 06/08/17 11:03 EMB TAL BUFDissolved

Analysis 200.7 Rev 4.4 1 361604 06/09/17 13:57 LMH TAL BUFDissolved

Prep 200.7 361305 06/09/17 11:10 EMB TAL BUFTotal Recoverable

Analysis 200.7 Rev 4.4 1 361793 06/12/17 23:12 LMH TAL BUFTotal Recoverable

Prep 245.1 361074 06/08/17 09:30 MVZ TAL BUFDissolved

Analysis 245.1 1 361228 06/08/17 14:30 MVZ TAL BUFDissolved

Analysis SM 2340B 1 362174 06/15/17 10:20 LMH TAL BUFTotal/NA

Prep 1664A 360840 06/07/17 09:06 DSC TAL BUFTotal/NA

Analysis 1664A 1 360951 06/07/17 09:06 DSC TAL BUFTotal/NA

Analysis 300.0 20 361248 06/09/17 11:44 DMR TAL BUFTotal/NA

Analysis 350.1 1 360366 06/03/17 17:54 SSS TAL BUFTotal/NA

Analysis SM 2540D 1 360405 06/05/17 00:54 KMB TAL BUFTotal/NA

Analysis SM 3500 CR D 1 360135 06/02/17 05:56 KMB TAL BUFDissolved

Analysis SM 3500 CR D 1 362229 06/15/17 10:26 LMH TAL BUFTotal/NA

Analysis SM 4500 Cl G 1 361021 06/07/17 19:00 LED TAL BUFTotal/NA

Client Sample ID: TRIP BLANK Lab Sample ID: 480-118849-2Matrix: WaterDate Collected: 06/01/17 06:00

Date Received: 06/02/17 02:00

Analysis 8260C 06/06/17 02:52 NEA1 360557 TAL BUF

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Client Sample ID: MASSAPOAG BROOK Lab Sample ID: 480-118849-3Matrix: WaterDate Collected: 06/01/17 11:20

Date Received: 06/02/17 02:00

Analysis 8260C 06/07/17 22:37 JAS1 361004 TAL BUF

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 625 360259 06/02/17 14:08 SMP TAL BUFTotal/NA

Analysis 625 1 360707 06/07/17 00:20 PJQ TAL BUFTotal/NA

Prep 200.7 361115 06/08/17 11:03 EMB TAL BUFDissolved

Analysis 200.7 Rev 4.4 1 361604 06/09/17 14:01 LMH TAL BUFDissolved

Prep 200.7 361305 06/09/17 11:10 EMB TAL BUFTotal Recoverable

Analysis 200.7 Rev 4.4 1 361793 06/12/17 23:15 LMH TAL BUFTotal Recoverable

Prep 245.1 361074 06/08/17 09:30 MVZ TAL BUFDissolved

Analysis 245.1 1 361228 06/08/17 14:32 MVZ TAL BUFDissolved

Analysis SM 2340B 1 362174 06/15/17 10:22 LMH TAL BUFTotal/NA

Prep 1664A 360840 06/07/17 09:06 DSC TAL BUFTotal/NA

TestAmerica Buffalo

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Page 54: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Lab ChronicleClient: Sovereign Consulting Inc. TestAmerica Job ID: 480-118849-1Project/Site: Shell--Stoughton MA

Client Sample ID: MASSAPOAG BROOK Lab Sample ID: 480-118849-3Matrix: WaterDate Collected: 06/01/17 11:20

Date Received: 06/02/17 02:00

Analysis 1664A 06/07/17 09:06 DSC1 360951 TAL BUF

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 300.0 1 360953 06/08/17 00:17 DMR TAL BUFTotal/NA

Analysis 350.1 1 361013 06/07/17 17:31 SSS TAL BUFTotal/NA

Analysis SM 2540D 1 360405 06/05/17 00:54 KMB TAL BUFTotal/NA

Analysis SM 3500 CR D 1 360135 06/02/17 05:56 KMB TAL BUFDissolved

Analysis SM 3500 CR D 1 362229 06/15/17 10:26 LMH TAL BUFTotal/NA

Analysis SM 4500 Cl G 1 361021 06/07/17 19:00 LED TAL BUFTotal/NA

Laboratory References:

TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY 14228-2298, TEL (716)691-2600

TestAmerica Buffalo

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Page 55: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Accreditation/Certification SummaryClient: Sovereign Consulting Inc. TestAmerica Job ID: 480-118849-1Project/Site: Shell--Stoughton MA

Laboratory: TestAmerica BuffaloAll accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.

Authority Program EPA Region Identification Number Expiration Date

Arkansas DEQ 88-06866State Program 07-06-17 *

California State Program 9 1169CA 09-30-17

Connecticut State Program 1 PH-0568 09-30-18

Florida NELAP 4 E87672 06-30-17 *

Georgia State Program 4 N/A 03-31-18

Illinois NELAP 5 200003 09-30-17

Iowa State Program 7 374 03-01-19

Kansas NELAP 7 E-10187 01-31-18

Kentucky (DW) State Program 4 90029 12-31-17

Kentucky (UST) State Program 4 30 03-31-18

Kentucky (WW) State Program 4 90029 12-31-17

Louisiana NELAP 6 02031 06-30-17 *

Maine State Program 1 NY00044 12-04-18

Maryland State Program 3 294 03-31-18

Massachusetts State Program 1 M-NY044 06-30-17 *

Michigan State Program 5 9937 03-31-17 *

Minnesota NELAP 5 036-999-337 12-31-17

New Hampshire NELAP 1 2337 11-17-17

New Jersey NELAP 2 NY455 06-30-17 *

New York NELAP 2 10026 03-31-18

North Dakota State Program 8 R-176 03-31-18

Oklahoma State Program 6 9421 08-31-17

Oregon NELAP 10 NY200003 06-09-18

Pennsylvania NELAP 3 68-00281 07-31-17 *

Rhode Island State Program 1 LAO00328 12-30-17

Tennessee State Program 4 TN02970 03-31-18

Texas NELAP 6 T104704412-15-6 07-31-17 *

USDA Federal P330-11-00386 11-26-17

Virginia NELAP 3 460185 09-14-17

Washington State Program 10 C784 02-10-18

Wisconsin State Program 5 998310390 08-31-17

TestAmerica Buffalo

* Accreditation/Certification renewal pending - accreditation/certification considered valid.

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Page 56: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Method SummaryTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Method Method Description LaboratoryProtocol

SW8468260C Volatile Organic Compounds by GC/MS TAL BUF

40CFR136A625 Semivolatile Organic Compounds (GC/MS) TAL BUF

EPA200.7 Rev 4.4 Metals (ICP) TAL BUF

EPA245.1 Mercury (CVAA) TAL BUF

SMSM 2340B Total Hardness (as CaCO3) by calculation TAL BUF

1664A1664A HEM and SGT-HEM TAL BUF

MCAWW300.0 Anions, Ion Chromatography TAL BUF

MCAWW350.1 Nitrogen, Ammonia TAL BUF

SMSM 2540D Solids, Total Suspended (TSS) TAL BUF

SMSM 3500 CR D Chromium, Hexavalent TAL BUF

SMSM 3500 CR D Chromium, Trivalent TAL BUF

SMSM 4500 Cl G Chlorine, Residual TAL BUF

Protocol References:

1664A = EPA-821-98-002

40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and

subsequent revisions.EPA = US Environmental Protection Agency

MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY 14228-2298, TEL (716)691-2600

TestAmerica Buffalo

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Page 57: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Sample SummaryTestAmerica Job ID: 480-118849-1Client: Sovereign Consulting Inc.

Project/Site: Shell--Stoughton MA

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

480-118849-1 MW-1 Water 06/01/17 08:45 06/02/17 02:00

480-118849-2 TRIP BLANK Water 06/01/17 06:00 06/02/17 02:00

480-118849-3 MASSAPOAG BROOK Water 06/01/17 11:20 06/02/17 02:00

TestAmerica Buffalo

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Page 58: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

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Page 59: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

Login Sample Receipt Checklist

Client: Sovereign Consulting Inc. Job Number: 480-118849-1

Login Number: 118849

Question Answer Comment

Creator: Williams, Christopher S

List Source: TestAmerica Buffalo

List Number: 1

TrueRadioactivity either was not measured or, if measured, is at or below background

TrueThe cooler's custody seal, if present, is intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the sample IDs on the containers and the COC.

TrueSamples are received within Holding Time (Excluding tests with immediate HTs)..

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

TrueIf necessary, staff have been informed of any short hold time or quick TAT needs

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

TrueSampling Company provided. SOVEREIGN

TrueSamples received within 48 hours of sampling.

TrueSamples requiring field filtration have been filtered in the field.

TrueChlorine Residual checked.

TestAmerica BuffaloPage 31 of 31 6/15/2017

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Page 60: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA

ATTACHMENT C

Page 61: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

1

Smith, James

From: Ruan, Xiaodan (DEP) <[email protected]>Sent: Monday, July 10, 2017 3:30 PMTo: Smith, JamesSubject: RE: Receiving Water LookupAttachments: Massapoag Brook.pdf

Hi Jim, Thank you so much for working with us together to make sure you have the right numbers for the 7Q10 and the dilution factor. Please see the attached SteamStats report. I am not sure why our reports are in different formats and give us different values, maybe they were run by different versions? BTW, I used StreamStats 4.0. The 7Q10 in the attached report is 0.426 cfs. Could you please take a look at it and let me know if you have any questions? Thanks. Xiaodan From: Smith, James [mailto:[email protected]] Sent: Monday, July 10, 2017 1:20 PM To: Ruan, Xiaodan (DEP) Subject: RE: Receiving Water Lookup It was run about 3 weeks ago by our office engineer. James M. Smith Senior Project Manager | email: [email protected] phone: 508-339-3200| mobile: 781-588-7370 Sovereign Consulting Inc. 16 Chestnut Street, Suite 520 Foxboro, MA 02035 www.sovcon.com Science. Service. Solutions. PLEASE NOTE: All information transmitted with and contained in this correspondence contains confidential, proprietary or legally privileged information and is intended for use only by the person or entity to which it is addressed. Any review, retransmission, dissemination or other use of, or taking of any action in reliance upon this information by persons or entities other than the intended recipient is prohibited. If you received this communication in error, please notify the sender immediately. Thank you.

From: Ruan, Xiaodan (DEP) [mailto:[email protected]] Sent: Monday, July 10, 2017 1:15 PM To: Smith, James <[email protected]> Subject: RE: Receiving Water Lookup Hi Jim‐ The format of the report looks different than what I got. Was this report run recently or was it from previous application? Thanks!

Page 62: S OVEREIGN C ONSULTING I NC - US EPA€¦ · NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA 3 collected from the nearest accessible

2

From: Smith, James [mailto:[email protected]] Sent: Monday, July 10, 2017 1:10 PM To: Ruan, Xiaodan (DEP) Subject: RE: Receiving Water Lookup Sure thing, here you go. The coordinates you listed below are indeed what the Streamstats 7Q10 was based on – unless I misinterpreted it. See attached. When I sent this to you last week, it seems I forgot to double‐side the scanner, so you didn’t get all of our calculations. With this attachment you’ll see the page where we captured the 7Q10 flow and converted it from cfs to mgd. Sorry about that. Jim James M. Smith Senior Project Manager | email: [email protected] phone: 508-339-3200| mobile: 781-588-7370 Sovereign Consulting Inc. 16 Chestnut Street, Suite 520 Foxboro, MA 02035 www.sovcon.com Science. Service. Solutions. PLEASE NOTE: All information transmitted with and contained in this correspondence contains confidential, proprietary or legally privileged information and is intended for use only by the person or entity to which it is addressed. Any review, retransmission, dissemination or other use of, or taking of any action in reliance upon this information by persons or entities other than the intended recipient is prohibited. If you received this communication in error, please notify the sender immediately. Thank you.

From: Ruan, Xiaodan (DEP) [mailto:[email protected]] Sent: Monday, July 10, 2017 12:58 PM To: Smith, James <[email protected]> Subject: RE: Receiving Water Lookup Hi Jim, I am sorry for my misjudgment! Could you please send me your StreamStats report? Cause I got a different 7Q10 by using the coordinates you provided in the earlier email, Lat – 42.1495436, Long ‐ ‐71.14949528. It will be very helpful if I can see in the report where you clicked exactly. Thank you. Xiaodan From: Smith, James [mailto:[email protected]] Sent: Monday, July 10, 2017 11:39 AM To: Ruan, Xiaodan (DEP) Subject: RE: Receiving Water Lookup Hi Xiaodan, thanks for your attention to working through this with me. For the GPs coordinates we used, Streatstats provided a 7Q10 of 0.7 cfs, which we converted to 0.452 MGD. So using 0.452, and using a design flow of 50 gpm (converted to 0.072 MGD) is how we came up with a dilution factor of 7.278. I don’t want to dispute the result, I just want to make sure I am calculating correctly. Can you please confirm that we did the cfs‐MGD conversion correctly or incorrectly? Thanks so much for your patience.

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Jim James M. Smith Senior Project Manager | email: [email protected] phone: 508-339-3200| mobile: 781-588-7370 Sovereign Consulting Inc. 16 Chestnut Street, Suite 520 Foxboro, MA 02035 www.sovcon.com Science. Service. Solutions. PLEASE NOTE: All information transmitted with and contained in this correspondence contains confidential, proprietary or legally privileged information and is intended for use only by the person or entity to which it is addressed. Any review, retransmission, dissemination or other use of, or taking of any action in reliance upon this information by persons or entities other than the intended recipient is prohibited. If you received this communication in error, please notify the sender immediately. Thank you.

From: Ruan, Xiaodan (DEP) [mailto:[email protected]] Sent: Friday, July 07, 2017 3:26 PM To: Smith, James <[email protected]>; Vakalopoulos, Catherine (DEP) <[email protected]> Subject: RE: Receiving Water Lookup Hi Jim, Looks like you didn’t convert the 7Q10 to MGD. The unit for 7Q10 in StreamStats report is cfs which needs to be converted to MGD in order to be used in the dilution factor calculation. So the dilution factor should be 4.18. Please let me know if you have any questions. Thanks. Have a nice weekend! Xiaodan From: Smith, James [mailto:[email protected]] Sent: Friday, July 07, 2017 3:17 PM To: Ruan, Xiaodan (DEP); Vakalopoulos, Catherine (DEP) Subject: RE: Receiving Water Lookup Sure thing – attached is the streamstats page, followed by our 7Q10 calculation. Jim James M. Smith Senior Project Manager | email: [email protected] phone: 508-339-3200| mobile: 781-588-7370 Sovereign Consulting Inc. 16 Chestnut Street, Suite 520 Foxboro, MA 02035 www.sovcon.com Science. Service. Solutions. PLEASE NOTE: All information transmitted with and contained in this correspondence contains confidential, proprietary or legally privileged information and is intended for use only by the person or entity to which it is addressed. Any review, retransmission, dissemination or other use of, or taking of any

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action in reliance upon this information by persons or entities other than the intended recipient is prohibited. If you received this communication in error, please notify the sender immediately. Thank you.

From: Ruan, Xiaodan (DEP) [mailto:[email protected]] Sent: Friday, July 07, 2017 3:01 PM To: Vakalopoulos, Catherine (DEP) <[email protected]>; Smith, James <[email protected]> Subject: RE: Receiving Water Lookup Hi Jim, I clicked on the stream cell that is very close to the coordinates that you gave and received a slightly different 7Q10 (see attached report). The 7Q10 in the report is 0.426 cfs, that equals to 0.229 MGD. So the dilution factor is: (0.229 MGD +0.072 MGD) / 0.072 MGD = 4.18. This value does not match what you had. Could you please send us your calculation? Thank you! Xiaodan From: Vakalopoulos, Catherine (DEP) Sent: Friday, July 07, 2017 12:15 PM To: Smith, James452 Cc: Ruan, Xiaodan (DEP) Subject: RE: Receiving Water Lookup Hi Jim, I will check what you sent after lunch but in the meantime I wanted to let you know that unfortunately I can’t answer your question re: FWS, NMFS, and NHPA. You will have to contact EPA. Shauna Little is on vacation but she said to have people contact George Papadopoulos 617‐918‐1579 or Newton Tedder 617‐918‐1038. I know George is in today so start with him. Cathy From: Smith, James [mailto:[email protected]] Sent: Friday, July 07, 2017 11:39 AM To: Vakalopoulos, Catherine (DEP) Cc: Ruan, Xiaodan (DEP) Subject: RE: Receiving Water Lookup Hi Kathy, Here are the coordinates we used to run streamstats and calculate the 7Q10: Lat – 42.1495436 Long ‐ ‐71.14949528 The design flow of the system is 50 gpm. The system will likely be running more like 20‐30 gpm when it is running. I also have another question – in Sections G and H – am I required to contact someone at FWS, NMFS, or NHPA as applicable, and get a written document from those parties in order to consider the determinations in these sections valid for the RGP application? Or can my review of available data (mainly online resources) suffice as a valid determination, to support this application? Jim James M. Smith Senior Project Manager | email:

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phone: 508-339-3200| mobile: 781-588-7370 Sovereign Consulting Inc. 16 Chestnut Street, Suite 520 Foxboro, MA 02035 www.sovcon.com Science. Service. Solutions. PLEASE NOTE: All information transmitted with and contained in this correspondence contains confidential, proprietary or legally privileged information and is intended for use only by the person or entity to which it is addressed. Any review, retransmission, dissemination or other use of, or taking of any action in reliance upon this information by persons or entities other than the intended recipient is prohibited. If you received this communication in error, please notify the sender immediately. Thank you.

From: Vakalopoulos, Catherine (DEP) [mailto:[email protected]] Sent: Thursday, July 06, 2017 5:28 PM To: Smith, James <[email protected]> Cc: Ruan, Xiaodan (DEP) <[email protected]> Subject: RE: Receiving Water Lookup Hi Jim, Xiaodan was out today so I looked at what you sent. Please check the attached StreamStats report because I came up with a different 7Q10 than you (I made sure to convert cfs to MGD and it was still different). It’s probably because I guessed at the exact discharge location and so please send me the lat/long of the discharge location on Massapoag Brook. If you didn’t save the StreamStats report, please run it again and you will see a lat/long of the location you clicked on to delineate. Also, please confirm that the 0.072 MGD (50 gpm) is indeed the design flow and not an average flow. Thanks! Cathy From: Smith, James [mailto:[email protected]] Sent: Wednesday, July 05, 2017 4:04 PM To: Vakalopoulos, Catherine (DEP) Subject: RE: Receiving Water Lookup Hi Cathy, thanks for your guidance. I might be a bit out of order, not having already submitting this to you, but can you please review the attached 7Q10 calculation for the receiving water referenced below: Dewatering location – 140 Sharon Street, Stoughton MA Receiving water location – Massapoag Brook, Canton MA, segment MA73‐21, Class B 7Q10 flow – 0.452 Dilution factor calculation – 7.278 I attached a MassDEP 21E Priority Resource Map if that is helpful. This is my first go‐round at the new RGP permit application. My sincere thanks for your patience and assistance, and apologies for asking what must seem like very silly questions! Jim James M. Smith Senior Project Manager | email: [email protected] phone: 508-339-3200| mobile: 781-588-7370

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Sovereign Consulting Inc. 16 Chestnut Street, Suite 520 Foxboro, MA 02035 www.sovcon.com Science. Service. Solutions. PLEASE NOTE: All information transmitted with and contained in this correspondence contains confidential, proprietary or legally privileged information and is intended for use only by the person or entity to which it is addressed. Any review, retransmission, dissemination or other use of, or taking of any action in reliance upon this information by persons or entities other than the intended recipient is prohibited. If you received this communication in error, please notify the sender immediately. Thank you.

From: Vakalopoulos, Catherine (DEP) [mailto:[email protected]] Sent: Thursday, June 29, 2017 12:46 PM To: Smith, James <[email protected]> Subject: RE: Receiving Water Lookup Hi Jim, StreamStats is only for figuring out the 7Q10 for rivers and streams. Here is where you can find the classification (A, B, SA, or SB): http://www.mass.gov/eea/docs/dep/water/laws/i‐thru‐z/tblfig.pdf. Waterbody IDs can be found in water quality assessment reports here: http://www.mass.gov/eea/agencies/massdep/water/watersheds/water‐quality‐assessments.html. Open the latest report for the watershed you are working in and do a search for the waterbody ID (also known as the segment, it looks like “MA##‐##). Larger rivers are split up into several segments and smaller stream may not have an ID so just list the name in the NOI. Let me know if you have any trouble and I can look for you. I’ve been out of the office for a couple of days and am a bit backed up with RGP emails but will get back to you as soon as I can. Cathy From: Smith, James [mailto:[email protected]] Sent: Wednesday, June 28, 2017 4:48 PM To: Vakalopoulos, Catherine (DEP) Subject: Receiving Water Lookup Hi Cathy, I am preparing an RGP application, and trying to determine the ID and classification of the receiving water. I went on USGS Streamstats 4.0, but I didn’t see the information needed in the application section B1. Could you point me in the right direction? Thanks so much, Jim James M. Smith Senior Project Manager | email: [email protected] phone: 508-339-3200| mobile: 781-588-7370 Sovereign Consulting Inc. 16 Chestnut Street, Suite 520 Foxboro, MA 02035

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www.sovcon.com Science. Service. Solutions. PLEASE NOTE: All information transmitted with and contained in this correspondence contains confidential, proprietary or legally privileged information and is intended for use only by the person or entity to which it is addressed. Any review, retransmission, dissemination or other use of, or taking of any action in reliance upon this information by persons or entities other than the intended recipient is prohibited. If you received this communication in error, please notify the sender immediately. Thank you.

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StreamStats Report

Basin Characteristics

Parameter Code Parameter Descr iption V alue U nit

DRNAREA Area tha t drains to a poin t on a stream 10.3 sq uare miles

BSLDEM250 Mean basin s lo pe computed from 1 :250K DEM 1.881 perc ent

DRFTP ERSTR Area of stra t if ied dr i ft per un i t of stream length 0.21 sq uare mile per mi le

MAREGION Region of M assach usetts 0 for Eastern 1 for Western 0 dimensionlesstest

Low-Flow Statistics Parameters [Statewide Low Flow WRIR00 4135]

Parameter Code Parameter Name Value U nits Min Limit Max Limit

DRNAREA Drainage Area 10.3 s quare mi les 1.61 149

BSLDEM250 M ean Basin S lope from 250K DEM 1.881 perc ent 0 .32 24.6

DRFTP ERSTR Strat if ied D ri f t per Stream Length 0.21 s quare mi le per mi le 0 1.29

MAREGION M assach usetts Region 0 dimensionlesstest 0 1

Low-Flow Statistics Flow Report [Statewide Low Flow WRIR00 4135]

PIl : P re d ic t i on Int er va l -Lowe r , P Iu : Pre d ic t ion I nte r va l - Up p e r , SEp : S tan da rd Er r or of Pr ed i ct i on , S E : St andar d Err or ( o the r - - se e r e por t )

Statistic Value Unit PI l PIu SE SEp

7 D ay 2 Year Low Flow 1.05 ft^3/s 0.397 2.67 49.5 49.5

7 D ay 10 Year Low F low 0.426 ft^3/s 0.125 1.35 70.8 70.8

Low-Flow Statistics Citations

Ries, K.G. , II I ,2 000, Methods for est imating low- flow statist ics for Massac huset ts streams: U .S. Geologic al Survey W ater Resourc es Investigations Report 00- 4135 , 81 p.

(http :/ /pubs.usgs.g ov/wr i/wr i0 0413 5/)

Region ID: MA

W orkspace ID: MA 20170710150443400000

Cl icked Point (Lat itude, Longi tude): 42.14969 , -71 .14909

Time: 2017-07-10 15 :05:32 -0400

Page 2 of 2StreamStats 4.0

7/10/2017https://test.streamstats.usgs.gov/ss/

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Enter number values in green boxes below Notes:Enter values in the units specified

↓ Freshwater: QR equal to the 7Q10; enter alternate QR if approved by the State; enter 0 if no dilution factor approved

0.275 QR = Enter upstream flow in MGD Saltwater (estuarine and marine): enter QR if approved by the State; enter 0 if no entry

0.072 QP = Enter discharge flow in MGD Discharge flow is equal to the design flow or 1 MGD, whichever is less0.275 Downstream 7Q10 Only if approved by State as the entry for QR; leave 0 if no entry

Enter a dilution factor, if other than zero Saltwater (estuarine and marine): only if approved by the State

↓ Leave 0 if no entry

4.82

Enter values in the units specified

↓200 Cd = Enter influent hardness in mg/L CaCO3 Freshwater only

45 Cs = Enter receiving water hardness in mg/L CaCO3

Enter receiving water concentrations in the units specified pH, temperature, and ammonia required for all discharges

↓ Hardness required for freshwater

6.39 pH in Standard Units Salinity required for saltwater (estuarine and marine)

24.8 Temperature in oC Metals required for all discharges if present and if dilution factor is > 1

0.052 Ammonia in mg/L Enter 0 if non-detect or testing not required

45 Hardness in mg/L CaCO3

0 Salinity in ppt0 Antimony in µg/L0 Arsenic in µg/L0 Cadmium in µg/L0 Chromium III in µg/L0 Chromium VI in µg/L0 Copper in µg/L

580 Iron in µg/L0 Lead in µg/L0 Mercury in µg/L 0 Nickel in µg/L0 Selenium in µg/L0 Silver in µg/L0 Zinc in µg/L

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Enter influent concentrations in the units specified if >1 sample, enter maximum

↓ if >10 samples, may enter 95th percentile

0 TRC in µg/L Enter 0 if non-detect or testing not required

0 Ammonia in mg/L0 Antimony in µg/L0 Arsenic in µg/L0 Cadmium in µg/L0 Chromium III in µg/L0 Chromium VI in µg/L0 Copper in µg/L0 Iron in µg/L0 Lead in µg/L0 Mercury in µg/L0 Nickel in µg/L0 Selenium in µg/L0 Silver in µg/L0 Zinc in µg/L0 Cyanide in µg/L0 Phenol in µg/L0 Carbon Tetrachloride in µg/L0 Tetrachloroethylene in µg/L0 Total Phthalates in µg/L0 Diethylhexylphthalate in µg/L0 Benzo(a)anthracene in µg/L0 Benzo(a)pyrene in µg/L0 Benzo(b)fluoranthene in µg/L0 Benzo(k)fluoranthene in µg/L0 Chrysene in µg/L0 Dibenzo(a,h)anthracene in µg/L0 Indeno(1,2,3-cd)pyrene in µg/L0 Methyl-tert butyl ether in µg/L

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Dilution Factor 4.8

A. InorganicsAmmonia Report mg/L ---

Chloride Report µg/L ---

Total Residual Chlorine 0.2 mg/L 42 µg/L 50 µg/L

Total Suspended Solids 30 mg/L ---

Antimony 206 µg/L 2444 µg/L

Arsenic 104 µg/L 38 µg/L

Cadmium 10.2 µg/L 1.0134 µg/L

Chromium III 323 µg/L 322.0 µg/L

Chromium VI 323 µg/L 43.7 µg/L

Copper 242 µg/L 34.8 µg/L

Iron 5000 µg/L 1604 µg/L

Lead 160 µg/L 11.75 µg/L

Mercury 0.739 µg/L 3.46 µg/L

Nickel 1450 µg/L 194.8 µg/L

Selenium 235.8 µg/L 19.1 µg/L

Silver 35.1 µg/L 13.8 µg/L

Zinc 420 µg/L 447.4 µg/L

Cyanide 178 mg/L 19.9 µg/L --- µg/LB. Non-Halogenated VOCsTotal BTEX 100 µg/L ---Benzene 5.0 µg/L ---1,4 Dioxane 200 µg/L ---Acetone 7970 µg/L ---Phenol 1,080 µg/L 1146 µg/LC. Halogenated VOCsCarbon Tetrachloride 4.4 µg/L 6.1 µg/L1,2 Dichlorobenzene 600 µg/L ---1,3 Dichlorobenzene 320 µg/L ---1,4 Dichlorobenzene 5.0 µg/L ---Total dichlorobenzene --- µg/L ---

WQBEL applies if boldedTBEL applies if boldedCompliance Level applies if shown

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1,1 Dichloroethane 70 µg/L ---1,2 Dichloroethane 5.0 µg/L ---1,1 Dichloroethylene 3.2 µg/L ---Ethylene Dibromide 0.05 µg/L ---Methylene Chloride 4.6 µg/L ---1,1,1 Trichloroethane 200 µg/L ---1,1,2 Trichloroethane 5.0 µg/L ---Trichloroethylene 5.0 µg/L ---Tetrachloroethylene 5.0 µg/L 12.6 µg/Lcis-1,2 Dichloroethylene 70 µg/L ---Vinyl Chloride 2.0 µg/L ---

D. Non-Halogenated SVOCs

Total Phthalates 190 µg/L --- µg/LDiethylhexyl phthalate 101 µg/L 8.4 µg/LTotal Group I Polycyclic Aromatic Hydrocarbons 1.0 µg/L ---Benzo(a)anthracene 1.0 µg/L 0.0145 µg/L --- µg/LBenzo(a)pyrene 1.0 µg/L 0.0145 µg/L --- µg/LBenzo(b)fluoranthene 1.0 µg/L 0.0145 µg/L --- µg/LBenzo(k)fluoranthene 1.0 µg/L 0.0145 µg/L --- µg/LChrysene 1.0 µg/L 0.0145 µg/L --- µg/LDibenzo(a,h)anthracene 1.0 µg/L 0.0145 µg/L --- µg/LIndeno(1,2,3-cd)pyrene 1.0 µg/L 0.0145 µg/L --- µg/LTotal Group II Polycyclic Aromatic Hydrocarbons 100 µg/L ---Naphthalene 20 µg/L ---E. Halogenated SVOCs

Total Polychlorinated Biphenyls 0.000064 µg/L --- 0.5 µg/LPentachlorophenol 1.0 µg/L ---F. Fuels ParametersTotal Petroleum Hydrocarbons 5.0 mg/L ---Ethanol Report mg/L ---Methyl-tert-Butyl Ether 70 µg/L 76 µg/Ltert-Butyl Alcohol 120 µg/L ---tert-Amyl Methyl Ether 90 µg/L ---

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NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA

ATTACHMENT D

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16 Chestnut Street, Suite 520 Foxborough, MA 02035 Tel: 508-339-3200 Fax: 508-339-3248

S O V E R E I G N C O N S U L T I N G I N C . July 6, 2017 James Donovan – Town Engineer Canton Town Hall 801 Washington Street Canton, Massachusetts 02021 Re: Notice of Remediation General Permit Discharge Application Shell-Branded Gasoline Station 140 Sharon Street Stoughton, Massachusetts MassDEP RTN 4-15064 Dear Mr. Donovan: In accordance with the National Pollutant Discharge Elimination System (NPDES) Remediation General Permit (RGP), this correspondence serves as notification that an application for discharge of treated groundwater from the site located at 140 Sharon Street in Stoughton MA, to the public storm drain system which discharges in Canton to Massapoag Brook, is planned for July and August 2017. Dewatering of petroleum-impacted groundwater will be conducted during gasoline station redevelopment construction activities beginning in later July 2017, and continuing through August 2017. During the construction, existing gasoline underground storage tanks (USTs), pump islands, and associated piping will be removed and replaced with a new UST system. Dewatering of groundwater will be performed during the installation of the replacement USTs, as the excavation depth for the replacement USTs will extend into the groundwater table. Groundwater dewatered during the construction activities will be treated through a series of bag filters and carbon filter units, under the NPDES RGP permit referenced above, prior to being discharged to the storm drain system, which discharges to a wetland area that feeds Massapoag Brook. A copy of the NDPES RGP application will be available upon request, once complete. Please feel free to contact me with any questions at the office number below, or by my mobile phone at 781-588-7370. Sincerely, SOVEREIGN CONSULTING INC.

James M. Smith Senior Project Manager cc: Marc Oler, Shell Oil Products US Sovereign File – 2P764

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16 Chestnut Street, Suite 520 Foxborough, MA 02035 Tel: 508-339-3200 Fax: 508-339-3248

S O V E R E I G N C O N S U L T I N G I N C . July 7, 2017 Cynthia O’Connell – Conservation Agent Canton Conservation Commission 801 Washington Street Canton, Massachusetts 02021 Re: Notice of Remediation General Permit Discharge Application Shell-Branded Gasoline Station 140 Sharon Street Stoughton, Massachusetts MassDEP RTN 4-15064 Dear Ms. O’Connell: In accordance with the National Pollutant Discharge Elimination System (NPDES) Remediation General Permit (RGP), this correspondence serves as notification that an application for discharge of treated groundwater from the site located at 140 Sharon Street in Stoughton MA, to the public storm drain system which discharges in Canton to Massapoag Brook, is planned for July and August 2017. Dewatering of petroleum-impacted groundwater will be conducted during gasoline station redevelopment construction activities beginning in later July 2017, and continuing through August 2017. During the construction, existing gasoline underground storage tanks (USTs), pump islands, and associated piping will be removed and replaced with a new UST system. Dewatering of groundwater will be performed during the installation of the replacement USTs, as the excavation depth for the replacement USTs will extend into the groundwater table. Groundwater dewatered during the construction activities will be treated through a series of bag filters and carbon filter units, under the NPDES RGP permit referenced above, prior to being discharged to the storm drain system, which discharges to a wetland area that feeds Massapoag Brook. A copy of the NDPES RGP application will be available upon request, once complete. Please feel free to contact me with any questions at the office number below, or by my mobile phone at 781-588-7370. Sincerely, SOVEREIGN CONSULTING INC.

James M. Smith Senior Project Manager cc: Marc Oler, Shell Oil Products US Sovereign File – 2P764

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NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA

ATTACHMENT E

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July 10, 2017

United States Department of the InteriorFISH AND WILDLIFE SERVICE

New England Ecological Services Field Office70 Commercial Street, Suite 300

Concord, NH 03301-5094Phone: (603) 223-2541 Fax: (603) 223-0104

http://www.fws.gov/newengland

In Reply Refer To:Consultation Code: 05E1NE00-2017-SLI-2037Event Code: 05E1NE00-2017-E-04460 Project Name: Massapoag Brook Wetland - Canton, MA

Subject: List of threatened and endangered species that may occur in your proposed projectlocation, and/or may be affected by your proposed project

To Whom It May Concern:

The enclosed species list identifies threatened, endangered, proposed and candidate species, aswell as proposed and final designated critical habitat, that may occur within the boundary of yourproposed project and/or may be affected by your proposed project. The species list fulfills therequirements of the U.S. Fish and Wildlife Service (Service) under section 7(c) of theEndangered Species Act (Act) of 1973, as amended (16 U.S.C. 1531 ).et seq.

New information based on updated surveys, changes in the abundance and distribution ofspecies, changed habitat conditions, or other factors could change this list. Please feel free tocontact us if you need more current information or assistance regarding the potential impacts tofederally proposed, listed, and candidate species and federally designated and proposed criticalhabitat. Please note that under 50 CFR 402.12(e) of the regulations implementing section 7 of theAct, the accuracy of this species list should be verified after 90 days. This verification can becompleted formally or informally as desired. The Service recommends that verification becompleted by visiting the ECOS-IPaC website at regular intervals during project planning andimplementation for updates to species lists and information. An updated list may be requestedthrough the ECOS-IPaC system by completing the same process used to receive the enclosed list.

The purpose of the Act is to provide a means whereby threatened and endangered species and theecosystems upon which they depend may be conserved. Under sections 7(a)(1) and 7(a)(2) of theAct and its implementing regulations (50 CFR 402 ), Federal agencies are required toet seq.utilize their authorities to carry out programs for the conservation of threatened and endangeredspecies and to determine whether projects may affect threatened and endangered species and/ordesignated critical habitat.

A Biological Assessment is required for construction projects (or other undertakings havingsimilar physical impacts) that are major Federal actions significantly affecting the quality of the

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07/10/2017 Event Code: 05E1NE00-2017-E-04460 2

human environment as defined in the National Environmental Policy Act (42 U.S.C. 4332(2)(c)). For projects other than major construction activities, the Service suggests that a biologicalevaluation similar to a Biological Assessment be prepared to determine whether the project mayaffect listed or proposed species and/or designated or proposed critical habitat. Recommendedcontents of a Biological Assessment are described at 50 CFR 402.12.

If a Federal agency determines, based on the Biological Assessment or biological evaluation, thatlisted species and/or designated critical habitat may be affected by the proposed project, theagency is required to consult with the Service pursuant to 50 CFR 402. In addition, the Servicerecommends that candidate species, proposed species and proposed critical habitat be addressedwithin the consultation. More information on the regulations and procedures for section 7consultation, including the role of permit or license applicants, can be found in the "EndangeredSpecies Consultation Handbook" at:

http://www.fws.gov/endangered/esa-library/pdf/TOC-GLOS.PDF

Please be aware that bald and golden eagles are protected under the Bald and Golden EagleProtection Act (16 U.S.C. 668 ), and projects affecting these species may requireet seq.development of an eagle conservation plan(http://www.fws.gov/windenergy/eagle_guidance.html). Additionally, wind energy projectsshould follow the wind energy guidelines (http://www.fws.gov/windenergy/) for minimizingimpacts to migratory birds and bats.

Guidance for minimizing impacts to migratory birds for projects including communicationstowers (e.g., cellular, digital television, radio, and emergency broadcast) can be found at:http://www.fws.gov/migratorybirds/CurrentBirdIssues/Hazards/towers/towers.htm;http://www.towerkill.com; andhttp://www.fws.gov/migratorybirds/CurrentBirdIssues/Hazards/towers/comtow.html.

We appreciate your concern for threatened and endangered species. The Service encouragesFederal agencies to include conservation of threatened and endangered species into their projectplanning to further the purposes of the Act. Please include the Consultation Tracking Number inthe header of this letter with any request for consultation or correspondence about your projectthat you submit to our office.

Attachment(s):

Official Species List

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Official Species ListThis list is provided pursuant to Section 7 of the Endangered Species Act, and fulfills therequirement for Federal agencies to "request of the Secretary of the Interior information whetherany species which is listed or proposed to be listed may be present in the area of a proposedaction".

This species list is provided by:

New England Ecological Services Field Office70 Commercial Street, Suite 300Concord, NH 03301-5094(603) 223-2541

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Project SummaryConsultation Code: 05E1NE00-2017-SLI-2037

Event Code: 05E1NE00-2017-E-04460

Project Name: Massapoag Brook Wetland - Canton, MA

Project Type: ** OTHER **

Project Description: Wetland area that feeds Massapoag Brook - outfall from RGP Permit -July/August 2017

Project Location: Approximate location of the project can be viewed in Google Maps:

https://www.google.com/maps/place/42.14229373115583N71.15070481908546W

Counties: Norfolk, MA

Endangered Species Act SpeciesThere is a total of 1 threatened, endangered, or candidate species on your species list. Species onthis list should be considered in an effects analysis for your project and could include speciesthat exist in another geographic area. For example, certain fish may appear on the species listbecause a project could affect downstream species. See the "Critical habitats" section below forthose critical habitats that lie wholly or partially within your project area. Please contact thedesignated FWS office if you have questions.

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Mammals

NAME STATUS

Northern Long-eared Bat (Myotis septentrionalis)No critical habitat has been designated for this species.Species profile: https://ecos.fws.gov/ecp/species/9045

Threatened

Critical habitats

There are no critical habitats within your project area.

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NPDES RGP Application July 11, 2017 Shell-Branded Gasoline Station – 140 Sharon Street, Stoughton, MA

ATTACHMENT F

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MACRIS Search Results

Town(s): Canton; Place: South Canton; Resource Type(s): Area, Building, Burial Ground, Object, Structure; Search Criteria:

CAN.B Revere, Paul and Son Copper Works Canton

CAN.C Rising Sun Stove Polish Factory Canton

CAN.D Neponset Street Area Canton

CAN.E American Net and Twine Company Worker Housing

Canton

CAN.F Neponset Cotton Mill District Canton

CAN.J Church and Washington Streets Canton

CAN.AD Kinsley Place Area Canton

CAN.102 American Net and Twine Company Bay St Canton c 1834

CAN.105 Boston and Providence Railroad Signalman's Shed

Beaumont St Canton c 1900

CAN.89 Ames, Oliver and Sons Shovel Manufactory 160 Bolivar St Canton 1847

CAN.90 Capen, E. House 17 Capen Pl Canton r 1840

CAN.91 Canton Baptist Parsonage 15 Church St Canton 1841

CAN.66 Canton Baptist Church 21 Church St Canton 1836

CAN.92 South Canton Schoolhouse - Canton Armory 22-24 Church St Canton c 1837

CAN.67 Leonard, Caroline House 31 Church St Canton r 1840

CAN.68 Leonard, Caroline House 33 Church St Canton r 1840

CAN.93 Leonard, Winthrop House 35 Church St Canton r 1865

CAN.216 Harrington, Andrew House 31 Dunbar St Canton 1881

CAN.901 High Street Bridge over Conrail High St Canton 1939

CAN.802 Leonard - Gridley Burial Ground Kinsley Pl Canton c 1764

CAN.217 American Net and Twine Company Worker Housing

13 Kinsley Pl Canton r 1870

CAN.218 Canton Hardware Company Double Worker Housing

19-25 Kinsley Pl Canton c 1836

CAN.219 Canton Hardware Company Worker Housing 27 Kinsley Pl Canton r 1860

CAN.906 Forge Pond Bridge Kinsley Pond Canton c 1845

Inv. No. Property Name Street Town Year

Thursday, July 6, 2017 1 3Page of

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CAN.296 Messinger, Virgil J. and Vernon S. House 166 Messinger St Canton c 1848

CAN.908 Canton Viaduct Neponset St Canton 1834

CAN.69 Union Hall Tavern 35 Neponset St Canton 1840

CAN.11 Revere, Joseph Warren House 91 Neponset St Canton c 1825

CAN.133 Tucker House 386 Neponset St Canton r 1840

CAN.134 Tucker, E. House 394 Neponset St Canton r 1840

CAN.401 Morrison, Francis J. House 260 Norfolk St Canton c 1927

CAN.400 McKay, Walter House 273 Norfolk St Canton c 1928

CAN.132 Rising Sun Stove Polish Factory - Storehouse 35 Pequit St Canton c 1884

CAN.95 Guild, Horace House 448 Pleasant St Canton r 1805

CAN.318 Gill, Benjamin House 469 Pleasant St Canton c 1825

CAN.330 Draper, Charles House 643 Pleasant St Canton c 1869

CAN.96 Canton Police Station 40 Revere St Canton 1931

CAN.126 Revere, Paul and Son Copper Rolling Mill 104 Revere St Canton 1850

CAN.127 Revere, Paul and Son Copper Draft Horse Stable 104 Revere St Canton c 1845

CAN.920 Revere, Paul and Son Copper Works Sluiceway 104 Revere St Canton r 1840

CAN.921 Revere, Paul and Son Copper Works Revetment Wall

104 Revere St Canton r 1850

CAN.97 Eureka Silk Mill #1 27 Rockland St Canton r 1885

CAN.98 Seavey, Foster and Bowman Boarding House 33 Rockland St Canton r 1870

CAN.104 Canton Junction Railroad Station 666 Sherman St Canton 1892

CAN.99 Boston & Canton Cotton Mill - Neponset Cotton Co.

59 Walpole St Canton c 1808

CAN.7 Washington St Canton r 1850

CAN.9 Washington St Canton r 1830

CAN.220 Belcher, Clifford Double House 115-117 Washington St Canton c 1840

CAN.221 Belcher, Clifford House 123 Washington St Canton 1845

CAN.222 McGharan, Thomas P. House 133 Washington St Canton c 1896

CAN.223 Presbry, Simon House and Machine Shop 142 Washington St Canton r 1826

CAN.224 Mansfield, William House 158 Washington St Canton r 1850

CAN.1 Dunbar, Dea. Thomas House 178-180 Washington St Canton c 1803

CAN.309 Robinson, J. Albert House 189 Washington St Canton c 1907

CAN.225 Kinsley, Adam Jr. - Shepard, James S. House 209 Washington St Canton r 1825

CAN.80 White, James House 216 Washington St Canton r 1815

CAN.226 American Net and Twine Company Worker Housing

239-241 Washington St Canton r 1860

CAN.70 Upham, Abner T. House 244 Washington St Canton r 1850

CAN.227 American Net and Twine Company Worker Housing

245-247 Washington St Canton r 1860

Inv. No. Property Name Street Town Year

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CAN.228 American Net and Twine Company Worker Housing

251 Washington St Canton 1882

CAN.229 Hayward, Joseph H. - Lord, William House 260 Washington St Canton 1835

CAN.393 Shepard, James S. Stable 270 Washington St Canton c 1854

CAN.230 Shepard, Luke House 271 Washington St Canton c 1820

CAN.394 Shepard, James S. Carriage Barn 272-274 Washington St Canton c 1865

CAN.71 Shepard, James Stratton House 294-296 Washington St Canton c 1854

CAN.399 Lancaster, James S. House 299 Washington St Canton c 1853

CAN.3 Gridley, Gen. Richard School 300 Washington St Canton 1854

CAN.384 Crane, Simeon House 316 Washington St Canton r 1825

CAN.81 Crane, Dr. Albert A. - Foster, Frederick A. House 352 Washington St Canton 1853

CAN.72 Wentworth, Nathaniel House 353 Washington St Canton r 1840

CAN.111 Allen, William H. House 366 Washington St Canton c 1876

CAN.5 Wentworth, Nathaniel House 391 Washington St Canton r 1800

CAN.82 Gardner, E. House 428 Washington St Canton r 1820

CAN.6 Smith, Sidney L. House 442 Washington St Canton r 1840

CAN.83 Webster, Frank G. House 455 Washington St Canton c 1870

CAN.84 Abbot, Dr. Ezra House 470-472 Washington St Canton c 1837

CAN.73 Messinger, Jonathan House 475 Washington St Canton r 1840

CAN.74 Capen, E. Building 482 Washington St Canton r 1855

CAN.75 Capen, E. Building 484-486 Washington St Canton r 1865

CAN.76 Crane, Friend Double House 505-507 Washington St Canton r 1820

CAN.85 Canton Institution for Savings 557 Washington St Canton 1927

CAN.120 Kinsley Axle Shop 641 Washington St Canton 1859

CAN.77 Hemenway School - Canton High School 660 Washington St Canton 1911

CAN.106 U. S. Post Office - Canton Main Branch 661 Washington St Canton 1935

CAN.78 Canton Public Library 786 Washington St Canton c 1901

CAN.103 Canton Town Hall - Memorial Hall 801 Washington St Canton 1878

CAN.86 Trinity Episcopal Church 824 Washington St Canton 1897

CAN.87 Beals, W. House 847 Washington St Canton r 1815

CAN.128 Rising Sun Stove Polish Factory - North Mill 869 Washington St Canton c 1884

CAN.129 Rising Sun Stove Polish Factory - South Mill 869 Washington St Canton c 1884

CAN.130 Rising Sun Stove Polish Factory - Boiler House 869 Washington St Canton c 1884

CAN.139 Rising Sun Stove Polish Factory - Boiler House 869 Washington St Canton c 1884

CAN.131 Rising Sun Stove Polish Factory - Carriage House

879 Washington St Canton c 1884

CAN.100 York District Schoolhouse #4 301 York St Canton r 1815

Inv. No. Property Name Street Town Year

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