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Russian Quartz
Company profile
Head office & production sites location Russia, Cheliabinsk region, Kyshtym
Shareholders ▪ OJSC «Kyshtymsky mining & processing plant», Russia
▪ Sumitomo Corp., Japan
▪ OJSC «RUSNANO», Russia
▪ «KvartzVIK» LLC , Russia
Foundation date August 2011
Products ▪High Purity Quartz Concentrates (HPQ)
grades: RQ-4K, RQ-3K, RQ-2K/Ki/Kf, RQ-1К;
Production capacity ▪3 500 MT/year - current HPQ production,
▪6 000 MT/year - planned in 2022
Employees 190 persons
Resourse base - reserves – more than 1 million tons of quartz ore
- unique vein 175 with proven by JORC audit quartz ore reserves for 30 year full-capacity production
Location of production sites
С
Ю
N
SChelyabinsk region
Moscow
Chelyabinsk
Kyshtym
100 km
- railway
- road
Wet Processing Plant (WPP) in Kyshtym (Wet Processing Site)
Underground mine at the vein 175 and Dry Processing Plant (DPP) near to the quartz deposit (vein 175) (Dry Processing Site)
Production sites of the Company are located in Kyshtym, Chelyabinsk region, Russia.This region is historically industrialized, so the Company does not have any limits in terms of infrastructure and logistics. In total, Russian quartz LLC has two production sites:
Resource base
Main source of raw quartz – vein 175SiO2
Year-round operations
> 30years
Reserves of vein 175 more than 500 000 MT (more than 30 years of Company life)
More than 1 million MT of quartz reserves for different applications
▪ Raw material base of Russian Quartz LLC is unique deposit of granular quartz in Kyshtym.
▪ Total length of deposit is 15km with width 1-3km, area – 20km2.
▪ Proven reserves of quartz ore in Kyshtym deposit are over 1 million tons.
▪ Kyshtym deposit of granular quartz was developed in 1960-1970 and for more than 50 years beensuccessfully used as a raw material for different applications
Vein 175 as a source of HPQ for semiconductor applications
▪ Vein №175 has natural quartz with uniqueproperties combination (like minimum B & Pcontent, the lowest Al, Alkali, Cu, Ni, Cr, Fecontent, low bubbles and mineral inclusionscontent).
▪ After purification total sum of impurities ingrades RQ-2K/1K less than 10 ppm that allowto use quartz from this vein in all applicationswhere quartz glass products are needed.
▪ The chemical and mineralogical composition ofquartz ore and HPQ produced from it, isunchanged in the entire volume of the vein175, which allows consumers to rely on theconsistently high and stable quality of Russianquartz products
▪ In 2014, an international company IMC Montan audited vein 175 and confirmed the resources of quartz orein the amount of more than 500 thousand tons
▪ For the organization of stable operation and reliability of supplies to consumers, the Company maintainsthe level of ore reserves at the warehouse sufficient for the smooth operation of the company for 9months. It also allows for an early analysis of the quality of ore entering the production.
Vein 175 as a source of HPQ for semiconductor applications
The constancy of the quality of the quartz ore of the vein 175 is confirmed by both the long-term operation ofthe mine and the stable qualitative characteristics of HPQ produced from this quartz ore. As an example, theaverage values of the chemical composition of the grade RQ-2K for the period 2014-2018 are given in thefollowing table:
Year Al B Ca Cr Cu Fe K Li Mg Mn Na Ni Ti
2014 5 0,08 0,33 0,03 0,01 0,35 0,2 0,3 0,1 0,01 0,41 0,01 3
2015 4 0,08 0,16 0,01 0,01 0,18 0,2 0,3 0,1 0,01 0,36 0,01 3
2016 4 0,08 0,16 0,01 0,01 0,20 0,2 0,3 0,1 0,01 0,35 0,01 3
2017 4 0,08 0,12 0,01 0,01 0,18 0,1 0,3 0,1 0,01 0,29 0,01 3
2018 4 0,08 0,11 0,01 0,01 0,14 0,1 0,3 0,1 0,01 0,29 0,01 3
Improving the quality of a number of elements is associated with the continuous improvement of theenrichment technology of Russian quartz, while the quality of the ore itself remains consistently high
RQ’s products
GradeSum of impurities,
no more thanApplication
RQ-3K <12 ppmQuartz lighting, including automotive xenon, halogen and HID
lamps, outer layer of crucibles for photovoltaic industry
RQ-2Kf <10 ppm Large diameter quartz tubes and ingots
RQ-2K <10 ppmCzochralski crucibles for PV industry,
quartz tubes and ingots, quartz lighting
RQ-2Ki <9 ppmCzochralski crucibles for PV and semiconductor industry (inner
layer), large diameter quartz tubes and ingots
RQ-1К <9 ppmRQ’s grade after chlorination process, developed for Czochralski
crucibles and quartz glass for semiconductor industry
RQ’s HPQ chemical content (typical value), ppm
Grade Al B Ca Cr Cu Fe K Li Mg Ni Na Ti
RQ-3K 6 n/a 0,5 n/a n/a 0,5 0,3 0,3 0,2 <0,1 0,6 2,9
RQ-2K 4,3 <0,1 0,2 <0,01 <0,01 0,2 0,2 0,3 0,1 <0,1 0,3 2,9
RQ-2Kf 4,2 <0,1 0,2 <0,01 <0,01 0,2 0,1 0,3 0,1 <0,01 0,3 2,8
RQ-2Ki 4,1 <0,1 0,1 <0,01 <0,01 0,1 0,1 0,3 0,1 <0,01 0,3 2,8
RQ-1K 3,8 0,07 0,1 <0,001 <0,001 0,05 0,03 0,3 <0,1 <0,001 0,06 2,8
Analytical lab
Russian quartz has a modern laboratory that allows to perform all thenecessary analyzes to assess the quality of ore and finished high-purityconcentrates, namely:
- Chemical analysis (ICP-OES method).Accuracy of determining the content of main impurity elements – 0,01 ppm, for Cu, Ni, Cr – 0,001 ppm
- Mineralogical analysis
- Particle size distribution analysis (sieve analysis)
- Bulk density analysis
All laboratory equipment undergoes the necessary checkout procedures in a timely manner, as well as cross-correlation procedures with consumers' analytical laboratories in order to avoid errors and deviations in assessing the quality of the finished product.
In addition, the laboratory of Russian Quartz has all the necessary competencies and equipment for the development of new grades of HPQ for the specific requirements of consumers.
RQ’s quality system: general principles
Russian Quartz’s production plantsare ISO 9001:2015 certified for production and enrichment of high-purity quartz concentrates by TUV NORD CERT GmbH (Germany)
In addition to the ISO 9001: 2015 standards, Russian Quartz has developed and applied its own quality control procedures, allowing to control all parameters and aspects of the production of HPQ, from ore quality control to finished product storage and logistics to the consumer
RQ’s quality system: organization chart
Chart of Quality System of Russian Quartz LLCQ
uality
Directo
r
Sta
ff
knowledge HR Director
skills Plant managers
motivation HR Director
Pro
duction
environm
ent plants Plant managers
warehouses Head of procurement department
Pro
duction p
rocess technological processes Chief technologist
materials Head of procurement department
equipment Chief engineer
Quality Control of the product
Head of QC Department
RQ’s quality system: traceability
As a fundamental document for tracing the technological parameters of the production of HPQ for each of the grade a quality control chart is used
RQ’s quality system: traceability
Based on the data defined in the quality control chart, a passport of lot of finished products is drawn up for each lot indicating the technological parameters of lot production at each stage of the production process and the quality characteristics of the finished product
Passport of finished products lot
No. of finished product lot 12I0028/18
Attritioning Flotation
№ КSО lot Date ShiftAttritioning
tank, №
HFWater volume
for attritioning, l
Timemin
HF Т, ⁰C pH Water volume, l
Conc.%
Volumel
conc,% 1 1
1Ф1379/3 25.06.18 1 1 22,1 4,1 120 20 21,1 22 3,0 541,0
Washing of intermediate product, dehydration
№ КSО lot Date regimeTimemin
Т, ⁰CWater volume, l
pH W, % Weight, kg
1ф1379/3 25.06.18 40 22 2600 5 14,4 412
Acid treatment
Washing, dehydration
№ КSО lot DateWeight of charge, kg
Regime Reactor, №
HF Т of treatment, ºС Time. min
рН W, % Time. minWater
volume, lconc.,% Volume, l 30 60
1ф1379/3 26.06.18 412 3/20.04.18 1 32,5 120,0 43,90 46,80 90,00 6 10,6 60 2500
Drying+calcination
Magnetic separation
Packing
№ КSО lot DateOverall time,
minDrying line,
№Drying furnace Т of drying, ⁰C
Calcination furnace.
Т of calcination, ⁰C
Magnetic separator Q, kg/h Type of packing Net weight, kg
1ф1379/3 05.07.18 145 3 Xerion 730 RGQJ-90-12 1100 CG-180x99,3
барабан 220
Bulk density, particle size distribution
Date of analysis Grade № of lotFraction, micron
Bulk density,g/ml+180 micron +160 micron +150 micron +125 micron +100 micron +75 micron +56 micron
06.07.2018 RQ-2Ki 12I0028/18 75-180 1,21 0,0 6,0 7,4 25,6 29,4 27,6 4,0
Chemical analysis results
Al B Ca Cr Cu Fe K Li Mg Mn Na Ni Ti
12I0028/18 4,1 0,06 0,07 0,01 <0,01 0,09 0,11 0,30 0,06 <0,01 0,28 <0,01 2,8
QC acceptance
Date Product solution Person in charge Full name Signature
09.07.18 Accepted Popova L.I.
Chief technologist _____________________________________
Head of QC Dept ___________________________________________
Deputy Head of WPP on production ______________________________
RQ’s quality system: SPC & PCN
In order to arrange continuous monitoring of production processes and product quality, Russian Quartz uses the SPC methodology to estimate deviations using the “3-sigma” method. At the same time, the average values (CL) and tolerances (UCL / LCL), which are updated annually on the basis of accumulated statistics, are established for each grade.
0
0,05
0,1
0,15
0,2
0,25
0,3
0,35
0,4
0,45
1 4 7 10 13 16 19 22 25 28 31 34 37 40 43 46 49 52 55 58 61 64 67
RQ-2K (Fe,ppm)
Spec (Fe)
UCL (Fe)
CL (Fe)
LCL (Fe)
Actual (Fe)
SPC data Grade: RQ-2K Period: 2018
Grade/RQ-2K Al B Ca Cr Cu Fe K Li Mg Mn Na Ni Ti
UCL 4,5 0,11 0,28 0,01 0,013 0,33 0,23 0,33 0,17 0,010 0,44 0,01 3,2
CL 3,9 0,08 0,13 0,01 0,010 0,18 0,14 0,30 0,11 0,010 0,29 0,01 2,9
LCL 3,3 0,05 0,01 0,01 0,001 0,03 0,05 0,27 0,05 0,001 0,14 0,01 2,6
In the event of a significant change in product/process parameters, the Company uses the PCN consumer notification procedure.
RQ’s quality system: SPC & PCN
Russian Quartz LLCAddress: 3, Kaslinskoye highway, Kyshtym, Chelyabinsk region, Russia, ZIP code: 456870tel.: +7 (35151) 4-38-45fax: +7 (35151) 4-38-48e-mail: [email protected]: http://russianquartz.com/