Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

25.2525

25.1369

27.2942

26.3845

26.4673

26.3715

25.2873

24.6068

25.4768

24.9591

25.1376

25.0026

Final Conc

24.8930

25.1833

25.3477

24.8839

25.3495

0.1597

0.2765

0.5871

0.7927

0.5443

0.3975

0.2897

0.0852

0.5228

0.3578

0.5034

0.3485

Resp Ratio

0.5683

0.2461

1.0045

0.5192

0.6646

12909

12909

4039

4039

4039

4039

8704

12909

10316

10316

6986

10316

ISTD Resp

4223

4223

4223

8704

8704

2062

3570

2372

3202

2199

1605

2521

1100

5393

3691

3517

3595

Resp

2400

1039

4242

4519

5785

4.545

4.653

5.391

5.816

6.334

6.438

3.518

3.902

4.169

4.035

4.056

4.106

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.982

1.174

2.465

3.194

3.286

D5-oxazepam

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

midazolam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Acq Time 3/8/2007 10:50 Acq Method Benzos Mix Unit Pos APCI Segs.m

Position P1-F3 Inj Vol -1

Data File Benzo Cal03.d Sample Name 25 Std

Sample Type Calibration Dilution 1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Instrument Operator

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:37 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:37:16.9984544-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 1 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Compound Graphics

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 2 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 3 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flurazepam

alprazolam

lorazepam

desalkylflurazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 4 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

temazepam

chlordiazepoxide

nordiazepam

midazolam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 5 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

diazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 6 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

49.0808

49.6216

43.8520

45.0893

45.3001

45.6232

48.6334

52.0534

48.3550

50.2325

48.9314

50.1603

Final Conc

50.4860

48.4112

48.0629

51.4854

48.2786

0.3151

0.5463

0.8780

1.4729

0.8937

0.6594

0.5977

0.1882

0.8937

0.6893

1.0320

0.7023

Resp Ratio

1.1754

0.5181

1.9755

1.1632

1.3451

13606

13606

4931

4931

4931

4931

8909

13606

10731

10731

6858

10731

ISTD Resp

4417

4417

4417

8909

8909

4287

7433

4330

7264

4407

3252

5325

2560

9590

7397

7077

7536

Resp

5192

2288

8725

10363

11983

4.540

4.658

5.404

5.831

6.324

6.449

3.513

3.905

4.170

4.031

4.058

4.110

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.982

1.178

2.467

3.192

3.287

D5-oxazepam

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

midazolam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Acq Time 3/8/2007 11:00 Acq Method Benzos Mix Unit Pos APCI Segs.m

Position P1-F4 Inj Vol -1

Data File Benzo Cal04.d Sample Name 50 Std

Sample Type Calibration Dilution 1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Instrument Operator

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:37 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:37:16.9984544-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 7 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Compound Graphics

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 8 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 9 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flurazepam

alprazolam

lorazepam

desalkylflurazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 10 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

temazepam

chlordiazepoxide

nordiazepam

midazolam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 11 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

diazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 12 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

122.2640

122.1752

128.0163

120.5695

126.9027

125.5977

123.3556

122.8973

125.7753

124.3526

130.7423

123.0284

Final Conc

125.4191

136.0114

130.6195

118.8979

127.1428

0.8085

1.3739

2.4551

4.2177

2.5097

1.8318

1.5835

0.4539

2.2815

1.7357

2.9265

1.7841

Resp Ratio

3.1011

1.6064

5.7017

2.7953

3.6855

13101

13101

4723

4723

4723

4723

8960

13101

11176

11176

6538

11176

ISTD Resp

4173

4173

4173

8960

8960

10592

17999

11594

19918

11852

8651

14188

5947

25498

19398

19133

19938

Resp

12941

6704

23794

25046

33023

4.534

4.650

5.392

5.814

6.327

6.437

3.509

3.898

4.165

4.018

4.054

4.106

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.982

1.176

2.465

3.188

3.286

D5-oxazepam

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

midazolam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Acq Time 3/8/2007 11:11 Acq Method Benzos Mix Unit Pos APCI Segs.m

Position P1-F5 Inj Vol -1

Data File Benzo Cal05.d Sample Name 125 Std

Sample Type Calibration Dilution 1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Instrument Operator

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:37 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:37:16.9984544-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 13 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Compound Graphics

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 14 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 15 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flurazepam

alprazolam

lorazepam

desalkylflurazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 16 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

temazepam

chlordiazepoxide

nordiazepam

midazolam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 17 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

diazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 18 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

264.0711

260.7158

281.6412

275.4278

275.7316

277.8351

266.4532

263.2900

255.3699

250.6731

242.2913

254.8781

Final Conc

246.5235

236.0636

247.2174

250.4847

248.5578

1.8343

3.0711

5.7596

9.8489

5.8837

4.4382

3.4714

0.9806

5.0634

3.7742

5.7023

3.9568

Resp Ratio

6.6792

2.9698

11.4914

5.9811

7.2888

12424

12424

4113

4113

4113

4113

9490

12424

11064

11064

7240

11064

ISTD Resp

4243

4243

4243

9490

9490

22790

38157

23692

40513

24202

18256

32945

12184

56020

41757

41287

43776

Resp

28338

12600

48755

56764

69174

4.545

4.662

5.400

5.833

6.315

6.447

3.517

3.906

4.175

4.025

4.064

4.111

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.984

1.179

2.470

3.196

3.292

D5-oxazepam

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

midazolam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Acq Time 3/8/2007 11:21 Acq Method Benzos Mix Unit Pos APCI Segs.m

Position P1-F6 Inj Vol -1

Data File Benzo Cal06.d Sample Name 250 Std

Sample Type Calibration Dilution 1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Instrument Operator

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:37 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:37:16.9984544-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 19 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Compound Graphics

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 20 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 21 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flurazepam

alprazolam

lorazepam

desalkylflurazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 22 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

temazepam

chlordiazepoxide

nordiazepam

midazolam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 23 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

diazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 24 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

491.2347

493.4810

479.3994

516.4187

482.3231

481.8240

487.4619

476.3922

495.0952

499.7925

504.1232

497.1498

Final Conc

503.0092

508.6383

499.4428

515.3953

506.6413

3.6690

6.2682

10.8233

18.6123

11.4809

8.7005

6.3872

1.7801

11.7231

8.7367

13.0904

8.6720

Resp Ratio

16.1584

7.3365

26.1271

12.3948

14.9478

12795

12795

4463

4463

4463

4463

9637

12795

10219

10219

6451

10219

ISTD Resp

3717

3717

3717

9637

9637

46946

80203

48302

83063

51236

38828

61553

22776

119797

89279

84446

88618

Resp

60068

27273

97125

119448

144052

4.548

4.660

5.399

5.827

6.319

6.443

3.518

3.910

4.177

4.024

4.065

4.114

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.983

1.180

2.471

3.200

3.295

D5-oxazepam

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

midazolam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Acq Time 3/8/2007 11:31 Acq Method Benzos Mix Unit Pos APCI Segs.m

Position P1-F7 Inj Vol -1

Data File Benzo Cal07.d Sample Name 500 Std

Sample Type Calibration Dilution 1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Instrument Operator

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:37 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:37:16.9984544-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 25 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Compound Graphics

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 26 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 27 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flurazepam

alprazolam

lorazepam

desalkylflurazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 28 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

temazepam

chlordiazepoxide

nordiazepam

midazolam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 29 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

diazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 30 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

0.5431

ND

ND

4.6309

ND

ND

3.5495

ND

ND

ND

2.1557

ND

Final Conc

ND

ND

ND

3.6723

3.7616

0.0014

0.0034

0.0017

0.0034

0.0099

0.0029

0.0033

0.0024

0.0014

Resp Ratio

0.0056

0.0240

12490

12490

3974

3974

3974

3974

8516

12490

10196

10196

6786

10196

ISTD Resp

4216

4216

4216

8516

8516

17

14

7

13

39

25

34

16

14

Resp

48

204

4.614

5.409

5.239

6.531

6.529

2.958

4.012

3.953

4.225

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

3.301

3.311

D5-oxazepam

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

midazolam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Acq Time 3/8/2007 10:40 Acq Method Benzos Mix Unit Pos APCI Segs.m

Position P1-F2 Inj Vol -1

Data File Benzo Cal02.d Sample Name Blank

Sample Type Blank Dilution 1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Instrument Operator

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:37 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:37:16.9984544-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 31 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Compound Graphics

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 32 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 33 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flurazepam

alprazolam

lorazepam

desalkylflurazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 34 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

temazepam

chlordiazepoxide

nordiazepam

midazolam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 35 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

diazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 36 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ND

ND

ND

ND

ND

ND

3.8224

ND

ND

ND

145.6462

ND

Final Conc

ND

ND

10.1229

ND

ND

0.0046

0.0065

0.0042

3.2845

Resp Ratio

0.3668

12808

12808

4277

4277

4277

4277

8160

12808

10428

10428

6522

10428

ISTD Resp

4599

4599

4599

8160

8160

20

53

43

21422

Resp

1687

5.355

3.507

3.749

4.058

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

2.463

D5-oxazepam

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

midazolam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Acq Time 3/8/2007 12:01 Acq Method Benzos Mix Unit Pos APCI Segs.m

Position P1-F9 Inj Vol -1

Data File Benzo Cal09.d Sample Name 123456

Sample Type Sample Dilution 1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Instrument Operator

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:37 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:37:16.9984544-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 37 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Compound Graphics

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 38 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 39 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flurazepam

alprazolam

lorazepam

desalkylflurazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 40 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

temazepam

chlordiazepoxide

nordiazepam

midazolam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 41 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

diazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 42 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

91.6483

98.9742

ND

4.6528

61.8378

ND

ND

97.7468

104.7185

ND

93.0424

52.9328

Final Conc

163.8184

99.0015

ND

95.4207

3.1130

0.5991

1.1047

0.0039

0.0025

1.2078

0.0019

0.3596

1.8838

2.0386

0.7419

Resp Ratio

4.1733

1.1346

2.2269

0.0047

13759

13759

4054

4054

4054

4054

8840

13759

11134

11134

7427

11134

ISTD Resp

4228

4228

4228

8840

8840

8243

15199

16

10

4897

8

4947

20974

15140

8260

Resp

17646

4797

19686

42

4.541

4.655

5.319

5.892

6.325

6.863

3.901

4.171

4.056

4.115

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.982

1.180

3.195

3.272

D5-oxazepam

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

midazolam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Acq Time 3/8/2007 11:51 Acq Method Benzos Mix Unit Pos APCI Segs.m

Position P1-F8 Inj Vol -1

Data File Benzo Cal08.d Sample Name Benzo QC

Sample Type QC Dilution 1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Instrument Operator

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:37 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:37:16.9984544-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 43 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Compound Graphics

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 44 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 45 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

flurazepam

alprazolam

lorazepam

desalkylflurazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 46 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

temazepam

chlordiazepoxide

nordiazepam

midazolam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 47 of 48 Printed at: 9:37 PM on: 2/26/2010

Quantitative Analysis Sample Report

diazepam

QuantReport_ISTD_NotDetected_B_04_00.xlsx Page 48 of 48 Printed at: 9:37 PM on: 2/26/2010