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Production advantages using laser cladding as an additive manufacturing method Objective Is it possible to obtain the same material characteristics of a component using laser cladding as an additive manufacturing method compared to producing the component conventionally? This poster describes industrial trials with laser cladding and precipitation hardening heat treatment of thinwalled structures with the 17-4 PH stainless steel alloy. Due to the great relevance of the AM production methods for the aviation industry, the mechanical strength of the alloy given by the MMPDS document is used as a baseline. In order to improve the properties of the produced specimens, hot isostatic pressing was applied Conclusion and Outlook • The fabricated AM 17-4 PH responds readily to conventional H900 and H1100 heat treatments. • Poor elongation caused by a porous initial microstructure can be improved by a HIP treatment. • With the HIP treatment, the AM 17-4 PH complies with MMPDS minimum mechanical strength and elongation values. It would be highly relevant for the applica- tion of 17-4 PH to the aviation industry to verify whether the fatigue strength pro- perties are also comparable to those of conventionally produced 17-4 PH. Uffe Ditlev Bihlet, Michel Honoré and Peter Tommy Nielsen Method and Tests The AM 17-4 PH samples are manufactured using a purpose-built and commercially available laser cladding system. The powder entering the laser focal point is melted and deposited on the sample surface. Laser powers in the range 1.4 kW to 2.1 kW were applied. Hereafter the items are heat treated as per scheme Table 1. Hot Isostatic Pressing (HIP) is a common post-treatment which is routinely used on cast turbine components and on powder metallurgical parts. This treatment causes a signifi- cant improvement of the mechanical properties by closing and diffusion bonding internal pores and defects. This is accomplished at a high external pressure in the range of 800- 1000 bar and at temperatures close to the melting point of the alloy. The mechanical properties were quantified by tensile testing and elongation. The tensile test was conducted as described by ISO EN 6892-1. Samples were oriented in the build direction as well as perpendicular to the build direction. The fracture surfaces were inspected using scanning electron microscopy. Table 1. Heat treatments. Treatment HIP Solution treatment Ageing As fabricated - - - H900 - 1030°C x ½ hour 482°C x 1 hour HIP+H900 X 1030°C x ½ hour 482°C x 1 hour HIP+H1100 X 1030°C x ½ hour 593°C x 4 hours Minimum value as defined by MMPDS-08 744 721 1291 1406 1190 1018 1060 1361 1560 1240 500 700 900 1100 1300 1500 1700 1900 As fabricated As fabricated - Z-direction H900 - Z-direction HIP+H900 HIP+H1100 MPa 0.2 % yield stress Ultimate tensile strength 7,7 5,8 3,4 13,2 14,1 0 2 4 6 8 10 12 14 16 % elongation Minimum value as defined by MMPDS -08 As fabricated As fabricated - Z-direction H900 - Z-direction HIP+H900 HIP+H1100 Electron microscopy image of fracture surface Microstructure of AM 17-4 PH before and after the HIP treatment As fabricated Porosity Closed porosity HIP+H900 Results The results show that a post processing treatment consisting of a HIP cycle and a conven- tional precipitation hardening, vastly improves the mechanical strength and elongation va- lues of printed specimens, causing them to exceed the specified MMPDS values. forcetechnology.com

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Production advantages using laser cladding as an additive manufacturing method

ObjectiveIs it possible to obtain the same material characteristics of a component using laser cladding as an additive manufacturing method compared to producing the component conventionally?

This poster describes industrial trials with laser cladding and precipitation hardening heat treatment of thinwalled structures with the 17-4 PH stainless steel alloy. Due to the great relevance of the AM production methods for the aviation industry, the mechanical strength of the alloy given by the MMPDS document is used as a baseline. In order to improve the properties of the produced specimens, hot isostatic pressing was applied

Conclusion and Outlook• The fabricated AM 17-4 PH responds

readily to conventional H900 and H1100 heat treatments.

• Poor elongation caused by a porous initial microstructure can be improved by a HIP treatment.

• With the HIP treatment, the AM 17-4 PH complies with MMPDS minimum mechanical strength and elongation values.

It would be highly relevant for the applica-tion of 17-4 PH to the aviation industry to verify whether the fatigue strength pro-perties are also comparable to those of conventionally produced 17-4 PH.

Uffe Ditlev Bihlet, Michel Honoré and Peter Tommy Nielsen

Method and TestsThe AM 17-4 PH samples are manufactured using a purpose-built and commercially available laser cladding system. The powder entering the laser focal point is melted and deposited on the sample surface. Laser powers in the range 1.4 kW to 2.1 kW were applied. Hereafter the items are heat treated as per scheme Table 1.

Hot Isostatic Pressing (HIP) is a common post-treatment which is routinely used on cast turbine components and on powder metallurgical parts. This treatment causes a signifi-cant improvement of the mechanical properties by closing and diffusion bonding internal pores and defects. This is accomplished at a high external pressure in the range of 800-1000 bar and at temperatures close to the melting point of the alloy.

The mechanical properties were quantified by tensile testing and elongation. The tensile test was conducted as described by ISO EN 6892-1. Samples were oriented in the build direction as well as perpendicular to the build direction. The fracture surfaces were inspected using scanning electron microscopy.

Table 1. Heat treatments.

Treatment HIP Solution treatment Ageing

As fabricated - - -

H900 - 1030°C x ½ hour 482°C x 1 hour

HIP+H900 X 1030°C x ½ hour 482°C x 1 hour

HIP+H1100 X 1030°C x ½ hour 593°C x 4 hours

Minimum value as defined by MMPDS-08

744 721

1291

1406

1190

10181060

1361

1560

1240

500

700

900

1100

1300

1500

1700

1900

As fabricated As fabricated -Z-direction

H900 -Z-direction

HIP+H900 HIP+H1100

MP

a

0.2 % yield stress Ultimate tensile strength

7,7

5,8

3,4

13,2

14,1

0

2

4

6

8

10

12

14

16

% e

long

atio

n

Minimum value as defined by MMPDS -08

As fabricated As fabricated -Z-direction

H900 -Z-direction

HIP+H900 HIP+H1100

Electron microscopy image of fracture surface

Microstructure of AM 17-4 PH before and after the HIP treatment

As fabricated

Porosity

Closed porosity

HIP+H900

ResultsThe results show that a post processing treatment consisting of a HIP cycle and a conven-tional precipitation hardening, vastly improves the mechanical strength and elongation va-lues of printed specimens, causing them to exceed the specified MMPDS values.

forcetechnology.com