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POTW Name: City of Asheboro WWTP NPDES #: Date Sampled Effluent (ug/L) CAS Number Analyte Name Acronym 7/10/2019 Lab Qualifier(s) 8/8/2019 Lab Qualifier(s) 9/5/2019 Lab Qualifier(s) 12/7/2017 89 375-22-4 Perfluorobutanoic acid PFBA ND U (<2.54) ND U (<10.1) ND U (<1.7) 1/11/2018 937 375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.54) ND U (<10.1) ND U (<1.7) 2/1/2018 1011 335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.54) ND U (<10.1) 24.4 3/1/2018 212 335-76-2 Perfluorodecanoic acid PFDA ND U (<2.54) ND U (<10.1) 4.51 4/5/2018 397 307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.54) ND U (<10.1) 7.07 5/9/2018 75.7 375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.54) ND U (<10.1) 2.03 6/13/2018 77.7 375-85-9 Perfluoroheptanoic acid PFHpA 4.62 ND U (<10.1) 5.95 7/17/2018 48 355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<2.54) ND U (<10.1) ND U (<1.7) 8/22/2018 764 307-24-4 Perfluorohexanoic acid PFHxA 8.74 B 13.5 12.4 9/11/2018 182 68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.54) ND U (<10.1) 2.19 10/25/2018 31.6 375-95-1 Perfluorononanoic acid PFNA ND U (<2.54) ND U (<10.1) 3.87 11/8/2018 58.3 754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.57) ND U (<10.1) ND U (<2.57) 12/6/2018 217 2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.54) ND U (<10.1) 4.09 1/9/2019 167 2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.54) ND U (<10.1) ND U (<1.7) 2/5/2019 613 2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.54) ND U (<10.1) ND U (<1.7) 3/13/2019 159 2706-90-3 Perfluoropentanoic acid PFPeA 25.8 ND U (<10.1) ND U (<1.7) 4/17/2019 228 376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.54) ND U (<10.1) 11.4 5/8/2019 37 72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.54) ND U (<10.1) 7.15 6/4/2019 46.5 2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.54) ND U (<10.1) 5.04 7/10/2019 49.2 62037-80-3 Gen-X HFPO-DA NA ND U (<354.62) NA 8/22/2019 423 335-67-1 Perfluorooctanoic acid PFOA 9.47 10.6 11.7 9/4/2019 18.2 1763-23-1 Perfluorooctanesulfonic acid PFOS 19.8 18.8 19.2 10/22/2019 184 Sum of PFOA and PFOS 29.27 29.4 30.9 Total PFAS 68.43 42.9 121 7/10/2019 Lab Qualifier(s) 8/22/2019 Lab Qualifier(s) 9/4/2019 Lab Qualifier(s) 1, 4 - Dioxane* 49.2 423 18.2 *The City of Asheboro is working closely with an industrial user who is installing best available treatment technology to reduce 1,4 Dioxane in its discharge to the wastewater treatment plant in Jan. 2020. Lab Qualifiers NA - Not Applicable ND - Analyte concentration is not detected above the detection limit. B - Analyte found in the sample and associated method blank. U - The sample was not detected in the sample at the Reporting Limit. NC0026123 Influent Grab (ng/L) eDMR Effluent Grab (ug/L) 1,4 - Dioxane eDMR data

POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

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Page 1: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: City of Asheboro WWTP NPDES #: Date Sampled Effluent (ug/L)

CAS Number Analyte Name Acronym 7/10/2019 Lab Qualifier(s) 8/8/2019 Lab Qualifier(s) 9/5/2019 Lab Qualifier(s) 12/7/2017 89

375-22-4 Perfluorobutanoic acid PFBA ND U (<2.54) ND U (<10.1) ND U (<1.7) 1/11/2018 937

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.54) ND U (<10.1) ND U (<1.7) 2/1/2018 1011

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.54) ND U (<10.1) 24.4 3/1/2018 212

335-76-2 Perfluorodecanoic acid PFDA ND U (<2.54) ND U (<10.1) 4.51 4/5/2018 397

307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.54) ND U (<10.1) 7.07 5/9/2018 75.7

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.54) ND U (<10.1) 2.03 6/13/2018 77.7

375-85-9 Perfluoroheptanoic acid PFHpA 4.62 ND U (<10.1) 5.95 7/17/2018 48

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<2.54) ND U (<10.1) ND U (<1.7) 8/22/2018 764

307-24-4 Perfluorohexanoic acid PFHxA 8.74 B 13.5 12.4 9/11/2018 182

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.54) ND U (<10.1) 2.19 10/25/2018 31.6

375-95-1 Perfluorononanoic acid PFNA ND U (<2.54) ND U (<10.1) 3.87 11/8/2018 58.3

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.57) ND U (<10.1) ND U (<2.57) 12/6/2018 217

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.54) ND U (<10.1) 4.09 1/9/2019 167

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.54) ND U (<10.1) ND U (<1.7) 2/5/2019 613

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.54) ND U (<10.1) ND U (<1.7) 3/13/2019 159

2706-90-3 Perfluoropentanoic acid PFPeA 25.8 ND U (<10.1) ND U (<1.7) 4/17/2019 228

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.54) ND U (<10.1) 11.4 5/8/2019 37

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.54) ND U (<10.1) 7.15 6/4/2019 46.5

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.54) ND U (<10.1) 5.04 7/10/2019 49.2

62037-80-3 Gen-X HFPO-DA NA ND U (<354.62) NA 8/22/2019 423

335-67-1 Perfluorooctanoic acid PFOA 9.47 10.6 11.7 9/4/2019 18.2

1763-23-1 Perfluorooctanesulfonic acid PFOS 19.8 18.8 19.2 10/22/2019 184

Sum of PFOA and PFOS 29.27 29.4 30.9

Total PFAS 68.43 42.9 121

7/10/2019 Lab Qualifier(s) 8/22/2019 Lab Qualifier(s) 9/4/2019 Lab Qualifier(s)

1, 4 - Dioxane* 49.2 423 18.2

*The City of Asheboro is working closely with an industrial user who is installing best available treatment technology to reduce 1,4 Dioxane in its discharge to the wastewater treatment plant in Jan. 2020.

Lab Qualifiers

NA - Not Applicable

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

U - The sample was not detected in the sample at the Reporting Limit.

NC0026123

Influent Grab (ng/L)

eDMR Effluent Grab (ug/L)

1,4 - Dioxane eDMR data

Page 2: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Northeast Brunswick Regional NPDES #:

CAS Number Analyte Name Acronym 7/8/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/3/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA 10.6 ND U (<1.41) ND U (<1.34)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<0.323) ND U (<1.41) ND U (<1.34)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<0.323) ND U (<1.41) ND U (<1.34)

335-76-2 Perfluorodecanoic acid PFDA 2.45 1.8 3.27

307-55-1 Perfluorododecanoic acid PFDoA ND U (<0.323) 0.196 J 1.02 JB

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<0.323) ND U (<1.41) ND U (<1.34)

375-85-9 Perfluoroheptanoic acid PFHpA 11.7 8.15 18.8

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<0.323) ND U (<1.41) ND U (<1.34)

307-24-4 Perfluorohexanoic acid PFHxA 27.9 19.9 29.5

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<0.323) ND U (<1.41) ND U (<1.34)

375-95-1 Perfluorononanoic acid PFNA 1.69 0.871 J 1.13 J

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<0.323) ND U (<1.41) ND U (<1.34)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<0.323) ND U (<1.41) ND U (<1.34)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<0.323) ND U (<1.41) ND U (<1.34)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<0.323) ND U (<1.41) ND U (<1.34)

2706-90-3 Perfluoropentanoic acid PFPeA 77.8 ND U (<1.41) ND U (<1.34)

376-06-7 Perfluorotetradecanoic acid PFTeA 1.13 ND U (<1.41) 0.639 JB

72629-94-8 Perfluorotridecanoic acid PFTriA 0.155 JB ND U (<1.41) ND U (<1.34)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<0.323) ND U (<1.41) ND U (<1.34)

62037-80-3 Gen-X HFPO-DA ND U (<11.3) ND U (<49.31) ND U (<46.8)

757124-72-4 4:2 Fluorotelomer sulfonate 4:2 FTS ND U (<0.323) ND U (<1.41) ND U (<1.34)

27619-97-2 6:2 Fluorotelomer sulfonate 6:2 FTS 0.944 B 0.738 J 0.617 JB

39108-34-4 8:2 Fluorotelomer sulfonate 8:2 FTS 1.67 B 0.513 J 1.09 JB

335-67-1 Perfluorooctanoic acid PFOA 12.9 10 11.2

1763-23-1 Perfluorooctanesulfonic acid PFOS 14.8 11.3 ND U (<1.34)

Sum of PFOA and PFOS 27.7 21.3 11.2

Total PFAS 163.739 53.468 67.266

7/8/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/3/2019 Lab Qualifer(s)

1, 4 - Dioxane 3.81 2.48 5.6

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0086819

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 3: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Town of Burgaw Collection System NPDES #:

CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<1.84) ND U (<8.96) ND U (<0.244)

375-73-5 Perfluorobutanesulfonic acid PFBS 1.66 1.86 ND U (<0.244)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<1.78) ND U (<1.74) ND U (<0.244)

335-76-2 Perfluorodecanoic acid PFDA 0.766 J ND U (<1.79) ND U (<0.244)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<1.84) ND U (<1.79) 1.4

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<1.74) ND U (<1.70) ND U (<0.244)

375-85-9 Perfluoroheptanoic acid PFHpA 0.701 J 0.701 J ND U (<0.244)

355-46-4 Perfluorohexanesulfonic acid PFHxS 0.782 J ND U (<1.63) ND U (<0.244)

307-24-4 Perfluorohexanoic acid PFHxA 4.64 18.9 ND U (<0.244)

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<1.76) ND U (<1.72) ND U (<0.24)

375-95-1 Perfluorononanoic acid PFNA 0.926 J ND U (<1.79) 0.802

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<1.71) ND U (<8.33) ND U (<0.369)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA 3.7 ND U (<3.58) ND U (<0.244)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<3.67) ND U (<17.9) ND U (<0.244)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<1.73) ND U (<1.68) ND U (<0.244)

2706-90-3 Perfluoropentanoic acid PFPeA ND U (<1.84) ND U (<1.79) ND U (<0.244)

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<9.18) ND U (<8.96) 1.45

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<9.18) ND U (<8.96) ND U (<0.244)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<1.84) ND U (<8.96) ND U (<0.244)

335-67-1 Perfluorooctanoic acid PFOA 1.14 J 1.45 J 3.95

1763-23-1 Perfluorooctanesulfonic acid PFOS 2.3 4.08 9.29

Sum of PFOA and PFOS 3.44 5.53 13.24

Total PFAS 16.62 26.99 16.89

7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

1, 4 - Dioxane ND U (<400)* ND U (<1000)* ND U (<1000)*

*Reporting limit elevated due to matrix interference.

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

WQCS00150 CS Pemit (Burgaw discharges to Wallace)

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 4: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: East Burlington WWTP NPDES #:

CAS Number Analyte Name Acronym 7/16/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA 116 141 ND U (<1.75)

375-73-5 Perfluorobutanesulfonic acid PFBS 49.5 ND U (<4.88) ND U (<1.75)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.62) ND U (<4.88) ND U (<1.75)

335-76-2 Perfluorodecanoic acid PFDA 20.8 25.3 ND U (<1.75)

307-55-1 Perfluorododecanoic acid PFDoA 4.86 7.47 ND U (<1.75)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.62) ND U (<4.88) ND U (<1.75)

375-85-9 Perfluoroheptanoic acid PFHpA 873 845 5.39

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<2.62) 16.1 5.1

307-24-4 Perfluorohexanoic acid PFHxA 511 706 8.00

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.62) ND U (<4.88) ND U (<1.75)

375-95-1 Perfluorononanoic acid PFNA 11.7 10.6 ND U (<1.75)

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.62) ND U (<4.88) ND U (<2.65)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA 8.37 ND U (<4.88) ND U (<1.75)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA 16.6 16.1 ND U (<1.75)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.62) ND U (<4.88) ND U (<1.75)

2706-90-3 Perfluoropentanoic acid PFPeA 374 523 ND U (<1.75)

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.62) ND U (<4.88) ND U (<1.75)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.62) ND U (<4.88) ND U (<1.75)

2058-94-8 Perfluoroundecanoic acid PFUnA 4.97 5.28 ND U (<1.75)

335-67-1 Perfluorooctanoic acid PFOA 73.0 64.6 10.8

1763-23-1 Perfluorooctanesulfonic acid PFOS 49.8 56.4 12.5

Sum of PFOA and PFOS 122.8* 121.0* 23.3

Total 1990.8 2295.85 18.49

7/16/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

1, 4 - Dioxane 21.3 15.6 18.7

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0023868

Influent Grab (ng/L)

Influent Grab (ug/L)

*Due to dilution in the receiving stream, the PFOS and PFOA concentrations listed in the table above are not expected to cause an instream concentration greater than the EPA drinking water health advisory concentration

of 70 ng/L at downstream water supply intakes.

Page 5: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: South Burlington WWTP NPDES #:

CAS Number Analyte Name Acronym 7/16/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<2.75) ND U (<5.07) ND U (<1.82)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.75) ND U (<5.07) ND U (<1.82)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.75) ND U (<5.07) ND U (<1.82)

335-76-2 Perfluorodecanoic acid PFDA ND U (<2.75) 7.20 4.70

307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.75) ND U (<5.07) ND U (<1.82)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.75) ND U (<5.07) ND U (<1.82)

375-85-9 Perfluoroheptanoic acid PFHpA 4.62 7.29 24.7

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<2.75) ND U (<5.07) 8.92

307-24-4 Perfluorohexanoic acid PFHxA 13.9 B 27.7 73.1

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.75) ND U (<5.07) ND U (<1.82)

375-95-1 Perfluorononanoic acid PFNA ND U (<2.75) ND U (<5.07) 6.64

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.75) ND U (<5.07) ND U (<2.74)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.75) ND U (<5.07) ND U (<1.82)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.75) ND U (<5.07) ND U (<1.82)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.75) ND U (<5.07) ND U (<1.82)

2706-90-3 Perfluoropentanoic acid PFPeA 35.6 107 ND U (<1.82)

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.75) ND U (<5.07) ND U (<1.82)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.75) ND U (<5.07) ND U (<1.82)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.75) ND U (<5.07) ND U (<1.82)

335-67-1 Perfluorooctanoic acid PFOA 13.2 22.9 29.7

1763-23-1 Perfluorooctanesulfonic acid PFOS 20.2 6.57 23.7

Sum of PFOA and PFOS 33.4 29.47 53.4

Total 54.12 149.19 118.06

7/16/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

1, 4 - Dioxane 4.91 3.80 5.80

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

U - The sample was not detected in the sample at the Reporting Limit.

NC0023876

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 6: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Wilmington - James A. Loughlin (Northside) WWTP NPDES #:

CAS Number Analyte Name Acronym 7/9/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA 4.22 ND U (<9.37) 9.73

375-73-5 Perfluorobutanesulfonic acid PFBS 12.3 6.23 11.0

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<1.73) ND U (<1.82) ND U(<1.80)

335-76-2 Perfluorodecanoic acid PFDA 1.28 J 0.973 J 1.64 J

307-55-1 Perfluorododecanoic acid PFDoA ND U (<1.79) ND U (<1.87) ND U (<1.86)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<1.70) ND U (<1.78) ND U (<1.76)

375-85-9 Perfluoroheptanoic acid PFHpA 4.79 4.96 7.69

355-46-4 Perfluorohexanesulfonic acid PFHxS 3.78 3.69 4.31

307-24-4 Perfluorohexanoic acid PFHxA 14.0 14.2 17.6

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<1.71) ND U (<1.80) ND U (<1.78)

375-95-1 Perfluorononanoic acid PFNA 1.27 J 0.861 J 2.04

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<1.66) ND U (<8.71) ND U (<1.73)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<1.68) ND U (<3.75) ND U (<3.72)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<17.9) ND U (<18.7) ND U

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<1.68) ND U (<1.76) ND U (<1.75)

2706-90-3 Perfluoropentanoic acid PFPeA 15.6 15.9 20.3

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<8.93) ND U (<9.37) ND U (<9.29)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<8.93) ND U (<9.37) ND U (<1.86)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<1.79) ND U (<1.87) ND U (<1.86)

83329-89-9 11-chloroeicosafluoro-3-oxaundecane-1-sulfonate PF3OUdS ND U (<3.36) ND U (<3.53) ND U (<3.50)

1691-99-2 2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol N-EtFOSE ND U (<1.79) ND U (<9.37) ND U (<1.86)

24448-09-7 2-(N-methylperfluoro-1-octanesulfonamido)-ethanol N-MeFOSE ND U (<1.79) ND U (<9.37) ND U (<9.29)

13252-13-62,3,3,3-Tetrafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy)-

propanoic acid PFPrOPrA 10.5 14.7 9.81

801212-59-9 4-(Heptafluoroisopropoxy)hexafluorobutanoic acid PFECA-G ND UX (<3.57) ND UX (<3.75) ND UX (<3.72)

73606-19-6 9-chlorohexadecafluoro-3-oxanonane-1-sulfonate PF3ONS ND U (<1.66) ND U (<1.75) ND U(<1.73)

120226-60-0 Fluorotelomer sulfonate 10:2 10:2 FTS ND U (<3.43) ND U (<3.60) ND U (<3.57)

757124-72-4 Fluorotelomer sulfonate 4:2 4:2 FTS ND U (<16.8) ND U (<88.1) ND U (<87.3)

27619-97-2 Fluorotelomer sulfonate 6:2 6:2 FTS ND U (<17.0) ND U (<89.0) ND U (<88.2)

39108-34-4 Fluorotelomer sulfonate 8:2 8:2 FTS ND U (<3.43) ND U (<3.60) ND U (<17.8)

29311-67-9 Nafion Byproduct 1 ND U (<3.57) ND UX (<3.75) ND UX (<3.72)

749836-20-2 Nafion Byproduct 2 ND U (<3.57) 1.27 JX 1.88 JX

4151-50-2 N-ethylperfluoro-1-octanesulfonamide N-EtFOSA ND U (<3.57) ND U (<18.7) ND U (<3.72)

31506-32-8 N-methylperfluoro-1-octanesulfonamide N-MeFOSA ND U (<17.9) ND U (<18.7) ND U (<18.6)

39492-90-5 Perfluoro(3,5,7,9-tetraoxadecanoic) acid PFO4DA 2.61 JX 3.27 JX 5.9 X

39492-89-2 Perfluoro(3,5,7-trioxaoctanoic) acid PFO3OA 12.9 X 14.0 X 19.7 X

39492-88-1 Perfluoro(3,5-dioxahexanoic) acid PFO2HxA 29.7 X 36.5 X 46.8 X

674-13-5 Perfluoro-2-methoxyacetic acid PFMOAA 43.1 X 48.0 X 55.5 X

377-73-1 Perfluoro-3-methoxypropanoic acid PFMOPrA 13.8 X ND UX (<3.75) 17.6 X

863090-89-5 Perfluoro-4-methoxybutanic acid PFMOBA ND UX (<3.57) 6.67 X 2.72 JX

67905-19-5 Perfluorohexadecanoic acid PFHxDA ND U (<1.79) ND U (<1.87) ND U (<9.29)

958445-44-8 Sodium dodecafluoro-3H-4,8-dioxanonanoate ADONA ND U (<1.79) ND U (<1.87) ND U (<1.86)

335-67-1 Perfluorooctanoic acid PFOA 6.61 7.46 10.9

1763-23-1 Perfluorooctanesulfonic acid PFOS 8.83 9.29 19.3

Sum of PFOA and PFOS 15.44 16.75 30.2

Total of all PFAS 169.85 171.22 234.22

7/9/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

1, 4 - Dioxane ND U (<1.0) ND U (<1.0) ND U (<1.0)

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

X - The standards used to make the initial calibration curve did not meet the ISO 17025 criterion.

U - Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.

J - Value is estimated. (The result was below the reporting limit but over the detection limit.)

NC0023965

Influent Grab (ng/L)

Influent Grab (ug/L)

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POTW Name: Wilmington - M'Kean Maffitt (Southside) WWTP NPDES #:

CAS Number Analyte Name Acronym 7/9/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA 4.28 ND U (<1.89) 15.0

375-73-5 Perfluorobutanesulfonic acid PFBS 6.83 6.40 9.18

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<1.69) ND U (<1.83) ND U (<1.72)

335-76-2 Perfluorodecanoic acid PFDA ND U (<1.74) ND U (<1.89) ND U (<1.77)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<1.74) ND U (<1.89) ND U (<1.77)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<1.65) ND U (<1.79) ND U (<1.68)

375-85-9 Perfluoroheptanoic acid PFHpA 4.80 5.89 7.68

355-46-4 Perfluorohexanesulfonic acid PFHxS 3.41 3.60 4.17

307-24-4 Perfluorohexanoic acid PFHxA 13.0 14.8 14.0

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<1.67) ND U (<1.81) ND U (<1.70)

375-95-1 Perfluorononanoic acid PFNA 0.683 J 0.952 J 1.09 J

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<1.62) ND U (<8.77) ND U (<1.65)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<3.47) ND U (<3.77) ND U (<3.54)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<17.4) ND U (<18.9) ND U (<17.7)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<1.63) ND U (<1.77) ND U (<1.67)

2706-90-3 Perfluoropentanoic acid PFPeA 15.1 17.3 18.4

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<8.69) ND U (<9.43) ND U (<8.86)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<8.69) ND U (<9.43) ND U (<1.77)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<1.74) ND U (<1.89) ND U (<1.77)

83329-89-9 11-chloroeicosafluoro-3-oxaundecane-1-sulfonate PF3OUdS ND U (<3.27) ND U (<3.55) ND U (<3.34)

1691-99-2 2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol N-EtFOSE ND U (<8.69) ND U (<9.43) ND U (<1.77)

24448-09-7 2-(N-methylperfluoro-1-octanesulfonamido)-ethanol N-MeFOSE ND U (<8.69) ND U (<9.43) ND U (<8.86)

13252-13-62,3,3,3-Tetrafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy)-

propanoic acid PFPrOPrA 11.7 20.3 11.8

801212-59-9 4-(Heptafluoroisopropoxy)hexafluorobutanoic acid PFECA-G ND UX (<3.47) ND UX (<3.77) ND UX (<3.54)

73606-19-6 9-chlorohexadecafluoro-3-oxanonane-1-sulfonate PF3ONS ND U (<1.62) ND U (<1.76) ND U (<1.65)

120226-60-0 Fluorotelomer sulfonate 10:2 10:2 FTS ND U (<3.34) ND U (<3.62) ND U (<3.40)

757124-72-4 Fluorotelomer sulfonate 4:2 4:2 FTS ND U (<81.7) ND U (<88.7) ND U (<333)

27619-97-2 Fluorotelomer sulfonate 6:2 6:2 FTS ND U (<82.5) ND U (<89.6) ND U (<84.1)

39108-34-4 Fluorotelomer sulfonate 8:2 8:2 FTS ND U (<3.34) ND U (<3.62) ND U (<85.0)

29311-67-9 Nafion Byproduct 1 ND U (<3.47) ND UX (<3.77) ND UX (<3.54)

749836-20-2 Nafion Byproduct 2 1.57 JX 1.75 JX 2.48 JX

4151-50-2 N-ethylperfluoro-1-octanesulfonamide N-EtFOSA ND U (<3.47) ND U (<3.77) ND U (<3.54)

31506-32-8 N-methylperfluoro-1-octanesulfonamide N-MeFOSA ND U (<17.4) ND U (<18.9) ND U (<17.7)

39492-90-5 Perfluoro(3,5,7,9-tetraoxadecanoic) acid PFO4DA 4.27 X 4.32 X 7.90 X

39492-89-2 Perfluoro(3,5,7-trioxaoctanoic) acid PFO3OA 15.0 X 16.3 X 25.3 X

39492-88-1 Perfluoro(3,5-dioxahexanoic) acid PFO2HxA 36.0 X 47.1 X 60.8 X

674-13-5 Perfluoro-2-methoxyacetic acid PFMOAA 52.0 X 56.7 X 69.3 X

377-73-1 Perfluoro-3-methoxypropanoic acid PFMOPrA ND UX (<3.47) ND UX (<3.77) 21.4 X

863090-89-5 Perfluoro-4-methoxybutanic acid PFMOBA ND UX (<3.47) 7.20 X 2.96 JX

67905-19-5 Perfluorohexadecanoic acid PFHxDA ND U (<1.74) ND U (<1.89) ND U (<8.86)

958445-44-8 Sodium dodecafluoro-3H-4,8-dioxanonanoate ADONA ND U (<1.74) ND U (<1.89) ND U (<1.77)

335-67-1 Perfluorooctanoic acid PFOA 4.89 6.50 6.98

1763-23-1 Perfluorooctanesulfonic acid PFOS 13.4 8.53 11.8

Sum of PFOA and PFOS 18.29 15.03 18.78

Total PFAS 168.64 202.61 271.46

7/9/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

1, 4 - Dioxane 0.60 J 0.86 J ND (<1.0)

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

X - The standards used to make the initial calibration curve did not meet the ISO 17025 criterion.

U - Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.

J - Value is estimated. (The result was below the reporting limit but over the detection limit.)

NC0023973

Influent Grab (ng/L)

Influent Grab (ug/L)

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POTW Name: Cary Western Wake Regional Water Reclamation Facility NPDES #:

CAS Number Analyte Name Acronym 7/9/2019 Lab Qualifer(s) 8/13/2019 Lab Qualifer(s) 9/4/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA 15 ND U (<380) ND U (<39)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<1.1) ND U (<95) ND U (<9.7)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.4) ND U (<95) ND U (<9.7)

335-76-2 Perfluorodecanoic acid PFDA 1.1 J ND U (<95) ND U (<9.7)

307-55-1 Perfluorododecanoic acid PFDoA ND <1.2 ND U (<95) ND U (<9.7)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND <1.1 ND U (<95) ND U (<9.7)

375-85-9 Perfluoroheptanoic acid PFHpA 3.6 ND U (<95) ND U (<9.7)

355-46-4 Perfluorohexanesulfonic acid PFHxS ND <1.1 ND U (<95) ND U (<9.7)

307-24-4 Perfluorohexanoic acid PFHxA 15 B ND U (<95) 14 J

68259-12-1 Perfluorononanesulfonic acid PFNS ND <2.4 ND U (<95) ND U (<9.7)

375-95-1 Perfluorononanoic acid PFNA 0.41 J ND U (<95) ND U (<9.7)

754-91-6 Perfluorooctanesulfonamide PFOSA ND <3.0 ND U (<95) ND U (<9.7)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND <2.5 ND U (<95) ND U (<9.7)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND <2.5 ND U (<110) ND U (<12)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND <1.1 ND U (<95) ND U (<9.7)

2706-90-3 Perfluoropentanoic acid PFPeA 15 ND U (<95) 18 J

376-06-7 Perfluorotetradecanoic acid PFTeA ND <1.2 ND U (<95) ND U (<9.7)

72629-94-8 Perfluorotridecanoic acid PFTriA ND <1.2 ND U (<95) ND U (<9.7)

2058-94-8 Perfluoroundecanoic acid PFUnA ND <1.2 ND U (<95) ND U (<9.7)

335-67-1 Perfluorooctanoic acid PFOA 4.4 ND U (<95) ND U (<9.7)

1763-23-1 Perfluorooctanesulfonic acid PFOS ND U (<1.2) ND U (<95) ND U (<9.7)

Sum of PFOA and PFOS 4.4 0 0

Total PFAS 54.51 0 32

7/9/2019 Lab Qualifer(s) 8/13/2019 Lab Qualifer(s) 9/4/2019 Lab Qualifer(s)

1, 4 - Dioxane ND U (<2.0) 2.32 2.66

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

J - The reported value is an estimate. The value is less than the Reporting Limit.

NC0088846

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 9: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: City of Clinton - Norman H. Larkins WWTP NPDES #:

CAS Number Analyte Name Acronym 7/11/2019 Lab Qualifer(s) 8/7/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<9.17) ND U (<10.1) ND U (<1.34)

375-73-5 Perfluorobutanesulfonic acid PFBS 1.12 J 2.6 ND U (<1.34)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<1.78) ND U (<1.97) ND U (<1.34)

335-76-2 Perfluorodecanoic acid PFDA ND U (<1.83) ND U (<2.03) 0.452 J

307-55-1 Perfluorododecanoic acid PFDoA ND U (<1.83) ND U (<2.03) ND U (<1.34)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<1.74) ND U (<1.93) ND U (<1.34)

375-85-9 Perfluoroheptanoic acid PFHpA 1.17 J 1.24 J 4.01

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<1.67) ND U (<1.84) ND U (<1.34)

307-24-4 Perfluorohexanoic acid PFHxA 10.7 8.47 9.21

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<1.76) ND U (<2.03) ND U (<1.34)

375-95-1 Perfluorononanoic acid PFNA ND U (<1.83) ND U (<2.03) 0.503 J

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<1.71) ND U (<1.88) ND U (<1.34)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<3.67) ND U (<4.05) ND U (<1.34)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<3.67) ND U (<4.05) ND U (<1.34)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<1.72) ND U (<1.91) ND U (<1.34)

2706-90-3 Perfluoropentanoic acid PFPeA 5.42 12.2 115

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<9.17) ND U (<10.1) ND U (<1.34)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<9.17) ND U (<10.1) ND U (<1.34)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<1.83) ND U (<2.03) ND U (<1.34)

335-67-1 Perfluorooctanoic acid PFOA 2.19 2.46 4.07

1763-23-1 Perfluorooctanesulfonic acid PFOS 2.29 2.54 10.2

Sum of PFOA and PFOS 4.48 5.00 14.27

Total PFAS 22.89 29.51 143.45

7/11/2019 Lab Qualifer(s) 8/7/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

1, 4 - Dioxane ND U (<400)* ND U (<1000)* ND U (<1000)*

*Reporting limit elevated due to matrix interference.

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0020117

Influent Grab (ng/L)

Influent Grab (ug/L)

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POTW Name: Columbus County WWTP NPDES #:

CAS Number Analyte Name Acronym

375-22-4 Perfluorobutanoic acid PFBA

375-73-5 Perfluorobutanesulfonic acid PFBS

335-77-3 Perfluorodecanesulfonic acid PFDS

335-76-2 Perfluorodecanoic acid PFDA

307-55-1 Perfluorododecanoic acid PFDoA

375-92-8 Perfluoroheptanesulfonic acid PFHpS

375-85-9 Perfluoroheptanoic acid PFHpA

355-46-4 Perfluorohexanesulfonic acid PFHxS

307-24-4 Perfluorohexanoic acid PFHxA

68259-12-1 Perfluorononanesulfonic acid PFNS

375-95-1 Perfluorononanoic acid PFNA

754-91-6 Perfluorooctanesulfonamide PFOSA

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA

2706-91-4 Perfluoropentanesulfonic acid PFPeS

2706-90-3 Perfluoropentanoic acid PFPeA

376-06-7 Perfluorotetradecanoic acid PFTeA

72629-94-8 Perfluorotridecanoic acid PFTriA

2058-94-8 Perfluoroundecanoic acid PFUnA

62037-80-3 Gen-X HFPO-DA

757124-72-4 4:2 Fluorotelomer sulfonate 4:2 FTS

27619-97-2 6:2 Fluorotelomer sulfonate 6:2 FTS

39108-34-4 8:2 Fluorotelomer sulfonate 8:2 FTS

335-67-1 Perfluorooctanoic acid PFOA

1763-23-1 Perfluorooctanesulfonic acid PFOS

Sum of PFOA and PFOS

Total PFAS

1, 4 - Dioxane

NC0087947

Influent Grab (ng/L)

Influent Grab (ug/L)

No Discharge Since 2018

No Discharge Since 2018

Page 11: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: City of Durham - South Durham Water Reclamation NPDES #:

CAS Number Analyte Name Acronym 7/8/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<1.23) ND U (<4.88) ND U (<4.87)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<1.23) ND U (<4.88) ND U (<4.87)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<1.23) ND U (<4.88) ND U (<4.87)

335-76-2 Perfluorodecanoic acid PFDA ND U (<1.23) 6.93 ND U (<0.422)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<1.23) ND U (<4.88) ND U (<4.87)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<1.23) ND U (<4.88) ND U (<4.87)

375-85-9 Perfluoroheptanoic acid PFHpA 5.45 7.01 ND <4.87

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<1.23) ND U (<4.88) ND U (<4.87)

307-24-4 Perfluorohexanoic acid PFHxA 15.8 B 26.7 ND U (<4.87)

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<1.23) ND U (<4.88) ND U (<4.87)

375-95-1 Perfluorononanoic acid PFNA 1.72 ND U (<4.88) ND U (<4.87)

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<1.25) ND U (<4.88) ND U (<4.87)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<1.23) ND U (<4.88) ND U (<4.87)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<1.23) ND U (<4.88) ND U (<4.87)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<1.23) ND U (<4.88) ND U (<4.87)

2706-90-3 Perfluoropentanoic acid PFPeA ND U (<1.23) 103 205

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<1.23) ND U (<4.88) ND U (<4.87)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<1.23) ND U (<4.88) ND U (<4.87)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<1.23) ND U (<4.88) ND U (<4.87)

62037-80-3 Gen-X HFPO-DA ND U (<43.07) NA NA

335-67-1 Perfluorooctanoic acid PFOA 10.7 22.1 5.86

1763-23-1 Perfluorooctanesulfonic acid PFOS 14.9 6.32 8.44

Sum of PFOA and PFOS 25.6 28.42 14.3

Total PFAS 48.57 172.06 219.3

7/8/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

1, 4 - Dioxane ND <1.00 1.74 2.76

Lab Qualifiers

NA - Not Applicable

ND - Analyte concentration is not detected above the detection limit.

U - The sample was not detected in the sample at the Reporting Limit.

B - Analyte found in the sample and associated method blank.

NC0047597

Influent Grab (ng/L)

Influent Grab (ug/L)

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POTW Name: Durham County Triangle Wastewater Treatment Plant NPDES #:

CAS Number Analyte Name Acronym 7/8/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<2.88) 50.2 44.8

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.88) ND U (<10.8) ND U (<1.89)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.88) 2.62 J ND U (<1.89)

335-76-2 Perfluorodecanoic acid PFDA 1.87 J ND U (<10.8) ND U (<1.89)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.88) ND U (<10.8) ND U (<1.89)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.88) ND U (<10.8) ND U (<1.89)

375-85-9 Perfluoroheptanoic acid PFHpA 3.4 1.34 J 1.99

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<2.88) ND U (<10.8) ND U (<1.89)

307-24-4 Perfluorohexanoic acid PFHxA 10.7 B 7.63 J 5.73

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.88) ND U (<10.8) ND U (<1.89)

375-95-1 Perfluorononanoic acid PFNA 1.42 J ND U (<10.8) 0.728 J

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.92) ND U (<10.8) ND U (<2.86)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.88) 0.964 J ND U (<1.89)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.88) ND U (<10.8) ND U (<1.89)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.88) ND U (<10.8) ND U (<1.89)

2706-90-3 Perfluoropentanoic acid PFPeA 36.4 ND U (<10.8) ND U (<1.89)

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.88) 1.45 J ND U (<1.89)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.88) 1.98 J ND U (<1.89)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.88) ND U (<10.8) ND U (<1.89)

335-67-1 Perfluorooctanoic acid PFOA 7.72 5.74 J 5.92

1763-23-1 Perfluorooctanesulfonic acid PFOS 11 7.19 J 6.89

Sum of PFOA and PFOS 18.72 12.93 12.81

Total PFAS 72.51 79.114 66.058

7/8/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/9/2019 Lab Qualifer(s)

1, 4 - Dioxane ND U (<2.00) 1.56 ND U (<1.00)

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

U - The analyte was not detected. The Estimated Detection Limit (EDL) may be reported for this analyte.

J - Indicates that an analyte has a concentration below the reporting limit (lowest point of the calibration curve).

B - The analyte was found in the method blank, at a concentration that was at least 10% of the concentration in the sample.

NC0026051

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 13: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Fayetteville - Cross Creek WWTP NPDES #:

CAS Number Analyte Name Acronym 7/16/2019 Lab Qualifer(s) 8/27/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA 21.3 1.58 12.5

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.75) 4.32 4.30

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.75) ND U (<11.3) ND U (<1.69)

335-76-2 Perfluorodecanoic acid PFDA 2.97 0.51 1.72 J

307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.75) ND U (<11.3) 0.05 J

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.75) 0.36 J 0.44 J

375-85-9 Perfluoroheptanoic acid PFHpA 11.9 8.13 J 14.65

355-46-4 Perfluorohexanesulfonic acid PFHxS 20.4 12.85 20.15

307-24-4 Perfluorohexanoic acid PFHxA 35.5 15.60 35.25

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.75) ND U (<11.3) ND U (<1.67)

375-95-1 Perfluorononanoic acid PFNA 1.77 J 0.65 1.67

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.75) ND U (<11.3) ND U (<1.62)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.75) ND U (<11.3) ND U (<3.48)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.75) ND U (<11.3) ND U (<3.48)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.75) 0.95 1.04

2706-90-3 Perfluoropentanoic acid PFPeA 30 20.65 26.55

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.75) ND U (<11.3) ND U (<17.4)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.75) ND U (<11.3) ND U (<17.4)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.75) ND U (<11.3) ND U (<1.74)

335-67-1 Perfluorooctanoic acid PFOA 18.2 9.21 J 17.1

1763-23-1 Perfluorooctanesulfonic acid PFOS 26.9 22.30 28.3

Sum of PFOA and PFOS 45.1 31.505 45.4

Total PFAS 168.94 97.09 163.71

7/16/2019 Lab Qualifer(s) 8/27/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

1, 4 - Dioxane 2.17 3.02 3.76

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

U - The analyte was not detected

J - Analyte has a concentration below the reporting limit (lowest point on the calibration curve)

NC0023957

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 14: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Fayetteville - Rockfish Creek WWTP NPDES #:

CAS Number Analyte Name Acronym 7/16/2019 Lab Qualifer(s) 8/27/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<2.95) 7.47 J 5.75

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.95) 3.93 3.79

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.95) ND U (<11.1) ND U (<1.76)

335-76-2 Perfluorodecanoic acid PFDA 1.23 J 0.51 1.15 J

307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.95) ND U (<11.1) ND U (<1.82)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.95) 0.31 ND U (<1.72)

375-85-9 Perfluoroheptanoic acid PFHpA 8.63 12.10 11.35

355-46-4 Perfluorohexanesulfonic acid PFHxS 12.1 9.89 J 6.33 J

307-24-4 Perfluorohexanoic acid PFHxA 20 B 23.90 20.20

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.95) ND U (<11.1) ND U (<1.74)

375-95-1 Perfluorononanoic acid PFNA 1.28 J 0.69 0.57 J

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.95) ND U (<11.1) ND U (<1.69)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.95) ND U (<11.1) ND U (<3.63)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.95) ND U (<11.1) ND U (<36.3)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.95) 0.61 0.76 J

2706-90-3 Perfluoropentanoic acid PFPeA 24.7 79.10 24.00

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.95) ND U (<11.1) ND U (<18.2)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.95) ND U (<11.1) ND U (<18.2)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.95) ND U (<11.1) ND U (<1.82)

335-67-1 Perfluorooctanoic acid PFOA 10.9 13.26 J 8.11

1763-23-1 Perfluorooctanesulfonic acid PFOS 19.6 14.25 7.70

Sum of PFOA and PFOS 30.5 27.505 15.805

Total PFAS 98.44 166.01 89.70

7/16/2019 Lab Qualifer(s) 8/27/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s)

1, 4 - Dioxane 2.44 3.02 3.76

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

U - The analyte was not detected

J - Analyte has a concentration below the reporting limit (lowest point on the calibration curve)

NC0050105

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 15: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: City of Graham NPDES #:

CAS Number Analyte Name Acronym 7/23/2019 Lab Qualifer(s) 8/22/2019 Lab Qualifer(s) 9/18/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<0.233) ND U (<1.25) ND U (<0.210)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<1.40) ND U (<1.25) ND U (<0.210)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<0.233) ND U (<1.25) ND U (<0.210)

335-76-2 Perfluorodecanoic acid PFDA 1.25 1.44 2.14

307-55-1 Perfluorododecanoic acid PFDoA ND U (<0.233) 0.726 J,B ND U (<0.210)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<0.233) ND U (<1.25) ND U (<0.210)

375-85-9 Perfluoroheptanoic acid PFHpA ND U (<0.233) 4.28 ND U (<0.210)

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<0.233) 0.144 J,B ND U (<0.210)

307-24-4 Perfluorohexanoic acid PFHxA ND U (<0.233) 11.8 0.822

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<0.233) ND U (<1.25) ND U (<0.210)

375-95-1 Perfluorononanoic acid PFNA 1.77 1.62 2.46

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<0.355) ND U (<1.25) ND U (<0.317)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<0.233) ND U (<1.25) ND U (<0.210)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<0.233) ND U (<1.25) ND U (<0.210)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<0.233) ND U (<1.25) ND U (<0.210)

2706-90-3 Perfluoropentanoic acid PFPeA 65.6 ND U (<1.25) ND U (<0.210)

376-06-7 Perfluorotetradecanoic acid PFTeA NA 2.82 B ND U (<0.210)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<0.233) 2.02 B 0.776

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<0.233) ND U (<1.25) ND U (<0.210)

62037-80-3 Gen-X HFPO-DA ND U (<8.16) ND U (<43.8) ND U (<7.33)

757124-72-4 4:2 Fluorotelomer sulfonate 4:2 FTS ND U (<0.233) ND U (<1.25) ND U (<0.210)

27619-97-2 6:2 Fluorotelomer sulfonate 6:2 FTS 3.19 1.33 B 1.48

39108-34-4 8:2 Fluorotelomer sulfonate 8:2 FTS 0.769 0.354 J,B ND U (<0.210)

335-67-1 Perfluorooctanoic acid PFOA 6.5 8.97 8.37

1763-23-1 Perfluorooctanesulfonic acid PFOS ND U (<0.233) 12.8 9.59

Sum of PFOA and PFOS 6.5 21.77 17.96

Total PFAS 79.08 48.30 25.64

7/15/2019 Lab Qualifer(s) 8/19/2019 Lab Qualifer(s) 9/16/2019 Lab Qualifer(s)

1, 4 - Dioxane 3.29 1.18 1.59

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0021211

Influent Grab (ng/L)

Influent Grab (ug/L)

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POTW Name: Greensboro - TZ Osborne WRF NPDES #: Date Sampled Effluent (ug/L)

CAS Number Analyte Name Acronym 7/8/2019 Lab Qualifer(s) 8/7/2019 Lab Qualifer(s) 9/17/2019 Lab Qualifer(s) 12/14/2017 26.3

375-22-4 Perfluorobutanoic acid PFBA 3.1 27.3 13.0 1/11/2018 18.2

375-73-5 Perfluorobutanesulfonic acid PFBS 2.5 39.3 25.0 2/15/2018 26.7

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.56) ND U (<10.2) ND U (<7.1) 3/8/2018 27

335-76-2 Perfluorodecanoic acid PFDA 2.9 ND U (<10.2) 0.8 4/12/2018 21

307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.56) ND U (<10.2) ND U (<7.4) 5/2/2018 229

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.56) ND U (<10.2) ND U (<1.70) 5/25/2018 41.5

375-85-9 Perfluoroheptanoic acid PFHpA 6.5 22.3 7.4 5/30/2018 665

355-46-4 Perfluorohexanesulfonic acid PFHxS 9.4 19.6 15.3 6/20/2018 16.7

307-24-4 Perfluorohexanoic acid PFHxA 24.7 54.6 18.0 7/25/2018 11.6

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.56) ND U (<10.2) ND U (<1.70) 8/16/2018 408

375-95-1 Perfluorononanoic acid PFNA ND U (<4.1) ND U (<10.2) ND U (<7.4) 9/26/2018 8.1

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.56) ND U (<10.2) ND U (<2.57) 10/25/2018 25

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<4.1) ND U (<18.0) ND U (<15.0) 11/16/2018 14.2

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<4.1) ND U (<18.0) ND U (<15.0) 12/19/2018 9.9

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.56) ND U (<10.2) ND U (<1.70) 1/10/2019 8.7

2706-90-3 Perfluoropentanoic acid PFPeA 22.0 66.9 20.0 2/13/2019 11.1

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.56) ND U (<10.2) ND U (<7.4) 3/14/2019 24.2

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.56) ND U (<10.2) ND U (<7.4) 4/24/2019 397.5

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.56) ND U (<10.2) ND U (<7.4) 5/22/2019 14.7

335-67-1 Perfluorooctanoic acid PFOA 11.2 24.7 14.9 6/12/2019 62.6

1763-23-1 Perfluorooctanesulfonic acid PFOS 25.6 36.2 47.1 7/8/2019 9.7

Sum of PFOA and PFOS 36.8 60.9 62.0 8/7/2019 957.5

Total PFAS 107.9 290.9 161.5 8/20/2019 429.7

8/26/2019 17.5

9/17/2019 6

July 2019 (Monthly Avg.) Lab Qualifer(s) August 2019 (Monthly Avg.)** Lab Qualifer(s) September 2019 (Monthly Avg.) Lab Qualifer(s)

1, 4 - Dioxane* 9.73 468.2 5.98

*An Enforcement Order is under consideration for the City of Greensboro in order to limit and enforce reductions of 1,4 Dioxane in their discharge.

**Monthly Average (3 samples), see 1,4-Dioxane eDMR data.

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0047384

Influent Grab (ng/L)

eDMR Effluent Grab (ug/L)

1, 4 - Dioxane eDMR data

Page 17: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: North Harnett Regional NPDES #:

CAS Number Analyte Name Acronym 7/8/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/4/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<1.25) 9.38 13.2

375-73-5 Perfluorobutanesulfonic acid PFBS 4.65 ND U (<4.91) ND U (<1.28)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<1.25) ND U (<4.91) ND U (<1.28)

335-76-2 Perfluorodecanoic acid PFDA 1.04 JB 0.297 JL 0.24 J

307-55-1 Perfluorododecanoic acid PFDoA 0.62 JB ND U (<4.91) ND U (<1.28)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<1.25) ND U (<4.91) ND U (<1.28)

375-85-9 Perfluoroheptanoic acid PFHpA 14.9 12.5 29.9

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<1.25) 5.31 ND U (<1.28)

307-24-4 Perfluorohexanoic acid PFHxA 38.7 22.9 36.2

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<1.25) ND U (<4.91) ND U (<1.28)

375-95-1 Perfluorononanoic acid PFNA 2.13 B 0.551 J 0.94 J

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<1.27) ND U (<4.91) ND U (<1.28)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA NA ND U (<4.91) ND U (<1.28)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<1.25) ND U (<4.91) ND U (<1.28)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<1.25) ND U (<4.91) ND U (<1.28)

2706-90-3 Perfluoropentanoic acid PFPeA ND U (<1.25) 55.7 139.0

376-06-7 Perfluorotetradecanoic acid PFTeA 0.964 J ND U (<4.91) ND U (<1.28)

72629-94-8 Perfluorotridecanoic acid PFTriA 0.656 JBQ ND U (<4.91) ND U (<1.28)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<1.25) ND U (<4.91) ND U (<1.28)

62037-80-3 Gen-X HFPO-DA ND U (<43.79) ND U (<172.0) ND U (<44.91)

757124-72-4 4:2 Fluorotelomer sulfonate 4:2 FTS NA ND U (<4.91) ND U (<1.28)

27619-97-2 6:2 Fluorotelomer sulfonate 6:2 FTS NA 1.08 J ND U (<1.28)

39108-34-4 8:2 Fluorotelomer sulfonate 8:2 FTS NA 0.53 J 0.157 J

335-67-1 Perfluorooctanoic acid PFOA 11.4 7.29 7.9

1763-23-1 Perfluorooctanesulfonic acid PFOS 29.4 18.5 12.6

Sum of PFOA and PFOS Sum of PFOA and PFOS 40.8 25.79 20.5

Total PFAS Total PFAS 104.46 134.038 240.1

7/8/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/4/2019 Lab Qualifer(s)

1, 4 - Dioxane 2.59 3.56 11.7

Lab Qualifiers

NA - Not Applicable

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

L - The analyte has a concentration below the Minimum Detection Limit (MDL).

Q - The labeled standard (ES) recovery is not within method control limits

NC0021636

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 18: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: City of High Point Eastside WWTP NPDES #: Date Sampled Effluent (ug/L)

CAS Number Analyte Name Acronym 7/8/2019 Lab Qualifer(s) 8/13/2019 Lab Qualifer(s) 9/16/2019 Lab Qualifer(s) 11/14/2018 1.15

375-22-4 Perfluorobutanoic acid PFBA ND U (<2.67) ND U (<10.8) ND U (<1.70) 12/19/2018 1.72

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.67) ND U (<10.8) ND U (<1.70) 1/30/2019 7.8

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.67) ND U (<10.8) ND U (<1.70) 2/13/2019 9.67

335-76-2 Perfluorodecanoic acid PFDA ND U (<2.67) ND U (<10.8) ND U (<1.70) 3/15/2019 73

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.67) ND U (<10.8) ND U (<1.70) 4/10/2019 8.15

375-85-9 Perfluoroheptanoic acid PFHpA 6.62 NA 3.7 5/15/2019 1.56

355-46-4 Perfluorohexanesulfonic acid PFHxS 11.3 ND U (<10.8) 9.16 6/19/2019 1.93

307-24-4 Perfluorohexanoic acid PFHxA 18.4 B 13.4 10.8 7/23/2019 1.55

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.672) ND U (<10.8) ND U (<1.70) 8/16/2019 1.51

375-95-1 Perfluorononanoic acid PFNA ND U (<2.67) ND U (<10.8) ND U (<1.70) 9/11/2019 2.16

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.67) ND U (<10.8) ND U (<2.57)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.67) ND U (<10.8) ND U (<1.70)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.67) ND U (<10.8) ND U (<1.70)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.67) ND U (<10.8) ND U (<1.70)

2706-90-3 Perfluoropentanoic acid PFPeA 27.1 60.8 55

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.67) ND U (<10.8) ND U (<1.70)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.67) ND U (<10.8) ND U (<1.70)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.67) ND U (<10.8) ND U (<1.70)

335-67-1 Perfluorooctanoic acid PFOA 14.2 ND U (<10.8) 6.8

1763-23-1 Perfluorooctanesulfonic acid PFOS 27.7 15.4 12.1

Sum of PFOA and PFOS 41.9 15.4 18.9

Total PFAS 105.32 89.6 97.56

7/23/2019 Lab Qualifer(s) 8/16/2019 Lab Qualifer(s) 9/11/2019 Lab Qualifer(s)

1, 4 - Dioxane 1.25 2.45 3.49

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

U - The sample was not detected in the sample at the Reporting Limit.

NC0024210

Influent Grab (ng/L)

Influent Grab (ug/L)

1,4 - Dioxane eDMR data

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POTW Name: Town Of Holly Springs NPDES #:

CAS Number Analyte Name Acronym 7/24/2019 Lab Qualifer(s) 8/13/2019 Lab Qualifer(s) 9/11/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<10) ND U (<8.2) 8

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<9.2) ND U (<7.2) 6

335-77-3 Perfluorodecanesulfonic acid PFDS ND D (<200) ND U (<7.9) 4.9

335-76-2 Perfluorodecanoic acid PFDA ND D (<210) ND U (<8.2) ND U (<5.1)

307-55-1 Perfluorododecanoic acid PFDoA ND D (<210) ND U (<8.2) ND U (<5.1)

375-85-9 Perfluoroheptanoic acid PFHpA 13 21 27

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<9.8) ND U (<7.7) ND U (<4.8)

307-24-4 Perfluorohexanoic acid PFHxA 19 27 37

375-95-1 Perfluorononanoic acid PFNA ND D (<210) ND U (<8.2) ND U (<5.1)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND D (<420) ND U (<16) ND U (<10)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND D (<420) ND U (<16) ND U (<10)

2706-90-3 Perfluoropentanoic acid PFPeA 19 21 31

376-06-7 Perfluorotetradecanoic acid PFTeA/PFTeDA ND D (<210) ND U (<8.2) ND U (<5.1)

72629-94-8 Perfluorotridecanoic acid PFTriA/PFTrDA ND D (<210) ND U (<8.2) ND U (<5.1)

2058-94-8 Perfluoroundecanoic acid PFUnA/PFUdA ND D (<210) ND U (<8.2) ND U (<5.1)

13252-13-6 Hexafluoropropylene Oxide dimer acid PFPrOPrA/HFPO-AA ND D (<21) ND U (<16) ND U (<10)

958445-44-8 Sodium dodecafluoro-3H-4, 8-dioxanonanoate NaDONA/GENx ND D (<21) ND U (<16) ND U (<10)

67905-19-5 Perfluoropalmitic acid PFHxDA ND D (<210) ND U (<8.2) ND U (<5.1)

16517-11-6 Perfluorooctadecanoic PFODA ND D (<210) ND U (<8.2) ND U (<5.1)

335-67-1 Perfluorooctanoic acid PFOA ND U (<10) 10 10

1763-23-1 Perfluorooctanesulfonic acid PFOS ND U (<10) 12 7.6

Sum of PFOA and PFOS 0 22 17.6

Total PFAS 51 69 113.9

7/10/2019 Lab Qualifer(s) 8/13/2019 Lab Qualifer(s) 9/11/2019 Lab Qualifer(s)

1, 4 - Dioxane ND U (<2.0) 4.3 10.2

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

D - Result obtained from analysis of diluted sample

U - The sample was not detected in the sample at the Reporting Limit.

NC0063096

Influent Grab (ng/L)

Influent Grab (ug/L)

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POTW Name: City of Mebane WWTP NPDES #:

CAS Number Analyte Name Acronym 7/9/2019 Lab Qualifer(s) 8/13/2019 Lab Qualifer(s) 9/10/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<2.70) ND U (<5.38) ND U (<5.31)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.70) ND U (<5.38) ND U (<5.31)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.70) ND U (<5.38) ND U (<5.31)

335-76-2 Perfluorodecanoic acid PFDA 5.16 7.64 ND U (<5.31)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.70) ND U (<5.38) ND U (<5.31)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.70) ND U (<5.38) ND U (<5.31)

375-85-9 Perfluoroheptanoic acid PFHpA 5.84 7.73 6.86

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<2.70) ND U (<5.38) ND U (<5.31)

307-24-4 Perfluorohexanoic acid PFHxA 28 B 29.4 28

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.70) ND U (<5.38) ND U (<5.31)

375-95-1 Perfluorononanoic acid PFNA ND U (<2.70) ND U (<5.38) ND U (<5.31)

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.74) ND U (<5.38) ND U (<5.31)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.70) ND U (<5.38) ND U (<5.31)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.70) ND U (<5.38) ND U (<5.31)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.70) ND U (<5.38) ND U (<5.31)

2706-90-3 Perfluoropentanoic acid PFPeA ND U (<2.70) ND U (<5.38) 284

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.70) ND U (<5.38) ND U (<5.31)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.70) ND U (<5.38) ND U (<5.31)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.70) ND U (<5.38) ND U (<5.31)

335-67-1 Perfluorooctanoic acid PFOA 17.4 24.3 17.1

1763-23-1 Perfluorooctanesulfonic acid PFOS 11.4 6.97 14.6

Sum of PFOA and PFOS 28.8 31.27 31.7

Total PFAS 67.8 76.04 350.56

7/9/2019 Lab Qualifer(s) 8/13/2019 Lab Qualifer(s) 9/10/2019 Lab Qualifer(s)

1, 4 - Dioxane 1.48 1.51 1.38

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

U - The sample was not detected in the sample at the Reporting Limit.

NC0021474

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 21: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: City of Raeford NPDES #:

CAS Number Analyte Name Acronym 7/15/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/16/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<240.0) ND U (<150.0) ND U (<17.0)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<120.0) 119 80.4

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<120.0) ND U (<77.0) ND U (<170)

335-76-2 Perfluorodecanoic acid PFDA ND U (<120.0) ND U (<380.0)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<120.0) ND U (<380.0) ND U (<420.0)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<120.0) ND U (<77.0) ND U (<170)

375-85-9 Perfluoroheptanoic acid PFHpA ND U (<120.0) ND U (<77.0) 4.44 J

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<120.0) 65.8 61.8 J

307-24-4 Perfluorohexanoic acid PFHxA ND U (<120.0) ND U (<77.0) 13.2

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<120.0) ND U (<77.0) ND U (<170)

375-95-1 Perfluorononanoic acid PFNA ND U (<120.0) ND U (<77.0) ND U (<170)

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<120.0) ND U (<77.0) ND U (<170)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<590.0) ND U (<1900.0) ND U (<830)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<590.0) ND U (<1900.0) ND U (<830)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<120.0) ND U (<77.0) 4.67 J

2706-90-3 Perfluoropentanoic acid PFPeA ND U (<120.0) ND U (<77.0) 10.3

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<120.0) ND U (<380.0) ND U (<170)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<120.0) ND U (<380.0) ND U (<170)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<240.0) ND U (<380.0) ND U (<170)

757124-72-4 4:2 Fluorotelomer sulfonate 4:2 FTS ND U (<240.0) NA NA

335-67-1 Perfluorooctanoic acid PFOA ND U (<120.0) ND U (<77.0) ND U (<170)

1763-23-1 Perfluorooctanesulfonic acid PFOS ND U (<120.0) 73.6 124 J

Sum of PFOA and PFOS 0 73.6* 124*

Total PFAS 0 258.4 298.81

7/15/2019 Lab Qualifer(s) 8/5/2019 Lab Qualifer(s) 9/16/2019 Lab Qualifer(s)

1, 4 - Dioxane 11.6 ND U (<1.0) 2.9

Lab Qualifiers

NA - Not Applicable

ND - Analyte concentration is not detected above the detection limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0026514

Influent Grab (ng/L)

Influent Grab (ug/L)

*Due to considerable dilution in the receiving stream, the PFOS and PFOA concentrations listed in the table above are not expected to cause an instream concentration greater than the EPA drinking water health advisory

concentration of 70 ng/L at downstream water supply intakes.

Page 22: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Town of Ramseur WWTP NPDES #:

CAS Number Analyte Name Acronym 7/8/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/4/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<0.311) ND U (<1.25) ND U (<1.24)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<0.311) 344 ND U (<1.24)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<0.311) ND U (<1.25) ND U (<1.24)

335-76-2 Perfluorodecanoic acid PFDA 0.586 ND U (<1.25) ND U (<1.24)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<0.311) ND U (<1.25) ND U (<1.24)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<0.311) ND U (<1.25) ND U (<1.24)

375-85-9 Perfluoroheptanoic acid PFHpA 1.24 ND U (<1.25) ND U (<1.24)

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<0.311) ND U (<1.25) ND U (<1.24)

307-24-4 Perfluorohexanoic acid PFHxA 6.97 4.77 4.64

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<0.31) ND U (<1.25) ND U (<1.24)

375-95-1 Perfluorononanoic acid PFNA 0.782 ND U (<1.25) ND U (<1.24)

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<0.316) ND U (<1.25) ND U (<1.24)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<0.311) ND U (<1.25) ND U (<1.24)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<0.311) ND U (<1.25) ND U (<1.24)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<0.311) ND U (<1.25) ND U (<1.24)

2706-90-3 Perfluoropentanoic acid PFPeA 41.8 103 313

376-06-7 Perfluorotetradecanoic acid PFTeA (PFTA) 0.761 ND U (<1.25) ND U (<1.24)

72629-94-8 Perfluorotridecanoic acid PFTriA (PFTrA) ND U (<0.311) ND U (<1.25) ND U (<1.24)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<0.311) ND U (<1.25) ND U (<1.24)

62037-80-3 Gen-X HFPO-DA ND U (<10.90) ND U (<43.9) ND U (<43.3)

757124-72-4 4:2 Fluorotelomer sulfonate 4:2 FTS ND U (<0.311) ND U (<1.25) ND U (<1.24)

27619-97-2 6:2 Fluorotelomer sulfonate 6:2 FTS ND U (<0.311) ND U (<1.25) ND U (<1.24)

39108-34-4 8:2 Fluorotelomer sulfonate 8:2 FTS ND U (<0.311) ND U (<1.25) ND U (<1.24)

335-67-1 Perfluorooctanoic acid PFOA 2.93 2 1.96

1763-23-1 Perfluorooctanesulfonic acid PFOS 6.52 45.7 8.06

Sum of PFOA and PFOS 9.45 47.7 10.02

Total PFAS 61.589 499.47 327.66

7/8/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/4/2019 Lab Qualifer(s)

1, 4 - Dioxane ND U (<1.0) 2 2.08

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0026565

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 23: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: City of Randleman NPDES #:

CAS Number Analyte Name Acronym 7/24/2019 Lab Qualifer(s) 8/14/2019 Lab Qualifer(s) 9/18/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<0.222) ND U (<1.38) ND U (<0.212)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<0.222) ND U (<1.38) ND U (<0.212)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<0.222) ND U (<1.38) ND U (<0.212)

335-76-2 Perfluorodecanoic acid PFDA 0.661 ND U (<1.38) 0.375

307-55-1 Perfluorododecanoic acid PFDoA ND U (<0.222) ND U (<1.38) ND U (<0.212)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<0.222) ND U (<1.38) ND U (<0.212)

375-85-9 Perfluoroheptanoic acid PFHpA 3.12 2.94 3.79

355-46-4 Perfluorohexanesulfonic acid PFHxS 6.07 ND U (<1.38) ND U (<0.212)

307-24-4 Perfluorohexanoic acid PFHxA 8.36 8.56 9.82

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<0.222) ND U (<1.38) ND U (<0.212)

375-95-1 Perfluorononanoic acid PFNA 1.04 0.846 J 1.5

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<0.337) ND U (<1.38) ND U (<0.320)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<0.222) ND U (<1.38) ND U (<0.212)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<0.222) ND U (<1.38) ND U (<0.212)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<0.222) ND U (<1.38) ND U (<0.212)

2706-90-3 Perfluoropentanoic acid PFPeA ND U (<0.222) ND U (<1.38) 96 *376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<0.222) 0.255 J ND U (<0.212)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<0.222) ND U (<1.38) ND U (<0.212)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<0.222) ND U (<1.38) ND U (<0.212)

62037-80-3 Gen-X HFPO-DA NA ND U (<48.22) ND U (<7.42)

757124-72-4 4:2 Fluorotelomer sulfonate 4:2 FTS NA ND U (<1.38) ND U (<1.38)

27619-97-2 6:2 Fluorotelomer sulfonate 6:2 FTS NA ND U (<1.38) ND U (<1.38)

39108-34-4 8:2 Fluorotelomer sulfonate 8:2 FTS NA ND U (<1.38) ND U (<1.38)

335-67-1 Perfluorooctanoic acid PFOA 5.7 5.52 7.05

1763-23-1 Perfluorooctanesulfonic acid PFOS 7.54 ND U (<1.38) 14.7

Sum of PFOA and PFOS 13.24 5.52 21.75

Total PFAS 32.491 18.121 133.235

7/24/2019 Lab Qualifer(s) 8/26/2019 Lab Qualifer(s) 9/18/2019 Lab Qualifer(s)

1, 4 - Dioxane 18.1 4.94 ND U (<4.0)

Lab Qualifiers

*Narrative in Enthalpy lab report states result could be a false positive.

NA - Not Applicable

ND - Analyte concentration is not detected above the detection limit.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0025445

Influent Grab (ng/L)

Influent Grab (ug/L)

Page 24: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: City of Reidsville NPDES #: Date Sampled Effluent (ug/L)

CAS Number Analyte Name Acronym 7/9/2019 Lab Qualifer(s) 8/7/2019 Lab Qualifer(s) 9/11/2019 Lab Qualifer(s) 12/11/2017 13.8

375-22-4 Perfluorobutanoic acid PFBA ND U (<2.54) ND U (<11.1) ND U (<1.69) 1/10/2018 99.8

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.54) ND U (<11.1) ND U (<1.69) 1/29/2018 701

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.54) ND U (<11.1) ND U (<1.69) 2/5/2018 217

335-76-2 Perfluorodecanoic acid PFDA 3.47 ND U (<11.1) 5.16 3/5/2018 38.9

307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.54) ND U (<11.1) ND U (<1.69) 4/3/2018 54.1

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.54) ND U (<11.1) ND U (<1.69) 5/7/2018 368

375-85-9 Perfluoroheptanoic acid PFHpA 7.34 ND U (<11.1) 10.6 6/19/2018 40.1

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<2.54) ND U (<11.1) ND U (<1.69) 7/18/2018 191.5

307-24-4 Perfluorohexanoic acid PFHxA 68.3 29.5 41.1 8/13/2018 17.2

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.54) ND U (<11.1) ND U (<1.69) 9/12/2018 50.7

375-95-1 Perfluorononanoic acid PFNA 2.68 ND U (<11.1) 2.27 10/5/2018 372

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.57) ND U (<11.1) ND U (<2.56) 10/15/2018 4.54

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.54) ND U (<11.1) ND U (<1.69) 11/7/2018 61.3

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.54) ND U (<11.1) ND U (<1.69) 11/23/2018 78.2

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.54) ND U (<11.1) ND U (<1.69) 12/5/2018 55.3

2706-90-3 Perfluoropentanoic acid PFPeA ND U (<2.54) 58.7 ND U (<1.69) 12/26/2018 10

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.54) ND U (<11.1) ND U (<1.69) 12/28/2018 13.1

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.54) ND U (<11.1) ND U (<1.69) 1/9/2019 273

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.54) ND U (<11.1) ND U (<1.69) 2/6/2019 280

335-67-1 Perfluorooctanoic acid PFOA 19.9 16.4 16.7 3/6/2019 98.3

1763-23-1 Perfluorooctanesulfonic acid PFOS 17.3 12.2 11.3 4/2/2019 40.4

Sum of PFOA and PFOS 37.2 28.6 28 5/2/2019 125

Total PFAS 118.99 116.8 87.13 6/12/2019 367

7/9/2019 17.3

8/7/2019 46.1

7/9/2019 Lab Qualifer(s) 8/7/2019 Lab Qualifer(s) 9/11/2019 Lab Qualifer(s) 9/11/2019 23.1

1, 4 - Dioxane* 17.3 46.1 23.1 10/4/2019 24.9

10/9/2019 24.9

*An Enforcement Order is under consideration for the City of Reidsville in order to limit and enforce reductions of 1,4 Dioxane in their discharge.

Lab Qualifiers 10/11/2019 1145

ND - Analyte concentration is not detected above the detection limit. 10/18/2019 398.5

U - The sample was not detected in the sample at the Reporting Limit. 10/25/2019 246

10/29/2019 23.6

10/30/2019 25.6

10/31/2019 68.2

NC0024881

Influent Grab (ng/L)

eDMR Effluent Grab (ug/L)

1, 4 - Dioxane eDMR data

Page 25: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Town of Rose Hill WWTP NPDES #:

CAS Number Analyte Name Acronym 7/22/2019 Lab Qualifer(s) 8/14/2019 Lab Qualifer(s) 9/18/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<8.49) 8.37 ND U (<0.242)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<7.56) 2.6 ND U (<0.242)

335-77-3 Perfluorodecanesulfonic acid PFDS NA ND U (<2.58) ND U (<0.242)

335-76-2 Perfluorodecanoic acid PFDA ND U (<1.70) ND U (<2.66) 0.3

307-55-1 Perfluorododecanoic acid PFDoA NA ND U (<2.66) 0.252

375-92-8 Perfluoroheptanesulfonic acid PFHpS NA ND U (<2.53) ND U (<0.242)

375-85-9 Perfluoroheptanoic acid PFHpA 2.24 40.7 1.56

355-46-4 Perfluorohexanesulfonic acid PFHxS ND U (<1.55) 2 J ND U (<0.242)

307-24-4 Perfluorohexanoic acid PFHxA 8.01 10.4 ND U (<0.242)

68259-12-1 Perfluorononanesulfonic acid PFNS NA ND U (<2.55) ND U (<0.24)

375-95-1 Perfluorononanoic acid PFNA 0.91 J 2.08 0.351

754-91-6 Perfluorooctanesulfonamide PFOSA NA ND U (<2.47) ND U (<0.365)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA NA ND U (<5.32) ND U (<0.242)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA NA ND U (<5.32) 0.274

2706-91-4 Perfluoropentanesulfonic acid PFPeS NA ND U (<2.50) ND U (<0.242)

2706-90-3 Perfluoropentanoic acid PFPeA 7.86 6.1 ND U (<0.242)

376-06-7 Perfluorotetradecanoic acid PFTeA NA ND U (<13.3) 0.408

72629-94-8 Perfluorotridecanoic acid PFTriA NA ND U (<13.3) 0.218 J

2058-94-8 Perfluoroundecanoic acid PFUnA NA ND U (<2.66) ND U (<0.242)

13252-13-62,3,3,3-Tetrafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy)-

propanoic acidPFPrOPrA ND U (<1.70) NA NA

749836-20-2 Nafion Byproduct 2 ND UX (<3.40) NA NA

39492-90-5 Perfluoro(3,5,7,9-tetraoxadecanoic) acid PFO4DA ND UX (<3.40) NA NA

39492-89-2 Perfluoro(3,5,7-trioxaoctanoic) acid PFO3OA ND UX (<3.40) NA NA

39492-88-1 Perfluoro(3,5-dioxahexanoic) acid PFO2HxA ND UX (<3.40) NA NA

674-13-5 Perfluoro-2-methoxyacetic acid PFMOAA ND UX (<3.40) NA NA

377-73-1 Perfluoro-3-methoxypropanoic acid PFMOPrA ND UX (<3.40) NA NA

863090-89-5 Perfluoro-4-methoxybutanic acid PFMOBA ND UX (<3.40) NA NA

335-67-1 Perfluorooctanoic acid PFOA 2.82 6.0 4.36

1763-23-1 Perfluorooctanesulfonic acid PFOS 6.06 11 8.74

Sum of PFOA and PFOS 8.88 17 13.1

Total 19.02 72.25 3.36

7/22/2019 Lab Qualifer(s) 8/14/2019 Lab Qualifer(s) 9/18/2019 Lab Qualifer(s)

1, 4 - Dioxane ND U (<400) ND U (<400) ND U (<1000)

Lab Qualifiers

NA - Not Applicable

ND - Analyte concentration is not detected above the detection limit.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0056863

Influent Grab (ng/L)

Influent Grab (ug/L)

X - The standards used to make the initial calibration curve did not meet the ISO 17025 criterion.

Page 26: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Sanford - Big Buffalo Creek WWTP NPDES #:

CAS Number Analyte Name Acronym 7/8/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/4/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA 12.1 15.4 ND U (<1.30)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<0.316) ND U (<1.27) ND U (<1.30)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<0.316) ND U (<1.27) ND U (<1.30)

335-76-2 Perfluorodecanoic acid PFDA 1.86 1.85 ND U (<1.30)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<0.316) ND U (<1.27) ND U (<1.30)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<0.316) ND U (<1.27) 16.6

375-85-9 Perfluoroheptanoic acid PFHpA 18.8 77.5 122

355-46-4 Perfluorohexanesulfonic acid PFHxS 31.9 6.38 21.3

307-24-4 Perfluorohexanoic acid PFHxA ND U (<0.316) 44.2 61.8

68259-12-1 Perfluorononanesulfonic acid PFNS 2.51 ND U (<1.27) ND U (<1.30)

375-95-1 Perfluorononanoic acid PFNA ND U (<0.316) 2.25 2.07

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<0.320) ND U (<0.322) ND U (<1.30)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<0.316) 0.134 J ND U (<1.30)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<0.316) ND U (<1.27) ND U (<1.30)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<0.316) ND U (<1.27) ND U (<1.30)

2706-90-3 Perfluoropentanoic acid PFPeA 50.8 75.7 130

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<0.316) 0.239 J ND U (<1.30)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<0.316) ND U (<1.27) ND U (<1.30)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<0.316) ND U (<1.27) ND U (<1.30)

62037-80-3 Gen-X HFPO-DA ND U (<11.06) ND U (<44.52) ND U (<45.6)

757124-72-4 4:2 Fluorotelomer sulfonate 4:2 FTS ND U (<0.316) 1.25 J 6.86

27619-97-2 6:2 Fluorotelomer sulfonate 6:2 FTS 80 ND U (<1.27) 2650

39108-34-4 8:2 Fluorotelomer sulfonate 8:2 FTS 1.78 6.09 4.68

335-67-1 Perfluorooctanoic acid PFOA 11.6 11.5 11

1763-23-1 Perfluorooctanesulfonic acid PFOS 46.3 40.8 1000

Sum of PFOA and PFOS 57.9 52.3 1011*

Total PFAS 257.65 283.29 4026.3

7/8/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/4/2019 Lab Qualifer(s)

1, 4 - Dioxane 2.91 4.67 13.2

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0024147

Influent Grab (ng/L)

Influent Grab (ug/L)

*PFOS and PFOA levels show potential to cause the downstream water supply intake to exceed the EPA drinking water health advisory concentration of 70 ng/L. Sanford’s Water Treatment Plant intake is the water supply intake that

could be affected by the wastewater treatment plant's discharge. DEQ will discuss additional sampling and source identification measures with the City of Sanford.

Page 27: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Siler City Waste Water Treatment Plant NPDES #:

CAS Number Analyte Name Acronym 7/8/2019 Lab Qualifer(s) 8/6/2019 Lab Qualifer(s) 9/8/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA ND U (<2.52) ND U (<10.1) ND U (<1.68)

375-73-5 Perfluorobutanesulfonic acid PFBS ND U (<2.52) ND U (<10.1) ND U (<1.68)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<2.52) ND U (<10.1) ND U (<1.68)

335-76-2 Perfluorodecanoic acid PFDA ND U (<2.52) ND U (<10.1) ND U (<1.68)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<2.52) ND U (<10.1) ND U (<1.68)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<2.52) ND U (<10.1) ND U (<1.68)

375-85-9 Perfluoroheptanoic acid PFHpA 2.1 J 0.717 J 2.05

355-46-4 Perfluorohexanesulfonic acid PFHxS 2 J ND U (<10.1) 1.46 J

307-24-4 Perfluorohexanoic acid PFHxA 9.94 B 5.89 J 6.15

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<2.52) ND U (<10.1) ND U (<1.68)

375-95-1 Perfluorononanoic acid PFNA ND U (<2.52) ND U (<10.1) ND U (<1.68)

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<2.56) ND U (<10.1) ND U (<2.53)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<2.52) ND U (<10.1) ND U (<1.68)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA ND U (<2.52) ND U (<10.1) ND U (<1.68)

2706-91-4 Perfluoropentanesulfonic acid PFPeS ND U (<2.52) ND U (<10.1) ND U (<1.68)

2706-90-3 Perfluoropentanoic acid PFPeA 14.5 B 13 ND U (<1.68)

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<2.52) ND U (<10.1) ND U (<1.68)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<2.52) ND U (<10.1) ND U (<1.68)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<2.52) ND U (<10.1) ND U (<1.68)

335-67-1 Perfluorooctanoic acid PFOA 5.49 4.02 J 3.71

1763-23-1 Perfluorooctanesulfonic acid PFOS 5.66 3.84 J 3.89

Sum of PFOA and PFOS 11.15 7.86 7.6

Total PFAS 39.69 27.467 17.26

7/9/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/10/2019 Lab Qualifer(s)

1, 4 - Dioxane 1.3 1.58 ND U (<1.0)

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

B - Analyte found in the sample and associated method blank.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0026441

Effluent Grab (ng/L)

Influent Grab (ug/L)

Page 28: POTW Name: NPDES Resources/GIS/Data...POTW Name: Town of Burgaw Collection System NPDES #: CAS Number Analyte Name Acronym 7/26/2019 Lab Qualifer(s) 8/8/2019 Lab Qualifer(s) 9/17/2019

POTW Name: Wallace Regional WWTP NPDES #:

CAS Number Analyte Name Acronym 7/11/2019 Lab Qualifer(s) 8/12/2019 Lab Qualifer(s) 9/18/2019 Lab Qualifer(s)

375-22-4 Perfluorobutanoic acid PFBA 3.41 ND U (<2.53) ND U (<0.239)

375-73-5 Perfluorobutanesulfonic acid PFBS 3.22 2.15 J ND U (<0.239)

335-77-3 Perfluorodecanesulfonic acid PFDS ND U (<1.71) ND U (<2.45) ND U (<0.239)

335-76-2 Perfluorodecanoic acid PFDA 0.789 J ND U (<2.53) ND U (<0.239)

307-55-1 Perfluorododecanoic acid PFDoA ND U (<1.77) ND U (<2.53) ND U (<0.239)

375-92-8 Perfluoroheptanesulfonic acid PFHpS ND U (<1.68) ND U (<2.40) ND U (<0.239)

375-85-9 Perfluoroheptanoic acid PFHpA 1.03 J 0.883 J 2.48

355-46-4 Perfluorohexanesulfonic acid PFHxS 0.808 J ND U (<2.30) ND U (<0.239)

307-24-4 Perfluorohexanoic acid PFHxA 6.9 20.7 6.77

68259-12-1 Perfluorononanesulfonic acid PFNS ND U (<1.70) ND U (<2.42) ND U (<0.24)

375-95-1 Perfluorononanoic acid PFNA ND U (<1.77) 1.04 J 0.506

754-91-6 Perfluorooctanesulfonamide PFOSA ND U (<1.64) ND U (<11.7) ND U (<0.362)

2991-50-6 2-(N-Ethylperfluorooctanesulfonamido) acetic acid N-EtFOSAA ND U (<1.17) ND U (<25.3) ND U (<0.239)

2355-31-9 2-(N-Methylperfluorooctanesulfonamido) acetic acid N-MeFOSAA 1.18 J ND U (<5.05) ND U (<0.239)

2706-91-4 Perfluoropentanesulfonic acid PFPeS 1.05 J ND U (<2.37) ND U (<0.239)

2706-90-3 Perfluoropentanoic acid PFPeA 6.26 ND U (<2.53) 299

376-06-7 Perfluorotetradecanoic acid PFTeA ND U (<8.83) ND U (<12.6) ND U (<0.239)

72629-94-8 Perfluorotridecanoic acid PFTriA ND U (<8.83) ND U (<12.6) ND U (<0.239)

2058-94-8 Perfluoroundecanoic acid PFUnA ND U (<1.77) ND U (<2.53) ND U (<0.239)

335-67-1 Perfluorooctanoic acid PFOA 2.96 2.96 4.9

1763-23-1 Perfluorooctanesulfonic acid PFOS 4.78 9.61 11.6

Sum of PFOA and PFOS 7.74 12.57 16.5

Total PFAS 32.39 37.34 325.26

7/11/2019 Lab Qualifer(s) 8/12/2019 Lab Qualifer(s) 9/18/2019 Lab Qualifer(s)

1, 4 - Dioxane ND U (<400) ND U (<1000) ND U (<1000)

Lab Qualifiers

ND - Analyte concentration is not detected above the detection limit.

J - The reported value is an estimate. The value is less than the Reporting Limit.

U - The sample was not detected in the sample at the Reporting Limit.

NC0003450

Influent Grab (ng/L)

Influent Grab (ug/L)