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Phase II Environmental Site
Assessment
21st Street Community Center and Band Shell Building and Parking Area West of Convention Center
Miami Beach, Miami-Dade County, Florida
February, 2015 E Sciences Project Number 7-0002-023
Prepared for: City of Miami Beach Office of the City Manager City of Miami Beach 1700 Convention Center Drive, Fourth Floor Miami Beach, FL 33139
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February 3, 2015 Ms. Thais Vieira, RA, LEED AP Senior Project Manager Office of the City Manager City of Miami Beach 1700 Convention Center Drive, Fourth Floor Miami Beach, FL 33139 Subject: Report of Phase II Environmental Site Assessment
21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Miami Beach, Miami-Dade County, Florida E Sciences Project Number 7-0002-023
Dear Ms. Vieira:
We are pleased to submit the enclosed Phase II Environmental Site Assessment (ESA) report for
the above referenced property. A summary of findings is provided in the Executive Summary.
Please read the report in its entirety for a comprehensive understanding of the items contained in
the Executive Summary.
This report is intended for the use of the City of Miami Beach only. E Sciences’ services have
been performed under mutually agreed-upon terms and conditions. If other parties wish to rely
on this report, please have them contact E Sciences so that a mutual understanding and agreement
of the terms and conditions for E Sciences’ services can be established via a Secondary Client
Agreement prior to their use of this information.
We appreciate the opportunity to perform these services for you. Please contact us at (954) 484-
8500 if you have questions regarding this information or if we can provide any other services.
Sincerely, E SCIENCES, INCORPORATED
Maria Paituvi, P.E. Nadia G. Locke, P.E., LEED AP Senior Engineer Senior Engineer Distribution: Addressee (1ec)
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TABLE OF CONTENTS
EXECUTIVE SUMMARY ........................................................................................................... ii
1.0 INTRODUCTION ............................................................................................................ 1
2.0 BACKGROUND INFORMATION ................................................................................ 2
3.0 STATEMENT OF OBJECTIVES .................................................................................. 3
4.0 SITE ASSESSMENT ACTIVITIES ............................................................................... 4
4.1 Incremental Soil Sampling ............................................................................................ 4 4.2 Soil Sampling Analytical Results .................................................................................. 5 4.3 Groundwater Sampling Activities ................................................................................. 7 4.3.1 Initial Groundwater Sampling Activities ....................................................................... 7 4.3.2 Additional Groundwater Sampling Activities ................................................................ 7 4.4 Groundwater Sampling Analytical Results ................................................................... 9
5.0 PHASE II ESA LIMITATIONS ................................................................................... 10
6.0 FINDINGS AND CONCLUSIONS .............................................................................. 11
7.0 REGULATORY INVOLVEMENT .............................................................................. 12
8.0 RECOMMENDATIONS ............................................................................................... 14
TABLES
1.1 Miami-Dade County Property Appraiser Information 1 4.1 Soil Analytical Scope 5 4.2 Summary of Soil Contaminant Detections 6 4.3 Initial Groundwater Analytical Scope 7 4.4 Additional Groundwater Analytical Scope 8 4.5 Monitoring Well Construction Detail 8 4.6 Summary of Groundwater Contaminant Detections 9
FIGURES 1 Location Map 2 USGS Topographic Map 3 Aerial Photograph 4A Soil Sampling Locations at Site A 4B Soil Sampling Locations at Site B 5 Groundwater Sampling Locations
APPENDICES
A Laboratory Analytical Reports and Chain of Custody Documentation B FDEP Groundwater Sampling Logs and Equipment Calibration Logs C Monitoring Well Construction and Development Logs
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EXECUTIVE SUMMARY
Report of Phase II Environmental Site Assessment (ESA) 21st Street Community Center and Band Shell Building and
Parking Area West of Convention Center Miami Beach, Miami-Dade County, Florida
E Sciences Project Number 7-0002-023
E Sciences conducted a Phase II Environmental Site Assessment (ESA) to evaluate the potential
presence of impacts associated with recognized environmental conditions (REC) identified during
the Phase I ESA performed by E Sciences and documented in a report provided under separate
cover dated November 4, 2014.
The Site is comprised of two separate areas: Site A and Site B. Site A is a paved parking lot
located west of the Miami Beach Convention Center adjacent to Convention Center Drive. Site B
is located south of Dade Boulevard and north of the Convention Center. Site A includes the 21st
Street Community Center and Band Shell Building, which are used by the Miami Beach Parks
and Recreation Division as part of their Teen Club center. The remaining portions of Site B
include a paved parking lot and the SoBe Institute of the Arts. These properties provide
recreational, cultural and parking services to residents and the public. The area surrounding Site
A and Site B consists of both residential and commercial properties. Both Site A and Site B are
owned by the City of Miami Beach (the City).
Based on a review of historical documentation, Site B and the eastern portion of Site A were part
of the Miami Beach Municipal Golf Course in the 1950s. Typical chemicals applied to golf
courses during this time included arsenates, organochlorine pesticides, and Ethylene Dibromide
(EDB). Arsenate pesticides were banned by the US Environmental Protection Agency (EPA) in
the 1980s. Oganochlorine pesticides include dieldrin, dichlorodiphenyltrichloroethane (DDT),
chlordane and toxaphene. Most organochlorine pesticides were banned in the 1970s and 1980s. Many pesticides constituents accumulate and persist over time. The historic operation of a golf
course is considered to be a REC due to the likelihood of the repeated historical application of
pesticides.
Groundwater and soil sampling and analysis were conducted as part of this Phase II ESA. The
sampling activities and laboratory analysis conducted were based on the nature of the REC and
the typically associated contaminants of concern (COCs).
Soil sampling was conducted using Incremental Sampling Methodology in order to collect soil
samples representative of site conditions. Site B and the eastern portion of Site A formerly
occupied by the historic golf course were defined as separate Decision Units (DU) as part of this
Phase II ESA. Groundwater samples were collected from each site using direct push technology
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and groundwater monitoring wells. The analytical scope for soil and groundwater samples
included organochlorine pesticides, organophosphate pesticides, metals, ammonia, nitrite and
nitrate.
Soil analytical results revealed the presence of arsenic concentrations above Miami-Dade
County’s Direct Exposure Residential Soil Cleanup Target Levels (SCTL) for the incremental
soil samples collected from Site A and Site B. The detected arsenic concentrations were above
the documented Barrier Islands Naturally Occurring Background Concentration published by
Miami-Dade County. Other compounds detected below regulatory standards include lead and
pesticides (4,4-DDE, Total Chlordane, and Dieldrin).
Laboratory analytical results for the groundwater samples did not reveal the presence of
groundwater contamination at Site A. Arsenic concentrations were detected above regulatory
criteria at one of the three groundwater sampling locations conducted within Site B. The arsenic
concentrations were confirmed during a confirmation sampling event. Further laboratory analysis
indicated that the presence of arsenic may be associated with dissolved metals in the
groundwater.
The City submitted a draft Phase II ESA report dated December 17, 2014 to Miami-Dade County
Regulatory and Economic Resources (RER) for review and comment. That report contained a
portion of the data contained herein.
On December 23, 2014, The city head a meeting with RER to discuss select contaminated sites
owned by the City including the subject sites. RER had conducted only a preliminary review of
the draft Phase II ESA at that time. RER requested that additional soil and groundwater testing be
conducted for both Site A and Site B and include offsite delineation of the potential impacts.
Further investigation regarding the past uses of the properties was also requested. RER noted that
additional comments and guidance would be provided upon review of the conceptual site
development plans.
The City responded to RER’s initial comments in email correspondence dated January 8, 2015.
The City indicated that offsite assessment would be conducted separately from the assessment of
the subject properties. Based on the results of additional aerial photographreview and interview
with key personnel, the City determined that the property's past uses do not suggest the need to
test additional parameters requested by RER. At this time RER has not responded to the City’s
email.
Based on the assessment information contained herein, the proposed development of the sites and
general regulatory guidance provided, we offer the following recommendations:
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• Installation of an engineering control across the sites as part of the site development. At
this time we understand that the engineering control will consist of a synthetic
impermeable and colored liner followed by 12 inches of clean fill and impermeable
pavement. The proposed engineering control shall be approved by RER prior to
installation.
• Development of a Soil Management Plan and implementation during site development
after regulatory approval by RER.
• Secure a dewatering permit that includes evaluation and management of impacted
groundwater within Site B. Based on the results of the filtered samples, we anticipate
that the application of a filter process will be sufficient to treat the water to regulatory
standards for disposal purposes if treatment is necessary.
• It is anticipated that RER would require a dewatering plan for the property if dewatering
is proposed as part of site development. If dewatering is being conducted in areas that
are demonstrated not to have arsenic impacts, then the dewatering plan would
demonstrate that the dewatering activities would not exacerbate or move groundwater
impacts. If dewatering activities will be performed in an area with impacted
groundwater, then treatment of the groundwater prior to discharge or disposal of
dewatering effluent would be required.
• Restrict the use of the irrigation wells to eliminate the influence of pumping impacted
groundwater.
• Route the point of discharge of drainage structures to outside the impacted area in Site B.
We recommend that the City seek RER’s conceptual approval of a site development approach
elected by the City including the above provisions. Regulatory closure will likely require
additional assessment.
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1.0 INTRODUCTION
The Site is comprised of two separate areas: Site A and Site B. Site A is a paved parking lot
located west of the Miami Beach Convention Center adjacent to Convention Center Drive. Site B
is adjacent south of Dade Boulevard and north of the Convention Center. Site A includes the 21st
Street Community Center and Band Shell Building, which are used by the Miami Beach Parks
and Recreation Division as part of their Teen Club center. The remaining portions of Site B
include a paved parking lot and the SoBe Institute of the Arts. These properties provide
recreational, cultural and parking services to residents and the public. The area surrounding Site
A and Site B consists of both residential and commercial properties. Both Site A and Site B are
owned by the City of Miami Beach (the City).
The western portion of Site A is comprised of six parcels. Site B and the eastern portion of Site
A are listed under the same folio number as the property developed with the Convention Center.
Portions of Site B were not linked to property information details on the Miami-Dade County
Property Appraiser website and a folio number was not identified. Table 1-1 provides
information obtained from the Miami-Dade County Property Appraiser.
TABLE 1-1 MIAMI-DADE COUNTY PROPERTY APPRAISER INFORMATION
FOLIO ADDRESS DESCRIPTION
02-3234-007-0110 1855 Meridian Avenue Western portion of Site A
02-3234-007-0100 Not provided Western portion of Site A
02-3234-007-0090 Not provided Western portion of Site A
02-3234-007-0080 Not provided Western portion of Site A
02-3234-007-0070 Not provided Western portion of Site A
02-3234-007-0060 1809 Meridian Avenue Western portion of Site A
02-3234-000-0090 500 17 Street Eastern portion of Site A and Site B
A Site location map is provided in Figure 1. A United States Geological Survey (USGS)
topographic map was used to help evaluate topographic information (Figure 2) and (Figure 3)
provides aerial coverage for the Site and surrounding properties.
The City is planning to redevelop the Site into a recreational park. E Sciences was engaged by
the City to perform a Phase II Environmental Site Assessment (ESA). The purpose of the Phase
II ESA was to evaluate the potential presence of contamination associated with recognized
environmental conditions (RECs) identified during a Phase I ESA conducted in November 2014
(see Section 2.0).
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2.0 BACKGROUND INFORMATION
E Sciences, Incorporated (E Sciences) performed a Phase I ESA in general accordance with the
consensus document known as ASTM International Practice E 1527-13, a guide for conducting
ESAs. The Phase I ESA was documented in a report dated November 4, 2014. The purpose of the
Phase I ESA was to identify potential sources of environmental contamination that constitute a
recognized environmental conditions (REC), as defined by the ASTM standard. The following
findings were documented during the Phase I ESA:
• Based on a review of historical documentation, Site B and the eastern portion of Site A
were part of the Miami Beach Municipal Golf Course in the 1950s. Typical chemicals
applied to golf courses during this time included arsenates, organochlorine pesticides, and
Ethylene Dibromide (EDB). Arsenate pesticides were banned by the US Environmental
Protection Agency (EPA) in the 1980s. Oganochlorine pesticides include dieldrin,
dichlorodiphenyltrichloroethane (DDT), chlordane and toxaphene. Most organochlorine
pesticides were banned in the 1970s and 1980s. Many pesticide constituents accumulate
and persist over time. The historical operation of a golf course is considered to be a REC
due to the likely historical repeated application of pesticides such as arsenate, DDT and
EDB.
• A review of historical documentation concerning the area surrounding the Site did not
reveal indications of contaminated properties or activities within the Site vicinity that
would, in our opinion, be considered a REC in relation to the Site with the exception of
the historic golf course.
• A review of regulatory documentation concerning the Site and surrounding area did not
reveal indications of contaminated properties or activities at the Site, or within the Site
vicinity, that would be considered a REC in relation to the Site.
• The site reconnaissance did not reveal the presence of Site conditions that would be
considered a REC in relation to the Site.
E Sciences was engaged by the City to perform a Phase II ESA. The scope of the Phase II ESA was
based on historical presence of the golf course within the Site.
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3.0 STATEMENT OF OBJECTIVES
The objective of the Phase II ESA activities was to evaluate the potential presence of
contamination based on the findings of the Phase I ESA. The Phase II ESA activities at the Site
were based on the suspected location of the RECs identified during the Phase I ESA (see Section
2.0). The sampling activities and laboratory analysis conducted were based on the nature of the
RECs and the potential contaminants of concern (COCs) associated with the historical activities at
the Site and adjacent properties.
The following scope of services was completed:
• Soil evaluation using Incremental Sampling Methodology (ISM).
• Groundwater sampling and analysis at predetermined locations.
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4.0 SITE ASSESSMENT ACTIVITIES
Field activities were conducted by E Sciences personnel on November 20 and 21, 2014 and
January 23,24 and 29, 2015. The drilling services were provided by our subcontractor and
licensed water well driller, JAEE Environmental Services, Inc. Laboratory analyses were
conducted by state-certified Palm Beach Environmental Laboratories, Inc. (PBEL) and Accutest
Laboratories, Inc. (Accutest). Sampling activities were conducted in accordance with FDEP
Standard Operating Procedures (SOPs) as applicable. The following sections document the
activities conducted and findings associated with the Phase II ESA activities.
For the purposes of the Phase II ESA, Site A and Site B were assessed separately and a similar
sampling scope and methodology was implemented on each site.
4.1 Incremental Soil Sampling
Soil samples were collected based on the concept of Incremental Sampling Methodology (ISM).
The Interstate Technology and Regulatory Council has published an ISM documented dated
February 2012. This methodology has been used on other sites within the State with regulatory
concurrence and we understand that the Florida Department of Environmental Protection (FDEP)
is drafting a guidance document for this process. This soil sampling methodology was
implemented in order to collect a representative sample of the Site based on potential historical
onsite contamination sources.
The eastern portion of Site A and Site B were defined as separate “Decision Units” (DU) (see
Figure 4A and Figure 4B). The DU boundaries for Site A were defined based on review of the
historical aerial photographs and location of the historical golf course. Large vehicles and
equipment were parked along the eastern and western boundaries of Site A; therefore, the DU
unit for Site A was limited to the readily accessible area. Each DU was subdivided into uniform
grid cells. Based on guidance documents for ISM, a minimum of 30 cells are required within
each DU in order to obtain a representative sample of the soil quality within the DU. A total of
32 cells on Site A and 31 cells in Site B were established. A pre-determined soil mass of
approximately 45 grams was collected within each grid cell using pre-measured sampling tools
provided by the laboratory. These individual samples are referred to as increments. Each
increment was collected at a random location and random depth from zero to 12 inches below
land surface (bls) within the cell but below the existing asphalt layer. Samples were collected
from the subsurface using Direct Push Technology (DPT). Individual increments collected were
placed into bulk sample containers. One bulk sample container was designated for analysis of
volatile compounds and a second bulk sample container for semi and non-volatile compounds.
An aerial photograph of the Site depicting the DU, grid and increment sampling locations is
included in Figure 4A and Figure 4B for Site A and B respectively.
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The soil samples were collected in laboratory provided containers and shipped to PBEL under
chain of custody protocol for ISM processing and analysis. Upon receipt of the samples, PBEL
processed the samples and initiated sub-sampling activities, which included air drying and sieving
the bulk sample to remove particles larger than two millimeters. The sieved bulk sample was
then spread into a thin layer and a grid was established. A total of 30 increments of equal mass
were collected in random locations across the spread-out sample to generate the final multi-
increment sample for analysis. This process is referred to as sub-sampling. The mass collected
from each sub-sampling location depended on the analytical test. The final multi-increment
sample for each DU (DU1 and DU2) was analyzed for the following contaminants: arsenic, lead,
organochlorine pesticides and organophosphate pesticides
TABLE 4-1 SOIL ANALYTICAL SCOPE
Contaminant of Concern EPA Analytical Method
Arsenic EPA Method SW846 6020B
Lead EPA Method SW846 6020B
Organochlorine Pesticides EPA Method 8081
Organophosphate Pesticides EPA Method 8270
Duplicate sample (DUP1 for DU-1 and DUP3 for DU-2) were collected in the field using the
same sampling methodology described above. The increments for theses duplicate samples were
collected at a location different from the original samples within the same cell. A third replicate
was collected using the same increment locations as the initial sample from each DU (DUP2 for
DU-1 and DUP4 for DU-2) to evaluate the accuracy of the laboratory procedures. The replicate
samples were analyzed per the analytical scope provided in Table 4-1 above.
4.2 Soil Sampling Analytical Results
Laboratory analytical results were compared to the Miami-Dade County Soil Cleanup Target
Levels (SCTLs) defined under Chapter 24 of the Miami-Dade County Code of Ordinances.
Furthermore, analytical results for Arsenic were compared to the “Barrier Islands Naturally
Occurring Background Concentrations” documented in the Miami-Dade County Regulatory and
Economic Resources (RER) Department’s memorandum regarding Miami-Dade County
Anthropogenic Background Study dated April 3, 2014.
Analytical results revealed the presence of pesticides compounds (4,4-DDE, Dieldrin and Total
Chlordane) and lead above the laboratory method detection limits in select samples. Arsenic
concentrations were detected above the Direct Exposure Residential SCTL for the incremental
samples collected from Site A and Site B. Table 4-2 presents a summary of the soil analytical
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results for the detected analytes. Laboratory analytical reports and chain of custody
documentation are included in Appendix A.
TABLE 4-2
SUMMARY OF SOIL PARAMETER DETECTIONS
Site Sample ID gamma-
Chlordane alpha-
Chlordane 4,4-DDE Dieldrin Total
Chlordane Arsenic Lead mg/kg
Site A
DU-2 0.0009 0.0006 0.0045 0.00004 U 0.0015 5.75 25.4
DUP3 0.0011 0.0008 0.0034 0.00004 U 0.0019 5.52 25.5
DUP4 0.0004 0.0003 0.0015 0.00004 U 0.0007 5.49 35.1
Site B DU-1 0.0011 0.0006 0.0067 0.00004 U 0.0017 9.04 45.5
DUP1 0.0007 0.0004 0.0032 0.0001 0.0012 9.13 311 E
DUP2 0.003 0.0003 0.0026 0.00004 U 0.0006 10.4 42.2 Miami-Dade Direct Exposure Residential SCTL NA NA 2.9 0.06 2.8 2.1 400 Miami-Dade Direct Exposure Commercial/Industrial SCTL NA NA 15 0.3 14 12 1400 Miami-Dade Leachability based SCTL NA NA 18 0.002 9.6 *** *** Barrier Islands Naturally Occurring Background Concentration NA NA NA NA NA 5.2 NA
Notes: This table presents only the concentrations of analytes detected. Other analytes were not detected above laboratory method
detection limits and are not included in this summary table.
Analytical results presented in mg/Kg unless specified mg/Kg: milligram per kilogram
U: Indicates analyte not detected above laboratory method detection limit. BOLD Indicates contaminant above Miami-Dade SCTL E: The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is
considered an estimate (CLP E-flag). *** Leachability values may be derived using the SPLP Test to calculate the site-specific SCTLs or may be determined using TCLP in the event of oily wastes are present. NA : Not Applicable
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4.3 Groundwater Sampling Activities
Groundwater sampling activities were conducted at the Site in order to evaluate the potential
presence of groundwater impacts associated with the historical operation of the golf course. Two
sampling events were conducted. An initial sampling event was conducted on November 21,
2013. A second event was conducted on January 25 and 29, 2015 based on information and
requirements presented by Miami-Dade County Regulatory and Economic Resources (RER)
department to include additional COCs (refer to Section 7.0).
4.3.1 Initial Groundwater Sampling Activities
The initial groundwater sampling was conducted using DPT by advancing probes to
approximately two feet into the water table using a stainless steel well point and withdrawing the
point to expose four feet of stainless steel screen. The groundwater sampling locations (DP-1 on
Site B and DP-2 on Site A) are depicted on Figure 5. Groundwater sampling activities were
conducted in accordance with FDEP Standard Operating Procedures (SOPs). Field parameters
(pH, conductivity, temperature, dissolved oxygen and turbidity) were measured during purging
using a multi-sensor probe and turbidity meter. Groundwater samples were collected in
laboratory supplied containers, packaged in ice-filled coolers and shipped to PBEL under chain of
custody protocol for analysis. Groundwater sampling logs are included in Appendix B. Table 4-
3 presents a summary of the COCs and analytical methods conducted during the initial sampling
event.
TABLE 4-3 INITIAL GROUNDWATER ANALYTICAL SCOPE
Contaminant of Concern EPA Analytical Method
Arsenic EPA Method SW846 6020B
Lead EPA Method SW846 6020B
Organochlorine Pesticides EPA Method 8081
Organophosphate Pesticides EPA Method 8270
4.3.2 Additional Groundwater Sampling Activities
Upon completion of the soil sampling and initial groundwater sampling events, a draft Phase II
ESA report dated December 17, 2014 was submitted to the City. The City submitted the draft
Phase II ESA report to RER for review and comment (See Section 7.0 for additional regulatory
involvement information). Based on this review, RER requested that the COCs for the
assessment include the following parameters:
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TABLE 4-4 ADDITIONAL GROUNDWATER ANALYTICAL SCOPE
Contaminant of Concern EPA Analytical Method
13 RCRA Metals* EPA Method SW846 6010/6020: As, Pb, Cd, Ag, Cr, Cu, Tl, Sb, Be, Ni, Se, Zn EPA Method SW846 7470/7471: Hg
Nitrates EPA Method 353.2
Nitrites EPA Method 353.2
Ammonia EPA Method 350.1 *Arsenic (As), Lead (Pb), Cadmium (Cd), Silver (Ag), Chromium (Cr), Selenium (Se), Mercury (Hg), Beryllium (Be), Zinc (Zn), Nickel (Ni), Copper (Cu), Antimony (Sb), Thallium (Tl).
Based on the anticipated dewatering activities at both sites during the proposed development, the
City elected to install two monitoring wells at each site to evaluate the potential presence of the
additional COC identified by RER.
Two monitoring wells were installed at Site A (MW-1 and MW-2) and Site B (MW-3 and MW-4)
as depicted on Figure 5. The monitoring wells were installed using DPT on January 23, 2015 by
JAEE under E Sciences oversight. The monitoring wells were installed to a maximum depth of l5
feet bls and constructed of ten feet of pre-packed well screen and a five-foot PVC riser. The
wells were completed with a well cap and a traffic-bearing manhole. Well construction and
development logs are provided in Appendix C. Well construction details are summarized in
Table 4-5 below.
TABLE 4-5 MONITORING WELL CONSTRUCTION DETAIL
SITE MONITORING
WELL ID.
Total Depth (ft
bls)
Screen Interval (ft
bls)
Well Diameter (inches)
Installation Method
Site A MW-1 15 5-15 1.25 DPT
MW-2 15 5-15 1.25 DPT
Site B MW-3 15 5-15 1.25 DPT
MW-4 15 5-15 1.25 DPT
The newly installed monitoring wells were sampled on January 24, 2015. Groundwater sampling
activities were conducted in accordance with FDEP Standard Operating Procedures (SOPs).
Field parameters (pH, conductivity, temperature, dissolved oxygen and turbidity) were measured
during purging using a multi-sensor probe and turbidity meter. Groundwater samples were
collected in laboratory supplied containers, packaged in ice-filled coolers and shipped to Accutest
under chain of custody protocols. Groundwater sampling logs are included in Appendix B. The
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analytical scope for these samples included the COCs identified by RER and also organochlorine
pesticides based on the detection of those parameters on the ISM soil samples collected.
4.4 Groundwater Sampling Analytical Results
Laboratory analytical results were compared to the Miami-Dade County Groundwater Cleanup
Target Levels (GCTLs) defined under Chapter 24 of the Miami-Dade Code of Ordinances. Intiial
analytical results revealed the presence of arsenic and lead above the laboratory method detection
limit but below GCTLs. The other COCs were not detected above the corresponding laboratory
method detection limit. A summary of the laboratory detections is provided in Table 4-4 below.
Laboratory analytical reports and chain of custody documentation are included in Appendix A.
TABLE 4-6 SUMMARY OF GROUNDWATER CONTAMINANT DETECTIONS
Antimony Arsenic Dissolved Arsenic
Chromium Lead Nickel Silver Zinc Ammonia
ug/l mg/l
Miami-Dade GCTL 6 10 10 100 15 100 100 5000 2.8
Site Sample
ID Sampling
Date
Site B
DP-1 11/21/2014 NA 8.3 NA NA 6 NA NA NA NA
MW-3 1/24/2015* 2.2 I 21.3 1.3 U 1.0 U 1.1 U 0.40 U 0.80 I 5.9 I 1.0
1/29/2015** NA 24.6 25 NA NA NA NA NA NA
MW-4 1/24/2015 1.5 I 4.1 I NA 1.8 I 1.1 U 1.6 I 0.70 U 4.4 U 0.22
Site A
DP-2 11/21/2013 NA
0.377 U NA NA 6 NA NA NA NA
MW-1 1/24/2015 1.0 U 1.3 U NA 1.5 I 1.1 U 0.40 U 0.70 U 8.1 I 1.6
MW-2 1/24/2015 1.1 I 1.3 U NA 1.4 I 1.1 U 0.40 U 0.70 U 6.4 I 1.4
Notes:
This table presents only the concentrations of analytes detected. Other analytes were not detected above laboratory method detection limits and are not included in this summary table. *Laboratory filtered with 0.45 micron filter. **Field filtered with 1.0 micron filter.
ug/L: Micrograms per Liter mg/L: Milligrams per Liter
U: Indicates analyte not detected above laboratory method detection limit. I: Indicates analyte concentration above the maximum detection limit but below practical quantitation limit. NA = Not Analyzed for that parameter.
BOLD Indicates contaminant above Miami-Dade GCTL
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5.0 PHASE II ESA LIMITATIONS
Although this assessment has attempted to identify the potential for environmental impacts to the
Site, potential sources of contamination may have escaped detection due to:
• the limited scope of this assessment
• the inaccuracy of public records
• the presence of undetected or unreported environmental incidents
• inaccessible areas or
• deliberate concealment of detrimental information by others
It was not the purpose of this study to determine the actual degree or extent of contamination, if
any, at the Site. The sampling conducted as part of the Phase II ESA was intended to confirm the
presence of impacts based on the identified RECs. No sampling or analysis was conducted
outside the locations identified within this document.
Due to the limited nature of this Phase II ESA, there is a possibility that conditions may exist
which were not apparent at the time of report preparation and completion of the previous Phase I
ESA. It is also possible that the testing methods employed at the time of the report may later be
superseded by other methods. The description, type, and composition of what are commonly
referred to as “hazardous materials or conditions” can also change over time. E Sciences does not
accept responsibility for changes in the state of the art, nor for changes in the scope of various
lists of hazardous materials or conditions. E Sciences believes that the findings and conclusions
provided in this report are reasonable. However, no other warranties are implied or expressed.
DRAFT
Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page 11 of 15 E Sciences Project Number 7-0002-023
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6.0 FINDINGS AND CONCLUSIONS
The Phase II ESA was designed to evaluate the potential presence of impacts from the historic
operation of a golf course at the Site identified during the previous Phase I ESA.
Soil analytical results revealed the presence of arsenic concentrations above Miami-Dade
County’s Direct Exposure Residential Soil Cleanup Target Levels (SCTL) for the incremental
soil samples collected from Site A and Site B. The detected arsenic concentrations were above
the documented Barrier Islands Naturally Occurring Background Concentration published by
Miami-Dade County. Other compounds detected below regulatory standards include lead and
pesticides (4,4-DDE, Total Chlordane, and Dieldrin).
Groundwater samples collected from Site A did not reveal the presence of COCs above the
corresponding GCTLs. Therefore, no groundwater impacts were identified within Site A during
this limited assessment.
Groundwater samples collected from Site B revealed the presence of arsenic concentration above
the GCTL in one of the three sampling locations. The arsenic concentration detected in
groundwater samples collected from MW-3 was reported above the GCTL as confirmed by a
second sampling event conducted based on initial results. To further evaluate the presence of
arsenic, the laboratory was asked to filter the sample collected on November 21, 2015 and
analyze for dissolved arsenic. The laboratory filtered the sample using a 0.45 micron filter, and
the results that dissolved arsenic concentration for the sample was not detected above the
laboratory detection limit or the GCTL. The second sample collected at this location on January
29, 2015 was filtered on the field using a 1.0 micron filter per FDEP SOPs. Analysis of this
sample revealed a similar concentration of arsenic for the unfiltered and filtered samples, both
above the GCTL. Based on these observations, we conclude that the laboratory filtering method
and 0.45 micron filter size was more effective in removing dissolved metals from the sample
aliquot.
Based on the results documented herein, arsenic concentration are present above the GCTL
within a portion of Site B. The extent of the arsenic impacts cannot be determined based on
results available at this time.
DRAFT
Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page 12 of 15 E Sciences Project Number 7-0002-023
This document is printed on recycled paper.
7.0 REGULATORY INVOLVEMENT
The City submitted the draft Phase II ESA report dated December 17, 2014 to Miami-Dade
County RER for review and comment regarding the regulatory course of action based on the
results of the ISM soil testing and initial soil and groundwater sampling.
On December 23, 2014, a meeting was held between RER, the City, Atkins and E Sciences
representatives to discuss select contaminated sites owned by the City including the subject sites.
RER had conducted only a preliminary review of the draft Phase II ESA at that time. Items
discussed during this meeting regarding the subject site included:
• The need to develop and implement a Soil Management Plan during construction
activities;
• The background naturally occurring arsenic concentration within the island is considered
to be the applicable cleanup standard for these sites;
• The extent of impacts has not yet been delineated based on the limited scope of the Phase
II ESA;
• Potential regulatory closure approaches;
• Engineering and institutional controls;
• Delineation and excavation of arsenic impacted soil;
• Drainage and dewatering considerations might be required and would be determined
based on additional groundwater sampling and analysis;
• Acceptable engineering control alternatives were discussed (i.e. artificial turf, asphalt and
concrete parking lots, geomembranes, clean soil cover).
RER issued initial comments regarding the Phase II ESA in email correspondence dated
December 24, 2014. RER requested that additional soil and groundwater testing be conducted for
both Site A and Site B and include offsite delineation of the potential impacts. Further
investigation regarding the past uses of the properties was also requested. RER noted that
additional comments and guidance will be provided upon review of the conceptual site
development plans.
The City responded to RER’s initial comments in email correspondence dated January 8, 2015.
The City indicated that offsite assessment would be conducted separately from the assessment of
the subject properties. The City stated that based on a more extensive review of additional
historical aerial photos, the presence of building structures just north of the original Convention
Center building were observed. The City interviewed a city employee who has been with the
City for 47 years, and he confirmed that these buildings and other activities visible in this area
were associated with the Parks & Recreation Department Headquarters housed at that location.
The Department used this property to store the maintenance equipment and products associated
DRAFT
Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page 13 of 15 E Sciences Project Number 7-0002-023
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with their operations throughout the City. Based on the results of additional aerial photograph
review and interview with key personnel, the City determined that the property's past uses do not
suggest the need to test additional parameters requested by RER. At this time RER has not
responded to the City’s email.
DRAFT
Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page 14 of 15 E Sciences Project Number 7-0002-023
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8.0 RECOMMENDATIONS
Based on the findings of this Phase II ESA and general guidance provided by RER, we provide
the following recommendations regarding the proposed development of Site A and Site B:
Recommendations pertaining to existing soil impacts are as follows:
• Prepare a Soil Management Plan (SMP) for review and approval by RER prior to
site development activities. The SMP should include the following provide
procedures and precautions to be implemented for the management of contaminated soil
during construction activities. The SMP should include information associated with the
following items, at a minimum:
o Background Information;
o Soil Management Requirements such as designated storage areas, stockpile
management and tracking protocols;
o Soil Characterization and Disposal Requirements;
o Dust Control measures;
o Waste Disposal;
o Decontamination procedures;
o Notification and responsibility requirements;
o Site control measures;
o Site maps.
• At this time we understand that the City has elected to proceed with the installation of an
engineering control in order to prevent exposure and migration of the impacted soil.
Based on the 30% design site plan provided by the City for the proposed development,
specific areas of Site A and Site B will be covered with a minimum of 12 inches of fill.
• Based on information provided by RER, installing a liner of specific characteristics (color
and impermeability) below 12 inches of fill may be sufficient to achieve the required
level of protection and serve as an engineering control for the Site. It is our
understanding that this engineering control alternative will be presented to RER for
formal approval. Liner characteristics may include, but are not limited to, impermeability
and color.
• Therefore, on those areas proposed to be raised by a minimum of 12 inches of fill, an
adequate liner will be installed prior to installation of the fill layer.
• The areas not currently proposed to be covered with a minimum of 12 inches of fill will
be excavated to a depth of 12 inches in order to install the liner followed by 12 inches of
clean fill. Please note that excavated soil will be subject to the SMP provisions and shall
be treated as contaminated soil.
• Those areas proposed to be covered by impermeable pavement (such as paved pathways,
roadways, parking) will serve as an engineering control (to be approved by RER).
DRAFT
Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page 15 of 15 E Sciences Project Number 7-0002-023
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Recommendations pertaining to existing groundwater impacts are as follows:
• Groundwater sampling did not indicate the presence of COCs within Site A. Therefore
no groundwater provisions are expected to be required during development on that site.
However, RER might request that additional groundwater sampling be conducted in the
specific dewatering areas to provide assurance that no groundwater impacts are present
within those areas and no potential groundwater contamination migration or exacerbation
occurs during dewatering.
• Arsenic concentrations were detected above the GCTL for the groundwater samples
collected from MW-3 at Site B. Therefore the following general recommendations are
provided:
o Secure a dewatering permit that includes evaluation and management of
impacted groundwater within Site B. Based on the results of the filtered samples,
we anticipate that the application of a filter process will be sufficient to treat the
water to regulatory standards for disposal purposes if treatment is necessary.
o It is anticipated that RER would require a dewatering plan for the property if
dewatering is proposed as part of site development. If dewatering is being
conducted in areas that are demonstrated not to have arsenic impacts, then the
dewatering plan would demonstrate that the dewatering activities would not
exacerbate or move groundwater impacts. If dewatering activities will be
performed in an area with impacted groundwater, then treatment of the
groundwater prior to discharge or disposal of dewatering effluent would be
required.
o Restrict the use of the irrigation wells to eliminate the influence of pumping
impacted groundwater.
o Route the point of discharge of drainage structures to outside the impacted area
in Site B.
We recommend that the City seeks RER’s conceptual approval of the closure approach elected by
the City including the above provisions. The above recommendations are concerning
development of the subject properties and do not include provisions regarding the regulatory
requirements regarding site assessment. Please note that RER may not grant regulatory closure of
the site based on the absence of soil impact delineation within the property boundaries and the
requirement for offsite delineation. Please note offsite assessment and implementation of a
restrictive covenant for the properties may be required to complete the regulatory closure of the
subject sites.
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FIGURES
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Site A
Site B
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E Sciences, IncorporatedFL Engineering Lic. #8691224 SE 9th StreetFt. Lauderdale, Florida 33316www.esciencesinc.comPhone: 954-484-8500Fax: 954-484-5146
DATE: 12/12/2014
SCALE:DRAWNBY: TV
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FIGURE21st Street Community Center and Band Shell Building and Parking
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0 500 1,000 1,500 2,000250
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USGS Topographic Map 21 "=1,000 '
E Sciences, IncorporatedFL Engineering Lic. #8691224 SE 9th StreetFt. Lauderdale, Florida 33316www.esciencesinc.comPhone: 954-484-8500Fax: 954-484-5146
DATE: 12/12/2014
SCALE:DRAWNBY: TV
CHECKEDBY: MP
FIGURE21st Street Community Center and Band Shell Building and Parking
Area West of Convention Center
0 500 1,000 1,500 2,000250
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PROJECT NUMBER:7-0002-023
Aerial Photograph 31 "=400 '
E Sciences, IncorporatedFL Engineering Lic. #8691224 SE 9th StreetFt. Lauderdale, Florida 33316www.esciencesinc.comPhone: 954-484-8500Fax: 954-484-5146
DATE: 12/12/2014
SCALE:DRAWNBY: TV
CHECKEDBY: MP
FIGURE21st Street Community Center and Band Shell Building and Parking
Area West of Convention Center
0 200 400 600 800100
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E Sciences, IncorporatedFL Engineering Lic. #8691224 SE 9th StreetFt. Lauderdale, Florida 33316www.esciencesinc.comPhone: 954-484-8500Fax: 954-484-5146
DATE: 12/12/2014
SCALE:DRAWNBY: TV
CHECKEDBY: MP
FIGURE21st Street Community Center and Band Shell Building and Parking
Area West of Convention Center
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Feet
Miami Beach, FL
DRAFT
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E Sciences, IncorporatedFL Engineering Lic. #8691224 SE 9th StreetFt. Lauderdale, Florida 33316www.esciencesinc.comPhone: 954-484-8500Fax: 954-484-5146
DATE: 12/12/2014
SCALE:DRAWNBY: TV
CHECKEDBY: MP
FIGURE21st Street Community Center and Band Shell Building and Parking
Area West of Convention Center
0 50 100 150 20025
Feet
Miami Beach, FL
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E Sciences, IncorporatedFL Engineering Lic. #8691224 SE 9th StreetFt. Lauderdale, Florida 33316www.esciencesinc.comPhone: 954-484-8500Fax: 954-484-5146
DATE: 1/28/2015
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FIGURE21st Street Community Center and Band Shell Building and Parking
Area West of Convention Center
0 100 200 300 40050
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Miami Beach, FL
DRAFT
APPENDIX A
DRAFT
Enclosed is the laboratory report for your project. All results meet the requirements of the NELAC standards. Please note the following:
(1) The samples were received as stated on the chain of custody, correctly labeled and at the proper temperature unless otherwise noted. The results contained in this report relate only to the items tested or to the samples as received by the laboratory.
(2) This report may not be reproduced except in full, without the written approval of the laboratory. Any
anomalies are noted in the case narrative.
(3) Results for all solid matrices are reported in dry weight unless otherwise noted.
(4) Results for all liquid matrices are analyzed as received in the laboratory unless otherwise noted.
(5) Samples are disposed of within 30 days of their receipt by the laboratory.
(6) A statement of Qualifiers is available upon request.
(7) Certain analyses are subcontracted to outside NELAC certified laboratories and are designated on your report.
(8) Precision & Accuracy will be provided when clients require a measure of estimated uncertainty.
(9) The issuance of the final Certificate of Analysis takes precedence over any previous Preliminary Report
Preliminary Data should not be used for regular purposes. Authorized signature(s) is provided on final report only
Please contact me if you have any questions or concerns regarding this report. Sincerely,
Pamela Shore QA Officer
December 04, 2014E Sciences
0013067
Maria Paituvi
Ft Lauderdale, FL 33316
(954) 484-8500
LOG #:
Page 1 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DP2-11212014Description:
Received:
Sampled:Lab ID: 0013067-01 11/21/14 12:45
11/21/14 16:00Matrix: Water Sampled By: Trent Van Allen
EPA Method 8081A
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
alpha-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-84-6 0.01110.004 0.004JEE, U
gamma-BHC (Lindane) SLug/L 11/25/14 11/26/14EPA 3510C / 8081A58-89-9 0.01110.004 0.004JEE, U
Heptachlor SLug/L 11/25/14 11/26/14EPA 3510C / 8081A76-44-8 0.01710.006 0.006JEE, U
Aldrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A309-00-2 0.01110.004 0.004JEE, U
beta-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-85-7 0.01310.004 0.004JEE, U
delta-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-86-8 0.01210.004 0.004JEE, U
Heptachlor epoxide SLug/L 11/25/14 11/26/14EPA 3510C / 8081A1024-57-3 0.01110.004 0.004JEE, U
Endosulfan I SLug/L 11/25/14 11/26/14EPA 3510C / 8081A959-98-8 0.01410.004 0.004JEE, U
gamma-Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081A5566-34-7 0.06010.020 0.020JEE, U
alpha-Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081A5103-71-9 0.06010.020 0.020JEE, U
4,4-DDE SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-55-9 0.01510.005 0.005JEE, U
Dieldrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A60-57-1 0.00210.00075 0.00075JEE, U
Endrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-20-8 0.01310.004 0.004JEE, U
Endosulfan II SLug/L 11/25/14 11/26/14EPA 3510C / 8081A33213-65-9 0.01710.006 0.006JEE, U
4,4-DDD SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-54-8 0.00710.002 0.002JEE, U
4,4-DDT SLug/L 11/25/14 11/26/14EPA 3510C / 8081A50-29-3 0.01310.004 0.004JEE, U
Endrin aldehyde SLug/L 11/25/14 11/26/14EPA 3510C / 8081A7421-93-4 0.01010.003 0.003JEE, U
Endosulfan sulfate SLug/L 11/25/14 11/26/14EPA 3510C / 8081A1031-07-8 0.00810.003 0.003JEE, U
Methoxychlor SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-43-5 0.01510.005 0.005JEE, U
Endrin Ketone SLug/L 11/25/14 11/26/14EPA 3510C / 8081A53494-70-5 0.01010.003 0.003JEE, U
Total Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081ANA 0.06010.020 0.020JEE, U
Toxaphene SLug/L 11/25/14 11/26/14EPA 3510C / 8081A8001-35-2 0.22510.075 0.075JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Decachlorobiphenyl %2051-24-3 Limit 46-153JEE, U
Surrogate: Tetrachloro-m-xylene %877-09-8 Limit 56-153JEE, U
Page 2 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DP2-11212014Description:
Received:
Sampled:Lab ID: 0013067-01 11/21/14 12:45
11/21/14 16:00Matrix: Water Sampled By: Trent Van Allen
EPA Method 8141 List in Water
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Bolstar, (Sulprofos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.0910.03 0.03JEE, U
Crotoxphos (Ciodrin) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.0810.009 0.009JEE, U
Dichlofenthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 5.010.02 0.02JEE, U
Aspon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C3244-90-4 0.110.04 0.04JEE, U
Azinphos, Methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C86-50-0 0.110.04 0.04JEE, U
Azinphos, Ethyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2642-71-9 0.110.04 0.04JEE, U
Carbophenothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C786-19-6 0.110.04 0.04JEE, U
Chlorpyrifos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2921-88-2 0.110.04 0.04JEE, U
Chlorpyrifos Methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C5598-13-0 0.0810.03 0.03JEE, U
Coumaphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C56-72-4 0.410.1 0.1JEE, U
Demeton O & S SLug/L 11/25/14 11/25/14EPA 3510C / 8270C8065-48-3 0.210.05 0.05JEE, U
Diazinon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C333-41-5 0.110.04 0.04JEE, U
Dichlorvos (DDVP) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C62-73-7 0.0410.01 0.01JEE, U
Dicrotophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C141-66-2 0.0410.02 0.02JEE, U
Dimethoate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C60-51-5 0.0510.02 0.02JEE, U
Dioxathion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C78-34-2 0.0910.03 0.03JEE, U
Disulfoton SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-04-4 0.210.08 0.08JEE, U
EPN SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2104-64-5 0.0910.03 0.03JEE, U
Ethion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C563-12-2 0.0810.02 0.02JEE, U
Ethoprop SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13194-48-4 0.0910.03 0.03JEE, U
Famphur SLug/L 11/25/14 11/25/14EPA 3510C / 8270C52-85-7 0.0810.03 0.03JEE, U
Fenitrothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C122-14-5 0.0410.02 0.02JEE, U
Fensulfothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C115-90-2 0.0210.005 0.005JEE, U
Fenthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C55-38-9 0.0910.03 0.03JEE, U
Fonophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C944-22-9 0.0510.02 0.02JEE, U
Leptophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C21609-90-5 0.210.06 0.06JEE, U
Malathion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C121-75-5 0.110.03 0.03JEE, U
Merphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C150-50-5 0.210.08 0.08JEE, U
Mevinphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C7786-34-7 0.0710.02 0.02JEE, U
Monocrotophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C6923-22-4 0.0210.007 0.007JEE, U
Naled SLug/L 11/25/14 11/25/14EPA 3510C / 8270C300-76-5 0.0310.01 0.01JEE, U
Parathion-ethyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C56-38-2 0.310.1 0.1JEE, U
Parathion-methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-00-0 0.0210.008 0.008JEE, U
Phorate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-02-2 0.0610.02 0.02JEE, U
Phosphamidon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13171-21-6 0.0510.02 0.02JEE, U
Ronnel SLug/L 11/25/14 11/25/14EPA 3510C / 8270C299-84-3 0.110.04 0.04JEE, U
Page 3 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DP2-11212014Description:
Received:
Sampled:Lab ID: 0013067-01 11/21/14 12:45
11/21/14 16:00Matrix: Water Sampled By: Trent Van Allen
EPA Method 8141 List in Water
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Stirophos (Tetrachlorvinphos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C22248-79-9 0.0510.02 0.02JEE, U
Sulfotepp SLug/L 11/25/14 11/25/14EPA 3510C / 8270C3689-24-5 0.0810.03 0.03JEE, U
Terbufos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13071-79-9 0.0610.02 0.02JEE, U
Thionazin (Zinophos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C297-97-2 0.0710.02 0.02JEE, U
Tokuthion (Prothiofos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C34643-46-4 0.0410.01 0.01JEE, U
Trichloronate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C327-98-0 0.210.06 0.06JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Nitrobenzene-d5 %NA Limit 47-131JEE, U
Surrogate: 2-Fluorobiphenyl %321-60-8 Limit 51-134JEE, U
Surrogate: p-Terphenyl-d14 %NA Limit 59-135JEE, U
Metals by EPA 6000/7000 Series Methods
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Arsenic DDmg/L 11/25/14 11/25/14EPA 6020B7440-38-2 0.00510.000377 0.000377U
Lead DDmg/L 11/25/14 11/25/14EPA 6020B7439-92-1 0.00510.006 0.00001
Page 4 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DU2-11212014Description:
Received:
Sampled:Lab ID: 0013067-02 11/21/14 14:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8081A
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
alpha-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-84-6 0.110.03 0.03U
gamma-BHC (Lindane) DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A58-89-9 0.110.04 0.04U
Heptachlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A76-44-8 0.110.04 0.04U
Aldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A309-00-2 0.110.03 0.03U
beta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-85-7 0.110.05 0.05U
delta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-86-8 0.110.04 0.04U
Heptachlor epoxide DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1024-57-3 0.110.04 0.04U
Endosulfan I DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A959-98-8 0.110.03 0.03U
gamma-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5566-34-7 0.110.9 0.04
alpha-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5103-71-9 0.110.6 0.04
4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.114.5 0.04
Dieldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A60-57-1 0.110.04 0.04U
Endrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-20-8 0.110.01 0.01U
Endosulfan II DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A33213-65-9 0.110.05 0.05U
4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U
4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U
Endrin aldehyde DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A7421-93-4 0.110.04 0.04U
Endosulfan sulfate DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1031-07-8 0.110.04 0.04U
Methoxychlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-43-5 0.110.1 0.1U
Endrin Ketone DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A53494-70-5 0.110.03 0.03U
Total Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081ANA 0.111.5 0.1
Toxaphene DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A8001-35-2 0.110.1 0.1U
% Recovery % Recovery LimitsQ
Surrogate: Decachlorobiphenyl 132 %2051-24-3 Limit 41-170
Surrogate: Tetrachloro-m-xylene 108 %877-09-8 Limit 40-175
Page 5 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DU2-11212014Description:
Received:
Sampled:Lab ID: 0013067-02 11/21/14 14:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Bolstar, (Sulprofos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0075410.00251 0.00251JEE, U
Crotoxphos (Ciodrin) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0018110.000602 0.000602JEE, U
Dichlofenthion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0068910.00230 0.00230JEE, U
Aspon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C3244-90-4 0.0073110.00244 0.00244JEE, U
Azinphos, Methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C86-50-0 0.0105010.00350 0.00350JEE, U
Azinphos, Ethyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2642-71-9 0.0087110.00290 0.00290JEE, U
Carbophenothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C786-19-6 0.0097810.00326 0.00326JEE, U
Chlorpyrifos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2921-88-2 0.0043010.00143 0.00143JEE, U
Chlorpyrifos Methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C5598-13-0 0.0063910.00213 0.00213JEE, U
Coumaphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C56-72-4 0.0192010.00641 0.00641JEE, U
Demeton O & S SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C8065-48-3 0.0159010.00530 0.00530JEE, U
Diazinon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C333-41-5 0.0043310.00144 0.00144JEE, U
Dichlorvos (DDVP) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C62-73-7 0.0055810.00186 0.00186JEE, U
Dicrotophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C141-66-2 0.00095610.000319 0.000319JEE, U
Dimethoate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C60-51-5 0.0024510.000816 0.000816JEE, U
Dioxathion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C78-34-2 0.0070010.00233 0.00233JEE, U
Disulfoton SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-04-4 0.0178010.00592 0.00592JEE, U
EPN SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2104-64-5 0.0079610.00266 0.00266JEE, U
Ethion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C563-12-2 0.0072510.00242 0.00242JEE, U
Ethoprop SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13194-48-4 0.0063810.00213 0.00213JEE, U
Famphur SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C52-85-7 0.0076510.00255 0.00255JEE, U
Fenitrothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C122-14-5 0.0044910.00150 0.00150JEE, U
Fensulfothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C115-90-2 0.0017710.00059 0.00059JEE, U
Fenthion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C55-38-9 0.0068010.00227 0.00227JEE, U
Fonophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C944-22-9 0.0035310.00118 0.00118JEE, U
Leptophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C21609-90-5 0.0124010.00413 0.00413JEE, U
Malathion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C121-75-5 0.0059410.00198 0.00198JEE, U
Merphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C150-50-5 0.0227010.00758 0.00758JEE, U
Mevinphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C7786-34-7 0.0027510.000916 0.000916JEE, U
Monocrotophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C6923-22-4 0.00095310.000318 0.000318JEE, U
Naled SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C300-76-5 0.0023110.000769 0.000769JEE, U
Parathion-ethyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C56-38-2 0.0290010.00967 0.00967JEE, U
Parathion-methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-00-0 0.0056710.00189 0.00189JEE, U
Phorate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-02-2 0.0081010.00270 0.00270JEE, U
Phosphamidon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13171-21-6 0.0014610.000487 0.000487JEE, U
Ronnel SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C299-84-3 0.0074710.00249 0.00249JEE, U
Page 6 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DU2-11212014Description:
Received:
Sampled:Lab ID: 0013067-02 11/21/14 14:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Stirophos (Tetrachlorvinphos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C22248-79-9 0.0036710.00122 0.00122JEE, U
Sulfotepp SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C3689-24-5 0.0081910.00273 0.00273JEE, U
Terbufos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13071-79-9 0.0069010.00230 0.00230JEE, U
Thionazin (Zinophos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C297-97-2 0.0066210.00220 0.00220JEE, U
Tokuthion (Prothiofos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C34643-46-4 0.00025318.40E-5 8.40E-5JEE, U
Trichloronate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C327-98-0 0.0092010.00307 0.00307JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Nitrobenzene-d5 %NA Limit 47-131JEE, U
Surrogate: 2-Fluorobiphenyl %321-60-8 Limit 51-134JEE, U
Surrogate: p-Terphenyl-d14 %NA Limit 59-135JEE, U
Metals by EPA 6000/7000 Series Methods
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Arsenic PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7440-38-2 0.20015.75 0.003
Lead PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7439-92-1 0.200125.4 0.007
Percent Dry Weight
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
% Solids AT% 11/23/14 11/26/14CalculationNA 1.01100 1.0
Page 7 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DUP3-11212014Description:
Received:
Sampled:Lab ID: 0013067-03 11/21/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8081A
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
alpha-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-84-6 0.110.03 0.03U
gamma-BHC (Lindane) DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A58-89-9 0.110.04 0.04U
Heptachlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A76-44-8 0.110.04 0.04U
Aldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A309-00-2 0.110.03 0.03U
beta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-85-7 0.110.05 0.05U
delta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-86-8 0.110.04 0.04U
Heptachlor epoxide DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1024-57-3 0.110.04 0.04U
Endosulfan I DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A959-98-8 0.110.03 0.03U
gamma-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5566-34-7 0.111.1 0.04
alpha-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5103-71-9 0.110.8 0.04
4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.113.4 0.04
Dieldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A60-57-1 0.110.04 0.04U
Endrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-20-8 0.110.01 0.01U
Endosulfan II DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A33213-65-9 0.110.05 0.05U
4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U
4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U
Endrin aldehyde DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A7421-93-4 0.110.04 0.04U
Endosulfan sulfate DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1031-07-8 0.110.04 0.04U
Methoxychlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-43-5 0.110.1 0.1U
Endrin Ketone DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A53494-70-5 0.110.03 0.03U
Total Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081ANA 0.111.9 0.1
Toxaphene DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A8001-35-2 0.110.1 0.1U
% Recovery % Recovery LimitsQ
Surrogate: Decachlorobiphenyl 137 %2051-24-3 Limit 41-170
Surrogate: Tetrachloro-m-xylene 112 %877-09-8 Limit 40-175
Page 8 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DUP3-11212014Description:
Received:
Sampled:Lab ID: 0013067-03 11/21/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Bolstar, (Sulprofos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0075410.00251 0.00251JEE, U
Crotoxphos (Ciodrin) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0018110.000602 0.000602JEE, U
Dichlofenthion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0068910.00230 0.00230JEE, U
Aspon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C3244-90-4 0.0073110.00244 0.00244JEE, U
Azinphos, Methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C86-50-0 0.0105010.00350 0.00350JEE, U
Azinphos, Ethyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2642-71-9 0.0087110.00290 0.00290JEE, U
Carbophenothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C786-19-6 0.0097810.00326 0.00326JEE, U
Chlorpyrifos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2921-88-2 0.0043010.00143 0.00143JEE, U
Chlorpyrifos Methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C5598-13-0 0.0063910.00213 0.00213JEE, U
Coumaphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C56-72-4 0.0192010.00641 0.00641JEE, U
Demeton O & S SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C8065-48-3 0.0159010.00530 0.00530JEE, U
Diazinon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C333-41-5 0.0043310.00144 0.00144JEE, U
Dichlorvos (DDVP) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C62-73-7 0.0055810.00186 0.00186JEE, U
Dicrotophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C141-66-2 0.00095610.000319 0.000319JEE, U
Dimethoate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C60-51-5 0.0024510.000816 0.000816JEE, U
Dioxathion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C78-34-2 0.0070010.00233 0.00233JEE, U
Disulfoton SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-04-4 0.0178010.00592 0.00592JEE, U
EPN SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2104-64-5 0.0079610.00266 0.00266JEE, U
Ethion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C563-12-2 0.0072510.00242 0.00242JEE, U
Ethoprop SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13194-48-4 0.0063810.00213 0.00213JEE, U
Famphur SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C52-85-7 0.0076510.00255 0.00255JEE, U
Fenitrothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C122-14-5 0.0044910.00150 0.00150JEE, U
Fensulfothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C115-90-2 0.0017710.00059 0.00059JEE, U
Fenthion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C55-38-9 0.0068010.00227 0.00227JEE, U
Fonophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C944-22-9 0.0035310.00118 0.00118JEE, U
Leptophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C21609-90-5 0.0124010.00413 0.00413JEE, U
Malathion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C121-75-5 0.0059410.00198 0.00198JEE, U
Merphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C150-50-5 0.0227010.00758 0.00758JEE, U
Mevinphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C7786-34-7 0.0027510.000916 0.000916JEE, U
Monocrotophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C6923-22-4 0.00095310.000318 0.000318JEE, U
Naled SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C300-76-5 0.0023110.000769 0.000769JEE, U
Parathion-ethyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C56-38-2 0.0290010.00967 0.00967JEE, U
Parathion-methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-00-0 0.0056710.00189 0.00189JEE, U
Phorate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-02-2 0.0081010.00270 0.00270JEE, U
Phosphamidon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13171-21-6 0.0014610.000487 0.000487JEE, U
Ronnel SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C299-84-3 0.0074710.00249 0.00249JEE, U
Page 9 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DUP3-11212014Description:
Received:
Sampled:Lab ID: 0013067-03 11/21/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Stirophos (Tetrachlorvinphos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C22248-79-9 0.0036710.00122 0.00122JEE, U
Sulfotepp SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C3689-24-5 0.0081910.00273 0.00273JEE, U
Terbufos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13071-79-9 0.0069010.00230 0.00230JEE, U
Thionazin (Zinophos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C297-97-2 0.0066210.00220 0.00220JEE, U
Tokuthion (Prothiofos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C34643-46-4 0.00025318.40E-5 8.40E-5JEE, U
Trichloronate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C327-98-0 0.0092010.00307 0.00307JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Nitrobenzene-d5 %NA Limit 47-131JEE, U
Surrogate: 2-Fluorobiphenyl %321-60-8 Limit 51-134JEE, U
Surrogate: p-Terphenyl-d14 %NA Limit 59-135JEE, U
Metals by EPA 6000/7000 Series Methods
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Arsenic PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7440-38-2 0.20015.52 0.003
Lead PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7439-92-1 0.200125.5 0.007
Percent Dry Weight
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
% Solids AT% 11/23/14 11/26/14CalculationNA 1.01100 1.0
Page 10 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DUP4-11212014Description:
Received:
Sampled:Lab ID: 0013067-04 11/21/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8081A
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
alpha-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-84-6 0.110.03 0.03U
gamma-BHC (Lindane) DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A58-89-9 0.110.04 0.04U
Heptachlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A76-44-8 0.110.04 0.04U
Aldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A309-00-2 0.110.03 0.03U
beta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-85-7 0.110.05 0.05U
delta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-86-8 0.110.04 0.04U
Heptachlor epoxide DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1024-57-3 0.110.04 0.04U
Endosulfan I DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A959-98-8 0.110.03 0.03U
gamma-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5566-34-7 0.110.4 0.04
alpha-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5103-71-9 0.110.3 0.04
4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.111.5 0.04
Dieldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A60-57-1 0.110.04 0.04U
Endrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-20-8 0.110.01 0.01U
Endosulfan II DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A33213-65-9 0.110.05 0.05U
4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U
4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U
Endrin aldehyde DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A7421-93-4 0.110.04 0.04U
Endosulfan sulfate DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1031-07-8 0.110.04 0.04U
Methoxychlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-43-5 0.110.1 0.1U
Endrin Ketone DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A53494-70-5 0.110.03 0.03U
Total Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081ANA 0.110.7 0.1
Toxaphene DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A8001-35-2 0.110.1 0.1U
% Recovery % Recovery LimitsQ
Surrogate: Decachlorobiphenyl 136 %2051-24-3 Limit 41-170
Surrogate: Tetrachloro-m-xylene 102 %877-09-8 Limit 40-175
Page 11 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DUP4-11212014Description:
Received:
Sampled:Lab ID: 0013067-04 11/21/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Bolstar, (Sulprofos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0075410.00251 0.00251JEE, U
Crotoxphos (Ciodrin) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0018110.000602 0.000602JEE, U
Dichlofenthion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0068910.00230 0.00230JEE, U
Aspon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C3244-90-4 0.0073110.00244 0.00244JEE, U
Azinphos, Methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C86-50-0 0.0105010.00350 0.00350JEE, U
Azinphos, Ethyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2642-71-9 0.0087110.00290 0.00290JEE, U
Carbophenothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C786-19-6 0.0097810.00326 0.00326JEE, U
Chlorpyrifos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2921-88-2 0.0043010.00143 0.00143JEE, U
Chlorpyrifos Methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C5598-13-0 0.0063910.00213 0.00213JEE, U
Coumaphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C56-72-4 0.0192010.00641 0.00641JEE, U
Demeton O & S SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C8065-48-3 0.0159010.00530 0.00530JEE, U
Diazinon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C333-41-5 0.0043310.00144 0.00144JEE, U
Dichlorvos (DDVP) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C62-73-7 0.0055810.00186 0.00186JEE, U
Dicrotophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C141-66-2 0.00095610.000319 0.000319JEE, U
Dimethoate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C60-51-5 0.0024510.000816 0.000816JEE, U
Dioxathion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C78-34-2 0.0070010.00233 0.00233JEE, U
Disulfoton SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-04-4 0.0178010.00592 0.00592JEE, U
EPN SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2104-64-5 0.0079610.00266 0.00266JEE, U
Ethion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C563-12-2 0.0072510.00242 0.00242JEE, U
Ethoprop SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13194-48-4 0.0063810.00213 0.00213JEE, U
Famphur SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C52-85-7 0.0076510.00255 0.00255JEE, U
Fenitrothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C122-14-5 0.0044910.00150 0.00150JEE, U
Fensulfothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C115-90-2 0.0017710.00059 0.00059JEE, U
Fenthion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C55-38-9 0.0068010.00227 0.00227JEE, U
Fonophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C944-22-9 0.0035310.00118 0.00118JEE, U
Leptophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C21609-90-5 0.0124010.00413 0.00413JEE, U
Malathion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C121-75-5 0.0059410.00198 0.00198JEE, U
Merphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C150-50-5 0.0227010.00758 0.00758JEE, U
Mevinphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C7786-34-7 0.0027510.000916 0.000916JEE, U
Monocrotophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C6923-22-4 0.00095310.000318 0.000318JEE, U
Naled SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C300-76-5 0.0023110.000769 0.000769JEE, U
Parathion-ethyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C56-38-2 0.0290010.00967 0.00967JEE, U
Parathion-methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-00-0 0.0056710.00189 0.00189JEE, U
Phorate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-02-2 0.0081010.00270 0.00270JEE, U
Phosphamidon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13171-21-6 0.0014610.000487 0.000487JEE, U
Ronnel SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C299-84-3 0.0074710.00249 0.00249JEE, U
Page 12 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21619
12/4/2014 9:24:08AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013067
DUP4-11212014Description:
Received:
Sampled:Lab ID: 0013067-04 11/21/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Stirophos (Tetrachlorvinphos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C22248-79-9 0.0036710.00122 0.00122JEE, U
Sulfotepp SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C3689-24-5 0.0081910.00273 0.00273JEE, U
Terbufos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13071-79-9 0.0069010.00230 0.00230JEE, U
Thionazin (Zinophos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C297-97-2 0.0066210.00220 0.00220JEE, U
Tokuthion (Prothiofos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C34643-46-4 0.00025318.40E-5 8.40E-5JEE, U
Trichloronate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C327-98-0 0.0092010.00307 0.00307JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Nitrobenzene-d5 %NA Limit 47-131JEE, U
Surrogate: 2-Fluorobiphenyl %321-60-8 Limit 51-134JEE, U
Surrogate: p-Terphenyl-d14 %NA Limit 59-135JEE, U
Metals by EPA 6000/7000 Series Methods
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Arsenic PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7440-38-2 0.20015.49 0.003
Lead PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7439-92-1 0.200135.1 0.007
Percent Dry Weight
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
% Solids AT% 11/23/14 11/26/14CalculationNA 1.01100 1.0
Page 13 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
Notes and Definitions
Analyte included in the analysis, but not detectedU
Analysis performed by Florida Environmental Cert#E86006JEE
Page 14 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
Enclosed is the laboratory report for your project. All results meet the requirements of the NELAC standards. Please note the following:
(1) The samples were received as stated on the chain of custody, correctly labeled and at the proper temperature unless otherwise noted. The results contained in this report relate only to the items tested or to the samples as received by the laboratory.
(2) This report may not be reproduced except in full, without the written approval of the laboratory. Any
anomalies are noted in the case narrative.
(3) Results for all solid matrices are reported in dry weight unless otherwise noted.
(4) Results for all liquid matrices are analyzed as received in the laboratory unless otherwise noted.
(5) Samples are disposed of within 30 days of their receipt by the laboratory.
(6) A statement of Qualifiers is available upon request.
(7) Certain analyses are subcontracted to outside NELAC certified laboratories and are designated on your report.
(8) Precision & Accuracy will be provided when clients require a measure of estimated uncertainty.
(9) The issuance of the final Certificate of Analysis takes precedence over any previous Preliminary Report
Preliminary Data should not be used for regular purposes. Authorized signature(s) is provided on final report only
Please contact me if you have any questions or concerns regarding this report. Sincerely,
Pamela Shore QA Officer
December 04, 2014E Sciences
0013068
Maria Paituvi
Ft Lauderdale, FL 33316
(954) 484-8500
LOG #:
Page 1 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DP1-11202014Description:
Received:
Sampled:Lab ID: 0013068-01 11/20/14 13:45
11/21/14 16:00Matrix: Water Sampled By: Trent Van Allen
EPA Method 8081A
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
alpha-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-84-6 0.01110.004 0.004JEE, U
gamma-BHC (Lindane) SLug/L 11/25/14 11/26/14EPA 3510C / 8081A58-89-9 0.01110.004 0.004JEE, U
Heptachlor SLug/L 11/25/14 11/26/14EPA 3510C / 8081A76-44-8 0.01710.006 0.006JEE, U
Aldrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A309-00-2 0.01110.004 0.004JEE, U
beta-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-85-7 0.01310.004 0.004JEE, U
delta-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-86-8 0.01210.004 0.004JEE, U
Heptachlor epoxide SLug/L 11/25/14 11/26/14EPA 3510C / 8081A1024-57-3 0.01110.004 0.004JEE, U
Endosulfan I SLug/L 11/25/14 11/26/14EPA 3510C / 8081A959-98-8 0.01410.004 0.004JEE, U
gamma-Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081A5566-34-7 0.06010.020 0.020JEE, U
alpha-Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081A5103-71-9 0.06010.020 0.020JEE, U
4,4-DDE SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-55-9 0.01510.005 0.005JEE, U
Dieldrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A60-57-1 0.00210.00075 0.00075JEE, U
Endrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-20-8 0.01310.004 0.004JEE, U
Endosulfan II SLug/L 11/25/14 11/26/14EPA 3510C / 8081A33213-65-9 0.01710.006 0.006JEE, U
4,4-DDD SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-54-8 0.00710.002 0.002JEE, U
4,4-DDT SLug/L 11/25/14 11/26/14EPA 3510C / 8081A50-29-3 0.01310.004 0.004JEE, U
Endrin aldehyde SLug/L 11/25/14 11/26/14EPA 3510C / 8081A7421-93-4 0.01010.003 0.003JEE, U
Endosulfan sulfate SLug/L 11/25/14 11/26/14EPA 3510C / 8081A1031-07-8 0.00810.003 0.003JEE, U
Methoxychlor SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-43-5 0.01510.005 0.005JEE, U
Endrin Ketone SLug/L 11/25/14 11/26/14EPA 3510C / 8081A53494-70-5 0.01010.003 0.003JEE, U
Total Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081ANA 0.06010.020 0.020JEE, U
Toxaphene SLug/L 11/25/14 11/26/14EPA 3510C / 8081A8001-35-2 0.22510.075 0.075JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Decachlorobiphenyl %2051-24-3 Limit 46-153JEE, U
Surrogate: Tetrachloro-m-xylene %877-09-8 Limit 56-153JEE, U
Page 2 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DP1-11202014Description:
Received:
Sampled:Lab ID: 0013068-01 11/20/14 13:45
11/21/14 16:00Matrix: Water Sampled By: Trent Van Allen
EPA Method 8141 List in Water
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Bolstar, (Sulprofos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.110.004 0.004JEE, U
Crotoxphos (Ciodrin) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.0310.009 0.009JEE, U
Dichlofenthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.0810.02 0.02JEE, U
Guthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 5.01JEE, U
Aspon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C3244-90-4 0.110.04 0.04JEE, U
Azinphos, Methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C86-50-0 0.110.04 0.04JEE, U
Azinphos, Ethyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2642-71-9 0.110.04 0.04JEE, U
Carbophenothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C786-19-6 0.110.04 0.04JEE, U
Chlorpyrifos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2921-88-2 0.110.04 0.04JEE, U
Chlorpyrifos Methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C5598-13-0 0.0810.03 0.03JEE, U
Coumaphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C56-72-4 0.410.1 0.1JEE, U
Demeton O & S SLug/L 11/25/14 11/25/14EPA 3510C / 8270C8065-48-3 0.210.05 0.05JEE, U
Diazinon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C333-41-5 0.110.04 0.04JEE, U
Dichlorvos (DDVP) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C62-73-7 0.0410.01 0.01JEE, U
Dicrotophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C141-66-2 0.0410.02 0.02JEE, U
Dimethoate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C60-51-5 0.0510.02 0.02JEE, U
Dioxathion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C78-34-2 0.0910.03 0.03JEE, U
Disulfoton SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-04-4 0.210.08 0.08JEE, U
EPN SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2104-64-5 0.0910.03 0.03JEE, U
Ethion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C563-12-2 0.0810.02 0.02JEE, U
Ethoprop SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13194-48-4 0.0910.03 0.03JEE, U
Famphur SLug/L 11/25/14 11/25/14EPA 3510C / 8270C52-85-7 0.0810.03 0.03JEE, U
Fenitrothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C122-14-5 0.0410.02 0.02JEE, U
Fensulfothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C115-90-2 0.0210.005 0.005JEE, U
Fenthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C55-38-9 0.0910.03 0.03JEE, U
Fonophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C944-22-9 0.0510.02 0.02JEE, U
Leptophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C21609-90-5 0.210.06 0.06JEE, U
Malathion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C121-75-5 0.110.03 0.03JEE, U
Merphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C150-50-5 0.210.08 0.08JEE, U
Mevinphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C7786-34-7 0.0710.02 0.02JEE, U
Monocrotophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C6923-22-4 0.0210.007 0.007JEE, U
Naled SLug/L 11/25/14 11/25/14EPA 3510C / 8270C300-76-5 0.0310.01 0.01JEE, U
Parathion-ethyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C56-38-2 0.310.1 0.1JEE, U
Parathion-methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-00-0 0.0210.008 0.008JEE, U
Phorate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-02-2 0.0610.02 0.02JEE, U
Phosphamidon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13171-21-6 0.0510.02 0.02JEE, U
Page 3 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DP1-11202014Description:
Received:
Sampled:Lab ID: 0013068-01 11/20/14 13:45
11/21/14 16:00Matrix: Water Sampled By: Trent Van Allen
EPA Method 8141 List in Water
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Ronnel SLug/L 11/25/14 11/25/14EPA 3510C / 8270C299-84-3 0.110.04 0.04JEE, U
Stirophos (Tetrachlorvinphos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C22248-79-9 0.0510.02 0.02JEE, U
Sulfotepp SLug/L 11/25/14 11/25/14EPA 3510C / 8270C3689-24-5 0.0810.03 0.03JEE, U
TEPP (Tetraethyl Pyrophosphate) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C107-49-3 5.01JEE, U
Terbufos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13071-79-9 0.0610.02 0.02JEE, U
Thionazin (Zinophos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C297-97-2 0.0710.02 0.02JEE, U
Tokuthion (Prothiofos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C34643-46-4 0.0410.01 0.01JEE, U
Trichlorfon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C52-68-6 5.01JEE, U
Trichloronate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C327-98-0 0.210.06 0.06JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Nitrobenzene-d5 %NA Limit 47-131JEE, U
Surrogate: 2-Fluorobiphenyl %321-60-8 Limit 51-134JEE, U
Surrogate: p-Terphenyl-d14 %NA Limit 59-135JEE, U
Metals by EPA 6000/7000 Series Methods
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Arsenic DDmg/L 11/25/14 11/25/14EPA 6020B7440-38-2 0.00510.0083 0.000377
Lead DDmg/L 11/25/14 11/25/14EPA 6020B7439-92-1 0.00510.006 0.00001
Page 4 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DU1-11202014Description:
Received:
Sampled:Lab ID: 0013068-02 11/20/14 15:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8081A
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
alpha-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-84-6 0.110.03 0.03U
gamma-BHC (Lindane) DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A58-89-9 0.110.04 0.04U
Heptachlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A76-44-8 0.110.04 0.04U
Aldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A309-00-2 0.110.03 0.03U
beta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-85-7 0.110.05 0.05U
delta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-86-8 0.110.04 0.04U
Heptachlor epoxide DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1024-57-3 0.110.04 0.04U
Endosulfan I DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A959-98-8 0.110.03 0.03U
gamma-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5566-34-7 0.111.1 0.04
alpha-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5103-71-9 0.110.6 0.04
4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.116.7 0.04
Dieldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A60-57-1 0.110.04 0.04U
Endrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-20-8 0.110.01 0.01U
Endosulfan II DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A33213-65-9 0.110.05 0.05U
4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U
4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U
Endrin aldehyde DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A7421-93-4 0.110.04 0.04U
Endosulfan sulfate DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1031-07-8 0.110.04 0.04U
Methoxychlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-43-5 0.110.1 0.1U
Endrin Ketone DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A53494-70-5 0.110.03 0.03U
Total Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081ANA 0.111.7 0.1
Toxaphene DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A8001-35-2 0.110.1 0.1U
% Recovery % Recovery LimitsQ
Surrogate: Decachlorobiphenyl 146 %2051-24-3 Limit 41-170
Surrogate: Tetrachloro-m-xylene 112 %877-09-8 Limit 40-175
Page 5 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DU1-11202014Description:
Received:
Sampled:Lab ID: 0013068-02 11/20/14 15:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Bolstar, (Sulprofos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C 0.0075410.00251 0.00251JEE, U
Crotoxphos (Ciodrin) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C 0.0018110.000060 0.000060JEE, U
Dichlofenthion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C 0.0068910.00230 0.00230JEE, U
Aspon SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C3244-90-4 0.0073110.00244 0.00244JEE, U
Azinphos, Methyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C86-50-0 0.0105010.00350 0.00350JEE, U
Azinphos, Ethyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C2642-71-9 0.0087110.00290 0.00290JEE, U
Carbophenothion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C786-19-6 0.0097810.00326 0.00326JEE, U
Chlorpyrifos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C2921-88-2 0.0043010.00143 0.00143JEE, U
Chlorpyrifos Methyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C5598-13-0 0.0063910.00213 0.00213JEE, U
Coumaphos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C56-72-4 0.0192010.00641 0.00641JEE, U
Demeton O & S SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C8065-48-3 0.0067410.00224 0.00224JEE, U
Diazinon SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C333-41-5 0.0045310.00144 0.00144JEE, U
Dichlorvos (DDVP) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C62-73-7 0.0055810.00186 0.00186JEE, U
Dicrotophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C141-66-2 0.0085610.00319 0.00319JEE, U
Dimethoate SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C60-51-5 0.0024510.000816 0.000816JEE, U
Dioxathion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C78-34-2 0.0070010.00233 0.00233JEE, U
Disulfoton SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C298-04-4 0.0178010.00592 0.00592JEE, U
EPN SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C2104-64-5 0.0079610.00266 0.00266JEE, U
Ethion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C563-12-2 0.0107010.00355 0.00355JEE, U
Ethoprop SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C13194-48-4 0.0063810.00213 0.00213JEE, U
Famphur SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C52-85-7 0.0076510.00255 0.00255JEE, U
Fenitrothion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C122-14-5 0.0044910.00150 0.00150JEE, U
Fensulfothion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C115-90-2 0.0017710.00059 0.00059JEE, U
Fenthion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C55-38-9 0.0068010.00227 0.00227JEE, U
Fonophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C944-22-9 0.0035310.00118 0.00118JEE, U
Leptophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C21609-90-5 0.0124010.00413 0.00413JEE, U
Malathion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C121-75-5 0.0059410.00198 0.00198JEE, U
Merphos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C150-50-5 0.0227010.00758 0.00758JEE, U
Mevinphos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C7786-34-7 0.0027510.000916 0.000916JEE, U
Monocrotophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C6923-22-4 0.00095310.000318 0.000318JEE, U
Naled SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C300-76-5 0.0023110.000769 0.000769JEE, U
Parathion-ethyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C56-38-2 0.0290010.00967 0.00967JEE, U
Parathion-methyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C298-00-0 0.0056710.00189 0.00189JEE, U
Phorate SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C298-02-2 0.0081010.00270 0.00270JEE, U
Phosphamidon SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C13171-21-6 0.0014610.000487 0.000487JEE, U
Ronnel SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C299-84-3 0.0074710.00249 0.00249JEE, U
Page 6 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DU1-11202014Description:
Received:
Sampled:Lab ID: 0013068-02 11/20/14 15:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Stirophos (Tetrachlorvinphos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C22248-79-9 0.0036710.00122 0.00122JEE, U
Sulfotepp SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C3689-24-5 0.0081910.00273 0.00273JEE, U
Terbufos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C13071-79-9 0.0069010.00230 0.00230JEE, U
Thionazin (Zinophos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C297-97-2 0.0066210.00220 0.00220JEE, U
Tokuthion (Prothiofos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C34643-46-4 0.0025318.40E-5 8.40E-5JEE, U
Trichloronate SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C327-98-0 0.0092010.00307 0.00307JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Nitrobenzene-d5 %NA Limit 47-131JEE, U
Surrogate: 2-Fluorobiphenyl %321-60-8 Limit 51-134JEE, U
Surrogate: p-Terphenyl-d14 %NA Limit 59-135JEE, U
Metals by EPA 6000/7000 Series Methods
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Arsenic PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7440-38-2 0.20019.04 0.003
Lead PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7439-92-1 0.200145.5 0.007
Percent Dry Weight
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
% Solids AT% 11/23/14 11/26/14CalculationNA 1.01100 1.0
Page 7 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DUP1-11202014Description:
Received:
Sampled:Lab ID: 0013068-03 11/20/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8081A
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
alpha-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-84-6 0.110.03 0.03U
gamma-BHC (Lindane) DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A58-89-9 0.110.04 0.04U
Heptachlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A76-44-8 0.110.04 0.04U
Aldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A309-00-2 0.110.03 0.03U
beta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-85-7 0.110.05 0.05U
delta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-86-8 0.110.04 0.04U
Heptachlor epoxide DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1024-57-3 0.110.04 0.04U
Endosulfan I DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A959-98-8 0.110.03 0.03U
gamma-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5566-34-7 0.110.7 0.04
alpha-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5103-71-9 0.110.4 0.04
4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.113.2 0.04
Dieldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A60-57-1 0.110.1 0.04
Endrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-20-8 0.110.01 0.01U
Endosulfan II DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A33213-65-9 0.110.05 0.05U
4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U
4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U
Endrin aldehyde DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A7421-93-4 0.110.04 0.04U
Endosulfan sulfate DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1031-07-8 0.110.04 0.04U
Methoxychlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-43-5 0.110.1 0.1U
Endrin Ketone DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A53494-70-5 0.110.03 0.03U
Total Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081ANA 0.111.2 0.1
Toxaphene DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A8001-35-2 0.110.1 0.1U
% Recovery % Recovery LimitsQ
Surrogate: Decachlorobiphenyl 163 %2051-24-3 Limit 41-170
Surrogate: Tetrachloro-m-xylene 145 %877-09-8 Limit 40-175
Page 8 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DUP1-11202014Description:
Received:
Sampled:Lab ID: 0013068-03 11/20/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Bolstar, (Sulprofos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C 0.0075410.00251 0.00251JEE, U
Crotoxphos (Ciodrin) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C 0.0018110.000602 0.000602JEE, U
Dichlofenthion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C 0.0068910.00230 0.00230JEE, U
Aspon SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C3244-90-4 0.0073110.00244 0.00244JEE, U
Azinphos, Methyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C86-50-0 0.0105010.00350 0.00350JEE, U
Azinphos, Ethyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C2642-71-9 0.0087110.00290 0.00290JEE, U
Carbophenothion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C786-19-6 0.0097810.00326 0.00326JEE, U
Chlorpyrifos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C2921-88-2 0.0043010.00143 0.00143JEE, U
Chlorpyrifos Methyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C5598-13-0 0.0063910.00213 0.00213JEE, U
Coumaphos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C56-72-4 0.0192010.00641 0.00641JEE, U
Demeton O & S SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C8065-48-3 0.0159010.00530 0.00530JEE, U
Diazinon SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C333-41-5 0.0043310.00144 0.00144JEE, U
Dichlorvos (DDVP) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C62-73-7 0.0055810.00186 0.00186JEE, U
Dicrotophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C141-66-2 0.00095610.000319 0.000319JEE, U
Dimethoate SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C60-51-5 0.0024510.000816 0.000816JEE, U
Dioxathion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C78-34-2 0.0070010.00233 0.00233JEE, U
Disulfoton SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C298-04-4 0.0178010.00592 0.00592JEE, U
EPN SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C2104-64-5 0.0079610.00266 0.00266JEE, U
Ethion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C563-12-2 0.0072510.00242 0.00242JEE, U
Ethoprop SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C13194-48-4 0.0063810.00213 0.00213JEE, U
Famphur SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C52-85-7 0.0076510.00255 0.00255JEE, U
Fenitrothion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C122-14-5 0.0044910.00150 0.00150JEE, U
Fensulfothion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C115-90-2 0.0017710.00059 0.00059JEE, U
Fenthion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C55-38-9 0.0068010.00227 0.00227JEE, U
Fonophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C944-22-9 0.0035310.00118 0.00118JEE, U
Leptophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C21609-90-5 0.0124010.00413 0.00413JEE, U
Malathion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C121-75-5 0.0059410.00198 0.00198JEE, U
Merphos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C150-50-5 0.0227010.00758 0.00758JEE, U
Mevinphos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C7786-34-7 0.0027510.000916 0.000916JEE, U
Monocrotophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C6923-22-4 0.00095310.000318 0.000318JEE, U
Naled SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C300-76-5 0.0023110.000769 0.000769JEE, U
Parathion-ethyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C56-38-2 0.0290010.00967 0.00967JEE, U
Parathion-methyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C298-00-0 0.0056710.00189 0.00189JEE, U
Phorate SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C298-02-2 0.0081010.00270 0.00270JEE, U
Phosphamidon SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C13171-21-6 0.0014610.000487 0.000487JEE, U
Ronnel SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C299-84-3 0.0074710.00249 0.00249JEE, U
Page 9 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DUP1-11202014Description:
Received:
Sampled:Lab ID: 0013068-03 11/20/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Stirophos (Tetrachlorvinphos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C22248-79-9 0.0036710.00122 0.00122JEE, U
Sulfotepp SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C3689-24-5 0.0081910.00273 0.00273JEE, U
Terbufos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C13071-79-9 0.0069010.00230 0.00230JEE, U
Thionazin (Zinophos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C297-97-2 0.0066210.00220 0.00220JEE, U
Tokuthion (Prothiofos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C34643-46-4 0.00025318.40E-5 8.40E-5JEE, U
Trichloronate SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C327-98-0 0.0092010.00307 0.00307JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Nitrobenzene-d5 %NA Limit 47-131JEE, U
Surrogate: 2-Fluorobiphenyl %321-60-8 Limit 51-134JEE, U
Surrogate: p-Terphenyl-d14 %NA Limit 59-135JEE, U
Metals by EPA 6000/7000 Series Methods
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Arsenic PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7440-38-2 0.20019.13 0.003
Lead PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7439-92-1 0.2001311 0.007E
Percent Dry Weight
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
% Solids AT% 11/23/14 11/26/14CalculationNA 1.01100 1.0
Page 10 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DUP2-11202014Description:
Received:
Sampled:Lab ID: 0013068-04 11/20/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8081A
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
alpha-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-84-6 0.110.03 0.03U
gamma-BHC (Lindane) DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A58-89-9 0.110.04 0.04U
Heptachlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A76-44-8 0.110.04 0.04U
Aldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A309-00-2 0.110.03 0.03U
beta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-85-7 0.110.05 0.05U
delta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-86-8 0.110.04 0.04U
Heptachlor epoxide DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1024-57-3 0.110.04 0.04U
Endosulfan I DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A959-98-8 0.110.03 0.03U
gamma-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5566-34-7 0.110.3 0.04
alpha-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5103-71-9 0.110.3 0.04
4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.112.6 0.04
Dieldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A60-57-1 0.110.04 0.04U
Endrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-20-8 0.110.01 0.01U
Endosulfan II DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A33213-65-9 0.110.05 0.05U
4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U
4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U
Endrin aldehyde DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A7421-93-4 0.110.04 0.04U
Endosulfan sulfate DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1031-07-8 0.110.04 0.04U
Methoxychlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-43-5 0.110.1 0.1U
Endrin Ketone DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A53494-70-5 0.110.03 0.03U
Total Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081ANA 0.110.6 0.1
Toxaphene DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A8001-35-2 0.110.1 0.1U
% Recovery % Recovery LimitsQ
Surrogate: Decachlorobiphenyl 127 %2051-24-3 Limit 41-170
Surrogate: Tetrachloro-m-xylene 111 %877-09-8 Limit 40-175
Page 11 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DUP2-11202014Description:
Received:
Sampled:Lab ID: 0013068-04 11/20/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Bolstar, (Sulprofos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C 0.0075410.00251 0.00251JEE, U
Crotoxphos (Ciodrin) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C 0.0018110.000602 0.000602JEE, U
Dichlofenthion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C 0.0068910.00230 0.00230JEE, U
Aspon SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C3244-90-4 0.0073110.00244 0.00244JEE, U
Azinphos, Methyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C86-50-0 0.0105010.00350 0.00350JEE, U
Azinphos, Ethyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C2642-71-9 0.0087110.00290 0.00290JEE, U
Carbophenothion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C786-19-6 0.0097810.00326 0.00326JEE, U
Chlorpyrifos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C2921-88-2 0.0043010.00143 0.00143JEE, U
Chlorpyrifos Methyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C5598-13-0 0.0063910.00213 0.00213JEE, U
Coumaphos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C56-72-4 0.0192010.00641 0.00641JEE, U
Demeton O & S SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C8065-48-3 0.0159010.00530 0.00530JEE, U
Diazinon SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C333-41-5 0.0043310.00144 0.00144JEE, U
Dichlorvos (DDVP) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C62-73-7 0.0055810.00186 0.00186JEE, U
Dicrotophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C141-66-2 0.00095610.000319 0.000319JEE, U
Dimethoate SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C60-51-5 10.0010.000816 0.000816JEE, U
Dioxathion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C78-34-2 0.0070010.00233 0.00233JEE, U
Disulfoton SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C298-04-4 0.0178010.00592 0.00592JEE, U
EPN SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C2104-64-5 0.0079610.00266 0.00266JEE, U
Ethion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C563-12-2 0.0072510.00242 0.00242JEE, U
Ethoprop SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C13194-48-4 0.0063810.00213 0.00213JEE, U
Famphur SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C52-85-7 0.0076510.00255 0.00255JEE, U
Fenitrothion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C122-14-5 0.0044910.00150 0.00150JEE, U
Fensulfothion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C115-90-2 0.0017710.00059 0.00059JEE, U
Fenthion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C55-38-9 0.0068010.00227 0.00227JEE, U
Fonophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C944-22-9 0.0035310.00118 0.00118JEE, U
Leptophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C21609-90-5 0.0124010.00413 0.00413JEE, U
Malathion SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C121-75-5 0.0059410.00198 0.00198JEE, U
Merphos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C150-50-5 0.0227010.00758 0.00758JEE, U
Mevinphos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C7786-34-7 0.0027510.000916 0.000916JEE, U
Monocrotophos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C6923-22-4 0.00095310.000318 0.000318JEE, U
Naled SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C300-76-5 0.0023110.000769 0.000769JEE, U
Parathion-ethyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C56-38-2 0.0290010.00967 0.00967JEE, U
Parathion-methyl SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C298-00-0 0.0056710.00189 0.00189JEE, U
Phorate SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C298-02-2 0.0081010.00270 0.00270JEE, U
Phosphamidon SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C13171-21-6 0.0014610.000487 0.000487JEE, U
Ronnel SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C299-84-3 0.0074710.00249 0.00249JEE, U
Page 12 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
LOG #:
PROJECT:
PROJECT #:
REPORTED:
COC#:
ATTN:
FAX: PHONE:
E Sciences
224 SE 9th Street
(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center
7-0002-023
21623
12/4/2014 9:38:04AM
Maria Paituvi
Ft Lauderdale, FL 33316
CERTIFICATE OF ANALYSIS
0013068
DUP2-11202014Description:
Received:
Sampled:Lab ID: 0013068-04 11/20/14 00:00
11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen
EPA Method 8141 List in Soil
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Stirophos (Tetrachlorvinphos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C22248-79-9 0.0036710.00122 0.00122JEE, U
Sulfotepp SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C3689-24-5 0.0081910.00273 0.00273JEE, U
Terbufos SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C13071-79-9 0.0039010.00230 0.00230JEE, U
Thionazin (Zinophos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C297-97-2 0.0066210.00220 0.00220JEE, U
Tokuthion (Prothiofos) SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C34643-46-4 0.00025318.40E-5 8.40E-5JEE, U
Trichloronate SLmg/kg 11/28/14 12/01/14EPA 3545 / 8270C327-98-0 0.0092010.00300 0.00300JEE, U
% Recovery % Recovery LimitsQ
Surrogate: Nitrobenzene-d5 %NA Limit 47-131JEE, U
Surrogate: 2-Fluorobiphenyl %321-60-8 Limit 51-134JEE, U
Surrogate: p-Terphenyl-d14 %NA Limit 59-135JEE, U
Metals by EPA 6000/7000 Series Methods
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
Arsenic PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7440-38-2 0.200110.4 0.003
Lead PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7439-92-1 0.200142.2 0.007
Percent Dry Weight
Parameter UnitsResults MDLMethod AnalystDateCAS # DF
Extraction Analysis
DatePQLQ
% Solids AT% 11/23/14 11/26/14CalculationNA 1.01100 1.0
Page 13 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
Notes and Definitions
Analyte included in the analysis, but not detectedU
Analysis performed by Florida Environmental Cert#E86006JEE
The concentration indicated for this analyte is an estimated value above the calibration range of the instrument.. This
value is considered an estimate (CLP E-flag).
E
Page 14 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702
EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083
DRAFT
DRAFT
DRAFT
02/02/15
Technical Report for
E Sciences, Inc
Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
7-0002-025
Accutest Job Number: FA21662
Sampling Date: 01/24/15
Report to:
E Sciences, Inc224 SE 9th StFt Lauderdale, FL [email protected]
ATTN: Maria Paituvi
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Andrea Colby 407-425-6700
Norm FarmerTechnical Director
Southeast
02/02/15
e-Hardcopy 2.0Automated Report
51
Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.
1 of 51FA21662
DRAFT
Table of Contents-1-
Sections:
Section 1: Sample Summary ................................................................................................... 3Section 2: Summary of Hits .................................................................................................... 4Section 3: Sample Results ........................................................................................................ 5
3.1: FA21662-1: MW1-01242015 ....................................................................................... 63.2: FA21662-2: MW2-01242015 ....................................................................................... 93.3: FA21662-3: MW3-01242015 ....................................................................................... 123.4: FA21662-3F: MW3-01242015 ..................................................................................... 153.5: FA21662-4: MW4-01242015 ....................................................................................... 16
Section 4: Misc. Forms ............................................................................................................ 194.1: Chain of Custody ........................................................................................................... 20
Section 5: GC Semi-volatiles - QC Data Summaries ............................................................ 255.1: Method Blank Summary ................................................................................................ 265.2: Blank Spike Summary ................................................................................................... 275.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 29
Section 6: Metals Analysis - QC Data Summaries ................................................................ 306.1: Prep QC MP28493: Hg .................................................................................................. 316.2: Prep QC MP28495: Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,Tl,Zn ........................................ 366.3: Prep QC MP28507: As .................................................................................................. 42
Section 7: General Chemistry - QC Data Summaries .......................................................... 487.1: Method Blank and Spike Results Summary .................................................................. 497.2: Matrix Spike Results Summary ..................................................................................... 507.3: Matrix Spike Duplicate Results Summary .................................................................... 51
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Sample Summary
E Sciences, IncJob No: FA21662
Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FLProject No: 7-0002-025
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
FA21662-1 01/24/15 10:00 TV 01/26/15 AQ Ground Water MW1-01242015
FA21662-2 01/24/15 10:35 TV 01/26/15 AQ Ground Water MW2-01242015
FA21662-3 01/24/15 11:10 TV 01/26/15 AQ Ground Water MW3-01242015
FA21662-3F 01/24/15 11:10 TV 01/26/15 AQ Groundwater Filtered MW3-01242015
FA21662-4 01/24/15 11:45 TV 01/26/15 AQ Ground Water MW4-01242015
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Summary of Hits Page 1 of 1 Job Number: FA21662Account: E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FLCollected: 01/24/15
Lab Sample ID Client Sample ID Result/Analyte Qual PQL MDL Units Method
FA21662-1 MW1-01242015
Chromium 1.5 I 10 1.0 ug/l SW846 6010CZinc 8.1 I 20 4.4 ug/l SW846 6010CNitrogen, Ammonia 1.6 0.10 0.030 mg/l EPA 350.1
FA21662-2 MW2-01242015
Antimony 1.1 I 6.0 1.0 ug/l SW846 6010CChromium 1.4 I 10 1.0 ug/l SW846 6010CZinc 6.4 I 20 4.4 ug/l SW846 6010CNitrogen, Ammonia 1.4 0.10 0.030 mg/l EPA 350.1
FA21662-3 MW3-01242015
Antimony 2.2 I 6.0 1.0 ug/l SW846 6010CArsenic 21.3 10 1.3 ug/l SW846 6010CSilver 0.80 I 10 0.70 ug/l SW846 6010CZinc 5.9 I 20 4.4 ug/l SW846 6010CNitrogen, Ammonia 1.0 0.10 0.030 mg/l EPA 350.1
FA21662-3F MW3-01242015
No hits reported in this sample.
FA21662-4 MW4-01242015
Antimony 1.5 I 6.0 1.0 ug/l SW846 6010CArsenic 4.1 I 10 1.3 ug/l SW846 6010CChromium 1.8 I 10 1.0 ug/l SW846 6010CNickel 1.6 I 40 0.40 ug/l SW846 6010CNitrogen, Ammonia 0.22 0.10 0.030 mg/l EPA 350.1
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Sample Results
Report of Analysis
Southeast
Section 3
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Report of Analysis Page 1 of 1
Client Sample ID: MW1-01242015 Lab Sample ID: FA21662-1 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 TT370659.D 1 01/29/15 EM 01/27/15 OP54722 GTT1590Run #2
Initial Volume Final VolumeRun #1 250 ml 5.0 mlRun #2
Pesticide PPL List
CAS No. Compound Result PQL MDL Units Q
309-00-2 Aldrin 0.0064 U 0.040 0.0064 ug/l319-84-6 alpha-BHC 0.0040 U 0.040 0.0040 ug/l319-85-7 beta-BHC 0.011 U 0.040 0.011 ug/l319-86-8 delta-BHC 0.0079 U 0.040 0.0079 ug/l58-89-9 gamma-BHC (Lindane) 0.0042 U 0.040 0.0042 ug/l12789-03-6 Chlordane 0.17 U 0.40 0.17 ug/l60-57-1 Dieldrin 0.0067 U 0.040 0.0067 ug/l72-54-8 4,4'-DDD 0.010 U 0.080 0.010 ug/l72-55-9 4,4'-DDE 0.015 U 0.080 0.015 ug/l50-29-3 4,4'-DDT 0.010 U 0.080 0.010 ug/l72-20-8 Endrin 0.0070 U 0.080 0.0070 ug/l1031-07-8 Endosulfan sulfate 0.0066 U 0.080 0.0066 ug/l7421-93-4 Endrin aldehyde 0.0065 U 0.080 0.0065 ug/l959-98-8 Endosulfan-I 0.0066 U 0.040 0.0066 ug/l33213-65-9 Endosulfan-II 0.0080 U 0.040 0.0080 ug/l76-44-8 Heptachlor 0.0062 U 0.040 0.0062 ug/l1024-57-3 Heptachlor epoxide 0.0072 U 0.040 0.0072 ug/l72-43-5 Methoxychlor 0.010 U 0.080 0.010 ug/l8001-35-2 Toxaphene 1.2 U 2.0 1.2 ug/l
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 87% 42-127%2051-24-3 Decachlorobiphenyl 76% 27-127%
U = Not detected MDL = Method Detection Limit I = Result >= MDL but < PQL J = Estimated valuePQL = Practical Quantitation Limit V = Indicates analyte found in associated method blankL = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID: MW1-01242015 Lab Sample ID: FA21662-1 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Total Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 1.0 U 6.0 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Arsenic 1.3 U 10 1.3 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Beryllium 0.20 U 4.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Cadmium 0.20 U 5.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Chromium 1.5 I 10 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Copper 1.0 U 25 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Lead 1.1 U 5.0 1.1 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Mercury 0.030 U 0.50 0.030 ug/l 1 01/27/15 01/27/15 JL SW846 7470A 1 SW846 7470A 3
Nickel 0.40 U 40 0.40 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Selenium 2.9 U 10 2.9 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Silver 0.70 U 10 0.70 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Thallium 1.4 U 10 1.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Zinc 8.1 I 20 4.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
(1) Instrument QC Batch: MA12180(2) Instrument QC Batch: MA12182(3) Prep QC Batch: MP28493(4) Prep QC Batch: MP28495
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Report of Analysis Page 1 of 1
Client Sample ID: MW1-01242015 Lab Sample ID: FA21662-1 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
General Chemistry
Analyte Result PQL MDL Units DF Analyzed By Method
Nitrogen, Ammonia 1.6 0.10 0.030 mg/l 1 01/28/15 11:21 DM EPA 350.1
Nitrogen, Nitrate a 2.5 U 5.0 2.5 mg/l 50 01/26/15 09:51 JA EPA 300/SW846 9056A
Nitrogen, Nitrite a 2.5 U 5.0 2.5 mg/l 50 01/26/15 09:51 JA EPA 300/SW846 9056A
(a) Dilution required due to matrix interference.
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Report of Analysis Page 1 of 1
Client Sample ID: MW2-01242015 Lab Sample ID: FA21662-2 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 TT370660.D 1 01/29/15 EM 01/27/15 OP54722 GTT1590Run #2
Initial Volume Final VolumeRun #1 260 ml 5.0 mlRun #2
Pesticide PPL List
CAS No. Compound Result PQL MDL Units Q
309-00-2 Aldrin 0.0062 U 0.038 0.0062 ug/l319-84-6 alpha-BHC 0.0038 U 0.038 0.0038 ug/l319-85-7 beta-BHC 0.010 U 0.038 0.010 ug/l319-86-8 delta-BHC 0.0076 U 0.038 0.0076 ug/l58-89-9 gamma-BHC (Lindane) 0.0040 U 0.038 0.0040 ug/l12789-03-6 Chlordane 0.16 U 0.38 0.16 ug/l60-57-1 Dieldrin 0.0064 U 0.038 0.0064 ug/l72-54-8 4,4'-DDD 0.0096 U 0.077 0.0096 ug/l72-55-9 4,4'-DDE 0.014 U 0.077 0.014 ug/l50-29-3 4,4'-DDT 0.0096 U 0.077 0.0096 ug/l72-20-8 Endrin 0.0067 U 0.077 0.0067 ug/l1031-07-8 Endosulfan sulfate 0.0064 U 0.077 0.0064 ug/l7421-93-4 Endrin aldehyde 0.0063 U 0.077 0.0063 ug/l959-98-8 Endosulfan-I 0.0063 U 0.038 0.0063 ug/l33213-65-9 Endosulfan-II 0.0077 U 0.038 0.0077 ug/l76-44-8 Heptachlor 0.0060 U 0.038 0.0060 ug/l1024-57-3 Heptachlor epoxide 0.0069 U 0.038 0.0069 ug/l72-43-5 Methoxychlor 0.0096 U 0.077 0.0096 ug/l8001-35-2 Toxaphene 1.1 U 1.9 1.1 ug/l
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 86% 42-127%2051-24-3 Decachlorobiphenyl 78% 27-127%
U = Not detected MDL = Method Detection Limit I = Result >= MDL but < PQL J = Estimated valuePQL = Practical Quantitation Limit V = Indicates analyte found in associated method blankL = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID: MW2-01242015 Lab Sample ID: FA21662-2 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Total Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 1.1 I 6.0 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Arsenic 1.3 U 10 1.3 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Beryllium 0.20 U 4.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Cadmium 0.20 U 5.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Chromium 1.4 I 10 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Copper 1.0 U 25 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Lead 1.1 U 5.0 1.1 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Mercury 0.030 U 0.50 0.030 ug/l 1 01/27/15 01/27/15 JL SW846 7470A 1 SW846 7470A 3
Nickel 0.40 U 40 0.40 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Selenium 2.9 U 10 2.9 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Silver 0.70 U 10 0.70 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Thallium 1.4 U 10 1.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Zinc 6.4 I 20 4.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
(1) Instrument QC Batch: MA12180(2) Instrument QC Batch: MA12182(3) Prep QC Batch: MP28493(4) Prep QC Batch: MP28495
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Report of Analysis Page 1 of 1
Client Sample ID: MW2-01242015 Lab Sample ID: FA21662-2 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
General Chemistry
Analyte Result PQL MDL Units DF Analyzed By Method
Nitrogen, Ammonia 1.4 0.10 0.030 mg/l 1 01/28/15 11:22 DM EPA 350.1
Nitrogen, Nitrate a 5.0 U 10 5.0 mg/l 100 01/26/15 10:08 JA EPA 300/SW846 9056A
Nitrogen, Nitrite a 5.0 U 10 5.0 mg/l 100 01/26/15 10:08 JA EPA 300/SW846 9056A
(a) Dilution required due to matrix interference.
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Report of Analysis Page 1 of 1
Client Sample ID: MW3-01242015 Lab Sample ID: FA21662-3 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 TT370636.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589Run #2
Initial Volume Final VolumeRun #1 260 ml 5.0 mlRun #2
Pesticide PPL List
CAS No. Compound Result PQL MDL Units Q
309-00-2 Aldrin 0.0062 U 0.038 0.0062 ug/l319-84-6 alpha-BHC 0.0038 U 0.038 0.0038 ug/l319-85-7 beta-BHC 0.010 U 0.038 0.010 ug/l319-86-8 delta-BHC 0.0076 U 0.038 0.0076 ug/l58-89-9 gamma-BHC (Lindane) 0.0040 U 0.038 0.0040 ug/l12789-03-6 Chlordane 0.16 U 0.38 0.16 ug/l60-57-1 Dieldrin 0.0064 U 0.038 0.0064 ug/l72-54-8 4,4'-DDD 0.0096 U 0.077 0.0096 ug/l72-55-9 4,4'-DDE 0.014 U 0.077 0.014 ug/l50-29-3 4,4'-DDT 0.0096 U 0.077 0.0096 ug/l72-20-8 Endrin 0.0067 U 0.077 0.0067 ug/l1031-07-8 Endosulfan sulfate 0.0064 U 0.077 0.0064 ug/l7421-93-4 Endrin aldehyde 0.0063 U 0.077 0.0063 ug/l959-98-8 Endosulfan-I 0.0063 U 0.038 0.0063 ug/l33213-65-9 Endosulfan-II 0.0077 U 0.038 0.0077 ug/l76-44-8 Heptachlor 0.0060 U 0.038 0.0060 ug/l1024-57-3 Heptachlor epoxide 0.0069 U 0.038 0.0069 ug/l72-43-5 Methoxychlor 0.0096 U 0.077 0.0096 ug/l8001-35-2 Toxaphene 1.1 U 1.9 1.1 ug/l
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 102% 42-127%2051-24-3 Decachlorobiphenyl 85% 27-127%
U = Not detected MDL = Method Detection Limit I = Result >= MDL but < PQL J = Estimated valuePQL = Practical Quantitation Limit V = Indicates analyte found in associated method blankL = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID: MW3-01242015 Lab Sample ID: FA21662-3 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Total Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 2.2 I 6.0 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Arsenic 21.3 10 1.3 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Beryllium 0.20 U 4.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Cadmium 0.20 U 5.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Chromium 1.0 U 10 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Copper 1.0 U 25 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Lead 1.1 U 5.0 1.1 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Mercury 0.030 U 0.50 0.030 ug/l 1 01/27/15 01/27/15 JL SW846 7470A 1 SW846 7470A 3
Nickel 0.40 U 40 0.40 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Selenium 2.9 U 10 2.9 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Silver 0.80 I 10 0.70 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Thallium 1.4 U 10 1.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Zinc 5.9 I 20 4.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
(1) Instrument QC Batch: MA12180(2) Instrument QC Batch: MA12182(3) Prep QC Batch: MP28493(4) Prep QC Batch: MP28495
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Report of Analysis Page 1 of 1
Client Sample ID: MW3-01242015 Lab Sample ID: FA21662-3 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
General Chemistry
Analyte Result PQL MDL Units DF Analyzed By Method
Nitrogen, Ammonia 1.0 0.10 0.030 mg/l 1 01/28/15 11:23 DM EPA 350.1
Nitrogen, Nitrate a 10 U 20 10 mg/l 200 01/26/15 10:25 JA EPA 300/SW846 9056A
Nitrogen, Nitrite a 10 U 20 10 mg/l 200 01/26/15 10:25 JA EPA 300/SW846 9056A
(a) Dilution required due to matrix interference.
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Report of Analysis Page 1 of 1
Client Sample ID: MW3-01242015 Lab Sample ID: FA21662-3F Date Sampled: 01/24/15 Matrix: AQ - Groundwater Filtered Date Received: 01/26/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Dissolved Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 1.3 U 10 1.3 ug/l 1 01/30/15 01/30/15 LM SW846 6010C 1 SW846 3010A 2
(1) Instrument QC Batch: MA12191(2) Prep QC Batch: MP28507
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Client Sample ID: MW4-01242015 Lab Sample ID: FA21662-4 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 TT370637.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589Run #2
Initial Volume Final VolumeRun #1 260 ml 5.0 mlRun #2
Pesticide PPL List
CAS No. Compound Result PQL MDL Units Q
309-00-2 Aldrin 0.0062 U 0.038 0.0062 ug/l319-84-6 alpha-BHC 0.0038 U 0.038 0.0038 ug/l319-85-7 beta-BHC 0.010 U 0.038 0.010 ug/l319-86-8 delta-BHC 0.0076 U 0.038 0.0076 ug/l58-89-9 gamma-BHC (Lindane) 0.0040 U 0.038 0.0040 ug/l12789-03-6 Chlordane 0.16 U 0.38 0.16 ug/l60-57-1 Dieldrin 0.0064 U 0.038 0.0064 ug/l72-54-8 4,4'-DDD 0.0096 U 0.077 0.0096 ug/l72-55-9 4,4'-DDE 0.014 U 0.077 0.014 ug/l50-29-3 4,4'-DDT 0.0096 U 0.077 0.0096 ug/l72-20-8 Endrin 0.0067 U 0.077 0.0067 ug/l1031-07-8 Endosulfan sulfate 0.0064 U 0.077 0.0064 ug/l7421-93-4 Endrin aldehyde 0.0063 U 0.077 0.0063 ug/l959-98-8 Endosulfan-I 0.0063 U 0.038 0.0063 ug/l33213-65-9 Endosulfan-II 0.0077 U 0.038 0.0077 ug/l76-44-8 Heptachlor 0.0060 U 0.038 0.0060 ug/l1024-57-3 Heptachlor epoxide 0.0069 U 0.038 0.0069 ug/l72-43-5 Methoxychlor 0.0096 U 0.077 0.0096 ug/l8001-35-2 Toxaphene 1.1 U 1.9 1.1 ug/l
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
877-09-8 Tetrachloro-m-xylene 109% 42-127%2051-24-3 Decachlorobiphenyl 94% 27-127%
U = Not detected MDL = Method Detection Limit I = Result >= MDL but < PQL J = Estimated valuePQL = Practical Quantitation Limit V = Indicates analyte found in associated method blankL = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Client Sample ID: MW4-01242015 Lab Sample ID: FA21662-4 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Total Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Antimony 1.5 I 6.0 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Arsenic 4.1 I 10 1.3 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Beryllium 0.20 U 4.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Cadmium 0.20 U 5.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Chromium 1.8 I 10 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Copper 1.0 U 25 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Lead 1.1 U 5.0 1.1 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Mercury 0.030 U 0.50 0.030 ug/l 1 01/27/15 01/27/15 JL SW846 7470A 1 SW846 7470A 3
Nickel 1.6 I 40 0.40 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Selenium 2.9 U 10 2.9 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Silver 0.70 U 10 0.70 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Thallium 1.4 U 10 1.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
Zinc 4.4 U 20 4.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4
(1) Instrument QC Batch: MA12180(2) Instrument QC Batch: MA12182(3) Prep QC Batch: MP28493(4) Prep QC Batch: MP28495
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: MW4-01242015 Lab Sample ID: FA21662-4 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
General Chemistry
Analyte Result PQL MDL Units DF Analyzed By Method
Nitrogen, Ammonia 0.22 0.10 0.030 mg/l 1 01/28/15 11:24 DM EPA 350.1
Nitrogen, Nitrate a 2.5 U 5.0 2.5 mg/l 50 01/26/15 10:42 JA EPA 300/SW846 9056A
Nitrogen, Nitrite a 2.5 U 5.0 2.5 mg/l 50 01/26/15 10:42 JA EPA 300/SW846 9056A
(a) Dilution required due to matrix interference.
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
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DRAFT
FA21662: Chain of CustodyPage 1 of 5
20 of 51FA21662
44.1
DRAFT
FA21662: Chain of CustodyPage 2 of 5
21 of 51FA21662
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FA21662: Chain of CustodyPage 3 of 5
22 of 51FA21662
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Job Change Order: FA21662_1/26/2015
Requested Date: 1/26/2015 Received Date: 1/26/2015
Account Name: E Sciences, Inc Due Date: 1/29/2015
Project Parking Lot & Community Center; 1700 Deliverable: COMMB
CSR: AC TAT (Days): 3
Sample #: Change: Please change TAT to 3 day, due 1/29/15. FA21662-all
Above Changes Per: Maria Paituvi Date: 1/26/2015
To Client: This Change Order is confirmation of the revisions, previously discussed with the Accutest Client Service
Page 1 of 1
FA21662: Chain of CustodyPage 4 of 5
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Job Change Order: FA21662_1/28/2015
Requested Date: 1/28/2015 Received Date: 1/26/2015
Account Name: E Sciences, Inc Due Date: 1/29/2015
Project Parking Lot & Community Center; 1700 Deliverable: COMMB
CSR: AC TAT (Days): 3
Sample #: Change: Please lab filter an unpreserved aliquot and FA21662-3 analyze for dissolved arsenic.
MW3-01242015
Above Changes Per: Maria Paituvi Date: 1/28/2015
To Client: This Change Order is confirmation of the revisions, previously discussed with the Accutest Client Service
Page 1 of 1
FA21662: Chain of CustodyPage 5 of 5
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DRAFT
Accutest Laboratories
GC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries• Blank Spike Summaries• Matrix Spike and Duplicate Summaries
Southeast
Section 5
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Method Blank Summary Page 1 of 1 Job Number: FA21662Account: ESFLFL E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP54722-MB TT370630.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589
The QC reported here applies to the following samples: Method: SW846 8081B
FA21662-1, FA21662-2, FA21662-3, FA21662-4
CAS No. Compound Result RL MDL Units Q
309-00-2 Aldrin ND 0.040 0.0064 ug/l319-84-6 alpha-BHC ND 0.040 0.0040 ug/l319-85-7 beta-BHC ND 0.040 0.011 ug/l319-86-8 delta-BHC ND 0.040 0.0079 ug/l58-89-9 gamma-BHC (Lindane) ND 0.040 0.0042 ug/l12789-03-6 Chlordane ND 0.40 0.17 ug/l60-57-1 Dieldrin ND 0.040 0.0067 ug/l72-54-8 4,4'-DDD ND 0.080 0.010 ug/l72-55-9 4,4'-DDE ND 0.080 0.015 ug/l50-29-3 4,4'-DDT ND 0.080 0.010 ug/l72-20-8 Endrin ND 0.080 0.0070 ug/l1031-07-8 Endosulfan sulfate ND 0.080 0.0066 ug/l7421-93-4 Endrin aldehyde ND 0.080 0.0065 ug/l959-98-8 Endosulfan-I ND 0.040 0.0066 ug/l33213-65-9 Endosulfan-II ND 0.040 0.0080 ug/l76-44-8 Heptachlor ND 0.040 0.0062 ug/l1024-57-3 Heptachlor epoxide ND 0.040 0.0072 ug/l72-43-5 Methoxychlor ND 0.080 0.010 ug/l8001-35-2 Toxaphene ND 2.0 1.2 ug/l
CAS No. Surrogate Recoveries Limits
877-09-8 Tetrachloro-m-xylene 94% 42-127%2051-24-3 Decachlorobiphenyl 90% 27-127%
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Blank Spike Summary Page 1 of 1 Job Number: FA21662Account: ESFLFL E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP54722-BS TT370628.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589
The QC reported here applies to the following samples: Method: SW846 8081B
FA21662-1, FA21662-2, FA21662-3, FA21662-4
Spike BSP BSPCAS No. Compound ug/l ug/l % Limits
309-00-2 Aldrin 1 1.0 100 61-126319-84-6 alpha-BHC 1 1.0 100 66-129319-85-7 beta-BHC 1 1.0 100 66-132319-86-8 delta-BHC 1 1.0 100 41-14258-89-9 gamma-BHC (Lindane) 1 1.1 110 68-13260-57-1 Dieldrin 1 1.1 110 66-13872-54-8 4,4'-DDD 1 1.0 100 63-13872-55-9 4,4'-DDE 1 0.92 92 59-13350-29-3 4,4'-DDT 1 0.96 96 55-14572-20-8 Endrin 1 1.1 110 71-1471031-07-8 Endosulfan sulfate 1 0.97 97 64-1287421-93-4 Endrin aldehyde 1 0.82 82 60-130959-98-8 Endosulfan-I 1 1.1 110 66-13333213-65-9 Endosulfan-II 1 0.93 93 65-13376-44-8 Heptachlor 1 0.98 98 63-1301024-57-3 Heptachlor epoxide 1 1.1 110 67-12972-43-5 Methoxychlor 1 0.87 87 60-136
CAS No. Surrogate Recoveries BSP Limits
877-09-8 Tetrachloro-m-xylene 86% 42-127%2051-24-3 Decachlorobiphenyl 80% 27-127%
* = Outside of Control Limits.
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Blank Spike Summary Page 1 of 1 Job Number: FA21662Account: ESFLFL E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP54722-BS2 TT370629.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589
The QC reported here applies to the following samples: Method: SW846 8081B
FA21662-1, FA21662-2, FA21662-3, FA21662-4
Spike BSP BSPCAS No. Compound ug/l ug/l % Limits
12789-03-6 Chlordane 5 6.8 136 62-1418001-35-2 Toxaphene 10 14.9 149 57-151
CAS No. Surrogate Recoveries BSP Limits
877-09-8 Tetrachloro-m-xylene 92% 42-127%2051-24-3 Decachlorobiphenyl 81% 27-127%
* = Outside of Control Limits.
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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: FA21662Account: ESFLFL E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP54722-MS TT370640.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589OP54722-MSD TT370641.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589FA21662-4 TT370637.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589
The QC reported here applies to the following samples: Method: SW846 8081B
FA21662-1, FA21662-2, FA21662-3, FA21662-4
FA21662-4 Spike MS MS Spike MSD MSD LimitsCAS No. Compound ug/l Q ug/l ug/l % ug/l ug/l % RPD Rec/RPD
309-00-2 Aldrin 0.038 U 1.92 2.4 125 1.92 2.0 104 18 61-126/21319-84-6 alpha-BHC 0.038 U 1.92 2.2 114 1.92 1.9 99 15 66-129/23319-85-7 beta-BHC 0.038 U 1.92 2.3 120 1.92 1.9 99 19 66-132/23319-86-8 delta-BHC 0.038 U 1.92 2.3 120 1.92 2.0 104 14 41-142/2758-89-9 gamma-BHC (Lindane) 0.038 U 1.92 2.3 120 1.92 2.0 104 14 68-132/2260-57-1 Dieldrin 0.038 U 1.92 2.5 130 1.92 2.2 114 13 66-138/2272-54-8 4,4'-DDD 0.077 U 1.92 2.4 125 1.92 2.1 109 13 63-138/2472-55-9 4,4'-DDE 0.077 U 1.92 2.0 104 1.92 1.8 94 11 59-133/2350-29-3 4,4'-DDT 0.077 U 1.92 2.1 109 1.92 1.9 99 10 55-145/2772-20-8 Endrin 0.077 U 1.92 2.5 130 1.92 2.3 120 8 71-147/231031-07-8 Endosulfan sulfate 0.077 U 1.92 2.2 114 1.92 2.0 104 10 64-128/267421-93-4 Endrin aldehyde 0.077 U 1.92 1.8 94 1.92 1.7 88 6 60-130/22959-98-8 Endosulfan-I 0.038 U 1.92 2.5 130 1.92 2.2 114 13 66-133/2133213-65-9 Endosulfan-II 0.038 U 1.92 2.1 109 1.92 1.9 99 10 65-133/2276-44-8 Heptachlor 0.038 U 1.92 2.3 120 1.92 1.9 99 19 63-130/231024-57-3 Heptachlor epoxide 0.038 U 1.92 2.5 130* 1.92 2.1 109 17 67-129/2372-43-5 Methoxychlor 0.077 U 1.92 1.8 94 1.92 1.7 88 6 60-136/25
CAS No. Surrogate Recoveries MS MSD FA21662-4 Limits
877-09-8 Tetrachloro-m-xylene 91% 80% 109% 42-127%2051-24-3 Decachlorobiphenyl 85% 81% 94% 27-127%
* = Outside of Control Limits.
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Accutest Laboratories
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries• Matrix Spike and Duplicate Summaries• Blank Spike and Lab Control Sample Summaries• Serial Dilution Summaries
Southeast
Section 6
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BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28493 Methods: SW846 7470A Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15
MB Metal RL IDL MDL raw final
Mercury 0.50 .03 .03 -0.0074 <0.50
Associated samples MP28493: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
31 of 51FA21662
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DRAFT
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28493 Methods: SW846 7470A Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15 01/27/15
FA21662-1 QC FA21662-1 Spikelot QC Metal Original DUP RPD Limits Original MS HGFLWS1 % Rec Limits
Mercury 0.0 0.0 NC 0-20 0.0 3.1 3 103.3 80-120
Associated samples MP28493: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
32 of 51FA21662
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DRAFT
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28493 Methods: SW846 7470A Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15
FA21662-1 Spikelot MSD QC Metal Original MSD HGFLWS1 % Rec RPD Limit
Mercury 0.0 3.1 3 103.3 0.0 20
Associated samples MP28493: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
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DRAFT
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28493 Methods: SW846 7470A Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15
BSP Spikelot QC Metal Result HGFLWS1 % Rec Limits
Mercury 3.1 3 103.3 80-120
Associated samples MP28493: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
34 of 51FA21662
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DRAFT
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28493 Methods: SW846 7470A Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15
FA21662-1 QC Metal Original SDL 1:5 %DIF Limits
Mercury 0.00 0.00 NC 0-10
Associated samples MP28493: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
35 of 51FA21662
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DRAFT
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28495 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15
MB Metal RL IDL MDL raw final
Aluminum 200 15 14
Antimony 6.0 2 1 0.30 <6.0
Arsenic 10 2 1.3 -0.90 <10
Barium 200 1 1
Beryllium 4.0 .5 .2 -0.10 <4.0
Cadmium 5.0 .5 .2 -0.30 <5.0
Calcium 1000 50 50
Chromium 10 1 1 0.20 <10
Cobalt 50 .5 .2
Copper 25 1 1 -0.40 <25
Iron 300 17 17
Lead 5.0 1.1 1.1 0.20 <5.0
Magnesium 5000 50 35
Manganese 15 .5 1
Molybdenum 50 .5 .3
Nickel 40 .5 .4 -0.20 <40
Potassium 10000 200 200
Selenium 10 2.3 2.9 -0.30 <10
Silver 10 .65 .7 -0.20 <10
Sodium 10000 500 500
Strontium 10 .4 .5
Thallium 10 1.5 1.4 -1.2 <10
Tin 50 .7 1
Titanium 10 .9 1
Vanadium 50 .5 .6
Zinc 20 3 4.4 0.0 <20
Associated samples MP28495: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
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DRAFT
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28495 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15 01/27/15
FA21662-4 QC FA21662-4 Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony 0.0 2.9 200.0(a) 0-20 0.0 549 500 109.8 80-120
Arsenic 4.1 2.5 48.5 (a) 0-20 4.1 2260 2000 112.8 80-120
Barium
Beryllium 0.0 0.0 NC 0-20 0.0 53.2 50 106.4 80-120
Cadmium 0.0 0.0 NC 0-20 0.0 49.7 50 99.4 80-120
Calcium
Chromium 1.8 0.0 200.0(a) 0-20 1.8 213 200 105.6 80-120
Cobalt
Copper 0.0 0.0 NC 0-20 0.0 281 250 112.4 80-120
Iron
Lead 0.0 0.0 NC 0-20 0.0 504 500 100.8 80-120
Magnesium
Manganese
Molybdenum
Nickel 1.6 1.5 6.5 0-20 1.6 501 500 99.9 80-120
Potassium
Selenium 0.0 0.0 NC 0-20 0.0 2240 2000 112.0 80-120
Silver 0.0 0.0 NC 0-20 0.0 56.7 50 113.4 80-120
Sodium
Strontium
Thallium 0.0 0.0 NC 0-20 0.0 1900 2000 95.0 80-120
Tin
Titanium
Vanadium
Zinc 4.2 3.9 7.4 0-20 4.2 509 500 101.0 80-120
Associated samples MP28495: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) RPD acceptable due to low duplicate and sample concentrations.
_________________________________________________________________________________________________________
Page 1
37 of 51FA21662
66.2.2
DRAFT
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28495 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15
FA21662-4 Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony 0.0 540 500 108.0 1.7 20
Arsenic 4.1 2230 2000 111.3 1.3 20
Barium
Beryllium 0.0 53.1 50 106.2 0.2 20
Cadmium 0.0 49.4 50 98.8 0.6 20
Calcium
Chromium 1.8 213 200 105.6 0.0 20
Cobalt
Copper 0.0 277 250 110.8 1.4 20
Iron
Lead 0.0 503 500 100.6 0.2 20
Magnesium
Manganese
Molybdenum
Nickel 1.6 499 500 99.5 0.4 20
Potassium
Selenium 0.0 2210 2000 110.5 1.3 20
Silver 0.0 57.0 50 114.0 0.5 20
Sodium
Strontium
Thallium 0.0 1900 2000 95.0 0.0 20
Tin
Titanium
Vanadium
Zinc 4.2 508 500 100.8 0.2 20
Associated samples MP28495: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
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DRAFT
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28495 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15
BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony 511 500 102.2 80-120
Arsenic 2050 2000 102.5 80-120
Barium
Beryllium 53.7 50 107.4 80-120
Cadmium 51.5 50 103.0 80-120
Calcium
Chromium 215 200 107.5 80-120
Cobalt
Copper 267 250 106.8 80-120
Iron
Lead 498 500 99.6 80-120
Magnesium
Manganese
Molybdenum
Nickel 531 500 106.2 80-120
Potassium
Selenium 2040 2000 102.0 80-120
Silver 49.4 50 98.8 80-120
Sodium
Strontium
Thallium 1990 2000 99.5 80-120
Tin
Titanium
Vanadium
Zinc 512 500 102.4 80-120
Associated samples MP28495: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
39 of 51FA21662
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DRAFT
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28495 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15
FA21662-4 QC Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony 0.00 0.00 NC 0-10
Arsenic 4.10 0.00 100.0(a) 0-10
Barium
Beryllium 0.00 0.00 NC 0-10
Cadmium 0.00 0.00 NC 0-10
Calcium
Chromium 1.80 0.00 100.0(a) 0-10
Cobalt
Copper 0.00 0.00 NC 0-10
Iron
Lead 0.00 0.00 NC 0-10
Magnesium
Manganese
Molybdenum
Nickel 1.60 0.00 100.0(a) 0-10
Potassium
Selenium 0.00 0.00 NC 0-10
Silver 0.00 0.00 NC 0-10
Sodium
Strontium
Thallium 0.00 0.00 NC 0-10
Tin
Titanium
Vanadium
Zinc 4.20 0.00 100.0(a) 0-10
Associated samples MP28495: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
40 of 51FA21662
66.2.4
DRAFT
POST DIGESTATE SPIKE SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28495 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/27/15
Sample Final FA21662-4 PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony 9.8 10 115.6 0.2 5 100 115.6 80-120
Arsenic 9.8 10 4.1 4.018 121.4 0.2 5 100 117.4 80-120
Barium
Beryllium 9.8 10 53.9 0.2 2.5 50 107.8 80-120
Cadmium 9.8 10 52.6 0.2 2.5 50 105.2 80-120
Calcium
Chromium 9.8 10 1.8 1.764 57 0.2 2.5 50 110.5 80-120
Cobalt
Copper 9.8 10 116.2 0.2 5 100 116.2 80-120
Iron
Lead 9.8 10 50.7 0.2 2.5 50 101.4 80-120
Magnesium
Manganese
Molybdenum
Nickel 9.8 10 1.6 1.568 106.2 0.2 5 100 104.6 80-120
Potassium
Selenium 9.8 10 113 0.2 5 100 113.0 80-120
Silver 9.8 10 61.2 0.2 2.5 50 122.4*(a 80-120
Sodium
Strontium
Thallium 9.8 10 94.4 0.2 5 100 94.4 80-120
Tin
Titanium
Vanadium
Zinc 9.8 10 4.2 4.116 267.8 0.2 12.5 250 105.5 80-120
Associated samples MP28495: FA21662-1, FA21662-2, FA21662-3, FA21662-4
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested(a) Spike recovery indicates matrix interference and/or outside control limits due to high level in
sample relative to spike amount.
_________________________________________________________________________________________________________
Page 1
41 of 51FA21662
66.2.5
DRAFT
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28507 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15 01/30/15
MB MB Metal RL IDL MDL raw final raw final
Aluminum 200 14 14
Antimony 6.0 1 1
Arsenic 10 1.3 1.3 -0.80 <10 -0.90 <10
Barium 200 1 1
Beryllium 4.0 .2 .2
Cadmium 5.0 .2 .2
Calcium 1000 50 50
Chromium 10 1 1
Cobalt 50 .2 .2
Copper 25 1 1
Iron 300 17 17
Lead 5.0 1 1.1
Magnesium 5000 35 35
Manganese 15 .5 1
Molybdenum 50 .3 .3
Nickel 40 .4 .4
Potassium 10000 200 200
Selenium 10 2.4 2.9
Silver 10 .7 .7
Sodium 10000 500 500
Strontium 10 .5 .5
Thallium 10 1.1 1.4
Tin 50 .9 1
Titanium 10 .5 1
Vanadium 50 .5 .6
Zinc 20 3 4.4
Associated samples MP28507: FA21662-3F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
42 of 51FA21662
66.3.1
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28507 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15 01/30/15
FA21734-1 QC FA21734-1 Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 0.0 0.0 NC 0-20 0.0 2110 2000 105.5 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28507: FA21662-3F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
43 of 51FA21662
66.3.2
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28507 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15
FA21734-1 Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony
Arsenic 0.0 2100 2000 105.0 0.5 20
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28507: FA21662-3F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
44 of 51FA21662
66.3.2
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SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28507 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15
BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 2080 2000 104.0 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28507: FA21662-3F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
45 of 51FA21662
66.3.3
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SERIAL DILUTION RESULTS SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28507 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15
FA21734-1 QC Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic 0.00 0.00 NC 0-10
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron anr
Lead anr
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28507: FA21662-3F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
46 of 51FA21662
66.3.4
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POST DIGESTATE SPIKE SUMMARY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28507 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15
Sample Final FA21734-1 PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic 9.8 10 104.7 0.2 5 100 104.7 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28507: FA21662-3F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
47 of 51FA21662
66.3.5
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Accutest Laboratories
General Chemistry
QC Data Summaries
Includes the following where applicable:
• Method Blank and Blank Spike Summaries• Duplicate Summaries• Matrix Spike Summaries
Southeast
Section 7
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METHOD BLANK AND SPIKE RESULTS SUMMARY GENERAL CHEMISTRY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
MB Spike BSP BSP QC Analyte Batch ID RL Result Units Amount Result %Recov Limits
Nitrogen, Ammonia GP25398/GN64997 0.10 0.0 mg/l 2.5 2.51 100.4 90-110% Nitrogen, Nitrate GP25385/GN64952 0.10 0.0 mg/l 2.5 2.36 94.4 90-110% Nitrogen, Nitrite GP25385/GN64952 0.10 0.0 mg/l 2.5 2.38 95.2 90-110%
Associated Samples: Batch GP25385: FA21662-1, FA21662-2, FA21662-3, FA21662-4Batch GP25398: FA21662-1, FA21662-2, FA21662-3, FA21662-4(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
49 of 51FA21662
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MATRIX SPIKE RESULTS SUMMARY GENERAL CHEMISTRY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Original Spike MS QC Analyte Batch ID Sample Units Result Amount Result %Rec Limits
Nitrogen, Ammonia GP25398/GN64997 FA21603-1 mg/l 0.030 U 2.5 2.4 96.0 90-110% Nitrogen, Nitrate GP25385/GN64952 FA21662-1 mg/l 2.5 U 2.5 3.3 132.0N(a) 90-110% Nitrogen, Nitrite GP25385/GN64952 FA21662-1 mg/l 2.5 U 2.5 3.7 148.0N(a) 90-110%
Associated Samples: Batch GP25385: FA21662-1, FA21662-2, FA21662-3, FA21662-4Batch GP25398: FA21662-1, FA21662-2, FA21662-3, FA21662-4(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(a) Spike recovery indicates possible matrix interference.
__________________________________________________________________________________________________________________________
Page 1
50 of 51FA21662
77.2
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MATRIX SPIKE DUPLICATE RESULTS SUMMARY GENERAL CHEMISTRY
Login Number: FA21662 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Original Spike MSD QC Analyte Batch ID Sample Units Result Amount Result RPD Limit
Nitrogen, Ammonia GP25398/GN64997 FA21603-1 mg/l 0.030 U 2.5 2.4 0.0 20% Nitrogen, Nitrate GP25385/GN64952 FA21662-1 mg/l 2.5 U 2.5 3.1 6.2 20% Nitrogen, Nitrite GP25385/GN64952 FA21662-1 mg/l 2.5 U 2.5 3.2 14.5 20%
Associated Samples: Batch GP25385: FA21662-1, FA21662-2, FA21662-3, FA21662-4Batch GP25398: FA21662-1, FA21662-2, FA21662-3, FA21662-4(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
51 of 51FA21662
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02/02/15
Technical Report for
E Sciences, Inc
Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
7-0002-023
Accutest Job Number: FA21783
Sampling Date: 01/29/15
Report to:
E Sciences, Inc224 SE 9th StFt Lauderdale, FL [email protected]
ATTN: Maria Paituvi
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Andrea Colby 407-425-6700
Norm FarmerTechnical Director
Southeast
02/02/15
e-Hardcopy 2.0Automated Report
18
Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.
1 of 18FA21783
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Table of Contents-1-
Sections:
Section 1: Sample Summary ................................................................................................... 3Section 2: Summary of Hits .................................................................................................... 4Section 3: Sample Results ........................................................................................................ 5
3.1: FA21783-1: MW3-01292015 ....................................................................................... 63.2: FA21783-1F: MW3-01292015 ..................................................................................... 7
Section 4: Misc. Forms ............................................................................................................ 84.1: Chain of Custody ........................................................................................................... 9
Section 5: Metals Analysis - QC Data Summaries ................................................................ 125.1: Prep QC MP28511: As ................................................................................................... 13
12
34
5
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Accutest Laboratories
Sample Summary
E Sciences, IncJob No: FA21783
Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FLProject No: 7-0002-023
Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID
FA21783-1 01/29/15 08:30 TV 01/30/15 AQ Ground Water MW3-01292015
FA21783-1F 01/29/15 08:30 TV 01/30/15 AQ Groundwater Filtered MW3-01292015
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Summary of Hits Page 1 of 1 Job Number: FA21783Account: E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FLCollected: 01/29/15
Lab Sample ID Client Sample ID Result/Analyte Qual PQL MDL Units Method
FA21783-1 MW3-01292015
Arsenic 24.6 10 1.3 ug/l SW846 6010C
FA21783-1F MW3-01292015
Arsenic 25.0 10 1.3 ug/l SW846 6010C
4 of 18FA21783
2
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Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
5 of 18FA21783
3
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: MW3-01292015 Lab Sample ID: FA21783-1 Date Sampled: 01/29/15 Matrix: AQ - Ground Water Date Received: 01/30/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Total Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 24.6 10 1.3 ug/l 1 01/30/15 01/30/15 LM SW846 6010C 1 SW846 3010A 2
(1) Instrument QC Batch: MA12190(2) Prep QC Batch: MP28511
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
6 of 18FA21783
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: MW3-01292015 Lab Sample ID: FA21783-1F Date Sampled: 01/29/15 Matrix: AQ - Groundwater Filtered Date Received: 01/30/15
Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
Dissolved Metals Analysis
Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method
Arsenic 25.0 10 1.3 ug/l 1 01/30/15 01/30/15 LM SW846 6010C 1 SW846 3010A 2
(1) Instrument QC Batch: MA12190(2) Prep QC Batch: MP28511
PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL
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Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
8 of 18FA21783
4
DRAFT
FA21783: Chain of CustodyPage 1 of 3
9 of 18FA21783
44.1
DRAFT
FA21783: Chain of CustodyPage 2 of 3
10 of 18FA21783
44.1
DRAFT
FA21783: Chain of CustodyPage 3 of 3
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44.1
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Accutest Laboratories
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries• Matrix Spike and Duplicate Summaries• Blank Spike and Lab Control Sample Summaries• Serial Dilution Summaries
Southeast
Section 5
12 of 18FA21783
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BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: FA21783 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28511 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15
MB Metal RL IDL MDL raw final
Aluminum 200 14 14
Antimony 6.0 1 1
Arsenic 10 1.3 1.3 -0.70 <10
Barium 200 1 1
Beryllium 4.0 .2 .2
Cadmium 5.0 .2 .2
Calcium 1000 50 50
Chromium 10 1 1
Cobalt 50 .2 .2
Copper 25 1 1
Iron 300 17 17
Lead 5.0 1 1.1
Magnesium 5000 35 35
Manganese 15 .5 1
Molybdenum 50 .3 .3
Nickel 40 .4 .4
Potassium 10000 200 200
Selenium 10 2.4 2.9
Silver 10 .7 .7
Sodium 10000 500 500
Strontium 10 .5 .5
Thallium 10 1.1 1.4
Tin 50 .9 1
Titanium 10 .5 1
Vanadium 50 .5 .6
Zinc 20 3 4.4
Associated samples MP28511: FA21783-1, FA21783-1F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
13 of 18FA21783
55.1.1
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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA21783 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28511 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15 01/30/15
FA21752-5F QC FA21752-5F Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 7.2 6.7 7.2 0-20 7.2 1930 2000 96.1 80-120
Barium
Beryllium anr
Cadmium anr
Calcium
Chromium
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese anr
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium anr
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28511: FA21783-1, FA21783-1F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
14 of 18FA21783
55.1.2
DRAFT
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA21783 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28511 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15
FA21752-5F Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony
Arsenic 7.2 1980 2000 98.6 2.6 20
Barium
Beryllium anr
Cadmium anr
Calcium
Chromium
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese anr
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium anr
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28511: FA21783-1, FA21783-1F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
15 of 18FA21783
55.1.2
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SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA21783 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28511 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15
BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 1940 2000 97.0 80-120
Barium
Beryllium anr
Cadmium anr
Calcium
Chromium
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese anr
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium anr
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28511: FA21783-1, FA21783-1F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
16 of 18FA21783
55.1.3
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SERIAL DILUTION RESULTS SUMMARY
Login Number: FA21783 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28511 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15
FA21752-5F QC Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic 7.20 8.40 16.7 (a) 0-10
Barium
Beryllium anr
Cadmium anr
Calcium
Chromium
Cobalt
Copper anr
Iron anr
Lead anr
Magnesium
Manganese anr
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium anr
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28511: FA21783-1, FA21783-1F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
17 of 18FA21783
55.1.4
DRAFT
POST DIGESTATE SPIKE SUMMARY
Login Number: FA21783 Account: ESFLFL - E Sciences, Inc
Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL
QC Batch ID: MP28511 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l
Prep Date: 01/30/15
Sample Final FA21752-5F PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic 9.8 10 7.2 7.056 108.5 0.2 5 100 101.4 80-120
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP28511: FA21783-1, FA21783-1F
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
18 of 18FA21783
55.1.5
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APPENDIX B
DRAFT
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DRAFT
DRAFT
APPENDIX C
DRAFT
Florida Department of Environmental Protection - Division of Waste Management- Bureau of Petroleum Storage Systems
WELL CONSTRUCTION AND DEVELOPMENT LOG
\\''ELL CONSTRUCTION DATA
wMcr~1 Site~e: FDEP Facility I.D. Number: !Well Ins~Jate(s): ~A.k< Nf L.C'I,. 1/ZJ l.o'5
Well Location and Type (check appropriate boxes): Well Purpose: 0 Perched Monitoring Well Install Method:
~ On-Site D Right-of-Way DSI Shallow (Water-Table) Monitoring DP-r 0 Off-Site Private Property 0 Intermediate or Deep Monitoring 0 Above Grade D Rush-to-Grade 0 Remediation or Other (describe) Surface Casing Install Method: ............................................................................................... If AG, list feet of riser above land surface:
Borehole Depth 1WellDepth ~~orehole Diameter · l~anhole Diameter Well Pad Size:
(feet): ' ') (feet): \5 (inches): 3, 2. ~ (inches): t)' \ feet by _..1_ feet -Riser Diameter and Material: Riser/Screen 0 Rush-Threaded Riser Length: .....l...._ feet
PVt., Connections: ·~
L)" lN(M .. D Other (describe) from 0 feet to .~ feet
Screen Diameter and Material: Screen Slot Size: Screen Length: J.2..._ feet
L~ ti\lct\ .. f~tPAL~ ~-C I C '!r.l\..1:-\ from ...s:_ feet to ~feet 1st Surface Casing Material: 1st Surface Casing I.D. (inches): 1st Surface Casing Length: feet --also check: D Permanent 0Temporary from 0 feet to feet
2nd Surface Casing Material: 2nd Surface Casing I.D. (inches): 2nd Surface Casing Length: feet --also check: D Permanent 0Temporary from 0 feet to feet
3rd Surface Casing Material: 3"' Surface Casing I.D. (inches): 3"' Surface Casing Length: -- feet
also check: D Permanent 0Temporary from 0 feet to feet
Filter Pack Material and Size: Prepacked Filter Around Screen (check one): Filter Pack Length: •o feet
~13c) SAI\l.O [jJ ves 0No from .5_ feet to r-s feet
Filter Pack Seal Material and Filter Pack Seal Length: -!:1..- feet Size: 3'0Jc:/S -~i~\"' 0_ from ' feet to _s__ feet
Surface Seal Material: Surface Seal Length: ~feet
6~oor /PuP-.l~w{) ( C:·M(r~l from 0 feet to \ feet
WELL DEVELOPMENT DATA Well Development Date: Well Development Method (check one): U Surge/Pump ~ Pump D Compressed Air
i {"1..3/"Zv( r:; D Other (describe)
Development Pump Type (check): Iii Centrifugal D Peristaltic Depth to Groundwater (before developing in feet):
0 Submersible 0 Other (describe) ~'-( I Pumping Rate (gallons per minute): I Maximum Drawdown of Groundwater During Well Purged Dry (check one):
0 :r: (.,..ft'\ Development (feet):~ 0 \ Oves ¥J No
Pumping Condition (check one): Total Development Water Development Duration Development Water Drummed
[iJ Continuous D Intermittent Removed (gallons): \o (minutes): ~() (check one): IZJ Yes 0No
Water Appearance (color and odor) At Start of Development: Water Appearance (color and odor) At End of Development:
~J t,\zr rr.- , NCJ 1\, c Lcr::~~r;},_ ( ~~1>\=.,
DRAFT
Florida Department of Environmental Protection- Division of Waste Management- Bureau of Petroleum Storage Systems
WELL CONSTRUCTION AND DEVELOPMENT LOG
WELL CONSTRUCTION DATA
WMtber: SiteNA e: FDEP Facility I.D. Number: 1Well Install Date(s):
,lid- 2 !tt~ \.( ;r"' lt Lv-r VZ1/LDL'( Well Location and Type (check appropriate boxes): Well Purpose: 0 Perched Monitoring Well Install Method:
~ On-Site D Right-of-Way ~ Shallow (Water-Table) Monitoring OPT 0 Off-Site Private Property 0 Intermediate or Deep Monitoring 0 Above Grade D Rush-to-Grade 0 Remediation or other (describe)
Surface Casing Install Method: ............................................................................................... If .\G, list feet of riser above land surfuce:
Borehole Depth IWellDepth ~~orehole Diameter ~~anhole Diameter Well Pad Size:
(feet): 1 ~- (feet): ~~ (inches): ], 2- ~ (inches): 0 ' _L_ feet by I feet
Riser Diameter and Material: Riser/Screen D Flush-Threaded Riser Length: _s_feet
j I ) liiiU\ ~v c.. Connections: D other (describe) . from _a_ feet to ...S::... feet
Screen Diameter and Material: Screen Slot Size: Screen Length: _.Lfeet
l , ~ ::T/\1{.~ ~£-PAl-l-. Q,D\w l NL"' from ~ feet to ..l...( feet
181 Surface Casing Material: 1 '1 Surface Casing I.D. (inches): 1st Surface Casing Length: feet --also check: 0 Permanent 0Temporary from 0 feet to feet
znd Surface Casing Material: zncl Surface Casing l.D. (inches): . znc! surface Casing Length: --feet
also check: D Permanent 0Temporary from 0 feet to feet
3rd Surface Casing Material: 3rd Surface Casing I.D. (inches): 3rd Surface Casing Length: --feet
also check: 0 Permanent 0Temporary from 0 feet to feet
Filter Pack Material and Size: Prepacked Filter Around Screen (check one): Filter Pack Length: &O feet --'?.ofJo 5At.JO [i ves 0No from __t::_ feet to _!..S_ feet
Filter Pack Seal Material and Filter Pack Seal Length: ___j_ feet Size: ~/0.{_ 5f\N~
..... from l feet to 0 feet
Surface Seal Material: Surface Seal Length: _ ?._feet
br>. o:.n J fvr~ ... :t't-Ai'l'O Lf:Mr; 1\JI from G feet to ..L..._ feet
WELL DEVELOPMENT DATA Well Development Date: Well Development Method (check one): U Surge/Pump ljl Pump 0 Compressed Air
·, /t..-:s ; w5 0 other (desaibe)
Development Pump Type (check): ~ Centrifugal D Peristaltic Depth to Groundwater (before developing in feet):
0 Submersible 0 Other (describe) rtb y ' Purnpin~Jite (gallons per minute): ~Maximum Drawdown of Groundwater During Well Purged Dry (check one):
Q, &AU..uN~ Development (feet): :;!J 0' DYes ~ No
Pumpin~ndition (check one): Total Development Water Development Duration Development Water Drummed
~ Continuous 0 Intermittent Removed (gallons): ~ (minutes): \ 4 (check one): fiLves 0No
Water Appearance (color and odor) At Start of Development: Water Appearance7 lor and odor) At End of Development:
'vJ ~~--~"1£ I ~J ~Ji'J n.- (\.-~-An... 'N Cf-.f [ I
DRAFT
Florida Department of Environmental Protection- Division of Waste Management - Bureau of Petroleum Storage Systems
WELL CONSTRUCTION AND DEVELOPMENT LOG
~7: : : :: : : : : ::: ::::: : :: :::: ::7 ::: :: :: :::: ::: :: ::: :: ::: ::: ::: :: ::: : : : :: :: ::: ::: :: : : :: :::~t.t.:~9~~r~v<:r:•P.~:j)~~~::: ::: :: :: : : :: :::: : :: ::: ::::: : ::: :::: : ::: : :::: ::: ::: : :::: ::: ::~ : :: ::: ::JJT?: fifeii' ~~~b~:· ~ tSite ~~~ ~~ . . (. FDEP Facility J.D. Number: I Well Install D~te(s): Mll\i-5 121 )1 ~--,n.~,, oMMurv:nt f.IV7~ ~ '/? 3 jz.oij;
Well Location and Type {check appropriate boxes): Well Purpose: 0 Perched Monitoring Well Install Method:
ltl On-Site 0 Right-of-Way [il Shallow (Water-Table) Monitoring Di>--r 0 Off-Site Private Property · 0 Intermediate or Deep Monitoring 0 Above Grade 0 Rush-to-Grade 0 Remediation or Other (describe) Surface Casing Install Method: w~ooooooooooouooouuooouoooooooooouooooo•onoo ooouuoooooooooooo o o o oo ooOooo ouooo oo ooooooo
If AG, list feet of riser above land surface:
·Borehole Depth !Well Depth I Borehole Diameter ~~anhole Diameter Well Pad Size:
(feet): r .... (feet): n ~ (inches):~,(.~ (inches): 1.:\ _!_feet by ! feet ~
Riser Diameter and Material: Riser/Screen 0 Flush-Threaded Riser Length: -~feet
1/~ D\Jr Connections: 0 Other (describe) from 6 feet to c; feet "1 .tJ.(t-\
Screen Diameter and Material: Screen Slot Size: Screen Length: _!SL feet
1.;- 'If\1(.\1 ~f~f\ t\4.... from ....:L feet to I ( feet
1st Surface Casing Material: 1"1 Surface Casing l.D. (inches): 1"1 Surface Casing Length: feet --also check: 0 Pennanent 0Temporary from 0 feet to feet -2'00 Surface Casing Material: 2nd Surface Casing l.D. (inches): 2JWJ Surface Casing Length: feet --also check: 0Permanent 0Temporary from 0 feet to feet -3nl Surface Casing Material: 3nl Surface Casing I.D. (inches): 3nl Surface Casing Length: - feet
also check: 0 Permanent 0Temporary from 0 feet to feet
Filter Pack Material and Size: Prepacked Filter Around Screen (check one): Filter Pack Length: If.~ feet
'-~l$oS~ . ll9 Yes 0No from _s:_ feet to t. '' feet
Filter Pack Seal Material and Filter Pack Seal Length: ....!::L_ feet
Size: 3D { t,~":. SAr"fD from ~ feet to ~ feet
Surface Seal Material: Surface Seal Length: _ \_feet
i G,.r-cu-r. / PortTI..fte () (f{Y)~N1' . from _Q_ feet to \ feet - - - '
Development Pump Type (check): []. Centrifugal 0 Peristaltic Depth to Groundwater (before developing in feet): d., t.l \ 0 Submersible 0 other (describe) , v \
Pumpin~ ~te (gallons per m!nute): !Maximum Drawdown of Groundwater During Well Purged Dry (check one): ,!"'' ( n.. 1\ ""' '- Development (feet): ,J. " \ 0 Yes 'Cl No .,_) 1 11'1\ I.,UI•./ N U i,fll.J
Development Duration Development Water Drummed Pumpingcondition (check one): Total Development Water
[jJ Continuous 0 Intermittent Removed (gallons): I{) (minutes): LO (check one): f!] Yes 0No
..
Water Appearance (color and odor) At Start of Development: Water Appearance (color and odor) At End of Development:
-~~W~H~~~~~L~~~c-~k~~ -------------~& __ c_~~A-~~/~~~o~~f~~ ------------~ •: :: ;::77::: :;: ;: ;:; :::; :; ::: ;: ;:;:;:;:: :: :: ::: W:Ef.ili :C.ffJ~TRU:CTI0~..£1RUEVELOP~!T::RE~S: ::: ::: :; :: :: :::~::: :: ;::: : :::: :: ::: ::: ::: :: ::;: : :::::
L0d\'~ll~l\,l~ 7._\~1 s1~t.ti.'1' C:>H\i'V\'J~--~,, Ur\l')~fl L:)'1 t vJtS1 .Sa.oc.
·---------------------------------------------------------·------------- ------·----------
DRAFT
Florida Department of Environmental Protection- Division of Waste Management- Bureau of Petroleum Storage Systems
WELL CONSTRUCTION AND DEVELOPMENT LOG
Well Location and Type (check appropriate boxes): Well Purpose: 0 Perched Monitoring Well In~ll Method:
[jJ On-Site 0 Right-of-Way [11 Shallow (Water-Table) Monitoring 0 Off-Site Private Property · 0 Intermediate or Deep Monitoring
0 Above Grade 0 Flush-to-Grade 0 Remediation or Other (describe) Surface Casing Install Method: •••••oooouooonoouuuuooooooouoouooooooouoounoooouuouonouoooooooooouooooooonoooo
·If AG,list feet of riser above land surface:
Borehole Depth rWell Depth !Borehole Diameter !Manhole Diameter
!<inches): :]. 'l"f !Cinches): ~ (feet): ) ') (feet): ( <; Riser Diameter and Material:
I , ) "J.II\Ji..'i_ - pJ L Riser/Screen 0 Flush-Threaded Connections: 0 Other (describe)
Screen Diameter and Material: Screen Slot Size:
\, ~ 'lr'\l<..~~~t. ~ ... ~jlkfd-JJ 111 Surface Casing Material: 1"1 Surface Casing l.D. (inches):
also check: 0 Permanent 0 Temporary
2nd Surface Casing Material: 2nd Surface Casing I.D. (inches):
also check: 0 Permanent 0 Temporary
3rc1 Surface Casing Material: 3nl Surface Casing I.D. (inches):
also check: 0 Permanent 0 Temporary
Filter Pack Material and Size: Prepacked Filter Around Screen (check one):
' '"to /so 5AI'J-D . . l!l ves 0 No
Filter Pack Seal Material and
Size: so;~S' St>~N'b Surface Seal Material:
Well Pad Size:
I feet by ' feet
Riser Length: ....::i._ feet ...;
from _Q__ feet to ~feet
Screen Length: '·~ feet
from ~
111 Surface Casing Length:
from 0
2nd Surface Casing Length:
from 0
3rci Surface Casing Length:
from 0
Filter Pack Length:
from S' Filter Pack Seal Length:
from J
feet to \ ( feet
feet --feet to feet
feet --feet to feet
feet --feet to feet
\~ feet
feet to I 5 feet
....:L feet feet to ~ feet
Surface Seal Length: _ \_ feet
from ___:u_ feet to \ feet I 4 PPLn f Port 1Lt\c~ l f.f\1\fJV 7 ~-~~ ~.. ~ ....... _ i!W ~-~
~----.... --·--·"'""'!'~'!""'":'~'-~~~~~~~~\'!·~''!'~~~'!"·:·~.~-. !'" .. "!"'. !'" .. -.' ~-. ~-.... :-~ ... ·. -. . - . -.. -.-.. .-........ ~·.-. . -.-.. - .. -.-.. -.-. . -.~--. - . -. - . -.. - .. --. _.,_,...__......._....11!1 :::;:;:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::~~~:~E.W.~Q~~:i)~J:'~::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::: ~~;I Development Dat;--,-· wcii~~mmt M;th~d(,check one): D Surge/Pump [jj Pu;p 0 Compressed-Air
. 1/21 /Zo•) 0 Other (describe)
Developnfent Pump Type (check): ftl Centrifugal D Peristaltic Depth to Groundwater (before developing in feet):
0 Submersible 0 Other (describe) ~~ \ Pumpl.nf te (gallons per minute): !Maximum Drawdown of Groundwater During Well Purged Dry (check one):
I - \ ... (). Development (feet): . t;J O Oves rn No
Pumpi~ Condition (check one): Total Development Water Development Duration Development Water Drummed
[ll.Continuous 0 Intermittent Removed (gallons): )6 (minutes): 7._0 (check one): ~ Yes 0No
Water Appearance (color and odor) At Ste,.0,1Development: .
IJ j,_'\'-; ~-'" • -;i~1 G ...... tJ: ,· WH'J-'"'ik../fJor~ Water Appearance (color and odor) At End of Development:
Ct...l AR. /IV or~£ ~o---~
:::: ::: ::; :;: ::::;:::;: :::::::::: ::: :: ::::::::: ;:;: :::W.EL'L~£2eU.cTI~.N:OR:UEVELOP.MENT::REM.AJU{s::::::::::::::::::::;::777:77::::::::;:::
iAxr1lzQr'\l; "1,(6 '1 ~~ R..f.Jt.~l (o!VItV'JLJJ~·l.·N Lf-r.rlf:/'1 Lo·-;, ti1J'-l S"ioP'
DRAFT