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DOI:10.21884/IJMTER.2020.7003.QFYNI 25
PARTIAL REPLACEMENT OF CEMENT BY FLY ASH AND
ADDITION OF PLASTIC WASTE FIBERS IN CONCRETE
Shikha Sapehiya1, Arjun Kumar
1, Kanav Mehta
1, Akshit Mahajan
1
1Department of Civil Engineering, Vaishno College of Engineering, Thapkour (H.P.)
Abstract—A large quantities of waste materials and by-products are generated from
manufacturing processes, service and municipal solid wastes, etc. As a result, solid waste
management has become one of the major environmental concerns in the world. Fly ash and
plastic waste are two very common materials which causes disposal problems in very large
amount. Fly ash (FA) is produced in the process of electricity generation in large quantity and
becomes available as a by-product of coal based power stations. It is fine powder resulting from
the combustion of powered coal, it possesses good pozzolanic property. Plastic waste fibers
(PWF) are wastes from used polythene bags, tins, packets and rubber. This plastic waste leads to
pollute the environment. So it is very important to dispose these wastes without affecting the
environment.
This research addresses the suitability of FA and PWF in concrete as partial replacement of
cement and addition respectively, so as to eliminate the disposal problems of FA and PWF
and also to minimize the cost of concrete structural work.
In this work M20 grade of concrete is used for experimental analysis. The cement is
partially replaced by FA at 0%, 5%, 10%, and 15% by weight. Water cement ratio was kept
0.5 in all concrete mixes. 48 specimens of sizes 150*150*150mm and 300*150mm were made
for testing compressive strength and split tensile strength of the concrete. The strength of
specimens is tested after 7 and 28 days of curing. Results show the more strength of concrete
when replacing cement partially by FA than the ordinary concrete. Results also show that 10%
replacement of cement by FA gives maximum compressive and split tensile strength at 0.5%, 1%
and 1.5% addition of PWF. Also the replacement of cement by FA increases the workability of
concrete.
Keywords— Plastic waste, fly ash waste, pozzolanic, M20 grade, concrete. cement,
compressive, split, tensile.
I. INTRODUCTION
Concrete is the most broadly utilized development material on the planet, more so in the
developing countries, and there are global concerns such as depletion of non-renewable mineral
deposits and emission of the greenhouse gas associate with the fabricate of bond, which is the
essential restricting individual in the concrete. Therefore, the need for conservative and more
natural amicable cementing materials have expanded the enthusiasm for other cementing materials
that can be utilized as halfway or aggregate replacements of the typical Portland cement. Many
endeavors have been made to build the utilization of cement replacing materials in concrete
production because cement production consumes high energy and is responsible for 5% of
global carbon dioxide (CO2) emissions (one ton of cement produces about one ton of carbon
dioxide) and the utilize of cement replacing materials can also improve the act of concrete.
Many trade wastes and byproducts for example, fly ash, blast heater slag, and silica fume and
so forth are used as cement substitute materials in concrete production. Amorphous silicon dioxide
(SiO2) present in such pozzolanic materials leads to the configuration of additional calcium
International Journal of Modern Trends in Engineering and Research (IJMTER) Volume 07, Issue 01, [January– 2020] ISSN (Online):2349–9745; ISSN (Print):2393-8161
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silicate hydrate (CS-H) when it reacts with calcium hydroxide (free lime formed during cement
hydration) and water. This is called secondary gel. This additional CSH, thus formed, increases
the concentration of the matrix and improves the pore structure leading to better toughness
of concrete and mostly of the time results in increase in strength also.
This use of industrial wastes has reduced the dumping land requirements and leads to creation
of wealth from waste.
Similarly agro-industrial wastes such as fly ash have been found to have good pozzolanic
properties. This is due to the occurrence of high SiO2 content in it and its amorphous nature,
which is governed by the burning conditions and usually controls the improvement in strength
and resilience of the end product .
II. METHODOLOGY
Procurement of FA from electricity power plants.
Lab testing of characteristics of FA and WPF such as specific gravity, physical state, odour, aspect ratio etc.
Preparation of design mix of M20 grade using relevant code.
Preparation of different concrete mix using FA as incomplete substitute of cement by 0%,
5%, 10%, 15%.
Addition of WPF beginning 0% to 1.5% by the weight of concrete.
Relative study of compressive and split tensile strength of concrete mix.
III. EXPERIMENTAL PARAMETERS
The experimental program extended in this research work has been carried out in accordance with
Indian Standards laid by Bureau of Indian Standards. All the materials used in this project satisfy
the standards given in their respective codes. Tests performed during this experimental research
are also in accordance with the standards given in IS codes.
[1] Testing:
A. Normal Consistency of Cement
It is the percentage water of cement paste at which of the paste becomes such that the plunger in
a specially designed apparatus (Vicat’s apparatus having plunger with 10 mm diameter and 50
mm length as per IS 5513:1996) penetrates a, depth 5 to 7 mm measured from the bottom of
mould. This test is performed in accordance with IS 4031(Part 4):1988. Take 400 g of cement
and place it in the enameled tray. Mix about 25% water by weight of dry cement thoroughly to
get a cement paste. Total time taken to obtain thoroughly mixed water cement paste i.e.
“Gauging time” should not be less than 3 minutes and not more than 5 minutes. Fill the Vicat’s
mould, resting upon a non-porous base plate, with this cement paste. After filling the mould
completely, smoothen the surface of the paste, making it level with top of the mould with the
help of trowel. Place this whole assembly (i.e. mould + cement paste + base plate) under the
Vicat’s plunger as shown in Fig. 1. Lower the plunger gently so as to touch the surface of the test
block and quickly release the plunger allowing it to sink into the paste. Measure the depth of
penetration and record it. Prepare trial pastes with varying percentages of water content and
follow the above steps until the depth of penetration becomes 33 to 35 mm.
B. Setting time of cement
Initial setting time is required to delay the process of hydration or hardening. It is the time period
between the time water is added to cement and time at which needle having 1 mm2 cross – sectional area fails to penetrate the cement paste, placed in the Vicat’s mould, 5 mm to 7 mm
from the bottom of the mould. Final setting time is the time when the cement paste completely
International Journal of Modern Trends in Engineering and Research (IJMTER) Volume 07, Issue 01, [January– 2020] ISSN (Online):2349–9745; ISSN (Print):2393-8161
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loses its plasticity. It is the time taken for the cement paste or cement concrete to harden
sufficiently and attain the shape of mould in which it is casted. It is the time period between the
time water is added to cement and the time at which needle having 1 mm2 cross-sectional area makes an impression on the paste in the mould but attachment having 5 mm diameter does not
make any impression.
This test is performed as per IS 4031(part 5):1988. According to IS 8112:2013, initial setting
time should not be less than 30 minutes and final setting time should not be more than 600
minutes for OPC 43 cement.
Fig. 1: Vicat’s apparatus for Normal Consistency.
Fig. 2: Vicat’s apparatus for Setting Time.
A neat cement paste with 0.85 P of water by weight of cement is prepared. P is normal
consistency of cement and weight of cement is 400 g. This cement paste is filled in Vicat’s
mould as shown in Fig. 2, resting on a non-porous base plate. This mould is placed under the rod
bearing the needle having cross sectional area of 1 mm2. The needle is gently lowered so that it
completely penetrates the test block. Time is recorded when this needle fails to penetrate the
block for about 5 mm measured from the bottom of the mould. Now needle is replaced with
annular attachment and time is recorded when needle within attachment leaves an impression
while the annular attachment fails to do so.
C. Fineness of cement
It is measured by sieving cement on standard sieve. The proportion of cement of which the grain
sizes are larger than the specified mesh size is thus determined. Fineness of cement has great
effect on the rate of hydration. Finer cement particles offers great heat of hydration and hence
faster development of strength.
This test is performed in accordance with IS 4031(part 1):1996. 100 g of cement sample is
sieved manually on 90 microns sieve as shown in Fig. 3 for 10 to 15 minutes. Weight of cement
retained on 90 micron sieve is recorded and fineness modulus of cement is determined.
D. Specific Gravity of cement
It is generally a ratio of density of cement to that of any known material. Generally
water is used as reference material but in this research, Kerosene oil is used because it does
International Journal of Modern Trends in Engineering and Research (IJMTER) Volume 07, Issue 01, [January– 2020] ISSN (Online):2349–9745; ISSN (Print):2393-8161
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not react with cement whereas water reacts with cement as soon as it came in contact .
Specific gravity of Kerosene oil is 0.79.
This test is performed in accordance with IS 4031(part 11):1988. Le-Chatelier flask as shown
in Fig. 4 of 250 ml capacity is used. 64 g of cement is used. Flask is filled with kerosene oil up to
upper mark (i.e. 1 ml) of graduations below the central bulb. After this 64 g of cement is poured
gently into the flask which results in increased level of Kerosene oil in the flask. The ratio of
weight of cement to displaced volume of kerosene gives the specific gravity of cement.
Fig. 3: 90 microns sieve Fig. 4: Le Chatelier flask
[2] Design Mix
It is the process of selecting suitable ingredients of concrete and determines the relative
proportions with the object of certain minimum strength as economically as possible. The
objective of concrete mix design is to achieve the stipulated minimum strength and to make the
concrete in the most economical manner. Cost wise all concretes depends primarily on two
factors, namely cost of material and cost of labor. Labor cost, by way of formwork, batching,
mixing, transporting and curing is normally same for good concrete. In this research design mix
is carried out for making M20 grade concrete. The process of making M20 concrete follows
the guidelines given in IS 10262:2009. Stipulations for proportioning are minimum water content
equal to 320 Kg/m, maximum water- cement ratio equals to 0.5 and maximum cement content
equals to 450 Kg/m3.
The replacement of fly ash has done with 0%, 5%, 10% and 15% by weight of cement.
The addition of waste plastic fibers by weight of concrete has been done with 0%, 0.5%, 1%,
1.5%.
48 cubes and 48 cylinders were casted and tested after 7 and 28 days for compressive strength and
split tensile strength.
MIX CALCULATIONS
For cubes
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Volume of cube = 150*150*150 = 0.003375m^3
1. Amount of cement= (1*1.57*1440*0.003375)/5.5 = 1.39 kg
2. Amount of sand= (1.5*1.57*1600*0.003375)/5.5 = 2.31 kg
3. Amount of coarse aggregates= (3*1.57*1700*0.003375)/5.5 = 4.91 kg
4. W/C ratio= 0.5
5. Water required = 0.5*1.39 = 0.695 kg
Table 1. Quantities of ingredients in concrete for cubes
FA+WPF CEMENT SAND C.A WATER FA WPF
+0 1.39 2.31 4.91 0.695 0 0
5+0 1.320 2.31 4.91 0.695 0.070 0
10+0 1.251 2.31 4.91 0.695 0.139 0
15+0 1.182 2.31 4.91 0.695 0.208 0
0+0.5 1.39 2.31 4.91 0.695 0 0.047
5+0.5 1.320 2.31 4.91 0.695 0.070 0.047
10+0.5 1.251 2.31 4.91 0.695 0.139 0.047
15+0.5 1.182 2.31 4.91 0.695 0.208 0.047
0+1.0 1.39 2.31 4.91 0.695 0 0.009
5+1.0 1.320 2.31 4.91 0.695 0.070 0.009
10+1.0 1.251 2.31 4.91 0.695 0.139 0.009
15+1.0 1.182 2.31 4.91 0.695 0.208 0.009
0+1.5 1.39 2.31 4.91 0.695 0 0.139
5+1.5 1.320 2.31 4.91 0.695 0.070 0.139
10+1.5 1.251 2.31 4.91 0.695 0.139 0.139
15+1.5 1.182 2.31 4.91 0.695 0.208 0.139
For Cylinders
Volume of cylinder 0f size 150*300 = πr^2h = 3.14*0.075^2*0.3 = 0.0053m^3
1. Amount of cement = (1*1.57*1440*0.0053)/5.5 = 2.179 kg
2. Amount of sand = (1.5*1.57*1600*0.0053)/5.5 = 3.631 kg
3. Amount of coarse aggregates = (3*1.57*1700*0.0053)/5.5 = 7.716 kg
4. W/C ratio = 0.5
5. Amount of water required = = 0.5*2.179 = 1.089 kg
Table 2. Quantities of ingredients in concrete for cylinders
FA+WPF
(kg)
CEMEN
T (kg)
SAND
(kg) C.A (kg)
WATER
(kg) FA (kg)
WPF
(kg)
0+0 2.179 3.631 7.716 1.089 0 0
5+0 2.070 3.631 7.716 1.089 0.109 0
10+0 1.961 3.631 7.716 1.089 0.218 0
15+0 1.852 3.631 7.716 1.089 0.327 0
0+0.5 2.179 3.631 7.716 1.089 0 0.073
5+0.5 2.070 3.631 7.716 1.089 0.109 0.073
10+0.5 1.961 3.631 7.716 1.089 0.218 0.073
15+0.5 1.852 3.631 7.716 1.089 0.327 0.073
0+1.0 2.179 3.631 7.716 1.089 0 0.015
5+1.0 2.070 3.631 7.716 1.089 0.109 0.015
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[3] Testing on fresh and hardened concrete
1. Slump Test
Slump is a measure indicating the consistency or workability of cement concrete. The vertical
subsidence of unsupported fresh concrete, flowing to the sides is known as slump. It gives an idea
of water content needed for concrete to be used for different works. A concrete is said to be
workable if it can be easily mixed, placed, compacted and finished. A workable concrete should
not show any segregation or bleeding. Slump flow test was performed as envisaged by BIS: 1199-
1959.
2. Compressive Strength of concrete
Cube specimens of size 150 mm were cast for compressive strength as per Indian standard
specifications BIS: 516-1959. After casting, all tests specimens were finished with steel trowel.
Immediately after finishing, the specimens were covered with sheets to minimize the
moisture loss from them. Specimens were demoulded after 24-hours and then cured in water at
approximately room temperature till testing. Compressive strength tests for cubes were carried
out at 7 and 28 days. All the specimens were tested in a Compression Testing Machine (CTM)
shown in Fig 6. The compressive strength was then calculated according to the formula
σ = P / A
Where, σ = Compressive Strength (N/mm2 );
P = Maximum load (N);
A = Cross section area of cube (mm2 )
Fig. 5: Slump Test
Fig. 6: Compression Testing Machine
3. Split Tensile Strength Test
10+1.0 1.961 3.631 7.716 1.089 0.218 0.015
15+1.0 1.852 3.631 7.716 1.089 0.327 0.015
0+1.5 2.179 3.631 7.716 1.089 0 0.219
5+1.5 2.070 3.631 7.716 1.089 0.109 0.219
10+1.5 1.961 3.631 7.716 1.089 0.218 0.219
15+1.5 1.852 3.631 7.716 1.089 0.327 0.219
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Split tensile strength test is an indirect method of measuring tensile strength of concrete. It applies
a diametric, compressive force along the length of the cylindrical specimen. Concrete cylinder is
loaded in compression on its side along a diameter plane In CTM as shown in the Fig. 7.
Generally, failure occurs by the splitting of the cylinder along the loading plane.
From theory of induced tensile stress concepts, the following formula is obtained and recommended for the evaluation of the splitting tensile strength, is given by
Ft = 2P/piDL
Where,
Ft = Split tensile strength (MPa) at which the cylinder is split into two or more pieces
P = Ultimate load (N) at which the splitting of cylinder takes place
D= diameter of the cylinder (mm)
L= Length of the cylinder (mm)
This property is useful in estimating the concrete load-carrying capacity in tension, mainly due to
direct compressive forces on it.
Fig. 7: Split Tensile Strength Test
IV. RESULTS AND DISCUSSIONS
A. Normal Consistency of cement
Table 3 and Fig. 8 shows the Normal Consistency values for OPC 43 grade cement and cement
modified with fly ash:
Table 3. Normal Consistency of OPC 43 modified with FA
FA Replacement Level (%) Normal Consistency (%)
0 32
5 31
10 29
15 28
International Journal of Modern Trends in Engineering and Research (IJMTER) Volume 07, Issue 01, [January– 2020] ISSN (Online):2349–9745; ISSN (Print):2393-8161
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Fig. 8: Normal Consistency of OPC 43 modified with FA
B. Setting time of cement
Table 4 and Fig. 9 shows the initial and final setting time of OPC 43 grade cement modified with
waste FA
TABLE 4. Setting times of OPC 43 modified with FA
FA Replacement Level
(%)
Initial Setting Time
(Minutes)
Final Setting Time
(Minutes)
0 102 294
5 114 302
10 119 300
15 130 320
Fig. 9: Setting times of OPC 43 modified with FA
26
27
28
29
30
31
32
33
0 5 10 15
Series2
0
50
100
150
200
250
300
350
0 5 10 15
Initial Setting Time (Minutes)
International Journal of Modern Trends in Engineering and Research (IJMTER) Volume 07, Issue 01, [January – 2020] ISSN (Online):2349–9745; ISSN (Print):2393-8161
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E. Fineness Modulus of cement
When 100 g of cement was sieved manually using 90 microns sieve, 2.3g cement got retained on
sieve. This gives fineness modulus (FM) of cement as 2.3. Following formula is used to determine the
Fineness Module of cement.
Weight retained on 90 microns sieve = 2.3 gms Total weight = 100 gms
Fineness Modulus (F.M) = 2.3
F. Specific gravity of cement
Weight of cement, W = 64 g
Initial reading after kerosene oil is poured, V1 = 1 ml Final reading after 64 g cement is poured,
V2 = 21 ml
Increase in volume = V2 – V1
= 21 – 1
= 20 ml
Specific gravity of cement = W/ (V2 – V1)
= 64/ 20
= 3.2
Thus, specific gravity of cement is 3
G. Slump Test Results
Table 5. Slump Values
FA (%) WPF (%) SLUMP VALUE
0
0 20 0.5 21.3
1.0 21.8
1.5 22
5
0 20
0.5 21
1.0 23
1.5 24
10
0 24.7 0.5 25
1.0 26
1.5 27
15
0 27 0.5 28
1.0 29
1.5 30
International Journal of Modern Trends in Engineering and Research (IJMTER) Volume 07, Issue 01, [January – 2020] ISSN (Online):2349–9745; ISSN (Print):2393-8161
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Fig. 10: Slump Test Results
H. Compressive Strength of Concrete
Compressive strength is the most valuable property of concrete, although in many practical cases
others characteristics, such as durability, impermeability, may in fact be more important. However,
incorporation of FA as partial replacement of cement improves the compressive strength of concrete
for optimum replacement level. For the 4 combinations (0%, 5%, 10%, 15%) of partially replacement
of cement with fly ash and addition of 0.5%, 1%, 1.5% in grade M20 the concrete was casted
and tested for its properties such as Compressive strength and Split Tensile Strength.
Table 6. compressive strength of concrete modified with FA and WPF
0
5
10
15
20
25
30
35
0 5 10 15
WPF(%)
SLUMP VALUE
FA(%)
WPF(%)
COMPRESSIVE STRENGTH(N/mm2)
7 days 28 days
0
0 20 28
0.5 21.3 28.76
1.0 22 30.3
1.5 22.7 32.50
5
0 23 34
0.5 23.5 38.96
1.0 24 39.2
1.5 24.3 40.37
10
0 25 36.34
0.5 25.4 32.38
International Journal of Modern Trends in Engineering and Research (IJMTER) Volume 07, Issue 01, [January – 2020] ISSN (Online):2349–9745; ISSN (Print):2393-8161
@IJMTER-2020, All rights Reserved 35
Fig. 11: Compressive Strength of concrete modified with FA and WPF
Table 6 shows that the strength of concrete improvement up to the 10 % replacement with fly ash
by cement. Compressive strength of the concrete (average of 3 cubes) is relatively higher for (FA
10% : Cement 90 %) compared with concrete having only OPC cement . The higher strength of
replacement could be attributed to the fact that with maximum density, the void content is least
resulting in higher strength. Moreover, with high density, the paste in excess will help in better
compatibility leading to higher strength.
It is well known that the calcium silicate hydrate(C-S-H) gel is the main source of strength of
cement. After addition of FA to the fresh cement, it chemically reacts to the CH to produce
additional C-S-H gel which contributes to improve microscopic property of cement. The production
of more C-S-H gel in concrete with fly ash may improve the concrete properties due to the reaction
among FA and calcium hydroxide in hydrating cement.
1.0 26.2 35.93
1.5 27 43.24
15
0 27.4 40.23
0.5 28 32.66
1.0 28.31 35.70
1.5 29 18.13
0
5
10
15
20
25
30
35
40
45
0 5 10 15
WPF(%)
COMPRESSIVE STRENGTH(N/mm2) 7 days
COMPRESSIVE STRENGTH(N/mm2) 28 days
International Journal of Modern Trends in Engineering and Research (IJMTER) Volume 07, Issue 01, [January – 2020] ISSN (Online):2349–9745; ISSN (Print):2393-8161
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I. Split Tensile Strength of Concrete
Split tensile strength increased with increase in fly ash and addition of waste plastic fibers content
to a certain limit and then decreased with further increase in fly ash content and waste plastic fibers.
At all replacement levels considered in this study, split tensile strength FA and addition of WPF
concrete was more than the respective control mix tensile strength. These results agreed well with the
earlier researches. The increase in strength may be attributed to the pozzolanic reaction and improved
pore structure of concrete. This shows that replacement with fly ash and addition of WPF in concrete
significantly increases split tensile strength in concrete. Small reduction in the split tensile strength
was observed at 15% replacement level as compared to other replacement levels.
Split tensile strength results at 7 days and 28 days are shown in Fig. 12 and Table 7.
Table 7: Split Tensile Strength of concrete modified with FA and WPF
FA
(%)
WPF
(%)
TENSILE
STRENGTH(N/mm2)
7 days 28 days
0
0 1.54 1.90
0.5 1.90 2.00
1.0 2.20 2.90
1.5 2.90 3.20
5
0 2.20 3.00
0.5 2.48 2.90
1.0 2.97 2.83
1.5 2.04 2.83
10
0 1.30 2.20
0.5 1.64 2.97
1.0 2.00 2.90
1.5 2.16 2.83
15
0 1.50 2.50
0.5 1.71 2.35
1.0 2.02 3.85
1.5 2.85 4.90
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Fig. 12: Split Tensile Strength of concrete modified with FA and WPF
V. CONCLUSION
In this work, need and importance of fly ash as cement replacing materials and addition of waste
plastic fibers has been discussed. Based on the literature review, characterization of fly ash was
carried out to find the suitability of fly ash as a pozzolanic material with addition of waste plastic
fibers in M20 mix of concrete. This research work recorded experimental results of test specimens
prepared by using cement partially replaced with FA with alternate percentages of WPF. The
following major conclusions can be drawn from this study:
1. The use of FA as partial replacement of cement and addition of WPF by volume of concrete decreases the normal consistency of cement.
2. The use of FA and WPF has insignificant effects setting times of cement.
3. The use of FA increases the workability of concrete.
4. The use of FA as partial replacement up to 10% increases the compressive strength of concrete.
5. The use of FA as partial replacement up to 10% and addition of 1% of WPF increases the tensile
strength of concrete
Future Scope
1. The strength of concrete replacing fly ash and adding waste plastic fibers can be carried out for
different concrete grades and different water cement ratios. 2. The replacement of fly ash can be increased upto 50% and optimum value can be calculated
which can fulfill every required properties of and hardened concrete.
3. The addition of waste plastic fibers can also be increased and strength properties can be increased
without reducing other required properties of concrete.
4. The temperature effect should also be checked in future study while increasing the percentage of
waste plastic fibers because of catching instant fire property during fire.
0
0.5
1
1.5
2
2.5
3
3.5
4
4.5
5
0 5 10 15
WPF(%)
TENSILE STRENGTH(N/mm2) 7 days
International Journal of Modern Trends in Engineering and Research (IJMTER) Volume 07, Issue 01, [January – 2020] ISSN (Online):2349–9745; ISSN (Print):2393-8161
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